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Home My WebLink AboutWQ0009267_Monitoring - 12-2020_20210129GW-59A COMPLIANCE REPORT FORM Permit #_WQ0009267 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. (10/31/2020) Will this monitoring report (GW-59 and GW-59A) be YES NO submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW 3 — p-Isopropyltoluene 24.2 ug/L, Toluene 25.0 ug/L MW 10 — TDS 579 mg/L MW 14 — Total Ammonia Nitrogen 1.96 mg/L Chloromethane: MW-2 (1.90ug/L), MW-3 (18.7ug/L), MW-4 (4.04ug/L), MW-5 (1.76ug/L), MW-7 (0.65ug/L), MW-8 (0.6'2`ug/L), MW-9 (1.60ug/L), MW-11 (1.22ug/L), MW-13 (1.70ug/L), MW-15 (0.93ug/L), MW-16 (0.68ug/L); MW-17 (1.13ug/L) o N 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same YES NO constituent(s) in the same well(s) in the last two years? No for chloromethane. Yes for Total Ammonia Nitrogen, TDS, Toluene and p-Isopropyltoluene. If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and saTmle collection date for each occurrence (for the last two years). MW3—12/2018 p-Isopropyltoluene (13.6 ug/L), Toluene (3.72 ug/L), 12/2019 p-Isopropyltoluene (2.46 ug/L) MW10 — all TDS—12/2018 (661 mg/L), 3/2019 (676.5), 612019 (648 mg/1), 9/2019 (643 mg/L), 12/2019t1868.<P mg/L), 3/2020 (618 mg/L), 612020 (596.5 mg/L), 9/2020 (628 mg/L) r� - MW14—6/2018 (2.Omg/L), 9/2018 (2.04mg/L), 12/2019 (2.02mg/L), 3/2019 (2.31 mg/L) 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Contacted NC DEQ — Wilmington Regional Office on Tuesday, 1/5/2021, to notify them of the presence of VOCs (Chloromethane) in MWs. Contacted Wilmington Regional Office on Friday, 1/8/2021, to notify them of the presence of Toluene and p-Isopropyltoluene in MW3. Env. Program Supervisor II, Tom Tharrington, advised that we resample the wells positive for VOCs. The samples will be sent to two different certified labs. NC DEQ will be updated when results are available. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. MW10 — high background TDS — noted in current permit VOCs — under the guidance of NC DEQ Wilmington Regional Office, we are currently in the process of resampling the wells that had VOCs present. These samples will be split and analyzed by two different certified labs for comparison. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge Z�'L•i1R 1/22/2021 Signature of Permittee(or Authorized Agent) Date ( A\ -59,\ 12 S 2003 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-1 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 16.6 ft. Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000lc 14.2 °C DRY at Depth to Water Level 82546: 4.3 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 1.1 ft. Odor 00085: check Volume of water pumped/bailed before sampling: 5.90 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 136 mg/L Al -Aluminum 01105 mg/L pH (Lab) oo403 4.81 units Ba - Barium 01007 ug/L TOC 00680 12 mg/L Ca - Calcium 00916 mg/L Chloride 00940 47 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 14 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William E. Brown - ORC Permittee (or Authorized Aqent) Name and Title - Please print or type (or (Date) 1 /22/2021 GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge W00009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (state) (21p) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-2 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 17.0 ft. Well Diameter: 2 in. pH 00400: 5.1 units Temp. 000lc 12.7 °C DRY at Depth to Water Level 82546: 4.3 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.4 ft. above land surface Relative M.P. Elevation: 1.9 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 6.10 gallons Appearance here: ❑ Samples for metals were collected unfiltered: X YES El NO and field acidified: X YES El NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 11 /100mL Nitrate (NO3) as N 00620 0.06 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 151.5 mg/L Al -Aluminum ol1o5 mg/L pH (Lab) oo403 5.06 units Ba - Barium 01007 ug/L TOC 00680 8.4 mg/L Ca - Calcium 00916 mg/L Chloride 00940 63 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 6 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance oo095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accura DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, it BrownWilliam E. •- Permittee (or Authorized .• .- GW-59 Rev. 1 •Total• that the laboratory analytical data wa of fines and imprisonment for knowir 0 . s. mg/L VOC Removal% (Date) 1 /22/2021 SUBMIT FORM ON YFI I nW PAPFR nNi Y GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (state) (4) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-3 No. of wells to be sampled: 17 ElWater Source Heat Pump ElOther: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 12/21/2020 FIELD ANALYSES: WAS Well Depth: 17.0 ft. Well Diameter: 2 in. pH 00400: 3.8 units Temp. 000l( 16 oC DRY at Depth to Water Level 82546: 4.1 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 0.9 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 6.19 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/21/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 68.5 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 3.77 units Ba - Barium 01007 ug/L TOC 00680 3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 8 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7870 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. William E. Brown - ORC 1 /22/2021 Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.8/2013 nature of Permittee (or Authorized Aqent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 CountyOnslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-4 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 12/21/2020 FIELD ANALYSES: WAS Well Depth: 16.0 ft. Well Diameter: 2 in. pH 00400: 4.6 units Temp. 000lc 15.4 °C DRY at Depth to Water Level 82546: 3.3 ft. below measuring point Screened Interval: 5.8 ft. to 14 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.68 ft. above land surface Relative M.P. Elevation: 0.62 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 6.10 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/21/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 120.5 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 4.55 units Ba - Barium 01007 ug/L TOC 00680 5.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 40 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 34 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7872 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William E. Brown - ORC Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (state) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-5 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-5 Date sample collected: 12/15/2020 FIELD ANALYSES: WAS Well Depth: 18.1 ft. Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000l( 17 °C DRY at Depth to Water Level 82546: 5.4 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.57 ft. above land surface Relative M.P. Elevation: 2.83 ft. Odor 00065: sampling,check Volume of water pumped/bailed before sampling: 6.10 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/15/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 24 mg/L Al -Aluminum 01105 mg/L pH (Lab) oo403 4.82 units Ba - Barium 01007 ug/L TOC 00680 2.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn -Manganese o1055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations William E. Brown - ORC 1 /22/2021 Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • OF ENVIRONMENT 8� NATURAL RESOURCES ffDEPARTMENT VISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 17 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) ❑ Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-6 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-6 Date sample collected: 12/21/2020 FIELD ANALYSES: WAS Well Depth: 16.8 ft. Well Diameter: 2 in. pH 00400: 5.5 units Temp. 000lc 15.8 °C DRY at Depth to Water Level 82546: 3 ft. below measuring point Screened Interval: 3.5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.65 ft. above land surface Relative M.P. Elevation: 0.35 ft. Odor 000ss: sampling,check Volume of water pumped/bailed before sampling: 6.62 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/21/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.1 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 223.5 mg/L Al - Aluminum 01105 mg/L pH (Lab) oo4m 5.53 units Ba - Barium 01007 ug/L TOC 00680 7.9 mg/L Ca - Calcium 00916 mg/L Chloride 00940 26 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 31 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Nermlttee (or Autnonzea Aqent) Name and I itle GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONI Y GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 CountyOnslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-7 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7 Date sample collected: 12/21/2020 FIELD ANALYSES: WAS Well Depth: 15.0 ft. Well Diameter: 2 in. pH 00400: 3.9 units Temp. 000lc 15.9 °C DRY at Depth to Water Level 82546: 3 ft. below measuring point Screened Interval: 2.5 ft. to 13 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 0 ft. Odor 00085: sampling, check Volume of water pumped/bailed before sampling: 5.76 gallons Appearance here. - Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/21/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2.94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 147.5 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 3.87 units Ba - Barium 01007 ug/L TOC 00680 7.6 mg/L Ca - Calcium oo91s mg/L Chloride 00940 57 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 47 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 [Mhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William E. Brown - ORC Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee (or Authorized Aqent) (Date) H�d��:Z�:7PZ•716? SUBMIT FORM ON YELLOW PAPFR ONI Y GROUNDWATER QUALITY MONITORING: • . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES COMPLIANCE REPORT FORM • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (Zip) X Spray Field ❑Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-8 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8 Date sample collected: 12/17/2020 FIELD ANALYSES: WAS Well Depth: 12.1 ft. Well Diameter: 2 in. pH 00400: 3.5 units Temp. 000lc 16 °C DRY at Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 3 ft. to 9 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 2.2 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 3.31 gallons Appearance here: ❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/17/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 297 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 3.46 units Ba - Barium 01007 ug/L TOC 00680 4.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 166 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. William E. Brown - ORC 1 /22/2021 Permittee (or Authorized Aqent) Name and Title - Please print or tvoe GW-59 Rev.8/2013 (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow El Lagoon El Remediation: Infiltration Gallery (City) (state) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-9 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 12/17/2020 FIELD ANALYSES: WAS Well Depth: 14.0 ft. Well Diameter: 2 in. pH 00400: 3.6 units Temp. 000l( 16.7 °C DRY at Depth to Water Level 82546: 4.9 ft. below measuring point Screened Interval: 7 ft. to 11 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.55 ft. above land surface Relative M.P. Elevation: 2.35 ft. Odor 00085: sampling, check Volume of water pumped/bailed before sampling: 4.37 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/17/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 228 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 3.56 units Ba - Barium 01007 ug/L TOC 00680 3.9 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 91 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William E. Brown - ORC Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 JULiMI I t-UKM UN TtLLUVV F'AI'IzK ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: City of Jacksonville Land Treatment System Permit Name (if different): Facility Address: 716 Firetower Road Jacksonville NC 28540 County Onslow (City) (State) (zip) Contact Person: Amy Palaschak Telephone#: (910)938-3620 Well Location/Site Name MW-10 No. of wells to be sampled: 17 WELL ID NUMBER (from Permit): MW-10 Date sample collected: Well Depth: 30.1 ft. Well Diameter: Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: Measuring Point is 2.9 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 11.66 gallons 12/17/2020 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: Expiration Date: 4/30/2022 Non -Discharge WQ0009267 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: 2 in. 17 ft. to 27 ft. 2.9 ft. Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO FIELD ANALYSES: pH 00400: 6.4 units Spec. Cond. 00094: Odor 00085: Appearance Temp. 000l( 17.5 °C uMhos Date sample analyzed: 12/17/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 1.64 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 579 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.41 units Ba - Barium 01007 ug/L TOC 00680 2.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 18 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 151 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7872 method # SM 6200C Total Ammonia 00610 0.11 mg/L Mg- Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% DRY at time of sampling, check here:❑ William E. Brown - ORC e. 1/22/2021 Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee (or Authorized Agent) (Date) GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC NPDES Other Permit Name (if different): Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-11 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 22.2 ft. Well Diameter: 2 in. pH 00400: 4.4 units Temp. 000lc 14.7 °C DRY at Depth to Water Level 82546: 6 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µMhos time of sampling,check Measuring Point is 2.25 ft. above land surface Relative M.P. Elevation: 3.75 ft. Odor 00085: Volume of water pumped/bailed before sampling: 7.78 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.42 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 38 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 4.35 units Ba - Barium 01007 ug/L TOC 00680 1.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg -Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee (or Authorized Aqent) (Date) GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY IGROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: City of Jacksonville Land Treatment System Permit Name (if different): Facility Address: 716 Firetower Road Jacksonville NC 28540 County Onslow (State) (Zip) Contact Person: Amy Palaschak Telephone#: (910)938-3620 Well Location/Site Name MW-12 No. of wells to be sampled: 17 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: Expiration Date: 4/30/2022 Non -Discharge WQ0009267 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: 5AMPLING INFURMATIDN If WELL WELL ID NUMBER (from Permit): MW-12 Date sample collected: 12/21/2020 FIELD ANALYSES: WAS Well Depth: 18.3 ft. Well Diameter: 2 in. pH 00400: 5.3 units Temp. 000lc 17.5 °C DRY at Depth to Water Level 82546: 4.3 ft. below measuring p g point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 000sa: µMhos time of Measuring Point is 3.04 ft. above land surface Relative M.P. Elevation: 1.26 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 6.72 gallons Appearance here: ❑ Samples for metals were collected unfiltered: X YES El NO and field acidified: X YES El NO Date sample analyzed: 12/21/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 115 mg/L Al -Aluminum oilo5 mg/L pH (Lab) 00403 5.3 units Ba - Barium 01007 ug/L TOC 00680 24.9 mg/L Ca - Calcium 00916 mg/L Chloride 00940 8 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 9 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES EN DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-13 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13 Date sample collected: 12/17/2020 FIELD ANALYSES: WAS Well Depth: 23.2 ft. Well Diameter: 2 in. pH 00400: 4.5 units Temp. 000l( 17.1 °C DRY at Depth to Water Level 82546: 14 ft. below measuring p g point Screened Interval: 10.5 ft. to 23.2 ft. Spec. Cond. 000sa: µMhos time of sampling,check Measuring Point is 2.75 ft. above land surface Relative M.P. Elevation: 11.55 ft. Odor 00085: Volume of water pumped/bailed before sampling: 4.27 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/17/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 68 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 4.49 units Ba - Barium 01007 ug/L TOC 00680 4.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 24 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 0.4 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge W00009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-14 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14 Date sample collected: 12/17/2020 FIELD ANALYSES: WAS Well Depth: 17.9 ft. Well Diameter: 2 in. pH 00400: 4.6 units Temp. 000lc 17 °C DRY at Depth to Water Level 825a6: 9.5 ft. below measuring p g point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 000sa: µMhos time of sampling, Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 6.3 ft. Odor 00085: check Volume of water pumped/bailed before sampling: 4.03 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/17/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids.Total 70300 54 mg/L Al -Aluminum oilo5 mg/L pH (Lab) 00403 4.61 units Ba - Barium 01007 ug/L TOC 00680 14.2 mg/L Ca - Calcium oo916 mg/L Chloride 00940 14 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 1.96 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William E. Brown - ORC Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (state) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-15 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-15 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 4.4 units Temp. 000lc 14.6 °C DRY at Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of sampling,check Measuring Point is 2.9 ft. above land surface Relative M.P. Elevation: 0.6 ft. Odor 00085: Volume of water pumped/bailed before sampling: 5.52 gallons Appearance here: ❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 2.15 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 103 mg/L Al - Aluminum oilo5 mg/L pH (Lab) oo403 4.42 units Ba - Barium 01007 ug/L TOC 00680 1.5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 43 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 0.19 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese olo55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # RemediationFor Only Total I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accura DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, it BrownWilliam E. •' GW-59 Rev. Permittee (or Authorized Aqent) Name and Title - Please print or tyoe mg/L Effluent Total VOCs: of Permittee (or Authorized Aqent) mg/L VOC Removal% (Date) 1 /22/2021 SUBMIT FORM ON YELLOW PAPFR ONI Y GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 County Onslow El Lagoon El Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-16 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-16 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: 4.5 units Temp. 000lc 16.8 °C DRY at Depth to Water Level 82546: 3 ft. below measuring point Screened Interval: 15 ft. to 20 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.4 ft. above land surface Relative M.P. Elevation: 0.6 ft. Odor 00085: sampling,check Volume of water pumped/bailed before sampling: 10.56 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 36.5 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 4.51 units Ba - Barium 01007 ug/L TOC 00680 1.