WQ0016376_Monitoring - 03-2020_20210201

0
Sl1BN11:' FURfA LINYr� '.'-AN _,ekor R i)ij! Y
OU 40WATER QUALITY MONITORING:
MPI_IANCE REPORT FORM
Print Clearly or Type
-acility Name: S & J Villari
3ermit Name (if different):
=acilitv.Address: 892 Penny Branch Rd.
Warsaw NC 28398
i a`�3 —
act Person: Gerald Matthews
Location/Site Name: MW-1
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 8
PERMIT Number: Expiration Date:
Non -Discharge WQ0016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
LL ID NUMBER (from Permit): 17568 _ Date sample collected: 3/16/2020
1 Depth: ft. Well Diameter: 2 in.
th to Water Level: 6.8 ft. below measuring point Screened Interval: ft. to _ft.
lsuring Point is ft. above land surface Relative M.P. Elevation: _ ft.
lme of water pumped/bailed before sampling: 100 gallons
iples for metals were collected unfiltered. ®YES ❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES:
pH 4.7 units
Spec. Cond. _
Odor None
Appearance Tan Tint
Temp.
WELL
15.9 °C DRY at
ttMhos time of
!sampling,
late sample analyzed: 3/16/2020
Laboratory Name.
Environmental Chemists,INC Certification No. 94/ DLS 37729
ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
<0.02 mg/I
Pb - Lead mg/I
Coliform MF Fecal
<1 /100ml
Nitrate (NO3) as N
0.11 mg/I
Zn - Zinc mg/I
Coliform: MF Total
<1 /100ml
Phosphorus: Total as P
0.09 mg/I
use Mf'N method toi highly turgid samples,
Orthophosphate
mg/I
Other (Specify Compounds ip entration Units)
Dissolved Solids: Total
57 mg/I
Al -Aluminum
mg/I
pH {when analyzed)
4.7 units
Ba - Barium
mg/I
_
F ,,,,,,,
TOC
<0.5 mg/I
Ca - Calcium
mg/I
Chloride
9 mg/I
Cd - Cadmium
I Vill /I
Arsenic
mg/I
Chromium: Totai
E mg/I
Grease and Oils
mg/I
Cu - Copper
ZU/mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgil
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC , method # 6200 C
Total Ammonia
<0.2 mg/1
Mg - Magnesium
mg/I
method #
(Ammon,a Nitrogen NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mgil
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
re:
�i

SUBMIT FORM ON YFLLQa PAPER ONLY
OUNDWATER QUALITY MONITORING:
MPLIANCOE REPORT FORM
Please Print Clearly or Type
Facility Namo: S & J Villari
Permit Name (if different):
Facility Address: 892 Penny Branch Rd.
Warsaw "` r' NC 28298
act Person: Gerald Matthews
Location/Site Name: MW-2
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 8
L ID NUMBER (from Permit): 17569 Date sample collected: 3/16/202C
Depth: ft. Well Diameter: 2 in.
i to Water Level: 8.8 ft. below measuring point Screened Interval: ft.
luring Point is ft. above land surface Relative M.P. Elevation:
ne of water pumped/bailed before sampling: 10 gallons
PERMIT Number: Expiration Date:
Non -Discharge W00016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
91 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
to _ ft.
ft.
FIELD ANALYSES:
pH 4.6 units
Spec. Cond.
Odor None
Appearance Clear
If WELL
Temp. 15.4 °C DRY at
µMhos time of
sampling,
a sample analyzed: 3/16/2020
Laboratory Name:
Environmental Chemists,INC Certification No. 94/ DLS 37729
;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
<0.02 mg/I
Pb - Lead mg/I
Coliform: MF Fecal
<1 /100ml
Nitrate (NO3) as N
1.72 mg/I
Zn - Zinc mg/I
Coliform: MF Total
<1 /100ml
Phosphorus: Total as P
.94 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
250 mg/I
Al -Aluminum
mg/I
pH (when analyzed)
4.6 units
Ba - Barium
mg/I
TOC
1.4 mg/I
Ca - Calcium
mg/I
Chloride
46 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) W No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6200 C
Total Ammonia
<0.2 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen: NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
re: ❑ I
GIN-59 Rev 1/2007

SUBMIT FORM ON YELLOVI PAPER ONLY
OUNDWATER QUALITY MONITORING:
MPLIANCE REPORT FORM
•u Iry wrno.w r1n1,1 Please Print Clearly or
Facility Name: S & J Villari
Permit Name (if different):
Facllit,; Adaress: 892 Penny Branch Rd.
Warsaw "`` " NC 28398 County Duplin
act Person: Gerald Matthews
Location/Site Name: MW-3
:LL ID NUMBER (from Permit): 17570
It Depth: ft.
)th to Water Level: 6.8 ft. below measuring point
asuring Point is ft. above land surface
ume of water pumped/bailed before sampling:
notes for metals were collected unfiltered: ®YES
Telephone#: [phone]
No. of wells to be sampled: 8
Date sample collected. 3/16/202C
Well Diameter: 2 in.
Screened Interval: ft.
Relative M.P. Elevation:
10 gallons
PERMIT Number: Expiration Date:
Non -Discharge W00016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
❑?C Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
to , ft.
ft.
❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES:
pH 5.9 units
Spec. Cond.
Odor Sulfur
Appearance Clear
Temp.
If WELL
16.3 °C DRY at
µMhos time of
sampling,
sample analyzed: 3/16/2020
Laboratory Name:
Environmental Chemists,INC Certification No. 94/ DLS 37729
;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
<Q.02 mg/I
Pb - Lead mg/I
Coliform. MF Fecal
<1 /100ml
Nitrate (NO3) as N
! <0,02 mg/I
Zn - Zinc mg/I
Coliform: MF Total
<1 /100ml
Phosphorus: Total as P
4.44 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
93 mg/I
At - Aluminum
_mg/I
pH (when analyzed)
5.9 units
Ba - Barium
mg/I
TOC
<0.5 mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
_ mg/I
_
Arsenic
mg/I
Chromium: Total
_.__mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg!I
Fe - Iron
_mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) IR No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6200 C
Total Ammonia
<0.2 mg/i
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. NH3as N:. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Gerald Matthews ORC
Permittee (or Authorized Aqent) Name and
GW-59 Rev. 112007
Title - Please print or type Signatur-e of Parr,itlee (or Authorized Agent) (Date)
Eli
2 �r v

