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NCG530172_application_20170605
eae• • sTrout Sunburst Firms TR T FARMS 314 IndustraI Park Drive Waynesville, INC 28786 828 648 3010°800 673 3051 0 Founded in 1948 www.sunbursttrout.com May 10, 2017 Dear Mr. Weaver: I am the CFO of Sunburst Trout LLC. Our fish processing facility is in the Waynesville Industrial Park. The waste water from our processing goes into the Junaluska Sanitary District. This request is asking that DENR DWR grant a general NPDES permit for our fish holding tanks to discharge into the storm water drain at the industrial park. Currently, the well water drawn is metered and that determines the cost of using the sewer discharge for the fish holding tanks. Currently, the discharge from the fish tanks goes directly into the sewer. The decision to use Junaluska Sanitary District for the fish tank discharge was made based on erroneous information from the company that sold and installed the recirculating fish tanks and equipment. The amount of water needed to efficiently operate the tank system information was drastically underestimated. We were told that this recirculating system would need almost no fresh well water to be added and discharged. Based on this data of water exchange and discharge, it was estimated that it would cost approximately $100 per month to operate the partial recirculating fish tank system. The partial recirculating system has four total tanks. Each "system" consists of two tanks, and a bead filter. Oxygen is introduced. The bead filter catches any solids in the system. The fish are not fed for 3 days prior to being put into the tanks and are not fed after they have been put in the system. Thus, very little solids are introduced into the tanks. However, if any solids go into the tanks, the filter catches the residual waste. These filters are backwashed into the sewer 3-4 times per week. We would continue to backwash into the sewer, even if we are granted a general NPDES permit. About 1 month after the tanks went into operation, we started getting feedback from some of our customers that the fish had an "off flavor". After much research, it was determined that the off flavor was coming from geosmin, the same organic matter in soil. It was determined that the only way to resolve this off -flavor issue was to continuously run the well and discharge at about 6 gallons per minute 24/7. If there is an upturn in consumer demand for our fish products, then the discharge number might go as high as 15 gpm due to increase in pounds of fish put into the system When we started having to use the well 24/7 at 6 gpm, it was costing about $1,700-$1,800 per month. Approximately 5 months after we started running the well constantly, Junaluska Sanitary District has almost doubled the rates. Today it is costing around $3,000 per month to run the well 24/7 at 6 gallons per minute. The annual cost $36,000 per year is a tremendous financial burden. For a company the size of Sunburst Trout, that money could hire another employee. Attached are: an application for a general NPDES permit, a diagram of how the fish holding tanks will discharge into the storm water drain beside the building, and a water analysis of the discharge from the tanks. Please contact me for a site visit if you want to see the fish holding tanks. In advance, consideration for this permit is greatly appreciated. Sincerely, Ben Eason, CFO Sunburst Trout LLC (1'• Family Grown • Sustainable • Quality • Steven W. Troxler Commissioner May 10, 2017 North Carolina Department of Agriculture and Consumer Services Division of Marketing Debra Sloan 208 Sugar Cove Rd Franklin, NC 28734 Agribusiness Development F& A XJuaculture Sp cia;ist 828.524 1264 — office 828 421 96(4 - cell debrasloan@ ear thlmk nc t Charles H. Weaver Environmental Specialist N C Division of Water Resources N C Department of Ft,nvironmental Q-aality 1617 Mail Service Center Raleigh, NC 27669-1617 Joe Sanderson Director RECEIVEDINCDEQIDWR J U N 0.5 