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 27 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 6 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 0.12 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022 Facility Name: City of Jacksonville Land Treatment System Non -Discharge WQ0009267 UIC Permit Name (if different): NPDES Other Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED Jacksonville NC 28540 CountyOnslow ❑ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Amy Palaschak Telephone#: (910)938-3620 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name MW-17 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-17 Date sample collected: 12/22/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: 4.1 units Temp. 000lc 16.8 °C DRY at Depth to Water Level 82546: 5.3 ft. below measuring p g point Screened Interval: 15 ft. to 20 ft. Spec. Cond. 000sa: µ Mhos time of sampling,check Measuring Point is 1.9 ft. above land surface Relative M.P. Elevation: 3.4 ft. Odor 00085: Volume of water pumped/bailed before sampling: 9.46 gallons Appearance here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 12/22/2020 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 81.5 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 4.07 units Ba - Barium 01007 ug/L TOC 00680 3.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 34 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 10 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia 00610 0.11 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 =� ��i�[��t�� Chemists, Inc. 6d02Windmill Way, Wilmington, N[284U5 ^ 91.0,3920223Lab ° 910.392.4424Fax 710Dor,rr»nvvnRoad, Monuco'NCzr954 ° 252.473.5702Lab/Fxx �z 255-A Wilmington Hi'bv,ay,Jacksonville, NC2854O ~ 910.347.5843Lab/Fax ANALYTICAL mCONSULTING CHEMISTS in566 oovimnmcnm|cbcmistacuoo City ofJacksonville Date ufReport: Dec 3O.202O Post Office Box 128 Customer P<]#: Jacksonville NC 28541 Customer ID: 08110015 Attention: Roport#: 2020-21385 Project ID: Monitoring Wells Lab ID Sample |D: Cn|0ectDatm/Timnm yNstdx Sampled by 20'54312 Sita:[NW-5 12/15X2020 1:00PN1 VVehar NB Test Method Results Date Analyzed Sulfate EPA »no» <5mg/L 12/21/2020 Chloride ew*o»oc/s 6mg/L 12/29/2020 Total Organic Carbon (T0C) sws»1«o 2.3mg/L 12/18/2020 1.1.1.2-Tetnaoh|onoathane am»uo«o «05pg/L 12/19/2020 1.1.1-Thch|oroethane sw*o»»o <O.bpg/L 12/18/2020 1`1.2.2'Tetoaoh|urumthene am000»o <0.5pQ/L 12/19/2020 1.1.2-Trich|onoethone um«uo»o <0.5Ug/L 12/19/2020 1.1-Dioh|oroethone amuzo»a <05pg/L 12/19/2020 1.1-Dioh/onoethene oMso»o <0.5pg/L 12/19t3020 1.1-Dich|oropropene amauo»a <0.5pg/L 12/19/2020 1.2.3'Trich|opobenz*no omsuo»e <0.5pg/L 12/19/2020 1.2.8-Trich|onopropane »Mu»»»» <0.5pg/L 12/19/2020 1.2.4-Trinh|uvobenzene sw6m»a <0.5pg/L 12/10/2020 1.2.4-Trimethy/benzena emou«ou <0.5pg/L 12/19/2020 1.2'Dibromo-3-Ch|onopnopone owau»»o ^0.6pg/L 12/19/2020 1.2'Oibvamoethane owam«a <0.5VQ/L 12/19/2020 1.2-Dioh|o,obenzene om«z«»a <0.5pg/L 12/19/2020 1.2-Diuh/ornethana oMoo»«u <0.5pg/L 12/19/ O2O 1.2'Oioh/oroAnopane sm«x»u» <0.5pg/L 12/10/2020 1.3.5'Trimethy|benzene »M«c»»o °0.5pg/L 12/19/2020 1.3'Dioh|orobenzene umoc»»B <0.5pO/L 12/19/2020 1.3-Oioh|onopropane amm»»a <0.5pg/L 12/19/2020 1.4-Dioh|orobenzane »Mso«a <0.5pg/L 12/19/2020 2.2'Dich|nnopropane »M«z»»a «05pg/L 12/19/2020 2-Ch|onoto|uene nwo««»o <0.5pg/L 12/19/2020 4'C}h|onoku|uene usuoo»a <0.5pg/L 12/19/2030 Sk ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab « 910.392.4424 Fax 710 8owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infwit environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Report #: 2020-21385 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/19/2020 Bromobenzene SM 62008 <0.5 pg/L 12/19/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Bromodichloromethane SM 62003 <0.5 pg/L 12/19/2020 Bromoform SM 6200B <0.5 pg/L 12/19/2020 Bromomethane SM 6200B <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/19/2020 Chlorobenzene SM 6200E <0.5 pg/L 12/19/2020 Chloroethane SM 6200B <0.5 pg/L 12/19/2020 Chloroform SM 6200B <0.5 pg/L 12/19/2020 Chloromethane SM 6200B 1.76 pg/L 12/19/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM 62008 <0.5 pg/L 12/19/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/19/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/19/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/19/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/19/2020 M+P Xylene SM 6200B <1.0 pg/L 12/19/2020 Methylene chloride SM 6200B <0.5 pg/L 12/19/2020 Naphthalene SM 6200B <0.5 pg/L 12/19/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/19/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/19/2020 p-lsopropyltoluene SM 6200B <0.5 pg/L 12/19/2020 sec-B utyl benzene SM 6200B <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/19/2020 Report # 2020-21385 Page 2 of 3 :enviroche mr] ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, rvlanteo, NC 27954 • 252,473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inI56'a environtnentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Report #: 2020-21385 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12119/2020 Trans-1,2-Dichloroethene SM 62008 <0.5 pg/L 12/19/2020 Trans-1,3-dichloropropene SM 5200B <0.5 pg/L 12/19/2020 Trichloroethene SM 62006 <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 5200B <0.5 pg/L 12/19/2020 Vinyl chloride SM 5200B <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 12/17/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.03 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/29/2020 Comment: , Reviewed by: Report #. 2020-21385 Page 3 of 3 :enviroche]m ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax info@enviroilmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-54598 Site: MW-8 12/17/2020 9:55 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 166 mg/L 12/21 /2020 Chloride SM 4500 CI E 7 mg/L 12/29/2020 Total Organic Carbon (TOC) sM 5310 B 4.8 mg/L 12/22/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5 pg/L 12/19/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trimethylbenzene SM 6200B <0,5 pg/L 12/19/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloroethane SM 6200E <0.5 pg/L 12/19/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 12/19/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 2-Chlorotoluene SM 62008 <0.5 pg/L 12/19/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 Report # : 2020-21509 Page 1 of 15 :envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.44.24 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 L.ab/Fax info@environtnentaIchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Benzene SM 62008 <0.5 pg/L 12/19/2020 Bromobenzene SM 6200B <0.5 pg/L 12/19/2020 Bromochloromethane SM 6200E <0.5 pg/L 12/19/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/19/2020 Bromoform SM 62008 <0.5 pg/L 12/19/2020 Bromomethane SM 62008 <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 5200B <0.5 pg/L 12/19/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/19/2020 Chloroethane SM 6200B <0.5 pg/L 12/19/2020 Chloroform SM 6200B <0.5 pg/L 12/19/2020 Chloromethane SM 6200B 0.62 pg/L 12/19/2020 cis-1,2-Dich loroethene SM 6200E <0, 5 pg/L 12/19/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM 6200B <0.5 pg/L 12/19/2020 Dichlorodifiuoromethane SM 6200E <0.5 pg/L 12/19/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/19/2020 Hexachlorobutadiene SM 62008 <0.5 pg/L 12/19/2020 1 sopropyl benzene SM 62008 <0.5 pg/L 12/19/2020 M+P Xylene SM 6200B <1.0 pg/L 12/19/2020 Methylene chloride SM 6200B <0.5 pg/L 12/19/2020 Naphthalene SM 6200E <0.5 pg/L 12/19/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/19/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/19/2020 p-lsopropyltoluene SM 6200B <0.5 pg/L 12/19/2020 sec-B utyl benzene SM 6200E <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert- B utyl benzene SM 6200B <0.5 pg/L 12/19/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/19/2020 Report #.. 2020-21509 Page 2 of 15 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax - 255-A Wilmington Highway, Jacksonville, NC 28340 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(a,etrvironmentalcliemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/19/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 12/19/2020 Trichloroethene SM 62006 <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 62006 <0.5 pg/L 12/19/2020 Vinyl chloride SM 5200B <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/18/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.09 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method 0.09mg/L 12/29/2020 Report #`. 2020-21509 Page 3 of 15 Environmental Chemists, Inc. r , • Aix, ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab r 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 r 252.473.5702 Lab/Fax 255-A Wilmington I-Iighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info a;environmentalchernists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-54599 Site: MW-9 12/17/2020 10:30 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 91 mg/L 12/21/2020 Chloride SM 4500 CI E 10 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 3.9 mg/L 12/22/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,2-Trichloroethane SM 6200E <0.5 pg/L 12/19/2020 1,1-Dichloroethane SM 62005 <0.5 pg/L 12/19/2020 1, 1 -Dichloroethene SM 5200B <0.5 pg/L 12/19/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichlorobenzene SM 6200e <0.5 pg/L 12/19/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromoethane SM 5200B <0.5 pg/L 12/19/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1, 3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 Report #. 