SUBMIT FORM ON YELLOW PAPER ONLY
OUNDWATER QUALITY MONITORING:
MPLIANCE REPORT FORM
ILITY INFORMATION mease runt ueany or t ype
lity Name: S & J Villari
nit Name (if different):
lity Address: 892 Penny Branch Rd.
irsaw " �`' NC 28398 County Duplin
act Person: Gerald Matthews Telephone#: [phone]
Location/Site Name: MW-9 No. of wells to be sampled:
L ID NUMBER (from Permit):
Depth: 19 ft.
h to Water Level: 5.5 ft. below measuring point
luring Point is ft. above land surface
ne of water pumped/bailed before sampling:
R
Date sample collected: 3/16/202C
Well Diameter: 2 in.
Screened Interval: ft.
Relative M.P. Elevation:
10 gallons
to _ ft
ft.
:RMIT Number: Expiration Date:
n-Discharge W00016376 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
❑fC Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL
FIELD ANALYSES:
pH 5.5 units
Spec. Cond. _
Odor Sulfur
Appearance Tan/Brown I here: D
Temp. 15.3 °C DRY at
µMhos time of
sampling,
sample analyzed: 3/16/2020
Laboratory Name:
Environmental Chemists,INC Certification No. 94/ DLS 37729
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/1
Nitrite (NO2) as N
0.08 mg/I
Pb - Lead mg/I
Coliform: MF Fecal
17 /100ml
Nitrate (NO3) as N
0.40 mg/I
Zn - Zinc mg/I
Coliform: MF Total
17 /100ml
Phosphorus: Total as P
1.01 mg/l
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
238 mg/i
Al - Aluminum
mg/I
pH (when analyzed)
5.5 units
Ba - Barium
mg/I
TOC
44.0 mg/I
Ca - Calcium
mg/I
Chloride
63 mg/I
Cd - Cadmium
_mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
_mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6200 C
Total Ammonia
4•2 mg/I
Mg - Magnesium
_mg/I
method #
(Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only --.. •
I certify that, to the best of my knowledge and belief the information submitted in this report is true, k(i
DWQ-certified laboratory, I am aware that there are significant penalties for submitting false information
Gerald
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
mg/L Effluent Total VOCs:
mg/L VOC Removal%
Z
of aermittee (or Authorized Agent) (Date)

SUBMITFORM ON YELLOW PAPER ONLY
OUNDWATER QUALITY MONITORING:
MPLIANCE REPORT FORM
Please Print Clearly or Type
Facility NafTie: S & J Villari
Permit Name (if different):
Facility Address: 892 Penny Branch Rd.
Warsaw NC 28398 County Duplin
ntact Person: Gerald Matthews
III Location/Site Name: MW-5
°LL ID NUMBER (from Permit): 17572
)II Depth: ft.
pth to Water Level: 6.7 ft. below measuring point
!asuring Point is ft. above land surface
lume of water pumped/bailed before sampling:
moles for metals were collected unfiltered: ®YES
Telephone#: [phone]
No. of wells to be sampled:
0
PERMIT Number: Expiration Date:
Non -Discharge W00016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
X1 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
Date sample collected: 3/16/2020
Well Diameter: 2 in.
Screened Interval: -ft. to _ft.
Relative M.P. Elevation: ft.
10 gallons
FIELD ANALYSES:
pH 5.6 units
Spec. Cond,
Odor None
Appearance Tan Tint
sample analyzed: 3/16/2020
Laboratory Name:
Environmental Chemists,INC Certification No. 94/ DLS 37729
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/i
Nitrite (NO2) as N
<0,02 mg/I
Pb - Lead mg/I
Coliform: MF Fecal
4 /100ml
Nitrate (NO3) as N
<0,02 mg/I
Zn - Zinc mg/I
Coliform MF Total
4 /100ml
Phosphorus: Total as P
0.65 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
85 mg/i
Al - Aluminum
mg/I
pH (when analyzed)
5.6 units
Ba - Barium
mg/I
TOC
4.9 mg/I
Ca - Calcium
mg/I
Chloride
8 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/l
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6200 C
Total Ammonia
<0.2 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Si4naluir_ n.
WELL
Temp. 15.4 °C DRY at
µMhos time of
sampling,
N
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
ATER QUALITY MONITORING:
CE REPORT FORM
FACILITY INFORMATION wease Pnnt Clearly or Type
Facility Name: S & J Villari
Permit Name (if different):
Facility Address: 892 Penny Branch Rd.
Warsaw "" NC 28398 County Duplin
act Person: Gerald Matthews
Location/Site Name: MW-6
Telephone#: [phone]
No. of wells to be sampled: 8
PERMIT Number: Expiration Date:
Non -Discharge W00016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
x❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
,AMPLING INFORMATION
If WELL
VELL ID NUMBER (from Permit): 17573
Date sample collected:
3/16/2020
FIELD ANALYSES:
WAS
Veil Depth: ft.
Well Diameter:
2 in.
pH 4.2 units Temp.
15.5 °C
DRY at
lepth to Water Level. 4.6 ft. below measuring point
Screened Interval
ft. to _ft.
Spec. Cond.
µMhos
time of
sampling,
leasuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor Slight Sulfur
check
olume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here: ❑
am les for metals were collected unfiltered: ® YES
❑ NO and field acidified: ❑
YES ❑ NO
ABORATORY INFORMATION
late sample analyzed: 3/16/2020
Laboratory Name Environmental Chemists,INC Certification No.
94/ DLS 37729
ARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
<0.02 mg/I
Pb - Lead
mg/I
Coliform: MF Fecal <1 /100ml
Nitrate (NO3) as N
<0.02 mg/I
Zn - Zinc
mg/I
Coliform MF Total <1 /100mi
Phosphorus: Total as P
0.60 mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total 376 mg/I
Al - Aluminum
—mg/I
pH (when analyzed) 4.2 units
Ba - Barium
mg/I
TOC 0.7 mg/I
Ca - Calcium
mg/I
Chloride 67 mg/I
Cd - Cadmium _
mg/I
Arsenic mg/l
Chromium: Total
—mg/►
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
_mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method # 6200 C
Total Ammonia
<0.02 mg/I
Mg - Magnesium
__—mg/I
method #
(Ammonia Nitrogen, NH3as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs. mg/L VOC Removal%
Gerald Matthews ORC
Permittee (or Authorized Aqent) Name and Title - Please print or type
GVV59 Rev. 1/2007
Signature of Fennittee (or Authorized Aqent)

