WQ0018087_Monitoring - 12-2020_20210129

-DAK Americas
January 14, 2021
Division of Water Resources
0
Information Processing Unit
LU n+
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
cn
:W
Subject: Permit No. WQ001087
Cape Fear Manufacturing Facility
Surface Disposal of Class B Residuals (Dedicated)
Brunswick County
Dear Division of Water Resources: C
Enclosed please find: �P
1. Two copies of Compliance and Monitoring Form (GW-59) for the 6 wells
associated with the Sludge Disposal Unit.
2. Laboratory analysis for these same wells.
3. Compliance Report Form GW-59a
4. Summary of the Groundwater Monitoring Results
As shown in the summary, some of the results in the monitoring wells are above the
permit limits. However, these results remain consistent with previous results and most
results show decreases in concentration. The regional office has reviewed this data and
requested that DAK continue sampling per the permit.
No additional actions are planned at this time.
If additional information is needed, please feel free to contact either myself on 910-371-
5232 or Larry Young on 910-264-2564.
Sincerely yours, Ob
Pe C. Mahoney
Sustamability Director
DAK Americas LLC
DAK Americas LLC • 1205 Culbreth Drive, Suite 100 . Wilmington, NC 28405
910-371-4863(Phone) • 910-371-4456 (Fax)
www.dakamericas.com
Restricted Internal Use

GW-59A COMPLIANCE REPORT FORM Permit # "90 ��?
(Submit one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. ( Will this monitoring report (GW-59 and GW-59A)
be submitted after the established due date.
YES
2
Was any required information missing on the G`V-59 report forms?
YESto
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
YES
NO
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
s afi-� �Gv
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
same constituent(s) in the same well(s) in the last two years?
S
NO
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection` date for each occurrence (for the last two years).
C
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
S
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
groundwater quality problem?
YES
NO
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
�n e 1 e.4.s 64 S� �oO /e T e aeW
g
The person completing this portion (GVI--59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby ackn edge that the ab ve information was evaluated and the information submitted in this
report (C p ' nce ort GW- A) is ue and complete to the best of my knowledge.
Signa Permittee (or Authoriz en Date
NO
GNV-59A 12/8/2003

Parameter
Permit
Limit
Units
MW-2A
MW-21B
MW-2C
Dec-16
T Dec-19
Dec-16
12/16 Rspl
Jun-17
Dec-17
Dec-18
Dec-19
Dec-20
Dec-16
Dec-17
Dec-18
Dec-19
Dec-20
Ammonia Nitrogen
1.5
mg/I
12.0
82.5
83.5
47.9
84.3
37.9
53.5
32.9
Total Dissolved Solids
500
mg/I
827
509
632
673
727
800
692
753
588
597
568
504
Nitrate
10
mg/I
14.3
10.8
21.2
Arsenic
0.01
1 mg/I
0.017
1 0.02
0.02
Parameter
Permit
Limit
Units
MW-21D
MW-2E
Dec-16
12/16 Rspl
Jun-17
Dec-17
Dec-18
Dec-19
Dec-16
Dec-17
Dec-18
Dec-19 Dec-20
Ammonia Nitrogen
1.5
mg/l
157
12.8
96.4
142
80.5
45.8
9.5
11.0
8.5
<1.5 5.5
Total Dissolved Solids
500
mg/1
678
846
532
Restricted Internal Use

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
Permit Name (if different):
NPDES NC0000663 Other
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington (street) NC 28405
County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (State) (ZIP)
❑ Spray Field Remediation:
Contact Person: Larry Young
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down gradient/Monitoring Well # 2A No. of wells to be sampled: 6
❑ Water Source Heat Pump © Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2A
Date sample collected:
12/09/20
FIELD ANALYSES:
WAS
Well Depth: 13.0 ft.
Well Diameter:
2.0 in.
pH 6.64 units Temp. 17.5 °C
DRY at
time of
Depth to Water Level: 5.1 ft. below measuring point
Screened Interval:
3.0 ft. to 13.0 ft. Spec. Cond. µMhos
sampling,
Measuring Point is 1.92 ft. above land surface
Relative M.P. Elevation:
20.39 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ®
YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/11/20- 12/22/20
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NO2) as N
0.03 mg/l
Pb - Lead <0.010 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0,02 mg/l
Zn - Zinc <0.015 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
<0.04 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 243 mg/I
Al - Aluminum
mg/l
Cobalt - <0.010 mg/I
pH (when analyzed) 7.0 units
Ba - Barium
mg/I
Selenium - <0.010 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride 7 mg/l
Cd - Cadmium
<0.005 mg/I
Arsenic <0.010 mg/I
Chromium: Total
<0.010 mg/I
Grease and Oils mg/I
Cu - Copper
<0.010 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/l
VOC method # SM 6200B
Total Ammonia <0.2 mg/1
Mg - Magnesium
2.43 mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N 0.6 mg/I
Ni - Nickel
<0.010 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
(Date)
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0018087 Expiration Date: .tan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
NPDES NC0000663 Other
Permit Name (if different):
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington ('`feet) NC 28405 County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(Cay) (State) (zip)
❑ Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down gradient/Monitoring Well # 213 No. of wells to be sampled:
6
❑ Water Source Heat Pump 9 Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2B
Date sample collected: 12/08/20
FIELD ANALYSES:
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 6.6 units Temp. 19.6 °C
DRY at
Depth to Water Level: 6.5 ft. below measuring point
Screened Interval: 3 ft. to 13
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is 2•9 ft. above land surface
Relative M.P. Elevation:
24 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
15 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: 5d YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/08/20 - 12/18/20
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
0.04 mg/I
Pb - Lead <0.010 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0.02 mg/I
Zn - Zinc <0.010 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
0.47 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 692 mg/I
Al - Aluminum
mg/I
Cobalt - 0.029 mg/I
pH (when analyzed) 6.6 units
Ba - Barium
mg/I
Selenium - <0.010 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride 19 mg/I
Cd - Cadmium
<0.005 mg/I
Arsenic 0.02 mg/I
Chromium: Total
<0.010 mg/I
Grease and Oils mg/I
Cu - Copper
<0.010 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # SM 6200E
Total Ammonia 32•9 mg/I
Mg - Magnesium
8.59 mg/I
method #
(Ammonia Nitrogen, NH3as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N 31.1 mg/I
Ni - Nickel
<0.010 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
re of
(Date)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
eff,
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
I
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
Permit Name (if different):
NPDES NC0000663 Other
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmin ton (s1feet) NC 28405 County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (State) (Zip)
❑ Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
ElRotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down gradient/Monitoring Well # 2C No. of wells to be sampled:
6
❑ Water Source Heat Pump © Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2C
Date sample collected: 12/08/20
FIELD ANALYSES:
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 5.93 units Temp. 19.2 °C
DRY at
Depth to Water Level: 5.2 ft. below measuring point
Screened Interval: 3 ft. to 13
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is 3.05 ft. above land surface
Relative M.P. Elevation:
25 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
12 gallons
Appearance Light brown
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ® YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/08/20 - 12/18/20
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
0.23 mg/I
Pb - Lead <0.010 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
21.2 mg/I
Zn - Zinc 0.015 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
1.18 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 504 mg/I
Al - Aluminum
mg/I
Cobalt - 0.017 mg/I
pH (when analyzed) 6.3 units
Ba - Barium
mg/I
Selenium - <0.010 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride 7 mg/I
Cd - Cadmium
<0.005 mg/I
Arsenic <0.010 mg/I
Chromium: Total
0.014 mg/I
Grease and Oils mg/I
Cu - Copper
0.011 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # SM 6200B
Total Ammonia 0.3 mg/I
Mg - Magnesium
8.48 mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N 7.7 mg/I
Ni - Nickel
0.012 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
(or
(Date)
GW-59 Rev.1/2007