2020-21509 Page 4 of 15 sr� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910,392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/19/2020 Bromobenzene SM 6200B <0.5 pg/L 12/1912020 Bromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12119/2020 Bromoform SM 6200B <0.5 pg/L 12/19/2020 Bromomethane SM 6200B <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/19/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/19/2020 Chloroethane SM 6200B <0.5 pg/L 12/19/2020 Chloroform SM6200B <0.5 pg/L 12/19/2020 Chloromethane SM 6200B 1.60 pg/L 12/19/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM 6200B <0.5 pg/L 12/19/2020 Dichlorodifluoromethane SM 62008 <0.5 pg/L 12/19/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/19/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/19/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/19/2020 M+P Xylene SM 62008 <1.0 pg/L 12/19/2020 Methylene chloride SM 6200B <0.5 pg/L 12/19/2020 Naphthalene SM 6200B <0.5 pg/L 12/19/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 n-Propylbenzene SM 62006 <0.5 pg/L 12/19/2020 ortho-Xylene SM 62008 <0.5 pg/L 12/19/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/19/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/19/2020 Report #:: 2020.21509 Page 5 of 15 Environmental . 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab + 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255 A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax infotC enviroiiinentalchemists.coin City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/19/2020 Trans- 1,2-Dichloroethene SM 62006 <0.5 pg/L 12/19/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Trichloroethene SM 6200B <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/19/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/18/2020 Nitrate+ N itrite-Nitrogen EPA 353,2 < 0.02 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Report #:: 2020-21509 Page 6 of 15 cl'IEnvironmental 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info�erivironmentalchemists.corxi City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54600 Site: MW-10 12/17/2020 11:32 AM Water NB Test Method Results Date Analyzed Sulfate EPA300.0 151 mg/L 12/21/2020 Chloride SM 4500 C E 18 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 2.8 mg/L 12/22/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,1-Trichloroethane SM 6200B <0,5 pg/L 12/19/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,2-Trichloroethane SM 62008 <0.5 pg/L 12/19/2020 1,1-Dichloroethane SM 62008 <0.5 pg/L 12/19/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichlorobenzene SM 6200E <0.5 pg/L 12/19/2020 1,2,3-Trcchloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trimethylbenzene SM 62008 <0.5 pg/L 12/19/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 12/19/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloropropane SM 6200B <0, 5 pg/L 12/19/2020 1,3,5-Trimethylbenzene SM 62008 <0.5 pg/L 12/19/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 Report # 2020-21509 Page 7 of 15 envirochilbm Std ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab s 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A 4 ilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax info@environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO M 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report M 2020-21509 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/19/2020 Bromobenzene SM 62008 <0.5 pg/L 12/19/2020 Bromochloromethane SM 62008 <0.5 pg/L 12/19/2020 8romodichloromethane SM 62008 <0.5 pg/L 12/19/2020 Bromoform SM 62008 <0.5 pg/L 12/19/2020 Bromomethane SM 6200B <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/19/2020 Chlorobenzene SM 62008 <0.5 pg/L 12/19/2020 Chloroethane SM 6200B <0.5 pg/L 12/19/2020 Chloroform SM 6200B <0.5 pg/L 12/19/2020 Chloromethane SM 6200E <0.5 pg/L 12/19/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM 6200B <0.5 pg/L 12/19/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/19/2020 Ethylbenzene SM 62008 <0.5 pg/L 12/19/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/19/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/19/2020 M+P Xylene SM 6200B <1.0 pg/L 12/19/2020 Methylene chloride SM 6200B <0.5 pg/L 12/19/2020 Naphthalene SM 6200B <0.5 pg/L 12/19/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/19/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/19/2020 p-Isopropyltoluene SM 6200E <0.5 pg/L 12/19/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/19/2020 Report # . 2020-21509 Page 8 of 15 [envirochem ANALYTICAL &. CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax into@environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project 1D: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/19/2020 Trans-1,2-Dichloroethene SM 62008 <0.5 pg/L 12/19/2020 Trans-1,3-dichloropropene SM 62008 <0.5 pg/L 12/19/2020 Trichloroethene SM 6200B <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/19/2020 Vinyl chloride SM 6200E <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/18/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Report # 2020-21509 Page 9 of 15 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.51102 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info'�i; environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54601 Site: MW-13 12/17/2020 8:05 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 <5 mg/L 12/21 /2020 Chloride SM 4500 CI E 24 mg/L 12/29/2020 Total Organic Carbon (TOG) Sna 5310 B 4.7 mg/L 12/22/2020 1,1,1,2-Tetrachioroethane SM 5200B <0. 5 pg/L 12/19/2020 1,1,1-Trichloroethane SM 52008 <0.5 pg/L 12/19/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5 pg/L 12/19/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichioroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 Report # 2020-21509 Page 10 of 15 envirochem Sid ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 I-ab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Vilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(a,em-ironmentalcliemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/19/2020 Bromobenzene SM 6200B <0.5 pg/L 12/19/2020 Bromochloromethane SM 62008 <0.5 pg/L 12/19/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/19/2020 Bromoform SM 6200B <0.5 pg/L 12/1912020 Bromomethane SM 6200B <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/19/2020 Chiorobenzene SM 6200B <0.5 pg/L 12/19/2020 Chloroethane SM 6200B <0.5 pg/L 12/19/2020 Chloroform SM 6200B <0.5 pg/L 12/19/2020 Chloromethane SM 6200B 1.70 pg/L 12/19/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM 6200B <0.5 pglL 12/19/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/19/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/19/2020 Flexachlorobutadiene SM 6200B <0.5 pg/L 12/19/2020 Isopropylbenzene SM 62006 <0.5 pg/L 12/19/2020 M+P Xylene SM 62006 <1.0 pg/L 12/19/2020 Methylene chloride SM 6200B <0.5 pg/L 12/19/2020 Naphthalene SM 6200B <0.5 pg/L 12/1912020 n-Butylbenzene SM 6200E <0.5 pg/L 12/19/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/19/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/19/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/19/2020 sec-B utyl benzene SM 6200B <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/19/2020 Report #. 2020-21509 Page 11 of 15 [envirocchem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington I lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax iafo@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Dec 30, 2020 Customer PO #: 215068 Customer ID: 08110015 Report M 2020-21509 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/19/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 Trans- 1,3-dichloropropene SM 6200B <0.5pg/L 12/19/2020 Trichloroethene SM 6200B <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/19/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 3532 < 0.02mg/L 12/18/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Report # 2020-21509 Page 12 of 15 i SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info{{i environmentalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54602 Site: MW-14 12/17/2020 9:03 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 <5 mg/L 12121 /2020 Chloride SM 4500 CI E 14 mg/L 12/29/2020 Total Organic Carbon (TOC) sM 5310 B 14.2 mg/L 12/22/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1,2,2-Tetrachloroethane SM 62006 <0.5 pg/L 12/19/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 12/19/2020 1,1-Dichloropropene SM 62008 <0.5 pg/L 12/19/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/19/2020 1,2-Dichlorobenzene SM 5200B <0.5 pg/L 12/19/2020 1,2-Dichloroethane SM 62006 <0.5 pg/L 12/19/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/19/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/19/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/1912020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/19/2020 Report # 2020-21509 Page 13 of 15 F7 0 0 7 g:viroichem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax in fota!environrnentalchemists. com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Benzene SM 62006 <0.5 pg/L 12/19/2020 Bromobenzene SM 6200B <0.5 pg/L 12/19/2020 Bromochloromethane SM 62008 <0.5 pg/L 12/19/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/19/2020 Bromoform SM 6200B <0.5 pg/L 12/19/2020 Bromomethane SM 6200B <0.5 pg/L 12/19/2020 Carbon tetrachloride SM 6200B <0.5pg/L 12/19/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/19/2020 Chloroethane SM 62006 <0.5 pg/L 12/19/2020 Chloroform SM 6200B <0.5 pg/L 12/19/2020 Chioromethane SM 62008 <0.5 pg/L 12/19/2020 cis-1,2-Dichioroethene SM 6200B <0.5 pg/L 12/19/2020 cis-1, 3-Dichloropropene SM 6200B <0.5 pg/L 12/19/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/19/2020 Dibromomethane SM62006 <0.5 pg/L 12/19/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/19/2020 Ethylbenzene SM 62006 <0.5 pg/L 12/19/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/19/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/19/2020 M+P Xylene SM 6200B <1.0 pg/L 12/19/2020 Methylene chloride SM 62006 <0.5 pg/L 12/19/2020 Naphthalene SM 6200B <0.5 pg/L 12/19/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 n-Propylbenzene SM 62006 <0.5 pg/L 12/19/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/19/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/19/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 12/19/2020 Styrene SM 6200B <0.5 pg/L 12/19/2020 tert-Butyl benzene SM 62008 <0.5 pg/L 12/19/2020 Tetrachloroethene SM 5200B <0.5 pg/L 12/1912020 Report # 2020-21509 Page 14 of 15 Eenvirocahem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 91.0.