SUBMIT FORM ON YFi I OW PAPER ONLY
OUNDWATER QUALITY, MONITORING:
MPLIANCE REPORT FORM
FACILITY INFORMATION rtease rnnt cteany or i ype
Facility Name: S & J Vlllari
Permit Name (if different):
Facility Address: 892 Penny Branch Rd.
Warsaw "``e`' NC 28398 _ County Duplin
act Person: Gerald Matthews
Location/Site Name: MW-7
:LL ID NUMBER (from Permit): 17574
II Depth: ft.
)th to Water Level: 4.9 ft. below measuring point
asuring Point is ft. above land surface
ume of water pumped/bailed before sampling:
Telephone#: [phone]
No. of wells to be sampled: 8
Date sample collected: 3/16/202C
Well Diameter: 2 in.
Screened Interval:
Relative M.P. Elevation:
10 gallons
PERMIT Number: Expiration Date:
Non -Discharge W00016376 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
K❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
to �ft.
ft.
FIELD ANALYSES:
pH 5.0 units
Spec. Cond. _
Odor Sulfur
Temp.
WELL
15.4 °C DRY at
µMhos time of
sampling,
Appearance Clear I here: f-1
sample analyzed: 3/16J2020 Laboratory Name: Environmental Chemists, INC Certification No. 94/ DLS 37729
;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
<0,02 mg/I
Coliform MF Fecal
<1 /100ml
Nitrate (NO3) as N
<0,02 mg/I
Coliforrn: MF Total
<1 /100ml
Phosphorus: Total as P
0.48 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
334 mg!l
Al - Aluminum _
mg/I
pH (when analyzed)
5.0 units
Ba - Barium
mg/I
TOC
3.2 mg/I
Ca - Calcium
mg/i
Chloride
64 mg/I
Cd - Cadmium _
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
µMhos
K - Potassium
mg/I
Total Ammonia
1.8 mg/I
Mg - Magnesium
mg/I
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ® No (0)
VOC method # 6200 C
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
of Permittee (or Authorized Agent)
(Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLQ16L PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Clearly or Type
Facility Name: S & J Villari
Permit Name (if different): _
Facility Address: 892 Penny Branch Rd.
Warsaw (`"` " NC 28398 County Duplin
act Person: Gerald Matthews Telephone#: [phone]
Location/Site Name: MW-8 No. of wells to be sampled: 8
-LL ID NUMBER (from Permit): 17575
all Depth: ft.
pth to Water Level: 6.2 ft. below measuring point
asuring Point is ft. above land surface
ume of water ptamped/bailed before sampling:
Date sample collected 3/16/202C
Well Diameter: 2 in.
Screened Interval: ft.
Relative M.P. Elevation:
10 gallons
to _ft.
ft.
:RMIT Number: Expiration Date:
,n-Discharge W00016376 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
© Lagoon ❑ Remediation: Infiltration Gallery
❑?C Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
If WELL
FIELD ANALYSES:
pH 5.0 units
Spec. Cond.
Odor None
Appearance Tan/Turbid I here: ❑
Temp.
15.2 °C DRY at
µMhos time of
sampling,
sample analyzed: 3/16/2020
laboratory Name:
Environmental Chemists,INC Certification No. 94/ DLS 37729
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
0.07 mg/I
Pb - Lead mg/I
Coliform MF Fecal
10 /loom]
Nitrate (NO3) as N
0.56 mg/I
Zn - Zinc mg/I
Coliform: MF Total
10 /100ml
Phosphorus: Total as P
0.96 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
_mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
282 mg;]
Al - Aluminum
_mg/I
pH (when analyzed)
5.0 units
Ba - Barium
mg/I
TOC
5.5 mg/I
Ca - Calcium
mg/I
Chloride
25 mg/I
Cd - Cadmium
_
mg/I
Arsenic
_mg/I
Chromium: Total
—mg/I
Grease and Oils
mg/I
Cu - Copper
__ :ng/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
_mg/I
Fe .. Iror
_-_.mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance
µMhos
K - Potassium
Nmg/I
VOC method # 6200 C
Total Ammonia
<0•2 mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
_mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only •
I certify that, to the best of my knowledge and belief. the information submitted in this report is tnle;`accu
DWQ-certified laboratory. I am aware that there are significant penalties for submitting false inforration
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
mg/L Effluent Total VOCs:
Signaium of
Aqent)
mg/L VOC Removal%
(Date)
a