CI IMAIT FhRf`A r)N VFI 101A/ PAPFR r1Nl V
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
Permit Name (if different):
NPDES NC0000663 Other
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmin ton (Stfeet) NC 28405 County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(city) (state) (zip)
❑ Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down gradient/Monitoring Well # 2D No. of wells to be sampled:
6
❑ Water Source Heat Pump © Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2D
Date sample collected: 12/09/20
FIELD ANALYSES:
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 6.5 units Temp. 18.3 oC
DRY at
time
Depth to Water Level: 5.8 ft. below measuring point
Screened Interval: 3 ft. to 13 ft. Spec. Cond. µMhos
sampling,
Measuring Point is 3•0 ft. above land surface
Relative M.P. Elevation:
22 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
12 gallons
Appearance Slightly brown
here: ❑
Samples for metals were collected unfiltered: ®YES
ElNO and field acidified: ® YES
ElNO
LABORATORY INFORMATION
Date sample analyzed: 12/09/20 - 12/22/20
Laboratory Name: Envlrochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
0.07 mg/1
Pb - Lead <0.010 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0,02 mg/I
Zn - Zinc <0.010 mg/I
Coliform: MF Total /100e1
Phosphorus: Total as P
<0.04 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 275 mg/I
Al - Aluminum
mg/I
Cobalt - <0.010 mg/I
pH (when analyzed) 6.8 units
Ba - Barium
mg/I
Selenium - <0.010 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride 7 mg/I
Cd - Cadmium
<0.005 mg/I
Arsenic <0.010 mg/1
Chromium: Total
<0.010 mg/I
Grease and Oils mg/I
Cu - Copper
<0.010 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # SM 6200B
Total Ammonia 0.2 mg/I
Mg - Magnesium
2.57 mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N 42.5 mg/I
Ni - Nickel
<0.010 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
(or
(Date)
GW-59 Rev. 1/2007

RI IRMIT FORM ON YFI I nW PAPFR ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EMC617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly orType
PERMIT Number: WQ0018087 Expiration Date: Jan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
Permit Name (if different):
NPDES NC0000663 Other
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington (Street) NC 28405 County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(city) (state) (zip)
❑ Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Down gradient/Monitoring Well # 2E No. of wells to be sampled:
6
❑ Water Source Heat Pump ® Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2E
Date sample collected: 12/08/20
FIELD ANALYSES:
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 5.85 units Temp. 16.6 oC
DRY at
time of
Depth to Water Level: 7.75 ft. below measuring point
Screened Interval: 3 ft. to 13 ft. Spec. Cond. µ Mhos
sampling,
Measuring Point is 3•0 ft. above land surface
Relative M.P. Elevation:
23 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
15 gallons
Appearance Slightly brown
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ® YES
❑ NO
LABORATORY ATORY INFORMATION
Date sample analyzed: 12/08/20 - 12/18/20
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
0.07 mg/I
Pb - Lead <0.010 mg/l
Coliform: MF Fecal /100ml
Nitrate (Nos) as N
<0,02 mg/I
Zn - Zinc 0.011 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
0.39 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 136 mg/I
Al - Aluminum
mg/I
Cobalt - <0.010 mg/1
pH (when analyzed) 6.1 units
Ba - Barium
mg/I
Selenium - <0.010 mg/1
TOG mg/I
Ca - Calcium
mg/I
Chloride 7 mg/I
Cd - Cadmium
<0.005 mg/I
Arsenic <0.010 mg/I
Chromium: Total
<0.010 mg/I
Grease and Oils mg/I
Cu - Copper
<0.010 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # SM 6200E
Total Ammonia 5.5 mg/I
Mg - Magnesium
1.24 mg/I
method #
(Ammonia Nitrogen: NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
, method #
TKN as N 6•5 mg/I
Ni - Nickel
<0.010 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOL; Removal io
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
ittee
(Date)
GW-59 Rev.1/2007

