NCS000295_2021 DMR_20210331

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aceAnalXical
www.pacelabs.com
March 29, 2021
Kiesha Bridges
Jackson Paper Mfg. Co.
152 West Main St.
Sylva, NC 28779
RE: Project: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
Dear Kiesha Bridges:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 16, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Koisha Bridges, Jackson Paper Mfg. Co.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent or Pace Analytical Services, L.L.C.
Page 1 of 21

laceAnalXica(
www.pacelahs.com
Project: 1 st art 21 SW 3116
Pace Project No.: 92528004
Pace Analytical Services Charlotte
9800 Kincey Ave, Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaA/ELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 21

lacmnalyfical"
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
1st Qrt 21 SW 3116
92528004
Analytes
Lab ID
Sample Ill
Method
Analysts
Reported
Laboratory
92628004001
OUTFALL # 1
EPA 1664B
CJM
1
PASI-C
SM 2130B-2011
NFW
1
PASI-A
SM 254OD-2011
ZMC
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92528004002
OUTFALL # 2
EPA 1664E
CJM
1
PASI-C
SM 213OB-2011
NFW
1
PASI-A
SM 2540D-2011
RED
1
PASI-A
SM 522OD-2011
JP1
1
PASI-A
92528004003
OUTFALL # 3
EPA 1664E
CJM
1
PASI-C
SM 213013-2011
NFW
1
PASI-A
SM 2540D-2011
RED
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92528004004
OUTFALL # 4
EPA 1664B
CJM
1
PASI-C
SM 213OB-2011
NFW
1
PASI-A
SM 2540D-2011
RED
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92528004005
CREEK PRE MILL
EPA 1664B
CJM
1
PASI-C
SM 213OB-2011
NFW
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92528004006
CREEK POST MILL
EPA 1664B
CJM
1
PASI-C
SM 213OB-2011
NFW
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C m Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wilhout the written consent of Pace Analytical Services, LLC. Page 3 of 21

(�IacieAnalj&a(
www,pacelab&com
ANALYTICAL RESULTS
Pace Analytical Services, 1-I.0
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
Sample: OUTFALL # 1 Lab ID: 92528004001 Collected: 03/16/21 10:46 Received: 03/16/21 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mglL
5.0 1 03/19/21 13:37
213013 Turbidity
Analytical Method: SM 2130B-2011
Pace Analytical Services -Asheville
Turbidity
18.9 NTU
1.0 1 03/17/2107:00
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
61.0 mglL
8.1 1 03/18/21 12:58
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
44.7 mg1L
25.0 1 03/27/21 01:39 03/27/21 07:06 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC, Page 4 of 21

Pace Analytical Services, LL.0
aceAnalyiicale 2225 Riverside Dr.
Asheville, NC 28804
www.pacelabsxum [phone]
ANALYTICAL RESULTS
Project: 1st Qrt 21 SW 3/16
Pace Project No.: 92528004
Sample: OUTFALL # 2 Lab ID: 92628004002 Collected: 03/16/21 11:00 Received: 03/16/21 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L 5.0 1 03/19/21 13:37
2130B Turbidity
Analytical Method: SM 213OB-2011
Pace Analytical Services -Asheville
Turbidity
17.7 NTU 1.0 1 0311712107:04
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services -Asheville
Total Suspended Solids
26.2 mg/L 5.0 1 03/22/21 18:25
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
26.1 mg1L 25.0 1 03/27/21 01:39 03/27/21 07:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC, Page 5 of 21

laneAnalyfical"
www.pacei1bs.c0m
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
Sample: OUTFALL # 3 Lab ID; 92528004003 Collected: 03/16/21 11:11 Received: 03/16/21 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEiVI, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0 1 03/19/21 13:37
2130B Turbidity
Analytical Method: SM 2134B-2011
Pace Analytical Services -Asheville
Turbidity
269 NTU
1.0 1 03/1712107:04
2540D Total Suspended Solids
Analytical Method: SM 264OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
200 mg/L
50.0 1 03/22/21 18:25
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
163 mg1L
25.0 1 03/27/21 01:39 03/27/21 07:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 21

