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HomeMy WebLinkAboutWQ0016376_Monitoring - 09-2020_20210129FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page _J_ of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: September Year: 2020 PPI: 001 Flow Measuring Point: ❑ tnfluent 2 Effluent ❑ No flow generated Parameter Monitoring Point: ❑ tnfluent 0 Effluent _1 Groundwater Lowering ❑ Surface water Parameter Code —► 00310 tf� 50060 t 00610 00620 00400 0Q8 70300 Qt?53t? `_�� C O 2 cr a R d p a S ~ cc U F tt µ S „ CC rZn " " .� 1 --mg!L 24-hr hrs GPD mg/L mg1L mglL 11100 9nL�� mg/L mg/L m / su rnr�IL mg/L rngtL� 1 07:00 10 91,130 _. _� 2 07:00 10 88,920 i 3 07:00 10 91 0a0 4 07:00 10�- 5 07:00 2 88120 6 7 00:00 00:00 0 0 20,000_�1--- 20,000- 8 9 10 07:00 07:00 07:00 10 10 10 79,890 ' 81.790 91.870 ! ` I ?- 13 t 11 07:00 10 SS,C� 12 07:00 4 79.220.._- -- _-- - v_ 131 00:00 0 20,000 141 07:00 10 80.7,110 10 8120 15 07:00 16 17 07:00 07:00 10 10 85,720 100710 _ -.--- 18 07:00 10 79,320 ❑_.v 19 07:00 10 go .q �- 201 00:00 0 20.000- - {-- 21 22 07:00 07:00 10 10 87.810 79,120 -} - - 23 07:00 10 80,100 i 48 i. 290001 70 j i 0.09 70,8 8 04 8 58 _ 319 - 1d! 24 25 07:00 07:00 10 10 77,890 78,700 261 07:00 10 86.700 I I —---.---- 27 00:00 0 20 000 28 07:00 10 89,1100 29 07:00 10 78 780 30 07:00 10 31 Daily Maximum: Average: 74.361 100,710 48.00 48.00 0.00 - - 2-�3 000, 73.50 Oi 'I C29.C10C;.� 73.50 �t a - 0.09 0.09 70.80 70 3D 8.04 8.58 8 58 319.00 319.00 144,G0 144.00 Minimum: 2.0,000 48.00 5.00; j 42 00A, 73.50 0 6G 0.09 70 80 " 8.04 8.58 319.00 144.00 = Sampling Type: RecDrder Grab Grab { �" f G a Grab "" Grab Grab � Grab Utah ? . Grab ab { — - Monthly Avg. Limit:[' — 100,260 Dail y Limit Sample Frequency ... �_ Monthly __. �.,, . `� ;;�-- Monthly y Monthly ,^ — Monthly t4i ' Monthly -- Monthll -- --.:.1 - -- __.-- FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page J__ of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warcounty: Duplin —Month: September 7 Year: 2020 PPI: 002 Flow Measuring Point: E] Influent 2 Efflu,,,,il No flow generated Parameter Monitoring Point: Ll influent E] Effluent L] Groundwater Lowering Surface water Parameter Code 0 00625 00620 J 1� 00665 31616 Z C 0 CD E E (D 0 C 2 0 0 a P U) z (D LL 0 GC 0 CL 0 24-hr hrs GPD mg/L mg1l. mg/L mg1L #/100 mL mg1t, 1 07:00 10 91180 2 3 07:00 07:00 10 10 88.920 91.000 . ... . ...... --- 4 07:00 10 90,120 5 07:00 2 88,120 T- 6 7 8 00:00 00:00 07:00 0 0 10 20.000 20,000 79,890 9 07:00 10 81,790 101 07:00 10 91,870 11 07:00 10 85tol 0 12 07:00 4 79.220 13 00:00 0 20.000 14 15 07:00 07:00 10 10 Kill) 81 720 161 07:00 10 8i, 720 17 07:00 10 100,710 1 10 79,320 ----------- 18 07:00 19 07:00 10 90.910 20 00:00 0 20,000 21 07:00 10 67,810 1 1 22 07:00 10 '79,120 23 07:00 10 80,110,10 5 <-0.2 2 98 0.2 120 3, F, 24 07:00 10 77,890 25 07:00 10 78300 26. 07:00 10 86,700 27 00:00 0 20.000 28 07:00 10 8141010 — ----------- 29 07:00 10 78,730 30 07:00 10 6-, 87,010 31 Average: 7 0.60 2.98 2 98 0,20 120.00 3.60 1 Daily Maximum: 1 0.60 298 ?0 120.00 _4 160 1 Daily Minimum: j, 20,-' 0.60 20 2.98 020 120.00 3,60 1 Sampling Type: Rees Grab Grab Grab Grab Monthly Avg. Limit: Daily Limit: Sample Frequency:[ Rei-ord Monthl y Monthly M. ly Monthly , FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page 3 of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -War sa county: Duplin Month: September Year: 2020 PPI: 003 Flow Measuring Point: ❑ influent ❑ Effluent ❑ No flow generated Parameter Monitoring Point: ❑ influent ❑ Effluent ❑ Groundwater Lowering ❑ Surface Water Parameter Code 0 00625 0066- P 00620 65 ' 31616 ` 600 > c Y £d dam, Y �o 0 U~ H y Z LL U C ~� Z 0 H 24-hr hrs GPD mg/L xri 9/L mg/L rngtL- ' #/100 mL mq1L 1 07:00 10 91,180 2 07:00 10 88.920 3 07:00 10 91,000 4 07:00 10 90,120 5 07:00 2 88,120.