CI IRRAIT Fnpm ON YFI I OW PAPFR ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQo018087 Expiration Date: .tan. 31, 2021
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge UIC
NPDES NC0000663 Other
Permit Name (if different):
Facility Address: 1205 Culbreth Drive, Suite 100
TYPE OF PERMITTED OPERATION BEING MONITORED
Wllmin ton (ytfeet) NC 28405 County Brunswick
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (stete) (zip)
❑ Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Background/Monitoring Well # 3A No. of wells to be sampled: 6
❑ Water Source Heat Pump ® Other: Surface Disposal Res.Sol
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 3A
Date sample collected:
12/09/20
FIELD ANALYSES:
WAS
Well Depth: 13.25 ft.
Well Diameter:
2.0 in.
pH 6.1 units Temp. 18.1 °C
DRY at
time ofsampling,
Depth to Water Level: 2.1 ft. below measuring point
Screened Interval:
3.25 ft. to 13.3 ft. Spec. Cond. µMhos
Measuring Point is 1.76 ft. above land surface
Relative M.P. Elevation:
24.78 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/09/20 - 12/22/20
Laboratory Name: Envlrochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
<0.02 mg/I
Pb - Lead <0.01 mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0,02 mg/1
Zn - Zinc <0.01 mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
<0.04 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 84 mg/I
Al - Aluminum
mg/I
Cobalt - <0.01 mg/I
pH (when analyzed) 6.3 units
Ba - Barium
mg/I
Selenium - <0.01 mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride 7 mg/I
Cd - Cadmium
<0.005 mg/I
Arsenic <0.01 mg/I
Chromium: Total
<0.01 mg/I
Grease and Oils mg/I
Cu - Copper
<0.01 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
<0.0002 mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 6200B
Total Ammonia <0•2 mg/I
Mg - Magnesium
0.879 mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N 0.6 mg/I
Ni - Nickel
<0.01 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Aqent) Name and Title - Please print or type
(Date)
GW-59 Rev.1/2007

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
cm, 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Date of Report: Dec 22, 2020
Customer PO M
Customer ID: 08100044
Report M 2020-20858
Project ID: Monitoring Well
Lab ID Sample ID:
20-53076 Site: MW-2A
Test
Collect Date/Time
12/9/2020 11:15 AM
Method
Matrix Sampled by
Water Larry Young
Results Date Analyzed
Arsenic
EPA 200.7
<0.010mg/L
12/11/2020
Chromium
EPA 200.7
<0.010mg/L
12/11/2020
Cobalt
EPA 200.7
<0.010 mg/L
12/11/2020
Copper
EPA 200.7
<0.010mg/L
12/11/2020
Lead
EPA 200.7
<0.010 mg/L
12/11/2020
Magnesium
EPA 200.7
2.43mg/L
12/11/2020
Nickel
EPA 200.7
<0.010mg/L
12/11/2020
Selenium
EPA 200.7
<0.010mg/L
12/11/2020
Zinc
EPA 200.7
0.015 mg/L
12/11/2020
Cadmium
EPA200.8
<0.005mg/L
12/15/2020
Mercury
EPA 245.1
<0.0002 mg/L
12/10/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
12/17/2020
Total Dissolved Solids (TDS)
SM 2540 C
243 mg/L
12/09/2020
Chloride
SM 4500 CI E
7 mg/L
12/18/2020
pH
SM 4500 H B
7.0 units
12/09/2020
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/18/2020
1, 1, 1,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12111 /2020
1,1,1-Trichloroethane
SM 6200B
<0.5pg/L
12/11/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5pg/L
12/11/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
12111 /2020
1, 1 -Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
1,2, 3-Trichlorobenzene
SM 62008
<0.5 pg/L
12/11/2020
1,2, 3-Trichloropropane
SM 5200B
<0.5 pg/L
12/11/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report #:: 2020-20858 Page 1 of 9

DAK Americas
Date of Report: Dec 22, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20858
Project ID: Monitoring Well
1, 2,4-Trimethyl benzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5pg/L
12/11/2020
1,2-Dibromoethane
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,3-Dichloropropane
SM 82008
<0.5 pg/L
12/11/2020
1,4-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/11/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
12/11/2020
Benzene
SM 6200B
<0.5 pg/L
12/11/2020
Bromobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Bromochloro methane
SM 6200B
<0.5 pg/L
12/11/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Bromoform
SM 6200B
<0.5 pg/L
12/11/2020
Bromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
12/11/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/11/2020
Chloroform
SM 6200B
<0.5 pg/L
12/11/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/11/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
cis-1, 3-Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Dibromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Ethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report #:: 2020-20858 Page 2 of 9

ti`envirochem
ri
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 22, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20858
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
12/11/2020
Isopropylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
M+P Xylene
SM 8200B
<1.0 pg/L
12/11/2020
Methylene chloride
SM 62008
<0.5 pg/L
12/11/2020
Naphthalene
SM 6200B
<0.5 pg/L
12/11/2020
n-Butylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
12/11/2020
p-Isopropyltoluene
SM 6200B
<0.5 pg/L
12/11/2020
sec-Butylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Styrene
SM 6200B
<0.5 pg/L
12/11/2020
tert-Butyl benzene
SM 6200B
<0.5 pg/L
12/11/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Toluene
SM 62008
<0.5 pg/L
12/11/2020
Trans-1 ,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5pg/L
12/11/2020
Trichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
12/11/2020
Nitrate Nitrogen (Caic)
Nitrite Nitrogen EPA 353.2
0.03 mg/L
12/10/2020
Nitrate+Nitrite-Nitrogen EPA353.2
< 0.02 mg/L
12/14/2020
Nitrate Nitrogen Subtraction Method
<0.02 mg/L
12/22/2020
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN) EPA351.2
0.6mg/L
12/18/2020
Total Nitrogen Total Nitrogen
0.6 mg/L
12/22/2020
Report #: 2020-20858 Page 3 of 9

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO: O- O
ADDRESS:
CONTACT NAME:
PO NO:
/oa
REPORT TO: rt- , o
PHONE/FAX: ---5
COPY TO:
email:,/VA rr cm
Sampled By: it : ov i L ,,%Wb%�AMPLE TYPE: I = Influent, E = EffluenfQW�- Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Coll ction
a
F
"
Z!
N t`0
i; c�
o o
"
_
C C7
:° `o
V a
G=
o rn
c) E
�,
p
w
x
a
O W
m g
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z-
z
x
0
N
x
0
=
0
Z
0Uj
�
0
H
LL
w
N
o
17
C
P
of
C
P
_
p
G
GL
C
4.
—(U
G
C
P
Y.
9-z /
r 77
G
c
tr
C- Z-
G
C
P
G
G
C
P
G
G
C
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or less) In the field at the time of collection. See reverse for Instructions
Transfer
linquished By:
Date/Time
Received By:
Date/Time
1.
—y - 2-0 ZOE.
2.
45

_116•' : rFr ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
/a a
REPORT TO: rr o
PH0NE/FAX: _-:2-5'4
AIC U
COPY TO:
email:
Sampled By: Y ovS i` i/rlatoAMPLE TYPE: I = Influent, E = Effluen W� Well. ST = Stream. SO = Soil. SL = Sludge. Other:
Sample Identification
Coll ction
a
I.-
°'
E
`°
m
W'd
06
o$
"
Ci;
9 `o
o a
"
C_
`o 6
v E
m
o
.°
o
a
oW
m 0°
g
Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
w
p
Z
�
=
ao
N
=
�
z
=
x
a
z
o
xLu
~
o
W.
a
w
►_-
O
t
C
P
L
G
G
C
G
C
P
V
g
G
G
C
P
G
G
C
P
G
G
C
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinaled (0.5 ppm or less) In the field at the time of collection. See reverse for instructions
Transfer
Relinquished By:
DatelTime,
Received By:
Date/Time
2.
Temperature
Delivered By
Comments:
G:_ v "a, C-= Accepted:
(C::, rs -Ior
_Time:
ND:

SM'
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 19, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20741
Project ID: Monitoring Well
Lab ID Sample ID:
20-52794 Site: MW-2B
Test
Collect Date/Time
12/8/2020 12:30 PM
Method
Matrix Sampled by
Water Young/Simmons
Results Date Analyzed
Arsenic
EPA 200.7
0.02mg/L
12/11/2020
Chromium
EPA 200.7
<0.010mg/L
12/11/2020
Cobalt
EPA 200.7
0.029 mg/L
12/11/2020
Copper
EPA 200.7
<0.010 mg/L
12/11/2020
Lead
EPA 200.7
<0.010 mg/L
12/11/2020
Magnesium
EPA 200.7
8.59mg/L
12/11/2020
Nickel
EPA 200.7
<0.010 mg/L
12/11/2020
Selenium
EPA 200.7
<0.010mg/L
12/11/2020
Zinc
EPA 200.7
<0.010 mg/L
12/11/2020
Cadmium
EPA200.8
<0.005mg/L
12/15/2020
Mercury
EPA245.1
<0.0002mg/L
12/10/2020
Ammonia Nitrogen
EPA350.1
32.9mg/L
12/14/2020
Total Dissolved Solids (TDS)
SM 2540 C
692 mg/L
12/09/2020
Chloride
SM 4500 CI E
19 mg/L
12/17/2020
pH
SM 4500 H B
6.6 units
12/09/2020
Total Phosphorus
SM 4500 P f
0.47 mg/L
12/16/2020
1,1,1,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1, 1, 1-Trichloroethane
SM 8200E
<0.5 pg/L
12/09/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5 ug/L
12/09/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
1, 1 -Dichloropropene
SM 6200B
<0.5 pg/L
12/09/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2,3-Trichloropropane
SM 62008
<0.5 pg/L
12/09/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Report #:: 2020-20741 Page 1 of 9

DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 19, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20741
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dibromoethane
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dichloroethane
SM e2ooB
<0.5 pg/L
12/09/2020
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,4-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
2,2-Dichloropropane
SM e200B
<0.5 pg/L
12/09/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/09/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
12/09/2020
Benzene
SM 6200B
<0.5 pg/L
12/09/2020
Bromobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Bromoform
SM 6200B
<0.5 pg/L
12/09/2020
Bromomethane
SM 6200B
<0.5 pg/L
12/09/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
12/09/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/09/2020
Chloroform
SM 6200B
<0.5 pg/L
12/09/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/09/2020
cis- 1, 2-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
cis-1,3-Dichloropropene
SM 6200B
<0.5 pg/L
12/09/2020
Dibromochloromethane
SM e2ooB
<0.5 pg/L
12/09/2020
Dibromomethane
SM 6200B
<0.5 pg/L
12/09/2020
Dichlorodifluoromethane
SM e200B
<0.5 pg/L
12/09/2020
Ethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Report #:: 2020-20741
Page 2 of 9

:enviroche mr]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Dec 19, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20741
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
12/09/2020
Isopropylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
M+P Xylene
SM 6200B
<1.0 pg/L
12/09/2020
Methylene chloride
SM 62008
<0.5 pg/L
12/09/2020
Naphthalene
SM 6200B
<0.5 pg/L
12/09/2020
n-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
12/09/2020
p-Isopropyltoluene
SM 6200B
<0.5 pg/L
12/09/2020
sec-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Styrene
SM 6200B
<0.5 pg/L
12/09/2020
tert-Butyl benzene
SM 62008
<0.5 pg/L
12/09/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Toluene
SM 6200B
<0.5 pg/L
12/09/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5 pg/L
12/09/2020
Trichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/09/2020
Vinyl chloride
SM 62008
<0.5 pg/L
12/09/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2
0.04 mg/L
12/08/2020
Nitrate+Nitrite-Nitrogen EPA353.2
<0.02mg/L
12/11/2020
Nitrate Nitrogen Subtraction Method
<0.02mg/L
12/18/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA351.2
31.1 mg/L
12/16/2020
Total Nitrogen Total Nitrogen
31.1 mg/L
12/18/2020
Report #: 2020-20741 Page 3 of 9

