WQ0000672_2020 Residual Annual Report_20210315

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0000672
Applicant/Permittee City of Lumberton
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * Michael C Hunt
Email Address*
[e-mail]
Project Information
........ .....................................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
9107385311
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00000672
Has Current Existing perm nurber
Applicant/Permittee Address* Post Office Box 1388
Facility Name * City of Lumberton RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Annual Report.pdf 66AMB
Upload only 1 PCFdocurrent (less than 250 fvB). Miltiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
(M01W& way, -
Submission Date 3/15/2021

ENVIRO.. H ICE
W
PO Box 309
Lumberton, NC 28359
Phone: [phone]
Fax: [phone]
March 10, 2021
NC Environmental Quality-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Attention: Compliance Representative
Subject: 2020 Annual Report for City of Lumberton Land Application Program
(City of Lumberton WQ0000672)
Dear Compliance Representative,
Enclosed is (1) copy of the monitoring and reporting information as requited in the referenced
permit for the City of Lumberton, North Carolina. This report was complied from land
application records provided by the City of Lumberton and Enviro-Choice Recycling. The report
includes: 1) a state required annual certification for and facility information page, 2) the 2020
annual application summary table, 3) annual residual sampling summary form and laboratory
analysis reports, 4) field loading reports, 5) pathogen and vector reduction documentation, and 6)
soil analysis reports.
In July 2020 the Permitee realized that the permitted 1500 dry tons would be exceeded with the
current permit. Therefore, a new permit modification was submitted to NCDEQ to increase the
dry tonnage to 2000 dry tons. This request was granted in the form of a new permit in September
2020.
Should you need more information regarding this land application program, please contact me at
910-738-5311 or envirochoicencgggmail.com.
4J
Michael C. Hunt
Enviro-Choice Recycling
CC: Henry Harper, Wastewater ORC, City of Lumberton WWTP
Office: 910-671-3859 hharper&ci.lumberton.nc.us

ANNUAL LAND APPLICATION CERTIFICATION FORM
Robeson
Year: 2020
WQ Permit#: W00000672 County:
Facility Name (as shown on permit): City of Lumberton
Land Application Operator: Enviro-Choice Recycling, LLC Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
10 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Agj2lication Summa
Total number of application fields in the =V 43
Total number of fields utilized for land application during the year: 19
Total amount of dry tons applied during the year for all application sites: 1952.5
Total number of acres utilizes for land application during the
464.3
Part B -Annual Comniance Statement:
2020 with all conditions of the land application permit
Facility was compliant during calendar year
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations." k1k s h
Henry Harper WWTP ORC
Permittee Name and Title (type or rmt) kignyf P ttee Date
15 2A 3
Signature of Preparer Date Signature of Land Aoplier Da e
(if different from Permittee) (if different from Permittee and Preparer)
DENR FORM ACF (12/2006)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00000672 Laboratory: 1) ENCO
Facility Name: City of Lumberton 2) Cameron Anayltical
Residual Source WQ # or WQ0000672 3) Pace Anaylitical
NPDES #: 4)
WWTP Name: City of Lumberton 5)
mubluual Pxllary3la Lata
Parameter
(mg/kg)
Conc.
Limit
m r/k a
Sam le or Com osite Date
3/20/202
0
6/23/202
0
9/22/202
0
11/30/20
20
Percent Solids (%)
NA
2.7
2.1
3.4
2.78
Arsenic
75
12.1
0.38 1
1.82
0.118
Cadmium
85
0.513
0.055
0.325
0.0102
Copper
4,300
407
276
336
4.85
Chromium
NA
228
228
108
Lead
840
21.6
19.8
9.79
0.169
Mercury
57
1.75
0.0002
0.261
ND
Molybdenum
75
7.81
7.24
3.5
0.0471
Nickel
420
39.3
41.3
18.6
0:297
Selenium
100
15.6
0.31
2.33
ND
Zinc
7,500
681
613
433
14.3
Total Phosphorus
NA
17000
16000
5100
15700
TKN
NA
14000
49000
11000
1420
Ammonia -Nitrogen
NA
6200
13000
2500
2180
Nitrate and Nitrite
NA
94
110
1.2
ND
For surface disposal facilities the ceiling concentration limits listed in tnis torm are not appncame. Keterence me wuivJuuai Nc11111L JUI uJcLa3
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pen lties for submitting fa e i ormation, including the possibility of fines and impris nment for knowing violations."
R
Signature of Preparer * 0 Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 215.09
Permit #: WQ000672 Cation Exchange Capacity (non 503 only):
Operator: Ozzell Baker Owner: Ozzell Baker Predominant Soil Series: Ra-Rains Sandy
Acres Used: 16.9 Acres Permitted: 16.9 Site #: NC-RO-16 Field #: I
v? emi,,Al Analytic data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or_.....
Com-
posite
Date
3/20/20
Z
6/23/20
3!
9/22/20
4'
11 /30/20
S
E>
7
8;
9�
10_,
12
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
A,nn..al Hoavv Metal Field Landings (Calculated in lbs/acre):
Total__.
DT/Ac./
�*
a�
App.
Event
3.89
8.84
Arsenic
0.000
0.003
0.032
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.035
Cadmium
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.000
2.146
5.940
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.086
Chromium
0.000
1.772
1.909
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.682
Lead
0.000
0.154
0.173
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.327
Mercury
0.000
0.000
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.056
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
denum
Nickel
0.000
0.321
0.329
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.650
Selenium
0.000
0.002
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Zinc
0.000
4.765
7.655
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
12.421
Total
Phos-
0.000
124.384
90.168
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
214.552
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violati s".
�5 2
Signature of Land AppliU D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Cron 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-01
Annual Dry Tons Applied: 97.3403 Site #: I
• Ra-Rains Sandy
Crop 1 Max. PAN: 151 Crop 2 Name:
Acres Utilized: 16.9
Acres Permitted: 16.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Volume applied
Volume
Residual Sources
Soil
Precip.
D
<
o
R.
K
z Y
- B
Nitrate
PAN Applied
pp
Name of Crop Type
`- t
(enter one) Solids/
"�o
Applied per
(NPDES #, WQ#.
Cond.
past 24
K a
X _
m `-+
TKN
o �
o0 o
and
Ibs/acre)
Receiving Residual
0
Solids
Acre
Fert., Animal
(Dry,
Hrs.
T
Fo
: -•
°
o 2
Nitrite
Application
QLiquid
Cu. Yds Gallons
310000
2.1
(Dry Tons/Ac)
Waste, etc)
Wet'
Moist)
inches
7
�
o
o'
/k
�n9 9
49000
m /k
9 9
m /k
9 9
Cra 1
p
Crop 2
P
Crop I
P
Crop 2
P
7/9
1.606
W00000672
Dry
0
S
0.5
0.3
13000
110
55.932
55.932
7/10
440200
2.1
2.281
xA'Q0000672
Dry
0
S
0.5
0.3
49000
13000
110
79.423
79.423
9/22
217000
3.4
1.820
W00000672
Dry
0
S
0.5
0.3
11000
2500
1.2
13.840
13.840
9/25
6200
3.4
0.052
WQ0000672
Dry
0
S
0.5
0.3
11000
2500
1.2
0.395
0.395
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
01
973400
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
I P
149.591
149.591
Lime Applied
Annuallbs/acre
0.035
0.006
8.086
3.682
0.327
0.005
0.118
0.650
0.044
12.421
214.552
Date
Ibs/ac
Prior Years Cumulative lbs/ac
Current Cumulative Ibs/ac
0.035
0.006
8.086
3.682
0.327
0.005
0.118
0.650
0.o44 .
12.421
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
E-1--EFT
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
inform tion, m lading the possib'lity fines and imprisonment for vowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
Signature of L nd Applier
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
35.84
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series: NoA- Norfolk
8.7 Acres Permitted: 8.7 Site #: NC-RO-16 Field #: 5
12ncidlnal Analvcic i)nta (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
._1...
3/20/20
7
6/23/20
3
9/22/20
4„
11 /30/20
_.._
?
8 ;
_91
10
1 ' _!
1.2.
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
A.,.,..ai Hoaww Metal Field I.narlinuc (Calculated in lbs/acre):
Total
D
-
p.
Event
Ey"IMIMMKINt
1 111
1 Itl
t Itl
1 111
1 Ilt
1 111
1 111
1 111
t 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
f
�1
®�
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 1.1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
�
1 111
1� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
1 111
1 11
1 111
1 tll
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
Total
' •
1 111
:1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:1:
•
"I certify, under penalty of law, t was prepare un er my irec ion
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations". iL4 5116-IZI
k�J &4
Signature of Land Appli ate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE .A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-05
.annual Dry Tons Applied: 35.8336 Site #: 5
Crop 1 Max. PAN:
. Ra-Rains Sandy
151 Crop 2 Name:
Acres Utilized: 8.7
Acres Permitted: 8.7
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
o
/o
Solids
2.1
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet,
Moist)
Precip.
past 24
Hrs.
inches
D
K v
C16.
x o
>
<
o
d K
>
m `;
a
N'
>
TKN
mg/kg
49000
Z
z D
o �
oo o
M.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pP
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
7/27
161200
1.623
W00000672
Dry
0
S
0.5
0.3
13000
110
56.498"
.,569
7/28
248000
2.1
2.496
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
HO
86.919
86.919
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TorAts
1 01
409200
Cd
Cu
Cr
Pb
H=
Mo
I Ni
Se
Zn
P
143.417
143.417
Lime Applied
Annuallbs/acre
0.003
0.003
0.000
0.000
2.274
2.274
1.878
1.878
0.163
0.163
0.000
0.000
0.060
0.060
0.340
0.340
0.003
0.003
5.050
5.050
131.808
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
F151
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
I, __V- *Application Method: S - Surface, IN - Injection, INC - Incorporation
•�t�lJ�, Z� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Lan pplier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series
14.8
Acres Permitted: 14.8 Site #:
92.14
NoA- Norfolk
NC-RO-16 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
3/20/20
?
6/23/20
31
9/22/20
4
11 /30/20
�..
Z
8;
9
9
]21
_.
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38 1
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
1 19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Anneal Fivaw NUtal Field i.nadings (Calculated in Ibs/acre):
.
...
a
_
._
8
9-
10 JTotal
12)
•�
DT/Ac./
°
>v
App.
v
Event
6.23
Arsenic
0.151
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.151
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
5.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.068
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.269
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.269
Mercury
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Molyb-
0.097
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.097
denum
Nickel
0.489
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.489
Selenium
0.194
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.194
Zinc
8.480
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
8.480
Total
Phos-
1.170
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.170
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision 1n accuruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing viola ti ns".
k �,s Z
Signature of Land Appl r ate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Cror► I Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-16-06 Acres Utilized: 14.8
Annual Dry Tons Applied: 92.1437 Site #: 6 Acres Permitted: 14.8
. NoA- Norfolk Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 230 Crop 2 Name: Crop 2 Max. PAN:
t
}-
Y o
0 2
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
2.7
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e1
Moist)
Precip.
Past 24
Hrs•
inches
K >
F 'a
= 0•
a c
°
o
d
d K
0
>
K.
" co
g
^'
>
TKN
mg/kg
53000
z 3
='
�o o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
3/21
279000
2.122
WQ0000672
Dry
0
S
0.5
0.3
6200
94
73'I'7
73.157
3/28
390600
2.7
2.971
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
102.420
102.420
3/30
148800
2.7
1.132
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
39.017
39.017
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
o
818400
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
214.595
214.595
Lime A lied
Annual lbs/acre
0.151
0.006 `
5.068
0.000
0.269
0.022
0.097
0.489
0.194
8.480
1.170
Date
lbs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative lbs/ac
0.151
1 0.006
5.068
0.000
0.269
0.022
0.097
0.489
0.194
8.480
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
230
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tnat
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possi tlity f fines and imprisonment for kowing violations."
Ak ,IM n^,(j t'/'!/' / *Application Method: S - Surface, IN - Injection, INC - Incorporation
���/// ` V
Signature of Land Applier
Volatilization Rate. our ace - . , nlec on ncorpora wn - .
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
""C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
The City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
17.5
Owner:
Acres Permitted: 17.5 Site #:
Predominant Soil Series
140.07
NoA-Norfolk
7 Field #: NC-RO-16-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
._!...
3/20/20
_.
6/23/20
3�
9/22/20
4_'
11 /30/20
_�
_�.;
.__s...
9
101
1
12L, ;
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
1 39.3
41.3
1 18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual v Metal Field Loadin s Calculated in Ibs/acre :
1 '
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 •
••.-
� • •
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•':
�
liiii'if8ii8L'®
1 1
1 1 1
1111
1111
1 111
1111
1 111
1111
1111
1111
11
1111
1 � :
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 . •
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
�
1 1.1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
�
1'
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®�
1 111
1 111
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:::
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violatio
Signature of Land ApplieO ate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-110-16-07 Acres Utilized: 17.5
Land Owner: Ozzell Baker Annual Dry Tons Applied: 140.0770 Site #: 7 Acres Permitted: 17.5
Operator: Ozzell Baker Predominant Soil Series: NoA-Norfolk Cation Exchange Capacity (non 503):
Cron 1 Name: Bermuda Cron 1 Max. PAN: 230 Crop 2 Name: Crop 2 Max. PAN:
a� o
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Precip.
past 24
Hrs.
inches
D
3 b
o C)
a _
,o
°
o
N
N
3
w `-°
w
N
TKN
mg/kg
53000
z >
o S
3 E.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
3/20
204600
2.7
1.316
WQ0000672
Dry
0
S
0.5
0.3
6200 1
94
45.372
45.372
3/21
248000
2.7
1.596
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
54.996
54.996
3/27
142600
2.7
0.917
W00000672
Dry
0
S
0.5
0.3
53000
6200
94
31.623
31.623
3/29
148800
2.7
0.957
W00000672
Dry
0
S
0.5
0.3
53000
6200
94
32.997
32.997
3/31
148800
2.7
0.957
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
32.997
32.997
10/6
279000
3.4
2.260
W00000672
Dry
0
S
0.5
0.3
11000
2500
1.2
17.184
17.184
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
-OT--11718001
As
Cd
Cu
Cr
Pb
H
Mo
Nil
Se
Zril
P
215.169
215.169
Lime Applied
Annuallbs/acre
0.140
0.006
4.698
0.000
0.249
0.020
0.090
0.453
0.179
7.889
2.933
Date
Ibs/ac
Prior Years Cumulative lbs/ac
2.26
Current Cumulative Ibs/ac
2.400
0.006
4.698
0.000
0.249
0.020
0.090
0.453
0.179
7.888
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
F 230
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibilift of fines and imprisonment for knowi g violations."
*Application Method: S - Surface, 1N - Injection, INC - Incorporation
/ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature kand Applier Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator:
Acres Used:
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 5 Site #: 16 Field #:
24.47
WaB-Wagram
NC-RO-16-16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
3/20/20
6/23/20
3
9/22/20
4
1 1 /30/20
5
6 I
7_I
8!
9
10..i
2
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
1 2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings Calculated in lbs/acre):
Total
D
-
• •.
Event
1.
1 1•:
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 t
MRIMI
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
• . -
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
My, :
1 111
1 111
t l
®
1 1
11
1 111
11
111
1 11
My 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
� �
11��
11 1
1111
1111
1 111
1111
1111
1111
1 111
1111
1 111
1111
1 1
�
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1'
1 1::
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
®
�
1111
1111
1111
1111
1 111
1 111
1 111
1111
1111
1111
• :�
' •
1
.• 1 •
1 111
1 111
1 111
1 111
1 111
1 Itl
1 111
1 111
1 111
1 111
••
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A�j Oj�' �L4 1'5 /� I -
Signature of Land Applieo I D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
WQ Permit #: W00000672
.annual Dry Tons Applied: 24.4320
Field #: NC-110-16-16
Site #: 16
Predominant Soil Series: WaB-Wagram
Crop I Max. PAN: 192 Crop 2 Name:
Acres Utilized: 5
Acres Permitted: 5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
`' r:
0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
a
K "a
'n
o m
a
o
N'
o
o'
K.
c°,
?3 a
w
* N
o'
o
TKN
mg/kg
49000
z D
q' S
o B
w o
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop _
Crop 1
Crop 2
4/27
161200
2.1
2.823
WO0000672
Dry
0
S
0.5
0.3
13000
110
1 98.306
98.306
7/16
117800
2.1
2.063
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
71.839
71.839
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o
0
0.000
Residuals .Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
o
279000
As
Cd
Cu
Cr
Pb
H 7
Mo
Ni
Se
Zn
P
170.145
170.145
Lime Applied
Annuallbs/acre
0.070
0.003
3.442
0.941
0.204
0.010
0.074
0.393
0.090
6.384
66.548
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative Ibs/ac
0.070
0.003
3.442
0.941
0.204
0.010
0.074
0.393
0.090
6.384
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility f fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Z**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of 4nd Applier Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
45.56
Operator: Ozzell Baker Owner: James Campen Predominant Soil Series: WaB-Wagram
Acres Used: 6 Acres Permitted: 6 Site #: 17 Field #: NC-RO-16-17
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
.. �..
3/20/20
Z
6/23/20
3�
9/22/20
-
11 /30/20
r
..
?.
8...;
9_
�_!
...
% Solids 1
2.7
2.1 1
3.4
2.78
Arsenic 1
12.1
0.38
1.82
0.118
Cadmiuml
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
1 41.3
18.6
0.297
Selenium
15.6
1 0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavv Metal Field LoadinEs (Calculated in Ibs/acre):
1 111
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
••�-
1 111
� •
1 1 1
�
1 111
1 111
1 11
�
1 111
1 111
1 111
1 111
•:
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
-.'
1111
11•
1111
111
1 111
1111
1111
1111
1 111
1111
1 111
1111
1 1•:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�-
1 111
1 1
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 i
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
••
1 111
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 ill
1 111
Tota
•
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•'
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
14-J1,10 esjik, 4A 3 ,5 Z 1
Signature of Land Ap r I D e
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPN' OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop I Name: Bermuda
NN'Q Permit #: NVQ0000672 Field #: NC-RO-16-17 Acres Utilized: 6
.Annual Dry Tons Applied: 45.5651 Site #: 17 Acres Permitted: 6.0
Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN:
`
°
°
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Sod
Cond.
(Dry'
Wet,
Moist)
Precip.
past 24
Hrs.
inches
D
o R
n_.
'
o
w �_
3
; '
o
TKN
mg/kg
49000
z
o 3
w.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied ( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/25
167400
2.1
2.443
W00000672
Dry
0
S
0.5
0.3
13000
110
85.072
85.072
12/29
124000
2 78
2.396
W00000672
Dry
0
S
0.5
0.3
14200
2180
0
22.501
22501
12/30
142600
2.78
2.755
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
25.877
25.877
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
01
4340001
As
Cd
Cu
Cr
Pb
lie
Mo
Ni
Se
In
P
133.450
133.450
Lime Applied
Annuallbs/acre
0.003
0.000
1.398
1.114
0.098
0.000
0.035
0.205
0.002
3.142
82.399
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative Ibs/ac
0.003
0.000
1.398
1.114
0.098
0.000
0.035
0.205
0.002
3.142
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
192
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly
gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment
for knowing viol ions." -�Lj )
3� �51 �1
j
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature dt'Land Applier Date ***
Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator:
Acres Used:
Ozzell Baker
Owner: James Campen Predominant Soil Series:
12.3 Acres Permitted: 12.3 Site #: 18 Field #:
112.03
WaB-Wagram
NC-RO-16-18
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
.._1...
3/20/20
?
6/23/20
_3....i
9/22/20
4....
1 I /30/20
5 ''
_�..'
7
8 '
9 ;
�_...;
11....1
Z
% Solids
2.7
1 2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
..
Event
.1
•
1 111
KIT,
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 ill
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•�•-
1111
�
'•
11�
1 111
1111
1 111
1111
1111
1111
1 111
1111
1 111
�
1 � 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
::
1 111
1 1
1 1 .
1 11
1 111
1 111
1 11
MET, M1
1 111
1 111
1 111
1 111
1
®
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
®
1 111
�
1 1••
1 11
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1
1 111
1 11
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1 1 1
®
1111
�
•1•
�
1111
1111
1111
1111
1 111
1111
1 111
1111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/g]&j ojA' 4W4 /6 Z
Signature of Land Applier D e
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop I Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-110-16-18
.annual Dry Tons Applied: 111.9737 Site #: 18
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Utilized: 12.3
Acres Permitted: 12.3
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
°' c
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #. WQ#.
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
a
K v
n '
oa o
* o
°
o
w °=
F _
K
w -,
g
�'
* a
n
TKN
mg/kg
49000
z Y
;' 3
o 3
w �•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/22
167400
2.1 1
1.192
W00000672
Dry
0
S
0.5
0.3 1
13000
110
41.499
41.499
4/28
192200
2.1
1.368
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
47.647
47.647
4/29
6200
2.1
0.044
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
1.537
1.537
7/15
260400
2.1
1.854
Vv00000672
Dry
0
S
0.5
0.3
49000
13000
110
64.554
64.554
10/7
403000
3.4
4.645
WQ0000672
Dry
0
S
0.5
0.3
11000
2500
1.2
35.316
35.316
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
U
0
0.000
Residuals .Applications totals on FORM FSF supp ( attach FORA FSF supp to this form):
0.000
0.000
TOTALS
u
lo-,),()(11
As
Cd
Cu
Cr
Pb
H =
Mo
Ni
Se
Zn
I P
190.551
190.551
LimeApplied
Annuallbs/acre
0.010
0.002
2.72t
1.588
0.141
0.001
0.051
0.287
0.010
4.931
106.052
Date
Ibs/ac
Prior Years Cumulative lbs/ac
Current Cumulative Ibs/ac
0.010
0.002
2.728
1.588
0.141
0.001
0.051
0.287
0.010
4.931
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, incl ility of to ding the possibes and imprisonment for knowin violations."
G&4
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of La d Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual): 8.90
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: James Campen Predominant Soil Series: WaB-Wagram
1.6 Acres Permitted: 1.6 Site #: 19 Field #: NC-RO-16-19
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kE, % Solids use Raw Percent ft
Sample or_4...J
Com-
posite
Date
3/20/20
6/23/20
9/22/20
11 /30/20
_L
6...!
�.;
8;
9
10
11
12
Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
Molyb-
denum
7.81
7.24
3.5
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
•
• pp
Event
1 111
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
re
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•�•-
1 111
••
1 111
1 111
1111
1 111
1 111
1111
1111
1111
1111
1111
•'
1 111
®
1 111
ffor, 1
1 111
1 111
1 111
111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
�
t 1
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1 111
1 ��:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
111
1 ��:
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
• •�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •�
Total
Phos-
__phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/d.- I D 0-t'- 4A 1 Sh I
gig a ure of Lan YXpp r t D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-110-16-19
Annual Dry Tons Applied: 8.6869 Site #: 19
Acres Utilized: 1.6
Acres Permitted: 1.6
Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503):
Crop I Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN:
o
N C
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
( ry'
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
q �
s �•
o K
n
m
_
_
N'
* K.
=
g
n,'
* v
TKN
mg/kg
49000
? >
o B
W o
d
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
4/29
99200
2.1
5.429
WQ0000672
Dry
0
S
0.5
0.3
13000
110
189.050
189.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0,000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
o
99200
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
189.050
189.050
Lime Applied
Annuallbs/acre
0.004
0.004
0.001
0.001
2.992
2.992
2.472
2.472
0.215
0.215
0.000
0.000
0.078
0.078
0.448
0.448
0.003
0.003
6.645 173.440
6.645
Date
Ibs/ac
Prior Years Cumulative lbs/ac
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the pols'sibili of fines and imprisonment for king violations."
�� - ouv
-1 I & *Application Method: S - Surface, 1N - Injection, INC - Incorporation
// - l-"�J CC'� wwtt�� �17-,-j **Volatilization Rate: Surface - 0.5, Injection/Incorporation 1.0
Signature o`PLand Applier
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series:
Acres Used: 28 Acres Permitted: 28 Site #: 13 Field #:
76.02
Lu-Lumbee
NC-RO-17-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
._1_
3/20/20
2 1
6/23/20
3._1
9/22/20
4...
1 1 /30/20
5
6_i
?
8 I
_�._`
0..1
11
12
% Solids
1 2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
1 41.3
18.6
0.297
Selenium
15.6
1 0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavv Metal Field Loadings (Calculated in Ibs/acre):
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Ili
�
1111
1111
1 111
1111
1111
1111
1111
1 111
1 1
�•
�••
Piiii•8f8Sii'
1 111
�
1 111
111
1 111
1 11
11
�
11
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 1 `
1 111
1111
1111
1 111
1 111
1 111
1111
1 111
1111
1111
11 •
�_�
1 111
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
'`
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
' .
1 111
: • ::1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
: • ::1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accor ance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier 0 ate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-110-17-03 Acres Utilized: 28
Land Owner: City of Lumberton Annual Dry Tons Applied: 76.0108 Site #: 3 Acres Permitted: 28
Operator: Delois Allen Predominant Soil Series: Lu-Lumbee Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop 1 Max. PAN: 137 Crop 2 Name: Crop 2 Max. PAN:
Y
�? p
0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDFS #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
D
C v
c,'
n o
°
o
°=
c^o -
N
;
K
v g
°
^'
TKN
mg/kg
49000
z
o 3
uo o
3
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/14
192200
2.1 1
0.601
WQ0000672
Dry
0
S
0.5
0.3 1
13000 1
110
20.930
20.930
5/15
192200
2.1
0.601
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
20.930
20.930
5/16
148800
2.1
0.465
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
16.204
16.204
5/18
334800
2.1
1.047
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
36.460
36.460
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
1
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
0
8680001
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
I Se
7.n
P
94.525
94.525
Lime Applied
Annuallbs/acre
0.002
0.000
1.499
1.238
0.108
0.000
0.039
0.224
0.002
3.329
86.880
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative Ibs/ac
0.002
0.000
1.499
1.238
0.108
0.000
0.039
0.224
0,002
3.329
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
137
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility fines and imprisonment for kn wing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of L d Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 102.91
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald Hammonds Owner:
Acres Used: 24.9 Acres Permitted:
Ronald Hammonds
24.9 Site #:
Predominant Soil Series:
8 Field #:
WkB-Wakulla
NC-RO-20-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
..? .
3/20/20
?.i
6/23/20
�._'
9/22/20
4
1 1 /30/20
6
L.1.1
8 i
9
10
1 1
1 2
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
1 39.3
41.3 1
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
:
1_'
8
9
10 ;
1 1 s
1
DT/Ac./
_Jj3
_2j
_6
o
App.
Event
3.99
0.14
Arsenic
0.000
0.003
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.000
2.202
0.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.299
Chromium
0.000
1.819
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.850
Lead
0.000
0.158
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.161
Mercury
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.058
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
denum
Nickel
0.000
0.330
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.335
Selenium
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Zinc
0.000
4.892
0.124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.016
Total
Phos-
0.000
127.680
1.459
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
129.139
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing tviolations".
11q1j,0j Pj, k,
Signature of Land Appi D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-03 Acres Utilized: 24.9
Land Owner: Ronald Hammonds Annual Dry Tons Applied: 102.9210 Site #: 3 Acres Permitted: 24.9
Operator: Ronalld Hammonds Predominant Soil Series: Wkb-Wakulla Cation Exchange Capacity (non 503):
Crop 1 Name: Bermuda Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN:
as o
Volume applied
PP
(enter one) Solids/
Liquid
Cu. Yds G8110nS
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
Dr
( Y'
Wet,
Moist)
Precip.
past 24
Hrs.
inches
D
a
g
o �
n.
,� 0
o
C -
N'
v
�
m `-;
� „
* -
0
TKN
mg/kg
49000
z
4
o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Ibs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/10
564200
2.1
1.984
W00000672
Dry
0
S
0.5
0.3
13000
110
69.090
69.090
4/15
266600
2.1
0.938
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
32.647
32.647
4/16
303800
2.1
1.068
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
37.203
37.203
7/17
40700
2.1
0.143
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
4.984
4.984
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS
n
117,5300
As
Cd
Cu
Cr
Pb
H r
Mo
Ni
Se
Z.n
P
1-4�.92
143.924
Lime A lied
Annual lbs,acrc
0.004
0.001
2.299
1.850
0.161
0.000
0.059
0.335
0.003
5.016
129.139
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.004
0.001
2.299
1.850
0.161
0.000
0.059
0.335
0.003
5.016
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of Ines and imprisonment for knowing violations."
OUA,6,;hl
*Application Method: S - Surface, IN - Injection, INC - Incorporation
l�1.t� Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Ll Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual)
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Charles Brown
31.2 Acres Permitted: 31.2 Site #:
192.50
Predominant Soil Series: WkB-Wakulla
4 Field #: NC-RO-20-4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/ktr, % Solids use Raw Percent 4):
Sample or
Com-
posite
Date
_?_
3/20/20
_'_.1
6/23/20
3_;
9/22/20
4
11 /30/20
�.
6„
7
8 V
_..
v'9
10
1'
2 /
% Solids
2.7
2.1
1 3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
1 111
1 11
1 11:
1 111
1 111
1 111
1 111
1 111
1 Ilt
t 111
1 111
1 111
1 1
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•..-
1111
��
1 11•
1111
1111
1111
1111
1 111
1111
1 111
1111
1 111
®
1 �•�
1 111
1 111
1 111
1 111
1 Ilt
®
11
1 111
1 111
1 111
1 •
1 1�
1 111
1111
1 111
1111
1111
1 11
1 Ilt
1111
1 1
1 •
®
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
� _� �
1 111M1
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 :
1 111
�
1 1:
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 111
:�
•:
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
1111
• •
1 :•
1 111
1111
1111
1111
1 111
1111
1111
1 111
.••
A certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing A��j &4 violati s".
3/,521
Signature of Land Appli Da
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Charles Brown
Operator: Ronald Hammond
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-04
Annual Dry Tons Applied: 192.5310 Site #: 4
Acres Utilized: 31.2
Acres Permitted: 31.2
Predominant Soil Series: WkB-Wakulla Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 192 Crop 2 Name:
Crop 2 Max. PAN:
o Y
V c
0
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
( ry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>
N
s �•
n w
o
°
o
X w
_
_
m
�; w
TKN
mg/kg
49000
z >
;'
o B
ao o
R.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
5/4
266600
2.1
0.748
WQ0000672
Dry
0
S
0.5
0.3
13000
110
26 055
'A 055'
5/8
297600
2.1
0.835
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
29.085
29.085
5111
241800
2.1
0.679
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
23.631
23.631
5/12
235600
2.1
0.661
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
23.025
23.025
7/18
229400
2.1
0.644
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
22.419
22.419
7/20
173600
2.1
0.487
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
16.966
16.966
7/22
186000
2.1
0.522
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
18.178
18.178
7/23
186000
2.1
1 0.522
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
18.178
18.178
7/17
40700
2.1
0.114
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
3.978
3.978
10/5
210800
3.4
0.958
WQ0000672
Dry
0
S
0.5
0.3
11000
2500
1.2
7.283
7.283
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS1
01
2068100
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
7,n
P
188.797
188.797
Lime Applied
Annuallbsiacre
0.011
0.002
3.161
1.827
0.161
0.001
0.058
0.327
0.012
5.593
117.669
Date
I Ibs/ac
Prior Years Cumulative lbs/ac
1
Current Cumulative lbs/ac
0.011
0.002
3.161
1.827
0.161
0.001
0.058
0.327
0.012
5.593
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of lKnes and imprisonment for 7,6
owi g violations."
n(j *Application Method: S - Surface, IN - Injection, INC - Incorporation
ZI **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of LanV Applier
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton
WQ0000672
Ronald G. Hammonds
Total Dry Tons Applied (Annual)
Cation Exchange Capacity (non 503 only):
Owner: Taylco, INC Predominant Soil Series:
6.7 Acres Permitted: 6.7 Site #:
Field #:
31.42
GoA-Goldsboro
NC-RO-20-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
3/20/20
2
6/23/20
3
9/22/20
4 i
11 /30/20
§_
6,
7._
S j
9 i
10
11
12
% Solids 1
2.7
2.1
1 3.4
1 2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
17000
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
F-Tota-1
• ••
00000000000
••
1 111
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•. -
1 111
:•
1111
1111
1111
�
1 11
1111
11 1
1111
11 1
111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 1•:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•:
•_
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
'
111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®.
Total
Phos-
1 11
1 1:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:1
• .
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
SL
Signature of Land Appla D e DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-06 Acres Utilized: 6.7
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 31.4201 Site #: 7 Acres Permitted: 6.7
Operator: Ronald G. Hammonds Predominant Soil Series: NoA-Norfolk Cation Exchange Capacity (non 503):
Crop I Name: Soybeans Crop I Max. PAN: 164 Crop 2 Name: Crop 2 Max. PAN:
p t
0 c
Q
Volume applied
PP
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Sod
Cond.
( ry
Wet
Moist)
Preci P
,
Past 24
Hrs.
inches
D
� i?
0
M °
<
o
A
� =
CD
0
o
K.
w
5
I KN
mg/kg
z D
4
8 =
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
P P
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
7/13
18600
2.1
0.243
W00000672
Dry
0 1
S
0.5 1
0.3
49000
13000
110
8.465
8.465
7/17
340200
2.1
4.446
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
154.826
154.826
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lo
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS
358800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
163.291
163.291
Lime Applied
Annuallbs/acre
0.004
0.001
2.589
2.139
0.186
0.000
0.068
0.387
0.003
5.750
150.0801
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
3/17
8.17 ton
Current Cumulative lbs/ac
0.004
0.001
2.589,
2.139
0.186
0.000
0.068
0.387
0.003
5.750
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
164
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility qA fines and imprisonment for knowin 'violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1 ♦ o, .A, / 7 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Lhnd Applier
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
65.70
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GOA-Goldsboro
Acres Used: 13 Acres Permitted: 13 Site #: 7 Field #: NC-RO-20-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/20/20
2
6/23/20
3
9/22/20
4
11/30/20
r
6
7
$._`
9._
14_I
1.....'
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
1 41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
17000
16000
5100
410
Annual Heavv Metal Field Loadings (Calculated in Ibs/acre):
Total
App.
Event
1 111
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
.�
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�I
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�II
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 I',
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
VIM
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
0
ff#Tlfo1
ff,11711
ffirlyl1
1 111
1 111
1 111
MT, M,
®
1 111
• ••
1 111
1 111
1111
1 Itl
1 111
1 111
1111
1111
1111
1111
. `•
' •
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-07 Acres Utilized: 13
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 65.6950 Site #: 7 Acres Permitted: 13
Operator: Ronald G. Hammonds Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop I Max. PAN: 176 Crop 2 Name: Crop 2 Max. PAN:
o
� ❑
°
C�
Volume applied
pp
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
p
Acre
D Tons/Ac
(Dry )
Residual Sources
NPDES #, W #
( Q
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
D
K S
o
cL
.o
°
C
°
� Ri
„ _
« N'
�_
°
o
e
r',
w
-
* "'
o
°
TKN
mg/kg
Z D
0 c
°
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/13
328600
2.1
1 2.214
R'Q0000672
Dry
0
1 S
0.5
0.3
1 49000
13000
1 110
77.074
77.074
7/14
421600
2.1
2.840
V1'Q0000672
Dry
0
S
0.5
0.3
49000
13000
110
98.887
98.887
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
U
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):F175.9621
00
0.000
TOTALS
o
7•0200
As
Cd
Cu
Cr
Pb
Ile
Mo
Ni
Se
Z.n
P
175.962
Lime Applied
Annuallbs/acre
0.004
0.004
0.001
0.001
2.790
2.790
2.305
2.305
0.200
0.200
0.000
0.000
0.073
0.073
0.417
0.417
0.003
0.003
6.196
6.196
161.729
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit l st/2nd Crop
176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility, of fines and imprisonment for knowing violations."
A4_11twi D 0 4J / Z *Application Method: S - Surface, IN - Injection, INC - Incorporation
1J, i -**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature o and Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual): 296.09
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series: GOA-Goldsboro
73.2 Acres Permitted: 73.2 Site #: 8 Field #: NC-RO-20-08
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
-1
3/20/20
_? 1
6/23/20
_3..
9/22/20
Lij
11 /30/20
L_�j...
?
8
Lai
10 j11
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
App.
Event
'
1
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•��•
'•
1 •1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
11
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
� •''
�
1 1
1 111
1 111
111
1 11
1 111
®
1 111
1 111
1 111
��
®�
1 11
1 11 t
1 1 1
1 1 1
1 111
1 111
1 111
11
1 11
1 111
1 1 1
�
�_•
11�.
1 1 •
1111
1111
1111
1111
1111
1111
1111
1111
1111
1 111
11•
��
1 1'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1®
1 1'
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
®
1 �
. •
111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
.1
Total
' .
M
.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
.'1
. •
"t certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier D to
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ronald Hammonds
Operator: Ronald Hammonds
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-08
Annual Dry Tons Applied: 296.0542 Site #: 8
Predominant Soil Series: GoA-Goldsboro
Crop I Name. Corn Crop 1 Max. PAN: 147 Crop 2 Name:
Acres Utilized: 73.2
Acres Permitted: 73.2
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
«0 o
c�
Ca
Volume applied
PP
(enter one Solids/
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
(Dry,
Wet,
Moist
Precip.
Past 24
Hrs.
inches
a
3 'a
d
5 °:
* e
°
o
� R
� =
fD N'
* Q
0
* -
e
o
TKN
mg/kg
1 53000
z Y
2
a°o c
0 �
rng/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
PP
(Ibs/acre)
Name of CropT
Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
1/9
241800
2.7
0.372
VVQ0000672
Dry
1 0
S
1 0.5
0.3
6200
94
12.819
12.819
1/10
210800
2.7
0.324
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
11.176
11.176
1/11
99200
2.7
0.153
N'00000672
Dry
0
S
0.5
0.3
53000
6200
94
5.259
5.259
1/23
173600
2.7
0.267
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
9.204
9.204
1/24
179800
2.7
0.277
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
9.532
9.532
3/13
272800
2.7
0.420
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
14.463
14.463
3/14
396800
1.7
0.610
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
21.037
21.037
3/30
62000
2.7
0.095
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
3.287
3.287
3/31
279000
2.7
0.429
WQ0000672
Dry
0
S
0.5
0.3
53000
6200
94
14.791
14.791
4/2
248000
2.1
0.297
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
10.331
10.331
4/3
223200
2.1
0.267
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
9.298
9.298
4/4
211000
2.1
0.260
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
9.039
9.039
0
229400
0.274
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
9.556
9.556
TOTALS.
a
2833400
As
Cd
Cu
Cr
Pb
H 7
Mo
Ni
Se
Zn
P
139.791
139.791
Lime Applied
Annuallbs/acre
0.072
0.072
0.003
0.003
3.005
3.005
0.501
0.501
0.171
0.171
0.010
0.010
0.062
0.062
0.322
0.322
0.093
0.093
5.360
5.360
35.690
Date
I Ibs/ac
Prior Years Cumulative Ibs/ac
3/17
95.16 to
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility f fines and imprisonment for kn wi g violations."
0,1 _(I / *Application Method: S - Surface, IN - Injection, INC - Incorporation
J 7 7i 1 I **Volatilization Rate: Surface - 0 5 Injection/Incor oration - 1 0
Signature of Uind Applier
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-20-08 Acres Utilized: 73.2
Land Owner: Ronald Hammonds Annual Dry Tons Applied: 296.054154 Site #: Acres Permitted: 73.2
Operator: Ronald Hammonds Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Name: Corn Crop 1 Max. PAN: 147.00 Crop 2 Name: Crop 2 Max PAN:
o
O
Volume applied (enter
one)
Cu. Yds Gallons
229400
o
/o
Solids
2.1
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet'
Moist)
Dry
Precip.
past 24
Hrs.
inches
D
a �
o
70 °
_
* N
o'
0.5
°
,
;u w
N•
o
TKN
mg/kg
49000
z a
El
o 3
na o
n R
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/6
0.274
WQ0000672
0
S
0.3
13000
110
9.556
9.556
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
229400
, �� <
0.274
9.5561
9.556
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for k owi g violations."
�� *Application Method: S - Surface, IN - Injection, INC - Incorporation
3 **Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Signature of Uand Applier ate ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 40.95
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GOA-Goldsboro
Acres Used: 10.6 Acres Permitted: 10.6 Site #: 14 Field #: NC-RO-20-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1_
3/20/20
2
6/23/20
3;
9/22/20
4J
11/30/20
6
_7 1
8._
9
10
1
12 ;
% Solids
1 2.7
2.1
1 3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
228
108
ND
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
17000
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
I
2
4J
11_
1 ?
_3
__5j
.,
DT/Ac./
App.
r
Event
0.33
3.53
Arsenic
0.008
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.268
1.951
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.219
Chromium
0.150
1.612
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.762
Lead
0.014
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.154
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.005
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
denum
Nickel
0.026
0.292
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.318
Selenium
0.010
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Zinc
0.448
4.333
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.781
Total
Phos-
11.186
113.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
124.274
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
16 /-Z
Signature of Land Ap 'er ate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Taylco, Inc
Operator: Ronald G. Hammonds
PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-14
Annual Dry Tons Applied: 40.9527 Site #: 14
Acres Utilized: 10.6
Acres Permitted: 10.6
Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Name: Corn Crop I Max. PAN: 147 Crop 2 Name:
Crop 2 Max. PAN:
c
0
Q
Volume applied
(enter one) Solids/
Li Liquid
9
Cu. Yds Gallons
%
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry',
het
Moist)
Precip.
Past 24
Hrs.
Inches
D
K
s
oa
d
_
ec -
r4
o'
X =
w
F R
r4
TKN
mg/kg
z a
q B
o R
°°
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of CropType
yP
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
1/8
31000
2.7
0.329
WQ0000672
Dry
1 0
S
1 0.5
0.3
530001
6200
94
1 11.349
11.349
4/7
217000
2.1
1.793
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
62.422
62.422
4/17
210800
2.1
1.741
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
60.639
60.639
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORA FSF supp to this form):
0.000
0.000
TOTALS
01
458800
As
Cd
Cu
Cr
Pb
H J
Mo
Ni
Se
7,n
P
134.410
134.410
Lime Applied
Annuallbs/acre
0.011
0.0I 1
0.001
0.001
2.219
2.219
1.762
1.762
0.154
0.154
0.001
0.001
0.056
0.056
0.318
0.318
0.012
0.012
4.781
4.781
124.2741
Date
Ibs/ac
Prior Years Cumulative lbs/ac
3/17
14.84 to
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
infor ation, ' eluding the 4 poss'bili of fines and imprisonment for kn9wind violations."
2 C *Application Method: S - Surface, IN - Injection, INC - Incorporation
,J 1 �/ **Volatilization Rate: Surface - 0 5 Injection/Incor oration - 1 0
Signature oftand Applier
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series:
36.1 Acres Permitted: 36.1 Site #: NC-RO-21 Field #:
27.33
NoA-Norfolk
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1...
3/20/20
�j
6/23/20
3]
9/22/20
L4j
1 1 /30/20
71
8
7 ,.
10
11 1
1.2
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
App.
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111 ''
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•� -
1 11
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 11
1 111
1 11
�
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 11 t
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1111
1111
1111
®
1111
1 111
1 111
1 111
1111
1 Ilt
1111
1111
�-�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
IV, ml
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
Total
'•
1 111
1 111
1 111
1.
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1.
. •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
' - �� 1
S n e o and ppli Da
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-21-1 Acres Utilized: 36.1
Land Owner: Fannie Oxendine Annual Dry Tons Applied: 27.3265 Site #: I Acres Permitted: 36.1
Operator: Lacy Cummings Predominant Soil Series: NoA- Norfolk Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop 1 Max. PAN: 164 Crop 2 Name: Crop 2 Max. PAN:
_
in
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet,
Moist
Preci P•
past 24
Hrs.
inches
D
Er o'
o W
n o•
°
o
%° _
�, -
* N'
coo
0
3
,�
io E.
+� -
o
TKN
/k
m9 9
14200
z a
o 3
= O
CD o
�•
m /k
9 9
2180
Nitrate
and
Nitrite
m /k
9 9
0
PAN Applied
( Ibs/acre)
Name of CropType
YP
ReceivingResidual
Application
Crop 1
p
Crop 2
P
Crop 1
P
Crop 2
P
12/2
124
2.78
0.000
WQ0000672
Dry
0
S
0.5
0.3
0.004
0.004
12/3
117800
2.78
0.378
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
3.553
3.553
12/4
117800
2.78
0.378
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
3.553
3.553
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
'roTALS
o
235724
As
Cd
Cu
Cr
Pb
H =
Mo
Ni
Se
Zn P
7.109
7.109
Lime Applied
Annual lbs,acre
0.000
0.000
0.000
0.000
0.007
0.007
0.000
0.000
0.000
0.000
#######
#######
#######
#######
0.000
0.000
#######
#######
0.022 0.621
0.022
Date
Ibs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
164
.1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false
information, including the possibi'litylqf fines and imprisonment fork owing violations."
/ - f *Application Method: S - Surface, IN - Injection, INC - Incorporation
�.7 **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
Signature of flind Applier Dat *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 48.00
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series: NoA-Norfolk
Acres Used: 38.4 Acres Permitted: 38.4 Site #: NC-RO-21 Field #: 2A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids use Raw Perepnr #il-
Sample or
Com-
posite
Date
,_?_..
3/20/20
2
6/23/20
3
9/22/20
4 !
1 1 /30/20
5
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
horus
94
16000
5100
410
Hnnuat rteavy ivietat meta Loadings Ualculated in lbs/acre :
•
1 •
1-
1 11�
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•�'
�
1 111
1 111
1 111
1 11
1 1
111
1 111
1 111
1 111
1 111
1 111
1 111
•.••
�
1 ••
1 111
1111
1111
1 111
1 111
1111
1111
1 111
1111
1111
1 111
1 � •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 . -
1 11
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
�•
1 11
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
oily
1 1
1 1.1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
RUM
1 11
1 11
1 111
1 111
1 111
i 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 •
®�®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1
1 111
1 111
1 111
1 11!
1 11!
1 111
1 111
1 111
1 ill
1 1 1
. -
1 certify, unuer penalty of taw, tnat tnts document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
LL �L4 5
v
Signature of Land Applier 0 1 Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-21-2A Acres Utilized: 38.4
Land Owner: Fannie Oxendine Annual Dry Tons .Applied: 47.9695 Site #: 2A Acres Permitted: 38.4
Operator: Lacy Cummings Predominant Soil Series: NoA- Norfolk Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Cron 1 Max. PAN: 164 Cron 2 Name: 9-- I OA TV.
L
c
O
i
Volume applied
PP •
enter one Solids/
( )
Li Liquid
9
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES k WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
(D
Wet,
Moist)
Preci p'
Past 24
Hrs.
inches
D
K •a
?
so.
o �
o.
*
�
o
°1
_
*
*
g
�
`;
w
-•
* iv
TKN
mg/kg
14000
z D
o� c
CD o
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
2/4
18600
2.7
1 0.055
WQ0000672
Dry
0
S
0.5
0.3
6200
1 94
0.604
0.604
2/27
6200
2.7
0.018
W00000672
Dry
0
S
0.5
0.3
14000
6200
94
0.201
0.201
2/28
31000
2.7
0.091
W00000672
Dry
0
S
0.5
0.3
14000
6200
94
1.006
1.006
12/9
124000
2.78
0.374
W00000672
Dry
0
S
0.5
0.3
14200
2180
0
3.516
3.516
12/10
117800
2.78
0.356
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
3.340
3.340
12/11
117800
2.78
0.356
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
3.340
3.340
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS
Annuallbs/acre
OF-4 1 S400
As
0.005
0.005
Cd
0.000
0.000
Cu
0.733
0.733
Cr
0.495
0.495
Pb
0.050
0.050
H =
0.001
0.001
Mo
0.018
0.018
Ni
0.103
0.103
Se
0.006
0.006
Zn
1.555
1.555
P 12.007 12.007
34.783
Lime A lied
Date Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
«.
164
• ". •. , ..... ' t,c. a t.Y Uaw, LnaL uus uucument was preparea unaer my mrectilon or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the posZu
fines and imprisonment for owin violations."
k1i LL ` *Application Method: S - Surface, IN - Injection, INC - Incorporation
3 Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of and Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual): 122.16
WQ0000672 Cation Exchange Capacity (non 503 only):
Carnell Locklear Owner: Robert Baskersville Predominant Soil Series: GoA
56.9 Acres Permitted: 56.9 Site #: 2 Field #: NC-RO-28-2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/k % Solids use R P t #
Sample or
?..'
3_a
4._
5_
g,
I
aw ercen
).
,_I
_F_
�
8
9
10
1 1 (
12
Com-
posite
Date
3/20/20
6/23/20
9/22/20
11 /30/20
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
94
16000
5100
410
horus
A.. ..1
II..�_w. A.i_._■
re_u
r
�u■■ua. i=cavy IvArUjll 1-1Clu L.UaU1112s It-alcularen In Ins/9Crelt
Total
1
_2j
_ 3_
_ ......
1._
9;
---
10;
_._..
11
2�
DT/Ac./
APP•
0
a,
Event
1.07
1.08
1
Arsenic
0.026
1 0.001
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.869
0.596
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.465
Chromium
0.000
0.492
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.492
Lead
0.046
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.089
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.004
Molyb-
denum
0.017
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Nickel
0.084
0.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.173
Selenium
0.033
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Zinc
1.453
1.324
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.777
Total
Phos-
0.201
34.560
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
34.761
horus
. �..y, u■.u0■ pcualay 0i law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2
Signature of Land ApplietO I E4te
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-28-2 Acres Utilized: 56.9
Land Owner: Robert Baskerville Annual Dry Tons Applied: 122.2636 Site #: 2 Acres Permitted 56.9
Operator: Carnell Locklear Predominant Soil Series: Goldsboro GoA Cation Exchange Capacity (non 503):
Crop 1 Name: Corn
Cron 1 Max. PAN: 147
Crnn 7 Nam -
_
Volume applied
(enter one) Solids/
Li uid
9
Cu. Yds Gallons
31000
%
Solids
2.7
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, W #
Q
Fert., Animal
Waste, etc)
Sod
Cond.
(Dry,
(
Wet,
Moist)
Precip.
past 24
Hrs.
Inches
D
_4 "a
0 "
o
Q.
<
o
A Q
=
„ N
o.
* -•
N
m
TKN
mg/kg
1 53000
z Y
?
V c
a
m
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Ib
( s/acre)
Name of CropTy e
P
Receiving Residual
Application
PP
Crop I
Crop 2
Crop I
Crop 2
3/2
0.061
WQ0000672
Dry
0
S
0.5
0.3
6200
94
1 2.114
2.114
3/3
3/4
3/10
3/11
3/12
105400
18600
68200
55800
43400
136400
80600
192200
241800
2.7
2.7
2.7
2.7
2.7
0.209
0.037
0.135
0.110
0.086
WQ0000672
WQ0000672
WQ0000672
6VQ0000672
WQ0000672
Dry
Dry
Dry
Dry
Dry
0
0
0
0
0
S
S
S
S
S
0.5
0.5
0.5
0.5
0.5
0.3
0.3
0.3
0.3
0.3
53000
53000
53000
53000
53000
6200
6200
6200
6200
1 6200
94
94
94
94
94
7.189
1.269
4.651
3.806
2.960
7.189
1.269
4.651
3.806
2.960
3/16
3/19
9/15
9/16
2.7
2.7
3.4
3.4
0.270
0.159
0.479
0.603
WQ0000672
WQ0000672
WQ0000672
WQ0000672
Dry
Dry
Dry
Dry
0
0
0
0
S
S
S
S
0.5
0.5
0.5
0.5
0.3
0.3
0.3
0.3
53000
53000
11000
11000
6200
6200
2500
2500
94
94
1.2
1.2
9.303
5.497
3.641
4.580
9.303
5.497
3.641
4.580
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF
supp to this form):
0.000
0.000
1s TOTA
Annuallbs/acre
o 973400
As
0.027
0.027
Cd
0.001
0.001
Cu
1.465
1.465
Cr
0.492
0.492
Pb
0.089
0.089
Hg
0.004
0.004
Mo
0.032
0.032
Ni
0.173
0.173
Se
0.034
0.034
Zn
2.777
2.777
P 45.010 45.010
34.761
Lime Applied
Date Ibs/ac
Prior Years Cumulative Ibs/ac
3/ 1719.49
t
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
147
--- --- ✓'------- .--------J -- --- ., -••-+• ..- aw4Yu­naa N. upal Cu uuucr my uirecuun or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonnIVnt for knowing violations."
_o., f r *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature ofVand Applier
o a zaton Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
I
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 393.38
Permit #: WQ0005672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Wab-Wagram
Acres Used: 62.5 Acres Permitted: 62.5 Site #: 6 Field #: NC-RO-39-09
Residual Analvsis Data tlFleaw Mntale anal Tntol Ph-h -..- .. _ ni 11 _u
Sample or
Z
3
I
5
--r-
6`
- -
•••5,••g,
iv vv■.u�
u�c
i�aw re[Cent
it):
_.._1_..'
7
8
9
10
1 1 i
12
Com-
posite
Date
3/20/20
6/23/20
9/22/20
1 1 /30/20
% Solids
2.7
2.1
3.4
2.78
Arsenic
12.1
0.38
1.82
0.118
Cadmium
0.513
0.055
0.325
0.0102
Copper
407
276
336
4.85
Chromium
228
108
Lead
21.6
19.8
9.79
0.169
Mercury
1.75
0.0002
0.261
ND
Molyb-
denum
7.81
7.24
3.5
ND
Nickel
39.3
41.3
18.6
0.297
Selenium
15.6
0.31
2.33
ND
Zinc
681
613
433
14.3
Total
Phos-
94
16000
5100
410
horus
An., -1
tl­A4..t..1
c:..v.a
r
Total
1
?
3
.1 ;
_7_
DT/Ac./
App.
0
iv
Event
0.85
4.07
1.38
y
Arsenic
0.021
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Cadmium
0.001
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000,
0.000
0.002
Copper
0.691
2.244
0.927
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.862
Chromium
0.000
1.854
0.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.152
Lead
0.037
0.161
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.225
Mercury
0.003
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
denum
0.013
0.059
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.082
Nickel
0.067
0.336
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.454
Selenium
0.026
0.003
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Zinc
1.156
4.984
1.195
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
7.335
Total
Phos-
0.160
130.080
14.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
144.316
horus
Ili r..rt;F,
nnrinr .,on..lr....0
1..... ♦l. ,.r
aL.1- _]_
, - c- ✓ - - ••7 ---'-` -••- """.. .. ..aa VA -Pa.- uuur, illy wrectlon or supervision In accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
I.� 2
Signature of Land Applier 1 liate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-09 Acres Utilized: 62.5
Land Owner: Tracy Bullard Annual Dry Tons Applied: 393.3945 Site #: 9 Acres Permitted: 62.5
Operator: Tracy Bullard Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503):
Crop 1 Name: Bermuda Crop 1 Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN:
Volume applied
o •�
Volume
Residual Sources
Soil
Precip.
a
<
o
a� c (enter one) Solids/
o
/o
pp per
Applied r
(NPDES #, WQ#,
Cond.
Past 24K"o
�' E
p
w
TKN
c}a 0 Liquid
Solids
Acre
Ferl., Animal
(Dry,
Hrs.
�'
co
' =
; N'
w
« N•
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc )
Wet
Moist)
inches
M °
* d
3/29 285200
2.7
0.514
WQ0000672
Dry
0
S
0.5
1 0.3
mg/kg
53000
3/30 186000
2.7
0.335
WQ0000672
Dry
0
S
0.5
1 0.3
53000
6/2/2020 12400
2.1
0.017
WQ0000672
Dry
0
S
0.5
0.3
49000
6/3/2020
322400
2.1
0.452
WQ0000672
Dry
0
S
0.5
0.3
49000
6/4/2020
434000
2.1
0.608
WQ0000672
Dry
0
S
0.5
0.3
49000
6/5/2020
105400
2.1
0.148
WQ0000672
Dry
0
S
0.5
0.3
49000
6/8/2020
55800
2.1
0.078
WQ0000672
Dry
0
S
0.5
0.3
49000
6/9/2020 192200 2.1
0.269
WQ0000672 Dry 0 S 0.5 0.3 49000
6/10/2020 260400 2.1
0.365
WQ0000672 Dry 0 S 0.5 0.3 49000
6/11/2020 117800 2.1
0.165
WQ0000672 Dry 0 S 0.5 0.3 49000
6/19/2020 297600 2.1
0.417
WQ0000672 Dry 0 S 0.5 3-1 49000
6/22/2020 173600 2.1
0.243
WQ0000672 D 0 S 0.5 0.3 49000
0 1674000
2.683
Residuals Applications totals on FORM FSF supp ( attach FORM FSF s
TOTALS 0 4116800
As
Cd Cu Cr Pb H MO Ni Se
Annuallbs/acre
0.029
0.002 3.862 2.152 0.225 0.004 0.082 0.454 0.035
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
0.029
0.002
3.862
2.152
0.225
0.004
0.082
0.454
0.035
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify under penalty of law that
thd
4
c
r
mg/kg
upp
Nitrate
and
Nitrite
mg/kg
PAN Applied
lb )
( s/acre
Name of Crop Type
Receiving Residual
Application
Cmp 1
Crop 2
Crop I
Crop 2
6200
94
17.709
17.709
6200
94
+11.549
11.549
13000
110
0.605
0.605
13000
110
15.729
15.729
13000
110
21.174
21.174
13000
110
5.142
5.142
13000
110
2.722
2.722
13000
110
9.377
9.377
13000
110
12.704
12.704
13000
110
5.747
5.747
13000
110
14.519
14.519
13000
110
8.469
8.469
to this
7,n
form):
58.333
58.333
P
183.779
183.779
Lime Applied
7.335
144.316
Date
Ibs/ac
7.335
192
1 , is ocument was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
informafi n, incl din the possibili of nes and imprisonment for lcno in violations."
*Application Method: S - Surface, IN - Injection INC - � Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of and Applier D to
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-39-09 Acres Utilized: 62.5
Land Owner: Tracy Bullard Annual Dry Tons Applied: 393.394464 Site #: 9 Acres Permitted: 62.5
Operator: Tracy Bullard Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503):
Crop 1 Name: Bermuda Crop 1 Max. PAN: 192.00 Crop 2 Name: Crop 2 Max PAN:
o
O
Volume applied (enter
one)
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SO1I
Cond.
(Dry,
Wet
Moist)
Precip.
Past )4
Hrs.
inches
D
K a
T
°n ?:
o
�, -
*
CD
m
h•
CD
o
TKN
mg/kg
1 49000
z Y
o' B
ao
C, 2.
mg/kg
Nitrate
and
Nitrite
mg/kg
Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop l
Crop 2
Crop 1
Crop 2
6/23
186000
2.1
1 0.261
W00000672
Dry
0
S
0.5
0.3
13000
110
9.074
9.074
6/24
179800
2.1
0.252
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
8.772
8.772
6/27
192200
2.1
0.269
W00000672
Dry
0
S
0.5
0.3
49000
13000
110
9.377
9.377
6/28
186000
2.1
0.261
WQ0000672
Dry
0
S
0.5
0.3
49000
13000
110
9.074
9.074
6/30
186000
2.1
0.261
WQ0000672
Dry
0
S
1 0.5
0.3
49000
13000
110
9.074
9.074
11/3
167400
2.78
0.310
W00000672
Dry
0
S
0.5
0.3
14200
2180
0
2.916
2.916
11/4
204600
2.78
0.379
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
3.564
3.564
11/5
111600
2.78
0.207
W00000672
Dry
0
S
0.5
0.3
14200
2180
0
1.944
1.944
11/24
124000
2.78
0.230
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
2.160
2.160
11/25
136400
2.78
0.253
WQ0000672
Dry
0
S
0.5
0.3
14200
2180
0
2.376
2.376
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
1674000
2.683
T,
:.
58.333
58.333
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibilioffi and imprisonment for kn wi g violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
I Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land plier Da ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ENCO Laboratories
9g
Accurate, Timely. Responsive. Iuuovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, April 6, 2020
Hunt Environmental Associates (HU017)
Attn: Jordan Davis
3330 Saddletree Road.
Lumberton, NC 28360
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: City of Lumberton
ENCO Workorder(s): CDO1355
Dear Jordan Davis,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, March 20, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OLdcc-'----�A
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 12

PROJECT NARRATIVE
Client: Hunt Environmental Associates (HU017)
Project: City of Lumberton
Lab ID: CD01355
Overview
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Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
No Comments
Quality Control Remarks
No Comments
Other Comments
Plant Available Nitrogen was calculated to be 160000 mg/Kg.
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Chuck Smith
Project Manager
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: WW-1
Lab ID: CDO1355-02
Sampled: 03/19/20 14:45
Received: 03/20/20 08:12
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC 9056A
WETS-88 Soil
12/13/22
03/31/20
09:56
03/31/20
09:56
Leaching
EPA 350.1
WETS-88 Soil
04/16/20 04/28/20
03/31/20
14:52
04/01/20
14:12
Leaching
EPA 351.2
Same
04/16/20
03/25/20
09:41
03/30/20
13:41
EPA 365.4
Same
04/16/20
03/25/20
09:41
03/25/20
19:28
EPA 6010D
EPA 3050B
09/15/20
03/20/20
09:45
03/24/20
14:26
EPA 7471B
EPA 7471B
04/16/20
03/20/20
09:38
03/23/20
16:49
EPA 9045D
Same
04/03/20 14:32
04/03/20
14:18
04/03/20
15:28
SM 254OG-2011
NO PREP
03/26/20
03/25/20
16:10
03/25/20
16:10
Client ID: WW-1
Lab ID: CDO1355-02RE1
Sampled: 03/19/20 14:45
Received: 03/20/20 08:12
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 9056A
WETS-88 Soil
03/22/20 03/27/20
11:47 03/25/20
11:47
03/26/20
07:20
Leaching
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 12

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SAMPLE DETECTION SUMMARY
Client ID: WW-1
Lab ID:
CD01355-02
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Aluminum - Total
24000
79.7
379
mg/kg dry
EPA 6010D
Ammonia as N
6200
D
170
380
mg/kg dry
EPA 350.1
Cadmium - Total
0.513
3
0.364
1.90
mg/kg dry
EPA 6010D
Calcium - Total
11000
213
949
mg/kg dry
EPA 6010D
Copper - Total
407
7.21
19.0
mg/kg dry
EPA 6010D
Lead - Total
21.6
4.55
19.0
mg/kg dry
EPA 6010D
Magnesium - Total
2170
35.3
949
mg/kg dry
EPA 6010D
Molybdenum - Total
7.81
3
3.79
19.0
mg/kg dry
EPA 6010D
Nickel - Total
39.3
3
13.7
94.9
mg/kg dry
EPA 6010D
Nitrate/Nitrite as N
94
7.8
19
mg/kg dry
CALC 9056A
pH
7.2
1.0
1.0
pH Units
EPA 9045D
Q-01
Phosphorus
17000
D
5500
15000
mg/kg dry
EPA 365.4
Potassium - Total
4220
152
949
mg/kg dry
EPA 6010D
Sodium - Total
18600
228
949
mg/kg dry
EPA 6010D
Temperature for pH (deg. C)
22
pH Units
EPA 9045D
Q-01
Total Kjeldahl Nitrogen
53000
D
6600
7300
mg/kg dry
EPA 351.2
Total Solids
2.7
0.0010
0.0010
% by Weight
SM 2540G-2011
Zinc - Total
681
41.7
94.9
mg/kg dry
EPA 6010D
Client ID: WW-1
Lab ID:
CD01355-02RE1
Anala
Results
Flag
MDL
POL
Units
Method
Notes
Nitrate as N
79
3B
78
380
mg/kg dry
EPA 9056A
3-01, Q-01
Nitrite as N
15
3
3.0
38
mg/kg dry
EPA 9056A
Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 12

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ANALYTICAL RESULTS
Description: WW-1 Lab Sample ID:CD01355-02 Received: 03/20/20 08:12
Matrix: Sludge Sampled:03/19/20 14:45 Work Order: CD01355
Project: City of Lumberton Sampled By:Jordan Davis % Solids: 2.64
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
24000
mg/kg dry
1
79.7
379
OC20013
EPA 6010D
03/24/20 14:26
JDH
Arsenic [7440-38-2]^
12.1
U
mg/kg dry
1
12.1
19.0
OC20013
EPA 6010D
03/24/20 14:26
JDH
Cadmium [7440-43-9]1
0.513
J
mg/kg dry
1
0.364
1.90
OC20013
EPA 6010D
03/24/20 14:26
JDH
Calcium [7440-70-2]1
11000
mg/kg dry
1
213
949
OC20013
EPA 6010D
03/24/20 14:26
JDH
Copper [7440-50-8]^
407
mg/kg dry
1
7.21
19.0
OC20013
EPA 6010D
03/24/20 14:26
JDH
Lead [7439-92-1]^
21.6
mg/kg dry
1
4.55
19.0
OC20013
EPA 6010D
03/24/20 14:26
JDH
Magnesium [7439-95-4]^
2170
mg/kg dry
1
35.3
949
OC20013
EPA 6010D
03/24/20 14:26
JDH
Mercury [7439-97-6]^
1.75
U
mg/kg dry
1
1.75
2.34
OC20012
EPA 7471B
03/23/20 16:49
KAH
Molybdenum [7439-98-7]1
7.81
J
mg/kg dry
1
3.79
19.0
OC20013
EPA 6010D
03/24/20 14:26
JDH
Nickel [7440-02-0]^
39.3
J
mg/kg dry
1
13.7
94.9
OC20013
EPA 6010D
03/24/20 14:26
JDH
Potassium [7440-09-7]^
4220
mg/kg dry
1
152
949
OC20013
EPA 6010D
03/24/20 14:26
JDH
Selenium [7782-49-2]^
15.6
U
mg/kg dry
1
15.6
19.0
OC20013
EPA 6010D
03/24/20 14:26
JDH
Sodium [7440-23-5]^
18600
mg/kg dry
1
228
949
OC20013
EPA 6010D
03/24/20 14:26
JDH
Zinc [7440-66-6]^
681
mg/kg dry
1
41.7
94.9
OC20013
EPA 6010D
03/24/20 14:26
JDH
Classical Chemistry Parameters
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By
Notes
Ammonia as N [7664-41-7]
6200
D
mg/kg dry
10
170
380
OC31030
EPA 350.1
04/O1/20 14:12
JAH
Nitrate as N [14797-55-8]
79
JB
mg/kg dry
1
78
380
OC24029
EPA 9056A
03/26/20 07:20
LJI
J-01,
Q-01
Nitrate/Nitrite as N
94
mg/kg dry
1
7.8
19
OC31014
CALC 9056A
03/31/20 09:56
LJI
Nitrite as N [14797-65-0]
15
J
mg/kg dry
1
3.0
38
OC24029
EPA 9056A
03/26/20 07:20
LJI
Q-01
PH
7.2
pH Units
1
1.0
1.0
OD03030
EPA 9045D
04/03/20 15:28
BDC
Q-01
Phosphorus [7723-14-0]
17000
D
mg/kg dry
50
5500
15000
OC24002
EPA 365.4
03/25/20 19:28
AKF
Temperature for pH (deg. C)
22
pH Units
1
OD03030
EPA 9045D
04/03/20 15:28
BDC
Q-01
Total Kjeldahl Nitrogen
53000
D
mg/kg dry
50
6600
7300
OC24003
EPA 351.2
03/30/20 13:41
JAH
Total Solids
2.7
% by Weight
1
0.0010
0.0010
OC25031
SM 2540G-2011
03/25/20 16:10
BDC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 12

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OC2OO12 - EPA 7471E
Blank (OC20012-BLKI)
Prepared: 03/20/2020 09:38 Analyzed: 03/23/2020 16:34
Spike Source a/oREC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.0418
U
0.0561
mg/kg wet
LCS (OC20012-BSI)
Prepared: 03/20/2020 09:38 Analyzed: 03/23/2020 16:36
Spike Source %REC
RPD
Analvte
Result
FFF`lau
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.582
0.0617
mg/kg wet
0.581 100 80-120
Matrix Spike (OC20012-MSI)
Prepared: 03/20/2020 09:38 Analyzed: 03/23/2020 16:41
Source: CD04603-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.713
0.0676
mg/kg dry
0.657 0.0504 U 108 80-120
Matrix Spike Dup (OC20012-MSDI)
Prepared: 03/20/2020 09:38 Analyzed: 03/23/2020 16:43
Source: CD04603-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.637
0.0676
mg/kg dry
0.636 0.0504 U 100 80-120 11
20
Post Spike (OC20012-PSI)
Prepared: 03/20/2020 09:38 Analyzed: 03/23/2020 16:45
Source: CD04603-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
5.63
0.514
ug/L
5.00 0.0620 111 75-125
Batch OC2OO13 - EPA 3050E
Blank (OC20013-BLKI)
Prepared: 03/20/2020 09:45 Analyzed: 03/24/2020 13:39
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Aluminum
2.10
U
10.0
mg/kg wet
Arsenic
0.320
U
0.500
mg/kg wet
Cadmium
0.00960
U
0.0500
mg/kg wet
Calcium
5.60
U
25.0
mg/kg wet
Copper
0.190
U
0.500
mg/kg wet
Lead
0.120
U
0.500
mg/kg wet
Magnesium
0.930
U
25.0
mg/kg wet
Molybdenum
0.100
U
0.500
mg/kg wet
Nickel
0.360
U
2.50
mg/kg wet
Potassium
4.00
U
25.0
mg/kg wet
Selenium
0.410
U
0.500
mg/kg wet
Sodium
6.00
U
25.0
mg/kg wet
Zinc
1.10
U
2.50
mg/kg wet
LCS (OC20013-BSI)
Prepared: 03/20/2020 09:45 Analyzed: 03/24/2020 13:59
Spike
Source
%REC RPD
Analvte
Result
Flaa Q
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
107
10.0
mg/kg wet
108
100
80-120
Arsenic
9.61
0.500
mg/kg wet
10.8
89
80-120
Cadmium
0.982
0.0500
mg/kg wet
1.08
91
80-120
FINAL
This report relates only to the sample as received by the laboratory, and
may only be reproduced in
full. Page 6 of 12

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OC2OO13 - EPA 3050E - Continued
LCS (OC20013-BSI) Continued
Prepared:
03/20/2020
09:45 Analyzed: 03/24/2020 13:59
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Calcium
107
25.0
mg/kg
wet
108
100
80-120
Copper
10.3
0.500
mg/kg
wet
10.8
96
80-120
Lead
10.0
0.500
mg/kg
wet
10.8
93
80-120
Magnesium
107
25.0
mg/kg
wet
108
99
80-120
Molybdenum
10.1
0.500
mg/kg
wet
10.8
94
80-120
Nickel
10.1
2.50
mg/kg
wet
10.8
94
80-120
Potassium
543
25.0
mg/kg
wet
538
101
80-120
Selenium
9.37
0.500
mg/kg
wet
10.8
87
80-120
Sodium
547
25.0
mg/kg
wet
538
102
80-120
Zinc
10.1
2.50
mg/kg
wet
10.8
94
80-120
Matrix Spike (OC20013-MS1)
Prepared:
03/20/2020
09:45 Analyzed: 03/24/2020 14:05
Source: CD04603-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
POL
Units
Level
Result
"/oREC
Limits
RPD
Limit
Notes
Aluminum
4920
11.0
mg/kg
dry
112
2380
NR
75-125
QM-07
Arsenic
10.0
0.548
mg/kg
dry
11.2
0.351 U
90
75-125
Cadmium
1.00
0.0548
mg/kg
dry
1.12
0.0275
87
75-125
Calcium
299
27.4
mg/kg
dry
112
324
NR
75-125
QM-07
Copper
13.0
0.548
mg/kg
dry
11.2
2.09
98
75-125
Lead
17.3
0.548
mg/kg
dry
11.2
6.70
95
75-125
Magnesium
263
27.4
mg/kg
dry
112
81.7
162
75-125
QM-07
Molybdenum
9.86
0.548
mg/kg
dry
11.2
0.110 U
88
75-125
Nickel
11.9
2.74
mg/kg
dry
11.2
0.678
101
75-125
Potassium
741
27.4
mg/kg
dry
559
123
110
75-125
Selenium
9.56
0.548
mg/kg
dry
11.2
0.449 U
86
75-125
Sodium
564
27.4
mg/kg
dry
559
19.8
97
75-125
Zinc
17.1
2.74
mg/kg
dry
11.2
4.32
114
75-125
Matrix Spike Dup (OC20013-MSD1)
Prepared:
03/20/2020
09:45 Analyzed: 03/24/2020 14:08
Source: CD04603-01
Spike
Source
%REC
RPD
Analyte
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
5030
11.0
mg/kg
dry
111
2380
NR
75-125
2
20
QM-07
Arsenic
10.4
0.548
mg/kg
dry
11.1
0.351 U
94
75-125
3
20
Cadmium
1.07
0.0548
mg/kg
dry
1.11
0.0275
94
75-125
6
20
Calcium
288
27.4
mg/kg
dry
111
324
NR
75-125
4
20
QM-07
Copper
12.9
0.548
mg/kg
dry
11.1
2.09
98
75-125
0.5
20
Lead
17.2
0.548
mg/kg
dry
11.1
6.70
95
75-125
0.5
20
Magnesium
258
27.4
mg/kg
dry
111
81.7
160
75-125
2
20
QM-07
Molybdenum
10.0
0.548
mg/kg
dry
11.1
0.110 U
91
75-125
2
20
Nickel
12.5
2.74
mg/kg
dry
11.1
0.678
107
75-125
5
20
Potassium
720
27.4
mg/kg
dry
553
123
108
75-125
3
20
Selenium
9.56
0.548
mg/kg
dry
11.1
0.449 U
86
75-125
0.006
20
Sodium
553
27.4
mg/kg
dry
553
19.8
96
75-125
2
20
Zinc
17.1
2.74
mg/kg
dry
11.1
4.32
116
75-125
0.2
20
Post Spike (OC20013-PS1)
Prepared:
03/20/2020
09:45 Analyzed: 03/24/2020 14:11
Source: CD04603-01
Spike
Source
%REC
RPD
Analyte
Result
Flaa
POLL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 12

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OC2OO13 - EPA 3050E - Continued
Post Spike (OC20013-PSI) Continued
Prepared: 03/20/2020 09:45 Analyzed: 03/24/2020 14:11
Source: CD04603-01
Spike
Source
a/oREC RPD
Anala Result Flaa
Q
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum 43.4
0.200
mg/L
2.00
40.8
132
80-120 QM-08
Arsenic 0.205
0.0100
mg/L
0.200
0.00159
102
80-120
Cadmium 0.0196
0.00100
mg/L
0.0200
0.000472
96
80-120
Calcium 7.35
0.500
mg/L
2.00
5.56
89
80-120
Copper 0.243
0.0100
mg/L
0.200
0.0359
104
80-120
Lead 0.325
0.0100
mg/L
0.200
0.115
105
80-120
Magnesium 3.52
0.500
mg/L
2.00
1.40
106
80-120
Molybdenum 0.206
0.0100
mg/L
0.200
0.000992
102
80-120
Nickel 0.213
0.0500
mg/L
0.200
0.0116
101
80-120
Potassium 12.8
0.500
mg/L
10.0
2.11
107
80-120
Selenium 0.189
0.0100
mg/L
0.200
-0.00921
94
80-120
Sodium 11.2
0.500
mg/L
10.0
0.340
108
80-120
Zinc 0.273
0.0500
mg/L
0.200
0.0741
99
80-120
Classical Chemistry Parameters - Quality Control
Batch OC24OO2 - Same
Blank (OC24002-BLKI) Prepared: 03/25/2020 09:41 Analyzed: 03/25/2020 19:25
Spike Source %REC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Phosphorus 2.9 U 8.0 mg/kg wet
LCS (OC24002-BSI) Prepared: 03/25/2020 09:41 Analyzed: 03/25/2020 19:26
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
120
8.0
mg/kg wet
124
98
80-120
Matrix Spike (OC24002-MS1)
Prepared: 03/25/2020 09:41 Analyzed: 03/25/2020 19:29
Source: CD01355-02
Spike
Source
%REC
RPD
Analyte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
21000
D
15000
mg/kg dry
1900
17000
197
80-120
QM-07
Matrix Spike Dup (OC24002-MSDI)
Prepared: 03/25/2020 09:41 Analyzed: 03/25/2020 19:33
Source: CD01355-02
Spike
Source
%REC
RPD
Analyte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
19000
D
15000
mg/kg dry
1820
17000
145
80-120 6
25
QM-07
Batch OC24003 - Same
Blank (OC24003-BLKI)
Prepared: 03/25/2020 09:41 Analyzed: 03/30/2020 13:37
Spike Source %REC
RPD
Analvte
Result Flaa Q Units Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
35 U 38 mg/kg wet
LCS (OC24003-BSI)
Prepared: 03/25/2020 09:41 Analyzed: 03/30/2020 13:39
Spike Source %REC
RPD
Analvte
Result Flaa Q Units Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 8 of 12

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OC24003 - Same - Continued
LCS (OC24003-BSI) Continued Prepared: 03/25/2020 09:41 Analyzed: 03/30/2020 13:39
Spike Source a/oREC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
990
38
mg/kg wet
931 106 90-110
Matrix Spike (OC24003-MSI)
Prepared: 03/25/2020 09:41 Analyzed: 03/30/2020 13:42
Source: CDO1355-02
Spike Source %REC
RPD
Anala
Result
Fla
NQ L
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
66000
D
7300
mg/kg dry
14200 530000 940 90-110
QM-07
Matrix Spike Dup (OC24003-MSDI)
Prepared: 03/25/2020 09:41 Analyzed: 03/30/2020 13:44
Source: CDO1355-02
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
73000
D
7300
mg/kg dry
1360 53000 NR 90-110 10
10
QM-07
Batch OC24029 - WETS-88 Soil Leaching
Blank (OC24029-BLKI)
Prepared: 03/25/2020 11:47 Analyzed: 03/26/2020 06:44
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Nitrate as N 2.0 1 10 mg/kg wet J-01
Nitrite as N 0.080 U 1.0 mg/kg wet
LCS (OC24029-BSI) Prepared: 03/25/2020 11:47 Analyzed: 03/26/2020 07:02
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate as N
47
B
10
mg/kg wet
50.0 94 80-120
Nitrite as N
10
1.0
mg/kg wet
10.0 101 80-120
Matrix Spike (OC24029-MSI)
Prepared: 03/25/2020 11:47 Analyzed: 03/26/2020 07:37
Source: CDO1355-02RE1
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate as N
680
B
380
mg/kg dry
759 79 80 80-120
Nitrite as N
390
38
mg/kg dry
379 15 99 80-120
Matrix Spike Dup (OC24029-MSDI)
Prepared: 03/25/2020 11:47 Analyzed: 03/26/2020 07:55
Source: CDO1355-02RE1
Spike
Source
%REC
RPD
Anala
Result Flaa Q Units
Level
Result
%REC Limits RPD
Limit Notes
Nitrate as N
620 B 380 mg/kg dry
759
79
71 80-120 10
15 QM-07
Nitrite as N
390 38 mg/kg dry
379
15
98 80-120 1
15
Batch OC25031 - NO PREP
Duplicate (OC25031-DUPI) Prepared & Analyzed: 03/25/2020 16:10
Source: CDO1355-02
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Total Solids 2.7 0.0010 % by Weight 2.7 0.5 25
Batch OC31030 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 12

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OC31030 - NO PREP - Continued
Blank (OC31030-BLKI) Prepared: 03/31/2020 14:52 Analyzed: 04/01/2020 14:05
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.45 U 1.0 mg/kg wet
LCS (OC31030-BSI) Prepared: 03/31/2020 14:52 Analyzed: 04/01/2020 14:07
Spike
Source
%REC
RPD
Analvte
Result
Flao
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
11
1.0
mg/kg wet
10.1
109
90-110
Matrix Spike (OC31030-MSI)
Prepared: 03/31/2020 14:52 Analyzed: 04/01/2020 14:13
Source: CDO1355-02
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
5900
D
380
mg/kg dry
150
6200
NR
90-110
QM-07
Matrix Spike Dup (OC31030-MSDI)
Prepared: 03/31/2020 14:52 Analyzed: 04/01/2020 14:15
Source: CDO1355-02
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
6100
D
380
mg/kg dry
148
6200
NR
90-110 4
10
QM-07
Batch OD03030 - Same
LCS (OD03030-BSI) Prepared & Analyzed: 04/03/2020 15:28
Spike Source %REC
RPD
Analvte
Result FFF`lau
Q
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.0
1.0
pH Units
7.00 100 99-101
Duplicate (OD03030-DUPI)
Prepared: 04/03/2020 14:18 Analyzed: 04/03/2020 15:28
Source: CDO1355-02
Spike Source %REC
RPD
Analvte
Result Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.3
1.0
pH Units
7.2 0.8
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 12

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
J-01 Result may be biased high due to positive results in the associated method blank at a concentration above
the MDL and/or greater than one-half the MRL.
Q-01 Analysis performed outside of method - specified holding time.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 12

EA ViR—:)NhiIIIGi`l t AL 44IDEeZa,ERVA i iVIV LfiSLJlC% TGKiES CHAN-OF-CUSTODY RECORD
• 10775 Central Por,, dr. 4610 Fzecubve Park Court. Suga i V 102-A Woodwinds Irdusiriai Couri
Orlando, FL 32824 J=ksonvifle. FL 32216-6r36.9 Cary. NC 27511
14071326-5314 Pax(407)I{59-045 [phone] Fax[phone] [9191467-3099 Fax[phone]
Stshmit by Email I - Print Form �
Page of
Ciient Nama
Fnviro-Choice Recycling, LLC
Project Number
Requested
Analyses
Requested Turnaround
Times
Note. Rush requesln eubjecl to
acceptance by the facility
Standard
— Expedited
Due —1— I_
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Lumberton, NC, 28360
PO4, BAI InrG
Tel
910-738-5311
Fax
Reporting Contact
Michael Hunt
ampler(s) Name. Affiliation (Print)
Davis
Billing Contact
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Cameron Testing Services, Inc. Laboratory Report Nc DENIR m&
NC PHHSm«
US A #NCO ,«B
Client: Env| - hoice Recycling LLC CTSPro. 2003- 64
Project: City of Lumberton Regulatory A.
Sample Information
Sampled J ya§s Date 03/15120 Received C. Cameron Date 02A5120
Analyses and Results
x . 2 / a Std.■
Labt & m �� I[)\ A el! n ! \ / \ & 2 % m
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62 £47% 0.01
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Review `
Lab 1 D
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Sanrcwd 27.330 c_m mk7_

219 S. Slaela Skr
Sanford, NC 27330
Phone: [phone]
Cameron Testing Services, Inc
NC >fiM?GW Cert 9654 NC PHHS CArt 10 37799 US EPA NCO 191€
Chain of Custody
Page of
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Sample Information
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ENCO Laboratories
9g
Accurate, Timely. Responsive. Iuuovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, July 31, 2020
Hunt Environmental Associates (HU017)
Attn: Jordan Davis
3330 Saddletree Road.
Lumberton, NC 28360
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: City of Lumberton
ENCO Workorder(s): CD07944
Dear Jordan Davis,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, June 24, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OLdcc-'----�A
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: WW-1
Lab ID: CD07944-01
Sampled: 06/23/20 13:45
Received: 06/24/20 08:47
Parameter
Preoaration
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 1010A
NO PREP
07/07/20
07/02/20
15:00
07/02/20 15:30
EPA 6010D
EPA 3010A
12/20/20
12/29/20
07/02/20
13:36
07/03/20 12:47
EPA 7470A
EPA 7470A
07/21/20
07/29/20
07/01/20
12:07
07/02/20 10:55
EPA 8081B
EPA 3510C
06/30/20
08/10/20
07/01/20
11:20
07/07/20 16:43
EPA 8151A
EPA 3510C
06/30/20
08/11/20
07/02/20
09:00
07/07/20 20:38
EPA 8260D
EPA 503013_MS
07/07/20
07/15/20
07/01/20
13:17
07/02/20 01:04
EPA 8270E
EPA 3510C_MS
06/30/20
08/10/20
07/01/20
13:30
07/06/20 16:19
SW-846 Ch.7 Sec.3
NO PREP
07/07/20
07/07/20
10:00
07/07/20 16:00
SW-846 Ch.7 Sec.3
NO PREP
07/07/20
07/07/20
10:00
07/07/20 17:00
Client ID: WW-2
Lab ID: CD07944-02
Sampled: 06/23/20 13:45
Received: 06/24/20 08:47
Parameter
Preoaration
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC 9056A
WETS-88 Soil
03/19/23
06/25/20
08:42
06/25/20 08:42
Leaching
EPA 350.1
WETS-88 Soil
07/21/20
07/22/20
06/24/20
15:46
06/26/20 12:51
Leaching
EPA 351.2
Same
07/21/20
07/02/20
08:10
07/06/20 11:22
EPA 365.4
Same
07/21/20
07/02/20
08:10
07/09/20 10:33
EPA 6010D
EPA 3050B
12/20/20
06/26/20
14:48
06/30/20 14:04
EPA 7471B
EPA 7471B
07/21/20
07/01/20
10:31
07/02/20 18:13
EPA 9045D
Same
07/31/20 11:29
07/31/20
11:15
07/31/20 11:15
EPA 9056A
WETS-88 Soil
06/26/20
06/26/20
13:04 06/24/20
13:04
06/24/20 19:44
Leaching
SM 254OG-2011
NO PREP
06/30/20
06/28/20
10:10
06/28/20 10:10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 23

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SAMPLE DETECTION SUMMARY
Client ID: WW-2
Lab ID: CD07944-02
Analvte
Results
Flag
MDL
2
Units
Method Notes
Aluminum - Total
23100
97.1
462
mg/kg dry
EPA 6010D
Ammonia as N
13000
D
420
920
mg/kg dry
EPA 350.1
Cadmium - Total
0.504
J
0.444
2.31
mg/kg dry
EPA 6010D
Calcium - Total
12300
259
1160
mg/kg dry
EPA 6010D
Chromium - Total
228
4.62
23.1
mg/kg dry
EPA 6010D
Copper - Total
276
8.78
23.1
mg/kg dry
EPA 6010D
Lead - Total
19.8
J
5.55
23.1
mg/kg dry
EPA 6010D
Magnesium - Total
2180
43.0
1160
mg/kg dry
EPA 6010D
Molybdenum - Total
7.24
J
4.62
23.1
mg/kg dry
EPA 6010D
Nickel - Total
41.3
J
16.6
116
mg/kg dry
EPA 6010D
Nitrate as N
97
JB
95
460
mg/kg dry
EPA 9056A J-01
Nitrate/Nitrite as N
110
9.5
23
mg/kg dry
CALC 9056A
Nitrite as N
13
JB
3.7
46
mg/kg dry
EPA 9056A J-01
pH
7.3
1.0
1.0
pH Units
EPA 9045D
Phosphorus
16000
D
670
1800
mg/kg dry
EPA 365.4
Potassium - Total
4030
185
1160
mg/kg dry
EPA 6010D
Sodium - Total
11400
277
1160
mg/kg dry
EPA 6010D
Temperature for pH (deg. C)
22
pH Units
EPA 9045D
Total Kjeldahl Nitrogen
49000
1600
1800
mg/kg dry
EPA 351.2
Total Solids
2.1
0.0010
0.0010
% by Weight
SM 2540G-2011
Zinc - Total
613
50.9
116
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 23

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ANALYTICAL RESULTS
Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47
Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944
Project: City of Lumberton Sampled By:CARRIGAN HARRIS
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By Notes
Arsenic [7440-38-2]^
0.380
U
mg/L
50
0.380
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Barium [7440-39-3]^
0.0550
U
mg/L
50
0.0550
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Cadmium [7440-43-9]^
0.0180
U
mg/L
50
0.0180
0.0500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Chromium [7440-47-3]^
0.0700
U
mg/L
50
0.0700
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Lead [7439-92-1]^
0.155
U
mg/L
50
0.155
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Selenium [7782-49-2]^
0.310
U
mg/L
50
0.310
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
Silver [7440-22-4]^
0.0950
U
mg/L
50
0.0950
0.500
0G02038
EPA 6010D
07/03/20 12:47
JDH
TCLP Volatile Organics by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By Notes
1,1-Dichloroethene [75-35-4]^
0.094
UD
mg/L
100
0.094
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
1,2-Dichloroethane [107-06-2]^
0.063
UD
mg/L
100
0.063
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
2-Butanone [78-93-3]^
0.45
UD
mg/L
100
0.45
0.50
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Benzene [71-43-2]^
0.071
UD
mg/L
100
0.071
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Carbon Tetrachloride [56-23-5]^
0.094
UD
mg/L
100
0.094
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Chlorobenzene [108-90-7]^
0.072
UD
mg/L
100
0.072
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Chloroform [67-66-3]^
0.080
UD
mg/L
100
0.080
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Tetrachloroethene [127-18-4]^
0.076
UD
mg/L
100
0.076
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Trichloroethene [79-01-6]^
0.089
UD
mg/L
100
0.089
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Vinyl chloride [75-01-4]^
0.071
UD
mg/L
100
0.071
0.10
0GO1040
EPA 8260D
07/02/20 01:04
KKW
Sunoaates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
By
Notes
4-Bromofluorobenzene
0.054
1
0.0500
107 %
41-142
0GO1040
EPA 8260D
07102120 01:04
KKW
Dibromofluoromethane
0.057
1
0.0500
113 %
53-146
0GO1040
EPA 8260D
07102120 01:04
KKW
Toluene-d8
0.053
1
0.0500
106 %
41-146
0GO1040
EPA 8260D
07102120 01:04
KKW
TCLP Semivolatile Organics by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL Q
Batch
Method
Analyzed
By
Notes
1,4-Dichlorobenzene [106-46-7]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
2,4,5-Trichlorophenol [95-95-4]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
2,4,6-Trichlorophenol [88-06-2]^
0.03
UD
mg/L
5
0.03 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
2,4-Dinitrotoluene [121-14-2]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
2-Methylphenol [95-48-7]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
QV-01
3 & 4-Methylphenol[108-39-4/106-44-5]^
0.04
UD
mg/L
5
0.04 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Hexachlorobenzene [118-74-1]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Hexachlorobutadiene [87-68-3]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Hexachloroethane [67-72-1]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Nitrobenzene [98-95-3]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Pentachlorophenol[87-86-5]^
0.04
UD
mg/L
5
0.04 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
Pyridine [110-86-1]^
0.02
UD
mg/L
5
0.02 0.05
0GO1036
EPA 8270E
07/06/20 16:19
jfi
surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,6-Tribromophenol
0.10
5
0.250
40 %
33-145
0GO1036
EPA 8270E
0710612016:19
jfi
2-Fluorobiphenyl
0.16
5
0.250
65 %
32-116
0GO1036
EPA 8270E
0710612016:19
jfi
2-Fluorophenol
0.10
5
0.250
40 %
11-100
0GO1036
EPA 8270E
0710612016:19
jfi
Nitrobenzene-d5
0.13
5
0.250
54 %
24-107
0GO1036
EPA 8270E
0710612016:19
jfi
FINAL
This report relates only to the
sample as received by the laboratory, and may only
be reproduced in full.
Page 4 of 23

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ANALYTICAL RESULTS
Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47
Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944
Project: City of Lumberton Sampled By:CARRIGAN HARRIS
TCLP Semivolatile Organics by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Sunoaates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vied
By
Notes
Phenol-d5
0.060
5
0.250
24 %
10-100
0GO1036
EPA 8270E
0710612016:19
jfi
Telphenyl-d14
0.19
5
0.250
78 %
52-150
0GO1036
EPA 8270E
0710612016:19
jfi
TCLP Pesticides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl
Results
Flag
Units
DF
MDL Q
Batch
Method
Analyzed
By
Notes
Chlordane (tech) [12789-03-6]^
0.00036
U
mg/L
1
0.00036 0.00050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
Endrin [72-20-8]^
0.000014
U
mg/L
1
0.000014 0.000050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
gamma-BHC [58-89-9]^
0.000021
U
mg/L
1
0.000021 0.000050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
Heptachlor [76-44-8]^
0.000026
U
mg/L
1
0.000026 0.000050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
Heptachlor epoxide [1024-57-3]^
0.000018
U
mg/L
1
0.000018 0.000050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
Methoxychlor [72-43-5]^
0.000020
U
mg/L
1
0.000020 0.000050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
Toxaphene [8001-35-2]^
0.00048
U
mg/L
1
0.00048 0.00050
0GO1025
EPA 8081B
07/07/20 16:43
JIB
surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
2,4,5,E-TCMX
0.0035
1
0.00500
70 %
38-142
0GO1025
EPA 8081B
0710712016:43
JJB
Decachloroblphenyl
0.0032
1
0.00500
64 %
34-159
0GO1025
EPA 8081B
0710712016:43
JJB
TCLP Herbicides by GC
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL 2
Batch
Method
Analyzed
By
Notes
2,4,5-TP (Silvex) [93-72-1]^
0.00044
U
mg/L
1
0.00044 0.00050
0G02006
EPA 8151A
07/07/20 20:38
RGG
2,4-D [94-75-7]^
0.00027
U
mg/L
1
0.00027 0.00050
0G02006
EPA 8151A
07/07/20 20:38
RGG
Sunoaates Results DF
Spike Lv/
% Rec % Rec Limits
Batch
Method
Analyzed
By Notes
2,4-DC4A 0.0073 1
0.0100
73 % 37-134
0GO2006
EPA 8151A
07107120 2038
RGG
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Orlando certified analyte [NC 424]
Analyte MAS Numberl Results Flag
Units
DF MDL Q
Batch
Method
Analyzed
Notes
Mercury [7439-97-6]^ 0.000230 U
mg/L
1 0.000230 0.00200
0GO1019
EPA 7470A
07/02/20 10:55
]SS
Classical Chemistry Parameters
Analyte MAS Numberl
Reactive Cyanide [57-12-5]
Reactive Sulfide [57-12-5]
Results Flag Units DF Q Batch Method Analyzed By Notes
250 U mg/L 1 250 0G07010 3W-846 Ch.7 Sec.- 07/07/20 16:00 PIR
500 U mg/L 1 500 0G08018 3W-846 Ch.7 Sec.- 07/07/20 17:00 PIR
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 23

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ANALYTICAL RESULTS
Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47
Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944
Project: City of Lumberton Sampled By:CARRIGAN HARRIS
Classical Chemistry Parameters
Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Flashpoint > 200 OF 1 OG02008 EPA 1O10A 07/02/20 15:30 SMA
Description: WW-2 Lab Sample ID:CD07944-02 Received: 06/24/20 08:47
Matrix: Sludge Sampled:06/23/20 13:45 Work Order: CD07944
Project: City of Lumberton Sampled By:CARRIGAN HARRIS % Solids: 2.16
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
23100
mg/kg dry
1
97.1
462
OF26026
EPA 6010D
06/30/20 14:04
JDH
Arsenic [7440-38-2]A
14.8
U
mg/kg dry
1
14.8
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Cadmium [7440-43-9]A
0.504
J
mg/kg dry
1
0.444
2.31
OF26026
EPA 6010D
06/30/20 14:04
JDH
Calcium [7440-70-2]A
12300
mg/kg dry
1
259
1160
OF26026
EPA 6010D
06/30/20 14:04
JDH
Chromium [7440-47-3]A
228
mg/kg dry
1
4.62
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Copper [7440-50-8]A
276
mg/kg dry
1
8.78
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Lead [7439-92-1]A
19.8
J
mg/kg dry
1
5.55
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Magnesium [7439-95-4]A
2180
mg/kg dry
1
43.0
1160
OF26026
EPA 6010D
06/30/20 14:04
JDH
Mercury [7439-97-6]A
2.13
U
mg/kg dry
1
2.13
2.85
OG01013
EPA 7471B
07/02/20 18:13
KAH
Molybdenum [7439-98-7]1
7.24
J
mg/kg dry
1
4.62
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Nickel [7440-02-0]A
41.3
J
mg/kg dry
1
16.6
116
OF26026
EPA 6010D
06/30/20 14:04
JDH
Potassium [7440-09-7]A
4030
mg/kg dry
1
185
1160
OF26026
EPA 6010D
06/30/20 14:04
JDH
Selenium [7782-49-2]A
19.0
U
mg/kg dry
1
19.0
23.1
OF26026
EPA 6010D
06/30/20 14:04
JDH
Sodium [7440-23-5]^
11400
mg/kg dry
1
277
1160
OF26026
EPA 6010D
06/30/20 14:04
JDH
Zinc [7440-66-6]1
613
mg/kg dry
1
50.9
116
OF26026
EPA 6010D
06/30/20 14:04
JDH
Classical Chemistry Parameters
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]
13000
D
mg/kg dry
20
420
920
OF24036
EPA 350.1
06/26/20 12:51
JAH
Nitrate as N [14797-55-8]
97
JB
mg/kg dry
1
95
460
OF24022
EPA 9056A
06/24/20 19:44
LJI J-01
Nitrate/Nitrite as N
110
mg/kg dry
1
9.5
23
OF25007
CALC 9056A
06/25/20 08:42
LJI
Nitrite as N [14797-65-0]
13
JB
mg/kg dry
1
3.7
46
OF24022
EPA 9056A
06/24/20 19:44
LJI 3-01
pH
7.3
pH Units
1
1.0
1.0
OG31023
EPA 9045D
07/31/20 11:15
LJI
Phosphorus [7723-14-0]
16000
D
mg/kg dry
5
670
1800
OG02010
EPA 365.4
07/09/20 10:33
JAH
Temperature for pH (deg. C)
22
pH Units
1
OG31023
EPA 9045D
07/31/20 11:15
LJI
Total Kjeldahl Nitrogen
49000
mg/kg dry
1
1600
1800
OG02011
EPA 351.2
07/06/20 11:22
JAH
Total Solids
2.1
% by Weight
1
0.0010
0.0010
OF28001
SM 2540G-2011
06/28/20 10:10
BDC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 23

(� �Eo
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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OF26O26 - EPA 3050E
Blank (OF26026-BLKI) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:41
Spike Source a/oREC RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
2.42
1
10.0
mg/kg wet
Arsenic
0.320
U
0.500
mg/kg wet
Cadmium
0.00960
U
0.0500
mg/kg wet
Calcium
5.60
U
25.0
mg/kg wet
Chromium
0.100
U
0.500
mg/kg wet
Copper
0.190
U
0.500
mg/kg wet
Lead
0.120
U
0.500
mg/kg wet
Magnesium
0.930
U
25.0
mg/kg wet
Molybdenum
0.100
U
0.500
mg/kg wet
Nickel
0.360
U
2.50
mg/kg wet
Potassium
4.00
U
25.0
mg/kg wet
Selenium
0.410
U
0.500
mg/kg wet
Sodium
6.00
U
25.0
mg/kg wet
Zinc
1.10
U
2.50
mg/kg wet
LCS (OF26026-BSI)
Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:44
Spike
Source
%REC RPD
Anala
Result
Flaa Q
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
104
10.0
mg/kg wet
106
97
80-120
Arsenic
10.3
0.500
mg/kg wet
10.6
97
80-120
Cadmium
1.07
0.0500
mg/kg wet
1.06
101
80-120
Calcium
116
25.0
mg/kg wet
106
109
80-120
Chromium
10.3
0.500
mg/kg wet
10.6
97
80-120
Copper
10.2
0.500
mg/kg wet
10.6
96
80-120
Lead
10.6
0.500
mg/kg wet
10.6
100
80-120
Magnesium
105
25.0
mg/kg wet
106
99
80-120
Molybdenum
10.5
0.500
mg/kg wet
10.6
99
80-120
Nickel
10.8
2.50
mg/kg wet
10.6
101
80-120
Potassium
533
25.0
mg/kg wet
532
100
80-120
Selenium
10.2
0.500
mg/kg wet
10.6
96
80-120
Sodium
508
25.0
mg/kg wet
532
96
80-120
Zinc
10.9
2.50
mg/kg wet
10.6
103
80-120
Matrix Spike (OF26026-MS1)
Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:49
Source: CD09771-38
Spike
Source
%REC RPD
Analvte
Result
FFFlau Q
Units
Level
Result
%REC
Limits RPD Limit
Notes
Aluminum
8630
11.3
mg/kg dry
119
3850
NR
75-125
QM-07
Arsenic
11.4
0.564
mg/kg dry
11.9
0.383
93
75-125
Cadmium
1.06
0.0564
mg/kg dry
1.19
0.0108 U
89
75-125
Calcium
315
28.2
mg/kg dry
119
201
96
75-125
Chromium
15.6
0.564
mg/kg dry
11.9
3.02
106
75-125
Copper
14.4
0.564
mg/kg dry
11.9
1.83
106
75-125
Lead
245
0.564
mg/kg dry
11.9
274
NR
75-125
QM-07
Magnesium
540
28.2
mg/kg dry
119
313
191
75-125
QM-07
Molybdenum
11.2
0.564
mg/kg dry
11.9
0.113 U
94
75-125
Nickel
13.1
2.82
mg/kg dry
11.9
0.581
105
75-125
Potassium
1230
28.2
mg/kg dry
594
485
126
75-125
QM-07
Selenium
8.33
0.564
mg/kg dry
11.9
0.463 U
70
75-125
QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be
reproduced in
full.
Page 7 of 23

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www.encolabs.com
QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OF26O26 - EPA 3050E - Continued
Matrix Spike (OF26026-MSI) Continued
Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:49
Source: CD09771-38
Spike
Source
a/oREC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Sodium
583
28.2
mg/kg dry
594
9.21
97
75-125
Zinc
24.6
2.82
mg/kg dry
11.9
9.55
127
75-125
QM-07
Matrix Spike Dup (OF26026-MSD1)
Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:57
Source: CD09771-38
Spike
Source
%REC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
7220
11.3
mg/kg dry
115
3850
NR
75-125
18
20
QM-07
Arsenic
10.5
0.564
mg/kg dry
11.5
0.383
88
75-125
8
20
Cadmium
1.04
0.0564
mg/kg dry
1.15
0.0108 U
90
75-125
1
20
Calcium
286
28.2
mg/kg dry
115
201
74
75-125
10
20
QM-07
Chromium
14.1
0.564
mg/kg dry
11.5
3.02
97
75-125
10
20
Copper
13.1
0.564
mg/kg dry
11.5
1.83
98
75-125
10
20
Lead
225
0.564
mg/kg dry
11.5
274
NR
75-125
8
20
QM-07
Magnesium
461
28.2
mg/kg dry
115
313
128
75-125
16
20
QM-07
Molybdenum
10.5
0.564
mg/kg dry
11.5
0.113 U
91
75-125
7
20
Nickel
12.2
2.82
mg/kg dry
11.5
0.581
101
75-125
7
20
Potassium
1080
28.2
mg/kg dry
576
485
103
75-125
13
20
Selenium
8.39
0.564
mg/kg dry
11.5
0.463 U
73
75-125
0.6
20
QM-07
Sodium
543
28.2
mg/kg dry
576
9.21
93
75-125
7
20
Zinc
21.6
2.82
mg/kg dry
11.5
9.55
105
75-125
13
20
Post Spike (OF26026-PSI)
Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 14:00
Source: CD09771-38
Spike
Source
%REC
RPD
Analvte
Result
Flaa Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Aluminum
65.7
0.200
mg/L
2.00
64.8
45
80-120
QM-08
Arsenic
0.220
0.0100
mg/L
0.200
0.00645
107
80-120
Cadmium
0.0215
0.00100
mg/L
0.0200
-0.000365
108
80-120
Calcium
5.53
0.500
mg/L
2.00
3.38
108
80-120
Chromium
0.260
0.0100
mg/L
0.200
0.0509
104
80-120
Copper
0.243
0.0100
mg/L
0.200
0.0309
106
80-120
Lead
4.71
0.0100
mg/L
0.200
4.61
49
80-120
QM-08
Magnesium
7.31
0.500
mg/L
2.00
5.27
102
80-120
Molybdenum
0.218
0.0100
mg/L
0.200
0.000870
109
80-120
Nickel
0.229
0.0500
mg/L
0.200
0.00978
110
80-120
Potassium
19.4
0.500
mg/L
10.0
8.17
112
80-120
Selenium
0.191
0.0100
mg/L
0.200
-0.0258
96
80-120
Sodium
10.9
0.500
mg/L
10.0
0.155
107
80-120
Zinc
0.370
0.0500
mg/L
0.200
0.161
105
80-120
Batch 0GO1O13 - EPA 7471E
Blank (OG01013-BLKI)
Prepared:
07/O1/2020
10:31 Analyzed: 07/02/2020 18:09
Spike
Source
%REC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.0460
U 0.0617
mg/kg wet
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 23

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0GO1013 - EPA 7471E - Continued
LCS (OG01013-BSI) Prepared: 07/O1/2020 10:31 Analyzed: 07/02/2020 18:11
Spike
Source
a/oREC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.594
0.0617
mg/kg wet
0.600
99
80-120
Matrix Spike (OG01013-MSI)
Prepared: 07/O1/2020 10:31 Analyzed: 07/02/2020 18:16
Source: CD07944-02
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
29.8
3.17
mg/kg dry
30.8
2.36 U
97
80-120
Matrix Spike Dup (OG01013-MSD1)
Prepared: 07/01/2020 10:31 Analyzed: 07/02/2020 18:17
Source: CD07944-02
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
32.1
3.42
mg/kg dry
33.3
2.55 U
96
80-120 7
20
Post Spike (OG01013-PSI)
Prepared: 07/01/2020 10:31 Analyzed: 07/02/2020 18:19
Source: CD07944-02
Spike
Source
%REC
RPD
Analyte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.72
0.514
ug/L
5.00
0.122
112
75-125
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 0GO2038 - EPA 3010A
Blank (OG02038-BLKI)
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 11:47
Spike Source %REC RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
0.380
U
0.500
mg/L
Barium
0.0607
1
0.500
mg/L
Cadmium
0.0180
U
0.0500
mg/L
Chromium
0.0700
U
0.500
mg/L
Lead
0.155
U
0.500
mg/L
Selenium
0.310
U
0.500
mg/L
Silver
0.0950
U
0.500
mg/L
LCS (OG02038-BSI)
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 11:52
Spike
Source
%REC RPD
Analvte
Result
Flao Q
Units
Level
Result %REC
Limits RPD Limit Notes
Arsenic
0.190
0.0100
mg/L
0.200
95
80-120
Barium
0.201
0.0100
mg/L
0.200
101
80-120
Cadmium
0.0193
0.00100
mg/L
0.0200
96
80-120
Chromium
0.192
0.0100
mg/L
0.200
96
80-120
Lead
0.195
0.0100
mg/L
0.200
97
80-120
Selenium
0.190
0.0100
mg/L
0.200
95
80-120
Silver
0.191
0.0100
mg/L
0.200
95
80-120
Matrix Spike (OG02038-MS1)
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:38
Source: CD10423-01
Spike Source %REC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Arsenic 8.99 0.500 mg/L 10.0 0.380 U 90 75-125
Barium 10.3 0.500 mg/L 10.0 0.779 95 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 23

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 0GO2O38 - EPA 3O1OA - Continued
Matrix Spike (OG02038-MS3) Continued
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:38
Source: CD10423-01
Spike
Source
a/oREC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Cadmium
0.925
0.0500
mg/L
1.00
0.0180 U
92
75-125
Chromium
9.12
0.500
mg/L
10.0
0.0700 U
91
75-125
Lead
9.37
0.500
mg/L
10.0
0.155 U
94
75-125
Selenium
9.24
0.500
mg/L
10.0
0.310 U
92
75-125
Silver
9.07
0.500
mg/L
10.0
0.0950 U
91
75-125
Matrix Spike Dup (OG02038-MSDI)
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:40
Source: CD10423-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
8.93
0.500
mg/L
10.0
0.380 U
89
75-125
0.7
20
Barium
10.2
0.500
mg/L
10.0
0.779
94
75-125
1
20
Cadmium
0.904
0.0500
mg/L
1.00
0.0180 U
90
75-125
2
20
Chromium
9.06
0.500
mg/L
10.0
0.0700 U
91
75-125
0.7
20
Lead
9.20
0.500
mg/L
10.0
0.155 U
92
75-125
2
20
Selenium
9.10
0.500
mg/L
10.0
0.310 U
91
75-125
1
20
Silver
9.16
0.500
mg/L
10.0
0.0950 U
92
75-125
1
20
Post Spike (OG02038-PSI)
Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:42
Source: CD10423-01
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
0.182
0.0100
mg/L
0.200
-0.00291
91
80-120
Barium
0.206
0.0100
mg/L
0.200
0.0156
95
80-120
Cadmium
0.0185
0.00100
mg/L
0.0200
0.000100
92
80-120
Chromium
0.183
0.0100
mg/L
0.200
0.000195
92
80-120
Lead
0.187
0.0100
mg/L
0.200
0.00295
92
80-120
Selenium
0.190
0.0100
mg/L
0.200
-0.000449
95
80-120
Silver
0.188
0.0100
mg/L
0.200
-0.000292
94
80-120
Classical Chemistry Parameters - Quality Control
Batch OF24O22 - WETS-88 Soil Leaching
Blank (OF24022-BLKI)
Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 19:09
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate as N
2.0
1
10
mg/kg wet
J-01
Nitrite as N
0.19
1
1.0
mg/kg wet
J-01
LCS (OF24022-BSI)
Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 19:26
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate as N
48
B
10
mg/kg wet
50.0 97 80-120
Nitrite as N
9.7
B
1.0
mg/kg wet
10.0 97 80-120
Matrix Spike (OF24022-MSI)
Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:02
Source: CD07944-02
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate as N
820
B
460
mg/kg dry
925 97 78 80-120
QM-07
FINAL
This report relates only to the sample
as received by the laboratory, and may only be reproduced in full.
Page 10 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OF24022 - WETS-88 Soil Leaching - Continued
Matrix Spike (OF24022-MSI) Continued Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:02
Source: CD07944-02
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 440 B 46 mg/kg dry 462 13 93 80-120
Matrix Spike Dup (OF24022-MSD3) Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:19
Source: CD07944-02
Spike Source %REC
RPD
Analvte
Result Flao Q Units
Level Result %REC Limits RPD
Limit Notes
Nitrate as N
810 B 460 mg/kg dry
925 97 78 80-120 0.1
15 QM-07
Nitrite as N
440 B 46 mg/kg dry
462 13 93 80-120 0.1
15
Batch OF24036 - NO PREP
Blank (OF24036-BLKI)
Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:44
Spike Source %REC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.45 U 1.0 mg/kg wet
LCS (OF24036-BSI) Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:49
Spike
Source
%REC
RPD
Analvte
Result
Flao
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
10
1.0
mg/kg wet
10.1
101
90-110
Matrix Spike (OF24036-MSI)
Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:53
Source: CD07944-02
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
13000
D
920
mg/kg dry
187
13000
NR
90-110
QM-07
Matrix Spike Dup (OF24036-MSDI)
Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:54
Source: CD07944-02
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
13000
D
920
mg/kg dry
187
13000
169
90-110 3
10
QM-07
Batch OF28001 - NO PREP
Duplicate (OF28001-DUPI) Prepared & Analyzed: 06/28/2020 10: 10
Source: CD07944-02
Spike Source %REC RPD
Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes
Total Solids 2.1 0.0010 % by Weight 2.1 0.6 25
Batch 0GO2010 - Same
Blank (OG02010-BLK3) Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:31
Spike Source %REC
RPD
Anala
Result Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
2.6 U
7.2
mg/kg wet
LCS (OG02010-BSI)
Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:32
Spike Source %REC
RPD
Anala
Result Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
120
8.0
mg/kg wet
126 92 80-120
FINAL
This report relates only to the sample
as received by the laboratory, and may only be reproduced in full.
Page 11 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0GO2010 - Same - Continued
Matrix Spike (OG02010-MSI)
Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:34
Source: CD07944-02
Spike Source a/oREC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
20000
D
1800
mg/kg dry
2250 16000 146 80-120
QM-07
Matrix Spike Dup (OG02010-MSDI)
Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:35
Source: CD07944-02
Spike Source %REC
RPD
Analvte
Result
Flao
Q
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
19000
D
1800
mg/kg dry
2350 16000 97 80-120 5
25
Batch 0GO2011 - Same
Blank (OG02011-BLKI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:19
Spike Source %REC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 32 U 35 mg/kg wet
LCS (OG02011-BSI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:21
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
990
38
mg/kg wet
946
104
90-110
Matrix Spike (OG02011-MSI)
Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:24
Source: CD07944-02
Spike
Source
%REC
RPD
Analvte
Result
Flao
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
63000
1800
mg/kg dry
16800
49000
87
90-110
QM-07
Matrix Spike Dup (OG02011-MSDI)
Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:26
Source: CD07944-02
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
65000
1800
mg/kg dry
17600
49000
93
90-110 3
10
Batch OG31023 - Same
LCS (OG31023-BSI) Prepared & Analyzed: 07/31/2020 11:15
Spike Source %REC
RPD
Analvte Result Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
pH 6.9
1.0
pH Units
7.00 99 99-101
Duplicate (OG31023-DUP3)
Prepared & Analyzed: 07/31/2020 11:15
Source: CD11905-01
Spike Source %REC
RPD
Analvte Result Flao
Q
Units
Level Result %REC Limits RPD
Limit Notes
pH 5.4
1.0
pH Units
5.4 0.7
25
TCLP Volatile Organics by GCMS - Quality Control
Batch 0GO1040 - EPA 5030E MS
Blank (OG01040-BLKI)
Prepared: 07/01/2020 13:17 Analyzed: 07/02/2020 00:02
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 23

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch 0GO1O4O - EPA 5030E MS - Continued
Blank (OG01040-BLKI) Continued Prepared: 07/O1/2020 13:17 Analyzed: 07/02/2020 00:02
Analyte
Result
Flaa
Q
Units
1,1-Dichloroethene
0.00094
U
0.0010
mg/L
1,2-Dichloroethane
0.00063
U
0.0010
mg/L
2-Butanone
0.0045
U
0.0050
mg/L
Benzene
0.00071
U
0.0010
mg/L
Carbon Tetrachloride
0.00094
U
0.0010
mg/L
Chlorobenzene
0.00072
U
0.0010
mg/L
Chloroform
0.00080
U
0.0010
mg/L
Tetrachloroethene
0.00076
U
0.0010
mg/L
Trichloroethene
0.00089
U
0.0010
mg/L
Vinyl chloride
0.00071
U
0.0010
mg/L
Spike Source a/oREC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 0.054
m91L
0.0500 108 41-142
Dibromofluoromethane 0.057
m91L
0.0500 114 53-146
Toluene-d8 0.053
m91L
0.0500 107 41-146
Blank (OG01040-BLK2)
Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 23:31
Spike
Source
%REC RPD
Analvte
Result
FFF`lau
Q
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.094
UD
0.10
mg/L
1,2-Dichloroethane
0.063
UD
0.10
mg/L
2-Butanone
0.45
UD
0.50
mg/L
Benzene
0.071
UD
0.10
mg/L
Carbon Tetrachloride
0.094
UD
0.10
mg/L
Chlorobenzene
0.072
UD
0.10
mg/L
Chloroform
0.080
UD
0.10
mg/L
Tetrachloroethene
0.076
UD
0.10
mg/L
Trichloroethene
0.089
UD
0.10
mg/L
Vinyl chloride
0.071
UD
0.10
mg/L
4-Bromofluorobenzene
0.054
m91L
0.0500
108
41-142
Dibromofluoromethane
0.054
m91L
0.0500
109
53-146
Toluene-d8
0.056
m91L
0.0500
113
41-146
LCS (OG01040-BSI)
Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:26
Spike
Source
%REC RPD
Analvte
Result
Flao Q
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.0080
0.0010
mg/L
0.0100
80
47-139
Benzene
0.0096
0.0010
mg/L
0.0100
96
56-136
Chlorobenzene
0.010
0.0010
mg/L
0.0100
100
51-139
Trichloroethene
0.0092
0.0010
mg/L
0.0100
92
62-135
4-Bromofluorobenzene
0.055
m91L
0.0500
111
41-142
Dibromofluoromethane
0.056
m91L
0.0500
113
53-146
Toluene-d8
0.055
m91L
0.0500
111
41-146
Matrix Spike (OG01040-MSI)
Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:57
Source: CD07944-01
Spike
Source
%REC RPD
Analvte
Result Flao Q
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
1.8 0.10
mg/L
2.00
0.094 U
91
47-139
Benzene
2.1 0.10
mg/L
2.00
0.071 U
103
56-136
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 23

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch 0GO1O4O - EPA 5030E MS - Continued
Matrix Spike (OG03040-MS3) Continued Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:57
Source: CD07944-01
Spike
Source
a/o RE
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Chlorobenzene
2.1
0.10
mg/L
2.00
0.072 U
104
51-139
Trichloroethene
2.1
0.10
mg/L
2.00
0.089 U
103
62-135
4-Bromofluorobenzene
5.4
m91L
5.00
109
41-142
Dibromofluoromethane
5.5
m91L
5.00
110
53-146
Toluene-d8
5.4
m91L
5.00
108
41-146
Matrix Spike Dup (OG01040-MSDI)
Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 22:28
Source: CD07944-01
Spike
Source
%REC
RPD
Anala
Result
Flag
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
1.7
0.10
mg/L
2.00
0.094 U
87
47-139
4
16
Benzene
2.0
0.10
mg/L
2.00
0.071 U
102
56-136
0.8
14
Chlorobenzene
2.2
0.10
mg/L
2.00
0.072 U
112
51-139
7
13
Trichloroethene
2.1
0.10
mg/L
2.00
0.089 U
107
62-135
4
20
4-Bromofluorobenzene
5.7
m91L
5.00
114
41-142
Dibromofluoromethane
5.6
m91L
5.00
112
53-146
Toluene-d8
5.5
m91L
5.00
111
41-146
TCLP Semivolatile Organics by GCMS - Quality Control
Batch 0GO1O36 - EPA 351OC MS
Blank (OG01036-BLK3)
Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 12:49
Spike
Source
%REC
RPD
Analvte
Result
Flag
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,4-Dichlorobenzene
0.0006
U
0.002
mg/L
2,4,5-Trichlorophenol
0.0008
U
0.002
mg/L
2,4,6-Trichlorophenol
0.001
U
0.002
mg/L
2,4-Dinitrotoluene
0.0006
U
0.002
mg/L
2-Methylphenol
0.0007
U
0.002
mg/L
3 & 4-Methylphenol
0.002
U
0.002
mg/L
Hexachlorobenzene
0.0006
U
0.002
mg/L
Hexachlorobutadiene
0.0008
U
0.002
mg/L
Hexachloroethane
0.0006
U
0.002
mg/L
Nitrobenzene
0.0006
U
0.002
mg/L
Pentachlorophenol
0.002
U
0.002
mg/L
Pyridine
0.0007
U
0.002
mg/L
2,4,6-Tribromophenol
0.037
m91L
0.0500
74
33-145
2-Fluorobiphenyl
0.042
m91L
0.0500
84
32-116
2-Fluorophenol
0.031
m91L
0.0500
63
11-100
Nitrobenzene-d5
0.040
m91L
0.0500
80
24-107
Phenol-d5
0.021
m91L
0.0500
43
10-100
Terphenyl-d14
0.046
m91L
0.0500
92
52-150
Blank (OG01036-BLK2)
Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 13:19
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
1,4-Dichlorobenzene 0.003 U 0.01 mg/L
2,4,5-Trichlorophenol 0.004 U 0.01 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 23

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch 0GO1O36 - EPA 351OC MS - Continued
Blank (OG01036-BLK2) Continued Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 13:19
Anala
Result
Flaa
Q
Units
2,4,6-Trichlorophenol
0.006
U
0.01
mg/L
2,4-Dinitrotoluene
0.003
U
0.01
mg/L
2-Methylphenol
0.004
U
0.01
mg/L
3 & 4-Methylphenol
0.008
U
0.01
mg/L
Hexachlorobenzene
0.003
U
0.01
mg/L
Hexachlorobutadiene
0.004
U
0.01
mg/L
Hexachloroethane
0.003
U
0.01
mg/L
Nitrobenzene
0.003
U
0.01
mg/L
Pentachlorophenol
0.008
U
0.01
mg/L
Pyridine
0.004
U
0.01
mg/L
Spike Source a/o REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
0.14
m91L
0.250
54
33-145
2-Fluorobiphenyl
0.13
m91L
0.250
51
32-116
2-Fluorophenol
0.098
m91L
0.250
39
11-100
Nitrobenzene-d5
0.12
m91L
0.250
47
24-107
Phenol-d5
0.069
m91L
0.250
28
10-100
Terphenyl-d14
0.24
m91L
0.250
97
52-150
Blank (OG01036-BLK3)
Prepared: 07/02/2020 10:30 Analyzed: 07/06/2020 13:49
Analvte
Result
Flao
Q
Units
1,4-Dichlorobenzene
0.0006
U
0.002
mg/L
2,4,5-Trichlorophenol
0.0008
U
0.002
mg/L
2,4,6-Trichlorophenol
0.001
U
0.002
mg/L
2,4-Dinitrotoluene
0.0006
U
0.002
mg/L
2-Methylphenol
0.0007
U
0.002
mg/L
3 & 4-Methylphenol
0.002
U
0.002
mg/L
Hexachlorobenzene
0.0006
U
0.002
mg/L
Hexachlorobutadiene
0.0008
U
0.002
mg/L
Hexachloroethane
0.0006
U
0.002
mg/L
Nitrobenzene
0.0006
Ll
0.002
mg/L
Pentachlorophenol
0.002
U
0.002
mg/L
Pyridine
0.0007
U
0.002
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
0.041
m91L
0.0500
82
33-145
2-Fluorobiphenyl
0.046
m91L
0.0500
93
32-116
2-Fluorophenol
0.035
m91L
0.0500
70
11-100
Nitrobenzene-d5
0.046
m91L
0.0500
91
24-107
Phenol-d5
0.025
m91L
0.0500
50
10-100
Terphenyl-d14
0.051
m91L
0.0500
102
52-150
LCS (OG03036-BSI)
Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 14:19
Spike
Source
%REC RPD
Analvte
Result Flaa Q
Units
Level
Result %REC
Limits RPD Limit Notes
1,4-Dichlorobenzene
0.04 0.002
mg/L
0.0500
76
10-101
Pentachlorophenol
0.03 0.002
mg/L
0.0500
50
5-139
2,4,6-Tribromophenol
0.035
m91L
0.0500
70
33-145
2-Fluorobiphenyl
0.043
m91L
0.0500
86
32-116
2-Fluorophenol
0.031
m91L
0.0500
62
11-100
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 23

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch 0GO1O36 - EPA 351OC MS - Continued
LCS (OG01036-BSI) Continued Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 14:19
Spike Source a/o RE RPD
Anal a
Result Flaa Q
Units
Level Result %REC Limits RPD Limit Notes
Nitrobenzene-d5
0.038
m91L
0.0500 75 24-107
Phenol-d5
0.024
m91L
0.0500 48 10-100
Terphenyl-d14
0.039
m91L
0.0500 78 52-150
Matrix Spike (OG03036-MS1)
Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 14:50
Source: AD04219-01
Spike
Source
%REC RPD
Analvte
Result Flao Q Units
Level
Result
%REC Limits RPD Limit Notes
1,4-Dichlorobenzene
0.19 D 0.05 mg/L
0.250
0.02 U
76 10-101
Pentachlorophenol
0.06 D 0.05 mg/L
0.250
0.04 U
25 5-139
2,4,6-Tribromophenol
0.14
m91L
0.250
58
33-145
2-Fluorobiphenyl
0.21
m91L
0.250
84
32-116
2-Fluorophenol
0.14
m91L
0.250
55
11-100
Nitrobenzene-d5
0.17
m91L
0.250
68
24-107
Phenol-d5
0.10
m91L
0.250
42
10-100
Terphenyl-d14
0.20
m91L
0.250
81
52-150
Matrix Spike Dup (OG01036-MSDI)
Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 15:20
Source: AD04219-01
Spike
Source
%REC
RPD
Analvte
Result Flao POLL Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dichlorobenzene
0.22 D 0.05 mg/L
0.250
0.02 U
87 10-101 13
18
Pentachlorophenol
0.07 D 0.05 mg/L
0.250
0.04 U
26 5-139 5
23
2,4,6-Tribromophenol 0.15
m91L
0.250
60
33-145
2-Fluorobiphenyl 0.23
m91L
0.250
91
32-116
2-Fluorophenol 0.15
m91L
0.250
61
11-100
Nitrobenzene-d5 0.19
m91L
0.250
74
24-107
Phenol-d5 0.11
m91L
0.250
45
10-100
Terphenyl-d14 0.20
m91L
0.250
82
52-150
TCLP Pesticides by GC - Quality Control
Batch 0GO1O25 - EPA 351OC
Blank (OG01025-BLKI) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:22
Anala
Result
Flao
POLL
Units
Chlordane (tech)
0.000072
U
0.00010
mg/L
Endrin
2.8E-6
U
0.000010
mg/L
gamma-BHC
4.2E-6
U
0.000010
mg/L
Heptachlor
5.2E-6
U
0.000010
mg/L
Heptachlor epoxide
3.6E-6
U
0.000010
mg/L
Methoxychlor
4.0E-6
U
0.000010
mg/L
Toxaphene
0.000096
U
0.00010
mg/L
2,4,5,E-TCMX
Decachlorobiphenyl
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
0.00066 m91L 0.00100
0.00070 m91L 0.00100
66 38-142
70 34-159
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 23

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QUALITY CONTROL DATA
TCLP Pesticides by GC - Quality Control
Batch 0GO1025 - EPA 3510C - Continued
Blank (OG01025-BLK2)
Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:35
Spike Source
a/oREC
RPD
Anala
Result
Flaa
Q
Units
Level Result
%REC Limits RPD
Limit
Notes
Chlordane (tech)
0.00036
U
0.00050
mg/L
Endrin
0.000014
U
0.000050
mg/L
gamma-BHC
0.000021
U
0.000050
mg/L
Heptachlor
0.000026
U
0.000050
mg/L
Heptachlor epoxide
0.000018
U
0.000050
mg/L
Methoxychlor
0.000020
U
0.000050
mg/L
Toxaphene
0.00048
U
0.00050
mg/L
2,4,5,E-TCMX
0.0034
m91L
0.00500
67 38-142
Decachlorobiphenyl
0.0034
m91L
0.00500
69 34-159
Blank (OG01025-BLK3)
Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:48
Spike Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level Result
%REC Limits RPD
Limit
Notes
Chlordane (tech)
0.00036
U
0.00050
mg/L
Endrin
0.000014
U
0.000050
mg/L
gamma-BHC
0.000021
U
0.000050
mg/L
Heptachlor
0.000026
U
0.000050
mg/L
Heptachlor epoxide
0.000018
U
0.000050
mg/L
Methoxychlor
0.000020
U
0.000050
mg/L
Toxaphene
0.00048
U
0.00050
mg/L
2,4,5,E-TCMX
0.0038
m91L
0.00500
76 38-142
Decachlorobiphenyl
0.0025
m91L
0.00500
50 34-159
Blank (OG01025-BLK4)
Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:00
Spike Source
%REC
RPD
Anala
Result
Flao
Q
Units
Level Result
%REC Limits RPD
Limit
Notes
Chlordane (tech)
0.00036
U
0.00050
mg/L
Endrin
0.000014
U
0.000050
mg/L
gamma-BHC
0.000021
U
0.000050
mg/L
Heptachlor
0.000026
U
0.000050
mg/L
Heptachlor epoxide
0.000018
U
0.000050
mg/L
Methoxychlor
0.000020
U
0.000050
mg/L
Toxaphene
0.00048
U
0.00050
mg/L
2,4,5,E-TCMX
0.0038
m91L
0.00500
77 38-142
Decachlorobiphenyl
0.0027
m91L
0.00500
54 34-159
Blank (OG01025-BLKS)
Prepared: 07/02/2020 09:30 Analyzed: 07/07/2020 12:12
Spike Source
%REC
RPD
Analvte
Result
Flao
Q
Units
Level Result
%REC Limits RPD
Limit
Notes
Chlordane (tech)
0.000072
U
0.00010
mg/L
Endrin
2.8E-6
U
0.000010
mg/L
gamma-BHC
4.2E-6
U
0.000010
mg/L
Heptachlor
5.2E-6
U
0.000010
mg/L
Heptachlor epoxide
3.6E-6
U
0.000010
mg/L
Methoxychlor
4.0E-6
U
0.000010
mg/L
Toxaphene
0.000096
U
0.00010
mg/L
2,4,5,E-TCMX
0.00075
m91L
0.00100
75 38-142
FINAL
This report relates only to the sample as
received by the
laboratory, and may only be
reproduced in full.
Page 17 of 23

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QUALITY CONTROL DATA
TCLP Pesticides by GC - Quality Control
Batch 0GO1025 - EPA 3510C - Continued
Blank (OG01025-BLKS) Continued Prepared: 07/02/2020 09:30 Analyzed: 07/07/2020 12:12
Spike Source a/o RE RPD
Anal a Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Decachlorobiphenyl 0.00054 m91L 0.00100 54 34-159
LCS (OG03025-BSI) Prepared: 07/01/2020 11:20 Analyzed: 07/07/2020 12:25
Spike Source %REC RPD
Analvte Result FFF`lao Q Units Level Result %REC Limits RPD Limit Notes
Endrin 0.00089 0.000010 mg/L 0.00100 89 28-143
2,4,5,E-TCMX
0.00076
m91L
0.00100
76
38-142
Decachlorobiphenyl
0.00083
m91L
0.00100
83
34-159
Matrix Spike (OG01025-MS3)
Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:37
Source: AD03718-02
Spike
Source
%REC
RPD
Analvte
Result
FFF`lau Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Endrin
0.0014
0.000010
mg/L
0.00100
2.8E-6 U
135
28-143
2,4,5,E-TCMX
0.00095
m91L
0.00100
95
38-142
Decachlorobiphenyl
0.0010
m91L
0.00100
103
34-159
Matrix Spike Dup (OG03025-MSDI)
Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:49
Source: AD03718-02
Spike
Source
%REC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Endrin
0.0011
0.000010
mg/L
0.00100
2.8E-6 U
111
28-143 20
22
2,4,5,E-TCMX 0.00077 m91L 0.00100 77 38-142
Decachlorobiphenyl 0.00088 m91L 0.00100 88 34-159
TCLP Herbicides by GC - Quality Control
Batch 0GO2006 - EPA 3510C
Blank (OG02006-BLKI) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 16:27
Spike Source %REC RPD
Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes
2,4,5-TP (Silvex) 0.000088 U 0.00010 mg/L
2,4-D 0.000054 U 0.00010 mg/L
2,4-DC4A
0.0017
m91L
0.00200 87 37-134
Blank (OG02006-BLK2)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 16:52
Spike Source %REC RPD
Analvte
Result FFF`lao Q
Units
Level Result %REC Limits RPD Limit Notes
2,4,5-TP (Silvex)
0.00044 U 0.00050
mg/L
2,4-D
0.00027 U 0.00050
mg/L
2,4-DC4A
0.0072
m91L
0.0100 72 37-134
Blank (OG02006-BLK3)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:17
Spike Source %REC RPD
Anala
Result Flaa Q
Units
Level Result %REC Limits RPD Limit Notes
2,4,5-TP (Silvex)
0.00044 U 0.00050
mg/L
2,4-D
0.00027 U 0.00050
mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 23

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QUALITY CONTROL DATA
TCLP Herbicides by GC - Quality Control
Batch 0GO2006 - EPA 3510C - Continued
Blank (OG02006-BLK3) Continued Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:17
Spike Source a/o RE
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit Notes
2,4-DC4A
0.0066
m9/L
0.0100 66 37-134
Blank (OG02006-BLK4)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:42
Spike Source %REC
RPD
Analvte
Result
FFF`lau
Q
Units
Level Result %REC Limits RPD
Limit Notes
2,4,5-TP (Silvex)
0.00044
U
0.00050
mg/L
2,4-D
0.00027
U
0.00050
mg/L
2,4-DC4A 0.0086 m9/L 0.0100 86 37-134
LCS (OG02006-BSI) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:07
Spike Source %REC RPD
Analvte
Result Flao Q
Units
Level Result %REC Limits RPD Limit Notes
2,4,5-TP (Silvex)
0.0024 0.00010
mg/L
0.00200 122 24-135
2,4-D
0.0022 P 0.00010
mg/L
0.00200 111 20-134
2,4-DC4A
0.0018
m9/L
0.00200 88 37-134
Matrix Spike (OG02006-MS3)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:32
Source: AD04272-03
Spike
Source
%REC RPD
Anala
Result Flaa Q Units
Level
Result %REC
Limits RPD Limit Notes
2,4,5-TP (Silvex)
0.0022 0.00010 mg/L
0.00200
0.000088 U 108
24-135
2,4-D
0.0022 P 0.00010 mg/L
0.00200
0.000054 U 108
20-134
2,4-DC4A
0.0018
m9/L
0.00200 88 37-134
Matrix Spike (OG02006-MS2)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 19:48
Source: AD04158-01
Spike Source %REC RPD
Anala
Result Flaa Q
Units
Level Result %REC Limits RPD Limit Notes
2,4,5-TP (Silvex)
0.0096 0.00050
mg/L
0.0100 0.00044 U 97 24-135
2,4-D
0.0084 0.00050
mg/L
0.0100 0.00027 U 84 20-134
2,4-DC4A
0.0078
m9/L
0.0100 78 37-134
Matrix Spike Dup (OG02006-MSD3)
Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:57
Source: AD04272-03
Analvte
2,4,5-TP (Silvex)
2,4-D
Result Flao 2
0.0021 0.00010
0.0018 P 0.00010
Units
mg/L
mg/L
Spike
Level
0.00200
0.00200
Source
Result
0.000088 U
0.000054 U
%REC
104
88
%REC
Limits RPD
24-135 5
20-134 20
RPD
Limit Notes
19
19 QM-11
2,4-DC4A
0.0017
m9/L
0.00200
83
37-134
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 0GO1019 - EPA 7470A
Blank (OG01019-BLKI)
Prepared: 07/O1/2020 12:07 Analyzed: 07/02/2020 09:42
Anale
Mercury
Spike Source %REC RPD
Result Flaa Q Units Level Result %REC Limits RPD Limit
2.30E-5 U 0.000200 mg/L
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 23

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 0GO1019 - EPA 7470A - Continued
Blank (OG01019-BLK2) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:45
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
Blank (OG01019-BLK3) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:48
Spike Source %REC RPD
Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
LCS (OG01019-BSI) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:57
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.00536
0.000200
mg/L
0.00500
107
80-120
Matrix Spike (OG01019-MSI)
Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 10:03
Source: AD04219-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0537
0.00200
mg/L
0.0500
0.000230 U
107
75-125
Matrix Spike Dup (OG01019-MSDI)
Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 10:07
Source: AD04219-01
Spike
Source
%REC
RPD
Analvte
Result
FFF`lau
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0553
0.00200
mg/L
0.0500
0.000230 U
111
75-125 3
20
Classical Chemistry Parameters - Quality Control
Batch 0GO7010 - NO PREP
Blank (OG07010-BLKI) Prepared: 07/07/2020 08:30 Analyzed: 07/07/2020 16:00
Spike Source %REC RPD
Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes
Reactive Cyanide 250 U 250 mg/L
LCS (OG07010-BSI) Prepared: 07/07/2020 10:45 Analyzed: 07/07/2020 16:00
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Reactive Cyanide
47
UD
6200
mg/L
99.9
47 22-100
Duplicate (OG07010-DUPI)
Prepared: 07/07/2020 09:15 Analyzed: 07/07/2020 16:00
Source: CD07944-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Reactive Cyanide
250
U
250
mg/L
250 U
30
Batch 0GO8018 - NO PREP
Blank (OG08018-BLKI) Prepared: 07/07/2020 08:30 Analyzed: 07/07/2020 17:00
Spike Source %REC RPD
Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes
Reactive Sulfide 500 U 500 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 23

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0GO8018 - NO PREP - Continued
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LCS (01308018-13SI) Prepared: 07/07/2020 10:45 Analyzed: 07/07/2020 17:00
Spike
Source
a/oREC
RPD
Anala
Result Flaa
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Reactive Sulfide
210 U
500
mg/L
249
84 50-150
Duplicate (01308018-DUPI)
Prepared: 07/07/2020 09:15 Analyzed: 07/07/2020 17:00
Source: CD07944-01
Spike
Source
%REC
RPD
Analvte
Result Flaa
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Reactive Sulfide
500 U
500
mg/L
500 U
30
Classical Chemistry Parameters - Quality Control
Batch 0GO2008 - NO PREP
Duplicate (OG02008-DUP3) Prepared: 07/02/2020 15:00 Analyzed: 07/02/2020 16:10
Source: CD07944-01
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Flashpoint > 200 U OF > 200 5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 23

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
J-01 Result may be biased high due to positive results in the associated method blank at a concentration above
the MDL and/or greater than one-half the MRL.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 23

14 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
ri �� 10775 Central Pori Dr. 4810 Executive Park Court, Suite 111 102-A Woodwmds !ndusrrial Ct.
CCE Nk"Orlando, F432824 Jacksonville, FL 32216-6069 Cary- NC 27511
[phone] (9W) 296-3007 Fax [phone] .r67.3090 Fax (919j 467-3515 Page Of
Client Name Project Number Requested Analyses Requested Turnaround
Hunt Environmental Associates HU017) Finmel z < Times
Address PTo)ect Name[Desc Q r j Note : Rush requests subject tb
3330 Saddletree Road. Ci of Lumberton �m m > co� acceptance by the Facil{Sy
City/STMp PO #! Billing Info U
Lumberton, NC 28360 T X ~ ��, Standard
Tel Fax Reporting Contact$ I� l 0
$ d Ci. U)
(9'10) 738-5311 Jordan Davis �� a � � � U c� �rA " o m _ Expedited
5 mpler(s) Name, Affiliation (Print) Biling Contact - a a (� u Q �
� 1 X N Cody Hunt if'A r T- F- m O E � a � x Due / 1
mplerls) Sign Site Location Dime zone jig T- r .- pp ti C t O Lab 1NoTkorder
M c7 O N cta
La,r r oD CYJ Q 0it IL Z T+Qfj�Q �
Preservation (See CodesJ (Combine as necessary) �J 0 �}�}
Collection Matrix ToW A of
Hem # Sample ID (Fie?d idant)lication) Collection Dale
n T!me omp! rab (see codes) Containers Sample Comments
WW-1 ') v �1 t WW 10 X X X X X X
WW-2 SL 4 X X X
< Total # of Containers
Sample Kit Prepared By
Date ime
Rolinqui ad By
DateMme
Rem
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DateMme
-
UzY1 J, 9 `
11.E-�awe�,-
Comments/Special RepotbKgTlig0roments I
R quished By
Daternme
c ' ed By
Da Ime
Relinquished By
DateRme
Received By
DatelTime
Cooler #'s & Temps on Receipt
!3
Cendition Upon Receipt
Acceptable Unacceptable
Matrix . GW-Groundwa!er SO-Soit 1]W-Drinking Water SE -Sediment SW -Surface Water INW-Waslewater A -Air 0.01her (detail in comments) Preservation: )-Ice H-HCl N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in commentg)
Note: All Samples submitted to );NCO Labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.coml
CO 13775 Central Port Dr. 4810 Executive Park Court. Suite 111 102-A Woodwinds lndustdal Ct.
Orlando, FL 32824 Jacksonville- FL 32216-6060 Cary. NO 27511
(Um(407) 826-5314 [phone] Fax [phone] [phone] Fax [phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
Hunt Environmental Associates HU017 none Times
Address Project Name/Desc Note: Rush requests subject to
(L acceplance by the facility
3330 Saddletree Road_ Ci of Lumberton(
City/STrZip PC it i Billing talo l '
Lumberton, NC 28360 C F Standard
Tel Fax Reporting Contact F d
[phone] Jordan Davis � �a _ Expedited
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Sampler(s) Name, Affiliation (Print) Billing Contact - C'V d F
(� G�I('i Cody Hunt a ta 4 Due / 1
samplers) signature Site Location / Time Zane , d J Lab Workorcier
U d" U
C ❑07 {] /t /(
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Collection Matrix Total # of
Item # Sample ID (Field identification) Collection Date jj-F�t amp / Grai] (see codes) Containers Sample Comments
WW-1 2 `1� WW 10 X X X
WW-2 St_ A
c Total # of Containers
Sample Kit Prepared By
Oates imle
/J
Relin ished By
i
Dateir7i fm�e 7�
Recei d By Dat
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quished By
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Condition Upon Receipt
[,
-A Acceptable Unacceptable
Matrix : GW-Groundwater SO -Sail DIN -Drinking Water SE -Sediment SW -Surface Water WW-Waslewater A -Air O-Other (detail in comments) Preservation: t-Ice H-HCi N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments)
Note : All samples submitted to ENCO labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Cameron Testing Services, Inc. Laboratory Report
Client; Enviro- hoice Recycling CTS Pro],
Project: City of Lumberton Requiatory
Sample Information
sampled Date 0612 + Q Receiv4ct
Analyses and Results
00-'I 0
M. S:ms
Lab ID Saillple I - E {A y = m
r �o 0 Analyte Result
J ro e O
NC DEN #654
NC PHHS #3779�
US EPA #NCol 918
pato 06123120
.: Std. Moth ods
Reference
2006-21 0 -
_1,d;c a Fac. Coliforrn,S <46700
crUeg
46700 06f24!20 RL 92220 - NI
-
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CFU9
46600
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46600
CFW9
46600
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<46500
CFU19
+46500
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<48700
CFwo
4VO
-7
<461DOO
ORNg
46900
Geomean 54600
2006- 10 -1
31vd¢t Gr TS {561 2.14%
D.DT DFW24120 RL 2540 G -T
-2
2.14%
n.oi
-3
2.14%
0.01
-4
.15%
0.01
-5
2.15%
o.oi
0
_14 %
a.m
Report
PeifiE'YV - 9�-
4� ProjectNlanager --6s
219 S. Steele Sir.
Sanford NC 27330 919-208-424,a
eh r is ray o amrnon r es to ng _ c Dora

219 S_ Sleaze Str.
Sanhad. NC 27330
Phone - 919-208-4240
Cameron Testing Services, inc_
NC Wb`1 GVd CPr1 0654 NC PHHS Cart 4 �7799 US EPA NC019Ta
Chain of Custody
Page of
05mpany
Contact,
Address {Clip,
State_ Zip}
Proyect
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Signature
Sample Information
Number of bottles * preservative
Required TestinglAnalysis
t1l1@Llt Sample
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ENCO Laboratories
9g
Accurate, Timely. Responsive. Iuuovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, September 22, 2020
Hunt Environmental Associates (HU017)
Attn: Jordan Davis
3330 Saddletree Road.
Lumberton, NC 28360
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: City of Lumberton
ENCO Workorder(s): CD11817
Dear Jordan Davis,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, September 10, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OLdcc-'----�A
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

PROJECT NARRATIVE
Client: Hunt Environmental Associates (HU017)
Project: City of Lumberton
Lab ID: CD11817
Overview
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Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods
referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in
the QC Remarks section below.
Quality Control Samples
No Comments
Quality Control Remarks
No Comments
Other Comments
The Plant Available Nitrogen (PAN) has been calculated as 3300 mg/Kg.
The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any
exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of
the report.
Released By:
Environmental Conservation Laboratories, Inc.
Chuck Smith
Project Manager
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: WW-1
Lab ID: CD11817-01
Sampled: 09/10/20 10:30
Received: 09/10/20 13:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC 9056A
WETS-88 Soil
06/06/23
09/18/20 15:26
09/18/20 15:26
Leaching
EPA 351.2
Same
10/08/20
09/14/20 10:00
09/17/20 11:22
EPA 365.4
Same
10/08/20
09/14/20 10:00
09/17/20 12:55
EPA 6010D
EPA 3050B
03/09/21
09/11/20 11:09
09/14/20 13:06
EPA 7471B
EPA 7471B
10/08/20
09/15/20 11:39
09/15/20 16:55
EPA 9045D
Same
09/21/20 14:25
09/21/20 14:11
09/21/20 15:36
EPA 9056A
WETS-88 Soil
09/13/20 09/13/20
09:21 09/11/20 09:21
09/11/20 19:43
Leaching
SM 254OG-2011
NO PREP
09/17/20
09/15/20 18:25
09/15/20 18:25
Client ID: WW-1
Lab ID: CD11817-01RE1
Sampled: 09/10/20 10:30
Received: 09/10/20 13:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 350.1
WETS-88 Soil
10/08/20 10/09/20
09/11/20 11:50
09/15/20 15:34
Leaching
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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SAMPLE DETECTION SUMMARY
Client ID: WW-1
Lab ID:
CD11817-01
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Aluminum - Total
11900
11.9
56.8
mg/kg dry
EPA 6010D
Cadmium - Total
0.325
0.0545
0.284
mg/kg dry
EPA 6010D
Calcium - Total
6450
31.8
142
mg/kg dry
EPA 6010D
Chromium - Total
108
0.568
2.84
mg/kg dry
EPA 6010D
Copper - Total
336
1.08
2.84
mg/kg dry
EPA 6010D
Lead - Total
9.79
0.682
2.84
mg/kg dry
EPA 6010D
Magnesium - Total
1030
5.28
142
mg/kg dry
EPA 6010D
Molybdenum - Total
3.50
0.568
2.84
mg/kg dry
EPA 6010D
Nickel - Total
18.6
2.04
14.2
mg/kg dry
EPA 6010D
pH
7.4
1.0
1.0
pH Units
EPA 9045D
Q-01
Phosphorus
5100
D
160
450
mg/kg dry
EPA 365.4
Potassium - Total
802
22.7
142
mg/kg dry
EPA 6010D
Sodium - Total
2880
34.1
142
mg/kg dry
EPA 6010D
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-01
Total Kjeldahl Nitrogen
11000
D
2000
2200
mg/kg dry
EPA 351.2
Total Solids
3.4
0.0010
0.0010
% by Weight
SM 2540G-2011
Zinc - Total
433
6.25
14.2
mg/kg dry
EPA 6010D
Client ID: WW-1
Lab ID:
CD11817-01RE1
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Ammonia as N
2500
D
130
290
mg/kg dry
EPA 350.1
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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ANALYTICAL RESULTS
Description: WW-1 Lab Sample ID: CD11817-01 Received: 09/10/20 13:00
Matrix: Sludge Sampled:09/10/20 10:30 Work Order: CD11817
Project: City of Lumberton Sampled By:Carrigan Harris % Solids: 17.60
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
11900
mg/kg dry
1
11.9
56.8
0111019
EPA 6010D
09/14/20 13:06
JDH
Arsenic [7440-38-2]^
1.82
U
mg/kg dry
1
1.82
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Cadmium [7440-43-9]1
0.325
mg/kg dry
1
0.0545
0.284
0111019
EPA 6010D
09/14/20 13:06
JDH
Calcium [7440-70-2]1
6450
mg/kg dry
1
31.8
142
0111019
EPA 6010D
09/14/20 13:06
JDH
Chromium [7440-47-3]1
108
mg/kg dry
1
0.568
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Copper [7440-50-8]^
336
mg/kg dry
1
1.08
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Lead [7439-92-1]^
9.79
mg/kg dry
1
0.682
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Magnesium [7439-95-4]^
1030
mg/kg dry
1
5.28
142
0111019
EPA 6010D
09/14/20 13:06
JDH
Mercury [7439-97-6]^
0.261
U
mg/kg dry
1
0.261
0.350
0115024
EPA 7471B
09/15/20 16:55
KAH
Molybdenum [7439-98-7]^
3.50
mg/kg dry
1
0.568
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Nickel [7440-02-0]^
18.6
mg/kg dry
1
2.04
14.2
0111019
EPA 6010D
09/14/20 13:06
JDH
Potassium [7440-09-7]^
802
mg/kg dry
1
22.7
142
0111019
EPA 6010D
09/14/20 13:06
JDH
Selenium [7782-49-2]^
2.33
U
mg/kg dry
1
2.33
2.84
0111019
EPA 6010D
09/14/20 13:06
JDH
Sodium [7440-23-5]^
2880
mg/kg dry
1
34.1
142
0111019
EPA 6010D
09/14/20 13:06
JDH
Zinc [7440-66-6]1
433
mg/kg dry
1
6.25
14.2
0111019
EPA 6010D
09/14/20 13:06
JDH
Classical Chemistry Parameters
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
2
Batch
Method
Analyzed
By
Notes
Ammonia as N [7664-41-7]
2500
D
mg/kg dry
51.43
130
290
0115020
EPA 350.1
09/15/20 15:34
JAH
Nitrate as N [14797-55-8]
12
U
mg/kg dry
1
12
57
0111008
EPA 9056A
09/11/20 19:43
LK
QB-02,
QL-01
Nitrate/Nitrite as N
1.2
U
mg/kg dry
1
1.2
2.8
0117039
CALC 9056A
09/18/20 15:26
LJI
Nitrite as N [14797-65-0]
0.45
U
mg/kg dry
1
0.45
5.7
0111008
EPA 9056A
09/11/20 19:43
LK
QB-02,
QL-01
pH
7.4
pH Units
1
1.0
1.0
0121023
EPA 9045D
09/21/20 15:36
DMJ
Q-01
Phosphorus [7723-14-0]
5100
D
mg/kg dry
10
160
450
0114005
EPA 365.4
09/17/20 12:55
JAH
Temperature for pH (deg. C)
23
pH Units
1
0121023
EPA 9045D
09/21/20 15:36
DMJ
Q-01
Total Kjeldahl Nitrogen
11000
D
mg/kg dry
10
2000
2200
0114006
EPA 351.2
09/17/20 11:22
JAH
Total Solids
3.4
% by Weight
1
0.0010
0.0010
0115034
SM 254OG-2011
09/15/20 18:25
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0111019 - EPA 3050E
Blank (0I33019-BLKI) Prepared: 09/11/2020 11:09 Analyzed: 09/14/2020 12:44
Spike Source a/oREC RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
2.10
U
10.0
mg/kg wet
Arsenic
0.320
U
0.500
mg/kg wet
Cadmium
0.00960
U
0.0500
mg/kg wet
Calcium
11.2
1
25.0
mg/kg wet
Chromium
0.100
U
0.500
mg/kg wet
Copper
0.190
U
0.500
mg/kg wet
Lead
0.120
U
0.500
mg/kg wet
Magnesium
0.930
U
25.0
mg/kg wet
Molybdenum
0.100
U
0.500
mg/kg wet
Nickel
0.360
U
2.50
mg/kg wet
Potassium
4.00
U
25.0
mg/kg wet
Selenium
0.410
U
0.500
mg/kg wet
Sodium
6.00
U
25.0
mg/kg wet
Zinc
1.10
U
2.50
mg/kg wet
LCS (0I11019-BSI)
Prepared: 09/11/2020 11:09 Analyzed: 09/14/2020 12:55
Spike
Source
%REC RPD
Anala
Result
Flaa Q
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
111
10.0
mg/kg
wet
102
109
80-120
Arsenic
10.6
0.500
mg/kg
wet
10.2
104
80-120
Cadmium
1.09
0.0500
mg/kg
wet
1.02
107
80-120
Calcium
119
25.0
mg/kg
wet
102
116
80-120
Chromium
11.0
0.500
mg/kg
wet
10.2
108
80-120
Copper
10.9
0.500
mg/kg
wet
10.2
107
80-120
Lead
10.6
0.500
mg/kg
wet
10.2
104
80-120
Magnesium
112
25.0
mg/kg
wet
102
110
80-120
Molybdenum
10.7
0.500
mg/kg
wet
10.2
105
80-120
Nickel
11.3
2.50
mg/kg
wet
10.2
110
80-120
Potassium
541
25.0
mg/kg
wet
510
106
80-120
Selenium
10.3
0.500
mg/kg
wet
10.2
101
80-120
Sodium
554
25.0
mg/kg
wet
510
109
80-120
Zinc
11.7
2.50
mg/kg
wet
10.2
114
80-120
Matrix Spike (0I11019-MS1)
Prepared:
09/11/2020 11:09 Analyzed: 09/14/2020 12:57
Source: CD14285-02
Spike
Source
%REC RPD
Analvte
Result
FFF`lau Q
Units
Level
Result
%REC
Limits RPD Limit
Notes
Aluminum
12600
11.9
mg/kg dry
120
6340
NR
75-125
QM-07
Arsenic
12.1
0.594
mg/kg dry
12.0
0.380 U
101
75-125
Cadmium
1.17
0.0594
mg/kg dry
1.20
0.0114 U
98
75-125
Calcium
782
29.7
mg/kg dry
120
682
83
75-125
Chromium
21.7
0.594
mg/kg dry
12.0
9.57
101
75-125
Copper
22.0
0.594
mg/kg dry
12.0
16.2
48
75-125
QM-07
Lead
38.5
0.594
mg/kg dry
12.0
53.5
NR
75-125
QM-07
Magnesium
592
29.7
mg/kg dry
120
430
134
75-125
QM-07
Molybdenum
12.3
0.594
mg/kg dry
12.0
1.75
88
75-125
Nickel
16.6
2.97
mg/kg dry
12.0
4.81
98
75-125
Potassium
1150
29.7
mg/kg dry
600
427
121
75-125
Selenium
4.90
0.594
mg/kg dry
12.0
0.487 U
41
75-125
QM-07
FINAL
This report relates only to the sample as received by the laboratory, and may only be
reproduced in
full.
Page 6 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0111019 - EPA 3050E - Continued
Matrix Spike (0I11019-MSI) Continued Prepared: 09/11/2020 11:09 Analyzed: 09/14/2020 12:57
Source: CD14285-02
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Sodium 658 29.7 mg/kg dry 600 21.8 106 75-125
Zinc 49.2 2.97 mg/kg dry 12.0 88.0 NR 75-125 QM-07
Matrix Spike Dup (0I11019-MSDI) Prepared: 09/11/2020 11:09 Analyzed: 09/14/2020 12:59
Source: CD14285-02
Spike
Source
%REC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
10600
11.9
mg/kg dry
129
6340
NR
75-125
17
20
QM-07
Arsenic
10.1
0.594
mg/kg dry
12.9
0.380 U
78
75-125
18
20
Cadmium
1.33
0.0594
mg/kg dry
1.29
0.0114 U
103
75-125
13
20
Calcium
502
29.7
mg/kg dry
129
682
NR
75-125
44
20
QM-07,
QM-11
Chromium
31.8
0.594
mg/kg dry
12.9
9.57
172
75-125
38
20
QM-07,
QM-11
Copper
23.3
0.594
mg/kg dry
12.9
16.2
55
75-125
6
20
QM-07
Lead
24.3
0.594
mg/kg dry
12.9
53.5
NR
75-125
45
20
QM-07,
QM-11
Magnesium
484
29.7
mg/kg dry
129
430
42
75-125
20
20
QM-07
Molybdenum
13.0
0.594
mg/kg dry
12.9
1.75
88
75-125
6
20
Nickel
17.0
2.97
mg/kg dry
12.9
4.81
94
75-125
2
20
Potassium
990
29.7
mg/kg dry
645
427
87
75-125
15
20
Selenium
0.487
U 0.594
mg/kg dry
12.9
0.487 U
75-125
20
QM-07
Sodium
699
29.7
mg/kg dry
645
21.8
105
75-125
6
20
Zinc
38.0
2.97
mg/kg dry
12.9
88.0
NR
75-125
26
20
QM-07,
QM-11
Post Spike (0I11019-PSI)
Prepared:
09/11/2020
11:09 Analyzed: 09/14/2020 13:01
Source: CD14285-02
Spike
Source
%REC
RPD
Anala
Result
Flaa Q
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
105
0.200
mg/L
2.00
105
13
80-120
QM-08
Arsenic
0.214
0.0100
mg/L
0.200
-0.00294
107
80-120
Cadmium
0.0207
0.00100
mg/L
0.0200
0.000183
103
80-120
Calcium
13.4
0.500
mg/L
2.00
11.3
107
80-120
Chromium
0.369
0.0100
mg/L
0.200
0.158
106
80-120
Copper
0.474
0.0100
mg/L
0.200
0.267
103
80-120
Lead
1.08
0.0100
mg/L
0.200
0.883
99
80-120
Magnesium
9.08
0.500
mg/L
2.00
7.10
99
80-120
Molybdenum
0.247
0.0100
mg/L
0.200
0.0289
109
80-120
Nickel
0.304
0.0500
mg/L
0.200
0.0794
112
80-120
Potassium
17.7
0.500
mg/L
10.0
7.05
107
80-120
Selenium
0.136
0.0100
mg/L
0.200
-0.0884
68
80-120
QM-08
Sodium
11.2
0.500
mg/L
10.0
0.360
109
80-120
Zinc
1.64
0.0500
mg/L
0.200
1.45
93
80-120
Batch 0115024 - EPA 7471E
Blank (0I15024-BLKI)
Prepared:
09/15/2020
11:39 Analyzed: 09/15/2020 16:50
Anale
Mercury
Spike Source %REC RPD
Result Flaa Q Units Level Result %REC Limits RPD Limit
0.0511 U 0.0686 mg/kg wet
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0115024 - EPA 7471E - Continued
LCS (0I15024-BSI) Prepared: 09/15/2020 11:39 Analyzed: 09/15/2020 16:53
Spike
Source
a/oREC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.581
0.0617
mg/kg wet
0.600
97
80-120
Matrix Spike (0I15024-MSI)
Prepared: 09/15/2020 11:39 Analyzed: 09/15/2020 16:57
Source: CD11817-01
Spike
Source
%REC
RPD
Analvte
Result
Flao
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
3.17
0.350
mg/kg dry
3.30
0.261 U
96
80-120
Matrix Spike Dup (0I15024-MSD1)
Prepared: 09/15/2020 11:39 Analyzed: 09/15/2020 16:59
Source: CD11817-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
3.42
0.350
mg/kg dry
3.53
0.261 U
97
80-120 8
20
Post Spike (0I15024-PSI)
Prepared: 09/15/2020 11:39 Analyzed: 09/15/2020 17:01
Source: CD11817-01
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.37
0.514
ug/L
5.00
-0.0190
107
75-125
Classical Chemistry Parameters - Quality Control
Batch 0111008 - WETS-88 Soil Leaching
Blank (0I11008-BLKI) Prepared: 09/11/2020 09:21 Analyzed: 09/11/2020 19:07
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Nitrate as N 2.0 1 10 mg/kg wet QB-02
Nitrite as N 0.18 1 1.0 mg/kg wet QB-02
LCS (0I33008-BSI) Prepared: 09/11/2020 09:21 Analyzed: 09/11/2020 19:25
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Nitrate as N
47
B
10
mg/kg wet
49.9
94
80-120
Nitrite as N
12
B
1.0
mg/kg wet
9.98
125
80-120
QL-02
Matrix Spike (0I11008-MSI)
Prepared: 09/11/2020 09:21 Analyzed: 09/11/2020 20:00
Source: CD11817-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Nitrate as N
13
]B
57
mg/kg dry
114
12 U
12
80-120
QM-07
Nitrite as N
59
B
5.7
mg/kg dry
56.8
0.45 U
104
80-120
Matrix Spike Dup (0I11008-MSDI)
Prepared: 09/11/2020 09:21 Analyzed: 09/11/2020 20:18
Source: CD11817-01
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Nitrate as N
24
]B
57
mg/kg dry
114
12 U
22
80-120 60
15
QM-07,
QM-11
Nitrite as N
63
B
5.7
mg/kg dry
56.8
0.45 U
111
80-120 6
15
Batch 0114005 - Same
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0114005 - Same - Continued
Blank (0I34005-BLK3) Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 12:53
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Phosphorus 2.9 U 8.0 mg/kg wet
LCS (0I14005-BSI) Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 12:54
Spike Source %REC RPD
Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes
Phosphorus LCS 8.0 mg/kg wet 124 7 80-120
believed
to not
have
been
spiked.
LCS from
as
LCS (0I14005-BS2) Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 14:02
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
130
8.0
mg/kg wet
128
104
80-120
Matrix Spike (0I14005-MS1)
Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 12:57
Source: CD11817-01
Spike
Source
%REC
RPD
Anala
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
5700
D
450
mg/kg dry
288
5100
228
80-120
QM-07
Matrix Spike Dup (0I14005-MSDI)
Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 12:58
Source: CD11817-01
Spike
Source
%REC
RPD
Analyte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Phosphorus
5600
D
450
mg/kg dry
287
5100
177
80-120 3
25
QM-07
Batch 0114006 - Same
Blank (0I14006-BLKI) Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 11:19
Spike Source %REC RPD
Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 35 U 38 mg/kg wet
LCS (0I14006-BSI) Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 11:21
Anale
Total Kjeldahl Nitrogen
Result Flaa POLL
LCS U 38
believed
to not
have
been
spiked.
LCS from
as
Spike Source %REC RPD
Units Level Result %REC Limits RPD Limit
mg/kg wet 933 90-110
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0114006 - Same - Continued
LCS (0I14006-BS2)
Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 13:48
Spike Source a/oREC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
940
38
mg/kg wet
960 98 90-110
Matrix Spike (0I14006-MSI)
Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 11:24
Source: CD11817-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
14000
D
2200
mg/kg dry
2160 11000 136 90-110
QM-07
Matrix Spike Dup (0I14006-MSDI)
Prepared: 09/14/2020 10:00 Analyzed: 09/17/2020 11:26
Source: CD11817-01
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
15000
D
2200
mg/kg dry
2150 11000 203 90-110 10
10
QM-07
Batch 0115020 - NO PREP
Blank (0I15020-BLKI)
Prepared: 09/11/2020 11:09 Analyzed: 09/15/2020 14:49
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.45
U
1.0
mg/kg wet
LCS (0I15020-BSI)
Prepared: 09/11/2020 11:09 Analyzed: 09/15/2020 14:51
Spike Source %REC
RPD
Analvte
Result
Flao
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
9.3
1.0
mg/kg wet
10.1 92 90-110
Matrix Spike (0I15020-MSI)
Prepared: 09/11/2020 11:09 Analyzed: 09/15/2020 14:58
Source: CD11817-01
Spike Source %REC
RPD
Anala
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
340
E
5.7
mg/kg dry
22.9 350 NR 90-110
QM-07
Matrix Spike Dup (0I15020-MSDI)
Prepared: 09/11/2020 11:09 Analyzed: 09/15/2020 14:59
Source: CD11817-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
320
E
5.7
mg/kg dry
22.9 350 NR 90-110 7
10
QM-07
Batch 0115034 - NO PREP
Duplicate (0I15034-DUPI)
Prepared & Analyzed: 09/15/2020 18:25
Source: CD11817-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
5.4
0.0010
% by Weight
3.4 47
25
QM-12
Batch 0121023 - NO PREP
LCS (0I21023-BSI) Prepared: 09/21/2020 15:23 Analyzed: 09/21/2020 15:36
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
pH 6.9 1.0 pH Units 7.00 99 99-101
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0121023 - NO PREP - Continued
Duplicate (0I21023-DUP3) Prepared: 09/21/2020 14:11 Analyzed: 09/21/2020 15:36
Source: CD11817-01
Spike Source a/oREC RPD
Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
pH 7.1 1.0 pH Units 7.4 4 25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method - specified holding time.
QB-02 The method blank contains analyte at a concentration above the MDL and/or greater than one-half the
MRL. The analyte was not detected in the sample.
QL-01 Sample results for the QC batch were accepted based on LCS/LCSD percent recoveries and RPD values.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

_9 10775 Central Port Or. Jack Executive Park Court, Suite 111 Cary, Woodwinds Sndustdat Cl.
Oriantld, FL 32624 Jacksonville, FL 32215-6969 Cary, NC 27511
VIIE�
[phone] Fax [phone] (994)296.W07 Fax[phone] [phone] Fax [phone] Page of
Client Name
Hunt Environmental Associates HL1017
Project Number
Inanel
Requested
Analyses
Requested Turnaround
limes
Note :Rush requests subject to
acceptance by [he facility
— Standard
Expedited
Due I I
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Cityof Lumberton
City/ST2ip
Lumberton, NC 28360
PO d i Billing We
Tel
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Fax
+'lepotting Contact
Jordan Davis
Sampler{s) Name, Affiliation (Prins)
V1 1
Billing Conlaet
Cady Hunt
pler(s) Sign u
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Site Location / Time Zone
Lab WDrkarder
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Preservation
4See
Codes)
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as necessary)
Item a
Sample ID (Field Identification)
Collection Date
Collection
Time
Comp ! Grab
Matrix
(see codes)
Total p of
Containers
1.Sample
Comments
WW-1
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X
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Total of Containers
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Condition U on Receipt
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Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: 1-Ice H-HCI N-HNO3 S-H25O4 NO-NaUH o-ulner (detail in comments)
Note: All samples submitted to ENCO Labs are in accordance wish the terms and conditions listed on the reverse of this lorm, unless prior written agreements exist

Cameron Testing Services, Inc. Laboratory Report
Client: Envir - h0|ce Recycling CTSP�lo,
Project: City of Lumberton Regulatory
Sample Information
Sampled C.H &r6 Date 0 D10/20 R od
Analyses and Result
2009- 82
NC NRmH
NC PH Hake
US EPA iONCO191B
rA Gert,p7a
J. Cameron Date 09110120
Lab JD mpg o
( k
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Sanford NC737 m

219 S. SIeele str.
sanfa'd. NC 27M
Phone. 9' 9-208.424d
Cameron Testing Services, Inc.
NC ww+GVV Cert 01554 NC PHHS Cert 9 37M US EPA N y s18
chain of Custody
Page of
Company_ Enviro-Choi a ReC ling
Email;
I}aacharris(Mgmail corn
CTS lab use only
CornaaL Car ' an Harris
ph�om:
stk738-5311
Sample
Lab ID {�
Address iCr«y, 3330 Saddletree Fed. �
Fax-
Ice (Y1N)
Stale. Zip} Lumberton, NC 28360
Notes:
Ie."1, ?YN
Project' CRY of LUmberton
Rush (YIN)
Due:
Collected: 15fa!rr Y:{ � 4
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5rgfidtum iY
FY
am pie Information
Number of bottles
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ANALYTICAL REPORT
December 11, 2020
Hunt Environmental Associates
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1291556
12/02/2020
Enviro-Choice Recycling
Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4��
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
aceAnalytical
National Center for Testing & Innovation
AW
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2 0 12:41 1 of34

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
WW-4 L1291556-01
5
Fn
WW-4 L1291556-02
6
Qc: Quality Control Summary
8
Fr
Total Solids by Method 2540 G-2011
8
Total Solids by Method 2540B
9
FC
Wet Chemistry by Method 350.1
10
F
Wet Chemistry by Method 351.2
13
Wet Chemistry by Method 353.2
14
[Al
Wet Chemistry by Method 365.4
15
Wet Chemistry by Method 365.4M
16
RC
Wet Chemistry by Method 4500 CN E-2011
17
Wet Chemistry by Method 9012B
18
Wet Chemistry by Method 9030B
19
Wet Chemistry by Method 9034-9030B
20
Wet Chemistry by Method 9040C
21
Wet Chemistry by Method 9056A
22
Wet Chemistry by Method D93/1010A
23
Mercury by Method 7470A
25
Mercury by Method 7471B
26
Metals (ICP) by Method 6010D
27
GI: Glossary of Terms
31
Al: Accreditations & Locations
32
Sc: Sample Chain of Custody
33
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates L1291556
12/11/2012:41 2 of34

ONE LAB. NATIONWIDE. *
WW-4 L1291556-01 Solid
Method
Total Solids by Method 2540 G-2011
Wet Chemistry by Method 350.1
Wet Chemistry by Method 365.4M
Wet Chemistry by Method 9012B
Wet Chemistry by Method 9030B
Wet Chemistry by Method 9056A
Wet Chemistry by Method D93/1010A
Mercury by Method 7471B
Metals (ICP) by Method 6010D
WW-4 L1291556-02 GW
Method
Total Solids by Method 2540B
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 4500 CN E-2011
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9040C
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Metals (ICP) by Method 6010D
1
SAMPLE SUMMARY
Collected by
Jordan Davis
Batch
Dilution Preparation
date/time
WG1588636
1 12/08/20 23:47
WG1584591
1 12/04/201105
WG1588405
5 12/08/2014:46
WG1587535
1 12/07/20 22:04
WG1588708
1 12/08/2015:00
WG1588344
1 12/08/20 22:02
WG1587456
1 12/06/20 22:50
WG1588828
1 12/09/20 08:02
WG1588539
1.351351 12/08/2016:43
Collected date/time Received date/time
11/30/2013:25 12/02/20 09:50
Cp
Analysis Analyst
date/time
12/08/20 23:58
12/09/20 20:23
12/09/20 05:22
12/08/20 22:23
12/08/20 23:30
12/09/20 05:20
12/06/20 22:50
12/09/2013:46
12/09/20 00:28
MMF
SDL
SDL
SDL
LDT
ELN
CO
BMF
EL
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
6
QC
Collected by
Collected date/time
Received date/time
Jordan Davis
11/30/2013:25
12/02/20 09:50
7
GI
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
8A1
WG1586539
1
12/07/20 22:38
12/07/20 22:44
MMF
Mt. Juliet, TN
WG1588058
10
12/10/20 0103
12/10/20 0103
DGR
Mt. Juliet, TN
WG1588739
200
12/05/2016:51
12/10/20 04:12
SDL
Mt. Juliet, TN
RC
WG1585894
1
12/08/2010:50
12/08/2010:50
MSP
Mt. Juliet, TN
WG1586958
100
12/05/2016:51
12/09/20 04:49
SDL
Mt. Juliet, TN
WG1587394
10
12/06/201103
12/07/2014:23
JER
Mt. Juliet, TN
WG1585917
100
12/03/20 20:38
12/03/20 20:38
LRP
Mt. Juliet, TN
WG1587740
1
12/07/2015:02
12/07/2015:02
KPS
Mt. Juliet, TN
WG1585888
1
12/03/2018:20
12/03/2018:20
CO
Mt. Juliet, TN
WG1586465
1
12/04/20 09:02
12/05/2013:35
ABL
Mt. Juliet, TN
WG1587599
1
12/07/20 22:48
12/08/20 04:28
CCE
Mt. Juliet, TN
WG1587599
5
12/07/20 22:48
12/08/2010:07
CCE
Mt. Juliet, TN
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 3 of34

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
FC
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1291556-02 WW-4 4500 CN E-2011
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2012:41 4 of34

WW-4
Collected date/time: 11/30/20 13:25
Total Solids by Method 2540 G-2011
SAMPLE RESULTS - 01
L1291556
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.78
1 12/08/2020 23:58
WG1588636
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 2180
360 1
12/09/2020 20:23
Wet Chemistry by Method 365.4M
Batch
WG1584591
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 15700 B 3600 5 12/09/2020 05:22 WG1588405
Wet Chemistry by Method 9012B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Cyanide ND 8.99 1 12/08/2020 22:23 WG1587535
Wet Chemistry by Method 9030B
Result (dry) Qualifier
RDL (dry)
Dilution Analysis
Analyte mg/kg
mg/kg
date / time
Sulfide ND
899
1 12/08/2020 23:30
Wet Chemistry by Method 9056A
Result (dry) Qualifier
RDL (dry)
Dilution Analysis
Analyte mg/kg
mg/kg
date / time
Nitrate -Nitrite ND
719
1 12/09/2020 05:20
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7471B
Qualifier Dilution Analysis
date / time
1 12/06/2020 22:50
Batch
WG1587456
Batch
WG1588708
Batch
WG1588344
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.44 1 12/09/202013:46 WG1588828
Metals (ICP) by Method 6010D
Result (dry)
Qualifier RDL (dry)
Dilution
Analysis
Batch
mg/kg
mg/kg
date / time
22200
972
1.351351
12/09/2020 00:28
WG1588539
ND
97.2
1.351351
12/09/2020 00:28
WG1588539
ND
24.3
1.351351
12/09/2020 00:28
WG1588539
10900
4860
1.351351
12/09/2020 00:28
WG1588539
436
97.2
1.351351
12/09/2020 00:28
WG1588539
ND
24.3
1.351351
12/09/2020 00:28
WG1588539
ND
4860
1.351351
12/09/2020 00:28
WG1588539
ND
24.3
1.351351
12/09/2020 00:28
WG1588539
10600
B 2430
1.351351
12/09/2020 00:28
WG1588539
ND
97.2
1.351351
12/09/2020 00:28
WG1588539
20700
4860
1.351351
12/09/2020 00:28
WG1588539
694
243
1.351351
12/09/2020 00:28
WG1588539
ACCOUNT: PROJECT: SDG:
Hunt Environmental Associates L1291556
ONE LAB. NATIONWIDE. *
FP
Fc
FS
Fn
Fc
F,
SAI
Rc
DATE/TIME: PAGE:
12/11/20 12:41 5 of 34

WW-4
Collected date/time: 11/30/20 13:25
Total Solids by Method 2540B
SAMPLE RESULTS - 02
L1291556
Result
Qualifier Dilution
Analysis Batch
Analyte mg/I
date / time
Total Solids 21900
1
12/07/2020 22:44 WG1586539
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution Analysis Batch
Analyte mg/I
mg/I
date / time
Ammonia Nitrogen 94.9
2.50
10 12/10/2020 0103 WG1588058
Wet Chemistry by Method 351.2
Result Qualifier RDL
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 1420 50.0
Wet Chemistry by Method 353.2
Dilution Analysis Batch
date / time
200 12/10/2020 04:12 WG1588739
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Nitrate -Nitrite ND 0.100 1 12/08/202010:50 WG1585894
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Phosphorus, Total 410
10.0
100
12/09/2020 04:49
WG1586958
Wet Chemistry by Method 4500 CN E-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Reactive Cyanide 0.0559
0.0500
10
12/07/202014:23
WG1587394
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/I mg/I
Reactive Sulfide 21.3 5.00
Wet Chemistry by Method 9040C
Dilution Analysis Batch
date / time
100 12/03/2020 20:38 WG1585917
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 6.98 T8 1 12/07/202015:02 WG1587740
Sample Narrative:
L1291556-02 WG1587740: 6.98 at18.4C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte deg F date/time
Flashpoint DNF at170 1 12/03/202018:20 WG1585888
Mercury by Method 7470A
Analyte
Mercury
Result Qualifier RDL Dilution Analysis Batch
mg/I mg/I date / time
0.000452 0.000200 1 12/05/202013:35 WG1586465
ONE LAB. NATIONWIDE. *
FP
Fc
FS
Fn
Fc
F,
SAI
Rc
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 6 of34

WW-4
SAMPLE
RESULTS - 02
ONE LAB. NATIONWIDE.
Collected date/time: 11/30/20 13:25
L1291556
Metals (ICP) by Method 6010D
Result
Qualifier RDL Dilution Analysis
Batch
FPAnalyte
mg/I
mg/I
date / time
Aluminum 437
0.200 1
12/08/2020 04:28
WG1587599
F
Arsenic 0.118
0.0100 1
12/08/2020 04:28
WG1587599
Cadmium 0.0102
0.00200 1
12/08/2020 04:28
WG1587599
Calcium 283
1.00 1
12/08/2020 04:28
WG1587599
FS
Copper 4.85
0.0100 1
12/08/2020 04:28
WG1587599
Lead 0.169
0.00600 1
12/08/2020 04:28
WG1587599
Fn
Magnesium 49.3
1.00 1
12/08/2020 04:28
WG1587599
Molybdenum 0.0471
0.00500 1
12/08/2020 04:28
WG1587599
Nickel 0.297
0.0100 1
12/08/2020 04:28
WG1587599
FA
Potassium 86.2
10.0 5
12/08/202010:07
WG1587599
Selenium ND
0.0100 1
12/08/2020 04:28
WG1587599
6
QC
Sodium 426
3.00 1
12/08/2020 04:28
WG1587599
Zinc 14.3
0.0500 1
12/08/2020 04:28
WG1587599
�GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556
12/11/2012:41 7 of34

WG1588636
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3601897-1 12/03/20 2358
MB Result
Analyte
Total Solids 0.000
MB Qualifier MB MDL MB RDL
L1293828-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1291556-01
(OS) L1293323-01 12/03/20 23:58 • (DUP) R3601397-3 12/03/20 23:58
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte % % %_
Total Solids 2.47 2.46 1 0.406 10
Laboratory Control Sample (LCS)
(LCS) R3601897-2 12/08/20 23:58
Spike Amount LCS Result
Analyte
Total Solids 50.0 50.0
LCS Rec. Rec. Limits LCS Qualifier
100 85.0-115
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 3 of34

WG1586539 QUALITY CONTROL SUMMARY
Total Solids by Method 2540B L1291556-02
Method Blank (MB)
(MB) R3601337-1 12/07/20 22:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Total Solids 1.00
L1291556-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1291556-02 12/07/20 22:44 • (DUP) R3601337-3 12/07/20 22:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Total Solids 21900 22100 1 0.909 5
Laboratory Control Sample (LCS)
(LCS) R3601337-2 12/07/20 22:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Total Solids 9500 9260 97.5 92.5-108
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/20 12:41 9 of 34

WG1584591
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 350.1
L1291556-01
Method Blank (MB)
C p
(MB) R3601933-1 12/09/20 20:04
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TC
I
Ammonia Nitrogen -17.00 10.0
FS
L1290625-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1290625-01 12/09/20 20:12 • (DUP) R3601933-3 12/09/20 2013
Original Result DUP Result
Dilution DUP RPD
DUP RPD
DUP Qualifier
(dry) (dry)
Limits
F
Analyte mg/kg mg/kg _ %_
Ammonia Nitrogen 870 896 1 2.95
20
L1291563-07 Original Sample (OS) • Duplicate (DUP)
GI
(OS) L1291563-07 12/09/20 20:36 • (DUP) R3601933-7 12/09/20 20:37
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
FAI
Analyte mg/kg mg/kg
Ammonia Nitrogen ND ND 1 0.000
20
Fc
Laboratory Control Sample (LCS)
(LCS) R3601933-2 12/09/20 20:05
Spike Amount LCS Result LCS Rec. Rec. Limits
LCS Qualifier
Analyte mg/kg mg/kg
Ammonia Nitrogen 500 525 105 90.0-110
L1291205-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1291205-01 12/09/20 20:14 • (MS) R3601933-4 12/09/20 2015
Spike Amount Original Result MS Result (dry) MS Rec.
(dry) (dry)
Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg
Ammonia Nitrogen 20500 452 20100 95.9
1 80.0-120
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556
12/11/2012:41 10 of34

WG1584591 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1291556-01
L1291563-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1291563-05 12/09/20 20:32 • (MS) R3601933-5 12/09/20 20:33 • (MSD) R3601933-6 12/09/20 20:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg
Ammonia Nitrogen 500 ND 401 406 80.3 81.2 1 80.0-120 1.13
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/20 12:41 11 of 34

WG1588058 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 350.1 L1291556-02
Method Blank (MB)
(MB) R3601969-1 12/09/20 23:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Ammonia Nitrogen U 0.117 0.250
L1291539-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1291539-01 12/10/20 00:00 • (DUP) R3601969-5 12/10/20 00:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Ammonia Nitrogen ND ND 1 0.000 10
L1291579-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1291579-02 12/10/20 00:21 • (DUP) R3601969-6 12/10/20 00:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Ammonia Nitrogen 0.515 0.510 1 0.976 10
Laboratory Control Sample (LCS)
(LCS) R3601969-2 12/09/20 23:50
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Ammonia Nitrogen 7.50 7.22 96.3
Rec. Limits LCS Qualifier
90.0-110
L1291528-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
Cp
ITC]
FSS
[Cn]
5
Sr
�GI
1711
FSCI
(OS) L1291523-02 12/09/20 23:53 • (MS) R3601969-3 12/09/20 23:55 • (MSD) R3601969-4 12/09/20 23:56
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Ammonia Nitrogen 5.00
ND
5.01
5.03 100 101 1 90.0-110 0.319 10
L1291603-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1291603-02 12/10/20 00:31 • (MS) R3601969-7 12/10/20 00:33
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
Ammonia Nitrogen 5.00 ND 5.07 101 1 90.0-110
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/20 12:41 12 of 34

WG1588739
Wet Chemistry by Method 351.2
Method Blank (MB)
(MB) R3601994-1 12/10/20 03:37
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN U 0.140
Laboratory Control Sample (LCS)
(LCS) R3601994-2 12/10/20 03:38
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Kjeldahl Nitrogen, TKN 15.2 14.1 92.8
QUALITY CONTROL SUMMARY
L1291556-02
MB RDL
mg/I
0.250
Rec. Limits LCS Qualifier
75.2-121
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 13 of34

WG1585894
Wet Chemistry by Method 353.2
Method Blank (MB)
(MB) R3601341-1 12/03/2010:43
MB Result
MB Qualifier MB MDL
Analyte mg/I
mg/I
Nitrate -Nitrite U
0.0500
Laboratory Control Sample (LCS)
(LCS) R3601341-2 12/08/20 10:44
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Nitrate -Nitrite 2.50 2.60 104
QUALITY CONTROL SUMMARY
L1291556-02
MB RDL
mg/I
0.100
Rec. Limits LCS Qualifier
90.0-110
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/20 12:41 14 of 34

WG1586958
Wet Chemistry by Method 365.4
Method Blank (MB)
(MB) R3601601-2 12/09/20 03:04
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Phosphorus, Total 0.0780 J 0.0350
Laboratory Control Sample (LCS)
(LCS) R3601601-3 12/09/20 03:05
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Phosphorus, Total 4.26 4.05 95.2
QUALITY CONTROL SUMMARY
L1291556-02
MB RDL
mg/I
0.100
Rec. Limits LCS Qualifier
82.4-117
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/20 12:41 15 of 34

WG1588405 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 365.4M L1291556-01
Method Blank (MB)
(MB) R3601602-2 12/09/20 05:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Phosphorus, Total 11.4 J 5.00 20.0
L1291556-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1291556-01 12/09/20 05:22 • (DUP) R3601602-7 12/09/20 05:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Phosphorus, Total 15700 17100 5 8.37 25
Laboratory Control Sample (LCS)
(LCS) R3601602-4 12/09/20 05:10
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Phosphorus, Total 170 172 101
Rec. Limits LCS Qualifier
83.3-116
L1291556-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1291556-01 12/09/20 05:12 • (MS) R3601602-5 12/09/20 05:14 • (MSD) R3601602-6 12/09/20 05:15
ONE LAB. NATIONWIDE. *
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg
Phosphorus, Total 7190 17600
22300
22800 65.1
72.8 1 50.0-150
E E 2.44 25
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556
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WG1587394
Wet Chemistry by Method 4500 CN E-2011
Method Blank (MB)
(MB) R3601127-1 12/07/201415
MB Result
Analyte mg/I
Reactive Cyanide U
QUALITY CONTROL SUMMARY
L1291556-02
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00180 0.00500
L1291551-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1291551-02 12/07/2014:21 • (DUP) R3601127-3 12/07/2014:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Reactive Cyanide ND ND 1 0.000 20
L1292423-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1292423-01 12/07/2014:43 • (DUP) R3601127-8 12/07/2014:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Reactive Cyanide ND ND 1 200 P1 20
Laboratory Control Sample (LCS)
(LCS) R3601127-2 12/07/201416
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Reactive Cyanide 0.100 0.101 101
Rec. Limits LCS Qualifier
90.0-117
L1291691-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1291691-01 12/07/2014:32 • (MS) R3601127-4 12/07/2014:33 • (MSD) R3601127-5 12/07/2014:34
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Reactive Cyanide 0.100
ND
0.0980
0.0948 98.0 94.8 1 90.0-110 3.32 20
L1291801-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1291301-02 12/07/2014:39 • (MS) R3601127-6 12/07/2014:40 • (MSD) R3601127-7 12/07/2014:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Reactive Cyanide 0.100 ND 0.0764 0.0850 76.4 85.0 1 90.0-110 J6 J6 10.7 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2012:41 17 of34

WG1587535 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012B L1291556-01
Method Blank (MB)
(MB) R3601561-1 12/03/20 2218
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Cyanide U 0.0733 0.250
L1291556-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1291556-01 12/03/20 22:23 • (DUP) R3601561-3 12/03/20 22:24
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Cyanide ND ND 1 20.0 20
L1292642-17 Original Sample (OS) • Duplicate (DUP)
(OS) L1292642-17 12/03/20 22:37 • (DUP) R3601561-6 12/03/20 22:38
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3601561-2 12/08/20 22:19
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Cyanide 2.50 2.55 102
Rec. Limits LCS Qualifier
85.0-115
L1292642-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1292642-07 12/03/20 22:30 • (MS) R3601561-4 12/03/20 22:31 • (MSD) R3601561-5 12/03/20 22:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Cyanide 1.67 ND 1.60 1.62 96.0 97.2 1 75.0-125 1.26 20
L1292642-27 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1292642-27 12/03/20 22:46 • (MS) R3601561-7 12/03/20 22:47 • (MSD) R3601561-8 12/03/20 22:48
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Cyanide 1.67 ND 1.60 1.65 95.9 98.9 1 75.0-125 3.13 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2012:41 13 of34

WG1588708
Wet Chemistry by Method 9030B
Method Blank (MB)
(MB) R3601553-1 12/03/20 2330
MB Result
Analyte mg/kg
Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1291540-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1291556-01
(OS) L1291540-01 12/03/20 23:30 • (DUP) R3601553-3 12/03/20 23:30
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3601553-2 12/08/20 23:30
Spike Amount LCS Result
Analyte mg/kg mg/kg
Sulfide 100 88.2
LCS Rec. Rec. Limits LCS Qualifier
88.2 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
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WG1585917
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3600167-1 12/03/20 20:29
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Reactive Sulfide U 0.0250
Laboratory Control Sample (LCS)
(LCS) R3600167-2 12/03/20 2029
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Reactive Sulfide 0.500 0.555 111
QUALITY CONTROL SUMMARY
L1291556-02
MB RDL
mg/I
0.0500
Rec. Limits LCS Qualifier
85.0-115
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 20 of34

WG1587740 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9040C L1291556-02
L1291580-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1291530-02 12/07/2015:02 • (DUP) R3601047-2 12/07/2015:02
Original Result DUP Result Dilution DUP RPD
Analyte su su
pH 9.10 9.10 1 0.000
Sample Narrative:
OS: 9.1 at19.3C
DUP: 9.1 at18.3C
L1292825-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
ONE LAB. NATIONWIDE. *
(OS) L1292325-01 12/07/2015:02 • (DUP) R3601047-3 12/07/2015:02
Original Result DUP Result
Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su
pH 6.99 6.99
1 0.000 1
Sample Narrative:
OS: 6.99 at18.4C
DUP: 6.99 at18.1C
Laboratory Control Sample (LCS)
(LCS) R3601047-1 12/07/20 15:02
Spike Amount LCS Result
LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
pH 10.0 10.0
100 99.0-101
Sample Narrative:
LCS:10.02 at18.2C
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556 12/11/20 12:41 21 of 34

WG1588344 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9056A L1291556-01
Method Blank (MB)
(MB) R3601634-1 12/03/20 23:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Nitrate -Nitrite U 1.06 20.0
L1291073-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1291073-01 12/09/20 01:06 • (DUP) R3601634-4 12/09/20 0122
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Nitrate -Nitrite ND ND 10 0.000 15
L1292353-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1292353-01 12/09/20 11:31 • (DUP) R3601744-1 12/09/201147
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Nitrate -Nitrite ND ND 5 36.8 P1 15
Laboratory Control Sample (LCS)
(LCS) R3601684-2 12/08/20 23:58
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Nitrate -Nitrite 40.0 38.4 96.0
Rec. Limits LCS Qualifier
80.0-120
L1291564-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1291564-01 12/09/20 07:52 • (MS) R3601634-5 12/09/20 08:09 • (MSD) R3601634-6 12/09/20 08:26
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Nitrate -Nitrite 100 ND 102 102 102 102 1 80.0-120 0.109 15
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/20 12:41 22 of 34

WG1585888 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1291556-02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE. *
(LCS) R3600152-1 12/03/2018:20 • (LCSD) R3600152-2 12/03/2018:20
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte deg F deg F deg F
Flashpoint 126 128 128 102 102 96.0-104 0.000 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2012:41 23 of34

WG1587456 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1291556-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE. *
(LCS) R3600830-1 12/06/20 22:50 • (LCSD) R3600830-2 12/06/20 22:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 126 127 131 101 104 95.6-104 3.10 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/2012:41 24 of34

WG1586465 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1291556-02
Method Blank (MB)
(MB) R3600669-1 12/05/2012:54
ONE LAB. NATIONWIDE. *
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Mercury U 0.000100 0.000200
Laboratory Control Sample (LCS)
(LCS) R3600669-2 12/05/201256
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Mercury 0.00300 0.00241 80.4 80.0-120
L1290501-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1290501-01 12/05/20 12:53 • (MS) R3600669-3 12/05/20 13:00 • (MSD) R3600669-4 12/05/20 13:02
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I
Mercury 0.00300 ND 0.00302 0.00294 101 98.1 1
75.0-125
2.62 20
ACCOUNT: PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556
12/11/20 12:41 25 of 34

WG1588828 QUALITY CONTROL SUMMARY
Mercury by Method 7471B L1291556-01
Method Blank (MB)
(MB) R3601735-1 12/09/2012:24
ONE LAB. NATIONWIDE. *
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3601735-2 12/09/20 12:27
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Mercury 0.500 0.473 94.5 80.0-120
L1291564-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1291564-01 12/09/2012:30 • (MS) R3601735-3 12/09/2012:32 • (MSD) R3601735-4 12/09/2012:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Mercury 0.500 ND 0.545 0.559 109 112
1 75.0-125
2.61 20
ACCOUNT: PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556
12/11/20 12:41 26 of 34

WG1587599
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3601257-1 12/03/20 04:11
MB Result
Analyte
mg/I
Aluminum
U
Arsenic
U
Cadmium
U
Calcium
U
Copper
U
Lead
U
Magnesium
U
Molybdenum
U
Nickel
U
Potassium
U
Selenium
U
Sodium
U
Zinc
U
MB Qualifier
Laboratory Control Sample (LCS)
(LCS) R3601257-2 12/08/20 0414
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Aluminum
10.0
9.03
Arsenic
1.00
0.888
Cadmium
1.00
0.916
Calcium
10.0
9.17
Copper
1.00
0.916
Lead
1.00
0.918
Magnesium
10.0
9.35
Molybdenum
1.00
0.935
Nickel
1.00
0.937
Potassium
10.0
9.12
Selenium
1.00
0.919
Sodium
10.0
8.94
Zinc
1.00
0.928
QUALITY CONTROL SUMMARY
L1291556-02
MBMDL
mg/I
MBRDL
mg/I
0.0561
0.200
0.00440
0.0100
0.000479
0.00200
0.0793
1.00
0.00368
0.0100
0.00299
0.00600
0.0853
1.00
0.00116
0.00500
0.00161
0.0100
0.261
2.00
0.00735
0.0100
0.504
3.00
0.00652
0.0500
LCS Rec. Rec. Limits LCS Qualifier
90.3
88.8
91.6
91.7
91.6
91.8
93.5
93.5
93.7
91.2
91.9
89.4
92.8
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
ONE LAB. NATIONWIDE. *
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/20 12:41 27 of 34

WG1587599 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1291556-02
L1292221-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1292221-02 12/03/20 04:17 • (MS) R3601257-4 12/03/20 04:22 • (MSD) R3601257-5 12/03/20 04:25
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Aluminum
10.0
ND
9.14
9.11
90.3
90.0
Arsenic
1.00
ND
0.899
0.897
89.9
89.7
Cadmium
1.00
ND
0.924
0.922
92.4
92.2
Calcium
10.0
5.72
14.8
14.7
90.9
90.0
Copper
1.00
ND
0.923
0.934
91.9
93.0
Lead
1.00
ND
0.926
0.927
92.6
92.7
Magnesium
10.0
ND
10.2
10.1
94.1
92.7
Molybdenum
1.00
ND
0.949
0.950
94.8
94.9
Nickel
1.00
ND
0.956
0.957
95.6
95.7
Potassium
10.0
ND
10.6
10.5
89.7
89.2
Selenium
1.00
ND
0.930
0.929
93.0
92.9
Sodium
10.0
33.2
40.3
40.5
71.5
72.9
Zinc
1.00
0.0579
0.995
0.993
93.7
93.5
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.255
20
1 75.0-125
0.247
20
1 75.0-125
0.243
20
1 75.0-125
0.567
20
1 75.0-125
1.23
20
1 75.0-125
0.0632
20
1 75.0-125
1.36
20
1 75.0-125
0.124
20
1 75.0-125
0.0405
20
1 75.0-125
0.513
20
1 75.0-125
0.0388
20
1 75.0-125
J6 J6 0.346
20
1 75.0-125
0.190
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 23 of34

WG1588539
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1291556-01
(MB) R3601533-7 12/09/20 0108
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Aluminum U
6.08
20.0
Arsenic U
0.518
2.00
Cadmium U
0.0471
0.500
Calcium U
10.6
100
Copper U
0.400
2.00
Lead U
0.208
0.500
Magnesium U
7.38
100
Molybdenum U
0.109
0.500
Potassium 36.9
J 20.9
50.0
Selenium U
0.764
2.00
Sodium U
41.2
100
Zinc U
0.832
5.00
Laboratory Control Sample (LCS)
(LCS) R3601588-2 12/08/20 23:36
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte
mg/kg
mg/kg
Aluminum
1000
996
99.6
80.0-120
Arsenic
100
95.7
95.7
80.0-120
Cadmium
100
97.5
97.5
80.0-120
Calcium
1000
1010
101
80.0-120
Copper
100
98.4
98.4
80.0-120
Lead
100
99.0
99.0
80.0-120
Magnesium
1000
979
97.9
80.0-120
Molybdenum
100
101
101
80.0-120
Potassium
1000
1180
118
80.0-120
Selenium
100
97.2
97.2
80.0-120
Sodium
1000
1120
112
80.0-120
Zinc
100
98.3
98.3
80.0-120
LCS Qualifier
L1291563-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1291563-05 12/03/20 23:39 • (MS) R3601533-5 12/03/20 23:47 • (MSD) R3601533-6 12/03/20 23:50
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
Aluminum
1000
577
1500
1700
92.1
113
1 75.0-125
12.8
20
Arsenic
100
ND
106
106
106
106
1 75.0-125
0.0341
20
Cadmium
100
ND
107
107
106
107
1 75.0-125
0.189
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291556 12/11/20 12:41 29 of 34

WG1588539 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1291556-01
L1291563-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1291563-05 12/03/20 23:39 • (MS) R3601533-5 12/03/20 23:47 • (MSD) R3601533-6 12/03/20 23:50
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
Calcium
1000
282000
295000
265000
1370
0.000
Copper
100
4.04
105
107
101
103
Lead
100
5.68
106
109
100
103
Magnesium
1000
4900
5040
5990
13.8
109
Molybdenum
100
ND
97.1
98.4
96.7
98.0
Potassium
1000
628
1520
1580
89.7
95.1
Selenium
100
ND
109
110
109
110
Sodium
1000
296
1340
1350
104
106
Zinc
100
10.3
106
109
95.8
98.8
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
E V E V 10.8
20
1 75.0-125
2.24
20
1 75.0-125
2.77
20
1 75.0-125
V_ 17.3
20
1 75.0-125
1.32
20
1 75.0-125
3.46
20
1 75.0-125
0.991
20
1 75.0-125
1.38
20
1 75.0-125
2.80
20
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1291556 12/11/2012:41 30 of34

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Rc
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J6
The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1291556 12/11/2012:41 31 of34

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
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KS
W o �AZ NM O�
T TX
AK
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C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
Hunt Environmental Associates
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1291556 12/11/2 0 12:41 32 of34

r
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HCF

ANALYTICAL REPORT
December 16, 2020
Hunt Environmental Associates
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1291565
12/02/2020
Enviro-Choice Recycling
Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4��
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
aceAnalytical
National Center for Testing & Innovation
AW
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291565 12/16/20 10:39 1 of 15

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2 FP
3
4
FS5
6 Fn
7
5G1
F
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291565 12/16/20 10:39 2 of 15

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
WW-4 L1291565-01 Solid Jordan Davis 11/30/2013:25 12/02/20 09:50 t C
P
Method
Batch
Dilution Preparation
Analysis
Analyst Location
date/time
date/time
Subcontracted Analyses
WG1586046
1 12/16/20 00:00
12/16/20 00:00
Subcontract
Collected by
Collected date/time
Received date/time
WW-4 L1291565-02 GW
Jordan Davis
11/30/2013:25
12/02/20 09:50
Method
Batch
Dilution Preparation
Analysis
Analyst Location
date/time
date/time
Subcontracted Analyses
WG1586046
1 12/16/20 00:00
12/16/20 00:00
Subcontract
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291565 12/16/20 10:39 3 of 15

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
5G1
6AI
4�z
Sc
Heather J Wagner
Project Manager
Project Narrative
L1291565 -01, -02 contains subout data that is included after the chain of custody.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291565 12/16/20 10:39 4 of 15

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
SDG Sample Delivery Group.
Uncertainty
(Radiochemistry) Confidence level of 2 sigma.
Fn
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section ofthe report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
F
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
R
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1291565 12/16/20 10:39 5 of 15

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN000032021-1
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
TN00003
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
Indiana C-TN-01
Oregon
TN200002
Rc
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 KY90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-20-18
Maine TN00003
Texas5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
998093910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
Hunt Environmental Associates
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1291565 12/16/20 10:39 6 of 15

�-{ kON t'fl V i rry- r-.� ( � 57 ^ (-
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Waypointo
ANALYTICAL
12/15/2020
Pace Analytical
SubOut Team
12065 Lebanon Rd.
Mt. Juliet, TN, 37122
Ref: Analytical Testing
Lab Report Number: 20-339-0040
Client Project Description: Work Order # WG1586046
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear SubOut Team:
Waypoint Analytical, LLC. received sample(s) on 12/4/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Rebekah Ross
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 7

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
06/30/2021
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
LA037
12/31/2020
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2021
Page 1 of 1 00001/20-339-0040
Page 2 of 7

•
Waypoint
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-339-0040
Client Project Description: Work Order # WG1586046
Lab No Client Sample ID Matrix Date Collected Date Received
89975
WW-4 33846875
Solids
11/30/2020
13:25
12/04/2020
89976
VVW-4
Aqueous
11/30/2020
13:25
12/04/2020
Page 3 of 7

Waypointo
ANALYTICAL
07705
Pace Analytical
SubOut Team
12065 Lebanon Rd.
Mt. Juliet , TN 37122
Report Number : 20-339-0040
Lab No : 89975
Sample ID: WW-4 33846875
Project
Information
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Work Order # WG1586046
REPORT OFANALYSIS
Report Date : 12/15/2020
Received : 12/04/2020
Rebekah Ross
Project Manager
Matrix: Solids
Sampled: 11/ 30/ 2020 13:25
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Calcium (saturated paste)
1.89
meq/L
0.005
1
12/15/20 13:13
PMW
Saturate Paste
Magnesium (saturated paste)
1.46
meq/L
0.008
1
12/15/20 13:13
PMW
Saturate Paste
Sodium (saturated paste)
12.7
meq/L
0.004
1
12/15/20 13:13
PMW
Saturate Paste
Sodium Absorption Ratio
9.81
1
12/15/20 13:13
PMW
Saturate Paste
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

Waypointo
ANALYTICAL
07705
Pace Analytical
SubOut Team
12065 Lebanon Rd.
Mt. Juliet , TN 37122
Report Number : 20-339-0040
Lab No : 89976
Sample ID: WW-4
Project
Information
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Work Order # WG1586046
REPORT OFANALYSIS
Report Date : 12/15/2020
Received : 12/04/2020
Rebekah Ross
Project Manager
Matrix: Aqueous
Sampled: 11/ 30/ 2020 13:25
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Calcium
388
mg/L
2.50
1
12/12/20 02:21
JTR
EPA-200.7
Magnesium
69.3
mg/L
0.500
1
12/12/20 02:21
JTR
EPA-200.7
Sodium
605
mg/L
2.50
1
12/12/20 02:21
JTR
EPA-200.7
Sodium Absorption Ratio
7.42
Ratio
0.01
1
12/12/20 02:21
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 5 of 7

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 07705
Customer Name: Pace Analytical
Report Number: 20-339-0040
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#99
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
® Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
® Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: ory Phillips Date & Time: 12/04/2020 10:26:29
Page 6 of 7

Sub -Contract Chain of Custody
Batch Date/1-imc: 12/03/20 13:03
Sub -Contract l.ab: ALANALAB
Address: 2790 Whitten Road
City/State: Memphis, '1-N 38133
Contact:
nosscc'wa►•po i ntanal ytical .com
WO: WG 1586046
Results Out Date; 12/16/20
FSC Purchase Order N. L 1291565
Send Reports to: James C Huckaba
Email: MTJLSuboutTeam@),paeetabs.com
. aceAr�alytical'
• hWnwrsr Lvrrrvr lw resr:�a 3 innw•a �.w
12065 Lebanon Rd
Mt. Juliet, TN 37122
eall:[phone]
Sample ID Matrix state Collect Date Description 5$m to Number Sample Comments
Container ID Tat Use only Lab Use Only
WW4 SS NC I1/30/20 13:25 Sodium Absorption Ratio by 29B 1. L1291565-01
33846875
WW.4 GW NC 11/30/20 13:25 Sodium Absorption Ratio by 29B 2. L1291565-02
'= Container used for multiple Samples alWor Analyses
Relinquished h1': Date /Z-3,vkP0
Recieved by: A 9
Date
Relinquished b 14 Date
Recie -ed hr Oat 3 Ir
Custody Seals
r 'ved on:
oter(s Container(s)
l lII lI 11l I l l I� l f I II K I if N l 111l l� l 4llll l l�l l IIII till 11111 94722020
pace analvhca1 !0 25 27
WarK Graer w tiuG 1586046
Page 7 of 7

Cameron Testing Services, Inc, Laboratory Report
NC DENR#654
NC PH"S #37709
US EPA IONC01018
Client:
Enviro-Choice Recycling CTSProj.
011- 10
DWCert#37799
Project:
City of Lumberton Regulatory
Yes
Sample Information
Samplad
J Davis Data 11130120 Deceived
J.
Cameron �
1113=0
Analyses and Results
M
4' qr'
Lab Id
►s s
Sample Id Anaiyte Result
�
� .E
CA
z m
Std. Methods
C]
_
Reference
011-210
-01sec, Colirurn-s <38500
GFurO
38500
12MI120 RL
?222D - VF
-02<39000
cFLX@
39M
-03 <36500
6FL4
385W
-04 e36700
cFu+o
38700
-05 76900
cFu+o
38400
-06 <38700
Uufg
38700
-07 <38800
GFUfe
30600
Geomean 4700
-01 3ludge c¢ T (%) 2,60%
GA 1
I M1120 RL
2640 G -TS
-02 2,57%
0.01
-03 2.59%
0.01
-04 2-59%
0.01
-05
0.01
.y_GO%
- L,
0.01
C5r80�A
-07 2-59%
0.01
Report
RWIPW A�
Lab Dir tew f]a6r
219 3, SWO Sk. 919-209-47 0
sword NC 272130 6FQGamcrontts1it1g_COM

219 S. Steele Str. Cameron Testing Services, Inc. Chain of'Custody
Sanford, NC 27334 Page A of
?hone 919-208-424G NC 4VMGVV Gert. #554 NC FHF;S Geri # 37709 US EPA NCO 1918
Company; Envir0- holce Rec ling
Contact' Carrigan Halms
Address j�ity, 0 Saddletree Fed,
state, Zip) Lumberton, N 8360
Project; City of Lumberton
Email,
Phone;
Fax:
Notes:
hea�h� rs gmaGl.aarn
—
910-73"311
Sample Temp
(M
Irrs (YN)
Permit �+� �
bush (YIN) `
CTS lab use only _
l3bID 1}
W '
_-
Due:
Collected: Name_ ` 4RJ4
signa.ura-
ample Information
Plumber of bottles
Requested Analysis
mplI
rL
H
U
.�
w
rd
[� o J C7
m o r
�
o
03
Preservatives: (U)npreserwed, H,Q1,
H2(SjQ4, H(N)O3, (Na)Thiosuliate, Ha(0)H.
Other ( ), Indicate
CT Lab
ID
r
Sal
Y
7
Set (7)
r
Relinquished:
„FCe
DatelTime
Rush mN k will require prior approval. Add Rio nal charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From l/l/2020 To
WQ Permit Number:
NPDES Number:
3/31 /2020
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogeng, ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion IZ
Anaerobic Digestion E-
lf applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
dences
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
mane
Minimum
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
36800
37400
40500
CFU/ g
Quarterly
Q Y
Grab
222D-MI
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) L7
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
u "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C. Hunt, ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 4/l/2020 To
WQ Permit Number:
NPDES Number:
6/30/2020
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogeng, ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion IZ
Anaerobic Digestion E-
lf applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
dences
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
mane
Minimum
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
46500
54600
139900
CFU/ g
uarterl
Q Y
Grab
222D-MI
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) L7
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
u "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C. Hunt, ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 7/l/2020 To
WQ Permit Number:
NPDES Number:
9/30/2020
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogeng, ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion IZ
Anaerobic Digestion E-
lf applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
dences
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
mane
Minimum
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
28100
30200
35400
CFU/ g
Quarterly
Q Y
Grab
222D-MI
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) L7
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
u "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C. Hunt, ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 10/1/2020 To
WQ Permit Number:
NPDES Number:
12/31 /2020
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogeng, ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion IZ
Anaerobic Digestion E-
lf applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
dences
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
mane
Minimum
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
38500
42700
76900
CFU/ g
Quarterly
Q Y
Grab
222D-MI
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) L7
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
u "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C. Hunt, ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL022796
�5' �141..tiL
Client: Carnell Locklear
Advisor: Michael Hunt
Predictive
3009 Daniel McLeod Rd.
Enviro-Choice Recycling
;•
Red Springs, NC 28377
3330 Saddletree Rd
f'. Soil Report Mehlich-3 Extraction
+_
Lumberton, NC28360
Sampled County : Robeson
Links to Helpful Information
Client ID: 275468
Advisor ID: 486968
Sampled: Received: 01/07/2021 Completed: 02/19/2021 Farm: NC-RD-28
Sample ID: R0281
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.0 0 0
0 0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
2.68 1.26 10.7 85 1.6 6.1 176 84 66 16
49 48 38 216 216
211 0.1 1
Noah 0' olina
i
I Awl'
Futaw frum FwW Curnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL020344
�5' �141..tiL
Client:
Carnell Locklear
Advisor: Michael Hunt
Predictive
3009 Daniel McLeod Rd.
Enviro-Choice Recycling
;•
Red Springs, NC 28377
3330 Saddletree Rd
f'. Soil Report Mehlich-3 Extraction
+_
Lumberton, NC28360
Sampled County : Robeson
Links to Helpful Information
Client ID: 275468
Advisor ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/01/2021 Farm: Nc-Ro-28
Sample ID: R028-2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean 0.5 0 0
0
0 0
0
0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.10 1.00 10.1 80 2.0 5.8 189 115 51 23
71
47
38
202
202
212 0.2 2
Sample ID: R028-3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean 0.7 0 0
40
0 0
0
0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.74 1.20 6.2 72 1.8 5.6 170 54 51 16
36
247
158
212
212
175 0.0
Noah 0' olina
i
I Awl'
Futaw frum FwW Curnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL020923
�5' �141..tiL
Client:
David McLean
Advisor: Michael Hunt
Predictive
919 McLean Rd
Enviro-Choice Recycling
;•
Lumberton, NC 28358
3330 Saddletree Rd
f'. Soil Report Mehlich-3 Extraction
+_
Lumberton, NC28360
Sampled County : Robeson
Links to Helpful Information
Client ID: 505228
Advisor ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/08/2021
Farm: Nc-Ro-18
Sample ID: R018-1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Cotton 1.3
50-70 0
110
0 0
0
0
0 1.0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.66 1.31 3.7 50 1.9 5.3 278 20
35 12
39
57
41
108
108
144 0.0
Sample ID: R018-2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Cotton 0.9
50-70 0
50
0 0
0
0
0 1.0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.92 1.24 5.2 68 1.7 5.7 221 49
43 20
46
87
59
150
150
204 0.0
Noah 0' olina
i
I Awl'
Futaw frum FwW Curnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL021083
Client:
Delois/Pete Allen
Advisor:
Michael Hunt
vo- Predictive
688 Deep Branch Rd.
Enviro-Choice Recycling
Lumberton, NC 28360
3330 Saddletree Rd
.'..,$� Soil Report
Mehlich-3 Extraction
Lumberton, NC 28360
_
Sampled County : Robeson
Links to Helpful Information
Client ID: 434958
Advisor
ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/09/2021
Farm: NC-RO-17
Sample ID: R017-1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.7
0 0
120
25 0
10
0
0
0
Note: 3
2 -
0.0
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.97 1.24 4.2 62 1.6 5.5
79 11
51 9
37
22
23
85
85
94
0.1 2
Sample ID: R017-2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.8
0 0
110
0 0
0
0
0
0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
2.15 1.31 6.8 71 2.0 5.6
149 16
61 9
33
38
33
170
170
86
0.0
Sample ID: R017-3
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.5
0 0
120
25 0
10
0
0
0
Note: 3
2 -
0.0
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
2.22 1.26 6.8 72 1.9 5.8
82 12
67 5
45
22
23
84
84
71
0.1 1
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL021083
Delois/Pete Allen
Page 2 of 3
Sample ID: R017-4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1-Soybean
0.0
0 0
120
0
0
$pH 0
0 0
Note: 3 Note: $
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.76 1.23 7.5 95 0.4 6.9
126 11
77 17 32
30
14
120 120
226 0.1 1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL021082
Client:
Fannie Oxendine
Advisor:
Michael Hunt
vo- Predictive
7623 NC HWY 711
Enviro-Choice Recycling
Pembroke, NC 28372
3330 Saddletree Rd
.'..,$� Soil Report
Mehlich-3 Extraction
Lumberton, NC 28360
_
Sampled County : Robeson
Links to Helpful Information
Client ID: 505230
Advisor
ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/09/2021
Farm: NC-RO-21
Sample ID: R021-1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
1.4
0 0
80
25 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 1.33 4.2 45 2.3 5.0
453 31
34 7
69
81
59
353
353
350
0.1 2
Sample ID: R0212A
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
1.0
0 0
80
0 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.86 1.38 5.0 62 1.9 5.4
451 30
45 14
69
83
60
369
369
387
0.1 2
Sample ID: R0212B
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.3
0 0
110
0 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.86 1.19 7.8 77 1.8 5.9
404 15
61 15
53
120
82
1102
1102
791
0.1 1
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL021082
Fannie Oxendine
Page 2 of 3
Sample ID: R021-3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.6
180-220 0
220
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.60 1.39 4.4
65 1.6 5.6 236 8
52 12
37
101
78
549
549
428 0.1
2
Sample ID: R021-4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 1.3
180-220 0
10
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.08 1.27 7.1
65 2.5 5.4 214 113
45 12
37
153
109
645
645
184 0.1
1
Sample ID: R021-5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain 1.1
120 - 160 0
130
25
25
0
0
0 0
Note: 3
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.36 1.49 2.7
37 1.7 4.9 208 9
29 7
22
83
67
207
207
171 0.0

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL021081
Client: Ozzell Arrin Baker Advisor: Michael Hunt
vo- Predictive 2996 Evergreen Church Rd Enviro-Choice Recycling
J`'{i { Pembroke, NC 28372 3330 Saddletree Rd
:.$� Soil I Report Mehlich-3 Extraction Lumberton, NC 28360
-A cSampled
County : Robeson
Links to Helpful Information
Client ID: 156712 Advisor ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/08/2021 Farm: Nc-Ro-16
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be
detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with
zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids
and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce
potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for
copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field.
Sample ID: R016-1
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0 180-220 0 70 0 0 0 0 0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
2.22 1.03 11.4 84 1.8 6.0 132 72 68 14 49 57 51 198 198 117 0.2 2
Sample ID: R016-2
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.6 180-220 0 0 0 0 0 0 0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
1.43 1.12 8.6 78 1.9 5.7 213 119 55 15 57 63 55 246 246 168 0.2 2
North Carolina
Tiobxiv Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL021081
Ozzell Arrin Baker
Page 2 of 5
Sample ID: R016-3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.5
180-220 0
130
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.02 1.28 6.2
76 1.5 5.7 229 42
61 11
40
60
53
145
145
113 0.1
2
Sample ID: R016-4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.8
180-220 0
110
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.01 1.05 7.4
75 1.9 5.6 104 50
57 14
56
58
52
158
158
130 0.3
4
Sample ID: R016-5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.3
180-220 0
20
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.74 1.01 11.8
84 1.8 5.9 227 108
68 12
52
70
59
304
304
172 0.1
1
Sample ID: R016-6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
10
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.55 1.14 8.7
82 1.6 5.9 205 110
63 12
46
87
69
205
205
139 0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL021081
Ozzell Arrin Baker
Page 3 of 5
Sample ID: R016-7
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
110
0
0
0
0
0
0
Note: 12
2 -Small Grain (SG) 0.0
80-100 0
40
0
0
0
0
0
0
Note: 3
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.56 1.29 6.2
87 0.8 6.3 300 49
70 13
35
119
83
76
231
231
188
0.0
Sample ID: R016-8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M 0.0
180-220 0
200
0
0
pH$
0
0
0
Note: 12 Note: $
2 -Small Grain (SG) 0.0
80-100 0
110
0
0
pH$
0
0
0
Note: 3 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.86 1.21 9.3
92 0.8 6.6 241 17
83 8
51
112
76
69
393
393
203
0.1
1
Sample ID: R01616
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
230
0
0
0
0
0
0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.60 1.43 5.5
81 1.0 6.1 223 7
70 11
37
43
41
260
260
305
0.1
2
Sample ID: R01617
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M 0.4
180-220 0
210
25
0
0
0
0
0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.76 1.39 5.2
73 1.4 5.8 260 12
65 7
45
123
91
977
977
227
0.1
2

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL021081
Ozzell Arrin Baker
Page 4 of 5
Sample ID: R01618
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 1.3
180-220 0
210
0
0
0
Z
0 0
Note: 12 Note: $
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.86 1.21 6.7
64 2.4 5.3 447 14
54 8
66
87
69
2515
2515
724 0.1
1
Sample ID: R01619
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
220
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.60 1.25 8.3
85 1.3 6.2 338 10
71 13
50
48
43
482
482
433 0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL022909
Client:
Patrick Bullard
Advisor:
Michael Hunt
vo- Predictive
4147 Prospect Rd. / PO
Box 1262
Enviro-Choice Recycling
Pembroke, NC 28372
3330 Saddletree Rd
.'..,$� Soil Report
Mehlich-3 Extraction
Lumberton, NC 28360
_
Sampled County : Robeson
Links to Helpful Information
Client ID: 260315
Advisor
ID: 486968
Sampled: Received: 01/19/2021 Completed: 02/20/2021
Farm: NC-RO-39
Sample ID: RO391A
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M
0.0
180-220 0
60
0 0
0 0
0
0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.49 1.21 7.1 81 1.4 5.9
64 74
60 16
42
70
59
136 136
95
0.2 3
Sample ID: R0391 B
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M
0.4
180-220 0
0
0 0
0 0
0
0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.31 1.17 7.5 80 1.5 5.8
145 121
54 17
40
73
61
202 202
144
0.1 1
Sample ID: R03902
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M
0.0
180-220 0
0
0 0
0 0
0
0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.81 1.25 8.4 82 1.5 5.9
147 123
59 17
43
105
80
324 324
169
0.1 1
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL022909
Patrick Bullard
Page 2 of 4
Sample ID: RO3903
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.6
180-220 80
130
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.76 1.18 7.2
80 1.4 5.6 24 41
61 16
37
35
38
61
61
40 0.1
1
Sample ID: RO3904
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0
180-220 0
30
0
0
pH$
0
0 0
Note: 12 Note: $
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.60 1.19 16.5
98 0.3 7.2 315 93
85 10
45
175
105
494
494
239 0.2
1
Sample ID: RO3905
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
0
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.08 1.24 9.2
87 1.2 6.2 195 120
63 17
48
93
69
284
284
153 0.2
2
Sample ID: RO3906
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
30
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.08 1.25 8.7
88 1.1 6.3 263 94
67 15
40
128
89
282
282
163 0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL022909
Patrick Bullard
Page 3 of 4
Sample ID: RO3909
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.7
180-220 0
190
25
0
0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.14 1.25 5.0 69 1.6 5.5 347 20
59 8 50
90
71
362 362
323 0.1 2

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL021084
Client:
Ronald G. Hammonds
Advisor:
Michael Hunt
vo- Predictive
1218 Hammonds Rd.
Enviro-Choice Recycling
Lumberton, NC 28360
3330 Saddletree Rd
.'..,$� Soil Report Mehlich-3 Extraction
Lumberton, NC 28360
_
Sampled County : Robeson
Links to Helpful Information
Client ID: 404031
Advisor
ID: 486968
Sampled: 11/25/2020 Received: 11/30/2020 Completed: 02/08/2021
Farm: NC-RO-20
Sample ID: R020-3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.6
180-220 0
120
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.71 1.21 10.4 79 2.2 5.8 445 48
64 13
46
202
138
1491
1491
784
0.1 1
Sample ID: R020-4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 1.0
180-220 0
160
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 1.31 7.6 71 2.2 5.5 475 32
58 11
44
142
102
1123
1123
588
0.2 3
Sample ID: R020-6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 0.7
120 - 160 60
30
0 0
0
0
0
0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 1.26 5.2 72 1.4 5.5 34 55
50 18
119
36
39
88
88
90
0.1 2
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL021084
Ronald G. Hammonds
Page 2 of 3
Sample ID: R020-7
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
70
0
0
0
0
0 0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.74 1.28 6.9
81 1.3 6.0
98 34
59 19
43
46
44
216
216
110 0.1
1
Sample ID: R020-8
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
1.0
120 - 160 0
20
0
0
0
0
0 0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.02 1.21 6.3
69 2.0 5.4
183 69
50 13
53
47
45
211
211
211 0.1
2
Sample ID: R02014
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
50
0
0
0
0
0 0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.61 1.29 7.0
78 1.6 5.9
106 47
62 13
57
59
52
165
165
162 0.1
1

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 1/14/2020 7:59am KCL Dig# 2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9530 g
Weight of dish + dried solids: 122.0584 g
Weight of dried solids: 0.1054 g
Total Solids: 21.08 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg1L)
oC
0
19.00
3.88
1
19.00
3.77
2
20.00
2.06
3
20.00
1.76
4
20.00
1.72
5
20.00
0.43
6
20.00
0.28
7
20.00
0.24
8
20.00
0.23
9
20.00
0.23
10
20.00
0.21
11
20.00
0.17
12
20,00
0.17
13
20.00
0.17
14
20.00
0.17
15
20.04
0.17
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19.875
0.22 mglLlminute
0.63 (mglg)lhr
If sewage sludge is > 20°C, SOUR = 0.63 (mglg)lhr
If sewage sludge is < 20°C, SOUR = 0.63 (mglg)Ihr
SOUR passes if result is:5 1.5 (mglg)hr
Version 1111/11

City of Lumberton
Environmental Laboratory
specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 1/15/2020 7:08am KCL Dig# 2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0795 g
Weight of dish + dried solids: 130.1869 g
Weight of dried solids: 0.1074 g
Total Solids: 21.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
°C
0
20.00
5.12
1
20.00
3.94
2
20.00
1.94
3
20.00
0.95
4
20.00
0.56
5
20.00
0.48
6
20.00
0.40
7
20.00
0.37
g
19.00
0.34
g
19.00
0.32
10
19.00
0.30
11
19.00
0.30
12
19.00
0.30
13
19.00
0.26
14
19.00
0.26
15
19.00
0.26
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19.5
0.22 mg/Llminute
0.61 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = 0.62 (mglg)Ihr
if sewage sludge is < 20°C, SOUR = 0.63 (mglg)Ihr
SOUR passes if result is 5 1.5 (rnglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR)-)Aorksheet
Date & Analyst: 1116/2020 6:55am KCL Dig# 2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0340 g
Weight of dish + dried solids: 89.1434 g
Weight of dried solids: 0.10949
Total Solids: 21.88 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
5.25
1
20.00
3.02
2
20.00
1.47
3
20.00
0.79
4
21.00
0.41
5
21.00
0.24
6
21.00
0.14
7
21.00
0.13
g
21.00
0.11
g
21.00
0.10
10
21.00
0.10
11
21.00
0.09
12
21.00
0.09
13
21.00
0.09
14
21.00
0.08
15
21.00
0.08
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
20.75
0.21 mg/Llminute
0.57 (mglg)Ihr
If sewage sludge is > 20'C, SOUR = 0.55 (mglg)Ihr
If sewage sludge is < 20°C, SOUR = 0.54 (mglg)Ihr
SOUR passes if result is 15 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 1117/2020 7:51am KCL Dig# 2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5320 g
Weight of dish + dried solids: 120.6303 g
Weight of dried solids: 0.0983 g
Total Solids: 19.66 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
°C
0
19.00
5.60
1
18.00
3.89
2
18.00
1.74
3
17,00
0.93
4
17.00
0.49
5
17.00
0.38
6
17.00
0.23
7
17.00
0.17
8
17.00
0.14
9
17.00
0.13
10
17.00
0.12
11
17.00
0.12
12
17.00
0.12
13
17.00
0.11
14
17.00
0.10
15
17.00
0.10
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
17.25
0.24 mg/Llminute
0.72 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = 0.83 (Piglg)Ihr
If sewage sludge is < 20°C, SOUR = 0.87 onglg)Ihr
SOUR passes if result is :5 1.5 (mgfg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 1/21/2020 6:48am KCL Dig# 2 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9520 g
Weight of dish f dried solids: 122-0588 g
Weight of dried solids: 0.1068 g
Total Solids: 21.36 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg1L)
oC
0
11.00
fi.02
1
10.00
5.56
2
10.00
5.03
3
10.00
4.75
4
10.00
4.56
5
10.00
4.32
6
10.00
4.11
7
11.00
3.90
8
11.00
3.69
9
11.00
3.47
10
11.00
3.27
11
11.00
3.06
12
11.00
2.90
13
11.00
2.68
14
11.00
2.48
15
11.00
2.25
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
10.625
0.23 mg/L/minute
0.65 (mglg)lhr
If sewage sludge is > 20°C, SOUR = 1.02 (mglg)Ihr
If sewage sludge is < 20°C, SOUR = 1.22 (mglg)Ihr
SOUR passes if result is:5 1.5 (mglg)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 1/22/2020 12:28pm KCL Dig# 2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2414 g
Weight of dish + dried solids: 121.3500 g
Weight of dried solids: 0.1086 g
Total Solids: 21.72 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
oC
0
14.00
6.97
1
14.00
6.89
2
13.00
6.56
3
13.00
6.27
4
13.00
6.00
5
13.00
5.83
6
14.00
5.64
7
13.00
5.36
8
13.00
5.08
9
13.00
4.91
10
13.00
4.69
11
14.00
4.47
12
14.00
4.29
13
14.00
4.07
14
14.00
3.88
15
14.00
3.68
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
13.5
0.22 mg/Llminute
0.62 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = (mglg)Ihr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is 5 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Work -sheet
Date & Analyst: 1/23/2020 9:02am KCL Dig# 2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 92.9734 g
Weight of dish + dried solids: 93.0676 g
Weight of dried solids: 0.0942 g
Total Solids: 18.84 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
oC
0
13.00
6.97
1
11,00
6.39
2
11.00
6.56
3
10.00
6.27
4
11.00
6.00
5
11.00
5.83
6
11.00
5.64
7
11.00
5.36
8
11.00
5.08
9
11.00
4.91
10
11.00
4.69
11
12.00
4.47
12
12.00
4.29
13
12.00
4.07
14
12.00
1 3.88
15
12.00
1 3.63
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
11.375
0.22 mglLlminute
0.71 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = (mglg)lhr
If sewage sludge is < 20°C, SOUR = (mglg)Ihr
SOUR passes if result is:5 1.5 (mglg)hr
version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4/15/2020 7:03am KCL Dig#
Total Solids
Sample volume used for total solids test; 5 mL
Weight of dish: 121.2469 g
Weight of dish + dried solids: 121.3450 g
Weight of dried solids: 0.0981 g
Total Solids: 19.62 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
18.00
5.99
1
18.00
4.87
2
1 B.00
3.79
3
18.00
2.65
4
18.00
1.50
5
18.00
0.87
6
18.00
0.30
7
18.00
0.21
8
19.00
0.20
9
19.00
0.18
10
19.00
0.16
11
19.00
0.14
12
19.00
0.11
13
19.00
0.09
14
19.00
0.08
15
19.00
0.08
Oxygen Consumption Rate
SOUR
0.34 mg/Llminute
1.03 (mglg)Ihr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
18.5
If sewage sludge is > 20'C, SOUR = (mglg)Ihr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is 5 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 4/16/2020 5:46am KCL Dig# 2 Uay.
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0794 g
Weight of dish + dried solids: 130.1764 g
Weight of dried solids: 0.0970 g
Total Solids: 19.4 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
°C
0
18.00
6.50
1
18.00
5.40
2
18.00
3.80
3
18.00
1.76
4
18.00
0.77
5
18.00
0.69
6
18.00
0.65
7
18.00
0.60
8
18.00
0.56
g
18.00
0.50
10
18.00
0.48
11
17.00
0.45
12
17.00
0.41
13
17.00
0.41
14
18.00
0.39
15
18.00
0.36
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
17.8125
0.31 mglLlminute
0.96 (mglg)lhr
If sewage sludge is > 20°C, SOUR = (mglg)Ihr
If sewage sludge is < 20°C, SOUR = (mglg)lhr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 4/17/2020 5:41am KCL Dig# 2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4076 g
Weight of dish + dried solids: 111.5089 g
Weight of dried solids: 0.1013 g
Total Solids: 20.26 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
17.00
6.04
1
17.00
5.96
2
17.00
3.02
3
17.00
2.24
4
17.00
1.67
5
17.00
0.87
6
17.00
0.74
7
17.00
0.60
g
17.00
0.63
9
17.00
0.54
10
17.00
0.49
11
17.00
0.45
12
17.00
0.41
13
17.00
0.39
14
17.00
0.38
15
17.00
0.36
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
17
0.31 mg/Llminute
0.93 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = (mglg)/hr
If sewage sludge is < 20°C, SOUR = (mglg)Ihr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 111101

City of Lumberton
Environmental Laboratory
S ecific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 4/20/2020 6:58am big# 2 Day 4 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: . 121.96201 g
Weight of dish + dried solids: 122. 7705 g
Weight of dried solids: 0.1085 g
Total Solids: 21.7 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
oC
0
19.
1.01
1
19.00
0.55
2
19.00
0.47
3
19.00
0.44
4
19.00
0.38
5
19.00
0.37
6
19.00
0.37
7
19.00
0.33
g
19.00
0.33
g
19.00
0.32
10
19.00
0.32
11
19.00
0.29
12
19.00
0.28
13
19.00
0.28
14
19.00
0.28
15
19.00
0.27
Oxygen Consumption Rate 0.03 mglLlminute
SOUR 0.08 (mglg)lhr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
If sewage sludge is > 20°C, SOUR = (mglg)Ihr
If sewage sludge is < 20°C, SOUR = (mglg)Ihr
SOUR passes if result is 5 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Workshoet
Date & Analyst: 412112020 7:eeam TLS big# 2 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4614 g
Weight of dish + dried solids: 125.5680 g
Weight of dried solids: 0.1066 g
Total Solids: 21.32 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
17.00
3.95
1
17.00
2.21
2
17.00
0.56
3
17.00
0.30
4
17.00
0.23
5
17.00
0.22
6
17.00
0.22
7
17.00
0.21
8
17.00
0.20
9
17.00
0.20
10
17.00
0.20
11
17.00
0.19
12
17.00
0.19
13
17.00
0.18
14
17.00
0.17
15
17.00
0.17
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
0C
17
0.13 mg/l_/minute
0.37 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = 0.43 (mglg)Ihr
If sewage sludge is < 20°C, SOUR = 0.45 (mglg)/hr
SOUR passes if result is 5 1.5 (mglg)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate {SOUR) Work -sheet
Date & Analyst: 4/22i2020 6:57am TLS Dig# 2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 92.9603 g
Weight of dish + dried solids: 93.0596 g
Weight of dried solids: 0.0993 g
Total Solids: 19.86 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
17.00
6.16
1
17.00
5.77
2
17.00
5.36
3
17.00
4.94
4
17.00
4.56
5
17.00
4.18
6
17.00
3.80
7
17.00
3.35
g
17.00
2.93
g
17.00
3.50
10
11
17.00
17.00
2.10
1.67
12
17.00
1.25
13
17.00
0.80
14
17.00
0.35
15
17.00
0.18
Oxygen Consumption Rate 0.41 mg/Llminute
SOUR 1.22 (mglg)Ihr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
4C
17
If sewage sludge is > 20°C, SOUR =
If sewage sludge is < 20°C, SOUR =
SOUR passes if result is:5 1.5 (mglg)hr
Version 1111/11
mglg)Ihr
mglg)Ihr

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 4/23/2020 6:50am TLS Dig# 2 Day 7
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
5
125.4554
125.5603
0.1049
20.98
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
17.00
7.60
1
17.00
7.27
2
17.00
6.95
3
17.00
6.56
4
17.00
6.24
5
17.00
5.94
6
17.00
5.57
7
17.00
5.19
8
17.00
4.79
g
17.00
4.43
10
17.00
4.01
11
17.00
3.59
12
17.00
3.16
13
18.00
2.77
14
18.00
2.35
15
18.00
1.94
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
17.1875
mL
9
9
9
g/L
0.38 mg1Llminute
1.08 (mglg)Ihr
If sewage sludge is > 2WC, SOUR = 1.24 (mglg)Ihr
If sewage sludge is < 20°C, SOUR = 1.31 (mglg)Ihr
SOUR passes if result is <_ 1.5 (mglg)hr
Version 1111111

City of Lumberton
Total Solids Analysis Worksheet
SM 2540 B. 2011
FOR PROCESS CONTROL ONLY
Sample # f -T+
�C
Checked by: Sample Day & Date:
Date & Time IN Oven: c]�� Q � � - 1 O cum_ Date & Time OUT of Oven eq: A
Analyst(s): Analyst(s): KC-1..
g = Grams, Wt = Weight Date & Time Completed 2 i
EME!
(g)
I
Solids
BOW*
Me M410 A
Mt. am
Owl,
M
19-4.
"ING
M I MV.6
. �-ffimsaz
MMMMM�M�'
% W-O.
r
Erene
I Mms 0
M.,
% Solids Calculation: Total Solids mg1l Calculation:
Dried Wt. Diff (g) %Total Dried Wt. Diff (g) x 1000
Sample Wet Wt. (g) X 100 Solids Volume (mis) Total Solids mg11
Dish # -- :--....,.-----:—:------.ter—„—Dish # -----------------------:—:--
}0 0. �2'1 x 100 =
L , 64o-7
19 0. J-4U0 x 100 =
y . 4Cy`l
CA 0.12$1 x 100 =
x 100 =
11 0' 8qsylo x 100 =
O� x 100 =
°lam
> 3%
3 o/
a
2-Va -V 3
> 2�1�
a
1 Initially use 50mis for Known and Unknowns samples and 25mis for regular samples.
it Knowns and Unknowns mulitply using 1,000,000
3. The sample volume must yeild at least 2.5 mg of residue.
4. To get the Wet Weight; subtract the Tare Weight from the Tare + Sample Weight
X1000 _
x1000
x1000 =
X1000
Known Certified Value:
Known Value Obtained:
Limit Range:
Revised 4/21/2020 T. Smith

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheef
Date & Analyst: 7115/2020 7.03am TLS Dig# 2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 92.9608 g
Weight of dish + dried solids: 93.0652 g
Weight of dried solids: 0.1044 g
Total Solids: 20.88 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
3.30
1
24.00
1.42
2
24.00
1.20
3
24.00
0.89
4
24.00
0.61
5
24.00
0.53
6
24.00
0.48
7
24.00
0.42
8
24.00
0.38
9
24.00
0.34
10
24.00
0.31
11
24.00
0.30
12
24.00
0.28
13
24.00
0.28
14
24.00
0.27
15
24.00
0.27
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
OC
24
0.12 mg/L/minute
0.34 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = �Mllllll(mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 1/16/2020 7:50am FLS Dig# 2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2459 g
Weight of dish + dried solids: 121.3447 g
Weight of dried solids: 0.0988 g
Total Solids: 19.76 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
3.79
1
24.00
1.64
2
24.00
1.35
3
24.00
1.20
4
24.00
1.16
5
24.00
1.06
6
24.00
1.01
7
24.00
0.96
8
24.00
0.80
9
24.00
0.71
10
24.00
0.66
11
24.00
0.63
12
24.00
0.47
13
24.00
0.36
14
24.00
0.30
15
24.00
0.27
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
24
0.14 mg/L/minute
0.42 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = N�ffmg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7/17/2020 6:18am TI.S Dig# 2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9558 g
Weight of dish f dried solids: 122.0558 g
Weight of dried solids: 0.1000 g
Total Solids: 20 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
aC
0
24.00
6.70
1
24.00
5.20
2
24.00
3.66
3
24.00
1.82
4
24.00
0.70
5
24.00
0.51
6
24,00
0.43
7
24.00
0.39
8
24.00
0.37
9
24.00
0.35
10
24.00
0.33
11
24.00
0.31
12
24.00
0,30
13
24.00
0.29
14
24.00
0.27
15
24.00
0.27
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.32 mglLlminute
0.95 (mglg)Ihr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.78....'; r (mglg)lhr
If sewage sludge is < 20°C, SOUR = (mglg)Ihr
SOUR passes if result is:5 1.5 (mglg)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst; 7/20/2020 5:39am kcl Dig# 2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2458 g
Weight of dish + dried solids: 121.3386 g
Weight of dried solids: 0.0928 g
Total Solids: 18.56 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
oC
0
25.00
5.20
1
25.00
2.96
2
25.00
1.74
3
25.00
0.93
4
25.00
0.71
5
_
25.00
0.68
6
25.00
0,44
7
25.00
0.40
8
25.00
0.37
9
25.00
0.36
10
25.00
0.35
11
25.00
0.34
12
26.00
0.33
13
26.00
0.33
14
25.00
0.32
15
25.00
0.32
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
QC
25.125
0.20 mg/Llminute
0.63 (mglg)Ihr
If sewage sludge is > 20°C, SOUR = (mg/g)Ihr
If sewage sludge is < 20°C, SOUR = r Y.
SOUR passes if result is:5 1.5 (mglg)hr
Version 1 1Yl111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 712112020 6:01am kcl Dig# 2 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 123.1048 g
Weight of dish { dried solids: 123.1981 g
Weight of dried solids: 0.0933 g
Total Solids: 18.66 gIL
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
25.00
6.20
1
25.00
5.10
2
25.00
3.72
3
25.00
2.50
4
25.00
1.41
5
25.00
0.62
6
25.00
0.45
7
25.00
0.39
8
25.00
0.36
9
25.00
0.34
10
25.00
0.33
11
25.00
0.32
12
25.00
0.32
13
25.00
0.31
14
25.00
0.31
15
25.00
0.31
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.32 mg/Llminute
1.03 (mglg)Ihr
Average Sewage Sludge
Temperature During Test
aC
25
If sewage sludge is > 20°C, SOUR =;;: D,,,' (mg/g)/hr
If sewage sludge is < 20°C, SOUR =
: (mg/g)/hr
SOUR passes if result is :5 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7/2212020 5:43am kcl Dig# 2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4574 g
Weight of dish + dried solids: 125,5489 g
Weight of dried solids: 0.0915 g
Total Solids: 18.3 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
CC
0
24.00
6.11
1
25.00
5.11
2
25.00
3.87
3
25.00
3.82
4
25.00
3.36
5
25.00
3.07
6
25.00
2,71
7
25.00
2.56
8
25,00
2.11
9
25.00
1.49
10
25.00
1.21
11
25.00
0.94
12
25.00
0.80
13
25.00
0.61
14
25.00
0.33
15
25.00
0.28
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.36 mg/L/minute
1.17 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24.9375
If sewage sludge is > 20°C, SOUR = 0.92 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.84 (mg/g)/hr
SOUR passes if result is :5 1.5 (mg/g)hr
Version I1/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7/23/2020 5:48am kcl Dig# 2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.63811 g
Weight of dish + dried solids: 125.7259 g
Weight of dried solids: 0.0878 g
Total Solids: 17.56 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
25.00
7.14
1
26.00
6.17
2
25.00
5.21
3
25.00
4.20
4
26.00
3.25
5
25.00
2.37
6
25.00
1.59
7
25.00
0.80
8
25.00
0.44
9
25.00
0.35
10
25.00
0.33
11
25.00
0.31
12
25.00
0.30
13
25.00
0.30
14
25.00
0.30
15
25.00
0.29
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.20 mg/L/minute
0.68 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
CC
25.125
If sewage sludge is > 20°C, SOUR = 03..;: , _ (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 048, 7 (mg/g)/hr
SOUR passes if result is:5 1.5 (rng/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 10/19/2020 0634 am TLS Dig# 3 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.6359 g
Weight of dish + dried solids: 125.7415 g
Weight of dried solids: 0.1056 g
Total Solids: 21.12 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
4.67
1
20.00
3.18
2
20.00
2.03
3
20.00
1.00
4
20.00
0.89
5
20.00
0.81
6
20.00
0.77
7
20.00
0.68
8
20.00
0.63
9
20.00
0.59
10
20.00
0.50
11
20.00
0.43
12
20.00
0.40
13
20.00
0.21
14
20.00
0.19
15
20.00
0.11
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20,0625
0.20 mg/Llminute
0.58 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = I(mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is:5 1.5 (mglg)hr
Version 111111I

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 10/20/2020 0630 am TLS Dig# 3 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 123.1055 g
Weight of dish + dried solids: 123.2076 g
Weight of dried solids: 0.1021 g
Total Solids: 20.42 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mglL)
oC
0
20.00
4.39
1
20.00
2.85
2
20.00
2.60
3
20.00
2.51
4
20.00
2.40
5
20.00
2.22
6
20.00
2.00
7
20.00
1.97
8
20.00
1.72
9
20.00
1.30
10
20.00
1.21
11
20.00
0.83
12
20.00
0.66
13
20.00
0.58
14
20.00
0.52
15
20.00
0.40
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20
0.22 mglL/minute
0.64 (mglg)/hr
If sewage sludge is > 20°C, SOUR = 0.64 (mglg)Ihr
If sewage sludge is < 20°C, SOUR = 0..64 (mglg)lhr
SOUR passes if result is:5 1.5 (mglg)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 10121/2020 0625 am TLS Dig# 3 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: ffl25.7431
g
Weight of dish + dried solids; g
Weight of dried solids: g
Total Solids: g/L
SOUR
:;TZime
Temperature
Dissolved
Oxygen (mg/L)
oC
21.00
2.63
1
21.00
1.97
2
21.00
1.80
3
21.00
1.69
4
21.00
1.45
5
21.00
1.21
6
21.00
1.00
7
21.00
0.87
8
21.005
0.60
9
21.00
0.51
10
21.00
0.43
11
21.00
0.36
12
21.00
0.26
13
21.00
0.26
14
21.00
0.25
15
21.00
0.25
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
21
0.15 mglL/minute
0.42 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.40 (mg/g)/hr
If sewage sludge is < 20'C, SOUR = 0.39 (mg/g)/hr
SOUR passes if result is:5 1.5 (mglg)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
S eCifiC OxVgen Uptake Rate SOUR Worksheet
Date & Analyst: 10122/2020 0628 am TILS Dig# 3 bay 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: ff.qg/L
g
Weight of dish + dried solids: g
Weight of dried solids; g
Total Solids:
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
22.00
3.87
1
22.00
2.80
2
22.00
2.69
3
22.00
2.38
4
22.00
2.01
5
21.00
1.72
6
21.00
1.26
7
21.00
0.96
8
21.00
0.76
9
21.00
0.69
1 D
21.00
0.64
11
21.00
0.59
12
21.00
0.54
13
21.00
0.52
14
21.00
0.46
15
21.00
0.41
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
M
ewage Sludgere During Test°C.3125
0.21 mg/L/minute
0.60 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.55 (mg/g)/hr
SOUR passes if result is:5 1.5 (rng/g)hr
Version 1111111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 10123/2020 0635 am TI_S Dig# 3 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.6368 g
Weight of dish f dried solids: 125.7430 g
Weight of dried solids: 0.1062 g
Total Solids: 21.24 gIL
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg1L)
CC
0
21.00
4.$0
1
21.00
4.41
2
21.00
3.74
3
21.00
2.90
4
21.00
2.08
5
21.00
1.47
6
21.00
1.17
7
21.00
0.83
8
21.00
0.70
9
21.00
0.66
10
21.00
0.64
11
21.00
0.58
12
21.00
0.54
13
21.00
0.53
14
21.00
0.49
15
21.00
0.46
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
21
0.28 mglL/minute
0.78 (mglg)lhr
If sewage sludge is > 20°C, SOUR = El(mg/g)/hr
(mglg)Ihr
If sewage sludge is < 20°C, SOUR = EE0.7
SOUR passes if result is :51.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 10126/2020 05:57am am kcl Dig#;c 3 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.6364 g
Weight of dish + dried solids: 125,7380 g
Weight of dried solids: 0.1016 g
Total Solids. 20.32 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
7.57
1
20,00
7.37
2
20.00
7.30
3
20.00
7,16
4
20.00
7.01
5
20.00
6.86
6
20.00
6.53
7
20.00
6.35
8
20.00
6.17
9
20.00
5.99
10
20.00
5.83
11
20.00
5.64
12
20.00
5.45
13
20.00
5.26
14
20.00
5.06
15
20.00
4.86
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
aC
20
0.18 mg/L/minute
0.54 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.5A (mglg)/hr
If sewage sludge is < 20°C, SOUR = EEO.54 (mg/g)/hr
SOUR passes if result is 5 1.5 (mg/g)hr
Version 1111/91

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate SOUR Worksheet
Date & Analyst: 10127/2020 05:53 am kci Ding# 3 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2463 g
Weight of dish + dried solids: 121.3535 g
Weight of dried solids: 0.1072 g
Total Solids: 21.44 gIL
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
20.00
7.91
1
19.00
7.35
2
19.00
7.24
3
19.00
7.10
4
19.00
7.00
5
19.00
8.83
6
19.00
6.69
7
19.00
6.52
8
19.00
6.37
9
19.00
6.21
10
19.00
5.96
11
19.00
5.91
12
19.00
5,71
13
19.00
5.56
14
19.00
5.41
15
19.00
5.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19.0,625
0.16 mg/L/minute
0.45 (mglg)/hr
If sewage sludge is > 20°C, SOUR ='_.!- q:x„ (mglg)Ihr
If sewage sludge is < 20°C, SOUR =. ;w'._{ ,�$iK;k (mglg)/hr
SOUR passes if result is15 1.5 (mglg)hr
Version 1111/11