SM,
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 152.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(,i environmentalchemists.coin
The Pork Company
892 Penny Branch Road
Warsaw NC 28398
Attention:
Date of Report: Apr 03, 2020
Customer PO #:
Customer ID: 08100099
Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-10872 Site: MW - 1
3/16/2020
2:00 PM Water jcb/envirochem
Test
Method
Results
Date Analyzed
Color
Color
Tan Tint
03/16/2020
Depth to water, ft.
Depth to water, Ft
6.8 feet
03/16/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
03/16/2020
Odor
Qualitative
None
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 C
57 mg/L
03/16/2020
Temperature
SM 2550 B
15.9 C
03/16/2020
Chloride
SM 4500 Cl E
9 mg/L
03/23/2020
pH
SM 4500 H B
4.7 units
03/16/2020
Total Phosphorus
SM 4500 P F
0.09 mg/L
03/31/2020
Total Organic Carbon (TOC)
SM 5310 B
<0.5 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF
<1 MPN/100ml
03/16/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/18/2020
Nitrate+Nitrite-Nitrogen
EPA 3532
0.11 mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method
0.11 mg/L
04/03/2020
Report # : 2020-04415 Page 1 of 8

envirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a emiromnentalchemists.com
The Pork Company Date of Report: Apr 03, 2020
892 Penny Branch Road Customer PO #:
Warsaw NC 28398 Customer ID: 08100099
Attention: Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID:
20-10873 Site: MW - 2
Test
Color
Depth to water, ft.
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
Chloride
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
Nitrate+ Nitrite -Nitrogen
Nitrate Nitrogen
Collect Date/Time Matrix
3/16/2020 1:45 PM Water
Method
Color
Depth to Water, Ft.
EPA 350.1
Gallons Bailed before sampling
Qualitative
SM 2540 C
SM 2550 B
SM 4500 CI E
SM 4500 H B
SM 4500 P F
SM 5310 B
SM 9222D MF
EPA 353.2
EPA 353.2
Subtraction Method
Results
Sampled by
jcb/envirochem
Date Analyzed
Clear
03/16/2020
8.8 feet
03/16/2020
< 0.2 mg/L
03/27/2020
10 gallons
03/16/2020
None
03/16/2020
250 mg/L
03/17/2020
15.4 C
03/16/2020
46 mg/L
03/23/2020
4.6 units
03/16/2020
0.94 mg/L
03/31 /2020
1.4 mg/L
03/17/2020
<1 MPN/100ml
03/16/2020
< 0.02 mg/L
03/18/2020
1.72 mg/L
03/30/2020
1.72 mg/L
04/03/2020
Report #: 2020-04415
Panes of R

77
Environmental Chemists,
Inc.
1
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424
Fax
710 Bowsertown Road, Manteo, NC 27954 o 252.473.5702 Lab/Fax
sM.
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843
Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(rr;environmentalchemists.c-oin
The Pork Company
Date of Report: Apr 03, 2020
892 Penny Branch Road
Customer PO #:
Warsaw NC 28398
Customer ID: 08100099
Attention:
Report #: 2020-04415
Project ID: Monitoring Wells
Lab lD Sample ID:
Collect Date/Time Matrix Sampled by
20-10874 Site: MW - 3
3/16/2020 2:15 PM Water jcb/envirochem
Test
Method Results Date Analyzed
Color
Color Clear
03/16/2020
Depth to water, ft.
Depth to water, Ft 6.8 feet
03/16/2020
Ammonia Nitrogen
EPA 350 1 < 0.2 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling 10 gallons
03/16/2020
Odor
Qualitative Sulfur
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 C 93 mg/L
03/17/2020
Temperature
SM 2550 B 16.3 C
03/16/2020
Chloride
SM 4500 Cl E 5 mg/L
03/23/2020
pH
SM 4500 H B 5.9 units
03/16/2020
Total Phosphorus
SM 4500 P F 4.44 mg/L
03/31 /2020
Total Organic Carbon (TOC)
SM 5310 B <0.5 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF <1 MPN/100ml
03/16/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2 < 0.02 mg/L
03/18/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2 < 0.02 mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method <0.02 mg/L
04/03/2020
eport #. 2020-04415
Pana "; of R

Environmental Chemists, Inc.
6602 Windmill Wav, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC: 27954 • 252.473.5,702 Lab/Fax
-IM 255-A Wilmington }-lighwav, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(ii�environmentalchemists.com
The Pork Company Date of Report: Apr 03, 2020
892 Penny Branch Road Customer PO #:
Warsaw NC 28398 Customer ID: 08100099
Attention: Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-10875 Site: MW - 5 3/16/2020 12:45 PM Water jcb/envirochem
Test
Method
Results
Date Analyzed
Color
Color
Tan Tint
03/16/2020
Depth to water, ft.
Depth to water, Ft
6.7 feet
03/16/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
03/16/2020
Odor
Qualitative
None
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 C
85 mg/L
03/17/2020
Temperature
SM 2550 8
15.4 C
03/16/2020
Chloride
SM 4500 Cl E
8 mg/L
03/23/2020
pH
SM 4500 H B
5.6 units
03/16/2020
Total Phosphorus
SM 4500 P F
0.65 mg/L
03/31 /2020
Total Organic Carbon (TOC)
SM 5310 B
4.9 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF
4 MPN/100ml
03/16/2020
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/18/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/03/2020
eport #: 2020-04415
Pane d of A