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Date of Report: Dec 19, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20741
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-52795 Site: MW-2C
12/8/2020 11:39 AM Water Young/Simmons
Test
Method
Results
Date Analyzed
Arsenic
EPA 200.7
<0.010 mg/L
12/11/2020
Chromium
EPA 200.7
0.014 mg/L
12/11/2020
Cobalt
EPA 200.7
0.017 mg/L
12/11/2020
Copper
EPA 200.7
0.011 mg/L
12/11/2020
Lead
EPA 200.7
<0.010 mg/L
12111 /2020
Magnesium
EPA 200.7
8.48 mg/L
12/11/2020
Nickel
EPA 200.7
0.012mg/L
12/11/2020
Selenium
EPA 200.7
<0.010 mg/L
12/11/2020
Zinc
EPA 200.7
0.015 mg/L
12/11/2020
Cadmium
EPA200.8
<0.005mg/L
12/15/2020
Mercury
EPA 245.1
<0.0002 mg/L
12/10/2020
Ammonia Nitrogen
EPA350.1
0.3mg/L
12/14/2020
Total Dissolved Solids (TDS)
SM 2540 c
504 mg/L
12/09/2020
Chloride
SM 4500 CI E
7 mg/L
12/17/2020
pH
SM 4500 H B
6.3 units
12/09/2020
Total Phosphorus
SM 4500 P F
1.18 mg/L
12/16/2020
1, 1, 1,2-Tetrachloroethane
SM 52008
<0.5 pg/L
12/09/2020
1, 1, 1 -Trichloroethane
SM e200B
<0.5 pg/L
12/09/2020
1,1,2,2-Tetrachloroethane
SM 62008
<0.5 pg/L
12/09/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1-Dichloroethene
SM 62008
<0.5 pg/L
12/09/2020
1,1-Dichloropropene
SM 6200B
<0.5 pg/L
12/09/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2,3-Trichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,2,4-Trichlorobenzene
SM 5200B
<0.5 pg/L
12/09/2020
ReportV 2020-20741 Page 4 of 9

r- - - 76� -7 -7
envirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info(a environmentalchemists.com
Date of Report: Dec 19, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20741
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dibromoethane
SM 62008
<0.5 pg/L
12/09/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichloropropane
SM 62008
<0.5 pg/L
12/09/2020
1,4-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/09/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
12/09/2020
Benzene
SM 6200B
<0.5 pg/L
12/09/2020
Bromobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Bromoform
SM 6200B
<0.5 pg/L
12/09/2020
Bromomethane
SM 6200B
<0.5 pg/L
12/09/2020
Carbon tetrachloride
SM 62008
<0.5 pg/L
12/09/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/09/2020
Chloroform
SM 6200B
<0.5 pg/L
12/09/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/09/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
cis-1,3-Dichloropropene
SM 6200B
<0.5 pg/L
12/09/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Dibromomethane
SM 6200B
<0.5 pg/L
12/09/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
12/09/2020
Ethylbenzene
SM 62008
<0.5 pg/L
12/09/2020
Report #:: 2020-20741
Page 5 of 9

Eenvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoC environmentalchemists.com
DAK Americas
Date of Report: Dec 21, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20741
Project ID: Monitoring Well
Hexachlorobutadiene
SM 62008
<0.5 pg/L
12/09/2020
Isopropylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
M+P Xylene
SM 6200B
<1.0 pg/L
12/09/2020
Methylene chloride
SM 6200B
<0.5 pg/L
12/09/2020
Naphthalene
SM 62008
<0.5 pg/L
12/09/2020
n-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
12/09/2020
p-Isopropyltoluene
SM 6200B
<0.5 pg/L
12/09/2020
sec-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Styrene
SM 6200B
<0.5 pg/L
12/09/2020
tert-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Toluene
SM 62008
<0.5 pg/L
12/09/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5pg/L
12/09/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5pg/L
12/09/2020
Trichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/09/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
12/09/2020
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA 353 2
0.23 mg/L
12/08/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
21.4 mg/L
12/15/2020
Nitrate Nitrogen
Subtraction Method
21.2 mg/L
12/18/2020
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
7.7 mg/L
12/16/2020
Total Nitrogen
Total Nitrogen
29.1 mg/L
12/18/2020
Report # 2020-20741 Page 6 of 9

- • 6, 19 ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
/Od
REPORT TO: 4o9rrV /f/, Y4
PHONE/FAX: D
' AI C- 8 p
COPY TO:
email• er
Sampled By: f .41, o,A-'fS a iA/btP!�%AMPLE TYPE: I = Influent, E = Effluen W Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a
F
°_'
E CL
N
O N
oo. t9
o o
"
_
C C7
° `o
° a
" V
C J
o �
u E
d
8
'
o
a
W
m �
g z
Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
d
Z
�
i
p
N
=
0
z
oz
¢_
Z
p
~
O
�
��
LL
W
°
C
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CQ I
G
C
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C
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/r/30
G
G
c
C-- L TD s kI;.
3
C
P
G
G
C
P
G
G
C
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechiorinated (0.5 ppm or less) In the field at the time of collection. See reverse for Instructions
Transfer
Relinquished By.
Date/Time
Received By:
DatelTime
2.
Temperature w e ceived 'C: l '
Delivered By. �—
Comments:
0
Zg
By: c<<
ple,Re nested:
? ' 4 r Time: ;L -' ZGPO/--
TURNAROUND:

Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM; 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
1205 Cuibreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Date of Report: Dec 22, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20858
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-53077 Site: MW-2D
12/9/2020 10:27 AM Water Larry Young
Test
Method
Results Date Analyzed
Arsenic
EPA200,7
<0.010mg/L
12/11/2020
Chromium
EPA 200.7
<0.010mg/L
12/11/2020
Cobalt
EPA 200.7
<0.010 mg/L
12/11/2020
Copper
EPA 200.7
<0.010 mg/L
12/11/2020
Lead
EPA 200.7
<0.010 mg/L
12/11/2020
Magnesium
EPA 200.7
2.57 mg/L
12/11/2020
Nickel
EPA 200.7
<0.010 mg/L
12/11/2020
Selenium
EPA 200.7
<0.010 mg/L
12/11/2020
Zinc
EPA 200.7
<0.010mg/L
12/11/2020
Cadmium
EPA 200.8
<0.005 mg/L
12/15/2020
Mercury
EPA 245.1
<0.0002 mg/L
12/10/2020
Ammonia Nitrogen
EPA350.1
0.2mg/L
12/17/2020
Total Dissolved Solids (TDS)
SM 2540 C
275 mg/L
12/09/2020
Chloride
SM 4500 ci E
7 mg/L
12/18/2020
pH
SM 4500 H B
6.8 units
12/09/2020
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/18/2020
1, 1, 1,2-Tetrachloroethane
SM 6200B
<0.5pg/L
12/11/2020
1, 1, 1 -Trichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12111 /2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2, 3-Trichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report #.: 2020-20858 Page 4 of 9

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ^ 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ^ 252.473.5702 Lab/Fax
L
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas Date of Report: Dec 22, 2020
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report #: 2020-20858
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dibromo-3-CInloropropane
SM 6200B
<0.5pg/L
12/11/2020
1,2-Dibromoethane
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
12111 /2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,3-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
1,4-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/11/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
12/11/2020
Benzene
SM 6200B
<0.5 pg/L
12/11/2020
Bromobenzene
SM 62008
<0.5 pg/L
12/11/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Bromoform
SM 6200B
<0.5 pg/L
12/11/2020
Bromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
12/11/2020
Chlorobenzene
SM 6200E
<0.5 pg/L
12/11/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/11/2020
Chloroform
SM 6200B
<0.5 pg/L
12/11/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/11/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
cis-1,3-Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Dibromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Ethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report # : 2020-20858
Page 5 of 9

:envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Dec 22, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20858
Project ID: Monitoring Well
Hexachlorobutad iene
SM 62008
<0.5 pg/L
12111 /2020
Isopropylbenzene
SM 6200E
<0.5 pg/L
12/11/2020
M+P Xylene
SM 6200E
<1.0 pg/L
12/11/2020
Methylene chloride
SM 6200B
<0.5 pg/L
12/11/2020
Naphthalene
SM 6200B
<0.5 pg/L
12/11/2020
n-Butlbenzene
SM 6200B
<0.5 pg/L
12/11/2020
n-Propylbenzene
SM 6200B
<0.5 Ng/L
12/11/2020
ortho-Xylene
SM 62008
<0.5 pg/L
12/11/2020
p-Isopropyltoluene
SM 6200B
<0.5 pg/L
12/11/2020
sec-Burylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Styrene
SM 62008
<0.5 pg/L
12/11/2020
tert-Burylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Toluene
SM 6200B
<0.5 Ng/L
12/11/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5pg/L
12/11/2020
Trichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
12/11/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2
0.07 mg/L
12/10/2020
Nitrate+Nitrite-Nitrogen EPA 353.2
< 0.02 mg/L
12/14/2020
Nitrate Nitrogen Subtraction Method
<0.02 mg/L
12/22/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA351 2
42.5mg/L
12/18/2020
Total Nitrogen Total Nitrogen
42.5 mg/L
12/22/2020
Report #:: 2020-20858 Page 6 of 9

ENVIRONMENTAL CHEMISTS, INC
Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
rni 1 FC_TIr1Al Arin r`uAiAi nc r`I Ic-rnnv
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO: Q— c0o 856
ADDRESS: Dx;-
CONTACT NAME:
PO NO:
REPORT TO: rr , o
PHONE/FAX: Q — � � iZ _ -:7-5`4 -�l
t ' j AIC-
I COPY TO:
email:
SamDled Bv: /(� Vo"A.YS- �,-,&fmbLmAMPI F TVPF• I = Infinnn4 P _ GfFl..- A ' tA►—!! cT — C4. en — —
Sample Identification
Coll ction
a
H
a
A
m
W la`0
a
U o
_
C CJ
o
t) a
C J
o m
U E
m
O
A
x
a
W
m
g Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
Z
x
o
N
=
0
=
0
Z
o
Cl
z
F
LL
w
Fx
O
C
P
G
GL
C
s
>/
<
G
C
P
Y
G
G
C
P
G
G
C
P
G
G
C
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or less) In the field at the time of collection. See reverse for Instructions
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
z.
Delivered By:eL�2
Comments: PA
��� .+• t . 1 /1l.GGIJIC.U. Ke�ecteu: KesarTipie
Received By: Date:_
Time: '3 7
D:

[envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 < 910.347.5843 Lab/Fax
infoCa-environmentalchemists.com
DAK Americas Date of Report: Dec 19, 2020
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report #: 2020-20741
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-52796 Site: MW-2E 12/8/2020 10:36 AM Water Young/Simmons
Test Method Results Date Analyzed
Arsenic
EPA 200.7
<0.010mg/L
12/11/2020
Chromium
EPA200.7
<0.010mg/L
12/11/2020
Cobalt
EPA 200.7
<0.010 mg/L
12/11/2020
Copper
EPA 200.7
<0.010 mg/L
12/11/2020
Lead
EPA 200.7
<0.010 mg/L
12/11/2020
Magnesium
EPA 200.7
1.24mg/L
12/11/2020
Nickel
EPA 200.7
<0.010mg/L
12/11/2020
Selenium
EPA 200.7
<0.010mg/L
12/11/2020
Zinc
EPA 2007
0.011 mg/L
12/11/2020
Cadmium
EPA 200.8
<0.005 mg/L
12/15/2020
Mercury
EPA 245.1
<0.0002 mg/L
12/10/2020
Ammonia Nitrogen
EPA 350.1
5.5 mg/L
12/14/2020
Total Dissolved Solids (TDS)
SM 2540 c
136 mg/L
12/09/2020
Chloride
SM 4500 CI E
7 mg/L
12/17/2020
pH
SM 4500 H B
6.1 units
12/09/2020
Total Phosphorus
SM 4500 P F
0.39 mg/L
12/16/2020
1, 1, 1,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1,1-Trichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
12/09/2020
1, 1 -Dichloroethene
SM e2008
<0.5 pg/L
12/09/2020
1,1-Dichloropropene
SM e200B
<0.5 pg/L
12/09/2020
1,2,3-Trichlorobenzene
SM 5200B
<0.5 pg/L
12/09/2020
1,2,3-Trichloropropane
SM 62008
<0.5 pg/L
12/09/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Report #:: 2020-20741 Page 7 of 9

Environmental Chemists, Inc.
envitrochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(denvironmentalchemists.com
DAK Americas
Date of Report: Dec 19, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20741
Project ID: Monitoring Well
1, 2,4-Trimethyl benzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dibromo-3-Chloropropane
SM 8200B
<0.5 pg/L
12/09/2020
1,2-Dibromoethane
SM 62008
<0.5 pg/L
12/09/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,2-Dichloroethane
SM 62008
<0.5 pg/L
12/09/2020
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
1,3-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
1,4-Dichlorobenzene
SM 62008
<0.5 pg/L
12/09/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/09/2020
4-Chlorotoluene
SM 62DOB
<0.5 pg/L
12/09/2020
Benzene
SM 6200B
<0.5 pg/L
12/09/2020
Bromobenzene
SM 62008
<0.5 pg/L
12/09/2020
Bromochloromethane
SM 6200E
<0.5 pg/L
12/09/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/09/2020
Bromoform
SM 5200B
<0.5 pg/L
12/09/2020
Bromomethane
SM 8200B
<0.5 iJg/L
12/09/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
12/09/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
12/09/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/09/2020
Chloroform
SM 6200B
<0.5 pg/L
12/09/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/09/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
cis- 1,3-Dichloropropane
SM 6200B
<0.5 pg/L
12/09/2020
Dibromochloromethane
SM 62008
<0.5 pg/L
12/09/2020
Dibromomethane
SM 62008
<0.5 pg/L
12/09/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
12/09/2020
Ethylbenzene
SM 62DOB
<0.5 pg/L
12/09/2020
Report #.: 202D-20741
Page 8 of 9

Environmental Chemists, Inc.
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmentalchemists.com
DAK Americas
Date of Report: Dec 19, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20741
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
12/09/2020
Isopropylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
M+P Xylene
SM 6200B
<1.0 pg/L
12/09/2020
Methylene chloride
SM 6200B
<0.5 pg/L
12/09/2020
Naphthalene
SM 6200B
<0.5 pg/L
12/09/2020
n-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
n-Propylbenzene
SM 52006
<0.5 pg/L
12/09/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
12/09/2020
p-Isopropyltoluene
SM 6200B
<0.5 pg/L
12/09/2020
sec-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Styrene
SM 6200B
<0.5 pg/L
12/09/2020
tert-Butylbenzene
SM 6200B
<0.5 pg/L
12/09/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Toluene
SM 6200B
<0.5 pg/L
12/09/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Trans-1,3-dichloropropene
SM 62008
<0.5 pg/L
12/09/2020
Trichloroethene
SM 6200B
<0.5 pg/L
12/09/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/09/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
12/09/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2
0.07 mg/L
12/08/2020
Nitrate+Nitrite-Nitrogen EPA353.2
0.03mg/L
12/11/2020
Nitrate Nitrogen Subtraction Method
<0.02 mg/L
12/18/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA351.2
6.5mg/L
12/16/2020
Total Nitrogen Total Nitrogen
6.5 mg/L
12/18/2020
Comment:
Reviewed by: EAU, \Ihnhr�j
Report #. 2020-20741 Page 9 of 9

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 3T729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO:
ADDRESS: p Y�
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX: D —.2 -.254
' AIC_ a'1p
COPY TO:
email: C
Sampled B r '. YovAWiA1ota_05AMPLE TYPE: I = Influent, E = Effluen W} Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Coli ction
0
o
s
a A
E t7
c 0
`o
c_
s E
m
o
c
o_ w
m
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
0
0
0
o
o
W
LL
o
C
P
t7r`IL��
��oo V
C
CP
�� l/4 L _
03 a
G
G
C
0 3-07
G
C
P
�7T
aS
G
G
C
o
G
C
P
G
G
C
P
G
G
C
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be deddorinated (0.5 ppm or less) in the field at the time of collection. See reverse for instructions
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
2.
Temperature when R ived `C:_
Delivered By: �-
Comments:
b
By:
Resample "uested:
_Date: ldI51-.' Time:
-�-% RF_SJ.GT S-, X6 TURNAROUND:

envirochem
6�L7
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
info;a environmentalchemists.com
Date of Report: Dec 22, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20858
Project ID: Monitoring Well
Lab ID Sample ID:
20-53078 Site: MW-3A
Test
Collect Date/Time
12/9/2020 12:11 PM
Method
Matrix Sampled by
Water Larry Young
Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L
12/15/2020
Chromium
EPA 200.7
<0.01 mg/L
12/15/2020
Cobalt
EPA 200.7
<0.01 mg/L
12/15/2020
Copper
EPA 200.7
<0.01 mg/L
12/15/2020
Lead
EPA 200.7
<0.01 mg/L
12/15/2020
Magnesium
EPA 200.7
0.879 mg/L
12/15/2020
Nickel
EPA 200.7
<0.01 mg/L
12/15/2020
Selenium
EPA 200.7
<0.01 mg/L
12/15/2020
Zinc
EPA 200.7
<0.01 mg/L
12/15/2020
Cadmium
EPA 200.8
<0.005 mg/L
12/15/2020
Mercury
EPA 245.1
<0.0002 mg/L
12/10/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
12/17/2020
Total Dissolved Solids (TDS)
SM 2540 c
84 mg/L
12/09/2020
Chloride
SM 4500 CI E
7 mg/L
12/18/2020
pH
SM 4500 H B
6.3 units
12/09/2020
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/18/2020
1,1,1,2-Tetrachloroethane
SM 6200B
<0.5pg/L
12/11/2020
1,1,1-Trichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1, 1 -Dichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,1-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
1, 1 -Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
1,2,3-Trichlorobe nzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2,3-Trichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report #: 2020-20858 Page 7 of 9

E-nvircooche7.1�.
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 22, 2020
Customer PO #:
Customer ID: 08100044
Report #: 2020-20858
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM e200B
<0.5 pg/L
12/11/2020
1,2-Dibromo-3-Chloropropane
SM 8200B
<0.5 pg/L
12/11/2020
1,2-Dibromoethane
SM 62008
<0.5 pg/L
12/11/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloroethane
SM 6200B
<0.5 pg/L
12/11/2020
1,2-Dichloropropane
SM e200B
<0.5 pg/L
12/11/2020
1,3, 5-Trimethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
1, 3-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
1,4-Dichlorobenzene
SM 62008
<0.5 pg/L
12/11/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
12/11/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
12/11/2020
4-Chlorotoluene
SM 62008
<0.5 pg/L
12/11/2020
Benzene
SM 6200B
<0.5 pg/L
12/11/2020
Bromobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Bromoform
SM 8200B
<0.5 pg/L
12/11/2020
Bromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
12/11/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
12/11/2020
Chloroethane
SM 6200B
<0.5 pg/L
12/11/2020
Chloroform
SM 6200B
<0.5 pg/L
12/11/2020
Chloromethane
SM 6200B
<0.5 pg/L
12/11/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
cis-1,3-Dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
12/11/2020
Dibromomethane
SM 6200B
<0.5 pg/L
12/11/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Ethylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
Report M. 2020-20858
Page 8 of 9

==envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Dec 22, 2020
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2020-20858
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
12/11/2020
Isopropyl benzene
SM 6200B
<0.5 pg/L
12/11/2020
M+P Xylene
SM 6200B
<1.0 pg/L
12/11/2020
Methylene chloride
SM 8200B
<0.5 pg/L
12/11/2020
Naphthalene
SM 82008
<0.5 pg/L
12/11/2020
n-Butylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
12/11/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
12/11/2020
p-Isopropyltoluene
SM 8200B
<0.5 pg/L
12/11/2020
sec -Butyl benzene
SM 6200B
<0.5 pg/L
12/11/2020
Styrene
SM 6200B
<0.5 pg/L
12/11/2020
tert-Butylbenzene
SM 6200e
<0.5 Ng/L
12/11/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Toluene
SM 6200B
<0.5 pg/L
12/11/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
12/11/2020
Trans- 1, 3-dichloropropene
SM 6200B
<0.5 pg/L
12/11/2020
Trichloroethene
SM 6200B
<0.5 Ng/L
12/11/2020
Trichlorofluoromethane
SM 6200B
<0.5 pg/L
12/11/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
12/11/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2
< 0.02 mg/L
12/1 U/2U2U
Nitrate+Nitrite-Nitrogen EPA 353.2
< 0.02 mg/L
12/14/2020
Nitrate Nitrogen Subtraction Method
<0.02 mg/L
12/22/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2
0.6 mg/L
12/18/2020
Total Nitrogen Total Nitrogen
0.6 mg/L
12/22/2020
Comment: nn
Reviewed by: V
Report #:: 2020-20858 Page 9 of 9

ENVIRONMENTAL CHEMISTS, INC
Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: D
PROJECT NAME:
REPORT NO:02 D - C20
ADDRESS:
CONTACT NAME:
PO NO:
�; ,-- loE,
REPORT TO: rr , o
PHONE/FAX:
AIC— p
COPY TO:
email: Pr Cm
Sampled By: Al. oVA W i` Siirlat AMPLE TYPE: I = Influent. E = Effluen Wi- Well. ST =Stream. SO = Soil. SL = Sludae. Other:
Sample Identification
Coll ction
a
IT
d
a
N
m
u/ N
a s
E
� o
_
C L7
� g
o o
0
9 J
5 m
]= E
t�
O
�
`o
a
w
m 0°
g
Z
PRESERVATION
V
ANALYSIS REQUESTED
Date
Time
Temp
w
z
�
�
x
0
a
i
0
Z
x
x
a
z
g
x
►-
O
w
w
.��
LL
w
x
O
Al L1 �
l ,Pl
[k`
C
or�
.�.o
Y'
�' _
CP � oo c ,
a
�
C
P
0
G
GL
C
d
G
C
P
V'
�
�
G
G
f
c
C-L
G
C
P
G
G
C
P
G
G
C
P
ITI
I
I
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or less) in the field at the time of collection. See reverse for Instructions
Transfer
elinquished By:
Date/Time
Received By.
Date/Time
1.
-L�
2.
Temperature whe eived °C:
Delivered B
Comments: _ fz�V i - 7
0
By:
Resarn I Re uested:
DateJJ /Z 2-O Timer '3"]
'!L r TURNAROUND: