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HomeMy WebLinkAboutWQ0004972_Monitoring - 11-2020_20210201SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004972 Expiration Date: Facility Name: Forest Lake ELS Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 192 Thousand Trails Drive TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Advance y` NC 27006 County Davie © Spray Field ❑ Remediation: Contact Person: Tracy Overdurf Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 46.00 ft. Well Diameter: 2 in. pH 00400: 6.59 units Temp. 000lo: 17.0 °C DRY at Dept to Water Level 41.99 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 1.25-Dry gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/20-12/05/2020 Laboratory Name: Pace Analytical Certification No. 40,12 & 633 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 <0.30 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 3•7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper o1042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #ACH LAB REPORT.) Sulfate 00945 mg/L Hg -Mercury 71900 ug/L Lab Report Attached , Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. (or Authorized Aoent) Name and Title - Please Ddnt or tvoe of Permittee (or Authorized (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004972 Expiration Date: Facility Name: Forest Lake ELS Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 192 Thousand Trails Drive TYPE OF PERMITTED OPERATION BEING MONITORED Advance ' ""I NC 27006 County Davie ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Tracy Overdurf Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 19.10 ft. Well Diameter: 2 in. pH 00400: 6.55 units Temp. 00010: 16.8 °C DRY at Dept to Water Level 8.60 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: pMhos — time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00095: check Volume of water pumped/bailed before sampling: 2.75-Dry gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/20-12/05/2020 Laboratory Name: Pace Analytical Certification No. 40,12 & 633 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 7.4 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 27.7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method # ACH LAB REPORT.) Sulfate 00945 mg/L Hg -Mercury 71900 ug/L Lab Report Attached? Yes (1) =No (0) Specific Conductance 00095 pMhos K - Potassium 00937 mg/L VOC 76732: method # 8260 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. /3�-rG✓. NC--(i ��z lam- )/q� >-ems1 Permittee (or Authorized Agent) Name and Title - Please Drint or tvoe Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and l copy to: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004972 Expiration Date: Facility Name: Forest Lake ELS Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 192 Thousand Trails Drive TYPE OF PERMITTED OPERATION BEING MONITORED Advance NC 27006 County Davie ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Tracy Overdurf Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 39.00 ft. Well Diameter: 2 in. pH 00400: 6.82 units Temp. 00010: 16.5 °C DRY at Dept to Water Level 34.44 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 1.50-Dry gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/20-12/05/2020 Laboratory Name: Pace Analytical Certification No. 40,12 & 633 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 1.0 /100mL Nitrate (NO3) as N 00620 1.0 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 5•1 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 uglL Fe Iron 01045 ug/L (Specify test and method #. AyTTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? Yes (1) D No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Permittee (or Authorized Aaent) Name and Title - Please print or tvoe Sianature of Permittee (or Authorized -asy� (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY Mail original DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: and 1 copy to: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004972 Expiration Date: Facility Name: Forest Lake ELS Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 192 Thousand Trails Drive TYPE OF PERMITTED OPERATION BEING MONITORED Advance y`'"'I NC 27006 County Davie ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Tracy Overdurf Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 90.00 ft. Well Diameter: 2 in. pH 00400: 6.54 units Temp. 000lo: 17.0 °C DRY at Dept to Water Level 64.61 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 5.00-Dry gallons Appearance here: ❑ Samples for metals were collected unfiltered: El YES El NO and field acidified: El YES El NO LABORATORY INFORMATION Date sample analyzed: 11/20-12/05/2020 Laboratory Name: Pace Analytical Certification No. 40,12 & 633 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg1L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 1.0 /100mL Nitrate (NO3) as N 00620 <0.30 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 3.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 1.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 IX ug/L Lab Report Attached? IJ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWQ-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. i3e-n,^- //L— ( Permittee (or Authorized Agent) Name and Title - Please print or Noe Signature of Permittee Authorized Aaent) (Date) GW-59 Rev.2/2010 aceAnaVical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-1 Lab ID: 92507312001 Collected: 11/19/20 08:39 Received: 11/19/20 12:30 Matrix: Water Parameters HACH 10206 Nitrogen, Nitrate Nitrogen, Nitrate M1310 9222D Fecal Coliform EDN Fecal Coliforms 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chlorcethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dich loroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene tran s-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Date: 12/08/2020 08:00 AM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: HACH 10206 Pace Analytical Services - Eden ND mg/L 0.30 1 11/20/2016:24 14797-55-8 Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden 1.0 CFU/100 mL 1.0 1 11/19/20 13:51 11/20/20 15:24 D6,u1 Analytical Method: EPA8260D Pace Analytical Services - Charlotte ND ug/L 25.0 1 11/23/2015:28 67-64-1 ND ug/L 1.0 1 11/23/2015:28 71-43-2 ND ug/L 1.0 1 11/23/2015:28 108-86-1 ND ug/L 1.0 1 11/23/2015:28 74-97-5 ND ug/L 1.0 1 11/23/2015:28 75-274 ND ug/L 1.0 1 11/23/2015:28 75-25-2 ND ug/L 2.0 1 11/23/2015:28 74-83-9 ND ug/L 5.0 1 11/23/2015:28 78-93-3 ND ug/L 1.0 1 11/23/2015:28 56-23-5 ND ug/L 1.0 1 11/23/2015:28 108-90-7 ND ug/L 1.0 1 11/2312015:28 75-00-3 ND ug/L 5.0 1 11/23/2015:28 67-66-3 ND ug/L 1.0 1 11/23/2015:28 74-87-3 v2 ND ug/L 1.0 1 11/23/2015:28 95-49-8 ND ug/L 1.0 1 11/23/2015:28 106-43-4 ND ug/L 5.0 1 11/23/2015:28 96-12-8 ND ug/L 1.0 1 11/23/2015:28 12448-1 ND ug/L 1.0 1 11/23/2015:28 106-93-4 ND ug/L 1.0 1 11/23/2015:28 74-95-3 ND ug/L 1.0 1 11/23/2015:28 95-50-1 ND ug/L 1.0 1 11/23/2015:28 541-73-1 ND ug/L 1.0 1 11/23/2015:28 106-46-7 ND ug/L 1.0 1 11/23/2015:28 75-71-8 ND ug/L 1.0 1 11/23/2015:28 75-34-3 ND ug/L 1.0 1 11/23/2015:28 107-06-2 ND ug/L 1.0 1 11/23/2015:28 75-35-4 ND ug/L 1.0 1 11/23/2015:28 156-59-2 ND ug/L 1.0 1 11/23/2015:28 156-60-5 ND ug/L 1.0 1 11/23/2015:28 78-87-5 ND ug/L 1.0 1 11/23/2015:28 142-28-9 ND ug/L 1.0 1 11/23/2015:28 594-20-7 ND ug/L 1.0 1 11/23/2015:28 563-58-6 ND ug/L 1.0 1 11/23/2015:28 10061-01-5 ND ug/L 1.0 1 11/23/2015:28 10061-02-6 ND ug/L 1.0 1 11/23/2015:28 108-20-3 ND ug/L 1.0 1 11/23/2015:28 100-41-4 ND ug/L 1.0 1 11/23/2015:28 87-68-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full.. without the written consent of Pace Analytical Services, LLC. Page 4 of 40 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-1 Lab ID: 92507312001 Collected: 11/19/20 08:39 Received: 11/19/20 12:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 82600 MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 2-Hexanone ND ug/L 5.0 1 11/23/20 15:28 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/23/20 15:28 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/23/20 15:28 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/23/20 15:28 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/23/20 15:28 1634-04-4 Naphthalene ND ug/L 1.0 1 11/2312015:28 91-20-3 Styrene ND ug/L 1.0 1 11/23/20 15:28 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/2312015:28 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/23/20 15:28 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/23/20 15:28 127-18-4 Toluene ND ug/L 1.0 1 11/23/20 15:28 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11123/2015:28 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/23/20 15:28 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11123/2015:28 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/23/20 15:28 79-00-5 Trichloroethene ND ug/L 1.0 1 11/23/20 15:28 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/23/20 15:28 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/23/20 15:28 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/23/20 15:28 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/23/20 15:28 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/23/20 15:28 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/23/20 15:28 179601-23-1 o-Xylene ND ug/L 1.0 1 11/23/20 15:28 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 11/23/20 15:28 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 11/23/20 15:28 17060-07-0 Toluene-d8(S) 102 % 70-130 1 11/23/20 15:28 2037-26-5 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 1.5 mg/L 1.0 1 12/02/20 00:30 16887-00-6 5310B TOC Analytical Method: SM 53106-2011 Pace Analytical Services -Asheville Total Organic Carbon 3.3 mg/L 1.0 1 12/05/20 06:00 7440-44-0 Date: 12/08;2020 08:00 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 5 of 40 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-2 Lab ID: 92507312002 Collected: 11/19i20 08:13 Received: 11/19/20 12:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate 1.0 mg/L 0.30 1 11/20/20 16:23 14797-55-8 MB10 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms 1.0 CFU/100 mL 1.0 1 11/19/20 13:51 11/20/20 15:24 ul 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone NO ug/L 25.0 1 11/23/20 15:46 67-64-1 Benzene NO ug/L 1.0 1 11/23/20 15:46 71-43-2 Bromobenzene NO ug/L 1.0 1 11/23/20 15:46 108-86-1 Bromochloromethane NO ug/L 1.0 1 11/23/20 15:46 74-97-5 Bromodichloromethane NO ug/L 1.0 1 11/23/20 15:46 75-27-4 Bromoform NO ug/L 1.0 1 11/23/20 15:46 75-25-2 Bromomethane NO ug/L 2.0 1 11/23/20 15:46 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 11/23/20 15:46 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 11/23/20 15:46 56-23-5 Chlorobenzene NO ug/L 1.0 1 11/23/20 15:46 108-90-7 Chloroethane NO ug/L 1.0 1 11/23/20 15:46 75-00-3 Chloroform NO ug/L 5.0 1 11/23/20 15:46 67-66-3 Chloromethane NO ug/L 1.0 1 11/23/20 15:46 74-87-3 v2 2-Chlorotoluene NO ug/L 1.0 1 11/2312015:46 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 11/23/20 15:46 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 5.0 1 11/23/20 15:46 96-12-8 Dibromochloromethane NO ug/L 1.0 1 11/23/20 15:46 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 1.0 1 11/23/20 15:46 106-93-4 Dibromomethane NO ug/L 1.0 1 11/23/20 15:46 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 11/23/20 15:46 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 11/23/20 15:46 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 11/23/20 15:46 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 11/23/20 15:46 75-71-8 1,1-Dichloroethane NO ug/L 1.0 1 11/2312015:46 