- 6 00:00 0 20,000 �1 7 00:00 0 20,000 I 8 07:00 10 79,890 9 07:00 10 81,790 10 07:00 10 91870 Y~t ---- 11 07:00 10 85,010 12 07:00 4 79,220�- 13 00:00 0 20.000 11 14 07:00 10 80.110 15 07:00 10 ---- 81,720 -- - 16 07:00 10 85,720���_� 17 07:00 10 100,710- i - 18 07:00 10 79,320 I 19 07:00 10 90.910- � 20 00:00 0 20,000 1 ------- �-- ------ ---- 21 07:00 10 87810 i - — 22 07:00 10 79.120 ? _ - -- -- - - --a- 23 07:00 10 80 i 0 i 1 24 07:00 10 77 89`� 251 07:00 1 10 78,700 4 3,7 2.2 0 2 2100 6,2 ( ; 26 07:00 10 86,7100 27 00:00 0 20 000 - 28 07:00 10- 29 07:00 10 78.780 30 07:00 10 87010 31 Average: 74.afa 4.00 3,70 2.20 J 42 2,100.00 Daily Maximum °{ t� ;. 4.00 370 2.20 0.42;2,100.00 _ E Daily Minimum:. 20 000 4.00 3:70 2.20 0"42' 2,100.00 °"' 6:20 Sampling Type:. Rec :er Grab Graf? Grab grab '' Grab - - —� — Av. Limit: MonthlYDai9Y ;— Monthl Monthly "Monthl, --- Limit: - - Sample FreuencY- - - - FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page — 1� of Sampling Person(s) Name: GERALD LAMAR MATTHEWS Name: Certified Laboratories Name: Environmentat Chemists INC. Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? 7 Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: GERALD LAMAR MATTHEWS Permittee: SAM VILLARI Certification No.: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the previous NDMR? (] yes ❑ No Phone Number: 910-293-2157 Permit Expiration: 11/30/2025 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _�_ of ±a Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020 ttField Name: 2�ld Name 3 Field Name: 4 Did irrigation occur - - Area (acresy, 0.65 Area (acres): 1.16 Area (across) 1 12 Area (acres): 1.07 at this facility --- - ___ ? Cauer Cre i stai errrf,.- a Cover Crop: F p' Coastal Bermuda Corer Crop r I Ccastai Bermuda Cover Crop: P� Coastal Bermuda ❑ YES I- NO Hourly Rate (in),! 0 6 Hourly Rate (in): 0.6 Hourly Rate (in) 06 Hourly Rate (in): 0.6 Annual Rate (in). j 41,96 Annual Rate (in): 41.96 Annual Rate (in): ` 41-96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated• s, yEO Field Irrigated? 0 YES ❑ No Field Irrigated?i ES I Field Irrigated? 0 YES ❑ NO o c m ca 1' a = >, zn; m y v rn Earn iu-ts �s E T; m y v rn E rn U I y O rn rn O � G.t � +J) �. .. in E is C' E i5 E °' ; N 4; E m �, C ' 5 7` C E� 'o E T I m GT ..0.. >, C l O i E" is E N a N„ E m Z, C 'v O C E v CL 'V o N a+ csa ; y J i$. I! CS g1 O 'm MM' � O _3 O Q rn �' .` m p K O M m 2 O Q'.. it rn i- 'y` m - O ;� o ro M T q O a rn H � M f7 O R o m is 2 O _ T OF in in in~gal min In in gal min in in gal min in in gal min in in 1 2 R C 0.08 57 0_! 7.382 2.42 _ 0,42 13,173 42 0.42 0.42 12719 40 E 0 42 0 42 12,151 39 0.42 0.42 3 4 C C 1 • 1 1,8(?t3 23 7.720 23 0.44 0,44 0.44 0 44 13,931 13,778 42 42 0.44 0.44 0.44 . 044 13,451 13,303 40 40 0.44� 0 44 0.44 + 0,44 12,850 12,709 39 39 0.44 0.44 0.44 0.44 5 C _ I ------ - I -+r--- 8 R 0.05- 9 CL 0.75 11 I 10 11 CL R 1.45 0.18 {- -- - - 13 C 15 C 16 CL 0.08 17 R 1.8 18 R 0.1 - 39 19 0.44 0.22 0.44 0.22 201 21 22 C I C C 7"r64 23 H> 1 € _0,44 122 0.44 : �Q.Z2 13,855 6,898 42 21 0.44 0.22 0.44 0.22 13,378 6,660 40 20 0.44 0.22 0,44 1 12,780 6,362 23 C 4,695 23 0, 0,27 8,379 42 0.27 0.27 8.090 40 0,27 0.27 7,729 39 0.27 0.27 24 C 0.05�� 25 R 0.55 27 28 C CL 0.05 {( I 29 R 1.05�� 30 C 42 0 311 1 3 r,2 i2 2.22 70,014 Monthly Loading 2.22 67,601 2 22ism 64.581 2.22 12 Month Floating Total (in): 16-17 ���; 16 17 a 6 1 _ . i 16 17 ,;i FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NE::R-1) Page _1L of . Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw Coa:nty: Duplin Month: September Year: 2020 Field Name: 6 imame:l I , Field Name: 8 Did irrigation occur-- ��-- --- - - -- Area (acres): 1 19 Area (acres): 1.17 Area (acres):' 1,05 Area (acres): 1.25 at this facility' - ` Cover-Cro Coastal rr uca Cover Crop:Coastal Bermuda �^ over Crop:!Coastal _ Bermuda Cover Crop: Coastal Bermuda ❑ YES ❑ No Hciuriy Rate (in):! 