aceAnalAcal
www.pacolabs,com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: ist Qrt 21 SW 3116
Pace Project No.: 92528004
Sample: OUTFALL # 4 Lab ID: 92528004004 Collected: 03/16/21 11:21 Received: 03116121 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mglL 5.0 1 03/25/21 06:24
2130E Turbidity
Analytical Method: SM 213OB-2011
Pace Analytical Services - Asheville
Turbidity
12.5 NTU 1.0 1 03/17/2107:09
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
26.0 mglL 3A 1 03/22/21 18:26
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mglL 25.0 1 03/27/21 01:39 03/27/21 07:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 21

aceAnalytical
www.pacelab3.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
Sample: CREEK PRE MILL Lab ID: 92628004005 Collected: 03/16/21 12:00 Received: 03/16/21 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L 5.0 1 03/19/21 13:37
2130E Turbidity
Analytical Method: SM 213OB-2011
Pace Analytical Services -Asheville
Turbidity
52.5 NTU 1.0 1 0311712107:07
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
185 mg1L 12.2 1 03/22/21 18:27
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
56.3 mg1L 25.0 1 03/27/21 01:39 03/27/21 07:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

laneAnalXical"
www.pacetaos.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1st Ort 21 SW 3116
Pace Project No.: 92528004
Sample: CREEK POST MILL Lab ID: 92528004006 Collected: 03/16121 12:10 Received: 03/16/21 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 166413
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L
5.0 1 03/19/21 13:37
2130B Turbidity
Analytical Method: SM 213OB-2011
Pace Analytical Services -Asheville
Turbidity
80.7 NTU
1.0 1 03117/2107:10
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
169 mg1L
14.7 1 03/22/21 18:27
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
79.6 mg1L
25.0 1 03/27/21 01:39 03/27/21 07:11
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 21

acmnalytical
www.pecelabs,catn
QUALITY CONTROL DATA
Projecl: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
QC Batch: 607972 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528004001, 92528004002, 92528004003, 92528004005, 92528004006
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3202696
Matrix: Water
Associated Lab Samples: 92528004001,
92528004002, 92528004003, 92528004005, 92528004006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mglL
ND 5.0
03/19/21 13:37
LABORATORY CONTROL SAMPLE:
3202697
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mglL
20 17.6
88 64-132
MATRIX SPIKE SAMPLE: 3202698
35619494001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mglL 5.OU 20 14.8 63 64-132 M1
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC,
Page 10 of 21

laneAnalj&al"
www.pacelabs.com
QUALITY CONTROL DATA
Project: 1 st Qr121 SW 3116
Pace Project No.: 92528004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 609020
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664B
Analysis Description:
1664 SGT-HEM, TPH
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92528004004
METHOD BLANK: 3208029
Matrix: Water
Associated Lab Samples: 92528004004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 5.0 03/25/21 06:24
LABORATORY CONTROL SAMPLE: 3208030
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mglL
20 15.3
76 64-132
MATRIX SPIKE SAMPLE: 3208031
35619192001 Spike
MS MS % Rec
Parameter
Units
Result Cone.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
5.01-1 20
15.0 56 64-132 M1
Results presented on this page are in the units indicated by the" Units" column except where an alternate "nit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. page 11 of 21

aceAnalXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: 1 st Qrt 21 SW 3116
Pace Project No.: 92528004
QC Batch: 607086 Analysis Method: SM 213OB-2011
QC Batch Method: SM 213OB-2011 Analysis Description: 2130E Turbidity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528004001, 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
METHOD BLANK: 3198432 Matrix: Water
Associated Lab Samples: 92528004001, 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU NO 1.0 03117/2106:47
LABORATORY CONTROL SAMPLE: 3198433
Parameter Units
Turbidity NTU
SAMPLE DUPLICATE: 3198434
Parameter Units
Turbidity NTU
SAMPLE DUPLICATE: 3198435
Parameter
Turbidity
Spike LCS
Conc. Result
10 10.3
92527589001 Dup
Result Result
41.6 43.5
92528004006 Dup
Units Result Result
NTU 80.7 80.6
Pace Analytical Services, L.L C
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LCS % Rec
% Rec Limits Qualifiers
103 90-110
RPD Qualifiers
4
RPD Qualifiers
0
Resmts presented on this page arc in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 21

laceAnaljNcal"
www.pacelabs.com
QUALITY CONTROL DATA
Project: 1 st Qrt 21 SW 3l16
Pace Project No.: 92528004
QC Batch: 607592 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528004001
METHOD BLANK: 3200726 Matrix: Water
Associated Lab Samples: 92528004001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 03/18/21 12:47
LABORATORY CONTROL SAMPLE:
3200727
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 3200821
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 3200822
Parameter
Total Suspended Solids
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 242 97 90-110
92527895002 Dup
Result Result RPD Qualifiers
61.0 79.5 16
92527950001 Dup
Units Result Result
mg1L 718 1220
RPD Qualifiers
52 D6
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC, Page 13 of 21

laucteAnalydical
www.pacelibs.com
QUALITY CONTROL DATA
Project: 1st Qrt 21 SW 3/16
Pace Project No.: 92528004
QC Balch: 608175 Analysis Method: SM 254OD-2011
QC Balch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
METHOD BLANK: 3203855 Matrix: Water
Associated Lab Samples: 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 03/22/21 18:23
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 3203856
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 244 97 90-110
SAMPLE DUPLICATE: 3204718
92528436001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 192 204 6
SAMPLE DUPLICATE: 3204719
92528004003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 200 212 6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

aceAnalytical
www.pacelabz.com
QUALITY CONTROL DATA
Project: 1st Qrt 21 SW 3116
Pace Project No.: 92528004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 609734
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528004001
METHOD BLANK: 3211546
Matrix: Water
Associated Lab Samples: 92528004001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
03/27/21 07:03
LABORATORY CONTROL SAMPLE: 3211547
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 759
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211548 3211549
MS MSD
92525439002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg1L ND
100 100 117
122 105 109
90-110 4 R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211550 3211551
MS MSD
92528004001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qua]
Chemical Oxygen Demand mg/L 44.7
100 100 135
152 91 107
90-110 11 R1
Results presented on this page are In the units indicated by the"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

aceAnalyiical
www.pacalabsxola
QUALITY CONTROL DATA
Project: 1 st Qrt 21 SW 3/16
Pace Project No.: 92528004
QC Batch: 609735 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
METHOD BLANK: 3241552 Matrix: Water
Associated Lab Samples: 92528004002, 92528004003, 92528004004, 92528004005, 92528004006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mglL ND 25.0 03/27/21 07:10
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 288o4
[phone]
LABORATORY CONTROL SAMPLE: 3211553
Spike LCS LCS % Rea
Parameter Units Cone, Result % Rea Limits Qualifiers
Chemical Oxygen Demand mglL 750 759 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211554 3211555
MS MSD
92528004002 Spike Spike MS MSD MS MSD % Roc
Parameter Units Result Conc. Cone. Result Result % Rea % Rea Limits RPD Qual
Chemical Oxygen Demand mg1L 26A 100 100 133 133 107 107 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3211556 3211557
MS MSD
92528910001 Spike Spike MS MSD MS MSD % Rea
Parameter Units Result Conc. Conc. Result Result % Rea % Rec Limits RP❑ Qual
Chemical Oxygen Demand mg1L 28.4 100 100 129 131 100 102 90-110 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LC.
Page 16 of 211

aceAnalyfical
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QUALIFIERS
Project: 1st Qrt 21 SW 3/16
Pace Project No.: 92528004
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-AdjustedMethod Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NG 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated fromA7obenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitfile by EPA
Method 8260.
N-Nitrosodiphonylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Ri RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
Phis report shall not be reproduced, except in full,
Date: 03/29/2021 10:26 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