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.58,13 Lab/Fax info@environtneritalchemists.com City of Jacksonville Date of Report: Dec 30, 2020 Post Office Box 128 Customer PO #: 215068 Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21509 Project ID: Monitoring Wells Toluene SM 62006 <0.5 pg/L 12/19/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 ug/L 12/19/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 12/19/2020 Trichioroethene SM 6200B <0.5 pg/L 12/19/2020 Trichlorofluoromethane SM 5200B <0.5 pg/L 12/19/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/19/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 12/18/2020 Nitrate+Nitrite-Nitrogen EPA 3532 < 0.02 mg/L 12/22/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Comment:° Reviewed by: Report #, 2020-21509 Page 15 of 15 :envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infof€environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54920 Site: MW-3 12/21/2020 1:40 PM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 <5 mg/L 12/29/2020 Chloride SM 4500 CI E 8 mg1L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 3.0 mg/L 12/22/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/29/2020 1, 1,1 -Trichloroethane SM 6200B <0.5pg/L 12/29/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1-Dich loroethene SM 6200B <0.5 pg/L 12/29/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 12/29/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2, 3-Trichloropropane SM 6200B <0.5 pg/L 12/29/2020 1, 2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 12/29/2020 1, 2-Dibromoethane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1, 2-Dichloropropane SM 62008 <0.5 pg/L 12/29/2020 1,3,5-Trimethyl benzene SM 6200B <0.5 pg/L 12/29/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1, 3-Dichloropropane SM 62008 <0.5 pg/L 12/29/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/29/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 12/29/2020 Report # 2020-21644 Page 1 of 15 :envirochemn] ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC: 28405 • 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.coni City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21644 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/29/2020 Bromobenzene SM 6200E <0.5 pg/L 12/29/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/29/2020 Bromodichloromethane SM 62008 <0.5 pg/L 12/29/2020 Bromoform SM 6200B <0.5 pg/L 12/29/2020 Bromomethane SM 6200B <0.5 pg/L 12/29/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/29/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/29/2020 Chloroethane SM 6200B <0.5 pg/L 12/29/2020 Chloroform SM 6200B <0.5 pg/L 12/29/2020 Chloromethane SM 6200B 18.7 pg/L 12/29/2020 cis- 1,2-Dich loroethene SM 6200B <0.5 pg/L 12/29/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12/29/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/29/2020 Dibromomethane SM 6200B <0.5 pg/L 12/29/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/29/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/29/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/29/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/29/2020 M+P Xylene SM 6200B <1.0 pg/L 12/29/2020 Methylene chloride SM 62006 <0.5 pg/L 12/29/2020 Naphthalene SM 6200B <0.5 pg/L 12/29/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/29/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/29/2020 p-Isopropyltoluene SM 6200B 24.2 pg/L 12/29/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 12/29/2020 Styrene SM 6200B <0.5 pg/L 12/29/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/29/2020 Report #. 2020-21644 Page 2 of 15 Foomw * envir6chtem s+ ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, tiTC 28405 • 910.392.0223 Lab 9 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inforu environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Paiaschak Report #: 2020-21644 Project ID: Monitoring Wells Toluene SM 6200B 25.0 pg/L 12/29/2020 Trans- l ,2-Dichloroethene sM 6200B <0.5 pg/L 12/29/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 12/29/2020 Trichlorcethene SM 6200B <0.5 pg/L 12/29/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/29/2020 Vinyl chloride SM 62008 <0.5 pg/L 12/29/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.03mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 0.03 mg1L 12/29/2020 Report #:: 2020-21644 Page 3 of 15 [enviroochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 + 91.0.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoi'4environmen talchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54921 Site: MW-4 12/21/2020 1:17 PM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 34 mg/L 12/29/2020 Chloride SM 4500 cl E 40 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 5.8 mg/L 12/22/2020 1,1,1,2-Tetrachloroethane SM 62006 <0.5 pg/L 12/30/2020 1, 1, 1 -Trichloroethane SM 62006 <0.5 pg/L 12/30/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 12/30/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloroethane SM 62006 <0.5 pg/L 12/30/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 1,1-Dichloropropene SM 62006 <0.5 pg/L 12/30/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1, 2, 3-Trichloropropane SM 62008 <0.5 pg/L 12/30/2020 1, 2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichloropropane SM 62008 <0.5 pg/L 12/30/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 4-Chlorotoluene SM 5200B <0.5 pg/L 12/30/2020 Report #:: 2020-216" Page 4 of 15 envirochm ANALYTICAL & CONSULTING CHEMISTS Environmental. Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax 255-A Wilmington I l.ighway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax infoicrenvironmen talchemists.conl City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Benzene SM 6200B <0.5 fag/L 12/30/2020 Bromobenzene SM 6200B <0.5 fag/L 12/30/2020 Bromochloromethane SM 6200B <0.5 fag/L 12/30/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/30/2020 Bromoform SM 6200B <0.5 fag/L 12/30/2020 Bromomethane SM 6200B <0.5 fag/L 12/30/2020 Carbon tetrachloride SM 6200B <0.5 fag/L 12/30/2020 Chlorobenzene SM 6200B <0.5 fag/L 12/30/2020 Chloroethane SM 6200B <0.5 fag/L 12/30/2020 Chloroform SM 6200B <0.5 fag/L 12/30/2020 Chloromethane SM 6200B 4.04 fag/L 12/30/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 cis-1,3-Dichloropropene SM 6200B <0.5 fag/L 12/30/2020 Dibromochloromethane SM 6200B <0.5 fag/L 12/30/2020 Dibromomethane SM 6200B <0.5 fag/L 12/30/2020 Dichlorodifluoromethane SM 6200B <0.5 fag/L 12130/2020 Ethylbenzene SM 6200B <0.5 fag/L 12/30/2020 Hexachlorobutadiene SM 6200B <0.5 fag/L 12/30/2020 Isopropylbenzene SM 6200B <0.5 fag/L 12/30/2020 M+P Xylene SM 6200B <1.0 fag/L 12/30/2020 Methylene chloride SM 6200B <0.5 fag/L 12/30/2020 Naphthalene SM 6200B <0.5 fag/L 12/30/2020 n-Butylbenzene SM 6200E <0.5 fag/L 12/30/2020 n-Propylbenzene SM 6200B <0.5 fag/L 12/30/2020 ortho-Xylene SM 6200B <0.5 fag/L 12/30/2020 p-Isopropyltoluene SM 6200B <0.5 fag/L 12/30/2020 sec-Butylbenzene SM 6200B <0.5 fag/L 12/30/2020 Styrene 8M 6200B <0.5 fag/L 12/30/2020 tert-Butyl benzene SM 62008 <0.5 fag/L 12/30/2020 Tetrachloroethene SM 6200B <0.5 fag/L 12/30/2020 Report #.; 2020-21644 Page 5 of 15 [enviriowhe]m s�i1�71 �:'Hii1►bY�l�l.IKd:I �u16�� Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392,0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax info;c"r: environmen talchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC 28541 Attention: Amy Palaschak Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21644 Project ID: Monitoring Wells Toluene SM 6200s <0.5 pg/L 12/30/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trans-1,3-dichloropropene SM 6200B <0.5 pg/L 12/30/2020 Trichloroethene SM 6200D <0.5 pg/L 12/30/2020 Trichlorofluoromethane SM 6200s <0.5 pg/L 12/30/2020 Vinyl chloride SM 6200s <0.5 pg/L 12/30/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA353.2 < 0.02 mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Report #: 2020-21644 Page 6 of 15 6en:v7ircoch]e ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington I lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC 28541 Attention: Amy Palaschak Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report M 2020-21644 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54922 Site: MW-6 12/21/2020 10:44 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 31 mg/L 12/29/2020 Chloride SM 4500 CI E 26 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 7.9 mg/L 12/22/2020 1. 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/29/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1,2-Trichloroethane SM62008 <0.5pg/L 12/29/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 12/29/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 12/29/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/29/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 1, 3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 12/29/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/29/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/29/2020 Report #:: 2020-21644 Page 7 of 15 [en rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 Y 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21644 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/29/2020 Bromobenzene SM 6200B <0.5 pg/L 12/29/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/29/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/29/2020 Bromoform SM 6200B <0.5 pg/L 12/29/2020 Bromomethane SM 6200B <0.5 pg/L 12/29/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/29/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/29/2020 Chloroethane SM 6200B <0.5 pg/L 12/29/2020 Chloroform SM 6200B <0.5 pg/L 12/29/2020 Chloromethane SM 6200B <0.5 pg/L 12/29/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/29/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12129/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12129/2020 Dibromomethane SM 6200B <0.5 pg/L 12/29/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12129/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/29/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/29/2020 Isopropyl benzene SM 6200B <0.5 pg/L 12/29/2020 M+P Xylene SM 6200B <1.0 pg/L 12/29/2020 Methylene chloride SM 6200B <0.5 pg/L 12/29/2020 Naphthalene SM 6200B <0.5 pg/L 12/29/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 n-Propylbenzene SM 620013 <0.5 pg/L 12/29/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/29/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/29/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 Styrene SM 6200B <0.5 pg/L 12/29/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 Tetrachloroethene SM 62006 <0.5 pg/L 12/29/2020 Report #: 2020-21544 Page 8 of 15 77779 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Toluene SM 62006 <0.5 pg/L 12/29/2020 Trans-1 ,2-Dichloroethene SM 6200B <0.5 pg/L 12/29/2020 Trans-1,3-dichloropropene SM 6200B <0.5 pg/L 12/29/2020 Trichloroethene SM 6200B <0.5 pg/L 12/29/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 12/29/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/29/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.10 mg/L 12/23/2020 Nitrate+N itrite-N itrogen EPA 353.2 0.03 mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method <0.02mg/L 12/29/2020 Report #: 2020-21644 Page 9 of 15 6re�nviroch:em ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inforu environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54923 Site: MW-7 12/21/2020 12:15 PM Water NB Test Method Results Date Analyzed Sulfate EPA300.0 47mg/L 12/29/2020 Chloride SM 4500 CI E 57 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 7.6 mg/L 12/22/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 µg/L 12/29/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 µg/L 12/29/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5 µg/L 12/29/2020 1,1,2-Trichloroethane SM 6200B <0.5 µg/L 12/29/2020 1,1-Dichloroethane SM 6200B <0.5 µg/L 12/29/2020 1,1-Dichloroethene SM 6200B <0.5 µg/L 12/2912020 1,1-Dichloropropene SM 6200B <0.5 µg/L 12/29/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 µg/L 12/29/2020 1,2, 3-Trichloropropane SM 6200B <0.5 µg/L 12/29/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 iJg/L 12/29/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 µg/L 12/29/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5µg/L 12/29/2020 1,2-Dibromoethane SM 6200B <0.5 µg/L 12/29/2020 1,2-Dichlorobenzene SM 6200B <0.5 µg/L 12/29/2020 1,2-Dichloroethane SM 6200B <0.5 µg/L 12/29/2020 1,2-Dichloropropane SM 6200B <0.5 µg/L 12/29/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 µg/L 12/29/2020 1, 3-Dichlorobenzene SM 6200B <0.5 µg/L 12/29/2020 1,3-Dichloropropane SM 6200B <0.5µg/L 12/29/2020 1,4-Dichlorobenzene SM 6200B <0.5 µg/L 12/29/2020 2,2-Dichloropropane SM 6200B <0.5 µg/L 12/29/2020 2-Chlorotoluene SM 6200B <0.5 µg/L 12/29/2020 4-Chlorotoluene SM 62006 <0.5 µg/L 12/29/2020 Report #:: 2020-21644 Page 10 of 15 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilnngton Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/29/2020 Bromobenzene SM 6200B <0.5 pg/L 12/29/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/29/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/29/2020 Bromoform SM 6200a <0.5 pg/L 12/29/2020 Bromomethane SM 6200a <0.5 pg/L 12/29/2020 Carbon tetrachloride SM 6200a <0.5 pg/L 12/29/2020 Chlorobenzene SM 6200a <0.5 pg/L 12/29/2020 Chloroethane SM 6200B <0.5 pg/L 12/29/2020 Chloroform SM 6200a <0.5 pg/L 12/29/2020 Chloromethane SM 6200a 0.65 pg/L 12/29/2020 cis-1,2-Dichloroethene SM 6200a <0.5 pg/L 12/29/2020 cis-1, 3-Dichloropropene SM 6200a <0.5 pg/L 12/29/2020 Dibromochloromethane SM 6200a <0.5 pg/L 12/29/2020 Dibromomethane SM 6200a <0.5 pg/L 12/29/2020 Dichlorodifluoromethane SM 5200B <0.5 pg/L 12/29/2020 Ethylbenzene SM 6200a <0.5 pg/L 12/29/2020 Hexachlorobutadiene SM 6200a <0.5 pg/L 12/29/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/29/2020 M+P Xylene SM 6200a <1.0 pg/L 12/29/2020 Methylene chloride SM 6200a <0.5 pg/L 12/29/2020 Naphthalene SM 62006 <0.5 pg/L 12/29/2020 n-Butylbenzene SM 6200a <0.5 pg/L 12/29/2020 n-Propylbenzene SM 62008 <0.5 pg/L 12/29/2020 ortho-Xylene SM 6200a <0.5 pg/L 12/29/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/29/2020 sec-Butylbenzene SM 6200a <0.5 pg/L 12/29/2020 Styrene SM 6200a <0.5 pg/L 12/29/2020 te rt-B utyl benzene SM 6200a <0.5 pg/L 12/29/2020 Tetrachloroethene SM 6200a <0.5 pg/L 12/29/2020 Report t1 2020.21644 Page 11 of 15 [envi rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Toluene SM 62008 <0.5 pg/L 12/29/2020 Trans-1,2-Dichioroethene SM 6200B <0.5 pg/L 12/29/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 12/29/2020 Trichloroethene SM 6200B <0.5 pg/L 12/29/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/29/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/29/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Report #': 2020-21644 Page 12 of 15 r7�1 a r • i • SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405+ • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertow-n Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC 28541 Attention'. Amy Palaschak Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21644 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54924 Site: MW-12 12/21/2020 11:40 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 9 mg/L 12/29/2020 Chloride SM 4500 CI E 8 mg/L 12/29/2020 Total Organic Carbon (TOC) SM 5310 B 24.9 mg/L 12/22/2020 1,1,1, 2-Tetrach loroethane SM 6200B <0.5 pg/L 12/29/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 12/29/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/29/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,1-Dichloroethene SM 6200B <0.5pg/L 12/29/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 12/29/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/29/2020 1,2,4-Trichlorobenzene SM 6200E <0.5 pg/L 12/29/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/29/2020 1,2-Dichloropropane SM 6200B <0.5 pq/L 12/29/2020 1, 3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 12/29/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/29/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/29/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/29/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/29/2020 Report #:: 2020-21644 Page 13 of 15 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 + 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inforti environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Jan 07, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21644 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/29/2020 Bromobenzene SM 6200B <0.5 pg/L 12/29/2020 Bromochloromethane sM 6200B <0.5 pg/L 12/29/2020 Bromodichloromethane SM 62008 <0.5 pg/L 12/29/2020 Bromoform SM 6200B <0.5 pg/L 12/29/2020 Bromomethane SM 6200B <0.5 pg/L 12/29/2020 Carbon tetrachloride SM 6200B <0.5pg/L 12/29/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/29/2020 Chloroethane SM 6200B <0.5 pg/L 12/29/2020 Chloroform SM 6200B <0.5 pg/L 12129/2020 Chloromethane SM 6200B <0.5 pg/L 12/29/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/29/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 12/29/2020 Dibromochloromethane SM 62008 <0.5 pg/L 12/29/2020 Dibromomethane SM 6200B <0.5 pg/L 12/29/2020 Dichlorodifluoromethane SM 62008 <0.5 pg/L 12/29/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/2912020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/29/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/29/2020 M+P Xylene SM 62006 <1.0 pg/L 12/29/2020 Methylene chloride SM 6200B <0.5 pg/L 12/29/2020 Naphthalene SM 6200B <0.5 pg/L 12/29/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/29/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/29/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/29/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 12/29/2020 Styrene SM 6200B <0.5 pg/L 12/29/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/29/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/29/2020 Report #:: 2020-21644 Page 14 of 15 Environmental Chemists, Inc. enviroc emJ 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax s } 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info?a-environmentalchemists.com City of Jacksonville Date of Report: Jan 07, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21644 Project ID: Monitoring Wells Toluene SM 62008 <0.5 pg/L 12/29/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/29/2020 Trans- 1,3-dichloropropene SM 6200e <0.5 pg/L 12/29/2020 Trichloroethene SM 6200B <0.5 pg/L 12/29/2020 Trichiorofluoromethane SM 6200B <0.5 pg/L 12/29/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/29/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.03 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA3532 0.02 mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/29/2020 Comment. - Reviewed by: z Report #:: 2020-21644 Page 15 of 15 Environmental Chemists, Inc. IlF 6602 Windmill Way, Wilmington, NC 28405 # 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 # 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 # 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55230 Site: MW-1 12/22/2020 9:50 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 14 mg/L 12/29/2020 Chloride SM 4500 CI E 47 