2017 Water Quality Permitting Section Dear Mr Weaver, As the western NC Aquaculture Specialist for NCDA & CS, I encourage NCDWR to issue Sunburst Trout Company LLC a NPD HS General Permit (NC53000) for discharging their fish holding tank water at the Waynesville Industrial Park in Waynesville As you can see the water analysis enclosed, it provides information which shows the discharge is well within the parameters of tilt General Permit. I have worked with Su:.bur >t for almost 30 years. This company is a WNC trout industry leader, the second largest trout processor, and vital to the trout industry When the new processing facility was built a year ago, they drilled a well to supply fresh water to their fish holding tanks. \When the new processing facility was built, the company elected to use the Junaluska Sanitary District for their discharge from their fish holding tanks since Pentair, the corporation that sold them the fish tanks and filtration system told them that their water usage was going to be minimal. To use the Junaluska Sanitary District cot the discharge, the well water withdrawal is metered andis at determines their cost. Given that information, and the estimated cost of only S100 per month for water, the ccmF z v decided to utilize the Junaluska Sanitary District for their fish tank discharge water All of Sunburst Trout Company i.t4C processing facility eliminates their processing water into tale municipal system, so they tied their tank water discharge into the municipal system. Sunburst management soon found that they were misled regarding the amount of water needed to keep the fish fresh and to avoid off flavor. To solve the problem more water was needed; the well water is pumped a.t 6 gpm 24/7. The cost for using the water has now escalated to S3,000 per month and is causing a si_nificant econo,ntc burden as well as poses a threat to the financial iTlablit7 of this company. In advance, than' ; c Best regards, Debra Sloan Fui .s consideration. If you have any questions, please contact;1� 1020 Mail Service Center, Raleigh, NC 276 99- i020 (919107.-3100 • Fax (919) 733-0999 www.nodErnar'ke:s.org An Equal Opportunity Employer Company Name Owner Name Street Address City Telephone # Cell # NCDENR Division of Water Resources National Pollutant Discharge Elimination System (NPDES) Application for Coverage Under General Permit NCG530000 Seafood packing, fish packing and fish.farms NOTICE OF INTENT Required by 15A NCAC 02H .0127(d); term definition see 15A NCAC 02H .0103 19 (Please print or type) 1) Mailing address of applicant: 51/41A r \ k r V-cf‘rfaNc LLL sts& s• IN 3 \NA ste.A vtik QAN 0 ( • W 1 (\esvCAL c„t\c6 %AA C-CO \\ i 2) Location of facility producing discharge: Facility Name Facility Contact Street Address City County Telephone # State i✓i'i Fax # Emai 1 FOR AGENCY USE ONLY Date Received Year Month Day ao ()co QC , Certificate of Coverage N C G 5 3 t)! -7 a Check # Amount k i 0— /HA - Assigned To: CJ'icic€Jts C RECEIVED/NCDEQ/DWR JUN 0 5 2017 Water Quality Permitting Section Zip Code till bv\ 02 \t:IAnrr 5 vskr isk 1 /ou\t ri.(S LLL C o DIN 3 \te\ "S,c)\ ,mkcc-c.\ 9frr\C \‘) ..\, ne j kes\\� State ivy \\a'1 WO ° A encn .).#\ Fax # 3) This Application applies to which of the following activities: Describe the activities to be ermitted in detail: S Lee. CO v Z r � te_kk et Zip Code 61-1 Seafood packing / rinsing Fish farms [aquaculture] 4) Description of Discharge: [Required by 15A NCAC 02H .0105(c)(1)] a. Volume of discharge (in GPD): ) 300 se tt_J ObD b. The discharge is: 'ens" Continuous n Intermittent If the discharge is intermittent, describe when the discharge occurs: c. Number of discharge points (outfalls): Page 1 of 3 Revised 9/1 /2013 d. What percentage of the discharge is treated? 0 NCG530000 New Application e S e. Describe the type of wastewater being discharged (including any known pollutants present in the discharge): -00 (0 \A,*\-\ 0\- \\vC.