,,!nvirochem
iswi',
ANALYTICAL $ CONSULTING CHEMISTS
The Pork Company
892 Penny Branch Road
Warsaw NC
Attention:
Lab ID Sample ID:
20-10876 Site: MW - 6
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, N4anteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonaille, NC 28540 • 910.347.5843 Lab/Fax
info(environmentalchemistscom
Date of Report: Apr 03, 2020
Customer PO #:
28398 Customer ID: 08100099
Report #: 2020-04415
Project ID: Monitoring Wells
Color
Depth to water, ft.
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
Chloride
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
Nitrate+Nitrite-Nitrogen
Nitrate Nitrogen
Collect Date/Time Matrix
3/16/2020 1 00 PM Water
Method
Color
Depth to Water, Ft.
EPA 350.1
Gallons Bailed before sampling
Qualitative
SM 2540 C
SM 2550 8
SM 4500 CI E
SM 4500 H B
SM4500PF
SM 5310 B
SM 9222D MF
EPA 353.2
EPA 353.2
Subtraction Method
Results
Sampled by
jcb/envirochem
Date Analyzed
Clear
03/16/2020
4.6 feet
03/16/2020
< 0.2 mg/L
03/27/2020
10 gallons
03/16/2020
Slight Sulfur
03/16/2020
376 mg/L
03/17/2020
15.5 C.
03/16/2020
67 mg/L
03/23/2020
4.2 units
03/16/2020
0.60 mg/L
03/31 /2020
0.7 mg/L
03/17/2020
<1 MPN/100ml
03/16/2020
< 0.02 mg/L
03/18/2020
< 0.02 mg/L
03/30/2020
<0.02 mg/L
04/03/2020
ieport # 2020-04415

ro"l.
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sM
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.3 7 .5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(aienviionmentalchemists.com
The Pork Company
Date of Report: Apr 03, 2020
892 Penny Branch Road
Customer PO #:
Warsaw NC 28398
Customer ID: 08100099
Attention:
Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-10877 Site: MW - 7
3/16/2020 1:15 PM Water jcb/envirochem
Test
Method Results Date Analyzed
Color
Color
Clear
03/16/2020
Depth to water, ft.
Depth to Water, Ft.
4.9 feet
03/16/2020
Ammonia Nitrogen
EPA 350.1
1.8 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
03/16/2020
Odor
Qualitative
Sulfur
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 c
334 mg/L
03/17/2020
Temperature
SM 2550 B
15.4 C
03/16/2020
Chloride
SM 4500 Cl E
64 mg/L
03/25/2020
pH
SM 4500 H B
5.0 units
03/16/2020
Total Phosphorus
SM 4500 P F
0.48 mg/L
04/01 /2020
Total Organic Carbon (TOC)
SM 5310 B
3.2 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF
<1 MPN/100ml
03/16/2020
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/18/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/03/2020
port # 2020-04415
P-R nrR

�sr�i1
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilrnington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info(ti environmentalchemists.com
The Pork Company
892 Penny Branch Road
Warsaw NC 28398
Attention:
Date of Report: Apr 03, 2020
Customer PO #:
Customer ID: 08100099
Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-10878 Site: MW - 8
3/16/2020
1:30 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Tan/Turbid
03/16/2020
Depth to water, ft.
Depth to Water, Ft
6.2 feet
03/16/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
03/16/2020
Odor
Qualitative
None
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 C
282 mg/L
03/17/2020
Temperature
SM 2550 B
15.2 C
03/16/2020
Chloride
SM 4500 Cl E
25 mg/L
03/25/2020
pH
SM 4500 H B
5.0 units
03/16/2020
Total Phosphorus
SM 4500 P F
0.96 mg/L
04/01 /2020
Total Organic Carbon (TOC)
SM 5310 B
5.5 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF
10 MPN/100ml
03/16/2020
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
0.07 mg/L
03/18/2020
Nitrate+ N itrite-N itrogen
EPA353.2
0.63mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method
0.56 mg/L
04/03/2020
port # 2020-04415

r--7 ,
Environmental Chemists,
Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424
Fax
SM)
710 6owsertown Road, Ma,nteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab /Fax
ANALYTICAL & CONSULTING CHEMISTS
info(a;environmentalcheinists.com
The Pork Company
Date of Report: Apr 03, 2020
892 Penny Branch Road
Customer PO #:
Warsaw NC 28398
Customer ID: 08100099
Attention:
Report #: 2020-04415
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-10879 Site: MW - 9
3/16/2020 2:30 PM Water jcb/envirochem
Test
Method Results Date Analyzed
Color
Color Tan/Brown
03/16/2020
Depth to water, ft.
Depth to water, Ft. 5.5 feet
03/16/2020
Ammonia Nitrogen
EPA 3501 4.2 mg/L
03/27/2020
Gallons bailed before sampling
Gallons Bailed before sampling 10 gallons
03/16/2020
Odor
qualitative Sulfur
03/16/2020
Total Dissolved Solids (TDS)
SM 2540 C 238 mg/L
03/17/2020
Temperature
SM 2550 B 15.3 C
03/16/2020
Chloride
SM 4500 Cl E 63 mg/L
03/25/2020
pH
SM 4500 H B
5.5 units
03/16/2020
Total Phosphorus
SM 4500 P F 1.01 mg/L
04/01 /2020
Total Organic Carbon (TOC)
SM 5310 B 44.0 mg/L
03/17/2020
Fecal Coliform
SM 9222D MF 17 MPN/100ml
03/16/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2 0.08 mg/L
03/18/2020
Nitrate+Nitrite-Nitrogen
EPA 353 2 0.48 mg/L
03/30/2020
Nitrate Nitrogen
Subtraction Method 0.40 mg/L
04/03/2020
Comment:
Reviewed by
'port #- 2020-04415