0-6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 T Annual Annual Rate (in): 41.96 Annual Rate (in) 41.96 Annual Rate (in): 41.96 Weather Freeboard I Field Irrigated? Y s ti. Field Irrigated? ❑YES ❑ No Field irrigated?( YES - No Field Irrigated? ❑YES ❑ No a 3 ° E o E rnC a c t CC E' .' c E Em m. MN E�T d rn 0 Q a, 0 �t O rn H Rx oR M=p0 a rr p a ;6 Q � rna op m S O fA ` i J 1 Q J J a. OF in in in gal mart in in gal min in in gal min I in gal min in in 1 2 R C 0.08 57 0 13,514 _ 43 0.42 0,42 L 13,287 42 0.42 1111 0.42 11,924 38 042 �0 42 14,195 45 0.42 0.42 3 C - 14.291 '43 0.44 Y0.44: 14,051 42 0.44 0.44 12,610 38 0 44'� 0,44 15,012 45 0.44 0.44 4 C 14.134 43 0.44 0,44 f 13,897 42 0.44 0.44 12.472 38 0.44 0.44 14,847 45 0,44 0.44 5 C 7 C 8 R 0.05 9 CL 0.75 101 CL 1.45 13 C 14 CL -- - ------ ___ 15 16 C CL 0.08 i _ - 17 R 1.8 I 18 R 0.1_Al- 43 _ z 0.44 0.44 13,975 42 0.44 0.44 12.542 38 i 0.44 0.44 � 14,930 45 0.44 0.44 19 20 21 CL C C 14,214 22 C 176 `i � 21 0.22 ` 0,22 6,957 21 0.22 0.22 6:243 19 0.22 0.22 7,433 22 0.22 0.22 23 C d. _ `j L_ 43 0 27 B T 0 27 8,451 42 0.27 0.27 8 38 0.27 0.27 9,029 45 0.27 0.27 24 25 C R 0.05_._ 0.55 28 CL 29 R 1.05 l 31 l i� 7i,81� 6� 2.22 " �' 75,446 Monthly Loading;r�, 70618 ,3 222 � 2.22 12 Month Floating Total (in):__�_ }. 16.17"" FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page -3 of 6 Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020- MW- g Field Name: 10terd Field Name: 12 Did irrigation occur -- Area {acres} g Area (acres): 1.46 1.43� Area (acres): 1.23 at this facility? Cover -Cover Crop: P�+ Coasta� Fermuda Cover Crop: P� Coastal Bermuda i3� Cro- Coastal Bermuda Cover Crop: P� Coastal Bermuda _ _ _ ❑ YES ❑ NO Hourly Rate (in):1 0 E Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 � Hourly Rate (in): 0.6 Annual Rate (in): 41 6 '11 Annual Rate (in): 41.96 Annual Rate (in): 41. Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? YES� t4o Field Irrigated? ❑ YES ❑ NO Field Irrigated? ES NO Field Irrigated? 0 YES ❑ NO C E . Eo oC f ig o 0 O' = M '0 £d T C � 'a� pU N 1 F O p z X C p9 7 K a CL 0 O0Y OT XE in > � _3 1 _ J J > 2 J 9 -j 1:d J ~ d °F in in in gal i min . in _ in gal min in in gal i Mtn in in gal min in in 1 R 0.08 57 0 2 C 11.356 3042 0.42 16,580 53 0.42 0.42 16,240 -51 _ ' 0 42 0,42 13,968 44 0.42 0.42 3 C 12.010 36 9 0,44 0.44 17,534 53 0.44 0.44 17,1 74 S'. 0.44 044 14,772 44 0.44 0.44 4 5 C C 111,,878 36 GA4 0.44 'I 17,341 53 0.44 0.44 16.985 5 1 - 0.44 1 044 14,609 44 0.44 0.44 6 C 8 R 0.05 9 CL 0.75 I 10 CL 1.45 l 11 R 0.18 12 CL 13 C 14 CL 15 C 16 CL 0.08 ^ 17 18 R R 1.8 0.1 _1 - 19 CL 20 C 21 C 11,944 36 0.44 0.44 17,439 53 0.44 0.44 17,080 51 0.44 044 14,692 44 0.44 0.44 22 C 5,946 18 0,22 8,681 26 0.22 0.22 8.503 26 022 0 22.. 7,314 22 0.22 0.22 23 C 7,223 336 0.27 �-0,22 027 10,546 53 0.27 0.27 10,329 5' i U 7 27 8,884 44 0.27 0.27 24 C 0.05 - _- 25 26 R C 0.55 i� N 27 C 0.05 ❑-__� _ +--_��_ 29 R 1.05 30 C 42 0 + 31 2.22 88,121 Monthly Loading: 2.22805,311 2.22 ° 74,239 2.22 12 Month Floating Total (m): 16.17 16.17 16.17 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page - of _� Permit No.: WQ0016376 Facility Name: S& Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020 rrte Did irrigation occur Field Name: 14E antej Field Name: 15 Area (acres): f 2.16 Area (acres): 13.73 cr Area (aes). 1 77 Area (acres): 0.73 at this facility? Cover Crop: Coastal Seerrnuda Cover Crop: Coastal Bermuda CoverCrop,) Coastal Bar Cover Crop: Coastal Bermuda ❑ YES ❑ NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 - --------- Hourly Rate (in):! f­­­ 0,6 Hourly Rate (in): 0.6 Annual Rate (in): 41 96 Yt.--s NO Annual Rate (in): Field Irrigated? 31.6 21 YES Ej NO Annual Rate (in): Field Irrigated? 24-21 Annual Rate (in): YF`, 4" Field Irrigated? 30.44 0 YES ❑ NO Weather Freeboard Vield Irrigated? 