- C 0 v\k- h 0 \ k Describe the nature of the business applying for coverage under the General Permit: mrdor t r cs\( ck too le.iSAk PO f. Identify the treatment methods in use at the facility (check all that apply): n Settling Ponds n Screens* n Floor Screens* Other (describe): v� A `gin Ac_ S � c, None Treatment Equi ment* \O a\ k \\\ tri Ce (0 f v 44fr) n *If checked, attach a description of all component specifications (design volume, retention time, surface area, etc.). Describe existing treatment facilities in detail and provide design criteria or operational data (including calculations) showing the facility can meet the requirements for coverage under the General Permit, as required by 15A NCAC 02I3.0127. g. Describe the discharge location (bay, stream, etc.): 4S4co r ( I (0,1 (, t\ h. A USGS topographic map (1:24000 scale) identifying the exact discharge location(s) must be submitted with this application. Identify all discharge points (outfalls) on this site map. �. Is the discharge directly to the receiving water? n Yes j. Name of receiving water(s): No — If no, mark the path taken by the discharge from the outfall to the receiving stream on the site map (including the pathway of any stortu sewers, ditches, canals, etc.). rt�1 5) Alternatives to Direct Discharge: [Evaluation required by G.S. § 143-215.1(b)(5)(a) and I5A NCAC 02H .0105(c)(2)) Address the feasibility of implementing each of the following non -discharge alternatives: a. Connection to a Regional Sewer Collection System - If the facility is existing and currently discharges to a POTW, when will connection not be allowed? b. Subsurface disposal (including nitrification field, infiltration gallery, injection wells, etc.) c. Spray irrigation The alternatives to discharge analysis should include boring logs and/or other information indicating that a subsurface system is neither feas ble nor practical as well as written evidence indicating that connection to a POTW is not an option. It should also include a present value of costs analysis as outlined in the Division's EncrineerinaAlternatives Analysi4 [EAA) Guidance Document. Page 2 of 3 Revised 9/1/2013 NCG530000 New Application Additional Application Requirements: For new or proposed discharges, the following information must be included in triplicate with this application or it will be returned as incomplete; per 15A NCAC 02H .0105(c) a. USGS topographic map (or photocopied portion thereof) with discharge location clearly indicated. If the discharge is not directly to a stream, the pathway to the receiving stream must be clearly indicated. b. If this application is being submitted by a consulting engineer (or engineering firm), include documentation from the applicant showing that the engineer (or firm) submitting this application has been designated an Authorized Representative of the applicant; per 15A NCAC 02H .0138(b)(1). c. Final plans for the treatment system (if applicable). The plans must be signed and sealed by a North Carolma registered Professional Engineer and stamped ' FINAL DESIGN - Not Released for Construction;" per 15A NCAC 02H .0139. d. Final specifications for all major treatment system components (if applicable). The specifications must be signed and sealed by a North Carolina registered Professional. Engineer and shall include a narrative description of the tieatment system to be constructed; per 15A NCAC 02H .0139. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Title: (Please review ISA NCAC 02H .0106(e0 for authorized signing officials) (Signature of Applicant tl (Date Signed) North Carolina General Statute 143-215.6B provides that: Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article, shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). 18 U.S.C. Section 1001 provides a punishment by a fine or imprisonment not more than 5 years, or both, for a similar offense. Design of treatment facilities must comply with requirements in 15A NCAC 02H .0138. Mail this application and one copy of the entire package to: NC DENR / DWR / Water Quality Permitting Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: Charles Weaver Page 3 of 3 Revised 9/1/2013 ME • • • 1 • g • • 3•,••'•t S,' t .9 r • •• i••[ .1••• . • , I•• • • :1•.•:-• • • • I •. •, ea, ▪ •1• • • i rat • A' ▪ .. • =,t:. r • • 1'1•• 't i•$ It.•.s4c4.•t1•,.1• .•t. • — • , - i.Fl3tit ••••• ,a s•i, r.- • • • • •r ••.r . .• it_ • ,• t{ra!aisl/aesra •r4 • ▪ ••') 1 - . . !. •i' •:.t.& .t..t .. • .• ,•;.. • •1 •. .aty 44 •f+'": t-s$t.* » 44sasii}. _> t z•: ...tr.; b•lLt KM!: Ct e• _�t.. eL t • t.. �,,•• • • .,-I• ll I i. I f�= ▪ . el;• ••t: .I • Zti~ • • i• • •Let _♦ •. 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I I' C . r_..:♦ - •e:1•• • • I �1%1 M•• Y •i •• . •f r. • • • %. • .1 rt. ••• • t••ilor.seri tla. 1•e.•;1's.0.;j•ter•�t. it) 2%1OVE iP.1.1411 1.f:11 rase 50 • • • 44 Veep*" mat i•••0191“tilie• • • • ; • • • ^ 15 -`. r • im•t ' � •1 elf • • • • 111 • • • • ... ft•Sa..:10.1.134.9.0.6143e4. •••••••••°; ‘ ilr;troll:::::• ; • • • • • • • • • • • • 44 • • • • • • • • iso • • • • • • • • • • • • • • • • • • 0 1 0 0 t • • • • • • • • • 14.4 • • • • • • 4 0 ft o • • • di • • • • tki • • • • • • • • • IT Pp • • • 11.1 • • • . *cis. • :t.t .7/60.44,i2•,..tr. •••• • . ... r • 10 I A • • 3 t • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • 1 • • • • • • • • • • • • • • • • • • • • • • • • • • 0 • • • • 1 • • 4 • • • It • • • • • • • • • • • • • • • • • • • • • • 1 • • • 0 0 • • • • 4 • I. ft • • • c3 • • • • 4 • • • • • • • • al 1 • • • • • • • ye • • • • 4 • • • • • • • • • • • • 4 • • is • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • to ret Cer • • • • rioLiceseoN cele • ace Anal kali® wwwpacelabs.cam April 26, 2017 P rivate Client P rivate Client P rivate Client Asheville, NC 28804 RE Project: Sunburst Trout Farm 4/14 Pace Project No: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 RECEIV D/NCDEQ/DWR JUN052017 Water Quality Permitting Section Dear Private Client: Enclosed are the analytical results for sample(s) received by the laboratory between April 14, 2017 and April 18, 2017 The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wntten consent of Pace Analytical Services, LLC. Page 1 of 13 ace Anal ical wwwpacetabs.com CERTIFICATIONS P roject Sunburst Trout Farm 4/14 P ace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification # E87648 Massachusetts Certification #. M-NC030 North Carolina Drinking Water Certification #: 37712 N orth Carolina Wastewater Certification #: 40 S outh Carolina Certification #. 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 ace Analytical® wwwpacelabs.com SAMPLE ANALYTE COUNT Project Sunburst Trout Farm 4/14 Pace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92337258001 92337258002 Holding Tanks Holding Tanks S M 2540D S M 2540F S M 5210B S M 5220D REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. CJH1 ALC MLS MDW 1 1 1 1 PASI-A PASI-A PASI-A PASI-A Page 3 of 13 aceAnalytical® wwwpacelabs.corn ANALYTICAL RESULTS Project: Sunburst Trout Farm 4/14 Pace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: Holding Tanks Lab ID: 92337258001 Collected: 04/14/17 08:00 Received: 04/14/17 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 04/15/17 00:53 2540F Total Settleable Solids Analytical Method: SM 2540F Total Settleable Solids ND mL/Uhr 0.10 1 04/14/17 14:45 Sample: Holding Tanks Lab ID: 92337258002 Collected: 04/18/17 07:15 Received: 04/18/17 09:06 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 2.5 mg/L 2.0 1 04/18/17 18:50 04/23/17 13:58 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND mg/L 25.0 1 04/18/17 22:20 Date: 04/26/2017 01:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnal lcat www. pacelabs.com QUALITY CONTROL DATA P roject: Sunburst Trout Farm 4/14 P ace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Q C Batch: 356772 Analysis Method. SM 2540D Q C Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92337258001 METHOD BLANK: 1979316 Matrix: Water Associated Lab Samples: 92337258001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/15/17 00:46 LABORATORY CONTROL SAMPLE: 1979317 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 268 107 90-110 SAMPLE DUPLICATE 1979318 92337252001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 12.0 11.6 3 SAMPLE DUPLICATE: 1979319 92337220001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6980 7960 13 J(D6) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 04/26/2017 01:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13 ace Analytical® www.psceIabs.com QUALITY CONTROL DATA P roject: Sunburst Trout Farm 4/14 P ace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Q C Batch: 356762 Analysis Method SM 2540F Q C Batch Method: SM 2540F Analysis Description: 2540F Total Settable Solids Associated Lab Samples: 92337258001 METHOD BLANK 1979241 Matrix: Water Associated Lab Samples: 92337258001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Settleable Solids mL/Uhr ND 0.10 04/14/17 14:45 SAMPLE DUPLICATE: 1979242 92337258001 Dup Parameter Units Result Result RPD Qualifiers Total Settleable Solids mL/Uhr ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 04/26/2017 01:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalitical® www.pacetebs.com QUALITY CONTROL DATA P roject: Sunburst Trout Farm 4/14 Pace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Q C Batch: 357013 Analysis Method. SM 5210B Q C Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92337258002 METHOD BLANK: 1980421 Matrix: Water Associated Lab Samples: 92337258002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 04/23/17 13:58 LABORATORY CONTROL SAMPLE: 1980422 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 181 91 84.6-115.4 SAMPLE DUPLICATE* 1980423 92337328001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 04/26/2017 01:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 13 ace Anal ical www pacelabs. COM QUALITY CONTROL DATA P roject: Sunburst Trout Farm 4/14 P ace Project No: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Q C Batch: 357109 Analysis Method. SM 5220D Q C Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92337258002 METHOD BLANK: 1981042 Matrix: Water Associated Lab Samples: 92337258002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 04/18/17 22w20 LABORATORY CONTROL SAMPLE: 1981043 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 1981044 1981045 MS MSD 92337376001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 10000 750 750 9850 9720 -24 -41 90-110 1 M6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 04/26/2017 01:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 13 accAnalytical wwwpacelabs.com QUALIFIERS Project: Sunburst Trout Farm 4/14 Pace Project No.: 92337258 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. N D - Not Detected at or above adjusted reporting limit. MDL - Adjusted Method Detection Limit. P QL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference N C - Not Calculable. S G - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N -Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. P ace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville ANALYTE QUALIFIERS J(D6) M6 Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS Date: 04/26/2017 01:13 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 13 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE P roject: Sunburst Trout Farm 4/14 P ace Project No.: 92337258 Lab ID Sample ID QC Batch Method QC Batch Analytical Analytical Method Batch 92337258001 92337258001 92337258002 92337258002 Holding Tanks Holding Tanks Holding Tanks Holding Tanks Date: 04/26/2017 01:13 PM S M 2540D S M 2540F SM 5210B SM 5220D 356772 356762 357013 SM 5210B 357109 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 357114 Page 10 of 13 0 Document Revised: Page 1 of Sept. 2 21,2016 Document Name: Sample Condition Upon Receipt(SCUR) ace Analytical F-CAR-CS-033-Rev.01 Document No.: Issuing Authority: Pace Quality Office Laboratory receiving sam Asheville ample Con scion Upon ltecetpt Courier Commercial Ederkk Greenwood Client Name.: Huntersville. UFed Ex ❑Pace ❑UPS EUSPS E Other: Custody Seal Present? [Yes Di Seals Intact? flYes Packing Material:. [Bubble Wrap ❑Bubble Bags Thermometer: DIR in ID: 5 Correction Factor: G) Cooler Temp Corrected (°C). Temp should be above freezin USDA Regulated Soil /A, water sample) Type of Ice:69 . L PrI W Raleigh❑ MechanicsvilleE �C"entin II I 11 IIIIIIIiIII ow. 92337258 ne COther: Blue [Done ❑Sampkeson ice, cooling process has be Biological Tissue Frozen? (_,_Yes DNo N/A 8 Date/Initials Person Examining Content Did originate in samples a quarantine zone within the United States: CA, NY, or SC (check maps)? Did sarnples originate from a foreign source (in ternationa y, Dyes ONa including Hawaii and Puerto Ricoj7 OYes Comments/Discrepancy. Chain of Custody Present? �[jNo ❑N/A 1, Samples Arrived Hold Time? within s QNo ❑N/A 2. Short Hold Time Analysis (<72 hr.j? C1 DNo ❑N/A 3se f M (C. c`G Rush Turn Around Time Requested? DYes. No DN/A 4. Sufficient Volume? II s DNo DN/A 5. Correct Containers Used? pelfgr DNo DN/A 6, -Pace Containers Used? DNo DN/A Containers Intact? Yes DNo ON/ Samples Field Filtered? DYes 1:1No. ril N/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? es II No DN/A 9. .. tiknut -Includes Date/i irrie/tu/Anatysis tviatrix: Headspace in VOA Vials (>5-6mm)? Dyes DNo / b.0. Trip Blank Present? Dyes DNo N/A 11, Trip Blank Custody Seals Present? l Des DNo /A ___ CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: (Arent-- of (t. brti Field Data Required? Des e)Pate/Tirne: Project Manager SCURF Review: Project Manager SRF Review: Date: 14 N` ©ate: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, outof temp, incorrect containers) Page 11 of 13 4. Analytical a Sample Condition Document Upon Name: Document Revised: Page 2 of Sept. 2 21, 2016 Receipt(SCUR) ace F-CAR-CS-033-F Document No.: ev,t1. Pace Issuing Quality Authority: Office *Check is verified mark and top within half of the box acceptance if pH and/or range dechlorination for Project3 preservation **Bottom half samples. box is PM: CLIENT: CD1 9pPrivate Due Date: 04/28/17 of to list number of bottles L Plastic Unpreserved (N/A) (CI-) L Plastic Unpreserved (N/A) L Plastic Unpreserved (N/A) -1 titer Plastic Unpreserved (N/A) L plastic HNO3 (pH < 2) IL Plastic ZN Acetate & NaOH (>9) Puthed.Glass jar Unpreserved ber Unpreserved (N/A) (GI-) ber HCI (pH < 2) tber H2SO4 (pH < 2) L Amber H25O4 (pH < 2) L VOA HO (NIA) L VOA Unp (N/A) airier ;. u LPlastic NaOH (pH > 12) I (6 vials per kit)-5035 kit (N/A) (3.vials per kit)-VPH/Gas kit.(N 2, L Arnber NH41 ;tic (N/A rile Plastic (N/A 11. CL ro Q 0. Q 0 U _cg) -g e G N M D D D 7 ua :7 X 0 S D Cl- x 6 Z ICJ U tip Q X h �4 ti FL .sE a) a PI re2 W 8 0 et) ate. E.' a"'. a 8 8 8 t8.7 L7 8 a a q� vWi m M sA M m ut al CO < < Q 4 ¢ d n > Q > S N m u > U" _____ hi ilik ilk iliiii IL 2 ..I.Iintat U. .11t_ iivaimili lamterm im unto al imaimmio Illiiiiiiiiiiimilma NI r II III *1. 9 10 iiik ItA L L. ,, 1 - iiiiimagro LAINis 111111 12 almat iimink lea III IIIIII . pH Adjustment Log for Preserved samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time adjusted preservation Amount of added Preservative Lot 0 Page 12 of 13 ire 5s 0 w 0 0 tQ n Q 3 0 a 0 C 31ddVVSJo3 r; 1dVUVS;o e SAMPLER NAME AND SIGNATURE Temp in °C 1111111111111111111111 IN 1 I III Ill n „3 111111 III MI I 1 a .1 .. II I mm 4 14 dr • if 1 IL Received on Ice (YIN) t Custody m Sealed Cooler CON) z tn Samples Intact (Y/N) s ITEM # o0 p� '* m g (nc 0. t. sr uiredaienf Information (1) 0 MATRIX CODE (see valid codto fait) SAMPLE TYPE (G=GRAB C=COMP) v rn rn SAMPLE TEMP AT COLLECTION # OF CONTAINERS ©31031100 Unpreserved H2SO4 HNO HCl NaOH Na2S2O3 Methanol Other Ana senneiresard Y/IV , DIMS IMO Residual Chlorine (YIN) 0 tot 0' er Co '1Y 0 1 u tiwn,N pe[oad i 1t S 074 ft! vtia \i 0 m r 0 0 z :aweN Pa(oid rn 9 9, :40N .Iepjp ese 0 3 0 3 0 z (n ~n r. —1 p rrt ?impei co 0 O 0 C . z- 0 i • 073 v A 0 µ0 1 • a 0 ge 1 The Chain -of -Custody 3of13