Dale: S /L�r
%notyst r ljr�>
Facility Name: r (
Certification # 94
�+
Permit Is- Gj aJt4
PH
Calibration 'rime
Cal Buffer 4 0 s u.
Cal ButTer 10 0 s u
n 13 -.v
Check Buffer 7.0 s u.
Instrument ID'. N
Comments
`oH check hulTer musr read
­kh + n I . U ­,.r.
.t su buffer Lot#/: Ricca 2901791 Exn I2/20 ' su buffer Lot#/ Ricca 2808744 Exo 7i10 10 su buffer Lot#Ricca 2905A94 Exp 10/20
Sample location
Sample Collection
Time•
Sample Analysis
Time*,.-
pH Result
su
►Post -analysis Buffer
Check value su.
CommentsiData Qualifiers
Arw -r Av • L
/voo /t tirf
/tF+i /3 ✓G
749%,�,
►ost analvsis huller the
Lr 4---A ..,tio....... v...�:_
04
" ---, ___ -....-...e.- ..... ,..." ,wa.1— a.w a —, ....u. i units of me Dutter's true value
411 pYou
es in PH units (i e., s.u.). Record all data to the ne 0 01 s u. and report to ohe nearest 0.1 s.u.
A�w r+. - 9 /Sao//tea /S3i Ny 1/�'
Total Residual CK brine (TRC)
Reference Methnd ant au)n ri_r.,ni t r a.<, up.
--- ---
Post -analysis s
-• ---• •
•• �•�
lease circle
applicable method
Instrument ID:
Dai Check
Standard Result
Check Std.
TSt� check
Sample
Sample
Sample
TRC Result
µg/L or mgfL
when analyzing
Analyzed
Location
Collection
Time
Anal sus
Time
Ng/L or mg/L
Comments/Data Qualifiers
at multiple sites
I
TRC Dailv Check
Standard nw vai..e
,ir _ .
... _rue value µ&' v.... ty...
Check standards must recover within t 10% of the check standard's t
lnnual Calibration Curve Verification Date:
Reagent Blank Value: _(When applicable. Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
Reference Method SM 4500 O G,-201 I Instrument ID
Calibration/ Calibration variable Meter reading • Post -analysis calibration
Verification or % efficiency enfication (when necessary)
Comments
Time after calibration 1
Temperature Bar°memo Theoretical Calculated
Pressure Value rngiL Value m&iL
I I
I.'Ne this row Nhen performing a vrriflcatHin instead of
' _.._ _ calihrvt4w
Sample Collection
Time
'Sample Analysis
rime
DO reading
Comments/DataQualifien
• When performm¢ analases
at mulnnie !nr nnns
rha .,,..:..
r -- ---.. -.._ ��.�, • �•� �• a ��-a. a,vs.s cauDrauon ventication must be performed
ramp e is nwasurCd dvectly �n dic IN
,beam andior omit:;_ unit hrnc .mal•.��1 t ould =.le �ccoidea ci h a ;;ole that ;hCN a L� nc•usuraci tit -atu or nnmediatCly
Temperature f �
Sample
Sample Temperature
cra c �emtw: am .oxi t5-1U10 Instrument ID.
Sample Location
Collection
time
I AnaNsis 1C
I
CommenWData Qualifiers
Tilpe I
�.w • r AtW L
/Yah
. /i t/l
., ,9
t
"f ;amply is measured dirocjk i tic` 1ucan7 n.L.)r .��. - uv'. c'd r&d . A r1ul� lhc, i. \nnual Verification Date I I'_020-..5.u...l �n =iv w nm-fi,ncly
Field Pe nnel %nte:
"W V rv9 /3s-/iw,a /3.i/r ryst
/s, L c/SS,I C
Rev 0712019 1)(N'.QA.Iri1l