75-34-3 1,2-Dichloroethane NO ug/L 1.0 1 11/2312015:46 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 11/23/20 15:46 75-354 cis-1,2-Dichloroethene NO ug/L 1.0 1 11/23/20 15:46 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 11/23/20 15:46 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 11/23/20 15:46 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 11/23/20 15:46 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 11/23/20 15:46 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 11/23/20 15:46 563-58-6 cis-1,3-Dichloropropene NO ug/L 1.0 1 11/23/20 15:46 10061-01-5 trans-1,3-Dichloropropene NO ug/L 1.0 1 11/23/20 15:46 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 11/23/20 15:46 108-20-3 Ethylbenzene NO ug/L 1.0 1 11/2312015:46 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 11/23/20 15:46 87-68-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/08 2020 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 40 aceAnalytical www.pacelahs.com ANALYTICAL RESULTS Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27234 336-996-2841 Sample: MW-2 Parameters Lab ID: 92507312002 Collected: 11/19/20 08:13 Results Units Report Limit DF Received: 11/19/20 12:30 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 2-Hexanone ND ug/L 5.0 1 11/23/20 15:46 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/23/20 15:46 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/23/20 15:46 75-09-2 4-Methyf-2-pentanone (IvIIBK) ND ug/L 5.0 1 11/23/20 15:46 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/23/20 15:46 1634-04-4 Naphthalene ND ug/L 1.0 1 11/23/20 15:46 91-20-3 Styrene ND ug/L 1.0 1 11/23/20 15:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/23/20 15:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/23/20 15:46 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/23/20 15:46 127-18-4 Toluene ND ug/L 1.0 1 11/23/20 15:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/23/20 15:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/23/20 15:46 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/23/20 15:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/23/20 15:46 79-00-5 Trichloroethene ND ug/L 1.0 1 11/23/20 15:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/23/20 15:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/23/20 15:46 96-184 Vinyl acetate ND ug/L 2.0 1 11/23/20 15:46 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/23/20 15:46 75-014 Xylene (Total) ND ug/L 1.0 1 11/23/20 15:46 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/23/20 15:46 179601-23-1 o-Xylene ND ug/L 1.0 1 11/23/20 15:46 9547-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 11/23/20 15:46 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 11/23/20 15:46 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/23/20 15:46 2037-26-5 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville Chloride 5.1 mg/L 1.0 1 12/02/20 00:33 16887-00-6 5310B TOC Analytical Method: SM 531 OB-2011 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 12/05/20 06:52 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Date: 12/0812020 08:00 AM Page 7 of 40 aceAnalj cal www,pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-3 Lab ID: 92507312003 Collected: 11/19/20 07:44 Received: 11/19/20 12:30 Matrix: Water Parameters HACH 10206 Nitrogen, Nitrate Nitrogen, Nitrate MBIO 9222D Fecal Coliform EDN Fecal Coliforms 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1, 1 -Dichloroethane 1,2-Dichloroethane 1, 1 -Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1, 1 -Dichloropropene cis- 1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Date: 12/08,2020 08:00 AM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: HACH 10206 Pace Analytical Services - Eden 7.4 mg/L 0.30 1 11/20/2016:23 14797-55-8 M1 Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden ND CFU/100 mL 1.0 1 11/19/20 13:51 11/20/20 15:24 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 1 11/23/2016:04 67-64-1 ND ug/L 1.0 1 11/23/2016:04 7143-2 ND ug/L 1.0 1 11/23/2016:04 108-86-1 ND ug/L 1.0 1 11/23/2016:04 74-97-5 ND ug/L 1.0 1 11/23/2016:04 75-27-4 ND ug/L 1.0 1 11/23/2016:04 75-25-2 ND ug/L 2.0 1 11/23/2016:04 74-83-9 ND ug/L 5.0 1 11/23/2016:04 78-93-3 ND ug/L 1.0 1 11/23/2016:04 56-23-5 ND ug/L 1.0 1 11/23/2016:04 108-90-7 ND ug/L 1.0 1 11/23/2016:04 75-00-3 ND ug/L 5.0 1 11123/2016:04 67-66-3 ND ug/L 1.0 1 11/23/2016:04 74-87-3 v2 ND ug/L 1.0 1 11/23/2016:04 95-49-8 ND ug/L 1.0 1 11/23/2016:04 10643-4 ND ug/L 5.0 1 11/23/2016:04 96-12-8 ND ug/L 1.0 1 11/23/2016:04 124-48-1 ND ug/L 1.0 1 11/23/2016:04 106-93-4 ND ug/L 1.0 1 11/23/2016:04 74-95-3 ND ug/L 1.0 1 11/23/2016:04 95-50-1 ND ug/L 1.0 1 11/23/2016:04 541-73-1 ND ug/L 1.0 1 11/23/2016:04 106-46-7 ND ug/L 1.0 1 11/23/2016:04 75-71-8 ND ug/L 1.0 1 11/23/2016:04 75-34-3 ND ug/L 1.0 1 11/23/2016:04 107-06-2 ND ug/L 1.0 1 11/23/2016:04 75-35-4 ND ug/L 1.0 1 11/23/2016:04 156-59-2 ND ug/L 1.0 1 11/23/2016:04 156-60-5 ND ug/L 1.0 1 11/23/2016:04 78-87-5 ND ug/L 1.0 1 11/23/2016:04 142-28-9 ND ug/L 1.0 1 11/23/2016:04 594-20-7 ND ug/L 1.0 1 11/23/2016:04 563-58-6 ND ug/L 1.0 1 11/23/2016:04 10061-01-5 ND ug/L 1.0 1 11 /23/20 16:04 10061-02-6 ND ug/L 1.0 1 11/23/2016:04 108-20-3 ND ug/L 1.0 1 11/23/2016:04 100-414 ND ug/L 1.0 1 11123/2016:04 87-68-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 40 aceAnalj tical wNx.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-3 Lab ID: 92507312003 Collected: 11/19/20 07:44 Received: 11/19/20 12:30 Matrix: Water Parameters 8260D MSV Low Level 2-Hexanone p4sopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrach loroethane 1,1,2,2-Tetrach loroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Tdchloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8(S) 4500 Chloride Chloride 5310B TOC Total Organic Carbon Date: 12/08/2020 08:00 AM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 5.0 1 11/23/2016:04 591-78-6 ND ug/L 1.0 1 11/2312016:04 99-87-6 ND ug/L 5.0 1 11/23/2016:04 75-09-2 ND ug/L 5.0 1 11/23/2016:04 108-10-1 ND ug/L 1.0 1 11/23/2016:04 1634-04-4 ND ug/L 1.0 1 11/23/2016:04 91-20-3 ND ug/L 1.0 1 11/23/2016:04 100-42-5 ND ug/L 1.0 1 11/23/2016:04 630-20-6 ND ug/L 1.0 1 11/2312016:04 79-34-5 ND ug/L 1.0 1 11/23/2016:04 127-18-4 ND ug/L 1.0 1 11/23/2016:04 108-88-3 ND ug/L 1.0 1 11/23/2016:04 87-61-6 ND ug/L 1.0 1 11/23/2016:04 120-82-1 ND ug/L 1.0 1 11/23/2016:04 71-55-6 ND ug/L 1.0 1 11/23/2016:04 79-00-5 ND ug/L 1.0 1 11/23/2016:04 79-01-6 ND ug/L 1.0 1 11/2312016:04 75-69-4 ND ug/L 1.0 1 11/23/2016:04 96-18-4 ND ug/L 2.0 1 11/23/2016:04 108-05-4 ND ug/L 1.0 1 11/23/2016:04 75-01-4 ND ug/L 1.0 1 11/23/2016:04 1330-20-7 ND ug/L 2.0 1 11/23/2016:04 179601-23-1 ND ug/L 1.0 1 11/23/2016:04 95-47-6 95 % 70-130 1 11/23/2016:04 460-00-4 95 % 70-130 1 11/23/20 16:04 17060-07-0 102 % 70-130 1 11/2312016:04 2037-26-5 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville 27.7 mg/L 1.0 1 12/02/20 00:34 16887-00-6 Analytical Method: SM 531OB-2011 Pace Analytical Services - Asheville ND mg/L 1.0 1 12/05/20 07:09 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 9 of 40 /�aceAnalyfical� www.pace[abs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-4 Lab ID: 92507312004 Collected: 11/19/20 07:18 Received: 11/19/20 12:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.30 1 11/20/20 16:21 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Eden Fecal Coliforms NO CFU/100 mL 1.0 1 11/19/20 13:51 11/20/20 15:24 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/23/20 16:22 67-64-1 Benzene ND ug/L 1.0 1 11/23/20 16:22 71-43-2 Bromobenzene NO ug/L 1.0 1 11/2312016:22 108-86-1 Bromochloromethane NO ug/L 1.0 1 11/2312016:22 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/23/20 16:22 75-27-4 