(�IaceAnalytical"
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
1 st Qrt 21 SW 3/16
92528004
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92528004001
OUTFALL #1
EPA 1664B
607972
92528004002
OUTFALL # 2
EPA 1664B
607972
92628004003
OUTFALL # 3
EPA 1664B
607972
92528004004
OUTFALL # 4
EPA 1664B
609020
92528004005
CREEK PRE MILL
EPA 1664B
607972
92528004006
CREEK POST MILL
EPA 1664B
607972
92528004001
OUTFALL # 1
SM 213OB-2011
607086
92528004002
OUTFALL # 2
SM 213OB-2011
607086
92528004003
OUTFALL # 3
SM 213OB-2011
607086
92528004004
OUTFALL # 4
SM 2130B-2011
607086
92529004005
CREEK PRE MILL
SM 213OB-2011
607086
92528004006
CREEK POST MILL,
SM 213OB-2011
607086
92528004001
OUTFALL # 1
SM 2540D-2011
607592
92528004002
OUTFALL # 2
SM 254OD-2011
608175
92528004003
OUTFALL # 3
SM 254OD-2011
608175
92528004004
OUTFALL # 4
SM 254OD-2011
608175
92528004005
CREEK PRE MILL
SM 254OD-2011
608175
92528004006
CREEK POST MILL
SM 254OD-2011
608175
92528004001
OUTFALL # 1
SM 5220D-2011
609734
SM 5220D-2011
609765
92528004002
OUTFALL # 2
SM 5220D-2011
609735
SM 5220D-2011
609766
92528004003
OUTFALL # 3
SM 5220D-2011
609735
SM 5220D-2011
609766
92628004004
OUTFALL # 4
SM 5220D-2011
609735
SM 5220D-2011
609766
92528004005
CREEK PRE MILL
SM 5220D-2011
609735
SM 5220D-2011
609766
92528004006
CREEK POST MILL
SM 5220D-2011
609735
SM 5220D-2011
609766
Date: 03/29/2021 10:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLG.
Page 18 of 21

Document Name: pocument Revised: October 28, 2020
IA
Sample Condition Upon Receipt(SCUR) Page 1 of 2
aceAnalytical Document No.: Issu ing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas quality Office
Laboratory rec lying samples:
Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Client Name: Wo# : 92528004
/� project Wti+
Courier: []Fed Ex ❑UPS ❑U� �Cllent
❑ Commercial ❑Pace ❑Other: l I I l II
82628004
Custody Seal Present? Dyes PNo Seals Intact? ❑yes [ No
Datef Initials Person Examining Contents: r /�
Packing Material: Bubble Wrap .Bubble [lags ❑Norte ❑ Other Biological Tissue F ozen?
Thermometer: ❑Yes ❑No IN/A
P9R Gun 10: ,! ❑wet ❑Eilue []None
? ' �6 i Type of ice:
Correction Factor:
Cooler Temp; Add/Subtract (°C) t) Temp should be above freezing to 6°C
❑Samples aut of temp criteria. samples on ice, cooling process
Cooler Temp Corrected (°C):. if �. �f hasbagun
USDA Regulated Soll { N/A, water sample]
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samp:es originate from a foreign source (internationally,
[]Yes ❑No
IncludingHawau ana r•uenu murr L-i— u••�
Comments/Dlscrepancy:
Chain of Custody Present?
es
❑No
❑N/A
1.
Samples Arrived within Hold Time?
j2fy-.s
[]No
❑N/A
2,
Short Hold Time Analysis (<72 hr.)?
tiles
❑IJo
❑N/A
3,
Rush Turn Around Time Requested?
❑yes
ONo
❑NIA
A.
Sufficient Volume?
Efyes
❑No
❑N/A
5.
Correct Containers Used?
❑No
❑N/A
G.
-Pace Containers Used?
.,--.yes
O r'es
No
❑N/A
Containers Intact?
yes
❑No
©NIA
7.
Dissolved analysis: Samples Field Filtered?
UYes
©No
S1A
a.
Sample Labels Match COC?
yes
[]No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
f1
Headspace in VOA Vials (>S-Gmm)?
❑Yes
❑No
N/A
10.
Trip Blank Present?
❑Yes
ONO
NIA
11.
Trip Blank Custody Seals Present?
Dyes
❑No
0-1,1/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? ❑Yes [—]Nib
Date: �P
Date:
Page 19 of 21

aC2Ana
f
Document Name:
Sample Condition Upon Receipt{SCUR)
Doctmient Revised: October 28, 2020
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.07
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliforin, TOC, Oil and Grease, DRO/8015 {water] DOC, LLHg
**Bottom half of box Is to list number of bottles
Project " ® 9 2528004
nM; CD1 Due Date! 03/3u/21
CLIENT: 93—Jackson P
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adjusted
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added
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Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will Le sent to the North Carolina ULHNR Lertuncauon umte p.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
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Page 21 of 21