En141ronmentai Chemist, Inc., 'Nilmington, .VC Lab #94
-602 Windmill 'Nay
.Vilmington. VC 28405
410.392.0223
Sample Receipt Checklist
)ate:3
4eport Number:
Receipt
of sample: Delivered
L7 YES 'D y0 'PS O �edEx O ❑
0 YES D VO Other
y/A 1. Were custody seals present On the cooler?
�N/A
Off final temperature upon receipt 2' if custody seals were present, were th
'C eY ntact/unbroken?
Haw temperature taken; O Tern Corre[ted temperature upon receipt )c
IR Gun l0: Thomas Traceable S/N 19251165 7ture Blank
against Bottles
C7 YES O y0 R Gun Correction Factor'C: 0.0
3. f temperature of cooler exceeded 6'C, Nas Pro ect M
YES O v0 4. 'Nere proper Gusto I gr /�► notified?
YES ❑ VO dV Procedures (relinquished/recetved) followed?
S• 'Nere sample 10's listed on the COC1
YES O VO 6. Were
samples iO,S listed on Sample
YES O VO 7. Were collection date and time listed on the COC?
YES O VO B. 'titre tests to be
YES O VO oerfared listed on the CCK
YES ? 9. mlid samples arrive in proper containers for each test?
O VO 10. Did samples arrive to
Conditin
YES ' O VO 11. Was adequate sample volume avaoab er?each test?
Sk YES ❑ VO 12. Were samples received within oro
Yor
ES O VO 13. were acid preserved samples receivedhatlalpHng tof time
.requested tests?
YES O NO 14. Were
O rE5 cyanide samples received at a off >12?
O VO 15. Were sulfide samples received at a pH >9T
DES ❑ VO 16, Were NH3
received
0 eES O VO 17. 'Nere Suifi a/Cyan de rhenole eiived ataa cnlot a nne res dualrine al of <0.5 rn
of <0.5 m/P
7OC/Volatdes are off checked at time of analysis and recorded an the benchsheet.
•' 9actena sampieS are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: Must be completed for an sam I
Sample(s) y p e s incorrectly preserved or with h
by adding (uncle one): eadsDace)
-t,50a NO vere received incorrectly preserved and were adiusted accordingly
-+
Time of oreservation: ' 7Cl `IaOH
Note. Not,fy cusrom f more than one ores
er Service mm ervatwe is ^eeded, notate �n
eoNtefy tar ,n�pr,►CtJV oreser•.,ed Sdmprei.�bfain a eew sam COnlmerits b
not1ty the state 'ab d directed t elOw
d analvrld bV �.r,! C�stomlr..Vh 0! Or
Volatiles Sdmolels) 'Mas ^oefed. Aate an
tl Cme•
vere received with head5oace
COMMENTS:

ton
ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910-392-02 3'IFAX9910 92-44245
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info 4environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO: L,)
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
H
n
N
o
E o
m
cL7
o
o a
e
��
o m
t E
"
¢
aw
M-
Z
PRESERVATION
ANALYSIS REQUESTED
a
Time
Temp
z
o
z
o
0
z
=
_z
4
z
4
F
o
Well: f
3 1C
f� '
C
P
���}L
X
TDS, Cl, NO2
G
G
Depth to water:
C
P
X
d
NO3, Total P, NH3
G
G
gallons bailed: / J
C
P
I
I
X
Fecal coliform
G
G
pH (field): V{ 4 }
C
P
X
TOC, (VOC-November only)
G
G
field color: ' ' '
C
P
G
G
field odor: A4-cr
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
I emperature when Heceived:_ )_ -----Accepted:
Delivered By:,S
'_R ted:__ _
Received By. _
Resam ple equ ted:
��
DattURNIAFROUND:
_
Time: ��
Comments

..
ENVIRONMENTAL CHEMISTS, I N C Efndmill 910-3 2-02 3Way'IFAX9ton910-392-4424 5
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info 0environmentalchemists.com
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
?I
F
a
.o
a o m
v
_
c c7
o`
v° a
c
o a
v E
0 w
M
z
PRESERVATION
ANALYSIS REQUESTED
to
Time
Temp
z
i
=
p
o
=
=
z
o
w
o
Well: !
!i -V
I joiX
TDS, Cl, NO2
G
G
Depth to water: t oC
C
P
X
IN03, Total P. NH3
G
G
gallons bailed: / a
C
P
X
Fecal coliform
G
G
pH (field):
C
P
X
TOC, (VOC-November only)
G
G
field color: �luJ
C
P
G
G
field odor: `" `
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
DateMme
Received By:
Date/Time
1.
2.
T_�
I einNerawre wnen neceweo:_ �. __Accepted _____ __ elected:_ Resample R sled: _
Delivered By: <V Received By: Date• 3 '17 Time 3 39
Comments:
TURNAROUND:

Windmill Way
ton,
ENVIRONMENTAL CHEMISTS, INC OFFI E:910-0 2-02231FAX[phone]
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
Analytical & Consulting Chemists
Cnl I FCTION AND CHAIN OF CUSTODY
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONEIFAX:
Permit: W00016376
email:
c.,--l-A ci..• SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a
F
a
E
y
w
n o
E 0
o
ct�
- o
o a
U
o
r E
U
�w
m
a
2
PRESERVATION
ANALYSIS REQUESTED
ate
Time
Temp
w
o
z
u
=
g
m
i
i
=
a
z
p
=
~
w
_
O
Well: 3
Of
CG
f'
X
JTDS,
Cl, NO2
G
G
le
Depth to water: (
C
P
�'
X
k03, Total P, NH3
G
G
gallons bailed: -
C
P
X
Fecal coliform
G
G
pH (field): S- W
C
P
X
ITOC, (VOC November only)
G
G
field color: Gib
C
P
G
G
field odor: A/z/
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Temperature when Received:_-_` - _ - _Accepted:-_-_- ✓ Helected:_
Delivered By:- _-_--- ___ _-- ----_-_-Received By:-4-
Comments:
rtesample Fir
_Date: � Time: 3
TU NAROUND:

•
Analytical 8 Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO: r�
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
n
a
c a
a `o m
m ^
24D
`o
m
c
`o �+
v E
9 w
m
'' z
PRESERVATION
ANALYSIS REQUESTED
e
Time
Tempa
T-69
a
o
x
c
z
o
w
o
Well:
S l
it v
C
P
(
X
TDS, C1, NO2
G
G
Depth to water: ` ,
C
P
X
I
IN03, Total P, NH3
G
G
gallons bailed: j'
C
P
X
Fecal coliform
G
G
H (field):
C
P
X
TOC, VOC-Novemberonl
G
G
field color:
C
P
G
G
field odor:
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
I emperature wnen Hecelvea: 3 � Accepted:
Delivered By: u v 1 Received By:
Comments:
—Time: 3

6602 Windmill Way
ton
C ENVIRONMENTAL CHEMISTS, INOFFICE:91a3 2-02 3'IFAX9910- 2�245
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info® environmentalchemists.com
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO: 2,'
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
cmmnlnrl Rue SAMPLE TYPE: I = influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample identification
Collection
a
m
�,
m
E
_
V a
t E
U
Q
a
J Z
PRESERVATION
ANALYSIS REQUESTED
to
Time
Temp
_
2
�_
$
=
0
2
0
Z
o
f'
=
~O
Well:
S is tN
Jl ��
s t
C
P
�t
X
TDS, CI, NO2
G
G3�
s "
Depth to water: SS
C
P
�'�
X
NO3, Total P, NH3
G
G
gallons bailed: 01
C
P
X
Fecal coliform
G
G
pH (field): y Lt-
C
P
X
I
TOC, (VOC-November only)
G
G
field color: �lev
C
P
G
G
field odor: 4
C
P
F G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer---T
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
J
Temperature when Received:_. _ _ _.-._Accepted:iected: _Resample R ted:
Delivered By: _-- -- ____-_ Y Ls
_ Received B ____ ____ _Date:. `� Time: _
Comments: __. __ TU N OUND• __

Windmill Way
ENVIRONMENTAL CHEMISTS, INC of E:910-n2-0223IFAX 910 2�245
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: The Pork Company -Warsaw
OJECT NAME: Monitoring Wells
REPORT NO: 2.-� `t`{f
ADDRESS:
NTACT NAME: Gerald Matthews, ORC
[REPORT
PO NO:
TO:
PHONE/FAX:
Permit: W00016376
email:
Sampled By: SAMPLE TYPE: 1= Influent. E = Effluent. W = Well. ST = Stream. SO = Soil_ SL = Siudnn_ Othar-
Sample Identification
Collection
K
d
E
�,
s
0
a o m
a
u
ct7
Yo
s
u
c
`o
c=i E
Ow
m m
-a' M
Z
PRESERVATION
ANALYSIS REQUESTED
D to
Time
Temp
c
Z
=
o
N
�,
Z
=
=
e
Z
o
=
''
W
o
Well:
/> •Y
C
P
�k
X
TDS, Cl, NO2
G
G
Depth to water: S
C
P
�'
{
X
IN03, Total P, NH3
G
G
gallons bailed:
C
P
I X
Fecal coliform
G
G
pH(field):
C
P
X
TOC, (VOC-November only)
G
G
field color: j
C
P
field odor: �../1t.�
C
P
G
G
C
P
G
G
C
P
G
G
CP
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
DatedTime
1.
2.
I emperature when Received: 1 — Accepted: R 'ected: Resample R ted:
Delivered By:� Received By: Date:_ /6 _ Time:
Comments: TU N RROUND:

ENVIRONMENTAL CHEMISTS, INC 6602 Windmill:0-3 2-=31FAX [phone]$
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
f_f1I i 9:( Tif)ld Atkin PWAM nt` fal leTnnv
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
SamDled Bv: 3 A gAUPI F TVPG- I - Infl.—f C - =M..en+ W - W-11 CT - ,^ - c. —.— -I--
Sample Identification
Collection
m
E
A
c a
0 a:
o 0
0
c
g
o a
U '"
c
o In
t E
"
o ¢
w
m m
4 M
z
PRESERVATION
ANALYSIS REQUESTED
gate,
Time
Temp
W
c
Z=
U
o
W
Z
x
x
a
z
o
=
''
ffi
x
o
Well:
1 is t.+
1 3
/$ q
C
P
X
TDS, CI, NO2
G
G
Depth to water: } S'
C
P
r
X
P
NO3, Total P, NH3
G
G
gallons bailed:
C
P
I X
Fecal coliform
G
G
H (field): S' '
C
P
X
I
ITOC, (VOC-November only)
G
G
field color:
G
G
field odor: ^"'�
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
Daterrime
1.
2.
Delivered By:Received
Comments:
riesampie ft u tea•
Date: 7a Time:
TUR OUND:

ill Way
ENVIRONMENTAL CHEMISTS, INC o��CE'n91n0392-02231FAx[phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info 0environmentalchemists.com
(_til 1 FCTI(VU AIUr% f%UAM ne r 1 ic-rnnv
Client: The Pork Company -Warsaw
PROJECT NAME: Monitoring Wells
REPORT NO: 1. I - L/i
ADDRESS:
CONTACT NAME: Gerald Matthews, ORC
PO NO:
REPORT TO:
PHONE/FAX:
Permit: W00016376
email:
Sam led 6 - —
V•_ SAIUPI F TYPF• I - inflnenf F-Cal.s..• W _ uu..0 O"r _
Sample Identification
Collection
a
a
a
E
�,
s
m a
Q o 2
E 0
o
cC7
M o
c
.a.
0
��
o
E
U
ow
m m
a�
J 7
z
PRESERVATION
yc, vane.
ANALYSIS REQUESTED
D to
Time
Temp
W
z
O
z
-+
Ct7
0
rA
0
=
_
0
Q
_
o
=
~
w
x
o
Well:
! r'� c
C
P
X
TDS, Cl, NO2
G
G
Depth to water:
C
P
0
X
NO3, Total P, NH3
G
G
allons bailed: l �
C
P
X
Fecal coliform
G
G
pH(field): { 5 q
C
P
X
TOC, (VOC-November only)
G
G
field color:" '� A
C
P
G
G
field odor: Sj
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Total of 8 wells: (1,2,3,5,6,7,8,9) due in March, July, November.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Tomnorntnrn when D__4L
- 1 I
.-I—.c.a • neaample
Delivered By: Received By:
Time:
D-