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 12.0 mg/L 12/29/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 01/06/2021 1,1,1-Trichloroethane SM6200B <0.5pg/L 01/06/2021 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 01/06/2021 1,1,2-Trichloroethane SM 6200B <0.5pg/L 01/06/2021 1,1-Dichloroethane SM 6200B <0.5pg/L 01/06/2021 1,1-Dichloroethene SM 6200B <0.5pg/L 01/06/2021 1,1-Dichloropropene SM62ooB <0.5pg/L 01/06/2021 1,2,3-Trichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,2,3-Trichloropropane SM 6200B <0.5pg/L 01/06/2021 1,2,4-Trichlorobe nzene SM 6200B <0.5pg/L 01/06/2021 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 01/06/2021 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 01/06/2021 1,2-Dibromoethane SM 6200B <0.5 pg/L 01/06/2021 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 01/06/2021 1,2-Dichloroethane SM 6200B <0.5pg/L 01/06/2021 1,2-Dichloropropane SM 6200B <0.5pg/L 01/06/2021 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichloropropane SM 6200B <0.5pg/L 01/06/2021 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 01/06/2021 2,2-Dichloropropane SM 6200B <0.5 pg/L 01/06/2021 2-Chlorotoluene SM 6200B <0.5 pg/L 01/06/2021 4-Chlorotoluene SM 6200B <0.5 pg/L 01/06/2021 Report #:: 2020-21759 Page 1 of 18 envir6ch6ni sM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 01/06/2021 Bromobenzene SM 6200B <0.5 pg/L 01/06/2021 Bromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Bromodichloromethane SM 62008 <0.5 pg/L 01/06/2021 Bromoform SM 6200B <0.5 pg/L 01/06/2021 Bromomethane SM 6200B <0.5 pg/L 01/06/2021 Carbon tetrachloride 8M 6200B <0.5 pg/L 01/06/2021 Chlorobenzene SM 6200B <0.5 pg/L 01/06/2021 Chloroethane SM 6200B <0.5 pg/L 01/06/2021 Chloroform SM 6200B <0.5 pg/L 01/06/2021 Chloromethane SM 6200B <0.5 pg/L 01/06/2021 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 01/06/2021 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 01/06/2021 Dibromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Dibromomethane SM 6200B <0.5 pg/L 01/06/2021 Dichlorodifluoromethane SM 6200B <0.5 pg/L 01/06/2021 Ethylbenzene SM 62008 <0.5 pg/L 01/06/2021 Hexachlorobutadiene SM 6200B <0.5 pg/L 01/06/2021 Isopropylbenzene SM 6200B <0.5 pg/L 01/06/2021 M+P Xylene SM 5200B <1.0 pg/L 01/06/2021 Methylene chloride SM 6200B <0.5 pg/L 01/06/2021 Naphthalene SM 6200B <0.5 pg/L 01/06/2021 n-Butylbenzene SM 6200B <0.5 pg/L 01/06/2021 n-Propylbenzene SM 6200B <0.5 pg/L 01/06/2021 ortho-Xylene SM 6200B <0.5 pg/L 01/06/2021 p-Isopropyltoluene SM 6200B <0.5 pg/L 01/06/2021 sec-Butylbenzene SM 6200B <0.5 pg/L 01/06/2021 Styrene SM 6200B <0.5 pg/L 01/06/2021 tert-B utyl benzene SM 6200B <0.5 pg/L 01/06/2021 Tetrachloroethene SM 6200B <0.5 pg/L 01/06/2021 Report #:: 2020-21759 Page 2 of 18 F"11107�� ' i f sM. ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project 1D: Monitoring Wells Toluene SM 6200B <0.5 pg/L 01/06/2021 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 01/06/2021 Trans-1,3-dichloropropene SM62008 <0.5pg/L 01/06/2021 Trichloroethene SM 62008 <0.5 pg/L 01/06/2021 Trichlorofluoromethane SM 6200B <0.5 pg/L 01/06/2021 Vinyl chloride SM 6200B <0.5 pg/L 01/06/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.03mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 0.03mg/L 01/08/2021 Report #.: 2020-21759 Page 3 of 18 SM ANALYTICAL d CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55231 Site: MW-2 12/22/2020 8:45 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 6 mg/L 12/29/2020 Chloride SM 4500 CI E 63 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 8.4 mg/L 12/29/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 12130/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 12/30/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichlorobenzene SM 62006 <0.5 pg/L 12/30/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1, 3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 Report #:: 2020-21759 Page 4 of 18 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Jan 08, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21759 Project ID: Monitoring Wells Benzene sM 6200B <0.5 pg/L 12/30/2020 Bromobenzene sM 6200B <0.5 pg/L 12/30/2020 Bromochloromethane sM 6200B <0.5 pg/L 12/30/2020 Bromodichloromethane sM 6200B <0.5 pg/L 12/30/2020 Bromoform sM 6200B <0.5 pg/L 12/30/2020 Bromomethane sM 6200B <0.5 pg/L 12/30/2020 Carbon tetrachloride sM 6200B <0.5 pg/L 12/30/2020 Chlorobenzene sM 5200B <0.5 pg/L 12/30/2020 Chloroethane sM 6200B <0.5 pg/L 12/30/2020 Chloroform sM 62008 <0.5 pg/L 12/30/2020 Chloromethane sM 6200B 1.90 pg/L 12/30/2020 cis-1,2-Dichloroethene sM 6200B <0.5 pg/L 12/30/2020 cis-1,3-Dichloropropene sM 6200B <0.5 pg/L 12/30/2020 Dibromochloromethane sM 6200B <0.5 pg/L 12/30/2020 Dibromomethane sM 6200B <0.5 pg/L 12/30/2020 Dichlorodifluoromethane sM 6200B <0.5 pg/L 12/30/2020 Ethylbenzene sM 6200B <0.5 pg/L 12/30/2020 Hexachlorobutadiene sM 6200B <0.5 pg/L 12/30/2020 Isopropyl benzene sM 6200B <0.5 pg/L 12/30/2020 M+P Xylene sM 6200B <1.0 pg/L 12/30/2020 Methylene chloride sM 6200B <0.5 pg/L 12/30/2020 Naphthalene sM 6200B <0.5 pg/L 12/30/2020 n-Butylbenzene sM 6200B <0.5 pg/L 12/30/2020 n-Propylbenzene sM 6200B <0.5 pg/L 12/30/2020 ortho-Xylene sM 6200B <0.5 pg/L 12/30/2020 p-Isopropyltoluene sM 6200B <0.5 pg/L 12/30/2020 sec-Butylbenzene sM 6200B <0.5 pg/L 12/30/2020 Styrene sM 6200B <0.5 pg/L 12/30/2020 tert-Butyl benzene sM 6200B <0.5 pg/L 12/30/2020 Tetrachioroethene sM 6200B <0.5 pg/L 12/30/2020 Report #:: 2020-21759 Page 5 of 18 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/30/2020 Trans- 1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trans-1,3-dichloropropene SM 6200B <0.5 pg/L 12/30/2020 Trichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/30/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/30/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 3532 <0.02mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA 3532 0.06mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 0.06 mg/L 01/08/2021 Report # : 2020-21759 Page 6 of 18 F""P7 7 Environmental Chemists, Inc. L:envirochem6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax s{ 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL R CONSULTING CHEMISTS info@envirotimentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC 28541 Attention: Amy Palaschak Date of Report: Jan 08, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55232 Site: MW-11 12/22/2020 10:35 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300 0 <5 mg/L 12/29/2020 Chloride SM 4500 CI E 6 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 1.3 mg/L 12/29/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5pg/L 12/30/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 12/30/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 12/30/2020 1, 2, 3-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1, 2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 Report # . 2020-21759 Page 7 of 18 envirochem SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/30/2020 Bromobenzene SM 6200B <0.5 pg/L 12/30/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/30/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/30/2020 Bromoform SM 6200B <0.5 pg/L 12/30/2020 Bromomethane SM 6200B <0.5 pg/L 12/30/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/30/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/30/2020 Chloroethane SM 6200B <0.5 pg/L 12/30/2020 Chloroform SM 620CB <0.5 pg/L 12/30/2020 Chloromethane SM 6200B 1.22 pg/L 12/30/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 cis-1,3-Dichloropropene SM 62008 <0.5 pg/L 12/30/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/30/2020 Dibromomethane SM 6200B <0.5 pg/L 12/30/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/30/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/30/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/30/2020 Isopropylbenzene SM 6200B <0.5 pg/L 12/30/2020 M+P Xylene SM 6200B <1.0 pg/L 12/30/2020 Methylene chloride SM 6200B <0.5 pg/L 12/30/2020 Naphthalene SM 6200B <0.5 pg/L 12/30/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/30/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/30/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/30/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/30/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 12/30/2020 Styrene SM 6200B <0.5 pg/L 12/30/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 12/30/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/30/2020 Report #:: 2020-21759 Page 8 of 18 7:77 SM: ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wihnington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC 28541 Attention: Amy Palaschak Date of Report: Jan 08, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21759 Project ID: Monitoring Wells Toluene SM 62008 <0.5 pg/L 12/30/2020 Trans- l ,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trans-1,3-dichloropropene SM 6200B <0.5 pg/L 12/30/2020 Trichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 12/30/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/30/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.42mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 0.42 mg/L 01 /08/2021 Report #:: 2020-21759 Page 9 of 18 Environmental Chemists, Inc. •nvirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55233 Site: MW-15 12/22/2020 9:05 AM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 <5 mg/L 12/29/2020 Chloride SM 4500 CI E 43 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 1.5 mg/L 12/29/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5pg/L 12/30/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 12/30/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 12/30/2020 1,2,3-Trichlorobenzene SM 6200E <0.5 pg/L 12/30/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dibromoethane SM 62008 <0.5 pg/L 12/30/2020 1,2-Dichlorobenzene SM 6200E <0.5 pg/L 12/30/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 12/30/2020 1,2-Dichloropropane SM 5200B <0.5 pg/L 12/30/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 12/30/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 12/30/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 12/30/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 12/30/2020 Report tl:: 2020-21759 Page 10 of 18 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 12/30/2020 Bromobenzene SM 6200B <0.5 pg/L 12/30/2020 Bromochloromethane SM 6200B <0.5 pg/L 12/30/2020 Bromodichloromethane SM 6200B <0.5 pg/L 12/30/2020 Bromoform SM 62008 <0.5 pg/L 12/30/2020 Bromomethane SM 6200B <0.5 pg/L 12/30/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 12/30/2020 Chlorobenzene SM 6200B <0.5 pg/L 12/30/2020 Chloroethane SM 62008 <0.5 pg/L 12/30/2020 Chloroform SM 6200B <0.5 pg/L 12/30/2020 Chloromethane SM 6200B 0.93 pg/L 12/30/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 12/30/2020 Dibromochloromethane SM 6200B <0.5 pg/L 12/30/2020 Dibromomethane SM 6200B <0.5 pg/L 12/30/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 12/30/2020 Ethylbenzene SM 6200B <0.5 pg/L 12/30/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 12/30/2020 Isopropyl benzene SM 6200B <0.5 pg/L 12/30/2020 M+P Xylene SM 6200B <1.0 pg/L 12/30/2020 Methylene chloride SM 6200B <0.5 pg/L 12/30/2020 Naphthalene SM 6200B <0.5 pg/L 12/30/2020 n-Butylbenzene SM 6200B <0.5 pg/L 12/30/2020 n-Propylbenzene SM 6200B <0.5 pg/L 12/30/2020 ortho-Xylene SM 6200B <0.5 pg/L 12/30/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 12/30/2020 sec-B u tyl benzene SM 6200B <0.5 pg/L 12/30/2020 Styrene SM 62006 <0.5 pg/L 12/30/2020 tert-Butyl benzene SM 6200B <0.5 pg/L 12/30/2020 Tetrachloroethene SM 6200B <0.5 pg/L 12/30/2020 Report #:: 2020-21759 Page 11 of 18 envirochem6602 sM; ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 12/30/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trans-1,3-dichloropropene SM 6200B <0.5 pg/L 12/30/2020 Trichloroethene SM 6200B <0.5 pg/L 12/30/2020 Trichlorofluoromethane SM 5200B <0.5 pg/L 12/30/2020 Vinyl chloride SM 6200B <0.5 pg/L 12/30/2020 Nitrate Nitrogen {Calc} Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA 3532 2.15mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 2.15 mg/L 01/08/2021 Report #.: 2020-21759 Page 12 of 18 F777:77 Environmental Chemists, Inc. • 6602 Windmill Way Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax �r 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55234 Site: MW-16 12/22/2020 12:55 PM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 6 mg/L 12/29/2020 Chloride SM 4500 CI E 27 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 1.6 mg/L 12/29/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg1L 01/06/2021 1,1,1-Trichloroethane SM 6200B <0.5pg/L 01/06/2021 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 01/06/2021 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 01/06/2021 1,1-Dichloroethane SM 6200E <0.5 pg/L 01/06/2021 1,1-Dichloroethene SM6200B <0.5pg/L 01/06/2021 1,1-Dichloropropene SM 6200B <0.5 pg/L 01/06/2021 1,2,3-Trichlorobenzene SM6200B <0.5pg/L 01/06/2021 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 01/06/2021 1,2,4-Trichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,2,4-Trimethylbenzene SM 6200B <0.5pg/L 01/06/2021 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 01106/2021 1,2-Dibromoethane SM 6200B <0.5 pg/L 01/06/2021 1,2-Dichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,2-Dichloroethane SM 6200B <0.5 pg/L 01/06/2021 1,2-Dichloropropane SM 6200B <0.5pg/L 01/06/2021 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichloropropane SM 6200B <0.5pg/L 01/06/2021 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 01/06/2021 2,2-Dichloropropane SM 6200B <0.5 pg/L 01/06/2021 2-Chlorotoluene SM 6200B <0.5 pg/L 01/06/2021 4-Chlorotoluene SM 6200B <0.5 pg/L 01/06/2021 Report #.. 2020-21759 Page 13 of 18 [enviro)--he]c ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 01/06/2021 Bromobenzene SM 6200B <0.5 pg/L 01/06/2021 Bromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Bromodichloromethane SM 6200B <0.5 pg/L 01/06/2021 Bromoform SM 6200B <0.5 pg/L 01/06/2021 Bromomethane SM 6200B <0.5 pg/L 01/06/2021 Carbon tetrachloride SM 6200B <0.5 pg/L 01/06/2021 Chlorobenzene SM 6200B <0.5 pg/L 01 /06/2021 Chloroethane SM 6200B <0.5 pg/L 01/06/2021 Chloroform SM 6200E <0.5 pg/L 01/06/2021 Chloromethane SM 6200B 0.68pg/L 01/06/2021 cis-1,2-Dichloroethene SM 6200B <0.5pg/L 01/06/2021 cis-1,3-Dichloropropene SM 6200B <0.5pg/L 01/06/2021 Dibromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Dibromomethane SM 6200B <0.5 pg/L 01/06/2021 Dichlorodifluoromethane SM 6200B <0.5 pg/L 01/06/2021 Ethylbenzen a SM 6200E <0.5 pg/L 01/06/2021 Hexachlorobutadiene SM 6200B <0.5 pg/L 01/06/2021 Isopropylbenzene SM 6200B <0.5 pg/L 01/06/2021 M+P Xylene SM 6200B <1.0 pg/L 01/06/2021 Methylene chloride SM 62008 <0.5 pg/L 01/06/2021 Naphthalene SM 6200B <0.5 pg/L 01 /06/2021 n-Butylbenzene SM 6200B <0.5 pg/L 01/06/2021 n-Propylbenzene SM 6200B <0.5 pg/L 01/06/2021 ortho-Xylene SM 6200B <0.5 pg/L 01/06/2021 p-Isopropyltoluene SM 6200B <0.5 pg/L 01/06/2021 sec-B utyl benzene SM 6200B <0.5 pg/L 01/06/2021 Styrene SM 6200B <0.5 pg/L 01/06/2021 tert-Butyl benzene SM 6200B <0.5 pg/L 01/06/2021 Tetrachloroethene SM 62008 <0.5 pg/L 01/06/2021 Report #:: 2020-21759 Page 14 of 18 [envi7rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 01/06/2021 Trans- 1,2-Dichloroethene SM 6200B <0.5 pg/L 01/06/2021 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 01/06/2021 Trichloroethene SM 6200B <0.5 pg/L 01/06/2021 Trichlorofluoromethane SM 6200B <0.5 pg/L 01/06/2021 Vinyl chloride SM 6200B <0.5 pg/L 01/06/2021 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.02mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method 0.02 mg/L 01/08/2021 Report #:: 2020-21759 Page 15 of 18 env 4 rlochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Post Office Box 128 Jacksonville NC Attention: Amy Palaschak 28541 Date of Report: Jan 08, 2021 Customer PO #: Customer ID: 08110015 Report #: 2020-21759 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-55236 Site: MW-17 12/22/2020 12:35 PM Water NB Test Method Results Date Analyzed Sulfate EPA 300.0 10 mg/L 12/29/2020 Chloride SM 4500 CI E 34 mg/L 12/30/2020 Total Organic Carbon (TOC) SM 5310 B 3.1 mg/L 12/29/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 pg/L 01/06/2021 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 01/06/2021 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 01/06/2021 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 01/06/2021 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 01/06/2021 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 01/06/2021 1, 1 -Dichloropropene SM 62005 <0.5 pg/L 01/06/2021 1,2,3-Trichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,2,3-Trichloropropane SM 6200B <0.5pg/L 01/06/2021 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 01/06/2021 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 01/06/2021 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 01/06/2021 1,2-Dibromoethane SM 6200B <0.5 pg/L 01/06/2021 1,2-Dichlorobenzene SM 62009 <0.5 pg/L 01/06/2021 1,2-Dichloroethane SM 6200B <0.5pg/L 01/06/2021 1,2-Dichloropropane SM 6200B <0.5 pg/L 01/06/2021 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichlorobenzene SM 6200B <0.5pg/L 01/06/2021 1,3-Dichloropropane SM 6200B <0.5pg/L 01/06/2021 1,4-Dichlorobenzene SM 6200B <0.5pg/L 01/06/2021 2,2-Dichloropropane SM 6200B <0.5 pg/L 01/06/2021 2-Chlorotoluene SM 6200B <0.5pg/L 01/06/2021 4-Chlorotoluene SM 6200B <0.5pg/L 01/06/2021 Report #:: 2020-21759 Page 16 of 18 r- 77 77 Environmental Chemists, Inc. • # 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SSA 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Benzene SM 6200B <0.5 pg/L 01/06/2021 Bromobenzene SM 6200B <0.5pg/L 01/06/2021 Bromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Bromodichloromethane SM 62008 <0.5 pg/L 01/06/2021 Bromoform SM 6200B <0.5 pg/L 01/06/2021 Bromomethane SM 6200B <0.5 pg/L 01/06/2021 Carbon tetrachloride SM6200B <0.5pg/L 01/06/2021 Chlorobenzene SM 6200B <0.5 pg/L 01/06/2021 Chloroethane SM 6200B <0.5 pg/L 01/06/2021 Chloroform SM 6200B <0.5 pg/L 01/06/2021 Chloromethane SM 6200B 1.13 pg/L 01/06/2021 cis-1,2-Dichloroethene SM 6200B <0.5pg/L 01/06/2021 cis-1,3-Dichloropropene SM 6200B <0.5pg/L 01/06/2021 Dibromochloromethane SM 6200B <0.5 pg/L 01/06/2021 Dibromomethane SM 6200B <0.5 pg/L 01/06/2021 Dichlorodifluoromethane SM 6200B <0.5 pg/L 01/06/2021 Ethylbenzene SM 6200B <0.5 pg/L 01/06/2021 Hexachlorobutadiene SM 6200B <0.5 pg/L 01/06/2021 Isopropylbenzene SM 6200B <0.5pg/L 01/06/2021 M+P Xylene SM 62008 <1.0 pg/L 01/06/2021 Methylene chloride SM 6200B <0.5 pg/L 01/06/2021 Naphthalene SM 6200B <0.5 pg/L 01/06/2021 n-Butylbenzene SM 6200B <0.5 pg/L 01/06/2021 n-Propylbenzene SM 6200B <0.5 pg/L 01/06/2021 ortho-Xylene SM 6200B <0.5 pg/L 01/06/2021 p-Isopropyltoluene SM 6200B <0.5 pg/L 01/06/2021 sec-Butylbenzene SM 62008 <0.5 pg/L 01/06/2021 Styrene SM 6200B <0.5 pg/L 01/06/2021 tert-Butylbenzene SM 6200B <0.5 pg/L 01/06/2021 Tetrachloroethene SM 6200B <0.5 pg/L 01/06/2021 Report #, 2020-21759 Page 17 of 18 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com City of Jacksonville Date of Report: Jan 08, 2021 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2020-21759 Project ID: Monitoring Wells Toluene SM 6200B <0.5 pg/L 01/06/2021 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 01/06/2021 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 01/06/2021 Trichloroethene SM 6200B <0.5 pg/L 01/06/2021 Trichlorofluoromethane SM 6200B <0.5 pg/L 01/06/2021 Vinyl chloride SM 6200B <0.5 pg/L 01/06/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353,2 < 0.02 mg/L 12/23/2020 Nitrate+Nitrite-Nitrogen EPA 3532 < 0.02 mg/L 12/28/2020 Nitrate Nitrogen Subtraction Method <0.02mg/L 01/08/2021 Comment: P Reviewed by: Report #.: 2020-21759 Page 18 of 18