Bromoform NO ug/L 1.0 1 11123/2016:22 75-25-2 Bromomethane NO ug/L 2.0 1 11/23/20 16:22 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 11/23/20 16:22 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/23/20 16:22 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/23/20 16:22 108-90-7 Chloroethane NO ug/L 1.0 1 11/23/20 16:22 75-00-3 Chloroform NO ug/L 5.0 1 11/23/20 16:22 67-66-3 Chloromethane NO ug/L 1.0 1 11/23/20 16:22 74-87-3 v2 2-Chlorotoluene NO ug/L 1.0 1 11/23/20 16:22 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/2312016:22 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 11/23/20 16:22 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/23/20 16:22 124.48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/23/20 16:22 106-93-4 Dibromomethane ND ug/L 1.0 1 11/23/20 16:22 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 11/23/20 16:22 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 11/23/20 16:22 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 11/23/20 16:22 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 11/23/20 16:22 75-71-8 1, 1 -Dichloroethane ND ug/L 1.0 1 11/23/20 16:22 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/23/20 16:22 107-06-2 1, 1 -Dichloroethene ND ug/L 1.0 1 11/23/20 16:22 75-35-4 cis- 1,2-Dichloroethene ND ug/L 1.0 1 11/23/20 16:22 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 11/23/20 16:22 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 11/23/20 16:22 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 11/23/20 16:22 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/23/20 16:22 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 11/23/20 16:22 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 11/2312016:22 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/23/20 16:22 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 11/23/20 16:22 108-20-3 Ethylbenzene NO ug/L 1.0 1 11/23/20 16:22 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 11/23/20 16:22 87-68-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/0812020 08:00 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 40 laceAnalytical* www.pacelabs.com Project: Groundwater Sampling (Nov) Pace Project No.: 92507312 Sample: MW-1 Parameters 8260D MSV Low Level 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8(S) 4500 Chloride Chloride 53106 TOC Total Organic Carbon Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 ANALYTICAL RESULTS Lab ID: 92507312004 Collected: 11/19/20 07:18 Received: 11/19/20 12:30 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260D Pace Analytical Services - Charlotte NO ug/L 5.0 1 11/23/2016:22 591-78-6 NO ug/L 1.0 1 11/23/2016:22 99-87-6 NO ug/L 5.0 1 11/23/2016:22 75-09-2 NO ug/L 5.0 1 11/23/2016:22 108-10-1 NO ug/L 1.0 1 11/23/2016:22 1634-04-4 NO ug/L 1.0 1 11/23/2016:22 91-20-3 NO ug/L 1.0 1 11/23/2016:22 100-42-5 NO ug/L 1.0 1 11/2312016:22 630-20-6 ND ug/L 1.0 1 11/23/2016:22 79-34-5 NO ug/L 1.0 1 11/23/2016:22 127-18-4 NO ug/L 1.0 1 11/23/2016:22 108-88-3 ND ug/L 1.0 1 11/2312016:22 87-61-6 NO ug/L 1.0 1 11/23/2016:22 120-82-1 NO ug/L 1.0 1 11/23/2016:22 71-55-6 ND ug/L 1.0 1 11/23/2016:22 79-00-5 NO ug/L 1.0 1 11/23/2016:22 79-01-6 NO ug/L 1.0 1 11/23/2016:22 75-69-4 NO ug/L 1.0 1 11/23/2016:22 96-18-4 NO ug/L 2.0 1 11/23/2016:22 108-05-4 NO ug/L 1.0 1 11/23/2016:22 75-01-4 NO ug/L 1.0 1 11/2312016:22 1330-20-7 NO ug/L 2.0 1 11/2312016:22 179601-23-1 NO ug/L 1.0 1 11/23/2016:22 95-47-6 95 % 70-130 1 95 % 70-130 1 102 % 70-130 1 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services - Asheville 3.7 mg/L 1.0 1 Analytical Method: SM 531OB-2011 Pace Analytical Services - Asheville NO mg/L 1.0 1 11/23/2016:22 460-00-4 11 /23/20 16:22 17060-07-0 11/23/2016:22 2037-26-5 12/02/20 00:37 16887-00-6 12/05/20 07:24 7440-44-0 Date: 12/08/2020 08:00 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 40