NCG510357_Regional Office Historical File Pre 2018

Michael F. Easley, Governor
June 12, 2006
Mrs. Mildred Berryhill
Tull Transport, Inc..
P.Q. Box 327
Troutman, N.C. 28166
NCDENR
North Carolina Department of Environment and Natural Resou
Division of Water Quality{ k-,
m
ces
am lS
Alan W.
JUN 1 9 '200
TER QUALM' 'SECTIOt
Subject: Rescission of NCG510357
Piney Woods Quick Stop
Catawba County
Dear Mrs, Berryhill:
ry
to
Division staff has confirmed that the subject Certificate of Coverage [issued under NPDES
General Permit NCG510000] is no longer required. Therefore, in accordance with the request
forwarded by your authorized representative, CDC NCG510357 is rescinded, effective
immediately.
If in the future your company wishes to discharge wastewater to the State's surface waters, they
must first apply for and receive a new NPDES permit. Discharge of wastewater without a valid
NPDES permit will subject the responsible party to a civil penalty of up to $25,000 per day.
If you have questions about this matter, please contact Charles Weaver of my staff at the
telephone number or address listed below.
cc: Contrallilea
trifle Rgnl Oe ;Mke Parker
NPDES Permit file
Fran McPherson, DWQ Budget Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
512 North Salisbury Street, Raleigh, North Carolina 27604
Internet: h2o.enr.state.nc.us
Phone: 919-733rv5083, extension 511 / FAX [phone]
charles.weavernmail,net
N©nrthCaro ma
Naturally
An Equal Opportunity/Affirmative Acton Employer - 50% Recycled/10% Post Consumer Paper

Michael F. Easley, Governor
CERTIFIED MAIL
RETURN RECEIPT E 'JESTED
Mildred R. Berryhill.
Tull Transport, Inc.
P.O. Box 327
Troutman,NC
Dear Permittee:
281.66
AvA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Williarri',GRAellr., Secretary
Atan'AVKlitnetitt Director
June 5„ 2006
JIG
Subject: Notice of Violation
Failure to Submit Permit Renewal Application
Certificate of Coverage NCG510357
Piney Woods Quick Stop
Catawba County
NPDES General Permit NCG51.0000, under which the subject facilityis covered, expires on
September 30, 2006, North Carolina Administrative Code (15A NCAC 2H.0105(e)) requires that an
application for permit renewal be filed at least 180 days prior to expiration of the current permit. To satisfy
this requirement, your renewal package should have been sent to the Division postmarked no later than
April 3, 2006.
The Division has not received a renewal request for the subject CoC. This is a violation of your
permit at Part II, B. 10, which states "Any permittee that has not requested renewal at least 180 days prior
to expiration_will subject the permittee to enforcement procedures as provided in NCGS 143-215.6 and 33
USG 1251 et. seq.",
To prevent an assessment of civil penalties you must submit a completed permit application (see
enclosed forms) no later than June 19s 2006. If th.e system is inactive due to lack of trust fund payments,
but the remecliation equipment is still on site, the CoC should be renewed,
If all remediation discharge from this facility has ceased and you wish to rescind this CoC [or if you
have any other questions], contact Charles Weaver of my staff. Mr. Weaver's telephone number, fax number
and e-mail address are listed at the bottom of this page.
Sincerely,
)RIGINAL SIGNED "S
-;At \.1 A WILSOY
Alan W. Klimek, P.E.
cc: Central F'iles
Mooresville Regional Office Surface Water Protection
NPDF,S File
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 919 733-5083, extension 511 (fax) 919 733-0719
VISIT us ON THE INTERNET @ http:/(112c.enr:state:nc:us/NPDES e-mail: charles,weaver@ncmail,net

NTAL ASSOCIATES, INC.
January 6,. 1999
Mr, Richard Bridgeman
North Carolina Department of Environment,
and Natural Resources
919 North Main Street
Mooresville, North Carolina 28115
Reference:
Dear Mr. Bridgeman:
December 7, 1998 Peniiit Limit Excursion
Pineywoods Quick Stop
Catawba County, North Carolina
NPDES Permit No: NCG510357
JAN
This letter serves as the written report for a permit limit exceedence which occurred on
Decernber 7, 1998 according to the attached laboratory report for the groundwater remediation
system (GRS) sample collected from the effluent sample port. The laboratory report indicated
40 mg/1 total suspended solids (TSS) which exceeded the permit limit of 30 mg/1 for TSS..
Shield estimates the flow which exceeded the TSS limit to be less than 1000 gallons. The sock
filter was changed prior to sampling the GRS effluent which may have caused excessive
turbidity and increased the TSS levels.
The system was shut down on December 22, 1998 due to the cold weather and will remain
down until the weather gets above freezing, Shield recommends changing out the sock filter
every week, however the NC Trust fund will only pre -approve one site visit every three
weeks. Therefore, Shield will install a smaller micron filter and allow the system to cycle
several times before sampling after a filter changeout.
If you have any questions or require any additional information, please contact Peter Jordan at
[phone].
Sincerely,
Peter D. Jordan
Project Manager
cc: Cissy Berryhill, Raymer Oil Co.
f: ._11950340\129Xbyps,ltr
Chatione
Carolina Business Center
2848 1-85 South
Suite F
Charlotte, NC 28208
istephone 704 394.6913
Toll Fres 80(7395,5220
Fax 704,394_69'68
LriA,w.shielgenv gong
Atlanta, GA
Lexiogton, KY
Pittsburgh, PA

Decent 24 1998
Pete Jordan
Shield Environmental Assoc
59 I-95 South
GharlOtte; NC 28
Pecs Project Nu
l ient Prot
Dear fir: Jordan
Srtics
.sust'tsrs cons
Sincerely;
Fel c a Aarogarl
Project Manager
Labe
NC Waste
NC ran
SC
Piney ' oct 19559 9
results of anff
n ro s rear
yses Ear sari e(sl r•ecei:rt by the l abo
please fell free to s
a
Pace Analytical Ser0ces, Inc:
9800 incey Avenue, Suite 100
Hnntersville, NC 8 7
Tel: [phone]
Fax. 70 - 75-9891
n Decentb
8 „199, if you have any
REPORT OF TORY ANALYSIS
1Cos report she not be reproduced, except
Anthoa t the written consent of Pace Analytical Services, Inc
Laboratory
KY Drinking
TN UST Lis
VA Drcnkr ig

Wield Eraviro
348 1.63 Sou
ental Assoc.
C 28208
ions; 470413'94
bars
reported do a dry eaght lac
ample Ni; 92233360
rrpl e C GRS EFFLUENT (PINEY EY W6221
ararreters
a
P lketa f s
on
Maranes
Date Di=eSted
Lean by
Le
Cate
Chem stry
Results
24
Pace Analytical ServIces. icc
9 0 Kincey Avenue, Suite 100
Htrntersviile„ NC 76
Tel [phone]
Fax: [phone]
DATE 12/24/98
PAGE:
Pace Project Number: 923287
Client Project ID: P1ney Wand! 961340
Date Col ter tew: 12/07/9;
Date Rene ied; 12106 98
Matrix: wa+
Units PRt Analyzed Analyst CAS Foot
od EPA 2`i''0.7
11
thod 239.2 Method;
Total Suspended Salyds
Total Suspended Scl ids 40
0rnbt?
NC Wa.
NC rirr9k.SC
slosh' ? Maier
water' 37706
99006
Method: EP4 I60.2
1<
GE
05
Prep tlethct EPA 2011
12 "23/98 TYM ?4.29 9.6
12/23796 TYM 7439 96.5
12222/9d
Prep Method: EPA OF
15/98 3AS 1439.9P
r 96
rrep Matb d. EPA
2/ 1.1 98 JML
Prep fm
LDRP
Prep M
SMP
SHP
SMP
SMP
;aP
16/98 SMP
SMP
PA 1011r902
2
REPORT OF LABO * TORY ANALYSIS
Trr4s report shall not be repr uced. except In full,
ut the written consent of Pace Analytical Services, lrao
Ladd
Orini
TN UT List
VA Drinking 'War

Pace Analytical Services, Inc;
9800 Kinsey Avenue® Suite 100
Htsnlersvtlle, NC 28078
Tel: [phone]
Fax: 7'94-875-9091
DATE 1.2724/98
PAGE: 2
Pace Project Number~: 923287
Cllent project tt° Riney Woodr'1981340
pie N.D. 0
Sample 1D: 2 2FLI SIT (PINEY tw00D)
,� n ]fi "it n I
NC Wastev+°ater o
NC f, rankrng Water 37706'
SC 99006
at Doi l ected: i2r'17 '98
Date Received: .12118'98
s ISnr is PRL
Analyzed Analyst
12/16/98 SNP 828-98-9
REPORT OF LABO TORTORY ANALYSIS
Th.s report sha61 not be reproduced, except to full,
without the written consent of Pace Analytical Services, l:
TN UST t
VA Orink rrg

ace Analytical
PAGE: 3
DATE; 12/24/98
9,800 Kincey Avenue, Suite 100
Pace Analytical Serif res, Inc,
Huntersville, NC 28078
Fax 704-8'75-9091
Tel: [phone]
AMMETER FOOTNOTES
Not Detected
Not Cal cul able
Pace Reporting Limit
S) Surrogate
Laboratory Certification IDs
NC Wastewater 12
e
DnnkIng Water 37706
SC 99006
Pace Project Nu -n'a 323257
Client Project ID Piney W0011/1952340
REPORT F LABO TC)RY ANALYSIS
This report shall not be reproduced, except n fult
thou": the wntten consent of Pace Analytical Sendces,Inc
,Ladoratary Certiktuu:
ick Drinking Water 90090
TN UST List
VA Drinking Water 213

Page Ana y cal
meld Envi carmen Assoc.
4d 1.85 South
tF
^arlatee, Mt 28208
stn Mr. Pete urdan
(7U4)394r0
a;tr
nalyryyei
Roci aced
ted Hese
d EPA ix
p
ranter
weal Suspended Sold.
µ'AMP":E:.
Susieneed Sol ds
I PLPLIt:A€ 4. 92238298
nr
astewater
ricking Water 3770
QUAI
3223e32
22233.3L
Units
Lrt
CO 0L DATA
Pace Analytical Sererrces Inc.
9800 Kinney Avenue, Suite 100
Huntersville, NC 807
Fax:
7704-875- 0
Fax X -815- 091.:
DATE 1 /24498
PAGE:4
Pace Project Nu era 923287
CI lent Project I[I: Piney Weacf/1950 4
53 Satch Method: EPA 15L.2
Ara(7°s s Sscr�
Method
l ar k
Result PRL t tnotes
Unix
Spi Se
Dup
Result RP
REPORT LABO TORY ANALYSIS
This report snail not be reproduced, except
tten consent of Pace .A.naiytical Seo
Lab
yr tcry L r
P Drinki
TN ST List
VA boning Water

ace Ana t
yield Environmental Assoc:
948 1.85 South
utteH
hone (704
NC 28208
94wo9
D: 6543
tet rod :
Pace 5a,mpl'
ssod:ated Pa
araaater
cad
92237627
Dar tples.
QUALITA' CONTROL DATA
SPIKE °I PLirA L: 92227'-
h Method: EPA 20OF
Ana' s(s DescrBLead by Eurrar~eo Method 239.
Pace Analytical Services, Inc.
9800 Kinsey Avenue, Suite 100
tiuntersville, NC 28078
Tel: [phone]
Fax: [phone]
DAB; ].2/ 4/98
PAGE 5
Pare Project Number: 923287
Li lent Project ID: Piney Wood1195D 4
r`+'k
RY =7EN7R L SAMPLE ` DSD; 92?,3ibr 8 9223 = 926
5utke
Lob retQr arts atl n
NC Wastewater" 12
NC r:rkeng Water 37706
SC 9,9006
PILL
005
Footnotes
7pie
Banc..
Matrix Spike
Spike 49 Dup. Dup
Rc" Res
53 0.33420 118
REPORT OF LABO
Spike
Dup
Red RPDFnotn
TORY ANALYSIS
This report malt not be reproduced: except in Bail.
e ^n r:tten-ansent of Pace Analytical Seneces, etc
Drinking Wate+
TN UST Li
A Drinking 4 later 2

Pace Analy
d mental Assoc:
8 185 uttl
it toH
�Ctte " C 28208
etc. Mr. Pete rirdan
rune; (704)394 59
Batch ID, 5559
aT 's s Method: EPA 200. r.
Pace Samples:
37800 bJ K: 922381C4
ssncaate Pase Samples:
erarmeter
0
to a ese
AIR!'
BUAi IT CO Cli.. DATA
Pace Analytical Services, lrc.
9800 Krncey Avenue, Suite 19
untersville NC 28078
Tel: [phone]
Fax: [phone]
LATE: 1212 C98
PAGE: 6
Pace ProjectNumber: 923287
ient Project 1C: Piney Woodll950340
Method EPA 21'S
is ,ri etst on;
92228C5C
TC193 CCNI? L SAMPLE & E :
angane e
Site*
Laborator/ rtfoaion
NC Wastewate
NC DrnkingWater 377 06
S
00
Method
k
AT
PRp Euctnrites
C 01
Spike
Result
22.80 25
z,vr
Spike
Rec
atrtx Spike
Spine Sp Cup. Culp
t Rec Res ralt Rec PPG Footnotes
66.4 44,40
8 1.9417 89.4
Solkra
Opp
92,0
Cup,
REPORT OF LABO
TORY ANA
4 28
This report shall not be reproduced; except in gall:,
the written consent of Pace Analytical Services, Inc
Y
KY Drornkis
TN UST Lis'
VA Dunking
e

ace An y cal
QUALITY CO OL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hunte€sville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 12/24r98
PAGE: 7
Pace Project Nu er: 92 287
21"ent Project ID, Piney Wood/1 0 40
AMPLE 2tiPLTCATE: 92238153
Dup.
eram to Latta 92230739 Result RP0 Footnotes
an rsr,{t ry ;m39
NC Wastewater 12
NC Drinking Wate 37706
SC 99006
REPORT OF ABO Y ANALYSIS
This report shal9 not be reproduced, except sn
cat the Mitten consent of Pace Anatyt, at Serhces, Inc:
rrratcru y6,it nii n
Drinking ter' 30090
TwNUST t,set
VA DrinkingWatr tit

ace Art i
elf Envrr5 ntaT Assoc,
1.5 South
eH
rlette, C 350
ne; (704)3i4 6'
t+
s?s PA 1664
ssuctatei Pura Samples:
' T
sso "a: w Pace
ame"ter
and Grease
SCI
hod
an
PRL
UAL I1YCOMA, DTA
P
Pace Analytical Services, Inc,
9800 Kincey ,Avenue, Suite 100
Huntersvdle, NC 28078
Tel: [phone]
Far 70 - 75-9t191
DATE 12 i34/90
PAGE 8
Pace Project Number: 923287
Client Pruje t 1D: Piney klc rld10503 0
CC Sat Wh Method: EPA 351C
Aralys s 13es,vrlp ,n: Hexane C:xtractaele Mat0rr
360
ND
aramete. Resin t a Re'n
40 l".20
tnotes
REPORT OF LA 0 TORY ANALYSIS
"Pus report shall not be reproduced, except In full,
oat the rittera consent ofPace Analytzal Services, rtc
att
nuking 4atei' 30090
TN UST last'
VA Orinktig 'a later

ce Analytical
iie d Env/ ronmental Assoc
1348 1-85 South
lu ( te 8
Marl 1:te. NC 23208
:tn : Mr . Pete 21)rdAh
none: [phone]
(C, Batch ID: 6721
ysi s Mtethod: EPA 6(:)1 /502
socl atea Pace Samol
LETHOD BLANK: 92245273
ssotiated Pace Samples:
92233)360
QUALITY CONTROL DATA
Pace Analytical Services, Inc,
9800 Kinsey Avenue, Suite-100
Huntersvine. NC 28078
fel: 704-875-9092
Fax [phone]
DATE: 12/24/98
PAGE: 9
Pace Project Number: 923287
Client Project ID Piney W00811950340
QC batch Method : EPA 601/602
Aral ys s Oesciri pt i on: Hal open & ,Aromati c la"ol Orgs
92233360
MeAtIod
81 ank
aramet,er Units. Rasp' t PRI Footnotes
.......... . .
2-Di C:hlogOettleme umAL ND
tlytart, - butyl Ether ND
enzene NC 1
el gene ug/L NC
:hyl benzene ug/L NC
.ape Xyl ene ug / L. NC 1
° X21 Roe 11,2 -Di methyl benzene) umCK NC
DI c)r0-3-61(lorobenaene (S) 95
TABORATORT CONTROL SAMPLE: 92245281
Spi ke JCS Spi ke
ararletern ts Ccbc, Resul 1Rec Boo trot,es
. ........
-01chi oride thane omit 20 17.45 871,3
BA fly l tert - butyl E trier
end: ene ug e L 21) 12.43 62.2
el Pene ug/L 23 34, *73:,) 73 _ 9
:hyl benzene og/L 20 15,11 75.5
X yl ene up/ L 40 30.96 li`17.4,
, apt 8,y-28 f 1 : 2 -DI me ,cfny 1 Lomat Pe ) otO 1 A 25 15.45 ve
Uhl or0 -3-Kluorobenzen(,? ( S ) 103
Laboretory Certificatibn
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABO* TORY ANALYSIS
Tars report shall not be reproduced, except n 18
without tre written consent of Pace Analytical Services,flc
Laboratory certificeirm I
KY Drinking Water 90090
TN UST List
VA Drinking Waler 213

PLE I UPLI .ATE: 92245299
tth liter
nzene
oluene
thy1 heroa
E p-Xyiere
7ylene (I,2-0 ethyl.Lenz
.L`hlaro-3. rirsc- tenzene 25)
methane
tyl 6
Labor ata alion IDS
NC Wteter 12
NC Drinking Water 37706
SC 99006
cal
lJ L'"
CONTR DATA
Chip
l ruts 92233881 Result RPD Footnotes
ught .°
Pace
5lien
Pace Analytical Services, Inc.
9800 Kinney Avenue, Suite 100
Huin ersvllle, NC zsoia
Tel [phone]
Fax: [phone]
CIAO'. 12 4 91
PAS.; 1ti
Jett ICU Piney Wood/195034
g L
0
ND NC
ND NC
ND
ND
NC
96
REPORT ANALYSIS
nking Later
TN UST List
VA Dfinking Water
Ttras report shalt not be reproduced, except sn full,
e written consent of Pace .Analytical Services,
213

e AnaJytical
„CALIT'f CO CL DATA P R El0TN0TE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite.100
Huntersville NC 2,8078
Tel: 70 - 7 -9092
Fax- 704- 7 - 091
DATE :° 4/98
PAGE: 11
Pace Project Number 23287
Client Project ID: Piney Wcc 1 1'0340
„ensttstent vritn EPA guidelines unfoundee cencentrattens are displayed and have been used tc caidui ate Pec and €1P0 vairyes.
"acted
Cal rr.)l ab
Deporting Lim
a
Pelati e Percent DItfcrence
gsarregat
NC Waste titer 1
# £ rink ng Water 37706
SC 99006
ANALYSISREPO OF BO TORY
This report strati not be reproduced, except in iur
vwritten consent of Pace .Analyt:ca9 Services, ors
tin
Y Onn ing " ater- 3C090
TN UST Ust
VA Drinking Water 21

SPECIALIZED ASSAYS, INC.
960 Foster Creighton Dr.
P.O. Box 40566
Nashville, TN 37204-0566
Phone [phone]
ACE ANAL YT I C AL 7228
7ELICIA GROG -AN
?SOO K1NC Y AVE STE 1 00
UNTERSVILLE, NC 28076
'rojEct:923287
ro ec t Name: P 1 NEY WOOD 1750340
i'1/41 L_ -r1 CL..FEFDFT
Lab Numb er 98—A155592
Sam p le ID: GRS EFFLUENT
Samp le Type: Water
Site ID.:
Date Co 1 1 ec ted: 12/ 77/99
Time CL-J1 1 ec ted: 14: 30
Date Received: 12/ 10/98
Time Received: 9: 00
AUPARIC PANIETED(
RiphthlIene
Acehipthene
Af/thrv:qme
FIuoranthefte
FIsfarehe
Pirehe
Gaio(,04athricehe
13,311roWpIrehe
Beazo(Whicrintheile
Phzo(kflucripthelle
Chrlseae
GihnWa,10.inthrmehe
Ii16.m)(1,2,3-od)pqrew
AceniphthIllhe
Silzo(1,h,Oprillene
PhehirithrenR,
ge5ult
RD
RD
RD
RD
RD
RD
RD
RD
RD
RD
ND
RD
RD.
RD
ND.
RD
= Act detected Bt tle report ).imit.
Iltraction Dt
Surrapte
Snits
Oil
Limit Limit Fictor Dite rime ftethod Ditch
1.0 1.0 1 12/1238 0111
1.0 1.0 1 12112/98 0:11
1.1111 0, 7 0, 7 1 1211238 0:11
tig/1 0,2 G, 2 1 12;1238 0:11
ug/1 0.2 0.2 1 1211238 0:11
tivl. G. 3 0. 3 1 12/12/98 0: 11
c111 G.1 0.1 1 12112198 0:11
0.1 0.1 1 12:12/98 0:11
1.1111. 0.2 0, 2 1 12/12/98 0: 11
filll 0.2 0.2 1 12/12/%3 0.: 11
uie'l 0.2 0.2 1 12,1_2198 0:11
u gil O. 3 02 1 12112/98 0:11
,J1.11 0. 4 0.4 1 1112/98 0:11
u1.11 2. 0 1. 0 1 1211238 0: 11
ti ql1 0_ 8 0, 8 1 12/12/98 0:11
U111 0, 6 0.6 1 122112/3 G:11
Extricted Extrict
-----------
?9t). 11 1.00
Aa4Ijit Nthail
12:11/9Z. FltNitr 310
PAR Surr. p -ter phenyl d14
Recover
54.
Tar.det R.e.31ge
------------
22, -' 141
Roorbikhlh 610
Roorbikhill 610
Roorblkh;ih 610
Roorbakhih 610
Nborbikhill 610
Roorbakhih 610
Rcorbikhih 610
Xclorbakhih 610
Kaorbikhill 610
RoorbildiJI 610
Hao0y*hitl 610
Koottikhih 610
't(oorbikhih 610
koorbikhi4 610
Hoorbikfit 610
Xoorbikk5h 610
37
3748
N48
3748
3748
37
a
374&
3748
3748
3748
3748
3748
3748
3718
.1- 1
COPY 1

fee
MISS *
Seel S ■! B.
N* SI
is SS
Allk
SPEC IZED ASSAYS, INC.
Mr Creighton
t7
-72 I77
Approved Bg
Number —:
Sap a : GRS EFFLUENT
Page
Tryeador Ph t.
rhea]: wr, Ter nice
Danny . Hale,S a or°a
Johnny A. Di ec a
CC ?1

SPECIALIZED ASSAYS, INC.
2960 Foster Creighton Dr,
PO, Box 40566
Nashville, TN 37204-056,6
Phone I-615-726-0 t77
F' Ft Li Ati
hal gte
pht haler*
Ace n pt trehe
Ant hr acene
FIuora Tither&
Fluttrene
Pgrehe
Deft2o,',, a)ant hrar..erte
rect a) mirth*
h)fluorant he he
De raw: k) Fluorant he*
Chr pin('
Di ben7o( a, h") ant hr acehe
Indeno,:1,2,3-cd)pgrerse
At-1, na phthglehe
8enzoi: g„h,i)perglene
P n ht hrehe
h gt
'piapht hal erre
Aoe n a pt het*.
Ant hracene
Fluor -ant herse
Fluor he
Pgreoe
De rs..7 M a) ant hr ace he
Ders2.0.>: pgrehe
Crzo.,: Fl vor BrA hew
'8enzo,:k.)Fluorarit he ne
Di rtz co: a h) ant hr ace he
'Tide ho;i 1 „2.„., 3-cd) grene
en apht hg.1 e he
hzo,: g „ h ) per gl e ne
gte
pht haler*
Ace h a pt her*
Ant hracene
FIuoranthehe
ftitrix Spike ReF:overg
units. Orig. 3J1,PI'S Val
rig/1
mg/1
419/1
mg/1
419/1
419/1
419/1
419/1
rsgil
419/1
mg/1
41
419/1
419/1
rtatrix 'Spike WO_
?Pi t4 t
g/l
gll
M9ii
mg11
m 911
mg/I
----------
0, r.;0106 C 00940
O. 00100 0, 0107
O. 00066 O. 0081.0
O. 00021 O. 00340
3,. 00021 00370
0. 00027 .0, OG.330.
G.,. 000I 3 0 00390
O. 00010 0. 00350
e. 0, 00013 0, 0.081At
O. (10017 0. 00.92.0
O. 00015 0, 013890
O. WO 3 Ct O. 00960
0, 00043 O. 008,60
O.,. 00200 0. 00830
e, O. ca76 a. oo7.91a
0„, 00064 O. 00320
Ur i
-G. 00940
01137
0, 00810
O. 0.0340
O. 00370
0, 00830
a, aueio
0. atina
cf. (tam
ona
ova
o, 000q.40
CL ao 30
0. 00790
0. 0082.0
L 4,S,r r t.r,)1 )171
0upl i orate
0. 0118
0. Mat
0, aci9s(4.
3. oa9.90.
a, ofroo
0100
13, 0103
O., 00970
O. 0105
0, 0106
O. 0.105
O. 01.04
O. 0103
0, 00940
00.9.90
0, 00960
'Spike CQ4C
0.0100
0.0100
O. 0100
O. ONO
0, 0100
O. 0,100
O. OHO
(1.0100
0, 0100
0.0100
0, 0100
0, 0100
0.0100
0, MO
O. 0100
O. 0100
13 Pt oat
Recover g
---------
74, 00
107, 00
81.. 00
34, 00
DO
38. 00
3.9. 00
85. GO
39, 00
92. 00
39, 00
96. DO
36, 00
33. DO
79. 0.0
32, GO
Target Range QC. Datch
-----------
51.
- 122.
42, - na.
25. - 112-
63. - 126.
57. - 114.
60. - 127.
62. - 112.
51_ - 119.
53. - 123.
57. - 123_
56. - 125.
- ,133.
59, - 127,
47. - 125.
60. - 123.
51. -
125.
RFD Linit O. i(atch
- - - -
22. 641 15. 3743
22. 92
3743
16. 95 19, 374:3
16. 39 19. 3743
7, 73 24, 3740
12.77 20, 3743
T.,.3 16, 3743
13.19 17, 3743
16,49! 16. 3743
14. 14 20, 3743
16, 49 17, 3743
3. 00 25, 3743..
17, 99 22, 3743
12, 43 30, 3743
22., 47 2:3 „ 3743
.15. 73 19. :374'3
JTi, 14;1711g-zed Ui Iarget R rig.e, O. C. 0 -at
_-_-_-_-__ ------------
0 0100 O. 5101
O. 0100 O. 00840
O. 0100 0,0930
0. 0100 O. 0091313
109
34.
93.
78.
------------
- 140
60 - 140
60 - 140
60 - 140
3748
3748
3748
3748
3748
3748
37
3748
3743
3748
3748
3748
3748
3748
3743
3748
3748
3748
3748
COPY 1

SPECIALIZED ASSAYS, LtiC.
2960 Foster Creighton Dr.
PO. Box 40566
Nashville.' TN 37204-0566
Phone l-615.726-0177
Laaoratary Control Data
11.%/0rene
Pipette.
4 enzo(a)an€Kracene
( )f1 anUeie
Lenzo(.1e,.) lu*s•anthere
R DL.„ A
Kncstn U.aI. 1 nalgze4 l), 1 r: Recauerg Target Range
0.0100 O.00 80
0,0100 0.+M1
0 , 0109 0. 0101
0,1)1013 0, 00950
0.0100 O. 0101
0, 01:3s1 O. 0102
0.0100 0.1t102
Rracene n9/1 0.0100 0.0103
{pgrene ng:`1 0, 0100 0, 0101
0, 0100 0,/308 0
lene ngr 1 10, 0100 0. 00960
0, 0100 0. 00920
G+1 Data
Klink Value On'F
>. O. NIA ng fl 3748
0,00100 ng1I 3748
�. 0. 00066 nil). 37 488
a, O. 00021 dill -'ii 4g
0,;10021 N9/i 3748
O. 00027 ngr'I 3748
0.00013 rt91I 3748
;, t), 00010 tigil 3748
.; 0,00018 ng<'I 3748
0,00017 riga 3748
0.00015 ng/I 3748
0_ 00030 HIV" 3748
0., 90043 ng<'1 37.48
9.00200 r1}4.. 3748
0,09076 ng,rl 3748
'0.00964 tt ^`1 37,18
COPY" 1
88. 60 - 1.40 3748
1 1. 60 - 1.40 3748
101. 60 - 140 3748
5. 60 - 140 3748
101. t+0 - 140 3748
102. 60 - 140 3748
102. 6) - 140 37.48
103. 60 - 140 3748
101_ 60 - 140 3748
86, 60 140 3748
96. 633 - 140 3748
9�, 60 - 140 3748

ace Anolytipal
PASI Inc: CharLotte
9899 KIGAAY Ave,
Suite 100
buntersvi L Le, NC 28078
Atte: Project management
Ehone: (704)87'5-9092
Solid resutt,s are reported on a lest weight basis
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Tel: [phone]
Fax [phone]
DATE: 12/16/98
PAGE: 1
Pace Project N r: 932682
Client Project ID: Shield 923287"
Pace SampIe No: 92127'660 Date Col. I:ebbed: 12/07798 Matrix: Water
ent Saelpte ID: ORS EFF1.JENT 11/4/98 92233360 Date Received: 12/10798
Earameters
4et 96emisTFY
Results bnITG PRI. Analyzed AnaLyst CAS# Footnotes
PIenalecs, Tots', RecoverabLe Met "a. EPA 420.1 Prep FleT.,hod: EPA 420.1
Phenol us, To t a I Recoverable ND bgi'L 0:005 12/15/98 KMII 108-95-2
NC Wastewater 40
NC Drinking Water 37712
SC Enwonmental 99030
REPORT OF LABON' ',TORY ANALYSIS
Ths report snail not be reproduced. except in futl.
w thout the wntten consent of Pace Analytcal Services. .11C,
LoQQttrULL tD,,a
TN Drinking Water C.
FL Environmental 963 7

ace Atia,lyt
PARA tR F
Nib
TEL
Nest Detected
Nbt ctltable
Pece Report frig
Pace Analytical Services, Inc:
54 Pavens r ft Drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 12, t6/98
PAGE : 2
Pace Prsaject Nt,Jriber: 932682
Client Project [ ; Shield 9287
Labratorrry ertirrcat n
NC Wastewater4(ii
NC €inin Water 3 r712
SC Environmental'
REPORT TORY
This report shall not be reproduced, except krs tint;
without the written consent of Pace Anelytcal ServIces, F
La.+arattry ertihasan lDS
TN DrinkingWater 02980
FL Env^irdnm

ace Arialyticai
SAS! Inc. Char ate
9800 Kincey Ave,
Suite 12:0
Auntersvitle, NC 28078
Attn: Project Management
shone: [phone]
OC Batch ID: 2922
Adakysis Metsod: EPA 420.1
Associated Pace samples:
QUALITY CONTROL DATA
93127660
Pace Analytical Services, Inc.
54 Ravenscrott Drive
Asheville, NC 28801
Fel: 704-254-7176
Fax [phone]
DATE: 12/16/98
PAGE: 3
Pace Art)ject 1 rt 932682
C1ient Pro et ID: Shied 923287
OC Saten Method: EPA 4201.
Analysis DescriptIon: Phcsnotics, Total Recoverable
METHOD BLANK; 93131993
Associated Pace Samptes:
93127660
Method
Stank
saramet,er Units Result RL Footnotes
^ m 4
Phenolics, Total Recoverabte mg/t
ND 0.005
AATRIX SPIKE: 93132058 Matrix
Spike Spike SPike
Parameter Units 93127603 Conc. Result % Res Footnotes
....... ..........
smenoLies, Total, Recoverab:e mg/I 0,108000 0.0250 0.03600 112
-ABORATORY CONTROL SAMPLE: 93132041
Spike LDS Spike
Ferameter Units Cons, Redutt % Red Footnotes
.......... ....... ..........
51B59luits, 507s1 Recoverable ms/L 0,..0250 0,02400 960
;AMPLE DUPLICATE: 93132033
Dup,
tarameter Umits 93128007 Result RSO Footnotes
Anent:tics, Teta: Recoverable Mg/L 2,202000 0.)08240 3
Laboratory Ceretication lOY
NC 17/ah1ewater 40
NC DfilikIng tiNater 37712
SC Environmental 99030
REPORT OF LABO TOR'Y ANALYSIS
This repast shaft not be reproduced, except in full,
without the written consent of Pace Analytical Seri/ices. ins
r 'fi n ID
TN Drinking Water 02980
FL Environmental 96117

ace Atiatytica41
Pace Analytical Services, Inc:
54 Ravenscraft Drive
Asheville, NC 28801
Tell 704-254-7176
Fax [phone]
DATE: 12/16/96
PAGE:
Pace Project N er: 932.7;2
Client Project 10: Shied 923387
DUALITY CONTROL DATA PARAMETER FOOTNOTES
Donsistent viith EPA guidelines unwounded concentrations are displayed and have been used to calculate % Rec and RPD values,
NO Not Detected
ND Not calculable
PRE Pace Reporting icimit
PPP Relative Percent Difference
boratory Certification t Db
NC Wastewater 40
INC Drinking Water 37712
SC Environmental 99030
EPORT OF LABO TORY ANALYSIS
True report shall not be reproduced, except in full,
without the wntien consent of Pace Analytcal Services, Inc
Laboratory CeritificsbDs [0:13,
TN Dtinkfrig Water 02580
FL Environmental 96317

Pace Ana
Cheat
Sampler Signature
TEM
NO.
Y'
SAMPLE DESCRIPTION
SHIPMENT METHOD AIR BILL NO.
Additional Comments
ca
Report Tu-
Bill To.
Name J No:
TIME MATRIX PACE No.
SHIPPING DATE OFCQONC ER
LERS
PRESERVATIVES
Temp:
Turn around Time
LI 24 Hours
48 Hours
.#.5 Days
1 Week 2 Weeks
°Normal 14 Days
ANALYSES,
S
.REQUEST
397549
CHAIN -OF -CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Project No, Cife,1
quested Due Da
REMARKS
RELINQUISHED SY A AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE
SAMPLE CONDITION
Recopied wed or r tr e : " YIN Sealed Cooler Y°! N
Samples Intact. fY ! N
SEE REVERSE SIDE FOR INSTRUCTIONS

ANA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Michael F. Easley, Governor William G. Ross, Jr, Secretary
Alan W. Klimek, PE. Director
Director
Mildred R. Berryhill
Tull Transport, Inc.
P.O. Box 327
Troutman, NC
Dear Permittee:
28166
February 1.0, 2006
Subject: NPDES Permit NCG510000 renewal
Certificate of Coverage (CoC) NCG510357
Piney Woods Quick Stop
Catawba County
The facility listed above is covered under NPDES permit NCG510000 for discharge of remediated
groundwater. NCG510000 expires on September 30, 2006. Federal (40 CFR 122A1) and North Carolina (15A
NCAC 2.1-1.0105(e)) regulations require that permit renewal applications must he filed at least 1.80 days prior
to expiration of the current permit. If you have already mailed your renewalrequest, you may
disregard this notice.
To satisfy this requirement, the Division must receive your renewal request postmarked no later than
April 3, 2006. Failure to request renewal by this ,date may result in a civil assessment of at least $500.00.
Larger penalties may be assessed depending upon the delinquency of the request.
Ifany discharge from the remediation system will occur after September 30, 2006, your Coe must be
renewed. Discharge of wastewater without a valid permit would violate North Carolina General Statute 143-
215.1; unpermitted discharges of wastewater may be assessed civil penalties of up to $25,000 per da,y.
If you have halted remediation activity due to lack of trust fund money, but your site ranking from the
Aquifer Protection Section requires future remediation & discharge, your CoC must he renewed.
If all discharge has ceased at your facility and you wish to rescind this CoC [or if you have other
questions], contact me at the telephone number or e-mail address listed below.
Sincerely,
Charles H. Weaver, Jr.
NPDES Unit
cc: Central Files
Mooresville Regional Office, Surface Water Protection
NPDES File
FEB 2 7 2006
1617 Mal Service Center, Raleigh, North Carolina 27699-1617
512 North Salisbury Street, Raleigh„ North Carolina 27604
Phone: [phone], extension 511 / FAX [phone] / charlesmeaver@ncmailmet
. One
NofthCarolina
Naturally
An Equal Opportunity/Affirmative Action Employer - 50% Recycled/10% Post Consumer Paper

DEh1 M©LRESV I LLE PA1
en
JAN- ®6-1999 17 : 01 FROM SHIELD ENV I RO 1ENTAL
A
TRANS
TTA]L SHEET
28481-85 Souti, suito 1i
Charlotte, North Carolina $208
Phone: [phone],
Phone: [phone]
Fax; 794) 394.6968
Division of Water Quality Telecopier No. 704-063- + 40
y, 'unwary 06, 1999
n: Richard Bridgernan Sender: Peter D. Jordan
of Pages Including This Transnaittal: , es
toed is e 5-day report for the permit lirnit exceedence at the abcve referenced facility. If
you have any questions or require any additional information please contact one.
Reference: Pineywoods Quick Stop
tamed in this facsimile message is legacy FRI
-._ded only for the use of the individual or entity rum
1pient (or the employee or agent responsiblett deliver i
any dissemination, distrihutkm or copy of this communi
rnunicstian in err©r, please notify us IMMEDIATELY
at the above address. Thank you"
as possible of any transmission problems,
CONFl NTIAL
lithe reader of this message
i', intended recipient), you are
strictly prohibited. ; if you
hone and return the original

JAIN-0E-1999 17:01 FROM SHIELD EMJ I RONMENTAL
end Bridgeman
Caxol .
every
several t x
If you have any+
704) 3` 4 69.3,
Since e y,
peter D .
Project Manager
so1ic& ASS) h" h exc `
TsS ii p
Co.
TO DEM MOORESOILLE P.02
tans. .gym
d exs.ve
Gen'orre
avedinai Palatal? Confer
28481.85 Sib'
Swift i r
Charlotte, WC
704.33469i$,
94

JAN-06-1" ' ' 17:03 FROM SH I ELL E LJ I RONMENTAL TO DIEM MOORESV I LLE F,03
Pace Analytical
93,00 Kincey Avenge 1
Huntarsv011e, IC2�8073 Tet CQy
Fax [phone]
v Ley the, la r°y
REPORT F LABORATORY ANALYSIS
report shag! not be repro:luc f, except in tuL
Consent of Pace Analyttcal Service , li

JAN-36-1999 17:04 FROM SHIELD Eh IRO1t1ENTF L TO DEM MOORESVILLE P,14
Date Collected:
. Date Received!
L
Methot EPA 200.7
24 m3/L , 0.05
;0' : IL 0.01
EPA 239..2
L 0,005 12/15/90
12/14/98
Pace Analytical.Serrices, Inc.
9800 Kinsey Avenue.. Suite 100
Harliersvitle.NC 28078
TOL 7047875.9092
Fat 704-875•9001
DATE: : 12/24/9$
Pea -
Pace Project I1untbar.: 923287
Client Pr41ect 10: Piney W000/1950340
Anal
Aa
' Prep Net o EPA
12/23/98 TYM 7439•86.t
12723/98 TYH 7439706.5
12122/' 8
Method:; EPA
7439.92.1
Ftn€�tes
7
OOF.
Prep Methcrt7EPA 160,2`
12!10/98 .]Mt
EPA 1664 Prep Het
mg/E 5 ' 12/15/9I3 DRP
EPA 601/602
ug/L ;
tag/L
ug/L
40/L 1
1
EPA 3510
Prep Methcicf, EPA 601/602
6SMP 107.06-2
smi2 183 04-4
L2/16198 SI4P 71.43.2
12/16/98 SMP 108 86.3.
12/16/98 SMP 10(-41-4
I2/16/98 SHP 7B16 64-0
12/166/96 SMP 95.4T 8
REPOT T OF LABORATORY ANALYSIS
This report shall not be reproduced, eiccapt in full,
* hvut the written consent of Pace AnayylIcal Services, trio.
U
VA *king Water

JAN—O6- 1999 17:04 FROM SHIELD ENVIRONMENTAL
DE1r1 MOORESU I LL.E P.05
92233360
GRS EFELUE
Pace Pro
Client
Pace Analytical lWinfices, Inv.
Win lancey Avenue. Suite WO,
Hu*t flee, 14C 28O a
Te1:704-875.9O92
Fax: [phone]O 1:
a4TC: 12/24/S8
PAGE: 2
923287
Piney Wood/1950344
Date Collected: 12/07/98 Matrix: Water
Date Received: 1Z/U8y98
iniis PRL Analyzed Analyst CAS#
12/16/98 SMP 625-98-9
REPORT OF BORATORY ANALY
be reproduced. except in full,
volhOtit the written sent of Pace Analytical Services, inc.
Threport
Rio notes

JAN-06-1999 1.7:05 FROM SHIELD ENVIRONMENTAL TO DEM MOORESUILLE P.06
Pace Analytical, Services, Inc.`
9800 klncey Avenue, Suite 100
tecls+rtlfe,1NC 28OT$
Tell: 704
.Fox 704-8T'r90
2/24/98
Pic Project Fleur*- 23
Client Project 10. Piney Wved/1950340.
REPORT OF LABORATORY ANALYSIS
7h+s report shall not be reproduced, except infull,
without the written °cement of Pace Analytical Services, Irv::
LEI mere M.:
lcr Dr . u
TN Us- List
VA Orinien; We
TOTAL P.06

DES Permit Number NCG510357
Authorization to Construct
Piney Wood Quick Stop
February 10, 1997
Engirt r"'sCertifcation
1, Paul. R. Wachsmuth, as a duly registered Professional Engineer in the State of North
Carolina, having been authorized to observe (periodically) the construction of the project,
Piney Wood Quick Stop , Catawba County, North Carolina for the Perrittee,
Project Name Location
hereby state that, to the best of my abilities, due care and diligence was used in the
observation of the construction such that the construction was observed to be built with
substantial compliance and intent of the approved plans and specifications.
Signature
Date March 5. 1997
f \document', f 9.503401'npdes;enge.cn
Registration No. 16. 23
Water Quality hereby
daviceplan.'eofthis. En irie rs

IPPState of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Ms. Mildred R. Berryhill
President
Tull Transport, Inc.
P.O. Box 327
Troutman, North Carolina 28166
February 10, 1997
DiVISIVI
Subject: NPDES Permit Issuance/Authorization to Construe
Permit No. NCG510357
Piney Wood Quick Stop
Catawba County
Dear Ms. Berryhill:
In accordance with your application for discharge permit received on July 31, 1996 by the
Division, we are forwarding herewith the subject Certificate of Coverage to discharge under the subject
state - NPDES general permit for petroleum contaminated groundwater remediation systems and one set of
final approved plans and specifications. Authorization is hereby granted for the construction and operation
of a 17,280 GPD groundwater remediation system consisting of a coalescing oil/water separator, a low
profile air stripper unit (two trays will be added to the existing three tray unit), and two carbon filtration
units with discharge of treated wastewater into an unnamed tributary to Murrays Mill Lake, a Class WS-IV
water in the Catawba River Basin. This Certificate of Coverage is issued pursuant to the requirements of
North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina
and the US Environmental Protection Agency dated December 6, 1983 and as subsequently amended.
Based on the source of your contamination, specifically gasoline and kerosene, effluent page A.
(3) applies to your facility and lists required effluent limitations and monitoring frequencies. Please note
that your stream classification is WS, which requires you to meet a Benzene limit of 1.19 µgr1 and to
monitor for Phenol..
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application and letter requesting coverage under an individual permit. Unless such demand is made, this
certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to
the Division of Water Quality. The Division of Water Quality may require modification or revocation and.
reissuance of the certificate of coverage in case of change of ownership or control of this discharge.
The Authorization to Construct is issued in accordance with Part III, Paragraph 2 of NPDES
Permit No. NCG510000, and shall be subject to revocation unless the wastewater treatment facilities are
constructed in accordance with the conditions and limitations specified in Permit No, NCG510000.
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]B3 FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Permit No. NCG510000
Permit Issuance/Authorization to Construct
Page 2
in the event that the facilities fail to perform satisfactorily, including the creation of nuisance
conditions, the Permittee shall take immediate corrective action, including those as may be required by this
Division, such as the construction of additional or replacement wastewater treatment or disposal facilities.
The Mooresville Regional Office, telephone number (704) 663 - 1699, shall be notified at least
forty-eight (48) hours in advance of operation of the installed facilities so that an in -place inspection can be
made. Such notification to the regional supervisor shall be made during the normal office hours from 8:00
a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays.
Upon completion of construction and prior to operation of this permitted facility a certification roust
be received from a professional engineer certifying that the permitted facility has been installed in
accordance with the NPDES Permit, the Certificate of Coverage, this Authorization to Construct and the
approved plans and specifications. Mail the Certification to the Permits and Engineering Unit, P.O. Box
29535, Raleigh, NC 27626-0535.
A copy of the approved plans and specifications shall be maintained on file by the Permittee for the
life of the facility.
Failure to abide by the requirements contained in this Authorization to Construct may subject the
Permittee to an enforcement action by the Division of Water Quality in accordance with North Carolina
General Statute 143-215.6A to 143-215.6C.
This permit does not affect the legal requirements to obtain other permits which may be required by
the Division of Water Quality or permits required by the Division of Land Resources, the Coastal Area
Management Act or any other Federal or Local governmental permit that may be required,
if you have any questions concerning this permit, please contact Jeff Myhra at telephone number
[phone], extension 597.
Sincerely,
Original Signed By
Da id A. Goodrich
A. Preston Howard, Jr., P. E.
Attachment
cc: Central Files
Mooresville Regional Office, W atr Quality Section
Facility Assessment Unit
Permits and Engineering Unit / Jeff Myhra
Mr. George E. Brant, Shield Environmental Associates, Inc.

STATE OF NORTH CAROLINA
DEPAR ENT OF ENVIRONMENT, HEALTH, AND NA
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG51009p
CERTIFICATE OF OVERAGE NO. NGG$103n
SOURCES
TO DISCHARGE PETROLEUM CONTAMINATED GROUNDWATER AND SITAR
WASTEWATERS UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as arnended,
Tull Transport, Inc.
is hereby authorized to construct and operate a 17,280 GPD groundwater re:mediation system for
gasoline and kerosene contaminated groundwater or similar waste streams with the discharge of
treated wastewater from a facility located at
Piney Wood Quick Stop
4549 East North Carolina Highway 10
Claremont
Catawba County
to receiving waters designated as unnamed tributary to Murrays Mill Lake in the Catawba River
Basin in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I, II, III and IV of General Permit No. NCGS10000 as attached.
This certificate of coverage shall become effective February 10, 1997
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day February 10, 1997.
Ortgi l igtfled Eiy
Devid h lGodri
A. Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

ROAD CLASSIFICATION
PRIMARY HIGHWAY I.IGHT.r3JrY ROAD, HARD OR
HARC SlIR;AC MMEMNIMil IMPROVED SURFACE
SECONDARY KEIHWAV
HARD SURFACE =MN= UNIMPROVED ROAD
Latitude 35`40'47* Longitude 81°06'18•
Map # E14NE Sub -basin 030832
Stream Class ws - Gv
Discharge Class Groundwater F medataar
Receiving Stream u.T. to Mu rays MilG Lake
Design Q 0.01728 MGD Permit expires 09/ 30/ 01
CONTOUR INTERVAL 20 FEET
Piney Wood QuickStop
NCG510357
Catawba County

CAROLINA BUSINESS CENTER
2848 i-85 SOUTH, SUITE F
CHARLOTTE, NC 28208
[phone]
1-800-395-5228
FAX: [phone]
November 18, 1996
Mr. E. Keith Overcash, P.E.
North Carolina Department of Envirorunent,
Health and Natural Resources
Mooresville Regional Office
919 North Main Street
Mooresville, North Carolina 2'8115
Reference: Cessation of Groundwater Remediation Activities
Piney Wood Quick Stop
Catawba County, North Carolina
Incident Number 8483
Dear Mr. Overcash:
This correspondence shall serve as the response to the North Carolina Department of
Environment, Health and Natural Resources (NCDEHNR) letter to Tull Transport dated
November 12, 1996 concerning a Notice of Violation of Commission Rule 15A NCAC 2H
.0204. As a result of a telephone call nude by Steven Bograd of the NCDEHNR, Mooresville
Regional Office, on October 14, 1996 to John Hill of Shield Environmental Associates, Inc.
(Shield), and including Brian Bishop of Shield and myself in conference, Shield deactivated the
groundwater treatment system (GTS) at the above referenced site on October 14, 1996. This
GTS, in its current configuration, is constructed to discharge treated groundwater into an
infiltration gallery located on -site.
As a result of the referenced phone conversation, it is Shield's understanding that this GTS,
regardless of the method of effluent discharge, should not be active until issuance of the NPDES
Permit for this site by the NCDEHNR. Shield, on behalf of Tull Transport, submitted an NPDES
Notice of Intent for Piney Wood Quick Stop to the NCDEHNR on July 15, 1996, but an NPDES
Permit has not yet been received. Pursuant to a recent request by Jeffrey Myhra of the
NCDEHNR NPDES Permits Group, Shield is currently providing additional information and
technical data regarding the proposed oil/water separator that must be reviewed by the Permits
Group prior to issuance of the NPDES Permit.
Shield has installed and activated a soil vapor extraction (SVE) unit at this site in accordance
with the Corrective Action Plan. Amendment dated February 5, 1996 and approved by your office
on May 29, 1996. This SVE unit is connected via underground piping to recovery well RW-6.
:Idoeumen tU 95©340Isv:deact.o tr
ATLANTA, GA • CHARLOTTE, NC
LEXINGTON, KY • PITTSBURGH, PA

Cessation of Groundwater Remediation
Piney Wood Quick Stop
Catawba County, NC
Though, as mentioned above, the GTS is now in five, the SVE unit rernains in operation s o
this date.
2
Should you have any questions concerning this correspondence or require additional information,
please contact me at [phone].
Sincerely,
ge E. Brant
Project Engineer
cc: Cissie Berryhill - Tull Transport
Steven Bograd - NCDEHNR Mooresville Water Quality Section
Rex Gleason - NCDEHNR Mooresville Water Quality Section
Bob Cheek - NCDEHNR Permits and Compliance Unit, Raleigh
R.D. Stonebraker - Shield. Environmental Associates, Inc.

State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr„ Governor
Jonathan B. Howes, Secretary
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
if).E-11\11FR,
DIVISION OF WATER QUALITY
November 12, 1996
Tull Transport
Post Office Box 327
Troutman, North Carolina 28166
Attention: Cissie Berryhill
RE:
Dear Ms, Berryhill:
Notice of Violation
15A NCAC 2H .0204-
Activities Which Require. a Permit.
Piney Wood Quick Stop
Site Priority Rank: 220B
incident Nig 8483
Catawba County, N.C.
A review of the Non -Discharge Permit Application, received
by this office on September 6, 1996, discloses that Tull
Transport is in violation of Commission Rule 15A NCAC 2H .0204
for operation of a non -permitted infiltration gallery at Piney
Wood Quick Stop, located at 4549 East North Carolina Highway 10,
Claremont, North Carolina, in Catawba county.
In order to correct the violation, Tull Transport must stop
operation of the infiltration gallery. Remediation activities
must cease until an appropriate permit is issued. You must
notify this office in writing within 7 days of receipt of this
letter, stating when the operation of the infiltration gallery
was discontinued. It should be noted that the violation cited
above and any additional documented violations could result in
the initiation of an enforcement action by this Office in
accordance with General Statute 143-215.6A, which provides for a
$10,000 assessment of civil penalties for each violation. Each
day that the violation continues may be considered a separate
violation.
919 North Main Street,
Mooresville, North Carolina 28115
Voice 704-663-1699
FAX [phone]
An Equal Opportunity/Affirmative Action Employer
50% recycled/10% post -consumer paper

Tull Transport
Incident NN 8483
Page Two
should you have any questions concerning this Notice,
contact Chuck Pippin at [phone], ext.268.
Sincerely,
Keith Overchsk, PE.
Regional Supervisor
cc: Rex Gleason - Mooresville Water Quality Section
Bob Cheek - Permits and Compliance Unit, Raleigh
George Brant - Shield Environmental Associates, Inc,

To:
SOC PRIORITY PROJECT: No
Permits and Engineering Unit
Water Quality Section
Attention: Jeffrey Myhra
Date: September 4, 1996
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Catawba
NPDES Permit No.: NCG510357
MR0 No.: 96-151
PART I - GENERAL INFORMATION
I. Facility and Addres : Piney Woods Quick Stop
% Tull Transport, Inc.
Post Office Box 327
Troutman, N.C. 28166
2, Date of Investigation.: August 30, 1996
Report Prepared By: Michael L. Parker, Environ. Engr. II
4. Person Contacted and Telephone Number: Mr. George Brant,
[phone].
Directions to Site: The site
quadrant of the jct. of Hwy.
eastern Catawba County.
, located in the southeast
and SR 1821 (Shiloh Rd.) in
6. Discharge Point(s), List for all discharge Points:
Latitude: 3540' 47"
Longitude: 81° 06' 18"
Attach a USGS Map Extract and indicate treatment plant si
and discharge point on map.
USGS Quad No.: E 14 NE
7. Site size and expansion area consistent with application:
Yes. Sufficient area exists for any expansion, if necessary.
. Topography (relationship to flood plain included): gently
rolling, 2-5% slopes. The site is not in a flood plain.
9. Location of Nearest Dwelling: Approx. 500± feet from the
proposed WWTP site.

!Illiiirlir'
10. Receiving Stream or Affected Surface Waters: U. T. Hurrays
Mill Lake
a. Classification: WS-IV
b. River Basin and Subbasin No.: Catawba 030 32
c. Describe receiving stream features and pertinent
downstream uses: The discharge will enter what appears
to be a zero flow tributary to a private lake. The lake
itself is not used as a water supply source, however,
the entire watershed is protected for water supply
uses. The lake ispart of, a historical site known as
Murray's Mill.
Page Two
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
I. a. Volume of Wastewater: 0.017280 MGD (Design Capacity)
b. What is the current permitted capacity: 0.003 MGD (non -
discharge Permit has not as yet been issued)
c. Actual treatment capacity of current facility (current
design capacity): 0.003 MGD
d. Date(s) and construction activities allowed by previous
ATCs issued in the previous two years: N/A
e. Description. of existing or substantially constructed
WWT facilities: The existing WWT facilities consist of
an oil/water separator followed by a. 600 gallon
equalization tank, an air strippingtower and a 300 ft'
infiltration gallery.
Description of proposed WWT facilities: The applicant
proposes to add carbon filters and a new oil/water
separator.
g. Possible toxic impacts to surface waters: Toxic
impacts have been documented in the effluents from GW
remediation systems. Consideration should. be given to
requiring toxicity testing.
h. Pretreatment Program (POTWs only): Not Needed,
2. Residual handling and utilization/disposal scheme: Residuals
generation is not expected.
Treatment Plant Classification: Class I
4. SIC Code(s): 0000 Wastewater Code(s): 66
5. MTU Code(s): 56000

Page Three
PART III - OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grant
Funds or are any public monies involved (municipals only)?
No
2. Special monitoring or limitations (including toxicity)
requests: See Part II, No. 1(g).
3. Important SOC/JOC or Compliance Schedule dates: N/A
4. Alternative Analysis Evaluation
a. Spray Irrigation: Insufficient area
b. Connect to regional sewer system: None availahle
the site.
c. Subsurface: The applicant is currently using an
infiltration gallery, however, a proposed increase in
flow is expected to exceed the infiltration gallery'
hydraulic capacity.
d. Other disposal options: None that we are aware,
PART IV - EVALUATION AND RECOMMENDATIONS
The applicant, Tull Transport, Inc. (TTI), requests the
issuance of an NPDES General Permit for the remediation of
gasoline and kerosene contaminated GW at the subject facility,
The contaminated GW is presently being treated by an existing
infiltration gallery for which a non -discharge Permit has been
applied for. Since the permittee is projecting an increase in
flow, and the existing WWT system is incapable, of handling any
additional flow, the applicant haschosen to apply tor a Permit
to discharge.
The discharge will enter surface waters presently classified
as a water supply. The DEH-Public Water Supply Section will need
to provide comments prior to Permit issuance,
Pending concurrence from the DEH and a technical review and
approval by P&E, it is recommended that an NPDES Permit he
issued.
Signature
Preparer Date
Water na S p_tvlso Da
10dWdsrg6\Piney.sr

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State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
)'
Mildred R. Berryhill, President
- Tull Transport
P.O. Box 327
Troutman, North Carolina 281.66
August 6, 1996
1""*"1
CALTH,
AUG 9 1996
MISHINr ENVIMMENTAt MANAGNUIT
MUNESILE RLaioNki
Subject: Permit Application No. NCG510357
Piney Wood Quick Stop
Catawba County
Dear Ms.. Berryhill:
The Division of Water Quality acknowledges receipt of the following information:
• Notice of Intent (NOI) for-m.
• NPDES Application Engineering Report.
• S550.00 application fee.
The Division has performed a preliminary review of the proposed treatment system. Based on this
review, the Division requires that more information be provided. Please address the following
issues:
• Please ovide the size (in gallons) of the separation chamber and the sludge chamber
for thc oil/water separator.
• Please provide the capacity of each carbon canister (in pounds). The canister capacity
identified in appendix B was illegible.
The Division recommends that the subject facility consider implementing a filtration system as part
of the remediation process to filter out naturally occurring iron and manganese in the groundwater.
These groundwater constituents often blind carbon systems and impair treatment efficiency.
By copy of this letter, I am requesting that our Mooresville Regional Office Supervisor prepare a
staff report and recommendations regarding this discharge. Your will be advised of any
comments, recommendations, questions, or other information necessary for the application review.
Should you have any questions, please do not hesitate to contact me at [phone], extension
597.
effrey T. Myra
NPDES Perrints Group
cc:
ermits and Engineering Unit
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10°4 post -consumer paper

AUG 1 6 € 96
CAROLINA BUSINESS CENTER
2848 1-85 SOUTH, SUITE F
CHARLOTTE, NC 28208
[phone]
1-800-395-5220
FAX: [phone]
Aunt 15. 1996
Mr. Jeffrey Myhra.
NPDES Permits Group
State of North Carolina
Department of Environment, Health
and Natural Resources
Division of Water Quality
P.Q. Box 29535
Raleigh, North Carolina 27626-0535
Subject: NPDES Permit Application No. NCG510357
Piney Wood Quick Stop
Catawba County
Dear Mr. Myhra:
Shield Environmental Associates, Inc. (Shield), on behalf of Tull Transport, is submitting this
correspondence in response to your letter, dated August 6, 1996, which requested additional
information pertaining to the above referenced permit application.
The following items provide the information requested by the Division of''ater Quality in the
aforementioned letter:
For the oil/water separator (Hydro -Flo Technologies, Inc. Model, DP-008 or equivalent),
the capacity of the separation chamber is 137 gallons. The capacity of the sludge
chamber is 19 gallons. See Figure 1 for oil/water separator drawings and specifications.
The Model GX-200/W carbon units by Enviro-Industries, Inc. have a capacity of 150
pounds per canister.
The En -Industries Model GX-200IW carbon units are specifically designed to
accommodate iron and manganese which can be found in groundwater. These carbon
units employ a bottom -to -top flow of water. The influx of water up the interior side walls
of the canister regularly rotates the carbon bed providing a backwashing effect which
reduces iron and manganese fouling. Based on our experience with active remediation
systems at numerous sites, the GX-200/W units require no prefilters to successfully
e\docament1195o34olapdartnpdinfo.add
ATLANTA, GA • CHARLOTTE, NC
LEXINGTON, KY • PITTSBURGH, PA

NPDES Pe Application No. NCG510357
Piney Wood Quick Stop
Catawba County
operate even at loci
Therefore, Shield fee
iron and tnang e occur at
n syste
ood Quick Stop
Should you have any questions orr• ," additio nfo
6913.
no * levels..
needed as of t.

C ESC►G SURFACE AR
G SURFACE AREA
COALESCING SURFACE AREA
PING WEIGHT
WEIGHT
CHAMBER CAPACITY
CHAMBER CAPACITY
R CAPACITY
WARIER CAPAPCITY
PARATOR CAPACITY
TRANSFER —
TRANSFER
A/8 NILYIC
I AJ° HIGH
YE`THYL£NE
NDARO DRLI
VY' DUTY Ali
VATED PLAT+
177 C.L.
F
FOR
FOR
¥NA— P.
DYNA— PAK
DYNA PAK
THT GLASS ASSEMBhT
Exl&E HOSE ASSEMBG
DISCONNECT
IL LEVEL 5.5. SWITCH
DESCRIPTION
dRFLUEHT DIFFUSION CHAMBER
INFLuENT DIFFUSION BAFFLE
SEPARATION CHAMBER
REMOVABLE PVC DTNA—PAK
HAW DUTY GASKET, "IY SHAPED
EFFLUENT WEIR
EFFLUENT SHEEN BAFFLE
EFFLUENT CHAMBER
REMOVABLE LID WITH HANDLES
ROTARY PIPE 01L SKIMMER
SLUDGE COLLECTION CHAMBER
AV AIi ABLE bl at V#RII US COALESCING MEDIA TYPES
PVC — CPVC — POLYPROPYLENE — FIBERGLASS
VARIOUS MEDIA PLATE SPACINGS — M15r — /2I — 34
PLEASE CONSULT THE FACTORY FOR SPECIFIC SIZING
CRITERIA, OPTIONS do APPLICATION INFORMATION
SC UPfl
IL RE5ERV01
LACK REIItA:
UOGE OWL .EI / ©RAIN,
L 'OUTLET I VENT, 2"o
L RESERVOIR' 4NIET. 2'A
RESERVOIR OUTLET, 2""r
EARANCE REQUIRED FOR DYNA—P
OYNA—PAK COALESCING TYPE OIL/WATER SEPARATOR
WITH ROTARY PIPE SKIMMER
MOLDED FIBERGLASS CONSTRUCTION
DP-008 GENERAL ARRANGEMENT DRAWING
P—S008—AO I

NOTICE OF ENT
ES`
STOP'
4549 EAST NOR C 0 A HIG AY 10
CAATA A COi C , T.1 A
D ER 1950340
Tull Tr posit
P.O. Box 327
Tr Carolina, 28166

State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Natjo
A. Preston Howard, Jr., PEE.
Acting Director
NOTICE OF INTENT
Pollutant Discharge Elimination System
Application for NPDES individual Permit; Groundwater remediation projects designed to treat petroleum
contaminated groundwater.
Name, Address, location, and telephone number of facility requesting Permit.
A. Official Name:
B. Mailing Address:
(1)Street Address;
(2)Cit ;
(3)State;
(4)Zip;
(5)County;
C. Location. (Attach map
(1)Street Ad
(2)City;
(3)State;
(4)County;
D. Telephone Number;
Facility Contact:
A. Name;
B. Title;
C. Company Name;
D. Phone Number;
Piney Wood. Quick Stop
c/o Tull Transport
P.U. Box 327
Troutman
NC
28166
Iredell
,litteating general facility location Figure 1)
ess; 4549 East North Carolina Highway 10
Claremont
NC
Catawba
[phone]
Ms. Mildred R. Berryhill
President
Tull Transport
[phone]
3, Application type (check appropriate selection):
A. New or Proposed; NEW
B. Existing; if previously permitted, provide permit number: NA, and issue date:
C. Modification;
(Describe the nature of modification):

Notice of Intent for Coverage
Under NPDES Individual Permit
Piney Wood Quick Stop, Catawba County
4. Description of discharge
A. Please state the number of separate discharge points.
One discharge point only.
B. Please describe the amount of wastewater being discharged per each separate discharge point:
One discharge point at 17.280 gallons per day (12 gpm system design flow rate).
C. Check the duration and frequency of the discharge, per each separate discharge point:
1, Continuous, 7 days per week.
2. Intermittent (please describe):
3. Seasonal (check month(s) the discharge occurs): January(}; February(); March{}; April{};May{};
June(}; July(); August{}; September(); October(); November(); December().
4. How many days per week is there a discharge?(check the days the discharge occurs): Monday{},
Tuesday I , Wednesday{}, Thursday(}, Friday { }, Saturday{}, Sunday(},
5. Row much of the volume discharged is treated?(state in percent) 100 %
D. Describe the type of wastewater being discharged per separate discharge point. Specify what is being removed
and products recovered. This includes a listing of any chemicals found in detectable amounts with the maximum
observed concentration reported. The summary of analytical results containing this maximum value should also
be submitted (i.e. the listing, not the graphical scan). The most recent sample must be no older than one year
previous to the date of this application. The following volatile organic compounds should be included along with
any suspected fuel additive;
The current wastewater is groundwater collected from a shallow, unconfined aquifer and treated by a low
profile air stripper and granular activated carbon filtration The remediation system will be equipped
with an oil/water separator to remove any remaining liquid phase hydrocarbons prior to treatment. The
analytical results listed below are those required by DEM and are presented as the "Worst Case Well,"
MW-5, except as noted. The laboratory analytical results are included in Appendix A.
Sample Date; April 1996 (unless otherwke notedi
1. Benzene*;
2. Toluene*;
3, Ethylbenzene*;
4. Xylenes";
5. Lead;
6. Methyl tert-butyl ether (MTBE);
7. 1,1-Diehloroethane;
8. 1,2-Dichloroethane;
9. Isopropyl ether;
10. Naphthalene;
11. Phenol
12. Trichlorofluoromethane
13. Dichloromethane (Methylene Chloride)
7,500 lig/I
55,000 ptg/I**
4,400 u.g)1**
22,000 ug/1**
17 ug/I***
2,300 ugr*
1.8 lign****
20 ig,/1'
390 ug/I
1,030 AO
Not tested
1.3 ng/1"
120 ug/IAAA
* An EPA approved method capable of detection levels to 1 ppb was used to detect these compounds.
** Collected from well MW-9 in July 1995.
*** Collected from well MW-12 in July 1996. Determined to be consistent with naturally occurring lead levels at
this site.
**** Collected from well DMW-1 in July 1995.
Collected from well MW-7 in July 1995.
44 Collected from well MW-1 in July 1995.
"4 Collected from well RW-6 in April 1996.
Sampling for these parameters will take place during the initial start-up of the groundwater treatment system if
requested.

Notice of Intent for Coverage
Under NPDES Individual Permit
Piney Wood Quick Stop, Catawba County
E. Please check the appropriate type oftreatment being used to treat the groundwater;
1, f?'iUWater Separator; X.
2. Low Profile Air Stripper; X
3. Diffused Aeration;
4. Activated Carbon Adsorption; X
5. ©ther(specify);.
6. Separately, please describe in detail(size, volume, capacity, design flow through treatment, etc.) each
type of treatment that was checked in 1 through 5. Include, if any, the manufacturer's information on
each type of treatment. Also provide the removal efficiency of each compound detected for the project,
if known. Give design specifics (i.e. design volume of each unit, materials used in air stripper, etc.).
Existing treatment facilities should be described in detail and design criteria or operational data should
be provided(including calculations) to ensure that the facility can comply with requirements of the
General Permit. Please include model and calculations used in determining the design requirements
for the air stripper.
Information regarding the design specifics of the above checked treatment equipment has been
attached in Appendix B. The groundwater treatment system design is presented in Figure 2,
Proposed System Layout, with equipment specification listings presented in. Table 1.
An existing groundwater remediation system, which discharges treated wastewater into an
infiltration gallery, is currently operational on -site.. The existing oil/water separator does not have
sufficient capacity to handle the proposed increased flow and therefore will be exchanged. The
specifications for the new oiVwater separator are included in Appendix R. Predicted contaminant
removal efficiencies after air stripper and carbon units are presented in Table 2 representing a
12 gpm flow rate and a 5 tray air stripper. The existing air stripper will be modified by adding
trays and a new blower to become a five tray unit. Refer to Appendix C for air stripper and
carbon usage calculations provided by vendors.
NOTE: The carbon usage rates are based on the conservative assumption that all six (6) recovery
wells are "worst case." Actual contaminant levels are much lower for a weight averaged flow of
the six recovery wells. Actual carbon usage should be significantly Tower than the quoted rates.
7. What are the well sizes and how many exist.
Six recovery wells (RW-1 through RW-6) exist on -site at the locations presented in Figure 3,
Proposed Site Plan. All recovery wells have 30 feet of 0.020 slot screen at the bottom of the well.
The total depth of the wells from ground surface is provided below:
RW-1 45'
RW-2 45'
RW-3 47'
RW-4 45.5'
RW-5 51'
RW-6 40'
8. Please state the pump sizes and their location in relation to the treatrtaent used in part 2.E.
The existing submersible recovery pumps are Grundfos Model 5E5's and will be sufficient to
continue service in recovery wells RW-1 through RW-5. Additionally, a Grundfos Model SE$
submersible recovery pump will be installed in PRW-6 to collect groundwater and deliver it to
the system.

Notice of Intent for Coverage
Under NPDES Individual Permit
Piney Wood Quick Stop, Catawba County
Refer to Figures 2 and 3 for the pump locations in relation to the groundwater treatment system.
The existing 1/2 HP Myers transfer pumps will be sufficient to provide the necessary flow and
pressure required for this configuration and will not need to be replaced. Refer to Table 1 for
component specifications and. Appendix B for manufacturer equipment specification sheets,
9. Please explain what fail-safe measures, such as audible and visual alarms or automatic shutoff systems, are
provided to ensure no system failures.
The oil/water separator and air stripper collection tank will tb be equipped with glow, high, and
high -high level shut off features to ensure that the recovery well pumps will shut off prior to
system overflow. The carbon units will be equipped with pressure gauges to ensure safe
operation.
In addition, the on -sate control panel is equipped with visual normal/alarm lights and manual
override switches.
10,. Is there an access to the effluent for sampling? (either an open pipe or a valve to obtain a sample).
Yes. The following effluent sampling locations will exist: One after the oil -water separator and
before the air stripper, one after the air stripper and before the first carbon filtration unit, one
between the two carbon filtration units and one at the discharge point. ,.Refer to Figure 2 for
sampling port locations.
NOTE: Construction of any wastewater treatment facilities require submission of three (3) sets of plans and
specifications along with their application. Design of treatment facilities must comply with requirement 15A.
NCAC 2H .0138. If construction applies to the discharge, include the three sets of plans and specifications with
the application.
What is the nature of the business applying for this permit,
Petroleum products distributor.
6. Name of receiving water or waters;,Muf['ays Ntill. , ite, Classt scat on: tom Attach a USGS topographical map
with all discharge point(s) clearly marked)
See Figures 4 and 5.
7. Is the discharge directly to the receiving water?(Y,N) No.
If no, state specifically the discharge point. Mark clearly the pathway to the potential receiving waters on the
site map. (This includes tracing the pathway of the storm sewer to its discharge point, if a storm sewer is the
only viable means of discharge).
The effluent will be discharged to an unnamed intermittent tributary feeding Murrays Mill lake.
See Figure 4 for the discharge location and pathway to Murrays Mill Lake,
Please address possible non -discharge alternatives for the following options:
A, Connection to a Regional. Sewer Collection System;
No Regional Sewer Collection System available.
4

Notice of Intent for Coverage
Under NPDES Individual Perrttit
Piney Wood Quick Stop, Catawba County
13, Subsurface Disposal,
Insufficient area, Existing infiltration gallery has proven inadequate in handling, discharge.
C. Spray Irrigation;
Insufficient area. Site and surrounding properties are heavily wooded.
I certify that I am familiar with the information contained in the application and that to the best of my knowledge
and belief such information is true, complete, and accurate.
Printed Name of Person Signing
Date Application Signed i 1 \ `1 6
Signature of Applicant s ► \ ,
4
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan or other document filed or required to be maintained under Article 21 or regulations of the Environmental
Management Commission implementing that Article, or who falsifies, tampers with or knowingly renders inaccurate any
recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the
EnvironmentalManagement Commission implementing that Article, shall be guilty of a misdemeanor punishable by a
fine not to exceed S 10,000, or by imprisonment not to exceed six months,.
or by both.(18 U.S.C.Section 1001 provides a punishment by a fine of not more than SI0,000 or imprisonment not snore
than 5 years, or both, for a similar offense).
Notice of Intent must be accompanied by a check or money order for S400.00
made payable to the North Carolina Department of Environment, Health, and
Natural Resources. Mail three (3) copies of entire package to:
Division of Environmental Management
NPDES Permits Group
Post Office Box 29535
Raleigh, North Carolina 27626-0535
5'

iEtIC N'ORMN
SWEET
CATAWBA, N.C.
N3537.5-W8100I7.5
1970
SITE LOCATION MAP
PINEY WOODS QUICI{ STOP
CL,AREMONT,, NORTH CAR©LINA
A i�03/95, . OR RCS
SCALE ; AS.
HOWN I
WN BY
CURE
N'W1RONMENTAL A OCIAT , .

MODIFIED
'T1IAI.LOw TRAY
AIR sTRIT`I''P;R
!EATING
MENT/TSTAT
'Ufi1S
ROOSVE
EXISTING
NOT'3TUR : , " CONCRETE
F,i°ARAT(I I F'AD
(NEw) SOIL VAPOR
EXTRACTION UNIT
A
Tn Nr IFs
EFFLUENT-'
FLOW MEYER
LEGEND'
t9PS
OPr FRF,SSIMF GAIICF;
Tr TRANSFER I*Uki!h
Rif Ri;('ovrRY WELL
SAFITI,F PORT
BALL vAvl,P:
EFFL1.IENT now METER
Ft,tm tip
:4vE vACt11TU LIMP;
EXI5T1N0 EQUR'MENT
jIC.1 d
AT SwITCtIES
NEW
Olt./w'ATER
SEPARATOR TANK
R£MoVA
*XP INC TANK)
FREE RQ UCT
:RAVI'TY FLOW
A
(XISTUMCNCCHAIN
K E E
0m Rw _ 1. . 1. 4, 5,
O OSLU , SYSTEM LAY-oi
NEY ' OD I) ,I.0
AST NORTN CAROUNA tl101tWAY tEt. CTARIOtONT
CA ATM COUNTY tORTt CAftOUNA
ATE; ANC.

TABLE 1
Equipment Specifications* for Additions to Groundwater Treatment System
PINEY WOOD QUICK STOP
Additional
Quantity Quantity Description
Existing Required
One
Three
Trays
One
None
Five
Two
One
One
None
None
One
One Oil -water separator, Hydro -Flo Model DP-8-F 21 or
equivalent.
Two Trays Modify ShallowTray Low Profile Air Stripper
Model 1331 to make equivalent of Model 1351.
One
Replace existing air stripper blower with new model
rated at 5 hp, 150 cfrn, 22"wc to accornodate
additional stripper trays.
Two Carbon filtration units, Enviro-Industries, Inc.
Model GX-200/W in series.
One
Grundfos submersible electric recovery pump
Model 5E8, or equivalent, supplied with discharge
hose and check valve..
None Myers 1/2 HP transfer pump.
None 500 gallon product collection tank.
None 500 gallon equalization tank.
One
One
One
Recirculation line for air stripper effluent to be used
as necessary to increase water treatment efficiency
and thereby improve carbon life.
Soil vapor extraction unit, Geopure Continental
Model 200SVE, or equivalent; pre -assembled, rated
for exterior operation, mounted to steel skid -stand
and including individual control panel and discharge
stack with rain guard.
Control panel addition/modification (existing panel
controls operation of system and five submersible
pumps; panel will be expanded to control additional,
submersible pump and new, larger air stripper /
blower).
Final Design - Not For Construction
f Idoeument1194O4'36ktable l.npd

V
2
c,
a

Pace Ankykki Setvic's. Inc.
9800 Itancay Avenue, Suit! 100
Iiunetsnle, NC 28078
Tot 784 875.9092
Fkc 704 875.9091
14
July 08, 1996
Mr. Brian Bishop
Shield Environmental Associates, Inc.
2848 I-85 South
Suite H
Charlotte. NC 28208
RE: PACE Project No. 660703.52I
Client Reference: 1950340/Pi Heywood
Dear Mr. Bishop:
Enclosed is the report of laboratory analyses for samples received
July 03, 1996.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Felicia C Grogan
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
whit the written consent of Pace Anaiydcal Services. inc

Pace Anafiticat
Shield Environmental Associates, Inc.
2848 1-85 South
Suite H
Charlotte, NC 28208
Attn: Mr. Brian Bishop
Client Reference: 1950340/Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
July 08, 1996
PACE Project Number: 660703521
92 0627342
07/03/96
07/03/96
MW-5
Units OD DATE ANALYZED
Acid Digestion Date 070396 3030C 07/03/96
Lead W/3030C Digestion mg/L 0.005 0.011 239.2 07/05/96
REPORT OF OR TO "" A ►;L,YSIS
s report Mal not be re•d.
without the written of P. Ansiytkai sennos., roc.

Mr. Brian Bishop
Page 2
Client Reference: 1
0340/Pine
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Acid Digestion
Lead W/3030C Digestion
ad
Units
T. Tt 875.9
Fm 70t4175-9091
July 08, 1996
PACE Project Number: 660703521
92 062.7350
07/03/96
07/03/96
MW--12
0 OA
ANALYZED
070396 3030C 07/03/96
0.005 0.017 239.2 07/05/96
These data have been reviewed and are approved for release.
Margaret S. Harding
Manager, Laboratory Operations.
REPORT OF LA TO ` ANALYSIS
This ispixt WWI n©S aa ravevdd, aax; -,A In rum,
*manta the *Mean mutant at Pace Analytical Sarviees, tr+c.

ent Referenda: 1
od t
July 99, 1996
PACE Pro ec

Mr. Brian Bishop
Page 4
QUALITY CONTROL DATA
Client Reference: 1950340 Pinevw!ood
Lead W/3030C Digestion
Batch: 92 47968
Samples: 92 0627342, 9Z 0627350
METHOD BLANK:
Parameter - Unit:
Lead W/3030C Digestion
SPIKE AND SPIKE DUPLICATE:
Parameter
Lead W/3030C Digestion
Tit 7 4 875-9092
Fax [phone]
July 08, 1996
PACE Project Number: 660703521
Method
Blank
DS N6
Units MDL
RTC— U7C5
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Parameter
Lead W/3030C Digestion
Spike
Spike Dupi
Recv 'Recv RPO
T%
Reference Dupl
Units MDL Value Recv Recv RPD
d05 0.025 75
REPORT OF LABORATORY ANALYSIS
This report shall not be r.pro duced. sweet in
withal the written cement at Pace Areagytleai Sievices, Inc.

OTES
far page
Reference: 1950340/Pin ywood
Method tie®
Not dete
Relative
ec ion Limit
aA or above s the
P ant Difference
July 8, 1996
PACE Project N

Sa
y ('R,INT):
Sarnpl a Signature
SAMPLE pESCI iPTlOtt TIME MAT PACE NO.
2
4
6
iIWENT ts1ETNOD
ATE RETURNED DATE
Additional Comments
To:
mBlllir
Project Name i
ll`S RVATIVES
3J.
CHAIN -OF -CUSTODY RECORD
Anelyllcel Request.
: pace Client Nd. yt I 3
ace Protect Manager
�ueeted Due Date:
SEE REVEdSE SIDE FOR INSTRUC:TIoNS

Pace Analytical ,
A
May 13, 1996
e at "110 A m T •
Mr. David Maxam
Shield Environmental Associates, Inc.
21348 1-65 South
Suite H
Charlotte, NC
RE: PACE Project No. 660429.504
Client Reference: 1950349/ Pineywood.
Dear Mr. Maxam:
Tel: [phone]
Fax: [phone]
,MAY j 1994
Enclosed is the report of laboratory analyses for samples received
April 29, 1996.
. Footnotes are given at the end of the report.
If you have any questions concerning this report, please faei free
to contact us.
Sincerely,
Felicia C Grogan
Project Manager
Enclosures
C
Aire, ovookt
REPORT OF LABORATORY ANALYSIS
Mc report shad net be reproduced. except in kg.
%relate the written ocinsent of Pace Analytical Services, Inc.

Shield Environmental Associates, Inc.
2848 I-85 South.
Suite H
Charlotte, NC
Attn: Mr. David Maxam
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Elate Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene
Date Extracted
PURGEABLE HALOCARBONS AND ARC
Dichlorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichorofluoromethane
I,1-Dichlaroethene
0ichioromethane
trans-1,2-0ichloroethene
1,1•-Dichlaroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichloroethene
1,2-0ichloropropanne
Bromodichlormethane
2-Chloroethoxyethene
cis -1,3-0ichlaropropene
trans-1,3-0ichloropropene
1,1,2-Trichlaroethane
Tetrachloroethene
Di brvmachloromethane
Bromoform
1,1,2,2-Te
achloroethane
AT
CS
Pace A/laryrocal Services. !rm.
9800 'IGncey Avenue. Suite 100
Huntersvlile. NC 28078
Tel: [phone]
Fax [phone]
May 13, 1996
PACE Project Number: 66042950
92 0589483
04/29/96
04/29/96
MW-4
Units
ug/L 1.2 NO
Date
ug/L
ug/L
ug/ L
ug/1.
ug/L
ug/ L
050196
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 ND
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
NO
NO
NO
NO
NO
NO
NO
4.1
NO
NO
NO
NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/ L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
610
601/602.
DATE ANALYZED
05/02/96
05/01./96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
REPORT OF LABORATORY ANALYSIS
Tail report shalt net be reproduced, except in full.
without t?re written consent of Pace Anatydpl 5e vieaes, Inc.

Mr. David Maxam
Page 2
Client Reference: 1950349/ Pineyr>od
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS ANO AROMATICS 601/602
Methyl-t-butyl ether ug/L 1.0 13 05/04/96
Isopropyl ether ug/L 1,.ii 6.7 05/04/96
Benzene
ug/L 25 100 . 05/04/96
Toluene ug/L 1.0 22 05/04/96
Chlorobenzene ug/L 1".0 NO 05/04/96
Ethylbenzene ug/L 1.0 3.6 O5/04/96
Xylenes ug/L 1.0 51 05/04/96
1,3-Dichlorobenzene ug/L 1.0 NO 05/04/96
1,4-©ichlorobenzene ug/L 1.0 NO 05/04/96
1,2-Dichlorobenzene ug/L 1.0 NO 05/04/96
May 13, 1996
PACE Project Number: 66042950
Units
92 0589483
04/29/96
04/29/96
MW-4
METHOD OAS' ANALYZED
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
without me written consent of Pace Anaydcal Services, Inc.

Pace, Ana ytica
Pace naryncai Services, Inc.
9800 KGncey Avenue, Suite 100
Hturtefsville. NC 28078
Mr. David Maxam May 13, 1996
Page 3 PACE Project Number: 66042950‘
Tel: [phone]
Par 704.875.9091
Client Reference:/950349/ Pine y reed
PACE Sample Numbers 92 0589491
Date Collected: 04/29/96
Date Received: 04/29/96
Client Sample ID: MW-5
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene
Date Extracted
Units MDL MEI EOD DATE ANALYZED
ug/L 1.2 1030
Date 050196
PURGEABLE HALOCARBONS AND AROMATICS
Dichlorodifluoromethane ug/L 10 NO
Chloromethane ug/L 10 NO
Chloroethene (Vinyl chloride) ug/L 10 NO
Bromomethane ug/L 10 ND
Chloroethane -ug/L 10 NO
Trichlorofluoromethane .ug/L 10 ND
610
601/602
96
96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
1,1-Dichioroethene ug/L 10 NO 05/04/96
Dichloromethane ug/L 10 NO 05/04/96
trans-1,2-Dichloroethene ug/L 10 NO 05/04/96
1,1-0ichloroethane ug/L 10 ND 05/04/96
Chloroform ug/L 10 NO 05/04/96
1,1,1-Trichloroethane ug/L 10 ND 05/04/96
Carbon tetrachloride
1,2-0ichioroethane
1,1, 2--Tri ch l oroethene
1,2-0ichloropropane
Bromodichlormethane
2-Chloroethoxyethene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
I,1,2-Trichloroethane
Tetrachloroethene
Di bromochloromethane
8ramoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
ug/L 10 NO
ug/L 10 NO
ug/L 10 ND
ug/L 10 ND
ug/L 10 NO
ug/L 10 ND
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
ug/L 10 NO 05/04/96
ug/L 10 NO 05/04/96
ug/L 10 ND 05/04/96
ug/L 10 NO 05/04/96
ug/L 10 NO 05/04/96
ug/L 10 NO 05/04/96
ug/L 10 NO OS/04/96
ug/L 20O 930 05/04/96
ug/L 200 390 05/04/96
ug/L 2O0 7500 05/04/96
REPORT OF LABORATORY ANALYSIS
This report snail riot be reproduced. except in full,
without the written comers of Pace Anal Sery c s. Inc.

Pace Analytical
Mr. David Maxam
Page 4
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGE/ME RALOCARBONS ANO AROMATICS
Toluene
Chlorobenzene
Ethyl benzene
Xylenes
1,3-Oichlorobenzene
1,4-Oichlorobenzene
1,2-Dichlorobenzene
Units
ug/L 1000
ug/L 10
ug/L , 200
ug/L 200
ug/L 10
ug/L 10
Pace Anary1ca Ser�5. Inc.
9800 IGncey Avenue. Suite 100
Huntersviie, NC 28078
're 104-8754092
Fax 704475-
May 13, 1996
PACE Project Number: 66042950-
92 0589491
04/29/96
04/29/96
MW-5
METFOD DATE ANALYZED
40000
NO
moa
16000
NO
NO
ug/L 10 NO
601/602
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
REPORT OF LABORATORY ANALYSIS
This repot shall net be reproduced. except in fug,
whets the written =resent of Pace Anstigreer Services, inc.

Pace Ana y►ica1
Mr. David Maxam
Page 5
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample I0:
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene
Date Extracted
PURGEABLE HALOCARBONS AND AROMATICS
0ichlorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoramethane
1,1-0ichloroethene
0ichlornmethane
trans-1,2-0ichloroethene
1,1-0ichloroethane
Chloroform
1,1,1-Trichlaroethane
Carbon tetrachloride
1,2-0ichlaroethane
1,1,2-Trichloraethene
1,2-Dichloropropane
Bromodichlormethane
2-Chloroethoxyethene
cis-1,3-0ichlor©propene
trans-1,3-0ichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Di bromoch1oromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Units
Pace Anaircal Serves. [ric..
9800 C.ircey Avenue. Sprite 100
Huntersyslie, Nc 2807®
uak 704875-9092
Fax [phone]
May 13, 1996
PACE Project Number: 66042950.
92 0589505
04/29/96
04/29/96
MW-8
MOL METIOD DATE ANALYZED
ug/L 1.2
Date
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
790
050196
50 NO
S0 NO
50 ND
5O NO
50 NO
50 ND
50 ND
50 NO
50 NO
50 NO
50 NO
50 NO
50 NO
50 NO
50 ND
50 NO
50 NO
50 NO
50 ND
50 NO
50 NO
50 NO
50 ND
50 NO
50 ND
50 1500
50 NO
50 990
REPORT OF LABORATORY ANALYSIS
Tttiis report shall not be reproduced. axcePt in kid,
610
601/602
05/06/96
05/01/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
05/04/96
w+fhcut the widen consent of Pace Analytical Services. inc.

Pace Analytical
Mr, David Maxam May 13, 1996
Page 6 PACE Project Nu
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Toluene ug/L 5D ND 05/04/96
Chiorobenzene ug/L 50 NO 05/04/96
Ethylbenzene ug/L 50 NO 05/04/96
Xyienes ug/L 50 59 05/04/96
1,3-Oichlorobenzene ug/L 50 NO 05/04/96
1,4-Dichlorobenzene
ug/L 50 NO 05/04/96
1,2-Dichiorobenzene ug/L 50 NO 05/04/96
er: 66
4
92 0589505
04/29/96
04/29/96
MW-8
Units i L i D DATE ANALYZED
601 /6D2
REPORT OF LABORATORY ANALYSIS
This report stud not be reproduced. except in haft,
**tout the wn nm iconsent of Pace Anafytiosi Servirass. inc.

ice An
Y
Mr. David Maxam
Page 7
Client Reference: 195349/ Pineywood
PACE Sample Number:
Date Collected:.
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene ug/L
Date Extracted Date
PURGEABLE HAL0CARBONS AND AROMATICS
Dichlorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromamethane
Chlor©ethane
Trichlorofl'uoromethane
1,1-0ichioroethene
Dichloromethane
trans-1,2-Oichloraethene
1,1-Cichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-0ichloroethane
1,1,2-Trichloroethene
1,2-Oichloropropane
Bromodichlormethane
2-Chloroethaxyethene
cis-1,3-01chloropropene
trans-1,3-0ichloropropene
1,1,2-Trichloraethane
Tetrachloroe.thene
0ibromochloromethane
Bromcforn
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Units
ug/L
ug/L
ug/L.
ug/L
ug/L
u9/L
ug/L
ug/L
ug/L
ug/L.
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L.
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/ L
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Face Mar= Services, Inc.
9800 I!' Avenue, Suite 100
Iutersville. NC 28078
rat 704-875-9092
Far 704-875 9091
May 13, 1996
PACE Project Number: 6604295C
92 0589513
04/29/96
04/29/96
MW-12.
NO
050196
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
REPORT OF LABORATORY ANALYSIS
610
-60
2
DATE ANALYZED
05/02/96
05/01/96
/08/96
/08/96
/08/96
8/96
/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
This report shell not be reproduced, except in full,
w'ttuwt the written ccnsant of Pace Analytical Services, lnc,

Pace An iyt c
Mr. David Maxam
Page 8 PACE Project Number: 6604295C
Pace malyxat Services, Inc.
9800 .iGncey Avenue, Sul ; 100
Huntersvifle, NC 28078
704.875-9092
Fax [phone]
Client Reference: 19 C349/ Pineywcod
PACE Sample Number:
DateCollected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Toluene ug/L 1.0 NO
Chlorobenzene ug/L 1.0 ND
Ethylbenzene ug/L 1.0 NO
Xylenes ug/L 1.0 NO
1,3-Oichlorobenzene ug/L 1.0 NO
1,4-Dichlorobenzene ug/L 1.0 NO
1,2-Dichlarabenzene ug/L 1.0 NO
May 13, 1996
92 0589513
04/29/96
04/29/96
MW-12
Units I DL ME'�O DATE ANALYZED
05/08/96
05/O8/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
REPORT OF LABORATORY ANALYSIS
This report shad not be reproduced, except in full,
%l ie u:set the written consent of Pecs Analytical Services. Ina

Pace A
yt
Mr. David Maxam
Page 9
Client Reference: 1950349/ Pineywood
PACE Sample Number: 92 0589521
Date Collected: 04/29/96
Date Received: 04/29/96
Client Sample ID: MW-14
Parameter Units MLIL METHOD DATE ANALYZED
ORGANIC ANALYSIS NAPHTHALEN 610
Naphthalene ug/L 1.2 NO 05/02/96
Date Extracted Date 050196 05/01/96
PURGEABLE HALOCARBONS AND AROMATICS 601/602
Dichlorodifluoromethane ug/L 1.0 NO 05/08/96
Chlorornethane ug/L 1.0 NO 05/08/96
Chloroethene (Vinyl chloride). ug/L 1.0 ND 05/08/96
Bromamethane. ug/L 1.0 NO 05/08/96
Chlarnethane ug/L 1.0 NO 05/08/96
Trichlorofiuoromethane ug/L 1.0' NO 05/08/96
1,1-Oichloroethene ug/L 1.0 NO 05/08/96
Oichlorornethane ug/L 1.0 ND 05/08/96
trans-1,2-Dichlaroethene ug/L 1.0 ND 05/08/96
1,1-Oichloroethane ug/L 1.0 NO 05/08/96
Chloroform ug/L 1.0 NO 05/08/96
1,1,1-Trichloroethane ug/L 1.0 NO
05/08/96
Carbon tetrachloride ug/L 1.0 NO 0S/08/96
1,2-0ichloroethane ug/L 1.0 ND 05/08/96
1,1,2-Trichloroethene ug/L 1.0 NO 05/08/96
1,2-Dichloropr©pane ug/L 1.0 NO 05/08/96
Bromodichlormethane ug/L 1.0 ND 05/08/96
2-Chlaroethoxyethene ug/L 1.0 NO 05/08/96
c-is-1,3-Oichloropropene ug/L 1.0 NO 05/08/96
trans-1,3-Dichloropropene ug/L 1.0 ND 05/08/96
1,1,2-Trichloroethane ug/L 1.0 NO 05/08/96
Tetrachloroethene ug/L 1.0 NO 05/08/96
Dibromochlorornethane ug/L 1.0 ND 05/08/96
Bromoform ug/L 1.0 NO 05/08/96
1,1,2,2-Tetrachloroethane ug/L 1.0 NO 05/08/96
Methyl-t-butyl ether ug/L 1.0 12 05/08/96
Isopropyl ether ug/L 1.0 NO 05/08/96
Benzene ug/L 1.0 NO 05/08/96
May 13,
PACE Pro
REPORT OF LABORATORY ANALYSIS
Nu
e
66042950
This report shaft not be reproduced, except is NH,
without the written cxanserit of Pace Analytical Service,. Inc

Pace AnatOcal Services.
MCC Kincey Avenue. Suite TOO
Hunteravdie. NC:3078
Mr. David Maxam
Page 10
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample 10:
Parameter
ORGANIC ANALYSIS
at 704-875-9192
Far T04-875-13091
May 13, 1996
PACE Project Number: 6604295C
92 0589521
04/29/96
04/29/96
MW-14
Units MOL MET}00 DME ANALYZED
PURGEABLE HALOCARBONS AND AROMATICS 601/602
Toluene ug/L 1.0 NO 05/08/96
Chlorobenzene ug/L 1.0 NO 05/08/96
Ethylbenzene ug/L 1.0 NO 05/08/96
Xylenes
,, , „, ,, ug/L 1.0 NO 05/08/96
1,3-Dichlorobenzene ug/L 1.0 NO 05/08/96
1,4-Dichlorobenzene ug/L 1.0 NO, 05/08/96
1,2-0ichlorobenzene ug/L 1.0 ND 05/08/96
REPORT OF LABORATORY ANALYSIS
Thee report sheaf net be reproduced. except in full,
vnthaut the written consent OE Pace .,kruttytk:al Seences, roc.

Pace Anatyncal Swam. Inc.
9800 Kinsey Avenue. Suite 100
Hurtle, NC 28078
Mr. David Maxam
Page 11
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYST
NAPHTHALEN
Naphthalene
Date Extracted
PURGEABLE HALOCARBONS AND AROMATICS
Dichlorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Oichloroethene
Oichloromethane
trans-1,2-Oichloroe ene
1,1-Oichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-0ichloroethane
1,1,2-Trichloroethene
1,2-Dichloropropane
Bromodichlormethane
2-Chloraethoxyethene
cis-1,3-Dichloropropene
trans-1,3-Oichloropropene
1,1,2-Trichloroethane
Tetrachloraethene
Dibromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Units
ug/L 1.2
Date
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
Tet 704.875.9092
Faz 704-875-9091
May 13, 1996
PACE Project Number: 66042950-
92 0589530
04/29/96
04/29/96
MW-15
ND
050196
NO
NO
NO
NO
ND
NO
NO
NO
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
1.0 NO
1.0 NO
1.0 NO
1.0 NO
METHOD DATE ANALYZED
610
601/602
05/02/96
05/01/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/0S/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
REPORT OF LABORATORY ANALYSIS
This report shad not be reproduced, except in full,
%/Ablaut the vattten consent of Pace Analytical Services, inc.

Pace Anaiytia[
Mr. David Maxam
Page 12 PACE Project Number: 6604295C
Pace Muy'tical Services, Inc.
9800 Kinsey Avenue. Suite 100
>s:anveite, NC 28078
Tel: [phone]
Fax [phone]
May 13, 1996
Client Reference: 195t349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID.
Parameter U
ORGANIC ANALYSIS
PURGEABLE HALOCARNS' AND AROMATICS
Toluene ug/L 1.0 NO
Chlorobenzene ug/L 1.0 NO
Ethylbenzene ug/L 1.0 NO
Xylenes ug/L 1.0 NO
1,3--Dichlorobenzene ug/L 1.0 ND
1,4-Oichlorobenzene ug/L 1.0 NO
1,2-Dichlorobenzene
ug/L 1.0 NO
92 059530
04/29/96
04/29/96
Fri-15
P.L. NE''OD DATE ANALYZE
601/602
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
REPORT OF LABORATORY ANALYSIS
repeat steal not be reproduced, except in full,
without the written conWt of Pace Analytical Servers, Inc

Mr.. David Maxam
Page 13
Client Reference: 1950349/ Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene
Date Extracted
Units MDL
Analytical Services, Inc.
9800 leicey Avenue, Suite 100.
Huntalsvile. NC 28078
vet; 704-875.9092
Fax [phone]
May 13, 1996
PACE Project Number: 66042
92 0589548
04/29/96
04/29/96
RW-3
E ANALYZED
610
ug/L 1.Z 240 05/06/96
Date 050196 05/01/96
PURGEABLE HALOCARBONS AND AROMATICS 6D1/602
Dichl©rodifluoromethane ug/L 0 ND 05/08/96
Chloromethane ug/L 5 NO 05/08/96
Chloroethene (Vinyl chloride) ug/L 50 ND 05/08/96
Bromomethane ug/L 50 ND 05/08/96
Chloroethane ug/L 50 NO 05/08/96
Trichlorofluoromethane ug/L 50 NO: 05/08/96
1,1-Dichloroethene ug/L 50 NO 05/08/96
Dichloromethane ug/L 50 110 C3 05/08/96
trans-1,2-Dichloroethene ug/L 50 NO 05/08/96
1,1-Dichloroetthane ug/L 50 NO 05/08/96
Chloroform ug/L 50 ND 05/08/96
1,1,1-Trichloroethane ug/L 50 NO 05/08/96
Carbon tetrachloride ug/L 50 ND. 05/08/96
1,Z-Oichloroethane 05/08/96
ug/L 50 NO
1,1,2-Trichloroethene ug/L 50 NO 05/08/96
1,2-4ichloroprapane ug/L 50 NO 05/08/96
Bromodichlormethane, ug/L 50 NO 05/08/96
2-Chloroethoxyethene ug/L 50 NO 05/08/96
cis-1,3-Dichloroprvpene ug/L 50 NO 05/08/96
trans-1,3-Dichloropropene ug/L 50 NO 05/08/96
1,1,2-Trichloroethane ug/L 50 NO 05/08/96
Tetrachloroethene ug/L 50 NO 05/08/96
Dibromachloromethane ug/L 50 NO 05/08/96
Bromoform ug/L 50 NO 05/08/96
1,1,2,2-Tetrachloroethane ug/L 50 ND 05/08/96
Methyl-t-butyl ether ug/L 50 270 05/08/96
Isopropyl ether ug/L 50 180 05/08/96
Benzene ug/L 50 570
05/08/96
REPORT OF LABORATORY ANALYSIS
This report slag not tie reproduced, excOpt in full.
without the written cnntaent of Pace Airelytical Services.. Inc.

Mr. David Maxam
Page 14
May 13, 1996
PACE Project Number: 6
4
Client Reference: 195G349/ P neywcod
PACE Sample Number: 92 0589548
Date Collected: 04/29/96
Date Received: 04/29/96
Client Sample IA: RW-3
Parameter Units MOL ETHO DATE ANALYZED
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS 601/602
Toluene ug/L 50 2000 05/08/96
Chlarabenzene ug/L 50 NO 05/08/96
Ethylbenzene ug/L 50 830 05/08/96
Xylenes ug/L 50 2000 05/08/96
1,3-0ichiarcbenzene ug/L 50 NO 05/08/96
1,4-Oichlarabenzene ug/L 50 ND 05/08/96
1,2-Oichlarabenzene ug/L 50 NO 05/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in hail,
*tires the written consent cr Pace Analytical Services, Inc.

Mr. David Maxam May 13, 1996
Page 15 PACE Project Number 66042950
1ek 704-875-9092
Fax: [phone]
Client Reference: 1950349/ Pineyllood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
NAPHTHALEN
Naphthalene
Date Extracted
Units
92 0589556
04/29/96
04/29/96
RW-6
ug/L 1.2 770
Date 050196
DATE ANALYZED
05/06/96
05/01/96
PURGEABLE NALOCARBONS AND AROMATICS 601/602
Dichloradifluoromethane ug/L 50 ND 05/08/96
Chloromethane ug/L 50 NO 05/08/96
Chloroethene (Vinyl chloride) ug/L 50 ND 05/08/96
Bromornethane ug/L 50- ND 05/08/96
Chloroethane ug/L 50 NO 05/08/96
Trichlorofivaromethane ug/L 50 ND 05/08/96
1,1-Oichioroethene ug/L 50 NO 05/08/96
Dichloronethane ug/L 50 120 C3 05/08/96
trans-1,2-9ichloroethene ug/L 50 ND 05/08/96
1,1-0ichioraethane ug/L 50 NO 05/08/96
Chloroform ug/L 50 ND 05/08/96
1,1,1-Trichloroethane ug/L 50 NO 05/08/96
Carbon tetrachloride . ug/L 50 ND 05/08/96
1,2-Oichloroethane ug/L 50 NO 05/08/96
I,1,2-Trichloroethene ug/L 50 NO 05/08/96
1,2-0ichioropropane ug/L 50 ND 05/08/96
Bromodichlormethane ug/L 50 ND 05/08/96
Z--Chloroethoxyethene ug/L 50 ND 05/08/96
cis-1,3-Dichloropropene
trans-1,3-9ichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibrornochlaromethane
Brornoform
ug/L 50 NO 05/08/96
ug/L 50 NO 05/08/96
ug/L 50 NO 05/08/96
ug/L 50 ND 05/08/96
ug/L 50 NO 05/08/96
ug/L 50 NO 05/08/96
1,I,Z,2-Tetrachloroethane ug/L 50 ND 05/08/96
Methyl-t-butyl ether ug/L 50 120 05/08/96
Isopropyl ether ug/L 50 380 05/08/96
Benzene ug/L 50 ND 05/g8/96
REPORT OF LABORATORY ANALYSIS
This report snail not be reproduced, except in fuU,
without the written consent of Pace Analytical Services, Nnc.

Pace Anatjca(
Mr, David Maxam
Page 16
Client Reference: 195
4
Pineywood
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Toluene
Chlorobenzene
Ethylbenzene
Xylenes
1,3-Dichlarobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Units
ug/L 50
ug/L 5a
ug/L 50
ug/L 50
ug/L 50
ug/L 50
Baca Anairizt Services. Inc.
9800 Wince, Avenue, Slate 100
Huntersirdie. IC 28078
Ix 704.875-9092
Fax [phone]
May 13, 1996
PACE Project Number: 660429504
92 0589556
04/29/96
04/29/96
RW--0
530
NO
1200
4100
ND
ND
ug/L 50 NO
These data have been reviewed and are approved for releas
41
Margaret 5, Harding
Manager, Laboratory Operations
601/602
DATE AI
YZED
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
05/08/96
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, eft in full,
Nome t the wnttebn consent of Pace Anatyticat Services, Inc

Pace An ytica
Mr. David Maxam FOOTNOTES
Page 17 for pages 1 through 16
Client Reference: 19D349/ Pineywood
C3 Gammon laboratory contaminant..
MOL Method Detection Limit
NO Not detected at or above the MOL.
7 m4-e754(42
Fax ?O4-875-go9i
May 13, 1996
PAC Project Number: 66042950
REPORT OF LABORATORY ANALYSIS
This resort s+ a not be reproduced.extra* infoil.
without the written consent at Pace Maty1ic I senriccs, fnc

Pace An.aiytica
Mr. David Maxam
Page 18 PACE Project Number: 66042950-
QUALITY CONTROL DATA May 13, 1996
Client Reference: 1950349/ Pineywood
PU'RGEABLE HALOCARBONS AND AROMATICS
Batch: 92 46167
Samples: 92 0589483, 92 0589491, 92 0589505
METHOD BLANK:
Method
Parameter Units MOL Blank
ff i ch l aradi fl uoromethane 17477 T NO
Chioromethane ug/L 1.0 NO
Chloroethene (Vinyl chloride) ug/L 1.0 NO
Bromomethane ug/L 1.0 ND
Chloroethane ug/L 1.0 NO
Trichlorofluoromethane ug/L 1.0 NO
1,1-Dichioroethene ug/L 1.0 NO
Dichior©methane ug/L 1.0 NO
trans-1,2-Dichloroethene ug/L 1.0 NO
1,1-Cichloroethane ug/L 1.0 NO
Chloroform ug/L 1.0 NO
1,1,1-Trichloroethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 NO
1,2-Oichloroethane ug/L 1.0 NO
1,1,2-Trichloroethene ug/L 1.0 NO
1,2-Dichloropropane ug/L 1.0 NO
Bromodichlormethane ug/L 1.0 F~ND
2-Chloroethoxyethene ug/L I.0 ND
cis-1,3-Oichloropropene ug/L 1.0 NO
trans-1,3-Dichloropropene ug/L 1.0 ND
1,1,2-Trichloroethane ug/L 1.0 NO
Tetrachloroethene ug/L 1.0 NO
Dibromochloromethane ug/L 1.0 NO
Bromoform ug/L 1.0 NO
1,1,2,2-Tetrachioroethane ug/L 1.0 ND
Methyl-t-butyl ether ug/L 1.0 NO
Isopropyl ether ug/L 1.0 NO
Benzene ug/L 1.0 NO
Toluene ug/L 1.0 NO
Chiorobenzene ug/L I.0 NO
Ethylbenzene ug/L 1.0 NO
Xylenes ug/L 1.0 NO
REPORT OF LABORATORY ANALYSIS
This report shad not be ►ecuoduced, except in tut,
without the woman consent of Pace Anayticsl Services, Inc.

Mr. David Maxam
Page 19
QUALIT ' CONTROL DATA
Client Reference: 1950349/ Pineywood
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 46167
Samples: 92 0589483, 92 0589491, 92 0589505
METHOD BLANK:
Parameter
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
SPIKE AND SPIKE DUPLICATE:
Parameter
Di der i orodi fl uoromethane.
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Di chl oroethene
Dichloromethane
trans-1,2-Dichioroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichioroethane
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichloroethene
1,2-D1chloropropane
Bromodichlormethane
cis-1,3-Dichloropropene
trans-1,3-©ichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
©1bromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Units
u-TE
ug/L
ug/L
Units
ug/L
ug/L
ug/L.
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/ L
ug/L
ug/ L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/L -
ug/L
ug/L
ug/L
ug/L
ug/L
MIL - No
Pace M ayncet Services. Inc.
9800 Kk cey Avenue. Suite 100
1-furnersvele. NC 28078
Tat 704 875-9092
ax 704-875-9091
May 13, 1995
PACE Project Number:. 66042950e-
Method
Blank
OD
NO
NO
1.0 1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 ND
1.0 NO
1.0 NO
1.0 NO
1.0 ND
1.0 NO
1.0 NO
1.0 NO
1.0 NO
1.0 ND
20
20
20
z0
20
20
20
20
20
20
20
20
20
20
20
20
1.0 NO 20
1.0 NO 20
1.0 NO 20
1.0- ND 20
1.0 NO 20
1.0 NO 20
1.0 NO 20
REPORT OF LABORATORY ANALYSIS
This report sfia4 not tie reproduced. except in null,
e
Spike
Recv
70%
105%
90%
100%
70%
90%
80%
90%
95%
90%
95%
95%
90%
90%
90%
100%
95%
95%
95%
95%
95%
95%
95%
Spike
Dup1
Recv
TUN
70%
105%
80%
105%
70%
_90%
80%
90%
95%
90%
95%
95%
90%
95%
90%
100%
95%
95%
95%
100%
95%
95%
100%
RN)
5%
0%
0%
12%
5%
0%
0%
0%
0%
0%
0%
0%
0%
0%
5%
0%
0%
0%
0%
0%
5%
0%
0%
5%
105% 95% 10%
without the written consent of Pace Anah/tice Services, inc

Mr. David Maxam
Page 20
Client Reference: 1950349/ Pineywood
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 46167
Samples: 92 0589483, 92 0589491, 92 058950
SPIKE AND SPIKE DUPLICATE:
Parameter
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyl benzene
Xylenes
1,3-0ichlorobenzene
1, 4-0i ch 1 orobenzene
1,2-0ichlorobenzene
LABORATORY CONTROL SAMPLE:
Parameter
Dichiorodi fl uoromethane
Ch1©romethane
Chloroethene (Vinyl chloride)
8romomethane
Chloroethane
Trichlorofluoromethane
QUALITY CONTROL DATA May 13, 1996
PACE Project Nu
4295C
Spike
Spike Dupi
Units MDL 920589335 S ike Recv Recv RPr
ug/L NO MI 707 T
ug/L 1.0 ND 20 100% 90% 11'
ug/L 1.0 ND 20 105% 90% 15;-
ug/L 1.0 NO 20 105% 95% 10
ug/L 1.0 ND 20 100% 85% 16;
ug/L 1.0 ND 60 103% 90% 13
ug/L 1.0 NO 20 100% 90% 11,
ug/L 1.0 NO 20 105% 90% 15%
ug/L 1.0 ND 20 105% 95% 10%
Units
ugug/1
ug/L
ug/L
ug/L
ug/ L
ug/L
L
1.0
1.0
1.0
1.0
1.0
1,1-Oichioroethene ug/L 1.0
Dichioromethane ug/L 1.0
trans-1,2-0ichloroethene ug/L 1.0
l,1-Oichloroethane ug/L 1.0
Chloroform ug/L 1.0
1,1,1--Trichloroeth,ane ug/L 1.0
Cartoon tetrachloride
1, 2-0i ch l oroethane
1,1,2-Trichloroethene
1,2-0ichloropropane
Brornodi ch l ormethane
2-Chloraethoxyethene
Reference
Value ecv
20
20
20
20
20
20
90%
115%
100%
110%
105%
20 95%
20 115%
20 95%
20 100%
.20 100%
20 100%
ug/L 1.0 20 100%
ug/L 1.0 20 95%
ug/L 1.0 20 95%
ug/L 1.0 20 90%
ug/L 1.0 20 100%
ug/L 1.0 20 42%
cis-1, 3-0i ch l oropropene ug/L 1.0 20 95%
REPORT OF LABOR TORY ANALYSIS
This apart sttall nctt ae monad . except in ftU.
we stout the written consent of Pace Anaytical Services. Inc.

P Anay�
David Maxam
e 21
QUALIT?' CONTROL DATA
Client Reference: 1950349/ Pineywood
PURGEABLE HAL0CARBONS AND AROMATICS
Batch: 92 46167
Samples: 92 0589483, 92 0589491, 92 0589505
LABORATORY CONTROL. S,AP
Parameter
trans-1, -0ich1oro ropene
1,1,2-Trichloroethane
Tetrachloroethene
0ibromochioromethane
8romoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
May 13,
PACE Pro
6
umber: 660429504
Reference
Units M1lL Value Recv
u 20 -455
ug/L 1.0 20 95%
ug/L 1.0 20 95%
ug/L 1.0 20 100%
ug/L 1.0 20 100%
ug/L 1.0 20 100%
ug/L 1.0 20 95%
ug/L 1.0 20 95%
ug/L 1.0 20 90%
ug/L 1.0 20 90%
ug/L 1.0 20' 95%
ug/L 1.0 20 80%
Xylenes ug/L 1.0 60 88%
1,3-0ichlorobenzene ug/L 1.0 20 85%
1,4-Dichlorobenzene ug/L 1.0 20 90%
1,2-Dichlorabenzene ug/L 1.0 20 95%
REPORT OF LABORATORY ANALYSIS
Th regxst VW not be rearotlebee. =ereinftel,
eitbout the veleefl s n .nt of Pace An*ybcel Senecas, Inc.

Mr. David Maxam
Page 22
QUALIT'!' CONTROL DATA
May 13, 1996
PACE Project Number: 5604
Client Reference: 1950349/ Pineywood
PURGEABLE HAL0CARBONS AND AROMATICS
Batch: 92 46254
Samples: 92 0589513, 92 0589521, 92 059530, 92 0589548, 92 0589556
METHOD BLANK:
Method
Parameter Units MDL ' Blank
5 c)llorodifluaramethane ug/ L ET NO
Chloromethane ug/L 1.0 ND
Chloroethene (Vinyl chloride) ug/L 1.0 NO
Bramomethane ug/L 1.0 ND
Chloroethane ug/L 1.0 NO
Trichlorofluoromethane ug/L 1.0 NO
I,T-Oichlaroethene ug/L 1.0 NO
0ichloramethane ug/L 1.0 ND
trans-1,2-Oichioroethene ug/L 1.0 ND
1,1-0ichloroethane ug/L 1.0 ND
Chloroform ug/L 1.0 ND
1,1,1-Trichlor©ethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 ND
1,2-Oichoroethane ug/L I.0 ND
1,1,2-Trichloroethene ug/L 1.0 ND
I,2-Oichloropropane ug/L 1.0 NO
Bromodichlormethane ug/L 1.0 ND
2-Chloroethoxyethene ug/L 1.0 ND
cis-1,3-Oich.loropropene ug/L 1.0 NO
trans-1,3-0ichloropropene ug/L 1.0 ND
1,I,2-Trichioraethane ug/L 1.0 ND
Tetrachloroethene ug/L 1.0 ND
0ibromochloromethane ug/L 1.0 ND
Bromoform ug/L 1.0 NO
1,I,2,2-Tetrachloroethane ug/L 1.0 ND
Methyl-t-butyl ether ug/L 1.0 NO
Isopropyl ether ug/L 1.0 ND
Benzene ug/L 1.0 ND
Toluene ug/L 1.0 ND
Chlorobenzene ug/L 1.0 NO
Ethylbenzene ug/L 1.0 ND
Xylenes ug/L 1.0 ND
REPORT OF LABORATORY ANALYSIS
be , c , except in tut.
witt eut tie written consent of Pace Artaytlpl Services. enc.

Pace, Anna
Mr. David Maxam
Page 23
Pace Metrical Services. Inc
9800 Kinc y Avenue. Suite 100
'fie. NC 28078
It 704 i75-2
Fax [phone]
QUALITY CONTROL DATA May 13, 1996
PACE Project Number: a6042950-
Client Reference: 1950349/ Pineywrood
PURGEABLE FfALOCARBONS AND AROMATICS
Batch: 92 46254
Samples: 92 0589513, 92 0589521, 92 0589530, 9
ETHOD BLANK:
eter
ichlorobenzene
fchlorobenzene
0ichlorobenzene
SPIKE AND SPIKE DUPLICATE:
05,69
92 0589556
Method
Units MOL Blank
uuTir- I; t3 k
ug/L 1.0 NO
ug/L 1.0 NO
920589513
Parameter Units MDL MW-12
0ichloradifluor©methane 17477 �.t NO
Chloromethane ug/L 1.0 ND
Chloroethene (Vinyl chioride) ug/L 1.0 NO
8romomethane ug/L I.0 NO
Chloroethane ug/L 1.0 NO
Trichl orofl uoromethane ug/L 1.0 NO
Spike
Spike nupi
Recv Recv
c05% TUN
95% 85%
110% 100%
90% 75%
100% 95%
80% 85%
1,1-0ichloroethene ug/L 1.0 NO 20 100% 90%
Dichlorvmethane ug/L 1.0 NO 20 125% 110%
trans-1,2-0ichloroethene ug/L 1.0 NO 20 95% 85%
1,1-Oichloroethane ug/L 1.0 NO 20 95% 90%
Chloroform ug/L 1.0 NO 20 95% 90%
1,1,1-Trichloroethane ug/L 1.0 ND 20 95% 85%
Carbon tetrachloride ug/L 1.0 ND 20 100% 90%
1,2-0ichioroethane ug/L 1.0 ND 20 100% 90%
1,1,2-Trichloroethene ug/L 1.0 NO 20 i00% 90%
1,2-0ichloropropane ug/L 1.0 NO 20 95% 85%
Bromadichlormethane ug/L 1.0 NO 20 100% 90%
cis-1,3-Oichloroprapene ug/L 1.0 NO 20 95% 95%
trans-1,3-0ichloropropene ug/L 1.0 NO
1,1,2-Trichloroethane ug/L 1.0 ND
Tetrachloroethene ug/L 1.0 NO
Dibromochloromethane ug/L 1.0 NO
Bromoform ug/L 1.0 ND
1,1,2,2-Tetrachloraethane ug/L 1.0 NO
RPG
0% A
20 90% 95% 5%
20 100% 95% 5%
20 100% 95% 5%
20 100% 100% 0%
20 100% 100% 0%
20 100% 100% 0%
Methyl-t-butyl ether ug/L 1.0 NO 20 100% 100% 0%
REPORT OF LABORATORY ANALYSIS
'11m report OW net be reproduced, except in Kitt,
without the wooer consent of Pare Analytical Services. Inc.

P.ace Analytical
Mr. David Maxam QUALITY CONTROL DATA
Page 24
Client Reference: 1950349/ Pineywood
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 46254
Samples: 92 0589513, 92 0589521, 92 058953
SPIKE AND SPIKE DUPLICATE:
Parameter
Isopropyl ache
Benzene
Toluene
Chlarcbenzene
Ethyl benzene
Xylenes
1,3-Oichlorabenzene
1,4-Dichlorabenzene
1,2-Dichlorobenzene
LABORATORY CONTROL SAMPLE:
Parameter
Dichlorodifluoramethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromamethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Dichloromethane
trans-1,2-0ichloroethene
1,1-Oichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Oichloroethane
1,1,2-Trichloraethene
1,2-0ichloroprvpane
Br©modichlormethane
2-Chloraethaxyethene
cis-1,3-Oichloropropene
Units
ug--7--_
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
ug/ L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
Pace Malynca1 elv,ces.Inc.
Avenue. Suite lra
Jiuntersvt1$e. NC 28078
ei: 704-875-9092
1=ax 704-875-9091
May 13, 1996
PACE Project Number: 5604295O
92 059548, 92 0589556
MOL
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
ug/L 1.0
92058951;3
MW-12
ND
NO
ND
NO
NO
ND
NO
ND
Spike
Spike Dupl
S ike Recv Recv RPO
TUUY a%
20 95% 95% 0%
20 75% 80% 6%
20 90% 85% 6%
20 65% 70% 7%
60 83% 80% 4%
20 85% 85% 0%
20 85% 85% ©%
20 85% 85% 0%
Reference
Value
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Recv
IUE
100%
105%
90%
100%
100%
100%
125%
95%
95%
100%
95%
100%
loft%
100%
95%
100%
90%
100%
REPORT OF LABORATORY ANALYSIS
Thin report shad not be reproduced, except in full.
*elms the varier, consent of Pace Analytical Services, lee.

Pace Ana icai
' ! Services. lne.
Apse, Suite t 00
4untemile, NC 28078
Mr. ©avid Maxam
Page 25
75-9092
75-9091
QUALITY CONTROL DATA May 13, 1996
PACE Project Number: 66042950
Client Reference: 1950349/ Pineywood
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 46254
Samples: 92 0589513, 92 0589521, 92 0589530, 92 0589548, 92 0589556
LA RATORY CONTROL SAMPLE:
Parameter
trans-1,3-0ichloropropene
1,1,2.-Tri,chlnroethane
Tetrachloroethene
Di bromochloronethane
Bromoform
1,1,2;2-Tetrachioroethane
Reference
Units MOL Value Recv
u9/7 20 Ng
ug/L 1.0 20 100%
ug/L 1.0 20 105%
ug/L 1.0 20 100%
ug/L 1.0 20 105%
ug/L 1.0 20 100%
Methyl-t-butyl ether ug/L 1.0 20 95%
Isopropyl ether ug/L 1.0 20 95%
Benzene ug/L 1.0 -'20 95%
Toluene. ug/L 1.0 20 85%
Chlorobenzene mm ug/L 1.0 20 85%
Ethylbenzene ug/L 1.0 20 75%
Xylenes ug/L 1.0 60 an
1,3-0ichlorobenzene ug/L 1.0 20 85%
1,4-Dichlorobenzene ug/L 1.0 20 85%
1,2-Oichlorobenzene, ug/L 1.0 20 85%
REPORT OF LA30R,ATORY ANALYSIS
'This refit had not be neractuced. 0=80t in NA,
*threw the wneen consent of .Pecs Anetytic ad Services. Inc.

°avid Maya
Page 26
:
Method pets
Not detw at eve
RPO Relative P+ ant O a rice
FOOTNOTES
Paget la through
50 4 / Pin d
May 3, 199
PACE Project Number:
2
PORT OF

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Pace A><alyticai
Pace Anaryacatt Services, Inc.
9800 Kinarf Avenue. Suite 100
I IunttrSvUte. NC 28078
lw* r w.l .nw r..a+.. *+•.".• a ..ww+rr eseeer.e+. .►* ...Frw+
610
610
630
610
610
610
610
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A C T OATA continued «---
O.*WO .WO.00 •Nf►w•w.. *w •w 0.0
QQS Till* %al QCWQS Seasoned QC2S i ;lac ACti,
•• 20.0 -91,3 L50
33 48154....E ._--. 7
20.0 16.89041 84.5 150
20..0 32.41312 162.1 150
20.0 63.72197 314.6 150
20.0 23.64261 118.2 L50
20.0 23.14971 115.7 150
10.0 23.16639 116.1 150
10.0 22.47400 7.33.4 150
10.0 23.21490 11.6.1 3.50'
10.0 21.14620 103.7 150
20.0 11.04713 91.2 250
20.0 21.14430 103.7 150
••~,
1.9.7316
20.4446
20.3147
31.1486
12..1:77
14.5542
24.0977
14.6375
10.3013
2].. 7560
14.5152
23.2714
44.4256
11.6326
17.4477
0%sp Sample Result Duo R37G
21.2192
23.7481
23.6497
33.6972.
'21.8976
22.0201
22.3233
11.5309
20.8791
23.1538
17.6624
32.0714
62.3293.
23.6146
21.2056
30
Tet 70-875-9092
Fax [phone]
r 0ec Oats
05/02/96
13/02/96
05/02/96
* 05/02/16
05/02/16
05/02/96
05/02/96
05/02/16
13/02/96
05/06/96
05/04/46
05/06/96
IXIL 9 ST
7.64136 41.
13.0221 28
14.7804 38
7.73243 39
14.0921 35
17.3638 40
7.64471 37
24.7428 40
106317 3.9
6.22464 40
11.5E39 47
31.8024 27
33.5322 30
8.66442 37
17.2152 25
REPORT OF LABORATORY ANALYSIS
This revert anatl net be neenSducect exceOt Mika
without the written consent of Race Analytical Services.. Inc..
111""flIuufl
Sss16 Oat Dace
0004515 05/02/96
000451.5 05/02/36
0004515 05/02/96
0004515 05/02/96
0004415 03/02/96
0004515 05/02/96
0004514 05/02/96
000451s OS/03/96
0004515 05/02/96
0004515 05/02/16
0004515 05/02/96
0004513 05/02/96'
0004515 OS/02/96
0004515 05/02/96
0004315 05/02/96

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I2333 acct.rc L14...._.. i.__.�.._._..
� 610 1.1
_
22333 610 .81
22333 Enisparra 13.Q , 37
22333 IluCrane 410 .7a
22233 1lurtnc ii.o 27
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610 1.3
332 33 a+ca 410 1.1
23333 6;0 1`_
1
22333 110 1.2
32333 410 1.1
23233 cc 410 1..2
22333 610 .o
223.13 Aare 610
22333 Sca�utacr. 610 .12.
22333 640 1
22333 610 84
22353 •pr0c 610 1
22353 c 410 1.3
22353 >wc 610 1
P,a An, yticaI
Pa Anaircai Servers. Inc.
9800 Kiraly Avenue. State 100
Hunan -wile, NC 28078
Tat 706-875-9092
Fax [phone]
•.i W •o.w• WO. 0Ms1.ee _M10►••••IY•••• w••n MV TO, 411yl�41. 1•••• 01m.i!WO .0W0MPw,11
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QC Ytemnar Aaalyn ;roe... _ _ Semple Z.stcl: ©trp 5,4m14 Rasa2 c � IMO 0a . ! 3!
. ...._. .._-- .. _ Saplil ]tic Dace
22333 93iascen 610 20.3344 .- -..•_ S.l•_
2=33 saap rC 610 22,437P 0.iS2SI -- -•__ ......
22333 Apia "i^, i10 L].7]1P 11.1134 1477 •37 36 0004515 05/02/94
11.1443 22.9744 4.31377 37 96 0004535 0/02/9
34 96 0004533 05/02./98
31 MIA 4
fate ule
REPORT OF LABORATORY ANALYSIS
This reoori shalt not be reproduced. amen* * in MI,.
without the whiten cansant of Pace Arranninel Sennema Inc.

au�r:
23333
3a. gut 23333 gar
voila* data.
Tel [phone]
Pax 704.875-9091
REPORT OF LABORATORY ANALYSIS
This reQ44t shall not be reproduced, axcEit in full,
without the written consent of Pace Anslyr1cal San/ices, Inc.

REPORT OF 0 TORY ANALYSIS

REPORT OF LABORATORY ANA YSS
199
Mr. John +e s
Shield Znvironmental Assoc aces,
2848 I -as south
Suite E
Charlotte, NC 28208
PAC Project No. 660125.506
Client .Reference: 1950349/Pineytrocd
Eess:.
Enclosed is the re sor of .laboratory analyses for s
January 25, 1996.
Footnotes are give a. at the end o
If you have any questions concerning this report
to contact us.
Sincerely,
.LCO1
rogam
er
cures
es received

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56/Z0/Z0 aN 0'7 1/bn
56/ZO/Z0 aN O'T 7/ft
96/ZO/Z0 aN 0'7
56/ZO/Z0 aN D'I V5n
96/ZO/Z0 CN or 7/5ri
56/ZO/Z0 aN 0'7
56/Z0/Z0 aN 0-7 lift
56/Z0/Z0 aN 0•7 7/bn
56/ZO/Z0 aN 0'7 7/bn
56/zoizo aN O*1 7/bn
96/ZO/Z0 aN 0'7 7/ft
56/Z0/Z0 aN 01 01/ft
56/Z0/Z0 aN 0'7 7/bn
96/ZO/Z0 aN O'I 7/bn
96/ZD/ZD OIN 0-7 Vft
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56/Z0/Z0 079
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96/zo/Z0
96/Z4/ZQ
96/to/Zo
96/Z0/Z0
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96/Z0/Z0
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Mr
3
Ness
C3 ient Sample
:Xarame=ems
TICS
Dich:Lorodiiluc romethera
Chloromethane
c L roethene (airyl ca
3romethane
Chioroethane.
T:ichlorofluorometAnus
Dichlo
oromet
-1,2-Dich,Loroethene
1,1-Dichioroechane
Ch oroform
3.-Trichloraec.ane
trachlo ride
oroet ane
chioroec ene
chlorcpropazae
ocdichlormetha ze
2-C .LQroethoxyethene
Dichloropropene
t3 ic.lrsrotsrotaene
h1. o
roethe_^-e
oromethan
1,1,2,2-Tetrach- roe
Meehyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
REPORT OF LABORATORY ANALYSIS
a
92 0541170
01/2S/96
01/25/96
KW-5
ug/L 2.8 430
ug/L 200
ucg,il, 200
ug/L 200
ug/L 200
ug/L 200
ug/L 200
N3
1996
610 02/02
601/602
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
uq/L 200 ND 02/02/ 6
ug/L 200 ND 02/02/96
ug/L 200 ND 02/02/96
ug/L 200 ND 02/02/56
ug/L 200 ND 02/02/96
ug/L 200 NB 02/02/56
ug/L 200 VD,
ug,/L 200 ID
ug/L 200 NJ
ug/L 200 ND
ug/L 200 ND
ug/L 200 ND
ug/L
g/L
ug/L
ug/L
ug/L
ug/L
200 ND
200 ND
200 ND
Z00 ND
200 NA
200 ND
ug/L 200 ND
uq/L 1.000 12000
ug/L 200
ug/L 1000
ug/L 1000 40000
12000
02/02/96
02/02/.6
02/02/96
02/02/`35
02/02/'96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/ 95
02/02/96
02/02/96
02/02/9E
02/02/96
02/02/96
02/02/96
9reO0 Av u
Huraesvdle, h10
TEL [phone]©92
FAX: [phone]

349Z 2 \CC
REPORT
OF
ORATORY ANA YS1S
2 0 00
200 \ 34000
200 §
200 - 2
200 < ?
m2
02 )2
02/02
02/
02/02/96
02/02/96
02/02/9

REPORT OF LABORATORY ANALYS S
Mr.
Page
5
.xe s s:
l ient. Reference; 1950349/Pineywood
PA
Date Collected.
Dace Received:
Client Sample LD:
? arlme Y er
GRC:ANIC ANALXS IS
LND r' TDUAL
Naphthalene
PUR.GZABLZ, RALOCARBONS AND AROMATICS
Dichlorodif? uoramet.aae
Cslcrocne t sne
Chloroetseue (vinyl chloride)
Hr©moraetyane
Chloroet_hane
T 'chlorofluoromethane
1, l_Dic orcethene
Dic.orometxe
ts-
is :Loroec :ene
.-Dic' thane
ethane
Car':-
1,
1,1,2-
1,2-Dice
Sromod .chlormechane
2-t.hlcroathoxvethese
ci:a 1,3-Dicdlaroprcoene
t�s-1,3-Dichloropropene
1, 1, 2-Trich.oroethane
cmc: ch.1 a rome thane
1,1,2
Nethf
Isco;
Benzene
Toluene
t_rach once
l Q.c
ug/L
9'2 05'i0
01/25/96
01/25/96
4W-3
2..8 160
SO ND
ug/L 50 ND
ug/L 5O ND
ug/L 50 ND
ug/L SO ND
ug/L 50 ND
ug/L SO ND
ug/L SO ND
ug/L SO NI9
ug/L S0 Nil
ug/L 50 ND
ug/L 50 ND
g/L
ug/L
ug/
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
g/L
ug/L
ug/L
ug/L
ug/L
5O Nt
O ND
ND
Nn
50 ND
S0 ND
50
50
SO
5d
S0
S0
50
SO
50
5O
50
54
ND
ND
yD
ND
1800
_ND
_996
Number
510 02/02/96
601/602
02/02/ 96
O2/02/96
02/02/96
02/02/95
02/02/96
02/02/96
02/02/96
02/02/96
02/02/95
02/02/966
02/02/96
02/02/96
02/0/95
02/02/96
02/02/95
02/02/ 55
02/02/95
02/02/96
02/02/95
02/02/55
02/02/95
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96

RE T ORATORY ]
02 %/
02/ »/96
02/02
»/9
02/02/56
2/56

Mr. Zahn aess
?age 7
Client Reference: 1390349/Pia
PACZ Sample Number:
Dace Collected:
Cate Received:
Client Sample LO:
?arame
ORSANI,- AN-
=771=AL PARA,t'...2.6RS
Naphthalene
REPORT OF LABORATORY ANALYSIS
Units
ry oa. 199
?AC= :Project Number: 6501:35
92 0.541197
01/2S/96
01/25/96
MW-12
MDL METaQD DAIS
ug/L 2.3 510 -02/02/96
ITURGEABLE HALOCARBONS AND AROMATICS 601/502
Dichlorodifluoromethane ug/L 1.0 ND 02/02/96
Chloromethane ug/L 1.0 ND 02/02/96
Chloroethene (Vinyl chloride) ug/L 1.0 ND 02/02/96
BromOmethane ug/L 1.0 ND 02/02/96
Chloroethane ug/L 1.0 NI) 02/02/96
Trichlorofluoromethane ug/L 1.0 ND 02/02/95
1,1-DichIcroethene
Dichloromethane
-Dcre
r4grte
Chloroform
1.1,1-Trichloroechane
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichlorcethe
1,2-Dichloropropane
dromodichlormethane
2-Chloroethoxyethene
ne
3irp-ene
.
trans-1,2-Dichloropropene
1,1,2-Trichloroethane
Tetrachlorceohene
Dthrrnoc1oromethane
Szomoform
1,1,2,2-Tetrachlorte
Methyl-t-buryl eche,'
Isopropyl ether
Bente
Toluene
haxe
ug/L 1.0 ND 02/02/95
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1,0 ND 02/02/96
ug/L. 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/35
ug/L, 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/95
ug/L 1,0 ND 02/02/94
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/95
ugIL 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/96
ug/ 1.0 ND 02/02/96
ug/L 1.0 1.4 02/02/96
ugll' 1.0 ND 02/02/96
ug/L 1.0 ND 02/02/35
ug/L 1.0 2.1 02/02/96
Avenue sui•
HuntarsvIg& NC zoom
7044754M
FAX [phone]
An egum Occararity eirour.

Xylenes
-lac
3,-:
L.1„2-Dichlorob<
349/Pczte
02/
0 / /
2
02/02/95
2/02/96
02/ /
a

56/ZQ/Z0
96/ZQ/Zo
96/ZD/Z0
95 /ZC7/Z0
96/ZD/ZC
56/Z0/Z0
6/Zfl/Z0
56/ZO/ZQ
96/Z©/Zfl
56/Z6/Z€i
95/Za/Z0
96/Zfl/Z0
96/Zq/Zp
5€/Zd/Z©
56/Za/Z0
96/t0/Z
56/ZO/ZC
5r /ZC?/Zfl
95/Z0/Zo
96/Z0/Zo
96/Z0 tO
96/Z0
96/Z0
96/ZC�/ZCS
96/Z©/Z©
96/ZCa/ZO
96/ZJ/ZQ
96/Z©/Zd
96✓ZC/Z©
ate
aN
UN
ZE
aN
0't
CiN ©' T
aN ©'T
aN 0'T
QJ
aN ©'T
aN 0'T
aN D ' T
CN 0'T
aN 0'T
aN p'T
aN
aN
©"T
t C'T 'T/bn
aN C'T Z/bn
aN G�'T 7/bn
aN C"T 'a/bn
aN 0 ' T 7 /bn
aN O'T 'I/bn
aN p'T Z/bn
aN 0 ' T 'I /bn
aN 0.7 Z/bn
as O ' T 7 /bn.
aN 0 ' T 7 /5r►
aid 0'T 'I/bn
T09
©T9 aN B'Z
noZ71.50 z6
auanToZ
a sa Z'S
TAacsaosz
TA na- -T47 jaia
zoL
ipowcze
'FC{-Z'T
-Z ^T •t
a-Z'T
ap acTzor :c rogsr
a�cacsT1.;37,T,-T .T • T
uac;oxoT
�y aC`«C3i`DTC-T''7
auwgmaca©T TQ-z'T-sires
axs"ypauioaorTQ
auegzacaoT7vTa .T ' T
auaTes;zgoeN
Strai Fid ''I�!t10EI2ICIt�II
S% I N ' DINYD11.o
a, s-rdwrs c tel=
paATacaE aoea
:pm?aTTC,Z area
rrr�N sTawes Cnte
6
Zy;
SSfl YNV AK) V110BY1 d Oda!

0
ORATORY
OF ANALYS S
1.0
`0
I
601/6 4
02/ 2 9¢
¢
02
02/0
02/02/96
02/02/96

REPORT OF LABORATORY ANALYSIS
Hess
?age 11
Client Reference: 1950349/?theywood
?ACE Sample Number:
Dace Collecmed:
Date Recei'red:
Client Sa
.a
0
Dichltsrrcdifluorcmethane
e (Vinyl chloride)
3romomethane
Chloroethane
ch3.orofiu
oroethene
Dichloromethane
trans-1 2-Dichloroethene
1,1.-Dichloroechaae
Chloroform
1,1,
loroernAne
Carbon tea..oride
1,2-Dichloroethane
1,1,2 Trichloroethend
1, 2-Dic`..lcronrocane
3romod chlor-ne _bane
2-Chloroethoxyethene
cis-1,3-Dichloroorooeae
trans-1, 3-Dichloroprolaene
1, 1, 2-Triciloroethane
Tetrad orcec ene
Dibromochla
From©form
1,1,2,2-Tetrachloroehane
Methyl-G-bucy1 ether
Isopropyl. echer
Benzene
Toluene
TICS
February L996
?ACE. ?rvjec Number:
92 051219
01/2/96
01/25/96
MW-15
2 8 02/02/96
1.0 ND
1.0 NI
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.. 0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L
ug/L
ug/L
ug/L
ug/L
1.0 ND
1.0 ND
1.0 ND
1.0 ND
1.0 1.5
601/602
02/02/95
02/02/96
02/02/96
02/02/95
02/02/96
02/02/96
02/02/96
02/02/95
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/6
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/96
02/02/95
02/02/96
02/02/95
02/0'2/95
02/02/95
02/02/96
02/02/96
02/02/95

YSIS
e
b e
eriz aria
REPORT OF ORATORY ANALYSIS
ugi
PAC: Pro - umber

Mr. John Mess
?age 13
Client Reference: 1950349/olua o ad
PACZ Sammie Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
flAN I C ANAL' S
1"NDTV:DUAL PARAMETERS
Naphthalene,_
PURGEABLE HALOCAP.9CNS AND ARO ATICS
Dichlorodiflueromethane
Chlorcrnecha.ne
Chloroethene (vinyl ide)
Bromsme thane
Chloroethane
Tricblor0fluore methane
-D%ch+].oroethene
methane-
,2-Dichlorcethene
1,1-Dichloroechane
Chloroform
1,1,1-Tricaloroer'wane
Carbon tetrach1cride
1, 2-Dichl oraetharie
1, 1, 2-T_rit_zl.aroet :sere
1,2-Dichloronrooare
3romodi chI o rme thane
2-Chloroethoxyechene
chi o rcn rop ene
Dichlorooronene
1, 1, 2-T::chl0roechane.
Tecra .tsr3ether_e
Dibromochlorcmethane
3romoform
1,1,2,2-Tetrachlorse
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
REPORT OF LAEORATORY ANALYSIS
ecr*,:ar
PAC? Pr
92 0541227
01/2S/96
01/25/96
RW-3
08,
560'_255
ug/L 2.8 39 610 02/02/96
601/602
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 NE
02/02/96
02/02/96
02/02/95
02/02/96
02/02/96
02/02/96
ug/L 50 ND 02/02/96
ug/L 50 ND 02/02/96
ug/L 50 ND 02/02/96
ug/L 50 ND 02/02/96
ug/L S0 ND 02/02/96
ug/L 50 ND 02/02/96
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L 50 ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/
50 ND
50 ND
50 ND
50 ND
S0 ND
50 ND
02/02/39
02/02/96
02/02/96
02/02/9�
02/02/966
02/02/96
02/02/95
02/02/95
02/02/39
02/02/96
0Z/02./'96
02/02/966
ug/L 50 NE 02/02/96
ug/L 50 220 02/02/96
ug/I. 50 ND 02/02/96
ug/L 50 530 02/02/96
ug/L 50 770 02/02/96
9800 (w'G rAvenue Sucre 100
Hureersvolle, NC 2807E
TEL Th 873 e092
FAX: T04-875•1

Ciies
Thee
SS
CS:
we
489✓oast
iew
RE ORT OF AT
u
ugIL
O
9
ease
tar'* 08 9
2160:ess umber:
02/0219
02
02
0 / 9

R 'ORT OF ORATORY ANALYSIS
etectacc
at
08
,

Mr. jo
Page 15
Hess
Client Reference
49/Pineywr od
REPORT OF 1„A ORATORY ANA .YSiS
?tRGZAZLE aALCc RRONS AND ARCMATICS
Satoh: 92 43415
Samples: 92 0541162, 92 0541170, 92 05411.89, 92 0541197, 92 0541200
92 0541219, 92 0541227'
fluoramethane
thane
Chloroethene (vinyl chloride)
Bromomethane
Ch.Loroathane
Trzchlorofluoromethane
1-Dichloroetheme
Dichtoromet arse
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
1, 1, 1-Tri chloroechane
Method
Units iDL
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0 ND
ND
ND
ND
ND
ug/L L.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 Nn
ug/L 1.0 ND
Carbon tetrach-de ug/L 1.0 ND
1, 2-Dichloroethaae uc/L 1.0 ND
1, 1, 2-Tric *io ethene ug/L 1.0 ND
1, 2-Dic:-.loropro cane ug/; 1.0 ND
BroModichlcrzethane ug/L 1.0 ND
2-C`loroethoxvethene ug/L 1.0 ND
1,3-Dichlorapropene
pene
Tetrachloroethene
Dibromoch r6,miTte
Bromofarm
1,1,2,2-Tetrac hlorae
Methyl-t-butyl ether
Isopropyl ether
Sew:ere
Toluene
Chlorobenzene
Ethylbenzere
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 ND
ug/L
ug/L
ug/'L.
ug/L
ug/L
ug / L.
ug/L
L.0 ND
1.0 ND
1.0 ND
1.0 ND
1.0 ND
1.0 ND
a
08, 1996
ject Number:

tS OOt 456
S $OOT %S6
40 465 %SE
%D O6 406
%C 406 #06
OZ
OZ
OZ
OZ
OZ
tS 456 06 OZ
eC &OOT %DOT OZ
40 406 106 OZ
40 406 406 OZ
`sS 456 406 OZ
4S 456 406 OZ
4,007 4007 OZ
4S6 406 OZ
°w04T 4S6 OZ
0 406 %06 OZ
%C S5 *SE OZ
46 456 406 OZ
49 406 SSE OZ
40 ' 5B 458 OZ
4501 SOOT OZ
,sS 456 406 OZ
;0 B' 48' OZ
LSL 'tOL OZ
TanG ex-cds
C1
0 ?
0-7
Cts O't
ctz
CIN O'T
CN 0't
CN 0't
CN O t
ciN 0 ' T
CIt3 0
CN
Clh
CN
CEN
CW
CN
CN 0'T
aN O"t
CN
0"i
/5n
i/bn
7,/b'n
n/5n
Z/bn
/bn
Z/bn
i/Bn
/bn
-1/bn
•I/5n
7,/5n
/bn
/bn
/bn
' /bn
/bn
Z/Bn
sztuD
alarcao
ima iczdozoT7 7c- E ' T sty :a
s�ttaa; zciosoTgz-FC F'T-sz'o
atria-, Z ai:za oT:; o-pOsuczE
atredcadcao TgoTC- Z ' T
a'c-a cscergt, - Z ' T ' T
rzr zaosaTt7C-Z "c
ap =TtT.z,r � ttorzr-j
> 4'07 CC'-
i7.,0TC-Z'T-rum
€3Lia '3acaCT'�;^'Cc-T't
atret;cawoaonT3oacTz lay
earrizaoac Tq-J
®tret;cowomozE
T t d atrawasaoz©Tt
otiv7z awcscTqD
0a scaczt T 7P0.2oTrazC
asaamexed.
eatraZAg
WEIVe
:XNY7E. COE
LZZT3,S0 Z6 '67.ZTri50 Z6
"L677'SO Z6 '68TTiS0 Z6 OLTZt O Z6
poor
ebva
9667

REPORT OF LA QRATORY ANALYSIS
?age _3
C .+I.T':'_' CC C3'L DA ` `eb uary 08. 1996
?:AC.0 Project Numbe
ence: 1950349/Pineyw©ad
? L CC. ONS AND AROMA: CS
gs tcb s 92 43416
Samples: 92 0541162, 92 0541170, 92 0541199,
92 0541219, 92 0541227
me
2,2-Tetrachloroethane
1-c-buty1 ether
Zsaprc+myl ether
Benzene
Toluene
Chia robenz ene
Bthylbenzene.
Xylenes
1, 3-i3ic'a? or©benzene
1, 4-'Dic lorobe nzene
1,2-Dichlcrcbenzene
Y CO3 COL SAMPt
ter
rodi.fluoromethaze
ethane
ae (Vinyl chloride)
Cr tetrac.las i
1, 2-Dich'_aroethane
Tr.ch
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug'/ L
ug/L
ug/L
ug/L
ug/L
ug/L
541497, 92 0541200
5aike
920541162 Spike Jun)
h[ iL KW-4 6oike Rec-r '.ec7 PC
1.0 ND 20 85t 85t 0%
1.0 3.7 20 920 97t 5%
1.0 3.6 20 92' 97t 5%
1.0 19 20 90t 90t 0%
1.0 6.3 20 109% 114t 4%
1.0 ND 20 95' 95't 0%
1.0 ND 20 95% 100t 5t
1.0 3.5 60 104't 113t 9L
1.0 ND 20 901c 90* 0%
1.0 NC) 20 95'r 95t 0%
1...0 ND 20 90t 90't 0.
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L
ug/L
ug/L
ug/ LL
1.0
1.0
1.0
1.0
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
35a
100'E
00!
100t
100t
95t
100,
95%
951
1.00t
100t
105%
95t
90%
95%
90t

REPORT OF i.ABORATORY ANALYSIS
?age 1:9
92 0
92 0541219,
2-Chlorcee
cis -I, 3-Dicb.io o rro a e
try-1,3-Dic:aropropene
1, 1, 2-Tricblorcetar_e
Tetrac.b1ore a tame
sruary '08, L996
?AC? ? Number Ei 0 12 330
ywcod
TICS
92 0541170, 92 0141199, 92 0541197, 92 05412,00
Dibramac'a.1arome thane
3romafcrm
1,1,2,2-Tecracb_1.oroeCSane
Methyl-c-butyl ether
Lscrprcpyi ether
Benzene
'I 114
Y
Xylenes
1,3-Dicb-orcbenc.
1, 4-Dic .orobenz
ne
e
Dichlorcbenzene
1227
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0
1.0
1.0
1.0
1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
uq/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
u'g/L 1.0
ug/L 1.0
e, ence
Value
20
20
20
20
2,0
20.
20
20
20
20
20
20
20
20
20
20
20
1©01
901
951
95k
901
90%
95k
951
90t
1.001
1001
1251
951
1001
100t
+.0 0'
951.
9r 1€1 ICuny Monte Sum 100
h truirs +rlit, NC ZE079
TEL TC4175-9042
FAX; 704475.3491

lei
3
eywood
ORATORY ANALYSIS

ANALYSISREPORT OF BORATORY
C1 ten Reference: 1ZS
66
071
0710
THCOK:
pht
Amor
aphtha1a e
QUALM LDATA
0717
0710925
1"PL Pi 7
0710
SAMPL
7 071
UPL 7 $::
Dupi

CT
30
R l
R f¥r nc ?
Sm
REPORTOF°? dORATORY ANALYSIS
TN
vet
icy
cent Oiff#r c
PqL.

[phone]
PROJECT NAME_ 'OA
SHIELD ENVIRONMENTAL ASSOCIATES, INC
'r c,
CONTACT NAME
Irki= TELEPHONE NO.
Kvk
PrijucL Nu:
SAMPLE
SAMPLE LOCATION
A
-
a
ANALYSIS
REMARKS
I 11
COMMENTS;
Dicfacciuui Iy jrwui—Tau Tuna

July 21,
REPORT OF
Mr. Mark McCormack
Shield Environmental A c ates, Inc.
2848 1S South
Suite
Charlotte, NC 2
RE: PACE Project No. 0707.514
Client Reference: piney Woods
ar Mr. McCormack:
Enclosed is the report of atory analyses for pl rac
July 07, 1.
Footnotes are given at the end of the report.
f you have any questions concerning this report, please feel
contact us.
Sincerely,
r
Pro,
Kommalan
Oct Manager
End Enclosures
v

Shield Environmental Associates, Inc.
2848 I-85 South
Suite H
Charlotte, NC 28208
Attn: Mr. Mark McCormack
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Dichlorodifluaromethane ug/L 20 NO
Chlor©methane ug/L 20 NO
Chloroethene (Vinyl chloride) ug/L 20 NO
Brom©methane ug/L 20 NO
Chloroethane ug/L 20 NO
Trichlorofluoromethane ug/L 20 NO
REPORT OF LABORATORY ANA YS1S
July 21, 1995
PACE Project Number: 650707514
92 0430433
07/05/95
07/07/95
RW-1
Units MOL M TI°l4D DATE ANALYZED
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
1,1-Dichloroethene ug/L 20 ND 07/13/95
Dichloromethane ug/L 20 NO 07/13/95
trans-1,2-Dichlorcethene ug/L 20 ND 07/13/95
1, I-€Ii ch l oroethane ug/L 20 NO 07/13/95
Chloroform ug/L 20 NO 07/13/95
1,1,1-Trichloroethane ug/L 20 NO 07/12/95
Carbon tetrachloride ug/L 20 NO 07/13/95
1,2-Dichlaroethane ug/L 20 NO 07/13/95
1,1,2-Trichloroethene ug/L 20 NO 07/13/95
1,2-Oichloropropane ug/L 20 NO 07/13/95
Bromodichlormethane ug/L 20 NO 07/13/95
2-Chiaroethoxyethene ug/L 20 NO 07/13/95
cis-1,3-Dichlorapropene- ug/L 20 NO 07/13/95
trans-1,3-Dichloroprcpene ug/L 20 NO 07/13/95
1,1,2-Trichlorcethane ug/L 20 NO 07/13/95
Tetrachioroethene ug/L. 20 ND 07/13/95
Dibromochloromethane ug/L 20 ND 07/13/95
8romoform ug/L 20 ND 07/13/95
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
ug/L 20 NO
ug/L 20 1200.
ug/L 20 54
ug/L 20 1300
07/13/95
07/13/95
07/13/95
07/13/95

REPORT OF LASORATORY ANA YS1S
Mr, Mark McCormack
Page 2
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample :0:
Parameter Units MDL
ORGANIC ANALYSIS
July 21, 1995
PACE Project Number: 650707514
92 0430433
07/05/95
07/07/95
RW-I
PURGEABLE HALOCARBONS AND AROMATICS
Toluene ug/L 20 290
Chlorobenzene ug/L 20 NO .
Ethyibenzene ug/L 20 450
Xylenes . ug/L 20 MO
1,3-0ichlorobenzene ug/L 20 NO
1,4-0ichiorobenzene ug/L 20 NO
1,2-Oichlorobenzene ug/L 20 NO
MOP DATE ANALYZED
601/602
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95

Mr. Mark McCormack
Page 3
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
data Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
REPORT OF LABORATORY ANALYSIS
Units
July 21, I995
PACE Project Number: 550707514
92 0430441
07/05/95
07/07/95
Rw-2
PURGEABLE HALOCARBONS AND AROMATICS
Dichlorodifluaromethane ug/L 1.0 ND
Chloromethane ug/L 1.0 ND
Chlaraethene (Vinyl chloride}. ug/L 1.0. NO
Bromomethane ug/L 1.0 NO
Chloroethane ug/L 1.0 ND
Trichlorofluoromethane ug/L 1.0 NO
1,1-Dichloroethene ug/L 1.0 NO
Dichloromethane ug/L 1.0 NO
trans-1,2-Oichloraethene ug/L 1.0 NO
1,1-Oichl©roethane ug/L 1.0 ND
Chloroform ug/L 1.0 NO
1,1,1-Trichloroethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 NO
i,2-Dichloraethane ug/L 1.0 NO
1,1,Z-Trichloroethene ug/L 1.0 NO
I,2-Dichlaropropane ug/L 1.0 NO
Bromodichlormethane ug/L 1.0 ND
2-Chloroethoxyethene ug/L 1.0 NO
601/602
OATE ANALYZED
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
cis-1,3-0ichloropropene ug/L 1.0 NO 07/14/95
trans-1,3-0ichlaroprapene ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethane ug/L 1.0. NO 07/14/95
Tetrachloroethene ug/L. 1.0 NO 07/14/95
Oibromochlaramethane ug/L 1.0 NO 07/14/95
Bramoform ug/L 1.0 NO 07/14/95
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
ug/L 1.0 NO
ug/L 1.0 29
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 ND
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

ORATORYREPORT OF ANALYSIS
Mark ack
Page 4
Client Reference: Piney ods
PACE Same Number:
Gaza Cec
Data Received.
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PUR 81. LOCA':ORS AN AR °TICS
Xyl enes
ch rcbenzerte
1,4- fc lorabenzerte
1,Z- orobenzene
Units
ug/L 1.0
ug/L 1.0
ug/t. 1.0
ug/L 1.0
July 21,
PACE Project
92 0430441
07/05/95
07/07/95
GATE ANALY7RO
1/602 '
07/14/95
07/14/95
07/14/95
07/14/95

ack
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARSONS AND AROMATICS
Dichlorodifluoromethane ug/L 20 NO 07/13/95
Chloromethane ug/L 20 NO 07/13/95
Chloroethene (Vinyl chloride) ug/L 20 ND 07/13/95
Bromamethane ug/L 20 NO 07/13/95
Chloroethane ug/L 20 NO 07/13/95
Trichlorafluoramethane ug/L 20 NO 07/13/95
1,1-Dichloroethene ug/L 20 NO 07/13/95
Dichloramethane ug/L 20 NO 07/13/95
trans-1,2-Dichloroethene ug/L 20 NO 07/13/95
1,1-0ichloroethane ug/L 20 NO 07/13/95
Chloroform ug/L 20 NO 07/13/95
1,1,1-Trichloroethane ug/L 20 NO 07/13/95
Carbon tetrachloride ug/L 20 NO 07/13/95
1,Z-Oichioroethane ug/L 20 NO 07/13/95
1,1,2-Trichloroethene ug/L 20 NO 07/13/95
1,2-Dichloropropane ug/L 20 NO 07/13/95
Bromodichlormethane ug/L 20 NO 07/13/95
2-Chloroethoxyethene ug/L 20 NO 07/13/95
REPORT OF ,ARORATORY ANALYSIS
July 2I, 1995
PACE Project turnber: 550707514
92 0430450
07/05/95
07/07/95
RW-3
Units MOL ME'Tl"100 DATE ANALYZE
cis-1,3-0ichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Di bromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane ..
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
601/602
ug/L 20 NO 07/13/95
ug/L 20 NO 07/13/95
ug/L 20 NO 07/13/95
ug/L 20 NO 07/13/95
ug/L 20 NO 07/13/95
ug/L 20 NO 07/13/95
ug/L 20 NO
ug/L 20 300
ug/L 20 NO
ug/L 20 1000
ug/L 50 2800
ug/L 20 NO
ug/L 20 930
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95

'
Page
Client Reference: Piney
PACE
Oate Col
Oate Rebel
Client Spie ID:
Paramete
Number:
Units
OR C ANALYSIS
PURGEABLE NALOCARBONS 0 ARO Tics
XY1Allbs
-Oichlorobenzene
1,4
1,2
ug/L
ug/L
og/L
u /L
ORATORYREPORT OF ANALYSIS
July 1-, 1995
PACE Pr ject, N m e 707514
92B4B0450
07/05/95
07/07/95
RW-3
NO
NO
NO
DATE ANALYZED
6012
07/
07/
07/13

Mr.. Mark McCormack
Page 7
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
REPORT OF A ORAT RY ANALYSIS
July 21., 1995
PACE Project Number: :i30707 1
92 04304G13
07/05/95
07/07/95
RW-4
Units DL METHOD DATE ANAL' ZED
PURGEABLE HALOCARBONS AND AROMATICS 5C1,/5 2
Dichlorodiflunromethane ug/L 1.0 NO 07/13/95
Chloromethane ug/L 1.0 NO 07/13/95
Chloroethene (Vinyl chloride) ug/L 1.0 NO 07/13/95
Bromomethane ug/L 1.0 NO 07/13/95
Chlaroethane ug/L 1.0 NO 07/13/95
Trichiorofluoromethane ug/L 1.0 NO 07/13/95
1,1-Dichloroethene ug/L 1.0 NO 07/13/95
Dichloromethane ug/L 1.0 NO 07/13/95
trans-1,2-Dichloroethene ug/L 1.0 ND 07/13/95
1,1-Dichloroethane ug/L 1.0 NO 07/13/95
Chloroform ug/L 1.0 NO 07/13/95
1,1,1-Trichloroethane ug/L 1.0 NO 07/13/95
Carbon tetrachloride ug/L 1.0 NO 07/13/95
1,2-0ichloroethane ug/L 1.0 1.7 07/13/95
1,1,,2-Trichloroe,thene ug/L 1.0 NO 07/13/95
1,2-Dichioropropane ug/L 1.0 NO 07/13/95
Bromodichlormethane ug/L 1.0 NO 07/13/95
2-Chloroethoxyethene ug/L 1.0 NO 07/13/95
cis-1,3-Dichloropr©pene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachlaroethene
Dibromochloromethane
B romo fo rn
1,1,2,2-Tetrachl
Methyl-t-butyl e
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyl benzene
e
r
ane
ug/L 1.0 NO 07/13/95
ug/L 1.0 NO 07/13/95
ug/L 1.0 ND 07/13/95
ug/L 1.0 NO 07/13/95
ug/L 1.0 ND 07/13/95
ug/L 1.0 NO 07/13/95
ug/L 1.0 NO
ug/L 20 380
ug/L 1.0 12
ug/L 5.0 130
ug/L 1.0 13
ug/L 1.0 NO
ug/L 1.0 4.3
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/95
07/13/9

k McCormack
Mr
Page
Client Reference: Piney Pods
RACE Sample Number::
Gate Collected:
Date Received:
Client Sample tC:
Parameter
ORGANIC ANALYSIS
PORGEABLE MALOCARBONSAND AROMATICS
Xylenes ug/L 71
1,3_Oic l red zed egiL .0 NO
1,4Cic iero e e ug/L NO
1,2 icr erzer ug/L .0
h
ORATORY ANALYSIS
duly
PACE Pr . , Number: 55 707514
2 0430468
7 05 5
7/07/95
-4
CATS ANAL'
07/
07/1
07/13/9
07/ 3 95

Mr. Mark McCormack
Page 9
Client. Reference: Piney Woods
PACESample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
Units
REPORT OF LABORATORY ANALYSIS
July 21, 1995
PACE Project Number: 6 0707514
92 0430476
07/05/95
07/07/95
RW-5
IETH00 GATE ANAL
7
PURGEABLE HALOCARBONS AND AROMATICS 501/602
Dichlorodifluor©methane ug/L 1.0 NO 07/14/95
Chloromethane ug/L 1.0 NO 07/14/95
Chloroethene (Vinyl chloride) ug/L 1.0 NO 07/14/95
Bromomethane ug/L 1.0 ND 07/14/95
Chloraethane ug/L 1.0 ND 07/14/95
Trichlorofluorarnethane ug/L 1.0 NO 07/14/95
1,1-Dichloroethene
Dichloramethane
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichoroethane
ug/L 1.0 NO 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 NO 07/14/95
Carbon tetrachloride ug/L 1.0 NO 07/14/95
1,2-Oichloroethane ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethene ug/L 1.0 NO 07/14/95
1,Z-0ichloropropane ug/L 1.0 NO 07/14/95
Bromodichlormethane ug/L 1.0 NO 07/14/95
2-Chloroethoxyethene ug/L 1.0 NO 07/14/95
cis-1,3-Oichloropropene ug/L 1.0 ND 07/14/95
trans-1,3-0ichloropropene ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethane ug/L 1.0 NO 07/14/95
Tetrachloroethene ug/L 1.0 ND 07/14/95
Oibromochlor©methane ug/L 1.0 NO 07/14/95
Bromoforrn ug/L 1.0 NO 07/14/95
1,1,2,2-Tetrachloroethane ug/L 1.0 NO 07/14/95
Methyl-t-butyl ether ug/L 5.0 55 07/14/95
Isopropyl ether ug/L 1.0 NO 07/14/95
Benzene ug/L 1.0 6.5 07/14/95
Toluene ug/L 1.0 NO 07/14/95
Chlorobenzene ug/L 1.0 NO 07/14/95
Ethylbenzene ug/L 1.0 NO 07/14/95
1100 Kiraly Minus. Sum ,
Asnetsvolle, NC 2E073
r m4-aaex
RV- 744.875.9091

Cient Reference: Pi ey Woods
PACE Sample Number
Date Collected:
Received:
pie 1
OR IC ANALYST
PURGEABLE WALOCARBONS
Xylenbs
1,3-Di' bl b
1,4 -Oichlorobbnbenb
1,2 -Oichlorobenzene
YSiS
AROMATICS
July 21,
PACE Arai
55`
ct Nur
er 55C707514
92 043 476
07/05/D5
0 5
RW-5
Units MO 0 DATE ANA YZE
601
1.0 ND 07/14 95
ug 1.0 /1455
ug/L 1.0 NO 0 4/95
9
ugil. 1.0 0 14/ 5.

Mr. Mark McCormack
Page 11
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample Ip:
Parameter
ORG.'NIC ANALYSIS
Pt1RGEABLE HAL0CARB0NS ANO ARC
Dichlorodifluoramethane
Chlaromethane
Chloroethene (Vinyl chloride)
Bramamethane
Chloraethane
Trichlorofluoramethane
1,1-Dichloroethene
Dichloromethane
trans-1,2-Oichloroethene
1,i-0ichloroethane
Chloroform
1,1,1-Trichloroethane
TICS
REROAT OF A ORATORY ANALYSES
Units
July 21, 19
PACE Pro
92 04304$4
07/05/g5
07/07/95
MW-1
501/602
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 1.3
550707 S i.4
DATE ANALYZE
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
Carbon tetrachloride ug/L 1.0 NO 07/14/95
1,2-Dichloroethane ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethene ug/L 1.0 NO 07/14/95
1,2-Dichlorapropane ug/L 1.0 NO 07/14/95
Bromodichlormethane ug/L 1.0 NO 07/14/95
2-Chloroethoxyethene ug/L 1.0 NO 07/14/95
cis-1,3-Dichlaropropene
trans-1,3-Dichloroprapene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochlaromethane
Bromoforr
1,1,2,2-Tetrechloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene.
Chlorobenzene
thylbenzene
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

dark cCormack
Page F
ClientReference: Piney W ods
PACE Sample Number::
Cate Collected*
GateRece ved:
Cl ent Samole
Parameter
ORGANIC ANALYSIS
R0R0EABLE HALOCANBONSAND ARO TICS
Xy1 enes
1,3
, 4 -Dicblorobenzene
,2 -Dichlercbenzene
u/L
u/-
u/L.
u/L
ORATORY ANALYSIS
July 21,
PACE
2 0430484
0705/95
07
NO
ND
N
D'
50707514
DATE ANAL"ZE
07/ 4/95
07/
07/
/4/95

Mr. Mark McCormack
Page 13
Client Reference: Piney Woods
PACE Sample Numbe'
Date Collected:
Date Received:
Client Sample ID:
Parameter
Uni
REPORT OF ,A8ORATORY ANALYSIS
July 21, 1995
PACE Project. Number:
92 0430492
07/05/95
07/07/95
MW-4
7
7514
ETHOD DATE ANALYZED
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS 501/602
Dichloradifluoromethane ug/L 1.0 ND 07/14/95
Chloromethane ug/L 1.0 ND 07/14/95
Chloroethene'(Vinyl chloride) ug/L 1.0 NO 07/14/95
Bromomethane ug/L 1.0 ND 07/14/95
Chloroethane ug/L 1.0 ND 07/14/95
Trichlorofluoramethane ug/L 1.0 NO 07/14/95
1,1-0ichlaraethene ug/L 1.0 NO 07/14/95
Dichloromethane ug/L 1.0 NO 07/14/95
trans-1,2-Dichloroethene ug/L 1.0 NO 07/14/95
1,1-Dichloroethane ug/L 1.0 NO 07/14/95
Chloroform ug/L 1.0 NO 07/14/95
1,1,1-Trichloroethane ug/L 1.0 NO 07/14/95
Carbon tetrachloride ug/L 1.0 NO 07/14/95
1,2-Dichloroethane ug/L 1.0 NO 07/14/95
1,1,2-Tr-ichlaroethene ug/L 1.0 NO 07/14/95
1,Z-Dichloropropane ug/L 1.0 ND ' 07/14/95
Bromodichlormethane ug/.L 1.0 NO 07/14/95
2-Chlaraethoxyethene ug/L 1.0 NO 07/14/95
cis-1,3•-Dichloropropene ug/L 1.0 NO 07/14/95
trans-1,3--Dichioropropene ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethane ug/L 1.0 NO 07/14/95
Tetrachloraethene ug/L 1.0 NO 07/14/95
Dibromachloramethane ug/L 1.0 NO 07/14/95
Bromoform ug/L 1.0 NO 07/14/95
1,1,2,2-Tetrachloroethane ug/L 1.0 NO 07/14/95
Methyl-t-butyl ether ug/L 1.0 2.3 07/14/95
Isopropyl ether ug/L 1.0 ND 07/14/95
3enzene ug/L 5.0 83 07/14/95
Toluene ug/L 1.0 28 07/14/95
Chiorobenzene, ug/L 1.0 NO 07/14/95
Ethylbenzene ug/L 1.0 1.6 07/14/95
98001Cn1ey Avenue. Suite 100
H nretsvIe, NC 28071
TEL [phone]
FAX: [phone]

Client Reference: Piney oods
PACE Sample Number:
Dote Collected:;
Date Received:
Client EemPle 1. t.,
etas
R R1C ANALYSIS
REPORT OF ORATO Y ANALYSIS
Units
July 21 595
PACE Project
92
07 7/95
4
PURGEAELE NALOCARBONSAROMATIC
XYlenen1.0 33
1,3 -Dicillonbnentene egiL0 ND
1,4 -Oichlorodenzene ug/L 1.0 NO
1,2- i bl b n ne 119/L0 R
62
er:
T
707514
ANALYZED
07/14/95
07/14/95
07/14/95
07/14/95

crwoorcrootuatm tr.
Mr. Mark McCormack
Page 15
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALQCARB0NS AND AROMATICS
Dichiorodifluoromethane ug/L SOO NO 07/14/95
Chloromethane ug/L 500 NO 07/14/95
Chloroethene (Vinyl chloride) ug/L 500 NO 07/14/95
Bromornethane ug/L SOO ND 07/14/95
Chloroethane ug/L 500 ND 07/14/95
Trichlorofluoromethane ug/L 500 ND 07/14/95
Units
REPORT OF LABORATORY ANALYSIS
July 21, 1995
PACE Project: Number: 6a►07C7514
92 04305p6
07/05/95
07/07/95
BMW-5
!0D
DATE ANALYZED
601/602
1,1-Dichloroethene ug/L 500 ND 07/14/95
Dichloromethane ug/L SOO NO 07/14/95
trans-1,2-Dichloroethene ug/L 500 ND 07/14/95
1,1-Dichloroethane ug/L 500 NO 07/14/95
Chloroform ug/L 500 ND 07/14/95
1,1,1-Trichloroethane ug/L 500 NO 07/14/95
Carbon tetrachloride ug/L 500 ND 07/14/95
1,2-Dichleroethane ug/L 500 NO 07/14/95
1,1,2-Trichloraethene ug/L 500 NO 07/14/95
1,2-Dichlorcpropane ug/L son ND 07/14/95
Bromodichlcrmethane ug/L. SOO NO 07/14/95
2-Chloroethoxyethene ug/L SOO ND 07/14/95
cis-1,3-0ichloropr0pene ug/L SOO NO 07/14/95
trans-113-Dichloropropene ug/L 500 NO 07/14/95
1,1,2-Trichloroethane ug/L 500 NO 07/14/95
Tetrachloroethene ug/L 500 ND 07/14/95
Dibromochloromethane ug/L 500 NO 07/14/95
3rcmaform ug/L Sap NO 07/14/95
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyl benzene
ug/L 500 NO
ug/L 500 520
ug/L 500 NO
ug/L SOO 5800
ug/L 1000 38000
ug/L 500 ND
ug/L 500 2200
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

Mr. Mark McCormack
Page 16
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
REPORT OF L.ORATORY ANALYSIS
Units
July 21, Tg55
PACE Project Number: 650707514
92 0430506
07/05/95
01/07/95
MW-5
DATE ANALYZED
PURGEABLE HALCCARSCNS AND AROMATICS 60I/602
Xylenes ug/L 500 12000 07/14/95
1,3-Oichiorobenzene ug/L 500 ND 07/14/95
1,4-0ichiorobenzene ug/L 500 NO 07/14/95
1,Z-0ichlarabenzene ug/L 500 NO 07/14/95

Mr. Mark McCormack
Page 17
Client Reference: Piney Woods
PAC' Sample Nurnber:.
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALQCARBONS AND AROMATICS
Oi chl oradi fl uoromethane
Chloromethane
Chiorrethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlor©fluoramethane
REPORT OF LABORATORY ANALYSIS
Units
July 21, 1995
PACE Project Number: 550707514
9Z 0430514
07/05/95
07/07/95
MW_7
M OU DATE ANALYZED
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
ugL 5.0 NO
ugL 5.0 NO
ug/L 5.0 NO
ug/L 5.0 NO
ug/L 5.0 NO
ug/L 5.0 NO
thene ug/L 5.0 NO 07/14/95
ane ug/L 5.0 ND 07/14/95
,2-0ichloroethene ug/L 5.0 ND 07/14/95
0ichl©rQethane ug/L 5.0 NO 07/14/95
Chloroform ug/L 5.0 NO 07/14/95
,1-Trichloroethane ug/L 5.0 NO 07/14/95
Carton tetrachloride
1,2-Qichloroethane
1,1, 2---Tr ch l oraethene
1, 2-:Oi chl or©propane
Bramodichlormethane
2-Chlorcethaxyethene
ug/L 5.0 ND 07/14/95
ug/L 5.0 20 07/1.4/95
ug/L 5.0 ND 07/14/95
ug/L 5.0 NO 07/14/95
ug/L 5.,9 NO 07/14/95
ug/L 5.0 NO 07/14/95
cis-1,3-Oichloropropene ug/L 5.0 NO 07/14/95
trans-1,3-0ichioropropene ug/L 5.0 NO 07/14/95
1,1,2-Trichloroethane ug/L 5.0 NO 07/14/95
Tetrachloroethene ug/L 5.0 NO 07/14/95
Dibromochlor©methane ug/L 5.0 NO 07/14/95
Brornoform ug/L 5.0 ND 07/14/95
1,1,2,2-Tetrachloroethane
Methyl--t-butyl ether
isopropyl ether
Benzene
Toluene
Chlorabenzene
Ethylbenzene
ug/L 5.0 NO
ug/L 20 370
ug/L 5.0 7.2
ug/L 20 420
ug/L 5.0 NO
ug/L 5.0 NO
ug/L 5.0 NO
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/9

Cl iens Reference: Piney Wilds
PACE
Cate Cec
Date Receive
Client
Parameter
REPORT OF8 .
Units
OR ANALYSIS
PURGEABLE HALOCARBON ANO AROMATICS
Xyl ug/L
1 , orobenzene ug/L
, 4-0i c l orobenzene og/L
1,411rdr ug/L
July 1,
PACE Project Number:650707514
0430514
07/07/96
M 7
OATS ANALYZED
0
07/
07/
07/
07/14/

Mr. Mark McCormack
Page 19
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Dichloradifluoromethane
Chlaromethane
Chloraethene (Vinyl chloride)
Bromamethane
Chloroethane
Trichlorofluoromethane
REPORT OF LABORATORY ANALYSES
Un
July 21, 1995
PACE Project Number:
92 0430522
07/05/95
07/07/95
MW-8
ug/L 10 NO
ug/L 10 NO
ug/L 10 NO
ug/L 10 NO
ug/L 10 NO
ug/L 10 NO
0
DATE ANALYZ7C
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
1,1-Dichloroethene ug/L 10 ND 07/14/95
Dichloromethane ug/L 10 NO 07/14/95
trans-1,2-Oichloroethene ug/L 10 NO 07/14/95
1,1-0ichloroethane ug/L 10 ND 07/14/95
Chloroform ug/L 10 ND 07/14/95
1,1,1-Trichlaroethane ug/L 10 NO 07/14/95
Carbon tetrachloride ug/L 10 ND 07/14/95
1,2-0ichloraethane ug/L 10 NO 07/14/95
1,1,2-Trichlbroethene ug/L 10 NO 07/14/95
1,Z-0ichlaropropane ug/L 10 NO 07/14/95
Bramodichlarznethane ug/L 10 NO 07/14/95
Z.-Chlorcethoxyethene ug/L 10 NO 07/14/95
cis-1,3-Dichloropropene
trans-1,3-0ichlorapropene
1,1,2-Trichloraethane
Tetrachloroethene
Dibramochiaromethane
Bromofarm
1,1,2,2-T e trachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyl benzene
ug/L 10 NO 07/14/95
ug/L 10 NO 07/14/95
ug/L 10 NO 07/14/95
ug/L 10 ND 07/14/95
ug/L 10 NO 07/14/95
ug/L 10- NO 07/14/95
ug/L 10 NO
ug/L 10 570
ug/L 10 NO
ug/L 50 1700
ug/L 10 72
ug/L 10 NO
ug/L 10 37
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

Mr. Mark
Page 20
CIent Reference: ineyl ads
PACE Sample Number::
Date Collected:
a Received:
Pt SamPle ID:
P r e er
ORGANIC ANALYSIS
PURGEA5L HALOCARBONS AROMATICS
Xyl enes
1,3-0i dill ctroteinzerte
4-01 Ibtilortidertzetie
12-01
ANALYSISREP FIT OF ORATORY
l ts
ug/L
u
uL
ug/L
July 1, 1995
PACE Project Number: 30707514
10
10
92 0430 2
07/05/95
07/07/95
75
NO
NO
NO
2
ATE ANAL ZED
07/
07/14/95
07/14/95
07/14/95

Mr. Mark McC©r ack
Page 21
Client Reference: Piney Woods
PACE Sample Numbe
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
Units
PORT OF .A RATORY ANALYSIS
July 21, 1995
PACE Project Number: r50707514
92 0430530
07/05/95
07/07/95
KW-9
PIJRGEASLE HALOCARSONS AND AROMATICS
Dichlorodifluoromethane ug/L 20 NO
Chloromethane ug/L 20 NO
Chloroethene (Vinyl chloride) ug/L 20 NO
Bromomethane ug/L 20 NO
Chloroethane _ ug/L 20 NO
Trichlorofluoromethane ug/L 20 ND
1,1-Dichlaroethene ug/L 20 NO
Dichlor©methane ug/L 20 ND
trans-1,2-Dichlaraethene ug/L 20 NO
1,1-Oichlaroethane ug/L 20 ND
Chloroform - ug/L 20 NO
1,1,1-Trichloroethane ug/L 20 NO
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichloroethene
1,2-Dichloropr©pane
Bromodichlorrnethane
Z-Chloroethoxyethene
cis-1,3-Dichlorapropene
trans-1,3-0ichlorapropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibramochioromethane
Brom©form
ug/L 20 NO
ug/L 20 NO
ug/L 20 NO
ug/L 20 ND
ug/L 20 NO
ug/L 20 NO
ug/L 20 NO
ug/L 20 " ND
ug/L 20 NO
ug/L 20 NO
ug/L 20 NO
ug/L 20 NO
1,1,2,2-Tetrachloroethane ug/L 20 ND
Methyl-t-butyl ether ug/L 1000 2300
Isopropyl ether ug/L 20 170
Benzene ug/L 1000 6800
Toluene . ug/L 1000 55000
Chlorobenzene ug/L 20 NO
Ethylbenzene
ug/L 1000 4400
601/60Z
GATE ANALYZED
07/14/95
07/14/95
07/14/95
07/14/95
07,/14/95
07/14/95
07/1.4/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/'14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

ark McC rmack
Page2
Client Reference: Piney oode
PACE ] lumber:
Gate Col acted:
Date Received:
Client Sample ID:
Perimeter
ORGANIC ANALYSIS
PURREABLE HALOCARBONSAd O AROMATIC
XYleees/L 1000 000
1,0hloo amens OL 20 NO
1,4 -Oichlorobenzene 1419/1. 20 NO
1,-Oh]rab gL 20 NO
REPORT OF
ORATORY MALYSIS
July 21, I
PACE
92 0430530
07/05/95
07/07/95
070714
07/14/95
07/14
07/14/95
07/14/95

Mr. Mark McCormack
Page 23
Client Reference: Piney Woods
REPORT OF LABORATORY ANALYSIS
July 21, 1995
PACE Project Number: 550707514
PACE Sample Number: 92 0430549
Date Collected: 07/05/95
Date Received: 07/07/95
Client Sample ID: RW-11
Parameter
ORGANIC ANALYSIS
•
Unit MOL METhOD DATE ANALYZED
PURGEABLE HALOCARBONS ANO AROMATICS 601/602
Dichlorodifluornmethane ug/L 1.0 NO 07/14/95
Chloromethane ug/L 1.0 NO 07/14/95
Chloroethene (Vinyl chloride) ug/L 1.0 NO 07/14/95
Bromomethane ug/L 1.0 NO 07/14/95
Chloroethane ug/L 1.0 NO 07/14/95
Trichlorofluoromethane ug/L 1.0 NO 07/14/95
1,1-Oichloroethene ug/L _ 1.0 NO 07/14/95
Dichioromethane ug/L 1.0 NO 07/14/95
trans-1,2-0ichloroethene ug/L 1.0 NO 07/14/95
1,1-0ichloroethane ug/L 1.0 NO 07/14/95
Chloroform ug/L 1.0 NO 07/14/95
1,1,1-Trich1oroethane ug/L 1.0 NO 07/14/95
Carbon tetrachloride ug/L 1.0 NO 07/14/95
1,2-Oichloroethane ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethene ug/L 1.0 NO 07/14/95
1,2-0ichloropropane ' ug/L 1.0 NO 07/14/95
Bromodichlormethane ug/L 1.0 NO 07/14/95
2-Chloroethoxyethene ug/L 1.0 NO 07/14/95
cis-1,3-Oichloropropene ug/L 1.0 NO 07/14/95
trans-1,3-Oichloropropene ug/t. 1.0 NO 07/14/95
1,1,2-Trichloroethane ug/L 1.0 NO 07/14/95
Tetrachloroethene ug/L. 1.0 NO 07/14/95
Oibromochloromethane ug/L 1.0 NO 07/14/95
Bromoform ug/L 1.0 NO 07/14/95
1,1,2,2-Tetrachloroethane ug/L 1.0 ND 07/14/95
Methyl-t-butyl ether ug/L 1.0 NO 07/14/95
isopropyl ether ug/L 1.0 NO 07/14/95
Benzene ug/L 1.0 NO 07/14/95
Toluene ug/L 1.0 NO 07/14/95
Chlorobenzene ug/L 1.0 NO 07/14/95
Ethylbenzene ug/L 1.0 NO 07/14/95
9000 Orgy Menus. Sung 100
Huntersville, PC MI
1E4 704473-4092
FAX [phone]
An anal Ocporaray encioyer

S AND AROMATICS
601 602
Mr o Mark cCo
Page 24
Client Reference: Piney
PACE p1 Nun
Data Collect
ate Pec1v
an Samp 1e
meter Units
ids
EPORT OF
ORGANIC A LSS
PURGEA8 HACA :C9
Xy1 enes
orobenzene
1, 4-01oh orobenzene
1, 1 h1 orobenzene
ug/L
ug/L
ug/L
ug
PACE Project Number: 7514
92 0430549
07/05/95
07/07/95
MW-
1.0
NO
NO
NO
NO
DATE ANALYZED
07/14
07/14
0 /14
07/14/9

REPORT OF
Mr, Mark McCormack
Page 25
Client Reference: Piney Woods
ORATORY ANALYSJS
July 21, 1995
PACE Pro ect Number: 55070751
PACE Sample Number: 92 0430557
Date Collected: 07/05/95
Cate Received: 07/07/95
Client Sample ID: MW-12
Parameter Units MOL
ORGANIC ANALYSIS
DATE ANALYZED
PURGEABLE HALOCARBONS AND AR TICS 501/5C2
Dichlorodifluor©methane ug/L 1.0 NO 07/14/95
Chloramethane ug/L 1.0 NO 07/14/95
. Chloroethene (Vinyl chloride) ug/L 1.0 NO 07/14/95
Bromomethane ug/L 1.0 NO 07/14/95
Chloroethane ug/L 1.0 NO 07/14/95
Trichlorox-1uoromethane ug/L 1.0 ND 07/14/95
1,1-0ichloroethene ug/L 1.0 ND 07/14/95
Dichloromethane ug/L 1.0 NO 07/14/95
trans-1,2-0ichloroethene ug/L 1.0 NO 07/14/95
1,1-0ichloroethane ug/L 1.0 NO 07/14/95
Chloroform ug/L 1.0 NO 07/14/95
1,1,1-Trichloroethane ug/L 1.0 ND 07/14/95
Carbon tetrachloride ug/L 1.0 NO 07/14/95
1,2.-0ichloroethane ug/L 1.0 NO 07/14/95
1,1,2-Trichloroethene ug/L 1.0 ND 07/14/95
1,Z-0ichloropropane ug/L 1.0 ND 07/14/95
Bromodichlormethane ug/L 1.0 NO 07/14/95
2-Chloroethoxyethene ug/L 1.0 NO 07/14/95
cis-1,3-Dichloropropene
trans-1,3-0ichloroprapene
1,1,2-Trichloraethane
Tetrachloroethene
0ibromochloromethane
Bromoform
1,1,2,2-Ttrachloreethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyl benzene
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 ND 07/14/95
ug/L 1.0 NO 07/14/95
ug/L 1.0 NO 07/14/95
ug/L. 1.0 NO
ug/L 1.0 1.2
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95
07/14/95

age
auk
6
lent Reference: Pins
PACE Sp1 berg
Cate Collected:
gate Received:
Client Samplel
Parameter
ORGAN7C ANALYSIS
PURGEABLE HALOCADDONAND ARO
RYlenes
1,0
1,4-Treee
1,-Tepee
REPORT OF
adz
Units
u9/L
ugiL 1.0
1.
1.0
July El, 1995
PACE Project. Nurnberg 50707514
92 0429557
97/99/99
07/07/95
MN -ID
0 DATE ANALYZED
07/14
07/14/
07/14/95
07/14/95

Mr. ,Mar, ` cCor ack
Page 27
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample IO:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS ANO AROMATICS
Cichlaradifluoromethane ug/L 1.0 NO 07/1,7/95
Chloromethane ug/L 1.0 NO 07/17/95
Chloraethene (Vinyl chloride) ug/L 1.0 NO 07/17/95
Bramomethane ug/L 1.0 NO 07/17/95
Chloroethane ug/L 1.0 NO 07/17/95
Trichlorafivaromethane ug/L 1.0 NO 07/17/95
ERORT OF LABORATORY ANALYSIS
July 21, 1995
PACE Project Number: 55O707514
92 0430565
07/05/95
07/07/95
MW-13
Units MOL ME'i`ElO0 CATE ANALYZED
1,1-Dichloraethene
Dichloramethane
trans-I,2-dichloraethend
1,1-Oichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,20ichloroethane
1,1,2.-Trichlaroethene
1,2-Dichloropropane
Bromadichlo methane
2-Chlaroethoxyethene
cis-1,3-Oichlorapropene
trans-1,3-Dichloroprapene
1,1,2-frichloroethane
Tetrachloroethene
Dibromochloromethane
8romafarm
1,1,2,2-Tetrachloroethane
4ethyl-t-butyl ether
Isopropyl ether
3enzene
Toluene
Chlorabenzene
Ethylbenzene
601/502
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L I.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L 1.0 NO 07/17/95
ug/L- 1.0 NO
ug/L -1.0 15
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO.
ug/L 1.0 NO
ug/L 1.0 NO
07/17/95
07/17/95
07/17/95
07/17/95
07/1.7/95
07/17/95
07/17/95

Page
Cl ent Reference: Piney oods
PACE SampleNumber':
pate Collected:
Data Received:
Client le ID:
Parameter
OR C ANALYSIS
PURGEABLE RALOCARBONS AND A O TICS
Xylenes
-Qi chie benzene
1,4-0 ch1 orebenzene
Z-Dichlorobenzene
CRT OF ORATORY ANALYSIS
Units
July 21, 1995
PACE Project
92 0430
07/05/95
07/07/95
W 13
11971, 0 NO
ut971. 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
50707
DATE ANALYZE
D
07/17/95
07/17/95
07/17/95
07/17/95

Mr. Mark McCcrmack
Page Z9
Client Reference: Piney Woods
PACE 'Sample Number:
Date Collected:
Date Received:
Client Sample 1D:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Dichiar©difluoroniethane ug/L 1.0 ND 07/18/95
Chl©ramethane ug/L 1.0 NO 07/18/95
Chloroethene (Vinyl chloride) ug/L 1.0 ND 07/18/95
Bromornethane ug/L 1.0 NO 07/18/95
Chloroethane_ ug/L 1.0 NO 07/18/95
Trichlor©fluor©methane ug/L 1.0 NO 07/18/95
Units
E'ORT OF LABORATORY ANA.YSS
July 21,
PACE Project Nu
92 0430573
07/05/95
07/07/95
MW-14
NAL.
601/602
1,1-Dichlaraethene ug/L 1.0 ND 07/18/95
Dichloromethane ug/L 1.0 NO 07/18/95
trans-1,2-Dichloroethene ug/L 1.0. NO 07/18/95
1,1-Dichlaroethane ug/L 1.0 NO 07/18/95
Chloroform ug/L 1.0 NO 07/18/95
1,1,1-Trichloraethane ug/L 1.0 NO 07/18/95
Carbon tetrachloride
1,2-Dichloroethane
1,1,Z-Trichleroethene
1,2-Oichlaropropane
Bromodichlormethane
2-Chloraethoxyethene
ug/L 1.0 NO 07/18/95
ug/L 1.0 ND 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 ND 07/13/95
cis-1,3-Oichloropropene ug/L 1.0 ND 07/18/95
trans-1,3-Dichioroprapene ug/L 1.0 NO 07/18/95
1,1,2-Trichloroethane ug/L 1.0 NO 07/18/95
Tetrachloroethene ug/L 1.0 NO 07/18/95
Dibromochloromethane ug/L 1.0 NO 07/18/95
Bramoform ug/L 1.0 NO 07/18/95
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethyibenzene
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
07/18/95
07/18/95
07/18/95
07/18/95
07/18/95
07/18/95
07/13/95

Mark
Page
Client
ce:
PACE 1e Number.
ate ected:
ate Received:
t Sample 1C:
Parameter
OR 1C ANALYSIS
PURGEASLE HALOCARSONSNO A
Xylenes
-Olchlorobenzene
-Dichlorobenzene
1, -Oichlurebeeteee
y
Pods
Units
July 21,
PACE Proje
92 0430573
07706/95
07/07/95
u97L, 1.0 Nib
u97L 1,0 N
JL 1.0 N
ug/L 1.0 N
707514
DATE ANALYZED
07/18/95
07/18/95
07/18/95
07/18/95

Mr. Mark McCormack
Page 31
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AND AROMATICS
Dichlorodifluoromethane ug/L 1.0 NO 07/18/95
Chloromethane ug/L 1.0 NO 07/18/95
Chioroethene (Vinyl chloride) ug/L 1.0 NO 07/18/95
Bromomethane ug/L 1.0 NO 07/18/95
Chloroethane ug/L 1.0 NO 07/18/95
Trichlor©fludromethane ug/L 1.0 NO 07/18/95
REPORT OF LABORATORY ANALYSIS
July 21, 1995
PACE Project Number: 5a50707514
92 0430581
07/05/95
07/07/95
MW-15
Units MOL ME HOO DATE ANALYZED
1,1-01chloroethene
Dichloromethane'
trans-1,2-Dichloroethene
I,1-0ichioroethane
Chloroform
1,1,1-Trick oroethane
0
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
Carbon tetrachloride ug/L 1.0 NO 07/18/95
1,2-Dichloroethane ug/L 1.0 NO 07/18/95
1,1,2-Trichlaraethene ug/L 1.0 ND 07/18/95
1,2-0ichiaropropane ug/L 1.0 NO 07/18/95
Bromodichlormethane ug/L 1.0 NO 07/18/95
Z-Chloroethoxyethene ug/L 1.0 ND 07/18/95
cis-1,3-Dichlaropropene ug/L 1.0 NO 07/18/95
trans-1,3-Dichloropropene ug/L 1.0 NO 07/18/95
1,I,2-Trichloroethane ug/L I.0 NO 07/18/95
Tetrachloroethene ug/L 1.0 NO 07/18/95
Dibromochloromet'hane ug/L 1.0 NO 07/18/95
Bromo€arm ug/L 1.0 NO 07/18/95
1,1,2,2-Tetrachloroethane ug/L 1.0 NO 07/18/95
Methyl-t-butyl ether ug/L 1.0 NO 07/18/95
Isopropyl ether ug/L 1.0 NO 07/18/95
Benzene ug/L 1.0 NO 07/18/95
Toluene ug/L 1.0 NO 07/18/95
Chlarabenzene ug/L 1.0 NO 07/18/95
Ethylbenzene ug/L 1.0 NO 07/18/'95
31103 Komi Avenue. Suite 1 CO
I4unresville, NC Z9am
TEL 70447S-90f2
FAX: [phone]f41

Eck
Client Reference: Piney Woods
PACE ple Number:
Date Collected.
Cate Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGEABLE RALOCAR50AND ARO T
l eues
1,3-Dichlorol3enzene
1,A-Dichlorobenzeme
I,2-Dichlor b
Units
ug/L
ug/L
ug/L
ORATORY ANALYSIS
July 51, 1995
PACE Pro ct eM S707514
92 0430581
07/05/95
07/07/95
MW-15
CO UTE ANALYZED
07/1
07/18/9
07/18/95
07/18/95

Mr. Mark McCormack
Page 33
Client Reference: Piney Woods
PACE Sample Number:
Date Collected:
Oate Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
PURGE4BLE KALOCAR8CNS AND AROMATICS
Dichlorodifluorcmethane ug/L 1.0 NO 07/18/95
Chloramethane ug/L 1.0 NO 07/18/95
Chloroethene (Vinyl chloride) ug/L 1.0 ND 07/18/95
Bromomethane ug/L 1.0 NO 07/1B/95
Chloroethane ug/L 1.0 NO 07/18/95
Trichlorofluoromethane ug/L 1.0 NO 07/18/95
Units
ORATORY ANALYSIS
July 2.1, 1995
PACE Project dumber: 550707514
92 0430590
07/05/95
07/07/95
OMW-1
DATE ANALYZED
601/602
1,1-0ichloroethene ug/L 1.0 1.3 B 07/18/95
Dichloromethane ug/L 1.0 NO 07/18/95
trans-1,2-0ichloroethene ug/L 1.0 NO 07/18/95
1,1-0ichloroethane ug/L 1.0 ND 07/18/95
Chloroform ug/L 1.0 NO 07/18/95
1,1,1-Trichloroethane ug/L 1.0 ND 07/18/95
Carbon tetrachloride ug/L 1.0 NO 07/18/95
1,2-0ichloroethane ug/L 1.0 2.1 07/18/95
1,1,2-Trichloraethene ug/L 1.0 ND 07/18/95
1,2-0ichloropropane ug/L 1.0 NO 07/18/95
Bromodichlormethane ug/L 1.0 ND 07/13/95
2-Chlaroethoxyethene ug/L 1.0 ND 07/18/95
cis-1,3-0ichlaroprapene
trans-1,3-Oichloropropene
1,1,2-Trichloraethane
Tetrachloroethene
Di bramochloromethane
Bromoform
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
ug/L 1.0 NO 07/18/95
1,1,Z,Z-Tetrachlaroethane ug/L 1.0 NO 07/18/95
Methyl-t-butyl ether ug/L 50 400 07/18/95
Isopropyl ether ug/L 1.0 10 07/18/95
Benzene ug/L 50 600 07/18/95
Toluene ug/L 1.0 1.9 07/18/95
Chlorobenzene ug/L 1.0 NO 07/18/95
Ethylbenzene ug/L 1.0 NO 07/18/95
4800 Kindly Avow 5u0! 100
m ma !emit. NC 20079
TEL [phone]

REPORT OFiORATORY ANALYS 1S
Client Reference: PineyWoods
PACE Semple Number;
ate Collected::
Date Received:
Client Sample I
Parameter
July 2
PACE Project Number: 704
92 0430590
07/05/95
07/07/95
M 1
Units MOL
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS AN ARO TICS'
Xylenes u9/L
1, - is i r be e e u9/L
1,4-0 chl r be e e u /L
1, - ichl rcben ene u9/L
These data have been reviewed and are approve,
DATE ANALYZED
1.0 1107/1
1.0 NO 07/1I
1.0 NO 07/
1.0 No 01/18/95
lease.

Reference: Piney Woods
Analyta f,
Method De°
Not dated
RE T OF BORATORY ANALYSIS
FOOTNOTES
pages 1 through 34
found i the
action Limit
ad at or above t
b ak
July 21,
PACE Prof
1
as irt
a

Mr Mark McCormack
Page 37
Client Reference: Piney Woods
E CRT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 37943
Samples: 92 0430433, 9Z 0430450, 92 0430468
METHOO BLANK:
Parameter
1;3-Oicnldrobenzene
1,4-0ichlorobenzene
1,2-Oichlorobenzene
SPIKE AND SPIKE DUPL
CATE:
Par meter
Ofchlorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Oichloromethane
trans-1,2-Dichloroethene
1,1-0ichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Oichloroethane
1,1,2-Trichloroethene
I,2-Oichloropropane
Bromodichlormethane
cis-1,3-Oichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Oibromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Units
ug/L
ug/L
ug/L
July 21, 1995
PACE Project Number: 55070751;
Method
MOL Blank
ITU NO
1.0 NO
1.0 NO
Spike
Spike Oup1
Units MDL 92042808Recv Recv RPD
ug/L -7.7 NO207317 -TUE -g5
ug/L 1.0 ND 20 55% 55% 0%
ug/L 1.0 NO 20 70% 70% 0%
ug/L 1.0 NO 20 65% 70% 7%
ug/L 1.0 ND 20 85% 85% 0%
ug/L 1.0 NO 20 80% 85% 6%
ug/L 1.0 NO 20 95% 95% 0%
ug/L 1.0 ND 20 65% 65Y 0%
ug/L 1.0 ND 20 95% 95% 0%
ug/L 1.0 NO 20 90% 95% 5%
ug/L • 1.0 ND 20 85% 85%
ug/L 1.0 NO 20 90% 95% 44 v„,
ug/L 1.0 NO 20 95% 90% 5%
ug/L 1.0 NO 20 85% 85% 0%
ug/L 1.0 ND 20 90% 90% 0%
ug/L 1.0 NO 20 85% 85% 0%
ug/L 1.0 ND 20 80% 80% 0%
ug/L 1.0 NO 20 85% 85% 0%
ug/L 1.0 NO 20 85% 85% 0%
ug/L 1.0 NO 20 85% 85% 0%
ug/L 1.0 NO 20 90% 90% 0%
ug/L 1.0 ND 20 80% 80% 0%
uga 1.0 NO 20 65% 65% 0%
ug/L 1.0 NO 20 80% 75% 6%
ug/L 1.0 9.5 20 98% 98% 0%

Mr. Mark McCormack
Page 36
Client Reference: Piney Woods
REPORT OF LAEORATORY ANALYSIS
QUALITY CONTROL OATA
PURGEABLE HALOCARBONS ANO AROMATICS
Batch: 92 37943
Samples: 92 0430433, 92 0430450, 92 0430468
MEMO BLANK:
July 2.1:, 199E
PACE Project Number: 650707514
Method
Parameter Units Mi1L Blank
Duch% orodi fl uoromethane ug/ L 1. 5 NO
Chloromethane ug/L 1.0 NO
Chloroethene (Vinyl chloride) ug/L 1.0 NO
Bramomethane ug/L 1.0 NO
Chloraethane ug/L 1.0 NO
Trichiorofluoromethane ug/L 1.0 NO
1,1-Oichloroethene ug/L 1.0 NO
Oichloromethane ug/L 1.0 NO
trans-1,2-0ichloraethene ug/L 1.0 NO
1,1-0ichlaroethane ug/L 1.0 NO
Chloroform ug/L 1.0 NO
1,1,1-Trichloroethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 NO
1,Z-Oichloroethane ug/L 1.0 NO
1,1,2-Trichloroethene ug/L 1.0 NO
1,2-0ichloropropane ug/L 1.0 ND
Bromodichlormethane ug/L 1.0 NO
2-Chloroethoxyethene ug/L 1.0 NO
cis-1,3-0ichloropropene ug/L 1.0 NO
trans-i,3-Oichloropropene ug/L 1.0 NO
1,1,2-Trichloroethane ug/L 1.0 NO
Tetrachloroethene ug/L 1.0 NO
Oibromochloromethane ug/L 1.0 NO
Bromoform ug/L 1.0 NO
1,1,2,2-Tetrachloroethane ug/L 1.0 NO
Methyl-t-butyl ether ug/L 1.0 ND
Isopropyl ether ug/L 1.0 NO
Benzene ug/L 1.0 NO
Toluene ug/L 1.0 NO
Chlorobenzene ug/L 1.0 NO
Eth lbenzene ug/L 1.0 NO
Xylenes ug/L 1.0 NO
9i'J00 Kin!»y AMU . SWIM 100
F rn soli. NC 2E078
lEL• 704475.9092
FAX, 704-375.9091

Mr. Mark McCormack
Page 38
Client Reference: Piney 'Woods
REPORT OF LABORATORY ANALYSES
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 37943
Samples: 92 0430433, 92 0430450, 92 0430468
SPIKE AND SPIKE DUPLICATE:
July 21, 199
PACE Project.
ber: 650707514
Spike
Spike Dupl
Parameter Units MOL 920428080 S ike Recv Recv RPO
isopropyl ether ug/L 1? NO Oa
Benzene ug/L 1.0 NO 20 90% 90% 0%
Toluene ug/L 1.0 NO 20 85% 90% 6%
Chlorobenzene ug/L 1.0 ND 20 85% 85% 0%
Ethyibenzene ug/L 1.0 ND 20 85% 90% 6%
Xylenes ug/L 1.0 NO 60 82% 85% 4%
1,3-Dichiarobenzene ug/L 1.0 NO 20 90% 90% 0%
1,4-0ichlorobenzene ug/L 1.0 NO 20 90% 90% 0%
1,2-0ichlarobenzene ug/L 1.0 NO. 20 90%, 90% 0%

Mr. Mark McCormack
Page 39
Client Reference: Piney Woods
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA
July 21, 1995
PACE Project Number: 650707514
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 38000
Samples: 92 0430476, 9Z 0430484, 92 0430492, 92 0430506, 92 0430514
92 0430522
METHOD BLANK:
Method
Parameter Units MOL Blank
Dichlorodifluoromethane ug/L r.7 ff0
Chloromethane ug/L 1.0 NO
Chloroethene (Vinyl chloride) ug/L 1.0 NO
Bromomethane ug/L 1.0 NO
Chloroethane - ug/L 1.0 NO
Trichlorofluoromethane ug/L 1.0 NO
1,1-Dichloroethene ug/L 1.0 NO
Dichloromethane ug/L 1.0 NO
trans-1,2-Dichioroethene ug/L 1.0 NO
1,1-Oichloroethane ug/L 1.0 NO
Chloroform ug/L 1.0 NO
1,1,1-Trichloroethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 ND
1,2-Dichloroethane ug/L 1.0 NO
1,1,2-Trichloroethene ug/L 1.0 NO
1,2-Dichloropropane ug/L 1.0 NO
Bromodichlormethane ug/L 1.0 NO
2-Chloroethoxyethene ug/L 1.0 NO
cis-1,3-Dichloropropene ug/L 1.0 NO
trans-1,3-0ichloropropene ug/L 1.0 NO:
1,1,2-Trichloroethane ug/L 1.0 NO
Tetrachloroethene ug/L 1.0 NO
Oibromochloromethane ug/L 1.0 NO
Bromoform ug/L 1.0 NO
1,1,2,2-Tetrachloroethane ug/L 1.0 ND
Methyl-t-butyl ether ug/L 1.0 NO
Isopropyl ether ug/L 1.0 NO
Benzene ug/L 1.0 NO
Toluene - ug/L 1.0 NO
Chlorobenzene ug/L 1.0 ND
Ethyl benzene
ug/L 1.0 NO
MOO Kinney Avenue. Selo 100
htuntermile. NC 2317'd
7044754092
FAX: 704-875-gC91
An equal Ouxrenty Effeilanor

Mr. Mark McCormack
Page 40
Client Reference: Piney Woods
RE '4RT OF LA ORATORY ANALYSIS
QUALITY CONTROL OATA.
July 21, 1995
PACE Project Number: 650 707514
PURGEABLE HALOCAR80NS AND AROMATICS
Batch: 92 38000
Samples: 92 0430476, 92 0430484, 92 0430492, 92 0430506, 92 0430514
92 0430522.
METHOD BLANK:
Method
Parameter Units MOL Blank.
Xyl enes ug/ L Tom€ NO
1,3-Oichlorobenzene ug/L 1.0 NCI
1,4-Oichlorobenzene ug/L 1.0 NO
I,2-Oichiorabenzene ug/L 1.0 NO
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MiIL Value Recv
Oichloradifluor©methane ugjL Tit ` /0 7)1
Chlaromethane ug/L 1.0 20 65%
Chlaroethene (Vinyl chloride) ug/L 1.0 20 75%
Bromomethane ug/L 1.0 20 75%
Chloroethane ug/L 1.0 ZO 90%
Trichlorafluoromethane ug/L 1.0 20 90%
1,I-Cichloraethene ug/L 1.0 20 105%
Clichloromethane ug/L 1.0 20 85%
trans-i,2-Oichloroethene ,ug/L 1.0 Z0 100%
1,1-Oichioroethane ug/L 1.0 20 95%
Chloroform ug/L 1.0 20 90%
1,l,1-Trichloroethane ug/L 1.0 20 95%
Carbon tetrachloride ug/L 1.0 20 95%
1,2-Oichloroethane ug/L 1.0 20 90%
1,1,Z-Trichioraethene ug/L 1.0 20 95%
1,2-Oichlor©propane ug/L 1.0 20 90%
Bromodichlormethane ug/L 1.0 20 85%
Z-Chloroethaxyethene ug/L 1.0 20 75%
cis-1,3--Oichloropropene ug/L 1.0 20 90%
trans-1,3-Oichloropropene ug/L 1.0 20 90%
1,1,2-Trichloroethane ug/L 1.0 20 85%
Tetrachlaroethene ug/L 1.0 20 95%
Oibromochloromethane ug/L 1.0 20 85%
3romofarm ug/L 1.0 20 75%
98QQ !Coney Avenue,, Sufi 1Qp
Ha. NC z ai
TEL m4-875-9092
FAX: 7f4. 75-9Q91

Mr. Mark McCormack
Page 41
Client Reference: Piney Woods
REPORT OF LAEORATORY ANALYSIS
QUALITY CONTROL DATA
July 21, 1995
PACE Project Number: 650707514
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 38000
Samples: 92 0430476, 92 0430484, 92 0430492, 92 0430506, 92 0430514
92 0430522
LABORATORY CONTROL SAMPLE:
Parameter
1,1,2,2-ietrachloroethane
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlorabenzene
Reference
Units MCL Value Recv
ug/ L T7U 20 7%
ug/L 1.0 20 90%
ug/L 1.0 20 95%
ug/L 1.0 20 90%
ug/L 1.0 20 90%
ug/L 1.0 20 90%
Ethylbenzene ug/L 1.0 20 90%
Xylenes ug/L 1.0 60 87%
1,3-Oichlorabenzene ug/L 1.0 20 90%
1,4-0ichlorobenzene ug/L 1.0 20 90%
1,2-0ichlorobenzene ug/L 1.0 20 90%

Mr. Mark McCormack
Page 43
Client Reference: Piney Woods
REPORT OF ORATORY ANALYSES
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 38060
Samples: 92 0430441, 92 0430530, 92 0430549, 92 0430557
METHOD BLANK:
Parameter
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-0ichlorobenzene
SPIKE AND SPIKE DUPLICATE:
Parameter
Dichlcro ifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Tri chl orofl uoroatethane
1,1-Dichloroethene
-0ichloromethane
trans-1,2-Oichloroethene
1,1-0ichloroethane
Chloroform
1,1,1-Trichloroethane
July 21, 1995
PACE Project Number: 650707514
Method
Units MDL Blank
ug/L T NO
ug/L 1.0 ND
ug/L 1.0 NO
Spike.
920430549 Spike Dub'
Units MDL MW-11 S ike Recv Recv RPO
ug/L 1.0 ND 65% 7.67
ug/L 1.0 ND 20 65% 85% 27%
ug/L 1.0 NO 2i1 70% 95% 30%
ug/L 1.0 NO 20 70% 80% 13%
ug/L 1.0 ND 20 85% 104 26%
ug/L 1.0 ND 20 60% 65% 8%
ug/L 1.0 NO. 20 100% 125% 22%
ug/L 1.0 NO 20 70% 90% 25%
ug/L 1.0 NO 20 100% 120% 18%
ug/L 1.0 NO 20 95% 115% 19%
ug/L 1.0 NO 20 95% 110% 15%
ug/L 1.0 NO' 20 95% 115M 19%
Carbon tetrachloride ug/L 1.0 ND 20 95% 110% 15
1,2-Dichloroethane ug/L 1.0 ND 20 100% 110% 10%
1,1,2-Trichloroethene ug/L 1.0 NO 20 100% 115% 14%
1,2-0ichloropr©pane ug/L 1.0 ND 20 95% 110% 15%
Bramodichlormethane ug/L 1.0 ND 20 90% 105% 15%
cis-1,3-Oichloropropene ug/L 1.0 NO ZO 100% 110% 10%
trans-1,3-Dichloropropene ug/L 1.0 NO 20 1000 115% 14%
1,1,Z-Trichloroethane ug/L 1.0 NO 20 100% 110% 10%
Tetrachloroethene ug/L 1.0 NO 20 100% 115% 14%
Oibromochloromethane ug/L 1.0 NO 20 95% 105% 10%
Brom©form ug/L 1.0 NO 20 95% 105% 10%
1,1,2,2-Tetrachloroethane ug/L 1.0 NO 20 115% 125% 8%
Methyl-t-butyl ether ug/L 1.0 ND 20 85% 80% 6%
Avenue. SW 100
Huntarsvile. NC 213 q79
FAX [phone]

Mr. Mark McCormack
Page 42
Client Reference: Piney Woods
REPORT OF LABORATORY ANA YS1S
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS ANO AROMATICS
Batch: 92 38060
Samples: 92 0430441, 92 0430530, 92 0430549, 9Z 0430557
METHOD BLANK:
July 21, 1995
PACE Project Number: 650707514
Method
Parameter Units MOL Blank
Olchiorodifluoromethane TITE- 177 NO
Chloromethane ug/L 1.0 NO
Chloroethene (Vinyl chloride) ug/L 1.0 NO
Bromomethane ug/L 1.0 NO
Chloroethane ug/L 1.0 ND
Trichlorofluoromethane ug/L 1.0 NO
1,1-0ichloroethene ug/L 1.0 NO
Oichloromethane ug/L 1.0 NO
trans-1,2-0ichloroethene ug/L 1.0 NO
1,1-0ichloroethane ug/L 1.0 ND
Chloroform ug/L 1.0 NO
1,1,1-Trichloroethane ug/L 1.0 NO
Carbon tetrachloride ug/L 1.0 NO
1,2-0ichloroethane ug/L 1.0 NO
1,1,2-Trichloroethene - ug/L 1.0 NO
1,2-0ichloropropane ug/L 1.0 NO
Bromodichlormethane ug/L 1.0 NO
2-,Chloroethoxyethene ug/L 1.0 NO
cis-1,3-0ichloropropene ug/L 1.0 NO
trans-1,3-0ichloropropene ug/L 1.0 NO
1,1,2-Trichloroethane ug/L 1.0 NO
Tetrachloroethene ug/L 1.0 NO
Dibromochloramethane ug/L 1.0 NO
Bromoform ug/L 1.0 NO
1,1,2,2-Tetrachloroethane ug/L 1.0 NO
Methyl-t-butyl ether ug/L 1.0 NO
Isopropyl ether. ug/L 1.0 NO
Benzene ug/L 1.0 NO
Toluene ug/L 1.0 NO
Chlorobenzene ug/L 1.0 NO
Ethyl benzene
Xylenes
ug/L 1.0 NO
ug/L 1.0 ND
IGncey AVOtILAIL, SOW 100
Huntersvile. NC Z8773
TEL; 704475-9092
FAX: [phone]

Mr. Mark McCormack
Page 44
Client Reference: Piney Woods
REPORT OF LABORATORY ANA .YSJS
QUALITY CONTROL DATA
PURGEABLE HAL0CAR80NS AND AROMATICS
Batch: 92 38060
Samples: 92 0430441, 92 0430530, 92 0430549, 92 04305-7
SPIKE AND SPIKE DUPLICATE:
Parameter
Isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
Xylenes
1,3-Dichlorobenzene
1,4-0ichlorobenzene
1,2-Dichlorobenzene
LABORATORY CONTROL SAMPLE:
Parameter
Dit i©radifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Dichloromethane
trans--1,2-Oichloroethene
1,1-©ichloroethane
Chloroform
1,1,1-Trichloraethane
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichloroethene
1,2-Dichloropropane
Bromodichlormethane
2-Chloroethoxyethene
cis-1,3-Dichlorapropene
Units
ug/L
ug/L
ug/L
ug/L
ug/ L
ug/L
ug/L
ug/L
ug/L
MDL
1.0
1.0
I.0
1.0
1.0
1.0
1.0
1.0
Units MDL
ug/L
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L- 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
ug/L 1.0
July 21, 1995
PACE Project Number: 650707514
Spike
920430549 Spike Dupl
MW-II S ike Recv Recv RP0
NO -7570.
NO 20 90% 90% 0%
ND 20 85% 90% 6%
NO 20 90% 90% 0%
NO 20 85% 90% 6%
ND 60 82% 85% 4%
NO
NO
NO
20 95% 105% 10%
20 100% 110% 10%
20 100% 110% 10%
Reference
Value Recv
20
20 60%
20 70%
20 75%
20 90%
20 80%
20 100%
20 75%
20 95%
20 90%
20 90%
20 90%
20 95%
20 85%
20 90%
20 90%
20 85%
20 75%
20 90%

Mr. Mark McCormack
Page 45
Client Reference: Piney Woods
REPORT OF LA ORATORY ANALYSIS
QUALITY CONTROL DATA
PURCEABLE HALOCARBONS ANO AROMATICS
Batch: 92 38060
Samples: 92 0430441, 92 0430530, 92 0430549, 92 0430557
LABORATORY CONTROL SAMPLE:
July 21, 1995
PACE Project Number: 650707514
Reference
Parameter Units MOL Value Recv
trans-1,3-Oichloropropene ugh- n
1,1,2-Trichloroethane ug/L 1.0 20 85%
Tetrachloraethene ug/L 1.0 20 95%
Oibromochloromethane ug/L 1.0 20 80%
Bromoform ug/L 1.0 20 75%
1,I,2,2-Tetrachloroethane ug/L 1.0 20 85%
Methyl-t-butyl ether ug/L 1.0 Z0 90%
Isopropyl ether ug/L 1.0 20 95%
Benzene ug/L 1.0 20 95%
Toluene ug/L 1.0 20 90%
Chlorabenzene ug/L 1.0 20 95%
Ethylbenzene ug/L 1.0 20 90%
Xylenes ug/L 1.0 60 88%
1,3--Oichlorobenzene ug/L 1.0 20 90%
1,4-0ichlarobenzene ug/L 1.0 20 90%
1,2-Oichlarabenzene ug/L 1.0 20 90%
MO Parer, Avenue. Sine 1t
Hurne[saN/. NC'Z O78
TEL: [phone]
FAX: 704-B7S-9091

Mr. Mark. McCormack
Page 46
Client Reference: Piney Woods
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS AND AROMATICS
Batch: 92 38174
Samples: 92 0430565, 92 0430573, 92 0430581, 92 0430590
METHOD BLANK:
July 21, 1995
PACE Project Number: 650707514
Method
Parameter Units MOL Blank
Dichiorodifluoromethane uTE 1TU NO
Carl oromethane ug/L 1.0 NO
Chioroethene (Vinyl chloride) ug/L 1.0 NO
Bromomethane ug/L 1.0 NO
Chloroethane ug/L 1.0 ND
Trichlorofluor©methane ug/L 1.0 ND
1,1-Dichloroethene
Dichloromethane
trans-1,2-Oichloroethene
1,1-0i chl or©ethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichioroethane
1,1,2-Trichloroethene
1,2-Cichloropropane
Bromodichlormethane
2-Chlaroethoxyethene
ug/L 1.0 2.4
ug/L 1.02.1
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/°L 1.0 1.7
ug/L 1..0 NO
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.p ND
cos-1,3-Oichlaroprapene ug/L 1.0 NO
trans-1,3-Qich1©raprapene ug/L 1.0 NO
1,1,2-Trichloroethane ug/L 1.0 ND
Tetrachlaroethene ug/L 1.0 ND
Dibromochloromethane ug/L 1.0. NO
Bromoform ug/L 1.0 ND
1,1,2,2-Tetrachioroethane
Methyl-t-butyl ether
isopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
Xylenes
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 1.3
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO

Mr. Mark McCormack
Page 47
Client Reference: Piney Woods
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA
PURGEABLE HALOCARBONS ANO AROMATICS
Batch: 92 38174
Samples: 92 0430555, 92 0430573, 92 0430581, 92 0430590
METHOD BLANK:
Parameter
1,3=-Dicniorobefizene
1,4-Dichlorobenzene
1,2-0ichlorobenzene
SPIKE ANO SPIKE DUPLICATE:
Parameter
Dichiorodifluoromethane
Chloromethane
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-0ichloroethene
Dichloromethane
trans-1,2-0ichioroethene
1,1-Dichloraethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
1,1,2-Trichloroethene
1,2-0ichloropropane
Bromodichlormethane
cis-1,3-Dichloropropene
trans-1,3-Oichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-t-butyl ether
Units
ug/ L
ug/L
ug/L
July 21, 1995
PACE Project. Number: 650707i4,
Method
MCI Blank
TTU NO
1.0 ND
1.0 NO
92043
Units MOL MW-13
ug/L17 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 ND
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 NO
ug/L 1.0 15
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Spike
Spike Oupl
Recv Recv
MT 1g5
80% 85%
85% 85%
95% 95%
85% 90%
130% 140%
105%
80%
105%
95%
90%
110%
100%
90%
95%
90%
85%
85%
85%
85%
95%
80%
75%
80%
105
80%
105
95%
90%
90%
100¼
90Y
100%
90%
85%
81%
RPO
6%
6%
0%
0%
7%
0%
0%
0%
0%
0%
20%
0%
0%
5%
0%
0%
0%
85% 0%
85% 0%
100%
75% 5%
70% 7%
80% 0%
20 80% SOA 0%
Kincay Avenue. Sun ice
Huvarsonlie. NC 2=1
TEL: [phone]
FAX [phone]

Mr. Mark McCormack
Page 48
Client Reference: Piney Woods
REPORT OF
ORATORY ANALYSIS
QUALITY CONTROL DATA July 21, 1995
PACE Project Number: 650707514
PURGEABLE HALOCARBONS ANO AROMATICS
Batch: 92 38174
Samples: 92 0430565, 92 0430573, 92 0430581, 92 0430590
SPIKE ANO SPIKE DUPLICATE:
Spike
92043055 Spike Oupl
Parameter Units MOL MW-13 S ile Recv Recv RPO
Isopropyl ether ug/L NO -IUK{
Benzene ug/L 1.0 NO 20 95% 95% 0%
Toluene ug/L 1.0 NO 20 90% 95% 5%
Chlorobenzene ug/L 1.0 NO 20 90% 90% 04
Ethylbenzene ug/L 1.0 NO 20 90% 95% 5%
Xylenes ug/L 1.0 NO 80 85% 88% 3%
1,3-Oichlorobenzene ug/L 1.0 NO 20 85% 85% 0%
1,4-Oichlorobenzene ug/L 1.0 NO 20 85% 90% 6%
1,2-0ichlorobenzene ug/L 1.0 NO 20 85% 85% 0%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MOL Value Recv
O ch1orodifluoromethane ug/L 717 20 757
Chloromethane ug/L 1.0 20 90%
Chlaroethene (Vinyl chloride). ug/L 1.0 20 95%
Bromamethane ug/L 1.0 20 100x
Chlaroethane ug/L... _1.0 20 952
Trichlorofluoromethane ug/L 1.0 20 100%
1,1-Oichloroethene ug/L 1.0 20 115%
Dichloromethane ug/L . 1.0 20 100%
trans-1,2-Dichloroethene ug/L 1.0 20 115%
1,1-Oichlaroethane ug/L 1.0 20 105%
Chloroform ug/L 1.0 20 100%
1,1,1-Trichioroethane ug/L 1.0 20 115%
Carbon tetrachloride ug/L 1.0 20 105%
1,2-Oichloroethane ug/L 1.0 20 100%
1,1,2-Trichloroethene ug/L 1.0 20 105%
1,2-Oichloropropane ug/L 1.0 20 95%
8romodichlormethane- ug/L 1.0 20 95%
2-Chloroethoxyethene ug/L 1.0 20 85%
cis-1,3-Oichloropropene
ug/L 1.0 20 100%
9600 Kingy A Stile 100
HummiYr, NC 2607Q
TEi; 761473-9092
FAX: 7 o-+a75.9i

Mr. Mark McCormack
Page 49
Client Reference: Piney Woods
E ORT OF BORATORY ANALYSIS
QUALITY CONTROL DATA
PURGEABLE HAL0CARBONS AND AROMATICS
Batch: 92 38174
Samples: 92 0430565, 92 0430573, 92 0430581, 92 0430590
LABORATORY CONTROL SAMPLE:
July 21, L995
PACE Project Number: 650707514
Reference
Parameter . Units MOL Value Recv
trans-1,3-0ichloropropene ugug-%L— 20 TUUK
1,1,2-Trichloroethane ug/L 1.0 20 100%
Tetrachloroethen ug/L 1.0 20 110%
Dibromochloromethane ug/L 1.0 20 90%
Bromoform ug/L 1.0 20 100%
1,1,2,2-Tetrachloroethane ug/L 1.0 20 100%
Methyl-t-butyl ether
Isopropyl ether
Benzene
Toluene
Chlor©benzene
Ethyl benzene
Xyl eves
1,3-0ic
1,4-0ic
1,2-0ic
ug/L 1.0 20 85%
ug/L 1.0 20 95%
ug/L 1.0 20 95%
ug/L 1.0 20 95%
ug/L 1.0 20 100%
ug/L 1.0 20 95%
ug/L 1.0 60 88%
orobenzene ug/L 1.0 20 100%
orobenzene ug/L 1.0 20 100%
arobenzene ug/L 1.0 20 100%

Page
lent Ref
OL
NO
APO
ney de
od et
detected atar Bove the
RelativePercent l ° rence
RE ORT OF
FOOTNOTES July 21, L99
pages 36 t r ugh 49 PACE Project Num er: 5 707514

Hydro -Flo Technologies, Inc. EngineeringSecification
205 E. Kehoe Blvd., Suite 2
Carol Stream, IL 60188
[phone]
FAX: [phone]
01-31-1996
COALESCING TYPE OIL/WATER SEPARATOR
Model # DP 8 F 21
1.0 EQUIPMENT SCOPE
1.1 The separator shall be a specially fabricated rectangular channel tank with
supporting structure. The separation process shall be fully automatic requiring
no moving parts. The design of the separator must satisfy the requirements of
API PUBLJCAT1ON 421, Feb, 1990 an DESIGN & OPERATION OF 011./WATER
SEPARATORS and Stoke's law. Performance enhancement must be achieved
by the use of DYNA-PAC cross corrugated coalescing media.
1.2 The separator must be designed to separate ail from wastewater meeting the
following criteria:
A) Designed flow rate = 12 gpm
B) Specific gravity of the wastewaters aqueous phase = 1.0
C) Specific gravity of the oil phase = .85
D) Oil droplet removal rate = 10 mg/I of oil droplets > 30 microns
E) Maximum allowable (dynamic) viscosity of the wastewater
to be .0115 poise
F) Media pack size to be 24 W x 24 D x 24 L (inches)
G) Maximum allowable wastewater temperature = 110 degrees F
H) Minimum protected surface area = 168 square feet
I) Minimum coalescing surface area = 336 square feet
J) Maximum cross sectional velocity.= 0.80 ftimin @ 12 gpm
K) Minimum separation chamber retention time = 7.48 min @ 12
L) Minimum sludge chamber capacity = 14 gal
M) Material of construction = molded fiberglass

Hydro -Flo Technologies, Inc. Engineering Specification
COALESCING TYPE OIL/WATER SEPARATOR
Modei # DP 8 - F 21
2.0 EQUIPMENT
2.1 The separator shall t e a specially fabricated rectangular channel
tank with supporting structure that includes:
2.1.A INFLUENT DIFFUSION CHAMBER
The flow shall enter the separator submerged, through an influent
diffusion chamber. Dispersion across the depth and width of the
OYNA-PAC is to be achieved through the use of a non -clog diffuser.
Heavy solids that fall out of suspension here must be channeled to
the sludge collection chamber.
2.1.8 SEPARATION CHAMBER
The separation chamber must be fitted with DYNA-PAC cross corrugated
coalescing media. Adequate space is to be left before and after the
chamber to prevent short circuiting through the pack.
2.1.0 SLUDGE COLLECTION CHAMBER
The sludge collection chamber must be located directly beneath the
coalescing media pack and provide ample storage capacity for the
settled sludge. The sides of the chamber must be sloped at 45
degrees to insure easy and complete removal of the settled sludge.
2.1.0 ROTARY PIPE OIL SKIMMER
The rotary pipe oil skimmer must be located at the effluent end of
the separation chamber and incorporate an adjustable oil skimming
weir. The rotating action rs to be achieved by the use of rotating
unions with zerk fittings for lubrication.
2.1.E RECOVERED PRODUCT STORAGE CHAMBER
The recovered product storage chamber must be located beneath the
separation charnber and include fittings for pump suction,
atmospheric vent, and both high and low level controls. Also, the
chamber must have provisions for the installation of an optional
sight glass. The sight glass is to be used for the visual
verification of recovered product level.
2.1.F EFFLUENT CHAMBER
The aqueous phase leaving the DYNA-PAC shall pass under the oil
retention baffle and up aver the effluent weir, which will maintain
the liquid level throughout the separator.
2.1.G REMOVABLE LIDS
The entire separator must be covered with a removable lid. The lid
must come with a D shaped, vapor tight, seal. The lid will be held
in place, and the seal compressed, by adjustable 1/2 tum draw
latches.

Hydra -Flo Technoi« gies¢ Inc. EngineeSpecifics
COALESCING TYPE CILlWATER SEPARATOR.
Model nOP8-F21
3.0 MATERIALS OF CONSTRUCTION
3.1 The tank shell. baffles and lids must be fabric
reinforced polyester resin consisting of 25%
minimum.
i of fiberglass
pped fiberglass as a
3.2 The media pack shall be fabricated of °leaphilic cross corrugated
coalescing media manufactured by HYDRA-Fi..© TECHNOLOGIES, INC.
or equal.
3.3 All piping must be type 1, grade 1, polyvinyl chloride as outlined
in ASTM 0-1784 unless specified otherwise.
3.4 All surfaces of the fabricated tank must be covered with a
continuous layer of chemically resistant, ultraviolet stabilized,
polyester gelcoat.
3.5 The rotary pipe skimmer must be fabricated of corrosion resistant
plastic and type 304 stainless steel.
3.6 The lid seal must be fabricated of closed cell, neoprene foam.
NOTE: All wetted fittings are to be fiberglass and must be molded as
an integral part of the separator. Bulkhead fittings with gaskets are
not allowed under any circumstances.
4.0 WARRANTY
4.1 The manufacturer shall warrant its products to be free of defects
in materials and workmanship. The warrantee period will last for cane
year from date of shipment.
5.0 INS'TALLATi©N, OPERATION AND MAINTENANCE MANUALS
5.1 The manufacturer shall supply three copies of the installation,
operation and maintenance manuals.
6.13 START-UP ASSISTANCE
6.1 A field representative shall be available to inspect the
installation and answer any questions pertaining to the installation,
operation and maintenance of the equipment_.
7.0 MANUFACTURERS
7.1 The unit shall be manufactured by HYDRO-FLO TECHNOLOGIES, INC.
or equal.

tow pro°ttte
System Performance Esti
Client & Proposal ilWormaticrt
George Brant
Shield Ertvbnrnmer of Me .. Inc..
Site 10: Pin Wood c]v cX stop
Contaminant
Qidaonow1hana 20 ppb
Benzene
Torun.
er
11 ppb
0.003064
4T. 85%
6ppb
0.000084
72. 5%
069 ppb 1 ppb
0.039203 f1,0442 3
87 0858% 08..3322%
1300
12.0 gprn
150 cfm
55.0 •F
5,0¥
93.5
None
Model 1341 Model1351
Effluent Effluent
Wul.r Water
Airtibalrt Air(1b.rhr)
twoarrat %rerr r+rel
1 ppb 41 ppb
0.000011 0.000011
90.9062% 9Q.9Q96%
2 ppb 1 ppb
0.000108 0.000114
92.6876% 06.1974%
17 ppb 3 ppb 1 ppb
0.044918 0.045002 0.045014
99.7846% 9097229E 90,9964%
4400 ppb 521 ppb 62 ppb 8 ppb
0.023284 0.D2'8039 0.04
80.164Q% 98.5993% 99.8342%
2300 ppb
1520 ppb
1412 ppb
0.005330
36:6367%
345 ppb
0.000610
8.2027%
56000 ppb 7083 ppb
0.282*7
8s
120 ppb
Xy4enes22000
PPb
0.000496
611.3<i80%
ppb 44S PPb
0,129387
97.9
CI Copyright 109s Ho* East Enviarr*rntd Ph
Valor 633295-70131 FAX:[phone] • J4
177
532 ppb 327 ppb 201 PPb
0.010613 0.011843 0.012000
7116061 x 85.3232% 01.3009%
796 ppb 720 ppb 641 ppb
0.001411 0.001907 0. 00216
22.8721% 29.2882% 36.1338:4
162 ppb 13Pb 4 ppb
1329173 0.320001 0.333121
00.7057% 099578% 99.9940%
4 ppb 2 PPb 1 ppb
0.023696 0.000709 0.000714
97.1221x. 99.11rm. ssuV7%
•ct ppb
0.132057
100.0000%
41 ppb-
0.132058
100.0000%

F+..CWRANGE: 1.2to7USGPM
cs MSS Environmental S btnersbie Meta Srclardj
Qpersanq Tamperatrac: 104°F (40 C)
Operating Pressure 220 PS
m Number el Starts Fsltr Haarr. 100
Resemraersted Flow Past Meter: 0.25 tti'aec
Franklin P•dirttc r Recovery raazoctr 'e optional.)
NFT
PUMP EN© ccNSTRUCTnCN MArEJ ALS: Stains Stee9 a 1 Tin*
INSTALLATION: ION: Unit to be installed vertical l r liar subroerge 3 eperat on.

y

Perf©r anc:. Curves
4
CAPAC I' (GPM)
lain less Steel
4 St* Mesa Sid
304 Stainless Slant & Tenon*
304 Stainless Steel
Tedorrs
304 Stainless Steel
304 Stainless Steel
304 Stainless Sleet
204 Stainless Steel
329/42C//4 1 Stainless Steel
3'04Staltttess Steel
304 Stainless Ste
304 Stainless Stet
Tallowy
GRUNCFCS Pumps C
Suptxtrr Can
Sand Slinger
Shall Extension
Dannregm
Stir Housing
RI Plug Screw
RI PtWasher
• Clovis. CA 38 t 2
: Allcntams. CA

100M M
PT Suc:icaet
HP 34521 AP!+i

SOIL VACUUM EXTRACTEXTRACTION
Sail Vacuum Extraction (S"VE) is used to
enhance volatilization of organics and as a
coilecdon system for in -situ air sparging.
Here's how it works: after an assessment of
the contamination or spill has been made,
a well or wells are drilled. A Soil Vacuum
Extraction System (SVE) is connected to the
well or wells to draw air/VCCs from the
surrounding soil. Granular activated carbon
(CAC) is available to capture the VCCs and
clean air is then released into the environ-
ment
Systems come pre -assembled and skid
mounted. Standard equipment includes a
55-gallon moisture separator, in -fine parti-
cle filter, relief valve, Minihelic pressure
gauge and motor starter. Systems are fitted
for pre -blower carbon adsorption units to
increase the life of the carbon.
OPTIONS:
High level shut -Off for the moisture separator
Automatic pump -Out of the moisture separator
Thermal or catalytic oxidation treatment systems available
Temperature gauges
Activated carbon far air discharce
Trailer mounted mobile units also available
Air flow measurement device
Model
30C SVE3
Blower Motor
Regenerative
Regenerative
Regenerative
Regenerative
Regenerative
HP Volts
1 135/230
2.0 115/230
5S no
6 230/460
10 230/460
Custom systems are available for any flaw rate with several blower opts
Ratron, NYB and Spencer. Model 1 OOSVE is available for rent for pilot stu
explosion -proof control station- Models ISt1SVE. MOVE and 300SVE have e
starters with overload protection.
Phase
1
1
Your
AFtTERS. 2300 NW TZS'T PLACE G.uNESVIU.L, Ft. 32b$ 3 rr.•*.
Blower
Performance
C'LM 0 39" WC
100GM036"WC
200CF+Mal40"WC
200 Gw @ 40"WC
300 CPA @ 45" WC
uding Cast, Paxton,
Model 40SVE has an
-proof magnetic
Inlet
Outlet
yr
7Z"
Y"
3"
73.7660

CEo RE
CONTINENTAL.
SPECIFICATIONS
200SVE, Soil Vacuum Extraction
Model:
Outlet
Blower
D
Inlet Filter
Relief Valve=
Vacuum Gaugc
Power Requirem
Optional Equipment
Demister Pump Out
D
Vapor Bx uu 3
36" - with steel skid -wand
Gast Regenerative Blower, Model R6P155Q-
200 cfm $ow, 15 Hp, c to ion -prom =tar
thermal overload. sealed air stream, rugged construction,
low rvaintesractcc
CES 55.gallon Mcasi
Solberg, CSL-F.3 53
Gast, Model AG253
Dwyer t
230 volt.
(Three Phase
C
e Phase, 30 amp,
o available)
Explosion proof controls autc nad
detuziter, pump 230 volt: 1/3 Hp,
Model 55MS, 1/2" FP"f drain
out water from the
of
Explosion proof level sw tch. turns aif blower an

low profile air
System Performance Estimate
Great & Proposal Informal an:
George Brant
SMMekkt Eavin nmarnl Rem.1nc.
Site ID: Piney Wood clack Stop
c
iers
Untreated Model 1311
influent Effluent
Meer* Target
1.t4DicMaroethene 2 ppb
Benzene
Toluene
XYfenee
7500 ppb
4400 ppb
2300 ptb
1030 ppb
Water !�
Alr(lbertir)
% removal
<1 ppb
0.000010
01.6686%
11 ppb
0.000064
472385%
069 ppb
0.039203
87.0858%
56000 ppb 7563 ppb
0.282827
"ss.
120 ppb
2200
37 ppb
t1.000496
pro 445 ppb
0.133387
97.9802%
Model 1321
Effluent
Water
Abrbelv%1
removal
<1 ppb
0.000011
29.3042%
6 ppb
0.000034
7'2.958S%
126 ppb
0.044263
08.3822%
62 ppb
0,02603Q
98.5093%
066 ppb
0.00e808
62.3479%
Pb
1130 ppb
0.323382
97.0462%.
12 tit*
0.0b0848
20. 806%
9 ppb
3.132004
Model chosen: 1300
Water Raw Rate: 12.0 gym
Alr Flaw Rale: 150 drn
Water Temp: 55.0 'F
Air temp: 55.0 'tF
ANY Ratio: 93.5
Safety Factor None
Model 1331
Effluent
Water
Mac
% rerrraval
<1 ppb
0.000011
99.9420%
3 ppb
0.000102
85 9380%
17 ppb
0.044918
99.7846%
532 ppb
0.0r10613
7& 1%
795 ppb
0.001411
22.8721.%
162 ppb
0.3s29173
00.7057
4ppb
0.000614i6
97.1031%
Model 1341
EffluentWSW
% removed
<1 ppb
0.000011
99,.9962%
2 ppb 1 ppb
0.000103 0.000114
92.6876% 96..1974%
3 ppb
0.045002
99.9722%
1 ppb
0.026406
69.9804%
32T ppb
0.011843
85.82326
729 ppb
0.001807
29.2582%
24 ppb
0.330001
130.9578%
2 ppb
0.000708.
913.1127%
1 ppb
0.132058
100.0000%
640 ppb
0.002167.
35.1338%
4 ppb
0.330121
99.9940%
1 ppb
0.000714
99.72:77%
<1 ppb
0.132058
100.fl000%

Liquid Phase Carbon Usage Estimate
FLOW IN GPM:
FLOW IN GED:
PERFORMANC:
Benzene
Toluene
MTBE
Methylene Chloride
1,2-Dichloroethane
Naphthalene
TOTALS
1200,
17280,00
CONO1
1
4
201
1
1
877
LB. CONT
PER DAY
0.00
OE00
0.02
0.00
0.00
0,08
LB. CARBON La. CONTI LB, CARBON/
PER iY *.# 1000 gat
0.10
0.07
11.30
15.
1.03
# ;
0,1 28.38
0.00
0,00
0.00
0.00
0.00
0.01
0.01
0,01
0.00
0.78
1.04
0.07
1.96