0 0 1 es m E 0) rn E :3 E rn 0 0) 0 M 0 - E z E 5 E .2 0 g E E 2 E m D E 2 i5 E - -5 = -a :5 E CL E CL Zi 00 M - Cn CL Cn C 0 0 :r 0 0. > M 0 M 0 M :r 0 C. '3 CL > < (z .9 > 0 0 M x 0 _j Cn J, _0F CL F in in in gal min In in gal min in in gal min in in gal min in in I R 0.08 57 0 L 2 C 11 24,530 78 0,42 0.32 127,314 384 0.34 0.05 71399 216 0,34 009 8,290 26 0.42 0.42 3 C 25,941 78 0A4 0 34 8,767 26 0.44 0.44 4 C 25,656 78 0.44 O34 8,671 26 0.44 0.44 5 C 6 C 7 C 8 9 R CL 0.05 0.75 10 CL 1.45 11 R 0.18 i 12 CL 131 C I 14 CL is C 16 CL 0.08 17 R 1.8 18 R 0.1 191 20 CL I C 21 C 25.800 78 0.44 0.34 8,719 26 0.44 0.44 22 C 2.844 19 022 0.22 129,350 384 0.35 0.045 72,542 216 0-35 0.10 4,341 13 0.22 0.22 23 C 1 15602 78 27 121,034 384 0.32 0.05 67,87 216 032 0.09 5,273 26 0.27 0.27 24 C 0.05 251 R 1 0.55 261 27 C I C 0.05 28 CL 29 R 1.05 30 C 42 0 31 130,373 2 ��"2 in 211,818 "N Monthly Loading: 1.01 44061 �­2 22 12 Month Floating Total (in): 15-09 6.17 11M FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page S of 4, Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw county: Duplin Month: September Year: 2020 t~fetd Name: 11a Field Name: 17 1"aeEd tame Field Name: - -- -- Did irrigation occur - -- - Area (ac s): i 1.26 Area (acres): 0.82 Area (acres) j Area (acres): at this facility? " Over Crop: Farr �a.� P ; Cover Crop: P Coastal Bermuda Cover Crop,E _P: Cover Crop: ❑� YES ❑ NO Hourly Rate (in): ( 06 Hourly Rate (in): 0.5 Hourly Rate (in):' Hourly Rate (in): Annual Rate (in):1 1 63 Annual Rate (in): 16.95 Annual Rate (in):! Annual Rate (in): Weather Freeboard Field Irrigated? i rt Field Irrigated? ❑YES No Field Irrtgated?� yc roc Field Irrigated? ❑YES ❑ No r m o m c E > m c y c o `a m ° ° ° °=°> x ° E E m 3 ° CL o vU E0 a = o rm E J to „. > ` _ J J *- J 2 ... > J J �. OF in in in gal niin T in I' in gal min in in gal min in in gal min in in 1 R 0.08 57 0 2 C 13,164 131 0.39 v 13 8,636 119 0.39 0.20 4 5 C C4 _ 6 C- 7 C��^ 8 R 0.05L----- 9 CL 0-75� 10 CL 1.45 11 12 R CL 0.18 13 C r �' 14 CL - 151 C I 16 CL 0.08 17 R - 18 R 0.1 0.1 19 20 CL C 211 22 23 C_ C C 24 C 0.05 25 R 0.55 26 C 271 C 1 0.05 28 CL 29 R 1.05 30 C 42 0 31 Monthly Loading:11 13,T64 11M5.5 0 39 8 5' 3 _-Y._...--�.. _ 0 39 5 53 0�� ._..�,.. _ ,__.......-.....__._...�...e. i 12 Month Floating Total (in): 'FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 6 of +o Did the application rates exceed the limits in Attachment B of your permit? Q Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? ❑ Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? E] Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? 0 Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? 2] Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. IOperator in Responsible Charge (ORC) Certification 11 Permittee Certification I I ORC: Gerald Lamar Matthews Certification No.: 993131 Grade: SI Phone Number: 910-289-7500 Has the ORC changed since the previous NDAR-1? ❑ Yes I] No sue` Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. Permittee: Sam Villari Signing Official: Signing Official's Title: Owner Phone Number: 910-293-2157 Permit Exp.: 11/302025 �i/✓`' /i 2 Signature Date I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 'FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page I of S Permit No.: W00016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020 Field Name: Zone 1 aime , - Zorfe 2 Field Name: Zone 3 Field Grne: Zore 4 Field Name: Zone 5 Area (acres): 0.65 Area,(acres): 1.16 Area (acres): 1.12 area (acres); 1 07 Area (acres): 1.19 Coastal BermuclE Cover Crop Goaslta+ Bermudg Cover Crop: Coastal Bermud Cover Crop: Coastal BermudE Cover Crop C,oasta,' Berry ti Cover Crop: � Load Type: PAN Load Type: FAN Load Type: PAN Load Type PAN Load Type: PAN Field Loaded? 0 YES ❑ NO Field Loaded?l Q s sic; Field Loaded? 0 YES No Field Loaded?, `5 �' r.s_ Field Loaded? ❑ YES No N Z Z: c a Z Z o Z« Z aO a M �C 0- � a a a'� 6J N 4 � O [ aac O p J Z > Z N �Z 3 Z 0 J Z a c ° a y C>oc aM o �O > J r - >o ° a - > 0 >o ° cON� a Month gal mg/L Ibs/ac Ibs/ac _ rngtLlbsdac t# Ibbfac > mg/L Ibs/ac Ibs/ac ___.. ttaslw. tbs.ac U> > Ibs/ac Ibs/ac 0 38 get gal I gal t"IL { gal mg/L October 0.0 0.0 0 ( 38 0.0 ' 0,0 0 38 0.0 0.0 0 ._ 38 0.�. 0.0 0 38 0.0 0.0 November 0 33.2 0.0 0.0 0 33 fi.0 0.0 0 33.2 0.0 0.0 0 33.2 O:Cx� 00 0 33.2 0.0 0.0 December 0 46.2 0.0 0.0 0 46.2 0�0 0" 0 0 46.2 0.0 0.0 , 0 46.2 0.0 0.0 0 46.2 0.0 0.0 January 25,030 43.5 14.0 14.0 44,672 1 43.5 14.0 14.0 43,131 43.5 14.0 14.0 1 41,204 43.5 14:0 14.0 45,825 43.5 14.0 14.0 February 29,973 43 16.5 30.5 53,491 43 E 15.5 30:5 51,647 43 16.5 30.5 49,34.1 43 -16.5 30.5: 54,875 43 16.5 30.5 March 42,537 48 26.2 56.7 75,912 48 26.2 56:7 73,294 48 26.2 56.7 70,023 48 26:2 56.7 77,876 48 26.2 56.7 April 30,195 48 18.6 75.3 51886 48 18.6 1 7 5;3 52,029 48 18.6 75.3 49,70b 4_ 186 75.3 55,280 48 18.6 75.3 May 42,852 38.4 21.1 96.4 76,474 38.4 21.1 ' 96.4 73,837 38.4 21.1 96.4 70.542 38 4 21.1 96.4 78,451 38.4 21.1 96.4 June 67,429 32.4 28.0 124.4 121;335 327 28.3e 124.7 116,185 32.4 28.0 124.4 ' 110.997 32.4 28.0 124.4 123,445 32.4 28.0 124.4 July 0 26.6 0.0 1 124.4 0 26.6 0,0 1124.7 1 0 26.6 1 0.0 124.4 0 2 h.6 0_t7 124 4 6.6 0.0 124.4 August 8,146 39.6 4.1 1 128.61 14F°,7 396 41 88 14,035 39.6 4.1 128.6 13,409 39.6 4.1 1286 14,913 39.6 4.1 128.6 September 39,232 36.1 18.2 146.8 70,01 36.1 182 147:0- 67,601 36.1 18.2 146 8 64,581 36.1 18.2 '146 8 . 71,825 36.1 18.2 146.8 12 Month Floating PAN Load 146.8 147.0 146.8 (Ibs/aclyr): " . /i ;, Annual PAN Load Limit (Ibs/aclyr): 350 350.00 �'y` �� i ;-' 350.00 350,00 350.00 FOI-:` NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page -I- of S Permit No.: WQO016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020 Field Name: Zone 6 7" TW,16,7 Field Name: Zone 8 FWd Name: Field Name: Zone 10 Area (acres): 1.17 Area ., cres}: 1,05 Area (acres): 1.25 Area (acres ;� Area (acres): 1.46 Cover Crop: Coastal Bermuda Cc?tik^• Crop, Caasta# Bear. Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Load Type: PAN L aakiTType: PAN __..._ Load Type: PAN � Lead Type � PAP! - Load Type: PAN Field Loaded? ❑� YES No Field Loaded? YES Field Loaded? ❑' YES NO field Loaded? � YES ._ ' Field Loaded? ❑ YES No v m a c Z o a:. Zs Q > c sz <;2 # �# i 10 m a c zo a Z a >a a is c Q• 0 1 < >"0 m c c Q o Q mD > a a o • a o CL i s a I a a a o ca I o a a a v o 0 ac, d N .+ t�0 N >, lC t+ J J Z � F ;w � M 4 cu C4j # 3 z Q d D C N Ga >, 10 -,, J J Z t ry ¢ 1 , l M J _.! -; Z Q N C M N �. M J J Z E y aCM c E Q F c E `m c E Q E i E m" .L c E Q 0 > o ° U �' P> 0 a >a,; ' > o rL 0 2 > o tsa c G va Q(� 0 i U C t j O > QU Q '�`J �mg/L _ a> U Month gal 0 mg/L Ibs/ac I Ibs/ac gFal rrag7i. ibslac #bstac gal mg/L Ibs/ac Ibs/ac i pal i ibsfac lbs/ao gal mg/L Ibs/ac Ibs/ac October 38 0.0 0.0 0 38 0.0 � 0,0 0 38 0.0 0.0 0 i 38 0.0 0,0 0 38 0.0 0.0 November 0 33.2 0.0 0.0 0 3:3 2 4 0 0 l 0,0 0 33.2 0.0 0.0 0 33 ? 00 00� 0 33.2 0.0 0.0 December 0 46.2 0.0 0.0 z 462 O.0 0.0 0 46.2 0.0 0.0 0 k 46.2 0.0� 0,0 0 46.2 0.0 0.0 January 45,055 43.58 14.0 14.0 4G,334 435 ' 3.9 13.9 48,136 43.5 14.0 14.0 38,510 43.5 E 14,0 14.0 56,224 43.5 14.0 14.0 February 53,953 43 16.5 30.5 48,420 43 16.5 30=5 57,641 43 16.5 30.5 46,113 43 I 16:0 30.5 67,324 43 16.5 30.5 March 76,567 48 26.2 56.7 68,714 ( 45 Z6.2� 55.7 81,803 48 26.2 56.7 65,442 48 26.2 56.7 95,545 48 26.2 56.7 April 54,352 48 18.6 75.3 48,777 48 18,6 75.3 58,068 48 18.6 75.3 1 46,453 48 186 3 E 75.P11, 67,823 48 18.6 75.3 May 77,133 38.4 21.1 96.4 69,224 38A 21,1 984 82,408 38.4 21.1 96.4 65.925 38.4 21 14 96,252 38.4 21.1 96.4 June 121,372 32.4 28.0 ''' 124.51 108;924 32.4 28.0 j 244 129,671 32.4 28.0 124.4 103.734 32.4 28.04 151,435 32.4 28.0 124.4 July August 0 14,662 26.6 39.6 0.0 4.1 124.5 0 26-6 0,0 1 286 13 158 39.6 4 1 1244 128 6 0 15,664 26.6 39.6 0.0 4.1 124.4 128.6 0 12,532 26.6 39.6 0.0 4.1 124A , 28 6 0 18,296 26.6 39.6 0.0 4.1 124.4 128.6 September 70,618 36.1 18.2 146.8 63,375 36.1 18.2 i46.7 75.446 36.1 18.2 146 8 60,35�� 36,' _ 18.2 �46 88.121 36.1 18.2 146.8 12 Month Floating PAN Loads 146.8 :45. 1468 �� 146.8 (lbs/ac/yr): Annual PAN Load Limit 350 3:_0,00 �,,� 350.00 350.t00dim 350.00 Ibs/ac/ r : FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page 3 of S _ Permit No.: W00016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: September Year: 2020 Field Name: Zone 11"#di``otie 1 "" Field Name: Zone 13 Field Name: Zone 14! Field Name: Zone 14W Area (acres): 1.43 1 Area (acre 1.23 Area (acres): 2.16 Area (acres): 1 ,'3 T Area (acres): 7.7 Cover Crop: p: Coastal Berrn ..s Cover Crop: p: Coastal Bermud Cover Crop:Coastal Bermudi Cover Crop,Coas+a` Be ;cud Cover Crop: P: Coastal Bermud � _-P � Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? YES ❑ NO field Loaded? Z .j �. �v# Z Q Field Loaded? El YES NO -Field Loaded` YFS Field Loaded? ❑' YES � NO O Z Z }........._._.- j 0�-7 Z O Z D ! Z Z O Z O Z a O a R N a :r to sa o i i a a to a d .. a C ('y C)< a 1 -tn� d a 0- to a N �. M 5 J '� ii � O j �.�M � � g1 ¢ N +`- T � � J ¢ u � ' s g'�1._�,i � f� ¢ G7 � >. A � J N _3 O > R N d V C > ¢ U « O Z tF3 1 J¢ _ = t} O 3 d > V -00 > !' gal mgfL 0.0 C 0.0 c i 0 38 2 t} S ",J k CB I ` lbs/ac 0.0 '":.. Z i (L $ 3 t i..7 - O _ > ` lbs/ac" gal 0.0 0 m N L V d C > ¢ U mg/L 38 t O C J O rL Ibs/ac 0.0 O Z E¢ 7 V a Ibs/ac 0.0 q} 'I~ O.. > gal 0 I i 9y C 7 £i' g g.'L 38 .�. O' :rL ' O 6 O UL f ..: _ lbs/ac Ibsac 0.0 0.0 O E > O gal 0 tt U L d C > ¢ �j mg/L 38 E O C J O L Ibs/ac 0.0 Z 7 ¢ U Q. Ibs/ac 0.0 Month g 0 g 38 October November 0 33.2 0.0 0.0 0 3� 0.0 }.0 €! 0 33.2 0.0 0.0 431;699 33.2 8.7 1 8.7 214,749 33.2 7.7 7.7 December January 0 55,068 46.2 43.5 0.0 0.0 i! 0 46.2 14.0 14.0 1! 47,365 43.5 I 0.0 ",4.0 _O.0 0 14.0:. 83,180 46.2 43.5 0.0 14.0 0.0 i 14.0 645,371 416;791 46.2 43.5 18.1 26.8 11 0 ! 37,8 321,039 233,744 46.2 43.5 16.1 11.0 23.8 34.8 February 65,942 43 16.5 30.5 �( %.719 43 ,6.5 30.E 99,604 43 16.5 30.5 489,300 43 12.8� 5016 274,406 43 12.8 47.6 March April p 93,582 66,428 48 48 26.2 56.7 l�ry 00 494 48, 18.6 75 3 '�,{ 139 48 26.2 i8�6 9.6.7 141,354 ; 5 l '£ � g 100,341 48 26.2 56.7 ' 3222,736 r 736,314 �48_ 48 3.4 60.0 21.5 ( 81.5 180,996 412,895 48 48 9.4 21.5 57.0 78.5 48 18.6 75 3 May 94,274 38.4 21.1 96.4 1 81.143 38.4 21 1 96.4 142,400 38.4 21.1 96.4 579,702 38.4 13.5 95.0 325,106 38.4 13.5 92.0 June 148,345 32.4 28.0 124.4 ,i 127,597 32.4 280 124 , 224,066 32.4 28.0 124.4 1,001,699 32.4 19.7 114.7 561,771 32.4 19.7 111.7 July 0 26.6 0.0 124.4 0 1 26.6 0.0 _ 124; ;: 0 26.6 0.0 124.4 0 26.6 0.0 114 7 : 0 26.6 0.0 111.7 August 17,920 39.6 4.1 128.6 i5,414 ; 39.6 41 128 27,068 39.6 4.1 128.6 1 386283 ' 3916 8.8 123.5 205,417 39.6 8.8 120.5 36.1 September 86,311 36.1 18.2 146.8 ,, 74,230 == 33 146.8 1 18.2 - 130,373 18.2 146.8 37E,698 36.1 8.3 211,818 36.1 8.3 128.8 12 Month Floating PAN Load�(� 146-8 146.8 131 8 128.8 (Ibs/ac/yr): Annual PAN Load Limit 350 350.00 350.00 lbs ac/r y� FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page � of S Permit No.: W00016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: , ;;,)lin Month: September Year: 2020 Field Name: Zone 15 it l re: 7one� Field Name: Zone 17 'Name : Field Name: Area (acres): 0.73 Area (acres): 25 Area (acres): 0.82 Area (acres):! Area (acres): Cover Crop: Norfolk Cover Cop �r natal Bermttd Cover Crop: Coastal Bermud r ovvr Crop:l Cover Crop: ._-Load iLoact Load Type: yp PAN � ype FAN Load Type: PAN Type 1N Load Type: PAN Field Loaded? ❑ YES ❑ NO Fie La a�ied� Field Loaded? ❑YES � No F e�id Ls>aded�t r 0 Field Loaded? ❑YES ❑ NO z o z o Qaa z o d� aaz zo aw m a v � i � g o � CL a ° LzQn C j T0 J Z d 2 �E J . > A Jp Joo E Z ' > ' a E Cz E 'i a o c a O U CL c i > b+ac > y U \2' V.r gal 0 mg/L Ibs/ac Ibs/ac gal mg7L lbsFac gal mg/L Ibs/ac Ibs/ac ga< ttL gal mg/L Ibs/ac cMonth Ibs/ao October 38 0.0 0.0 J 38 :0 0 F 0.0 0 38 0.0 0.0 November 0 33.2 0.0 0.0 0 33.2 0.0 0.0 0 33.2 0.0 0.0- December 0 46.2 0.0 0.0 0 462 0.0 ? 0,0 0 46.2 0.0 0.0 January 28,112 43.5 14.0 14.0 23,420 43.5 6.8 6,8 15,363 43.5 6.8 6.8 February March 33,663 47,771 43 48 16.5 26.2 30.5 56.7 0 24,998 43 0.0 6. 1, 0 43 0.0 6.8 48 &0 ?4i=. 16,399 48 8.0 14.8 April 33,911 48 18.6 75.3 si,371 48 10.0 24.8 20,580 48 10.0 24.8 May 48,126 38.4 21.1 96.4 19,846 38A 51 29 9 13,019 38.4 5.1 29.9 June 75,728 32.4 28.0 124.4 50.918 38-4 13,0 430 33,403 38.4 13.0 43.0 _ - -- July 0 26.6 0.0 124.4 0 26.6 0.0 43.0 0 26.6 0.0 43.0 August 9,148 39.6 4.1 128.6 24.143 39.6 6,4 .4 15,838 39.6 6.4 49.4 September 44,061 36.1 18.2 146.8 13,'!84 36.1 3.2 52.5 8 636 36.1 3.2 52 5 12 Month Floating PAN Load« (Ibslaclyr): 146.8 52.5 52.5 0.0, , 0.0 Annual PAN Load Limit �- (Ibs/ac/yr): 350 350.00 350.00 0.00 9 0.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page -(---Of 5- Did the mass loading rates exceed the limits in Attachment B of your permit? ❑ Compliant ❑ Non -compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: SAM VILLARI Certification Number: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the previous NDMLR? ❑ yes ❑ No Phone No.: 910-293-2157 Permit Exp.: 11 /30/25 Signature By this signature, I certify that this report is accurrate and complete to the best of my knowledge. - G rrw Date Signature Date I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 envirochem SM ANALYTICAL & CONSULTING CHEMISTS Villari Foods -Warsaw 1012USHwy 117 Warsaw NC 28398 Attention: Gerald Matthews Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoL environmentalchemists.com Lab ID Sample ID: 20-42022 Site: PPI-001 Eff Test Method PAN Calculation Used 30% Mineralization Rate Date of Report: Oct 08, 2020 Customer PO #: Customer ID: 11110024 Report #: 2020-16422 Project ID: WWTF Effluent Collect Date/Time Matrix Sampled by 9/25/2020 8:00 AM Water Gerald Matthews Results Date Analyzed Ammonia Nitrogen EPA 350.1 Ammonia rn'trogen and TKN are within limits of uncertainty. Total Dissolved Solids (TDS) SM 2540 C Residue Suspended (TSS) SM 2540 D Chloride SM 4500 Cl E Total Phosphorus SM 4500 P F BOD SM 5210 B Fecal Coliform SM 9222D MF Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 3532 Nitrate+Nitrite-Nitrogen EPA 353.2 Nitrate Nitrogen Subtraction Method Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA 351.2 Total Nitrogen Total Nitrogen 36.1 mg/L 10/07/2020 73.5 mg/L 10/05/2020 319 mg/L 09/25/2020 144 mg/L 09/26/2020 < 5 mg/L 09/30/2020 8.58 mg/L 10/06/2020 48 mg/L 09/25/2020 29000 Colon ies/100mL 09/25/2020 0.10 mg/L 09/25/2020 0.19 mg/L 09/28/2020 0.09 mg/L 10/07/2020 70.6 mg/L 10/02/2020 70.8 mg/L 10/07/2020 Report #.: 2020-16422 Page 1 of 2 6:z7irochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(denvironmentalchemists.com Villari Foods -Warsaw Date of Report: Oct 08, 2020 1012 US Hwy 117 Customer PO #: Warsaw NC 28398 Customer ID: 11110024 Attention: Gerald Matthews Report #: 2020-16422 Project ID: WWTF Effluent Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-42023 Site: PPI-002 (ups) 9/25/2020 8:30 AM Water Gerald Matthews Test Method Results Date Analyzed Ammonia Nitrogen EPA 350 1 < 0.2 mg/L 10/05/2020 Total Phosphorus SM 4500 P F 0.20 mg/L 10/06/2020 Fecal Coliform SM 9222D MF 120 Colonies/100mL 09/25/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 09/25/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 2.98mg/L 09/29/2020 Nitrate Nitrogen Subtraction Method 2.98 mg/L 10/07/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2 0.6 mg/L 10/02/2020 Total Nitrogen Total Nitrogen 3.6 mg/L 10/07/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-42024 Site: PPI-003 (down) 9/25/2020 8:45 AM Water Gerald Matthews Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1 3.7 mg/L 10/05/2020 Total Phosphorus SM 4500 P F 0.42 mg/L 10/06/2020 Fecal Coliform SM 9222D MF 2100 Colonies/100mL 09/25/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 0.02 mg/L 09/25/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 2.23mg/L 09/29/2020 Nitrate Nitrogen Subtraction Method 2.20 mg/L 10/07/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2 4.0 mg/L 10/02/2020 Total Nitrogen Total Nitrogen 6.2 mg/L 10/07/2020 Report #:: 2020-16422 Page 2 of 3 re" nviroehe7 m 6 ANALYTICAL & CONSULTING CHEMISTS Viliari Foods -Warsaw 1012USHwy 117 Warsaw NC 28398 Attention: Gerald Matthews Comment: / Reviewed by:� Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 08, 2020 Customer PO #: Customer ID: 11110024 Report #: 2020-16422 Project ID: WWTF Effluent Report #. 2020.16422 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client:_%i � `r I �oe(s Date: -1 2 ZD Report Number: 2D— I �y Zz— Receipt of sample: A DelivereclA UPS ❑ FeclEx ❑ Other ❑ ❑ YES ❑ NO N/A 12. 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A If custody seals were present, were they intact/unbroken? Original temperature upon receipt ,C Cor cted temperature upon receipt How temperature taken: O Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 ❑ YES 10 NO 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified? YES 10 NO 4. Were proper custody procedures (relinquished/received) followed? Ig YES JE1 NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES 10 NO 7. Were collection date and time listed on the COC? YES I0 NO 8. Were tests to be performed listed on the COC? YES JE1 NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 110. Did samples arrive in good condition for each test? YES ❑ NO Ill. Was adequate sample volume available?' YES 10 NO 122. Were samples received within proper holding time for requested tests? YES ❑ NO 113. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 114. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 115. Were sulfide samples received at a pH >9? YES ❑ NO 116. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Samples) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2501 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obta'n a new sample or notify the state lab if directed to ana'yzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 °C Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CHIRTrinv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Villari Foods -Warsaw PROJECT NAME: WWTF Effluent REPORT NO: 7j)— ZZ ADDRESS: 1012 US Hwy 117 CONTACT NAME: PO NO: Warsaw, NC 28398 REPORT TO: Gerald Matthews, ORC PHONE/FAX: Permit Number: W00016376 email: Sampled By: r,ll L 1 5 Lr/ SAMPLE TYPE: I = Influent. E = Effluent- W = WplI ST = St roam cn = Coil ci = c1... 4.,e nfk Sam Sample Identification p Collec Ion a d E rn o E EF c a " _ t E U LU m Z PRESERVATION ANALYSIS REQUESTED Date Time Temp o = u = H _ i _ a _ = ' = ~O PPI-001 (Effluent-1/month) Jy 22S 0ZZ. X BOD,TSS,NO2 G G PPI-001 (Effluent-1/month) C P f L 1 X 2� NO3, NH3, TKN,Total P, PAN, Total N G G tt PH (field): .Q 1 C P X Fecal Coliform G G C P G G March, July, November PPI-001 (Effl-Triannuals) C P X TDS, Chloride G G C P G G PPI-002 (Upstream) ' = Y � C P X NO2 G G PPI-002 (Upstream) C P 'K� n �{l TKN, NH3, NO3, Total P, Total N G G PPI-002 (Upstream) C P X Fecal Coliform G G C P G G PPI-003 (Downstream) J C P 7(1 X NO2 G G PPI-003 (Downstream) C P X TKN, NH3, NO3, Total P, Total N G G PPI-003 (Downstream) C P X Fecal Coliform G G Samples due 1/month Transfer Relinquished By: DatelTime Received By: DatelTime 2. I emperature when Received -C: `T ) Accepted: 11� 4 Dejected: Resample Requested: Delivered By: Received By: 5-� . lh Dated ZS ZO Time: 1 1 a Comments: TURNAROUND: