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HomeMy WebLinkAboutWQ0001990_2017 Residual Annual Report_20171201 Annual Report Review Class A Distribution l.� D�j' Reporting Period: I �1 - t 2/31 /1 Permit Details: W Is 503?Y Class®or B? Maximum Dry Tons Per Year: 5 CAD • Number of acres permitted: N h Number of fields in permit: NA Counties that land is permitted for: ►JA • Monitoring Frequency for TCLP: 4j, I W-01 • Monitoring Frequency for Residuals Analysis:8a�'A u.()"+ 15A - Monitoring Frequency for Pathogen&Vector Attraction Reduction: B-,p6j Pu 1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form�( / Was a certification form submitted? r +/ Was distribution conducted during e reported period?y 1 �\ Dr • How many dry tons were produced and distributed? le Y /lp 0 1 Were the distributions with the permitted amount? Were recipients information listed?y Did it indicate compliance? 1 • Was form complete?� Was it signed by the ppropriate people?�/ 2. Monitoring Were the analyses conducted at the required frequency?y °""� ' R( '; e Was an analyses taken for each source that was distributed? AKaIkg Ids ©'- res�� .S c3�y Were the metals analyses reported on the Residual Sampling Summary Form? Were the results reported in mg/kg? qr _ Were the pH's 6.0 or greater for each residual sample? 4'� 11�= �� rook Were the heavy metals within ceiling concentration permit limits?\r , riV = :3 w-- Were the lab analyses attached? Were all the required parameters tested �� 5 ��� V �d u� lS'✓ M ���}1�W�r Was TCLP analysis conducted? o N c d n^(� ,Lc h[_e es jd (s `�" Were the TLCP contaminants within regulatory limits?y epR C'm� �s Was a corrosivity, ignitability, and reactivity analysis conducted?�/ o0 ca+wp� 5�c� Rom; � 1 b�tk Souete -CSj&e- 411ti 3. Pathogen and Vector Attraction Reduction Aa d Z4,1b+giJ 4ukt Was a signed copy of the Pathogen anVector Attractioneduction Form submitted? �o � ; Did the form indicate the eriod of coverage,the residual class,and the p thogen reduction alternative and the vector a raction reduction option u d? • Was the appropriate documentation to show patho en and vector attraction reduction included in the report? Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? Class A Pathogen Review To be Class A,residuals shall meet either fecal Coliform density or salmonella density. jam`? —,7ri W_gx4 A&, A6 1` 6 ktit a0 "kt Uk comp o-xi— _ Fecal Coliform density Was the sampling conducted at the required frequency? Were multiple samples taken? alb Was each sample less than 1000 MPN/gram of total solids? OR Salmonella density Was the sampling conducted at the required frequency? Were multiple samples taken? Was each sample less than 3 MPN/4 grams of total solids? To be Class A,residuals shall meet one of the following alternatives: Alternative 1 —Time/Temperature Were the residuals maintained for correct time and temperature? Were logs submitted showing time and temperature? Were temperatures within range for complete time period? Alternative 2—Alkaline Treatment Were logs submitted showing time and temperature? Was the pH raised to 12 or greater and maintained for 72 hours or longer? Was the temperature 52°C(126°F)for 12 hours or longer while the pH was 12 or greater? Were logs submitted showing time and pH? Was the temperature corrected to 25°C(77°F)? Alternative 5 —Process To Further Reduce Pathogens PFRP Composting • Were the within-vessel method or static aerated pile methods used? • Was the residuals temperature maintained at 55°C (131°F)or higher for three consecutive days or longer in the within-vessel method or static aerated pile method? OR •�- / Was the windrow composting method used? Was the residuals temperature maintained at 55°C or higher for 15 consecutive days or longer in the windrow method, and the windrow turned a minimum of five times during this time? PFRP Heat Drying • Was the residuals dried by direct or indirect contact with hot gases and the moisture content of residuals reduced to 10% or lower? • Did the temperature of the residuals or the of the wet bulb temperature of the gas in contact with the residuals as the residuals leave the dryer exceed 80°C(176°F)? Vector Attraction Reduction Review • Was the sampling conducted at the required frequency? Option 1 —38%Volatile Solids Reduction Was there 38%reduction? Were lab sheets/calculations in report? Was the reduction on volatile solids(not total solids)? Were the samples taken at beginning of digestion process and before application (Inspection)? Were calculations correct? Option 2—40-Day-Bench Scale Test Were residuals from anaerobically digested treatment(Inspection)? Were residuals anaerobically digested in lab? Was the test run for 40 days? Was the test done between 30°C (86°F) and 370C (99°F)? Was the reduction of on volatile solids(not total solids)? Was the reduction less than 17%? Were lab sheets/calculations in report? Were calculations correct? Option 3 —30-Day Bench Scale Test Were residuals from aerobically digested treatment(Inspection)? Were residuals aerobically digested in lab? Were residuals 2% or less total solids? If not 2%total solids,was the test ran on a sample diluted to 2%with unchlorinated effluent? Was the test run for 30 days? Was the test done at 20°C(68°F)? Was the reduction of on volatile solids(not total solids)? Was the reduction less than 15%? Were lab sheets/calculations in report? Were calculations correct? Option 4—Specific Oxygen Uptake Rate(SOUR) Were residuals form aerobically digested treatment(Inspection)? Were residuals 2% or less total solids(dry weight basis)(not diluted)? Was the test done between 10°C(50°F) and 30°C(86°F)? Was the temperature corrected to 20°C (68°F)? Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids(dry weight basis)? Was the sampling holding time two hours? Was the test started within 15 minutes of sampling or aeration maintained? Option 5— 14-Day Aerobic Process Were the residuals from aerobically digested treatment(Inspection)? Were the residuals treated for 14 days? Was the residuals temperature higher tI 40°C(104°F)for a 14-day period? ' Was the average residuals temperature higher than 450C(113°F)?�� Option 6—Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? Did the pH of residuals remain at 12 or higher for two hours without the addition of more alkali? • Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? Was the pH corrected to 25°C (77°F)? r Option 7—Drying of Stabilized Residuals Does the residuals contain any unstabilized residuals? Were the residuals mixed with any other materials? Were the residuals dried up to 75%total solids? Option 8—Drying of Unstabilized Residuals Were the residuals mixed with any other materials? Were the residuals dried to 90%total solids? Option 9—Injection • Was there any significant amount of residuals on land surface one hour after injection (Inspection)? Was injection done on pasture or hay field? Was injection done at time that crop was growing? If Class A with respect to pathogen,were residuals injected with eight hours after discharge from pathogen treatment? 4.General Was the report in the proper format?y Was the annual report complete? I Was the report submitted on time?� C I TOWN OF VALDESE. LAKE RHODHISS WWTP 2100 Lake Rhodhiss P.O. Box 339 Valdese,-N.C. 28690 (828) 879 - 2131 February 13, 2018 North Carolina Department of Environmental and Natural Resources Division of Water Resources Water Quality Permit Section Non-Discharge Permit Unit �� 1636 Mail Service Center Raleigh, NC 27699-1636 F� Enclosed is our 2017 composted sludge report,which includes Form DMSDF, supplementary Information,Form RSSF,the lab sheets, and Form PVRF 02T.Also included are all additional supporting materials including,recipients,temperatures and process description. In the interest of conservation, information is contained on both sides of each sheet of paper(where applicable). If you require additional information concerning the report,please contact us at the above number. Regards, �-� FFES ivisiaoaYcr Resourcos 2 6 2018 As /5", plater nUality Regional Operations Greg A. Padgett Water Resources Director / ORC State Non-Discharge Permit for Composted Sludge WQ0001990 State NPDES NC0041696 2017 Name Address Usage #of Scoops Aaron Byrd Valdese soil amendment 110 Bob Stoughton 4701 Burns Rd, Granite Falls soil amendment 6.25 Curtis Cates 4951 Cornerstone Lane, Connelly Springs soil amendment 0.5 Dann 's Bulldozing soil amendment 41 David Perry, 2118 Coy Lane, Morganton soil amendment 0.25 Dennis Barus 3311 Barus St., Valdese soil amendment 0.5 Donnie Smith 2071 Flat Gap Rd,Valdese soil amendment 140 Frank Buff 2555 Rid eview,Valdese soil amendment 1 'Gene Gouge 2253 Liberty Ch Rd, Hickory soil amendment 2.5 Harold Rillo 5875 Faris Loop, Morganton soil amendment 4 Ivan Sain soil amendment 0.5 James Hinson 2485 Lone Pine Place, Lenoir soil amendment 0.5 Jerry VanHorn 5891 Miller Bridge Rd, Connelly Springs soil amendment 8 John Dubry 1007 Faet St. SW,Valdese soil amendment 2 Key Mobley Paradise Harbor, Connelly Springs soil amendment 2 Paul Barnes 3886 Glilland Hall, Lenoir soil amendment 2 Phil Eller Flat Gap Rd, Valdese soil amendment 304 Regina Hess 5860 Miller Bridge Rd, Connelly Springs soil amendment 9 Rocky Taylor 5932 Miller Bridge Rd, Connelly Springs soil amendment 214 Roger Edwards 5481 Parkview, Lenoir soil amendment 1.5 Settlem re Nursery Drexel Rd,Valdese soil amendment 230 Steve Hildebran 4077 Cook Rd. Ext, Valdese soil amendment 2.5 Tom Morris 11091 Iris Place, Granite Falls soil amendment 4.5 Total Scoops 1086.5 r I - CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT#: 1990 FACILITY NAME: Lake Rhodhiss Wastewater Treatment Plant PHONE: 828-879-2131 COUNTY: Burke OPERATOR: Greg Padgett FACILITY TYPE(please check one): ® Surface Disposal(complete Part A(Source(s)and "Residual In"Volume only)and Part C) p Distribution and Marketing(complete Parts A,B,and C) Was the facility in operation during the post calendar ear? Yes El No ® -o- If No skip arts A,B,C and certify form below Part A*: Part B*• Sources(s)(include NPDES#if Amen Bulking Agent tons Reci Tent Information Month applicable) g Ag .ent Residual In Product Out Name(s) Volume(dry tons) Intended use(s) January NCO041696 19.21 3.85 23.06 Soil Amendment February NCO041696 3.51 0.7 4.22 Soil Amendment March NCO041696 18.04 3.62 21.66 Soil Amendment April NCO041696 169.83 34.07 203.91 Soil Amendment May NCO041696 67.23 13.49 80.72 Soil Amendment June NCO041696 1.17 0.23 1.41 SEE ATTACHED SHEET Soil Amendment July NCO041696 0.23 0.05 0.28 Soil Amendment August NCO041696 71.68 14.38 86.06 Soil Amendment September NCO041696 46.03 9.23 55.27 Soil Amendment _ October NCO041696 79.06 15.86 94.92 Soil Amendment November NCO041696 32.33 6.49 38.81 Soil Amendment December NCO041696 0.7 0.14 0.84 Soil Amendment Total from FORM DMSDF sup) Totals: Annual d tons 509.02 ;1:02'1 1 ,_a" 611 16 ,Amendments used:I Wood Chips -- BuMniz Agent(s)used: *If more space is required,attach additional information sheets(FORM DMSDF(supp)): Total Number of Form DMSDF(Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below)issued by the Division of Water Resources: 11 No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached. 2._All operation and maintenance requirements were compiled with or,in the case of a deviation,prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." 1 r . /3 Signature f Permittee D to Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) nMio rnORA notAcnr i4,i)nnc% 2017 COMPOST DISTRIBUTED IN DRY TONS Month #of Scoots Loaded Amendment(DT) Residuals (DT) (DT) Distributed January 41 19.21 3.85 23.06 February 7.5 3.51 0.70 4.22 Mar 38.5 18.04 3.62 21.66 April 362.5 169.83 34.07 203.91 May 143.5 67.23 13.49 80.72 June 2.5 1.17 0.23 1.41 July 0.5 0.23 0.05 0.28 Aug 153 71.68 14.38 86.06 l Sept 98.25 46.03 9.23 55.27 Oct 168.75 79.06 15.86 94.92 Nov 69 32.33 6.49 38.81 Dec 1.5 0.70 0.14 0.84 TOTAL 1086.5 509.0 102.1 611.2 Dry Weight of 1 % Solids Scoop % Cake 38 1125,, 16.71 Z C by %Solids=average percent solids of compost from lab test Dry weight of 1 scoop=3000 Ibs wet weight times%solids average %Cake=average%solids from operator centrifuge solids testing sheet � 32-� ANNUAL RESIDUAL SAMPLING SUMMARY FORM 4D Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FOP.M RSSF-B WQ Permit Number: 1990 Laboratory: 1) Blue Ridge Labs(NC Lab#275) Facility Name: Lake Rhodhiss Wastewater Treatment Plant 2) Residual Source WQ#or �, 3) A NPDES#: NCO041696 R ��� 4) Mll� WWTP Name: Lake Rhodhiss Wastewater Treatment Plant APR 2 6 2018 5) DWRResidual Analysis Data XION ggQCESECTION SING UNIT Conc. Sample or Composite Date Parameter Limit (mg/kg) m Lk a 1-30-17 3-31-17 6-2-17 7-31-17 10-9-17 12-11-17 Percent Solids(%) NA 20.1 14.4 ✓ 16.1 v 15.9'' 14.8 18.3 Arsenic 75 * � t ,c},' * * 1 *' c„ *j,;lZ * Indicates Sample is below MQL Cadmium 85. Copper 4,300 263 ✓ 201 ✓ 113 266✓ lb5-✓ 1'99 Chromium NA Lead 840 *(�� g Be� (�•% Mercury 57 O.Oj-J 0.0717 0.063 0.043 0.6-23v 0.0591 Molybdenum 75 *,� * * 'r; ) ; Nickel 420 _ * :�-t: ) 20:2 Selenium 100 Zinc 7,500 11517 1095 2065 V h Total Phosphorus NA 17811" 16992 v 26087 181' Ml4v 18584 �<; ' �, 0 TKN NA 8905 8507 V 8472 v 9006 8756 ✓ 8650 Ammonia-Nitrogen NA 2831 • 3270 3055 3916 4979 3169 b Nitrate and Nitrite NA 224 �/ 312 279 243 362 253 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. L6I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant p alties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Signature of repar r Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM RSSF(12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Pvrmit Number: WQ0001990 Laboratory: 1) Blue Ridge Labs (NC#275 ) Facility Name: Lake Rhodhiss WWTP 2) Residual Source NC 0041696 3) NPDES#or WQ#: 4) WWTP Name: Lake Rhodhiss WWTP 5) Residual Analysis Data r (,I-,B St\w�A Na GDk I Sample or Composite Date Parameter (mg/kg) 1-30-17 3-31-17 6-2-17 7-31-17 10-9-17 12-11-17 Aluminum 20560 19958 P 17876 t, 20145 v 19695 17218 v Calcium 6730 6521 V 10212 v. 8954 V 10845 v 8011,/ Magnesium 1812 1756 v 1836 V 1794 V 1807 2748 ✓ * Indicates Sample is below MQL Potassium 2497 ' 470 436 ✓ 308/ 2824✓ 3622 ( 5 ?7 Sodium 313 ✓ 3638 ✓ 435 , 449 V 5324 V 2601 i� ?7 PAN 3055 3582 ✓ 3341 4159v 5341✓ 3422 -pH( S.U. ) 10.3 5.1. ✓ 10.5✓ 9.9 V 8.2 ✓ 10.1 ✓ Ignitability Not Ign. Not Ign. Not Ign. Not Ign. Not Ign. Not Ign. Corrosivity as pH 10.3 ✓ 5.1 10.5✓ 9.9 ✓ 8.2 10.1 Reactivity ) * ✓ ✓ * ✓ ✓ "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are si ificant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Lq Signature of birepariV Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM RSSF- B(12/2006) Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 - blueridgelabslenoir@gmaii.com Client: Town of Valdese P. O.Box 339 Valdese,N. C.28690 s, Attention: Mr.C. Bortnick C, O Date Received: 31-Jan-17 Report Date: 09-Mar-17 Q Sample Date: 30-Jan-17 ash 0 BRL#:' BRL-2017-0055 Lab Sample ID: LSID-2017-00277 Client Sample ID: Cake Analysis aiysis Parameter Result MQL Unit Method Time ate Analyst Total Phosphorus 17811 18.9 dry mg/kg 200.7 1994 13:54 2/27,12017 KCJ Al by ICP-AES 20560 4.74 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ As by ICP-AES * 9.5 dry mg/kg 200.7 1994 13:54 2/27./2017 KCJ Ca by ICP-AES 6730 24.1 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Cd by ICP-AES * 0.1898 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Cu by ICP-AES 263 0.949 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ K by ICP-AES 2497 3.7 dry mg/kg 200.7 1994 13:06 2,120/2017 KCJ Mg by ICNAES 1812 4.74 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Mo by ICP-AES * 0.949 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Na by ICP-AES 313 18.5 dry mg/kg 200.7 1994 13:06 2120/2017 KCJ Ni by ICP-AES + 0.949 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Pb by ICP-AES * 9.5 dry mg/kg 200.7 1994 13:54 2!27/2017 KCJ Se by ICP-AES * 9.5 dry mg/kg 200.7 1994 13:54 2/27/2017 KCJ Zn by ICP-AES 1151 0.949 dry mg./kg 200.7 1994 13:54 2/27/2017 KCJ Hg by Cold Vapor AAS 0.0500 0.0477 dry mg/kg 7470A 1994 13:17 2/21/2017 KCJ Reported By: S.J D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 7 of 14 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoirOgmail.com Client: Town of Valdese P. O.Box 339 Valdese,N. C.28690 Attention: Mr.C.Bortnick Date Received: 31-Jan-17` Report Dater 09-Mar 17 Sample Date: `IN-Jan-17 BRL##: % BRL-2017-0055 Lab Sample ID: LSIU2017-00278 Client Sampl,ID: .Cake- Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 2831 404 dry mg/kg SM4500 199 13:04 2/17/2017 KCJ Reported By: S. .Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 8 of 14 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-OU9 blueridgelabsienoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690. Attention: Mr. C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 30-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00279 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 20.1 0.1 % %Solids 12:51 2/9/2017 KCJ Plt Available Nitrogen 3055 423 dry mg/kg Plant Availabl 13:20 2/24/2017 KCJ pH 10.3 0.1 SU SW-846-9040 10:20 2/9/2017 KCJ Reported By: S. hnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 9 of 14 Blue Ridge .dabs P4 Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N. C.28690 Attention: Mr.C. Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 30-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00280 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Y Nitrate+Nitrite Nitrogen(N2+ 224. 19 dry mg/kg 4500-NO3-E 11:22 2/2412017 KCJ Total Kjeldahl Nitrogen(TKN) 8905 964 dry mg/kg 4500-Norg B 9:01 2/16/2017 KCJ Reported By: S. .Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 10 of 14 > , t Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirCgmail.com Client: Town of Valdese P. O.Box 339 Valdese,N.C. 28690 Attention: Mr.C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 30-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00281 Client Sample ID: Cake Analysis Analysis Parameter _ Result MQL Unit Method Time Date Analyst ignitability Not Ignitable 70 Deg.F. 1030 SW-846 13:25 2/9/2017 KCJ Corrosivity as pH 10.3 0.1 su 9045C SW-8 10:20 2i9/2017 KCJ Reported By: S. ohnson,D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 I of 14 Blue Midge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr. C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 30-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00282 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivity as CN * 1 mg/kg SW-846-7.3.3 16:45 2/9!2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 14:22 2/9/2017 KCJ Reported By: S. Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 12 of 14 Blue Ridge Labs, Inc. yr P.O. Box 2940 Lenoir,NC 28645 Telephone(828)728-0149 Fax(828)728-0131 Chain of Custody NPDS Reporting Groundwater Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/Trust Fund Reporting Report To: Bill To: Town of Vladese Chris Hartnie Project Name: PO Number: Ice Present: Y N Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field ' Sample ID Sample Date Time Sulfide Present/ Field Dechlorinatibn pH Resid Temp Sampler Analysis Requested Type HIII Cheek Removed Check Chlor °C Initials °C Y N Y N Y N Y N PorA I - �'t �3 CA VE 00' _PA CA�,c�l�j N�f -ice ft,� r• �in �' Re ' ''shed Date: Time: R5!5� 1131117 05, -5 ec Date: Time: L - Upon submission of samples,client agrees that invoices are due at the time work is completed. Open accounts are due 20 days following invoice date. A finance charge of 1.5%per month will be imposed on all"due accounts. When relinquishing samples to Blue Ridge Labs(BRL),buyer authorizes BILL to perform only the analysis indicated above and also agrees to pay collection and attorney fccf the account becomes delinquent, Blue Ridge Labs reserves the right to deny documentation fbr any work where payment has not been made.in effect rendering that data unsupported for regulatory.purposes. ORL cannot guarantee that any regulatory authority will accept any work ,submitted,therefore it is the dient's responsibility to request on this form appropriate tests. NC DENR Cenined Lab#275 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com client: Town of Valdese P.O.Box 339 CwaterQ �.11R ® Valdese,N.C.28690 our., Attention: Mr.C. Bortnick Date Received: 04-Apr-17 32018 Report Date: 02-May-17eg�oSample Date: 31-Mar-17 nai pper Mons BRL fit: BRL-2017-0202 -� Lab Sample ID: LSID-2017-00869 `Client Sample ID k Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 16992 28.8 dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ Al by ICP-AES 19958 7.22 dry mg/kg 200.7 1994 -14:50 5/1/2017 KCJ As by ICP-AES * 14A dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ Ca by ICP-AES 6521 36.1 dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ Cd by ICP-AES * 0.2888 dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ Cu by ICP-AES 201 1A dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ K by ICP-AES 4708 34.7 dry mg/kg 200.7 1994 4127.12017 Summit Mg by ICP-AES 1756 . 7.2 dry mg/kg 200.7 1994 14:50 5/U2017 KCJ Mo by ICP-AES * I dry mg/kg 200.7 1994 '14:50 5/1/2017 KCJ Na by ICP-AES 3638 173 dry mg/kg 200.7 1994 4/27r2017 Summit Ni by ICP-AES * IA dry mg/kg 200.7 1994 14.50 5/1/2017 KCJ Pb by ICP-AES * 14.4 dry mg/kg 200.7 1994 14:50 5/l/2017 KCJ Se by ICP-AES * 14.4 dry mg/kg 200.7 1994 14:50 5/l/2017 KCJ Zn by ICP-AES 1095 1.4 dry mg/kg 200.7 1994 14:50 5/1/2017 KCJ Hg by Cold Vapor AAS 0.0717 0.658 dry mg/kg 7470A 1994 14:14 4/20/2017 KCJ Reported By: son,D.R.WssingeS.J. n e r *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.-Box 339 Valdese,N. C. 28690 Attention: Mr.C. P.p nick Date Received:;.:. ,04-Apr-17 Report Date: 02-May-17 Sample Date: 31-Mar-17 BRL#: BRL-2017-0202 Lab Sample ID: . LSID-2017-00870 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 3270 1061 dry mg/kg SM4500 199 14:50 5r11!2017 KCJ Reported By: S.J. son,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 2 of 6 Blue Ridge Labs PO Box 2940 .Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmall.com Client: Town of Valdese P.O.Box 339 Valdese,N. C.28690 Attention: Mr. C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 31-Mar-17 BRL 4: BRL-2017-0202 v Lab Sample ID: LSID-20.17-00871 Client Sample ID: Cake Analysis Analysis Parameter Result MQL unit Method Time Date Analyst %Solids 14.4 .0.I % %Solids 10:22 4!5;7017 KCJ Pit Available Nitrogen 3582 1086 dry mglkg Plant Availabl 16:59 5f1/2017 KCJ PH 5.1 0.1 SU SW-846-9040 9:12 4/5/2017 KCJ f Reported By: S. has, D.R.Wessinger "Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoirOgmail.com Client: Town of Valdese P. O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 31-Mar-17 BRL#: BRL-2017-6202 Lab Sample ID: LSID-2017-00872 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 312 24.5 dry mg/kg 4500-NO3-E 16:43 5/1,12017 KC] Total Kjeldahl Nitrogen(TKN) 8507 1380 dry mg/kg 4500-Norg B 10:l6 4/26/2017 KCJ Reported po 13y: . _. S.J. nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 31-Mar-17 BRL#: BRL-2017-0202 Lab Sample ID: LSID-2017-00873 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 11:40 4l5;2017 KCJ Corrosivity as pH 5.1 0.1 su 9045C SW-8 9:12 4i5.2017 KCJ Reported By: S.ijwnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 5 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-72"149 blueridgelabstenoi ftmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C. 28690 Attention: Mr.C. Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 31-Mar-17 BRL#: BRL-2017-0202 Lab Sample ID: LSID-2017-00874 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivity as CN * 1 m;/kg SW-846-7.3.3 16:47 4,6/2017 KCJ Reactivity as Sulfide * 5 mg,-kg SW-846-7.3.3 14:27 4,6.-2017 KC:J Reported By: S.I hnson,D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 6 MUM L &OW 0-Sz bZ9 WMPOS L MILM Bow 00'9 919 ujnpoe4od no ;sAlow 8080£MS on08MS (009)Sf$A*TVNV SIVIM pwApmv aleQ 3Q W.Ofl Tea 'Iad Mau sosiimv 699 (E[aldweg;uaro cli'IOS -Iw;vH 900'981 DOLT ¢W 4B'I srsjlloud Qo=ewgwl ,Parojd Wd OO:zz:l L T OVI£/£ :Siva aalf alloy 'oul`sgvT alprd an1H ZN I'I;3 PwodoN awa 98TROLT :#0/g 686i-ur(OEF) Xb'dI as-Est(0£f):mz (palmomoo) SZt6i•OPIO%71vd 0&7gmfn0 s �r.•. :t;-, rc=Cr_c.t, s .. . .- 'tS ulif}Olflwwnq £ oda� �aije>� ,,.I ra�so(ouyaaT 1a,uawuot?na�,�ew � , Blue Midge Labs, Inc. P.O. Box 2940 Lenoir,NC 28645 Telephone: (828)728-0 149 Fax(828) 728-0131 Chain of Custody NPDS Reporting Groundwater Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/"Trust Fund Reporting Report To: Bill To: Town of Vladese Chris Bortnie Project Name: _ PO Number: _ Ice Present: Y N (Field Preservatives Lab Check 'rime& Field Resid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested Type I-IR:MM Check Removed Check Chlor °C Initials °C Y N Y N Y N Y N PorA i,e•,q 1 «s� ��k . ph, N. M:,,Je- 2_,, At,01j",C,, lVc: (� M-t j p m i IJ:r Y j TKd, P. ? aAn �r u l ���'� � '��,t'1 �. � J � =5n�t�.l,.t,•f•y� C.a••�,.y.d.ry i e Re.l• Isliedy: . Date: Time: Rec ' Date- Time: 0 Upon submission of samples,client agrees that invoices are due at the time work is completed. Open accounts are(Inc 20 days following invoice date. A finance charge of 1.5%per month will be imposed on all pa�due accounts. When relinquishing samples to Blue Ridge Labs(BRl..),buyer authorizes IiRL to perform only the analysis indicated above and also agrees to pay collection and attorney Ice!the accoutre becomes delinquent, Blue Ridge Labs reserves the right to deny documentation ror any work where payment has not been made,in effect rendering drat data unsupported for regulatory purposes. 13121.eannot guarantee that any regulatory authority will accept any work Lab 11275 submitted,therctirre it is the client's responsibility to request on this l'ortn appropriate tests. NC'DENR L'erti6ed Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box'339 0 . Valdese,N.C.28690 Attention: Mr.C.Bortnick 9A9 9es Date Received: 05-Jun-17 Report Date: 08-Aug-17 gshP4�i Sample Date: 02-Jun-17 01& ' BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01479 Q'f 1 d1 Client Sample ID: Cake Analysis Analysis -Parameter - - Result MQL Unit Method Time Date Analyst Total Phosphorus 26087 11.7 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Al by ICP-AES 17876 2.9 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ As by ICP-AES * 5.9 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Ca by ICP-AES 10212 14.6 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Cd by ICP-AES * 0.117 dry mg/kg 200.7 1994 15:07 6.129/2017 KCJ Cu by ICP-AES 113 0.59 dry mg/kg 200.7 1994 15:07 6.2912017 KCJ K by ICP-AES 436 3.97 mg/kg 200.7 1994 18:48 6/12/2017 Summit Mg by ICP-AES 1836 2.9 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Mo by ICP-AES * 0.59 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Na by ICP-AES 435 19.8 mg/I 200.7 1994 18:48 6/12/2017 Summit Ni by ICP-AES 20.2 0.59 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Pb by ICP-AES * 5.9 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Se by ICP-AES * 5.9 dry mg/kg 200.7 1994 15:07 6/29i2017 KCJ Zn by ICP-AES 2065 0.59 dry mg/kg 200.7 1994 15:07 6/29/2017 KCJ Hg by Cold Vapor AAS 0.06.30 0.06 dry mg/kg 7470A 1994 14:28 6/15/2017 KCJ Reported By: S. nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 7 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirOgmail.com Client : Town of Valdese P.O. Box 339 -Valdese,N. C.28690 Attention: Mr.C.,Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 02-Jun-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01480 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 3055 1093 dry mg/kg SM4500 199 10:11 6/23/2017 KCJ Reported By: S.J neon,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 8 of 12 Blue Ridge Labs PO Box 2940. Lenoir,NC 28645 828-72"149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 02-Jun-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01481 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 16.1 0.1 --- % %Solids ----13:04 6/7/2017 KCJ Pit Available Nitrogen 3341 1117 dry mg/kg Plant Availabl 10:33 6/26/2017 KCJ PH 10.5 0.1 SU SW-846-9040 10:17 6/7/2017 KCJ Reported By: tS. nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 9 of 12 Blue Ridge Labs P4 Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienojr@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 02-Jun-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01482 Client Sample ID: Cake Analysis Analysis Parameter Result MQL unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 279 24.7 dry mg/kg 4500-NO3-E 15:47 6/26/2017 KCJ Total Kjeldahl Nitrogen(TKN) 8472 ' 1375 dry mg/kg 4500-Norg B 10:31 6/26/2017 KCJ Reported By: Oe S.J.Jo a,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 10 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NYC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N. C.28690 ' Attention: Mr.C. Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17- Sample Date: 02-Jun-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01483 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst lgnitability Not Ignitable 70 Deg.F. 1030 SW-846 11:25 6/8,12017 KCJ Corrosivity as pH 10.5 0.1 su 9045C SW-8 10:21 6/7/2017 KCJ Reported By: S.J.J on,D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 11 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmaii.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 02-Jun-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01484 Client Sample ID: Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analvst Reactivity as CN * I mg/kg SW-846-7.3.3 16:28 6/12/2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7,3.3 11:43 6/12/2017 KCJ Reported By: _ S.J.JWon,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 12 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick S�O�Ov, �°'� Date Received: 02-Aug-17 ,gyp 9es l� Report Date: 28-Sep-17 Sample Date: 31-Jul-17 qs P��aj <90 1 8 BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02150 Client Sample ID: Feed Cake Analysis Analysis,-,- Parameter Result MQL_ Unit Method Time Date Analyst Total Phosphorus . 18153 17.5 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ Al by ICP-AES 20145 8.75 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ As by ICP-AES * 8.9 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ Ca by ICP-AES 8954 43.9 dry mg/kg 200.7 1994 16:30 8/3112017 KCJ Cd by ICP-AES * 0.175 dry mg/kg 200.71994 16:30 8/31/2017 KCJ Cu by ICP-AES 266 0.875 dry mg/kg '200.7 1994 16:30 8/31/2017 KCJ K by ICP-AES 308 4.95 mg/kg 200.7 1994 14:59 8/16/2017 Summit Mg by iCP-AES 1794 4.4 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ 'Mo by ICP-AES * 0.875 dry mg/kg 200.7 1994 16:30 8131,2017 KCJ Na by ICP-AES 449 . 21.7 mg/kg 200.7 1994 18:04 8/17/2017 Summit Ni by ICP-AES • 0.875 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ Pb by ICP-AES * 8.8 dry'mg/kg 200.7 1994 16:30 8/31/2017 KCJ Se by ICP-AES * 8.8 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ 7.n by ICP-AES 1542 0.875 dry mg/kg 200.7 1994 16:30 8/31/2017 KCJ fig 0.0430' 0.0409 dry mg/kg 245.1 1994 12:18 8/30/2017 KCJ Reported By: S.J.%gason,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 10 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O, Box 339 Valdese,N. C.28690 Attention: Mr.C. Bortnick Date Received: W'-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BRL k BRL-2017-0584 Lab Sample ID: LSID-2017-02151 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 3916 635 dr},mg/kg SM4500 199 18:12 8/23/2017 KCJ Reported By: Si.J.Jo n,D.R Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 7 of 10 Blue Ridge Labs P4 Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirOgmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C. 28690 Attention: Mr.C. Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02152 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 15.9 0.1 % %Solids 10:27 8/3/2017 KCJ Pit Available Nitrogen 4159 659 dry mglkg Plant Availabl 13:12 8/3/2017 KCJ PH 9.9 0.1 SU SW-846-9040 11:08 8/3/2017 KCJ Reported By: 7S.7�j. son,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 8 of 10 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149. blueridgelabsienoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02153 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 243 24.9 dry mg/kg 4500-NO3-E 13:12 8/3/2017 KCJ Total Kjeldahl Nitrogen(TKN) 9006 1237 dry mg/kg 4500-Norg B 10:12 8/30/20I7 KCJ e Reported By: t S.J nson,D.R.Wessinger *Concentrations are below Minimum Quantification Unit except where noted. NC Laboratory Certificate No.275 Page 9 of 10 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31 Jul-17 BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02154 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 9:26 8/10/2017 KCJ Conosivity as pH 9.9 0.1 su 9045C SW-8 l 1:08 8/3/2017 KCJ Reactivity as CN * I mg/kg SW-846-7.3.3 16:47 8/9/2017 KCJ Reactivity as Sulfide • 5 mg/kg SW-846-7.3.3 15:16 8!9/2017 KCJ Reported By: S.Wbusen,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 10 of 10 R' idge Labs, -Inc. Icy PJI Box 2940 Lenoir. NC28645 Teleplimic (828) 72M 149 Ax (828) 7280131 C'hain of Custody WDS Reporting oroullckvater Sallilary I'all(lCill I tax"ll-CIOLIS W Iste 1111.11,.I.Stlilil CK QC Non State Reportijig, IST/TRISt FUlld JCp()y[jilli lzupol-( To: Bill To: Prqjecl. Namu: _0�_ ........... ------ PC) Number Re Pmwm: Y N LN(Aiinpuskc Preservatives kah Check Q (And) Time&I Field Resid Telly FiLld Sulfide Field trample 11) SaIllpic IMW him. S11111de Preskmt FicId Dechlorilla(ioll p1l fiesid Tcm Type W IM N't Check IWIloved lheck 011or OC 1) Sampler Amilysis Kequested .Z. ------ "C Y N Y N Y N y IN Initials or A At A. 8L _14 —A RcJinq4,11Cd 14. ,.: J Date: Time: Received By. e: 11me: ............ :IgI tx.s H I a I III% )IL%:.%NI V LIUL:31 111C Inn;:bulb 1,0)1111)1 C I CL l)]IV.]I AIIIIIlC 1.5",li,po immili will III,-IIIIIjt,%c-tj I)p;111 Im"(111C;jecImIlls III 11111t:Rid.-_-C 1.;Ills I lip I.).bll)c; allilml i/v<JIM Ao lIvI Imill 45111y I lie all;I I ms 111dia1vt ablIN v m I I ;I lso avl"�it)pil) Col I a I I alld It It I I i f Ill v I I I I ti wC111 I I cs ill:Ill)(I I I u I I I 11111C Ridge 1 :11)% 111 IMN H01 IIL'Cfl lll;ltlt7 Ill 0,16:1 foldvitly Oull data 1111'.1liquilwd IIII lil"I .::IIIIJM IVtIIl;II0I\ Mllhora� will mxcpi;m) file 6.011 In deer (olan� %wik Miew 1IMIM • . Ilielefow if 1�,Ill,'1,11OWN it,ft:kIllt::,I j,11 fill.,1411111apploplulle INIC DFNIR Cellilliol 1.11)o l;i tunit i f Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client:. Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 09-Oct 17 3 PSO°°�S Report Date: 02-Nov-17 �ShQGai O�O Sample Date: 09-Oct-17 �8 BRL#: BRL-2017-0802 �'Qoa�op Lab Sample ID: LSID-2017-03065 Client Sample ID: Feed Cake s Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 12314 13.1 dry mg/kg 200.7 1994 16:54 11/112017 KCJ Al by ICP-AES 19695 3.2 dry mg/kg 200.7 1994 16:54 11/1/2017 KCJ As by ICNAES * 6.54 - dry mg/kg 200.7 1994 16:54 11/1,12017 KCJ Ca by ICP-AES 10845 16.4 dry mg/kg 200.7 1994 16:54 11/l/2017 KCJ Cd by ICNAES * 0.1308 dry mg/kg 2003 1994 16;54 11/l/2017 KCJ Cu by ICNAES 105 0.654 dry mg/kg 200.7 1994 16:54 ]l/1/2017 KCJ K by ICP-AES- 2824 286 dry mg/kg 200.7 1994 12:27 10,116/2017 Summit Mg by ICP-AES 1807 3.2 dry mg/kg 200.7 1994 16.54 11/1/2017 KCJ Mo by ICNAES * 0.654 dry mg/kg 200.7 1994 16:54 l 1/1,2017 KCJ Na by ICP-AES 5324 286 dry mg/kg 200.7 1994 14:31 10/16/2017 Summit Ni by ICP-AES * 0.654 dry mg/kg 200.7 1994 16:54 11/i/2017 KCJ Pb by ICNAES * 6.54 dry mg/kg 200.7 1994 16:54 11/1/2017 KCJ Se by ICP-AES * 6.54 dry mg/kg 200.7 1994 16:54 11/1/2017 KCJ Zn by ICP-AES 3133 0.654 dry mg/kg 200.7 1994 16:54 11,1112017 KCJ Hg by Cold Vapor AAS 0.0523 0.0455 drymg/kg 7470A 1994 14:42 10/26/2017 KCJ I Reported By:. S.4onson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page]1 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirOgmail.com Client: Town of Valdese P.0.Box 339 Valdese,N. C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: .02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03066 Client Sample Ilk Feed Cake Analysis Analysis Parameter _ Result MQL _ Unit _ Method Time _ Date Analyst Ammonia Nitrogen 4979 2372 drymg/kg SM4500 199 16:13 10/3.0/2017 KCJ Reported By: S.J nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 12 of 20 I Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-128-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese P. O.Box 339 Valdese,N.C. 28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: . BRL-2017-0802 Lab Sample ID: LSID-2017-03067 Client Sample ID: Feed Cake Parameter Analysis Analysis Result MQL Unit Method Time Date Analyst Solids 14.8 0.1 % %Solids -- 10:20 — - 10/10/2011 KCJ Pit Available Nitrogen 5341 2425 dry mg/kg Plant Availabl 16:32 10/30/2017 KCJ PH 8.2 0.1 SU SW-846-9040 10:41 10/10/2017 KCJ i i i Reported By: S.J. soa,D.R.Wessinger — --- -- *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 13 of 20 ■ Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-72"149 blueridgelabslenoir@gmail.com Client: Town of Valdese P. O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02 Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03068 Client Sample ID: Feed Cake Analysis Analysis Parameter — Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 11:40 . 10/10/2017 KCJ Corrosivity as pH 8.2 0.1 su 9045C SW-8 10:41 10/10/2017 KCJ Reported By: S D.R.Wessinger i -- -_ *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory-Certificate No.275 Page 14 of 20 0 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P. O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03069 Client Sample ID: Feed Cake Parameter Result MQL Unit Method Analysis AnalysisTime Date Analyst Reactivity as CN * 1 mg/kg SW-846-7.3.3 14:23 10/16i2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 16:47 10/16/2017 KCJ i i 9 Reported By: S.J.J on,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 15 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03070 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate Nitrite Nitrogen(N2+ 362 53.2 dry mg/kg 4500-NO3-E 15:17 10/25/2017 KCJ Total Kjeldahl Nitrogen(TKN) 8756 1203 dry mg/kg 4500-Norg B 11:32 10/30/2017 KCJ Reported By: S.J.Jo on,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 16 of 20 i Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-72"149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample 1D: LSID-2017-03071 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time_ Date Analyst Hg by Cold Vapor AAS • 0.005J mg/l 7470A 1994 10/17/2017 Summit TCLP Extraction Metals extracted SW-846-1311 Summit Ag 1.25✓ mg/1 SW-846-6010 10/17/2017 Summit As • 1.25✓ mg/l SW-846-6010 10/17/2017 Summit Ba 12.5✓ mg/l SW-846-6010 10/17/2017 Summit Cd + 0.25 J mg/l SW-846.6010 10/17/2017 Summit Cr * 0,5✓ mg/l SW-846-6010 10/17/2017 Summit Pb 1.25 1✓ mg/l SW-846-6010 10/17/2017 Summit Se * 0.125 ✓ mgil SW-846-6010 10/17/2017 Summit 1 Reported By: t.J on,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 17 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 . 828-728-0149 bluendgeiabslenoir@gmail.com Client: Town of Valdese P.Q.Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick Date Received: 09-00-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03072 Client Sample ID: Feed Cake Analysis Analysis Parameter — Result MQL Unit _ _Method Time Date_ Analyst TCLP ZHE Volatiles Extraction extracted SW-846-1311 Summit Benzene * 0.1 ^�• mg/I SW846-8260 10/19/2017 Summit Carbon Tetrachloride * 0.1 V ` mg/l SW846-8260 10/19/2017 / Summit Chlorobenzene * 0.1 J mg/l SW846-8260- 10/19/2017 Summit Chloroform * 0.1 ✓ mg/1 SW846-8260 10119/2017 Summit Dichloroethane, 1,2- * 0.1 V mg/1 SW846-8260 10/19/2017 Summit Dichloioethene, 1,1- * 0.1 N( mg/1 SW846-8260 10/19/2017 Summit MEK * 2 mg/l SW846-8260 10/19/2017 Summit Tetrachloroethene • 0.1-./ mg/l SW846-8260 10/19/2017 Summit Trichloroethene * 0.1 V mg/l SW846-8260 10/19/2017 Summit Vinyl Chloride * 2,/ mg/l SW846.8260 10119/2017 Summit Reported By: *Concentrations are below Minimum Quantification Limit except where noted. . NC Laboratory Certificate No.275 Page 18 of 20 i Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C. 28690 Attention: Mr:C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03073 Client Sample ID: Feed Cake Parameter _ Result MQL Unit Method Analysis AnalysisTime Date Analyst TCLP Semi-VOC Extraction extracted ----SW-846-1311- _..... -- -- ummit Cresols(Total) * 4 mg/l SW-846-8270 10/17/2017 ummit Dichlorobenzene, 1,4 * 0.08 ✓ mg/I SW-846-8270 10/17/2017 ummit Dinitrotoluene,2,4 * 0.1 mg/1 SW-846-8270 1.0117/2017 ummit Hexachloro-1,3-13utadiene * 0.1"/ mg/1 SW-846-8270 10/17/2017 ummit Hexachlorobenzene * 0.1'/ mg/I SW 846-8270 10/17/2017 ummit Hexachloroethane * 0.08 ../ mg/I SW-846-8270 10/17,12017 ummit Nitrobenzene * 0.08✓ mg/l SW-846-8270 10/17/2017 ummit Pentachlorophenol * 0.2 mg/1 SW-846-8270 10/17/2017 ummit Pyridine * 0.2✓ mg/1 SW-846-8270 10/17/2017 ummit Trichlorophenol,2,4,5- * 0.2 "" mg/l SW-846-8270 10/17/2017 ummit Trichlomphenol,2,4,6- 0.2 t/ mg/l SW-846-8270 10/17/2017 umm it Reported By: = %x�� $.J.Jo n,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 19 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03074 Client Sample ID: Feed Cake Parameter Result MQL Unit _ —Method Analysis AnalysisTime Date Analyst TCLP Semi-VOC Extraction extracted SW-846-1311 Summit 2 4,5-TP(Silvex) * 0.5 mall SW-846-8080 10:21r2017 Summit 2.4-D * i z/ mg/l SW-846-8080 10/21/2017 Summit Chlordane * 0.01 a, mg/1 SW-846-8080 10/21/2017 Summit Endrin * 0.001� mg7 SW-846-8080 I0,121/2017 Summit Heptachlor * 0.0014 mg/l SW-846-8080 10/21,2017 Summit Heptachlor Epoxide 0.001 J mg/l SW-846-8080 10/21/2017 Summit Lindane i 0.001✓ mg/l SW-846-8080 10/21/2017 Summit Methoxychlor * 0.001✓ mg/1 SW-846-8080 10/21/2017 Summit Toxaphene * 0.02✓ mgn SW-846-8080 10,2 V2017 Summit Reported By: / S.J.Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 20 of 20 Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir,NC 28645 Telephone(828)728-0149 Fax(828)728-013) I Chain of Custody C No NPDS Reporting X_Groundwater Sanitary Landfill Hazardous Waste Industrial or Q n State Reporting Report To: — UST/Trust Fund Reporting Bill To: Town of Vladese Chris ISortnlc Project Name:. PO Number. Ice Present: Y N Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested Type HR:MM Check Removed heck Chlor °C Initials i °C Y N Y N Y N Y N PorA R<sz to".4,s- �n , G� , �M1141/1141c- Cr ,bh ` NNd PM.^/t r+v4,'1Kd, P PAM `y ! �iw I i ishe Date: Time: y: Date: Time: Upon submission of samples,client agrees that invoices are due at the time watt is completed, Open accounts are due 20 days following invoice date. A finance When relinquishing samples to Bloc Ridge Labs(BRL),buyer authorizes BRL to perform only the analysis indicated above and also a charge of I.5°/.per month will be imposed on all pastue accounts. reserves the right to deny documentation for any work whore agrees to pay collection and attorney fee!'the account becomes delinquent, Muc Ridge Labs payment has not been made,in efFect rendering that data unsupported for regulatory purposes. BRL canoW guarantee that any regulatory authority will accept any work submitted,theratbm it is the client's responsibility to regLml on this tbrm appropriate testa NC DENR Certified Lab#275 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 _ _blueridgelabslenoir@gmail om Client: Town of Valdese o� Y. O. Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick ������ LP 00�� Date Received: 11-Dec-17 o � Report Date: 26-Jan-18 Sample Date: I I-Dee-17 BRL#: BR1:20';7-0999 °ems Lab Sample ID: LSID-2017-03952 Client Sample ID: Fced Cake � ... Parameter Analysis Analysis Result MQL Unit Method Time Date Analyst Total Phosphorus 18584 12.4 dry mg/kg 200.7 1994 16:25 12/28/2017 KCJ Al by ICP-AES 17218 3.l l dry mg/kg 200.7 1994 .16:25 I2178/2017 KCJ As by [CP-AES * 6.22 dry mg/kg 200.7 1994 16:25 12/28/2017 1 KCJ Ca by ICP-AES 8011 15.5 dry mg/kg 200.7 1994 16:25 12i28/2017 KCJ Cd by ICP-AES 0.124 dry mg/kg 200.7 1994 16:25 12)8/2017 KCJ Cu by ICP-AES 199 0.622 dry mg/kg 200.7 1994 16:25 12/28/2017 K byICP-.AL-S KCJ 3622 253 dry mg,'kg 200.7 1994 13:16 12/15/2017 Summit Mg by ICP-AES 2748 3.11 dry mg/kg 200:7 1994 16:25 12/28/2017 KCJ NIo by ICP:AES * 0.622 dry mg/kg 200.7 1994 I6:25 12/28!2017 KCJ Na by ICP-AES 2601 191 dry-my/kg- 200.7 1994 15:10 12/26,12017 Summit Ni by ICP-AES * 0.622 drys mg/kg 200.7 1994 16:25 12!28/2017 KCJ Pb by ICP:AES * 6.22 dry mg,k. 200.7 1994 16:25 12/28/2017 KCJ Se by ICP-A£S 6.22 dry mg/kg 200.7 1994 16:25 12128/2017 KCJ Zn by ICP-AES 238 0.622 dry mg/kg 200.7 1994 16:25 12,218,2017 KCJ ]lg 0.0591 0.0538 dry mg/kg 245A 1994 16:06 12/20/2017 KCJ Reported By: S.rnson,D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page"of 12 Blue Ridge Labs PO Box 2940 Lenoir,.NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese R-0. Box 339 \Valdese,,N. C.28690 Attention: Mr; C. Bortnick Date Received"' 1 1-Dec-17 Report Date::� 26-Jan-18 Sample Date: 11-Dec-17 BRL#: BRL-2017-0999 Lab Sample ID: LSID-2017-03953 Client Sample ID: feed Cake Analysis Analysis Parameter Result M L Q Unit Method_ Time Date Anals.-st Ammonia Nitrogen 3169 103 dry mg/ko SN14500 199 10:06 118i2018 CCCJ i Reported By: 5. of uson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 8 of 12 Blue ,Ridge .Labs , PO Bur 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,,N. C.28690 Attention: Mr.C. Bortnick Date Received: 11-I]ec-17 Report Date: 26-Jan-18 Sample Date: 11-1)ec-17 BRL#: BRL-2017-0999 Lab Sample ID: LSID-2017-03954 Client Sample ID: Feed Cake Analysis , Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 18.3 0.1 % °fin Solids 13:11 12/12?2017 KCJ PH 10.1 0-1 su 4500H+B 200 13:20 12/12/2017 KCJ Pit Available Nitrogen 3422 143 dry mg:kg Plant Availabl 14:14 ]r8/20I8 KCJ I i 1 Reported BY: clhn D.R.�Wple�ssinge rnsu � I *Concentrations are below Minimum Quantification Limit except where noted. ` NC Laboratory Certificate 11o.275 Page 9 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese P. 0. Box 339 Valdese,N. C. 28690 Attention: Mr.C. Bortnick Date Received: I I-Dec-17 Report Date: 26-Jan-18 Sample Date: I 1-Dec-1 7 BR[. BRI,2017-0999 Lab Sample ID: I,SID-2017-03955 Client Sample ID: Erred Cake Analysis Analysis Parameter Result MQL i7nit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2-- 253 39.6 dry mgikg 4500-NO3-E 16:01 W2712017 KCJ Total Kjeldahl Nitrogen (TK\) 8650 799 dry mg/kg 4500-Norg B 1 1:33 12j28i2017 KCJ VSO�hnpson-, Reported By: --D.R Wessinger *Concentrations are below Minimum Quantifications Limit except where noted. NC Laboratory Certificate No.275 Page 10 of 12 Blue Ridge Labs PO Box 2940 Lenoir,ll'C 28645 828-728-0149 biueridgelabslenoir@gmaii.00m Client: Town of Valdese P. 0. Box 9 Valdese,N. C. 28690 Attention: Mr.C. Bonnick Date Received: I I-Dec-17 Report Date: 26-Jan-18 Sample Date: l 1-Dec-17 BRL#: BRL-2017-0999 Lab Sample ID: LSID-2017-03956 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst 1;_nitability Not Ignitable 70 Deg.F.- 1030 SW-846 14:22 12i12:'2017 KCJ Corrosivity as p1i 10.1 0.1 su 9045C SW-8 13:20 12i12.12017 KCJ - Reported By: - .Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 1 of 12 \ Blue Ridge Labs PO Box 2940 Lenoir,JVC 28645 828-728-0149 _ blueridgelabslenoir@gmaii.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 11-Dec-]7 Report Date: 26-Jan-18 Sample Date: 1 ]-Dec-]7 BRL#: RRI..-2017-0999 Lab Sample ID: 1.SID-2017-03957 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date. Analyst Reactivity as CN 1 mg/kg SW-846-7.3.3 16:27 12/18!2017 KCJ Reactivity as Sulfide a 5 mg/kg SW-846-7.3.3 15:12 12/18!2017 KCJ MT Reported By: �ssssabs S.J.&- nson. D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 12 of 12 317 .nahtical Report (Allcctinn Date. l_ i 1 'i t" Ia ea, ,,%1 Project: i.:;?:;asi,•c. 1' vAaaric: 1i? ('liens Sample 11) 9; Arm l)s8' Wsult PQf. fiu:al I nit, IAI: Date. MAIN Peal METALS ANALYSES(6010) SW6010D S%J3050B craws! WS Pr�fass,i:mfK r� ,:}j g'w`: e a+ _,n Sq FfA �rr�mal Page; 12 of 29 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B WQ Permit Number: 1990 Laboratory: 1) Blue Ridge Labs (NC Lab#275) Facility Name: Lake Rhodhiss Wastewater Treatment Plant 2) Residual Source WQ#or NCO041696 3) NPDES#: 4) WWTP Name: Lake Rhodhiss Wastewater Treatment Plant 5) Residual Analysis Data Ceiling Sample or Composite Date EParameter Conc. (mpg) Limit "PUP 1e7. �5 � r '7 IT =$7;ff Percent Solids(%} NA 31.2 39.6 v 777-37XV 40.4✓ 39.2 V - Arsenic 75n * �a * �,* ✓ * Indicates Sample is below M L Cadmium 85 c,112.6* tm.9 * ✓ s * ✓ o,k, * Vbg otS�` osg2* Copper 4,300 321 V 252 140 ✓ 269 ✓ 493 V 14.7 Chromium NA Lead 840 45.6* 5x)* �,3. * yo * �,� * A'yb Mercury 57 0.0349 0.0367 0.F57J 0.0303. 0.041 Molybdenum 75 ,a a. �a Nickel 420 `��* ✓ �,y * ✓ 18.1 V, 0,5 * ✓ fig* ��t, Selenium 100 45.io* °,o * �� * y`o *. y� * 2q�* Zinc 7,500 383 370 971 495 1 Total Phosphorus NA 11163 12145 10862 10926 14198 6670 TKN NA 71867. 7558 v 7475 5717 6051 6727 - Ammonia-Nitrogen NA 1917 1820V 2469 V 2905 2275 Nitrate and Nitrite NA 1 476 355 332 134 ✓ 205 V1 207 V 8 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen4ties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 6 Signature of repare Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) MMKIM cr%n1ke n[+c+r iAninnnn% ANNUAL RESIDUAL'SAMPLING SUMMARY FORM -B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001990 Laboratory: 1) Blue Ridge Labs (NC#275 ) Facility Name: Lake Rhodhiss WWTP 2) Residual Source NC 0041696 3) NPDES#or WQ#: 4) WWTP Name: Lake Rhodhiss WWTP 5) Residual Analysis Data A& Sample or Com osite Date. Parameter (mg/kg) 1-31-17 =i 5-31-17 7 1-17 10-9-17 12-11-17 Aluminum 14367 JI 19310 12236 14789 14356 9395 - Calcium 6932 13777 9765 ✓ 10126 10980 V 5574 Magnesium 1993 3 � jLa j 2019 V 1879 V 11 * Indicates Sample is below MQL Potassium 4743 ✓ -2297 -- - ✓ 392 ✓ 935M79 Sodium 666 ✓ ' _ O 310 ✓ 318 ✓ Mrs, PAN 2393 ✓ 2175✓ 1 3879 2601 v H(S.U. 8.6 ✓ 8.4 8.1 ✓ 6.5 ✓ SAR 1 V 0.69 ✓ 1.2 V 0.45V, 0.46 V 2.1 Ignitability Not Ign. Vot I Not I Vot I Not-I Not-Igre Not I Corrosivity as pH 9.6 5.8 9.4 8.1 6.5 7.9 Reactivity * V * * * * V 1 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Signature of reparer� Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102(26) Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03071 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Hg by Cold Vapor AAS * 0.005 mg/l 7470A 1994 10/17/2017 Summit TCLP Extraction Metals extracted SW-846-1311 Summit AS + 1.25 mg/1 SW-846-6010 I0l17/2017 Summit As s 1.25 mg/l SW-846-6010 10117/2017 Summit Ba • 12,5 mg/1 SW-846-6010 10/17/2017 Summit Cd + 0.25 mg/l SW-846-6010 10/17/2017 Summit Cr + 0.5 mg/1 SW-846-6010 10/17/2017 Summit Pb * 1.25 mg/l SW-846-6010 10/17,12017 Summit Se + 0.125 mgjl SW-846-6010 10/17/2017 Summit -J Reported By: - �iii�We;slnge S.13 on, r *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 17 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28646 828-728-0149 blueridgelabslenoir@gmall.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-00-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03072 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP ZHE Volatiles Extraction extracted SW-846-1311 _ Summit Benzene * 0.1 mg/I SW846-8260 10/19/2017 Summit Carbon Tetrachloride • 0.1 mg/l SW846-8260 10/19/2017 Summit Chlorobenzene * 0.1 mg/l SW846-8260 10/19/2017 Summit Chloroform * 0.1 mg/l SW846-8260 10/192017 Summit Dichloroethane,1,2- * 0.1 mg/l SW846-8260 10/19I2017 Summit Dichlomethene, 1,1- * 0.1 mg/l SW846-8260 10/19/2017 Summit MEK * 2 mg/l SW846-8260 10/19/2017 Summit Tetrachloroethene • 0.1 mg/1 SW846-8260 10/19/2017 Summit Trichloroethene * 0.I mg/l SW846.8260 10/19/2017 Summit Vinyl Chloride * 2 mg/l SW846-9260 I0/192017 Summit Reported By: S.J. n,D.R.Wessinger --'— *Concentrations Are below Minimum Quantifleation Limit except where noted. NC Laboratory Certificate No.275 Page 18 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirOgmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C. 28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#:.. BRL-2017-0802 Lab Sample ID: LSID-2017-03073 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP Semi-VOC Extraction extracted ----SW-846-1311 - Summit Cresols Consols(Total) + 4 mg/l SW-846-8270 10/17/2017 Summit Dichlorobenzene, 1,4 • 0.08 mg/l SW-846-8270 10117,12017 Summit Dinitrotoluene,2,44 rt 0.1 mg/l SW-846-8270 10./17/2017 Summit Hexachloro-1,3-13utadiene + 0.1 mg/1 SW-846-9270 10/17/2017 Summit Hexachlorobenzene 0.1 mg/l SW-846-8270 10/17/2017 Summit Hexachloroethane • 0.08 mg/l SW-846-8270 10/17/2017 Summit Nitrobenzene • 0.08 mg/l SW-846-8270 10/17/2017 Summit Pemachlorophenol • 0.2 mg/l SW-846-8270 10/17/2017 Summit Pyridine • 0.2 mg/I SW 846-8270 10/17/2017 Summit Trichlorophenol,2,4,5- + 0.2 mg/ SW-846-8270 1011712017 Summit Trichlomphenol,2,4,6- + 0.2 mg/l SW-846-8270 10/17/2017 Summit Reported By: S.J.Jo n,D.R.Wessinger — "Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 19 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C. Bottnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BR'#: BRL-2017-0802 Lab Sample ID: LSID-2017-03074 Client Sample ID: Feed Cake Analysis Analysis Parameter Result MQL Unit —Method Time Date' Analyst TCLP Semi-VOC Extraction extracted SW-846-1311 Summit 2,4,5-TP(Silvex) * 0.5 mg/l SW-846-8080 1012112017 Summit 2.4-1) * 1 mg/I SW-846-8080 10/2112017 Summit Chlordane + 0.01 mg/l SW-846-8080 10/21/2017 Summit Endrin * 0,001 mg/l SW-846-8080 10,21!2017 Summit Heptachlor • 0.001 mg/I SW-846-8080 10,121,2017 Summit Heptachlor Epoxide « 0.001 mg/l SW-846-8080 10/21,12017 Summit Lindane + 0.001 mg/1 SW-846-8080 10/21/2017 Summit Methoxychlor * 0.001 mg/I SW-846-8080 10/21/2017 Summit Toxaphene « 0.02 mg/1 SW-846-8080 10421,'2017 Summit tt. Reported By: S.J.Johnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 20 of 20 Lo Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese SAA co 0CA P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 31 Jan-17 Report Date: 09-Mar-17 Sample Date: 153TeJ-0-917p BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00271 Client Sample ID: ayB" Compost~ Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 11163 11.2 dry mg/kg 200.7 1994 13:47 2/27,'2017 KCJ Al by ICP-AES 14367 2.8 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ As by ICP-AES * 5.6 dry mg/kg 200,7 1994 13.47 2/27/2017 KCJ Ca by ICP-AES 6932 14.1 dry mg/kg 200,7 1994 13:47 2/27/2017 KCJ Cd by ICP-AES * 0.1126 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ Cu by ICP-AES 321 0.563 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ K by ICP-AES '4743 4 dry mg/kg 200.7 1994 13:06 2/20/2017 Summit Mg by ICP-AES 1993 2.8 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ Mo by ICP-AES * 0.563 dry mg/kg 200.7 1994 13:47 2,27/2017 KCJ Na by ICNAES 666 20 dry mg/kg 200.7 1994 13:06 2/20/2017 Summit Ni by ICNAES * 0.563 dry mg/kg 200.71994 13:47 2/27/2017 KCJ Pb by ICP-AES * 5.6 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ Se by ICNAES * 5.6 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ Zn by ICP-AES 383 0.563 dry mg/kg 200.7 1994 13:47 2/27/2017 KCJ Ha 0.0349 0.0303 dry mg/kg 245.1 1994 13:15 2/21/2017 KCJ Reported By: S. /dohnson,D.&Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 of 14 t Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirCgmaii.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 31-Jan-17 sRL#: BRL-201 7-00s5 Lab Sample ID: LSID-2017-00272 Client Sample ID: Bay Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 1917 273 dry mg/kg SM4500 199 I2:08 2.17/2017 KCJ Reported By: S ohnson,D.R Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 2 of 14 ■ Blue Ridge Labs PO Box 2940 ' Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client. Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-1.7 Sample Date: 31-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00273 Client Sample ID: Bay Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids -_ 31.2' 0.1 % %Solids 12:50 2/9!2017 KCJ Pit Available Nitrogen 2393 323 dry mg/kg Plant Availabl 13:15 2/24:2017 KCJ pH 8.6 0.1 SU SW-846-9040 10:16 2/9(2017 KCJ Reported By: tSohnson,D.R.Wessinger "Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 14 Client : Town of Valdese P. O. Box 339 Valdese_N.C. 28690 Attention: Mr.C. Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 31-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00274 Client Sample ID: Bay Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 476 50.2 dry mg/kg 4500-NO3-E 11:20 2/24/2017 KCJ Total Kjeldahl Nitrogen(TKN) 7186 583 dry mg/kg 4500-Norg B 8:05 2/16/2017 KCJ Reported By: S. ohnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 14 Blue Midge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N. C.28690 Attention: Mr. C.Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 31-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00275 Client Sample ID: Bay Compost Analysis Analysis Parameter - Result MQL _ Unit _Method Time _Date_ Analyst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 13:30 2/9/2017 KC) Corrosivity as pH 9.6 0.1 su 9045C SW-8 10:16 2/9/2017 KCJ I Reported B : Po . Y S. ohnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.215 Page 5 of 14 0 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Toswm of Valdese P. 0.Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick Date Received: 31-Jan-17 Report Date: 09-Mar-17 Sample Date: 31-Jan-17 BRL#: BRL-2017-0055 Lab Sample ID: LSID-2017-00276 Client Sample ID: Bay Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivity as CN * 1 mg/kg SW-846-7.3.3 16:43 2/9/2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 14:20 2/9/2017 KCJ Reported By: Vlohnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 14 Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir,NC 28645 Telephone(828)728-0149 Fax(828)728-0131 Chain of Custody NPDS Reporting Groundwater Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/Trust Fund Reporting Report To: Bill To: Town of Vladese Chris Bortnic Project Name: PO Number: Ice Present: Y N Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested Type HR:MM Check Removed heck Chlor °C Initials °C Y N Y N Y N Y N PorA M , 't I� P'� e�!(r C �c:S A J•4�. 5 �rn /lS , r+ MQ,Se- Ln Al,M,y,C41M41 �K CAL l `�33.11 1 nt Ha� *.�; K v T_5n;*%.4.t,+yj C.srr;.3,v:*y hl ir.•i' �/caKia.sa t-3t.17 �,3t SPa�:.� �•: .G 13 V�! 4ar Ca n ^Q % Re ' shed Date: Time: Rec Date: Time: .1,315- 7`- Upon submission of snmples,client agrees that invoices are due at the lime work is completed. open accounts are due 20 days following invoice date. A finance charge of 1.5%per month will be imposed on all paslue accounts. When relinquishing samples to Blue Ridge Labs(HRL),buyer authorizes BIRL to perform only the analysis indicated above and also agrees to pay collection and attorney feef the account becomes delinquent, Blue Ridgc Labs reserves the right to deny documentation 1br any work where payment has not been made,in effect rendering that data unsupported for regulatory purposes, 13RL cannot guarantee that any regulatory authority will accept any work submitted,therefore it is the client's responsibility to request on this form appropriate tests. NC DENR Certified Lab#275 9 Ca Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 1 Attention: Mr_C. Bortnick C-T9 Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 3�i1 A:p�"'W7 BRL#: BRL-2017-0201 Lab Sample ID: LSID-2017-00863 Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 12145 10 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ AI by ICP-AES 19310 2.5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ As by ICP-AES « 5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ Ca by ICP-AES 13777 12.5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ Cd by ICP-AES k 0.1 dry mg/kg 200.7 1994 14:46 5/1!2017 KCJ Cu by ICP-AES 5w+y`4'"'" 252 0.5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ K by ICP-AES C`1I0) 2297 10.4 dry mg/kg 200.7 1994 4/27/2017 summit Mg by ICP-AES 3106 2.5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ Mo by ICP-AES + 0.5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ Na by ICP-AES 00-) 550 522 dry mg/kg 200.7 1994 4/27/2017 Summit Ni by ICP-AES * 0.5 dry mg/kg 200.7 1994 14:46 51I L017 KCJ Pb by ICP-AES * 5 dry mg/kg 200.7 1994 14:46 5/1'2017 KCJ Se by ICP-AES * 5 dry mg/kg 200.7 1994 14:46 5/l/2017 KCJ Zn by ICP-AES 370 5 dry mg/kg 200.7 1994 14:46 5/1/2017 KCJ Hg by Cold Vapor AAS 0.0367 0.0242 dry mg/kg 7470A 1994 14:12 5/1/2017 KCJ Reported By: tVhuson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page I of 6 ■ Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgeiabslenoir@gmaii.com Client : Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr. C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 03-Apr-17 BRL#: BRL-2017-0201 Lab Sample ID: LSID-2017-00864 Client Sample 1D: Bay 1 -Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 1820 282 dry mg/kg SM4500 199 9:20 4/24/2017 KCJ Reported By: S.tinsont,DIRL.Wessinger " Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 2 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese RO.Box 339 Valdese,N.C.28690 Attention: Mr. C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 03-Apr-17 BRL#: BRL-2017-0201 Lab Sample ID: LSID-2017-00865 Client Sample ID: Bay 1 -Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 39.6 0.1 % %Solids 10:20 4..5/2017 KCJ Pit Available Nitrogen 2175 321.5 dry mg/kg Plant Availabl 16:52 5/1/2017 KCJ pH 5.8 0.1 SU SW-846-9040 9:10 4/512017 KCJ Reported By: S.J. nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 03-Apr-17 BRL#: 13RL-2017-0201 Lab Sample ID: LSID-2017-00866 Client Sample ID: Bay 1 -Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 355 39.5 dry mg/kg 4500-NO3-E 16.41 5/1/2017 KCJ Total Kjeldahl Nitrogen(TKN) 7558 465 dry mg/kg 4500-Norg B 9:25 4/26/2017 KCJ Reported By: S.I son,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N.C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 03-Apr-17 BRL#: BRL-2017-0201 Lab Sample ID: LSID-2017-00867 Client Sample ID: Bay 1 -Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg. F. 1030 SW-846 11:25 4r5/2017 KCJ Corrosivity as pH 5.8 0.1 SU 9045C SW-8 9:10 4/5.12017 KCJ Reported By: S.J.J son,D.R Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 5 of 6 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 04-Apr-17 Report Date: 02-May-17 Sample Date: 03-Apr-17 BRL#: BRL-2017-0201 Lab Sample ID: LS1D-2017-00868 Client Sample ID: Bay 1 -Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivity as CN * 1 mg/kg SW-846-7.3.3 16:45 4;612017 KCJ Reactivity as Sulfide * 5 mglkg SW-846-7.3.3 14:25 4/6/2017 KCJ Reported By: 4J. en,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 6 o Summit Environmental Technologies,Inc. S U M i i _ 1 3310 Win Si. Analytical Report CtryahogaFalk ONG44223 (ca�ualidatal) :. _... TEL:(330)253.8111 FAX'(330)253-4489 WOlI: 17041186 Website: 'Date Reported: CLIENT: Blue Ridge Labs,Inc. Collection Date: 4/3/201710:38:00 AM Project: Laboratory Analysis Lab ID: 17041196-005 Matrix: SOLID Client Sample ID $63 Analyses Result PQL Qual Units DF Date Analyzed METALS ANALYSIS(6010) SW6010C SW3050B Analyst CM ` Potnasium 910 4.13 mg/Kg 1 412712017 Sodium 218 20.7 mg1Kg 1 4127/2017 Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir,NC 28645 ` 1 Telephone(828)728-0149 Fax(828)728-0131 Chain of Custody NPDS'Reporting X Groundwater Sanitary Landfill Hazardous Waste Industrial or QC Non State Re rtin UST/Trust Fund Reporting I;— Report To: Bill To: Town of Vladese Chris Bortnie Project Name: PO Number: Ice Present: Y N Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested Type HR:MM Check Removed heck Chlor °C Initials °C Y N Y N Y N Y N PorA L 1 � ro1:, Se L-r At,My,Cyr Nc; ,tom PH,V'L T-1:tp P P Rel' shed Date: Time: Rec Date Time: i�� If-")-,-7 Upon submission orsamples,client agrees that invoices are duc at the time work is completed. Open accounts are due 20 days following invoice date. A finance charge of 1.3%per month will be imposed on all pastue accounts. When relinquishing samples to Blue Ridge Labs(BRL),buyer authorizes BRL to perform only the analysis indicated above cord also agrees to pay collection and attorney ILvilhe account becomes delinquent. Blue Ridge Lubs reserves llte right to deny documentation for any work where payment has not been made,in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any rc:gulniory authority will accept any work submitted,therefore it is the client's responsibility to request on this form appmpriate tests. NC DENR Certified Lab#273 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese SAR P.O.Box 339 (OZ* Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 31- a3e_1. BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01473 Client Sample ID: •omgoS Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 10862 4.5 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Al by ICP-AES 12236 1.13 dry mg/kg 200.7 1994 15:01 6i29/2017 KCJ As by ICP-AES * 2.3 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Ca by ICP-AES 9765 5.6 dry mg/kg 200.7 1994 . 15:01 6/29/2017 KCJ Cd by ICP-AES * 0.0454 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Cu by ICP-AES 140 . 0.23 dry mg/kg 200.7 1994 15:01 6/29l2017 KCJ K by ICP-AES 00 5'' , 2225 10.6 dry mg/kg 200.71994 18.45 6/12/2017 Summit Mg by ICP-AES 1661 1.13 m - 200.7 1994 15:01 .6,1229/2017 �' Pig KCJ Mo by ICP-AES * 0.23 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Na by ICP-AES G�> 790 53 dry mg/kg 200.7 1994 18:45 6/12/2017 Summit Ni by ICP-AES 18.1 0.23 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Pb by ICP-AES * 2.3 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Se by ICP-AES 2.3 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Zn by ICP-AES 971 0.23 dry mg/kg 200.7 1994 15:01 6/29/2017 KCJ Hg by Cold Vapor AAS 0.0357 0.0252 dry mg/kg 7470A 1994 14:26 6/15/2017 KCJ r Reported By: S. Pb -�n .Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 31-May-17 BRL#: BRL-20]7-0391 Lab Sample ID: LSID-2017-01474 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen .2469 490 dry mg/kg SM4500 199 9:20 6/23/2017 KCJ Reported By: t- neon,D.-,R..Wessinger *Concentrations are below Minimum Quantification Limit except where noted. .7. NC Laboratory Certificate No.275 Page 2 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoil@gmail.com Client: Town of Valdese P.0.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample.Date: 31-May-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01475 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 37.7 0.1 % %Solids 13:02 6/7/2017 KCJ Plt Available Nitrogen . 2801 529 dry mg/kg Plant Availabl 10:30 6/26/2017 KCJ PH 8.4 0.1 SU SW-846-9040 10:15 6/7/2017 KCJ Reported By: S.J. ioson,MIL Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 31-May-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01476 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 332 38.7 dry mg/kg 4500-NO3-E 15:45 6/26/2017 KCJ Total Kjeldahl Nitrogen(TKN) 7475 494 dry mg/kg 4500-Norg B 9:12 6/26/2017 KO Reported By: S.J nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr. C.Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 31-May-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01477 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 11:20 6/8/2017 KCJ Corrosivity as pH 8.4 0.1 su 9045C SW-8 10:15 6/7/2017 KCJ Reported By: S.J. son,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 5 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N. C. 28690 Attention: Mr.C. Bortnick Date Received: 05-Jun-17 Report Date: 08-Aug-17 Sample Date: 31-May-17 BRL#: BRL-2017-0391 Lab Sample ID: LSID-2017-01478 Client Sample ID: Compost Analysis Analysis Parameter- —_ Result MQL Unit Method Time Date Analyst Reactivity as CN + 1 mg/kg SW-846-7.3.3 16:25 6/12/2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 11:40 6/12/2017 KCJ Reported By: S.J Vnsn,D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 12 Suinnia Enviromptenial Zechnohjgies,Inc. '3/0 Win Analytical Report tf:= Cin-ahaga rills.Ohio 44223 laLnsulsslatcdt TFL(330i 253-8711 F4X-t330i 253-4489 14'o=: 17060564 h/117:-it it Date Reported: 611312017 CLIENT- Blue Ridge Labs. Inc. Collection Date: 6--2/20 17 8:39:00 AM Project: Metals Testing Lab ID: 17060564-0021 Matrix: SOIL Client Sample ID 1479 Analyses Result PQL Qual Units DIF Dke Analvzed METALS ANALYSIS(6010) SW6010C SW3050B Analyst: JEB Potassium(K) 436 397 mg/Kg 1 611212017 6:48:19 PM Sodium(Na) 435 19.8 mg/Kg 1 6112/2017 6:48:19 PM Qualifiers- oid'np nines pn�va"31rii anah,!,Lc­jtd lnre�awn iiied to detumint area tL�powie ".I Va=c'I 0 KSD is greater than R-SNitnit P1, Partin L=1 RL RTomstig D.tcc,.n i oi., tamptL mniimwr r—venrui c is out of Imi m smirted Li[S5:LJiC Original Sunntttt F.niironnrental Technologies hic.3310 ltbr St. Analytical Report C uvahoga Falls.Ohio 44223 1 consol idated) F£L:i331)i?S 3-8'll F4-1'. (33111 2 5 3-4481) \1"U�: 17060564 iti&ctre him. utrtfsellekewn Date Reported: 6/13/2017 CLIENT: Blue Rid--re Labs. Inc. Collection Date: 53 F 21017 2:18:00 PM Project: Metals Testing. Lab ID: 1 706056 4-00 1 Matrix: SOIL Client Sample ID 1473 Analyses Result PQL Qual Units DF Date Analvzed METALS ANALYSIS(6010) SW6010C SW3050B Analyst: JEB Potassium(K) 839 4.00 mglKg 1 6/12/2017 6:45:38 PM Sodium(Na) 298 20.0 mg/Kg 1 6/12/2017 6:45:38 PM Qualifiers: H Holdmg imies Rn p;walanen at anaKsu e:cecde3 \I \L nual Inaentivn used w dctemunear�re-;"n;e ND Not De:mied 0 RID u L mlw than R%'DLmia PL P al Ltmn RI Repormg Delm,—Limo 11 tiamp!c cantnmel tcmrmturr a out ci limn as spwf"'d at 1i lcmc Original Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC.28645 Telephone(828)728-0149 Fax(828) 728-0131 Chain of Custody NPDS Reporting Groundwater ',Sanitary Landfill Fund Waste Industrial or QC Non State Reporting I.1S'17'1"-list Aind Reporting Report To: Bill To: Town of Vladese Chris Hor(nic Project Name: PO Number: —----- Ice Present: Y Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field Sample 11) Sample Date 'rime Stillide Present/ Field Dechlorination pl-1 Resid Temp Sampler Analysis Requested Type 11RAM Check Runoved Check chlor "C' Initials 0C Y N Y N Y N y N 11 or A ')?C' CQ k u pk) .V., i-k 2_,, Ak,fAy' Cr." pjt" K T14qj. P A�k � I+ C6 Re 4,11s,iedZ Date: Time: 1�m lVed 1'33v: J/ Date: Time: 1 -7 UP011 SUbmissloo ol,gaillpleS.client agrees that invoices are due at the lime work is completed OPeo accounts are dtic 20 clays ibilowilig invoice(late. A tinance charge of 1.3%per month Will he impond()It 1111 I)WALIC aCCOU111s When 1clinquishing.snjilples to Illoe Ridge Labs buyerauthorizes IML to perlbrin only ilic analysis indicated altove and also agrees to pay collection and aitorney 1�efllie account becomes delinquent. HILIC Ridge 1.91hN reserves the right to deny documentation lbrany work where payment has not been made•in effeet rendering that data 1111slIpprIcEl lor regulatory purposes. 13111,canoot,guarantee Him my regulatory authority will necept any York submitted.(h.crelbre it is the client's responsibility to request on this liarm appropriate tests. NCDENR Certified LA)9275 e Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client : Town of Valdese (9. H P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 021.- .I IT BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02145 Client Sample ID: @1-de"s-ORn -Mis p Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 10926 10 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Al by ICP-AES 14789 2.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ As by ICP-AES # 5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Ca by ICP-AES 10126 12.5 dry mglkg 200.7 1994 16:24 8/31/2017 KCJ Cd by ICP-AES # 0.1 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Cu by ICP-AES 269 0.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ K by ICP-AES 392 4.1 mg/kg 200.7 1994 2:56 8/16/2017 Summit Mg by ICP-AES 2019 2.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Mo by ICP-AES * 0.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Na by ICP-AES 310 21.9 mg/kg 200.7 1994 18:01 8/17/2017 Summit Ni by ICP-AES * 0.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Pb by ICP-AES * '5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Se by ICP-AES * 5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Zn by ICP-AES 495 0.5 dry mg/kg 200.7 1994 16:24 8/31/2017 KCJ Hg 0.0303 0.0261 dry mg/kg 245.1 1994 12:16 8/30/2017 KCJ Reported By: S.J.J son,D.R.Wessinger *Concentrations are below Minimuni Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 of 10 Blue .Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.0.Box 339 Valdese,N.C.28690 Attention: Mr. C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BRL#: BRL-2017-0584 Lab Sample ID: LSID-2017-02146 Client Sample ID: Oldest Row Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 3745 461 dry mg/kg SM4500 199 17:39 8/23/2017 KCJ Reported By: f� S.I Jo n,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 2 of 10 1 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir�gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 13-Jul-17 BRL#: BRL-2017-0584 Lab.Sample ID: LSID-2017-02147 Client Sample ID: Oldest Row Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 37.1 0.1 % %Solids 10:25 8/3/2017 KCJ Plt Available Nitrogen 3879 471 Plant Availabl 17:41 8/23/2017 KCJ pH 8.1 0.1 SU SW-846-9040 11:05 8/3/2017 KCJ Reported By: Si ohnson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 10 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.0.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BRL#: 13RL.-2017-0584 Lab Sample ID: LSID-2017-02148 Client Sample ID: Oldest Row Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 134 10.7 dry mg/kg 4500-NO3-E 13:12 8/3/2017 KCJ Total Kjeldahl Nitrogen(TKN) 5717 498 dry mg/kg 4500-Norg B 9:16 8/30/2017 KCJ Reported By: S.J.J son,D.R.Wessinger -- *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 10 r Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick Date Received: 02-Aug-17 Report Date: 28-Sep-17 Sample Date: 31-Jul-17 BILL#: BRL-2017-0584 Lab Sample 11D: LSID-2017-02149 Client Sample ID: Oldest Row Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analvst Ignitability Not Ignitable 70 Deg.F. 1030 SW-846 9:15 8/10/2017 KCJ Corrosivity as pH 8.1 0.1 su 9045C SW-8 11:05 8/3;2017 KCJ Reactivity as CN * 1 mg/kg SW-846-7.3.3 16:45 8/9/2017 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 15:14 8/9/2017 KCJ Reported By: S.J.J n,D.R.Wessinger Concentrations are below Minimum Quantification Limit 1 xcept where noted. NC Laboratory Certificate No.275 Page 5 of 10 �� �0 |f� �� ~ '����� Labs, Inc.��� ^~� ��l�� 0� �� � ' ��.~ �� �� �^� p1l Box 294O Lcnoir.NCZ864i 7e|cphonw (828) 72Q'O}4q Fax (028) 728'0l]| Chain �� Custody � �x�^�~' "��x��� ��� ����� ��u�'���' NMDS Reporting / (}couodv«atcrSaoiiary Landfill l|uzuukuu Vyunte �_ luduu�/iu| ur [)CNon State Reporting @S'[7]ioo� �uod �c�urdn� --- }{ql' ---- Pnijcn Name: P0Number: --- Y ------'-------- --'- -- |co �Pneocn/� /� Cflmpoubv Pruscm 6 | hC| cuk Temp Field. Suffide Chlor Field Sample 11) Sample Date l'inle 8111fide Present I Field Dechloriil;ltioll p1l Resid Tellip Sampler Analysis lkC(lLJC.qtCd ILI Time Field Resid Re 'n )shed, Date: Ti me: Z ei ed 13 Date: Time: zy Z'Mli�"12� 11111111"Llbillissioll 111'salliples.cliew aglee.s thal ifivolces aic title ill file"'lle%Vt)Fk IN Coll)VIVICd 0I)CH 1MILIHIS Me(life-'if jj;l%S 1j)1lowifla invoice thile. A I'llmilt:v Char c ill'1.5%pet Xv- WhOl(0111(jilimllillp,N;111111les it)Mile Ridge Labs OWL).hmei autholize a (I a mv mid also agi-ces to pm collcowil and allollin fices il'ific uccill"ll llccilllik--�%t1clintluem I'llite Ritlg-e kih% ~~""~~,�""~""»«'o�m^«�"» "w/r *mp�m"vm^^mnoMv"puu�sk ^xC|xmxcn�nm|,m^zn '—'--"--` '~r'^` ^^' `~"^"�""""`/"nmr'"�m*'� "mmm4 °«/:�~, *» wv: ■ Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienolrOgmail-com Client: Town of Valdese P. O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: ,9-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03060 Client Sample ID: Compost Analysis Analysis Parameter ReMsul MQL _ Unit Method Time Date Analyst Nitrate+Nitrite Nitrogen(N2+ 205 18 dry mg/kg 4500-NO3-E 15:15 10/25/2017 KCJ Total Kjeldahl Nitrogen(TKN) 6051 450 dry mg/kg 4500-Norg B 10:15 10/30/2017 KCJ Tlg boo - -apor PAW 0 223 0.0455 dry mg/kg 7470A 1994 14:42 10/26/2017 KCJ Reported By: !' S.J.J on,D.R.Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 20 Blue Ridge Labs , PO Box 2940 Lenoir,NC 28645 828-728-0149 b(ueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03059 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method .Time Date Analyst Reactivity as CN + 1 mg/kg SW-846-7.3.3 14:21 10/16/2017 KCJ Reactivity as Sulfide R 5 mg/kg SW-846-7.3.3 16:45 10/16/2017 KCJ Reported By: S.J.Jo ,D.R.Wessinger *Concentrations are below.Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 5 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 biueridgelabslenoirfgma-H.Com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-0ct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03058 Client Sample ID: Compost Analysis Analysis Parameter ' Result MQL Unit Method Time Date Analyst -— ---- -----..-.. -...-..--- --- lgnitability Not Ignitable 70 Deg.F. 1030 SW-846 11:25 10/10/2017 KCJ Corrosivity as pH 6.5 0.1 su 9045C SW-8 10:20 I0/10i2017 KCJ Reported By: S.J, son,D.R.Wessinger "Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 4 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-72"149 blueridgelabsienoir@gmaii.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL##: BRL-2017-0802 Lab Sample ID: LSID-2017-03057 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 40.4 0.1 % %Solids 10:15 1011012017 KCJ Pit Available Nitrogen 1 0 Plant Availabl PH 6.5 0.1 SU SW-846-9040 10:20 10/10/2017 KCJ Reported By: S.J ason,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 3 of 20 ------------- -- — Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-7284149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-00-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03056 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst - ---- ---- --- ----- - ----------------._.. . . Ammonia Nitrogen 2905 451 dry mg/kg SM4500 199 15:25 10/30/2017 KCJ Reported By: S. nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 2 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmall.com Client: Town of Valdese d `VA G P.O.Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: il - BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03055 Client Sample ID:4UWI Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 14198 4.56 dry mg/kg 200.7 1994 16:48 1111/2017 KCJ Al by ICP-AES 14356 1.14 dry mg/kg 200.7 1994 16:48 l l/l/2417 KCJ As by ICP-AES * 2.2 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ Ca by ICP-AES 10980 5.7 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ Cd by ICP-AES * 0.0456 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ Cr by ICP-AES 0.228 dry mg/kg 200.7 1994 16:48 11/IJ2017 KCJ Cu by ICP-AES 493 0.228 dry mg/kg 200.7 1994 16:48 11/1t2017 KCJ K by ICP-AES 935 60.8 dry mg/kg 200.7 1994 12:17 10/16/2017 Summit Mg by ICP-AES 1879 1.14 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ Mo by ICP-AES * 0.228 dry mg/kg 200.7 1994 16.48 l I/1/2017 KCJ Na by ICP AES 318 60.8 dry mg/kg 200.71994 14:25 10/16/2017 Summit Ni by ICP-AES * 0.228 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ Pb by ICP-AES * 2.2 dry mg/kg 200.7 1994 16:48 l l/l/2017 KCJ Se by ICP-AES * 2.2 dry mg/kg 200.7 1994 16:48 1111/2017 KCJ Zn by ICP-AES 1301 0.228 dry mg/kg 200.7 1994 16:48 11/1/2017 KCJ g by Co d Vapol•71A`Si�, �*0?04TW 0.0237 dry mg/kg 7470A 1994 14:40 10/26/2017 KCJ Reported By: =Jns-on, .R. Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 1 of 20 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: ToAm of Valdese P. O. Box 3')9 Valdese,N.C. 28690 Attention: Mr-C. Bortnick Date Received: I I-Dee-17 Report Date: 26-Jan-18 Sample Date: 51filem-e- M- BRL 4: BRL-2017-0999 . Lab Sample ID: I-SID-2017-03946 Client Sample ID: (40-h-Upo"MW Parameter Result MQL Un'i' Method Analysis Analysis t Time Date Analyst Total Phosphorus 6670 5.92 dry"rn&/kg 200.7 1994 16-15 12M/2017 KCJ Al by ICP-AES 9395 1.5 dry mg/kg 200.71994 16:15 12/28/2017 KCJ As by ICP-AES a il-g 200.7 1994 16:15 12/28/2017 2.9.6 dry m, KCJ Ca by ICP-AES 557'4"--- drying g 200-71994 16:15 "k 121/2812017 KCJ Cd O.d"'921 by ICP-AES ' dry nig/kg 200.71994 16:15 11,28/2017 KCJ 1 5 Cu by IC)I-AFS 1 14.7 0.592 dry mg/kg 200.71994 16:15 12/28!2017 KCJ K by ICP-AES ML--bv [CP-AES 1892 121 dry mg/kg 200.7 L994 13:12 12/1512017 Summit 1136 1.5 dry mg/kg 200.7 1994 16:15 12/28!2017 KCJ Mo by ICP-AES 0.296 dry mg/kg 200.7 1994 16:15 12128!2017 .KCJ Na by ICP-AES 00FI) 1043 102 dry mg/kg 200.7 1994 15:06 12-,2&2017 Summit Ni by ICP-AES a 0.296 dry mg/kg 200.7 1994 16:15 12/28.,'2017 KCJ Pb by ICP-AES 2.96 dry mglk- 200.7 1994 16-15 12.,'28!2017 KC Se by ICP-AFS 16:15 12!28/2017 KCj 2.96 dry rngikg 200.7 1994 Zn bk, TCI)-Af,:S 101 0.296 dry mg/kg 200.71994 16:15 12/28/2017 I(Cj 11 . 0.0410 .0.243 dry m&'kg 245.1 1994 16:04 12,-20/2017 KC.1 Reported By: �7-�Jhjn-S-O'In D.R..Wessinger Concentrations are below Minim um,Quantification'Limit except where noted. NC Laboratory Certificate No.275 Page I of 12 r 6 - Blue Ridge Labs PO Bo_r 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P. 0.Box 339 Valdese,N.C.28690 Attention: Mr. C. Bortnick Date Received: I I-Dee-17 Report Date: 26-Jan-18 Sample Date: I I-Dee-17 BRL#: BRL-20I7-0999 Lab Sample ID: LSID-2017-03947 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 2275 451 'dry mg/kg SM4500 199 9:10 1/8/2018 KCJ 0' Reported By: S. Johnson,D.R Wessinger . *Concentrations are below Minimum Quantification Limit except where noted. SIC Laboratory Certificate No.275 Page 2 of 12 s Blue Midge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabsienoir@gmaii.com. Client : Town of Valdese P.0.Box 339 Valdese,N. C.23690 Attention: Mr.C. Bortnick Date Received: 11-Dec-17 Report Date: 26-Jan-18 Sample Date: l 1-Dec-17 BRL#: BRI.-2017-0999 Lab Sample U): LSID-201 7-03948 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst %Solids 39.2 O.1 % %Solids 13:10 12/12/2017 KCJ pH 7.9 0.1 su 45001-1+B 200 13:16 121 12,2017 KCJ Plt Available Nitrogen 2482 470 dry mg/kg Plant Availabi 14:12 1/V2018 KCJ Reported By: S.J nson,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted, NC Laboratory Certificate No.279 Page 3 of 12 Blue Ridge dubs PO Box 2940 Lenoir, ,'VC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese,N.C.28690 Attention: Mr.C. Bortnick Date Received: I I-Dec-17, Report Date: 26-.1 an-]8 Sample Date: I 1-Dec-i 7 BRI.ff: BRL-2017-0999 Lab Sample ID: LSID-2017-03949 Client Sample IID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analvst Nitrate—Nitrite Nitrogen(N2+ 207 18.5 dry mglkg 4500-NO3-E 15:59 12/27,12017 KCJ Tofa1 Kjeldahl Nitrogen(TKN) 6727 375 dry mg/kg 4500-Nora B 10:11 1212812017 KCJ Reported By: S. nson, D.R.Wessinger *Concentrations are below Minimum Quantification limit except where noted. NC Laboratory Certificate No.275 Page 4 of 12 5 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 _ ✓ ✓� blueridgelabsienoir@gmail.com Client : Town of Valdese P.O. Box 339 Valdese,N. C.28690 Attention: Mr.C. Bortnick Date Received: 11-Dec-17 Report Date: 26-Jan-18 Sample Date: 1 1-Dec-17 BRI,#: BRL-2017-0999 Lab Sample ID: -LSIi)-2017-03950 Client Sample ID: Compost Analysis Analysis Parameter Result A9Q1, Unit Method Time Date Analyst Igniiability Not Ignitable 70 Deg.F. 1030 SW-846 14.20 12/12/2017 KCJ Corrosivity as pH 7.9 0.1 su 9045C SW-8 13:16 12/1212017 KCJ _.r Reported By: tJnson,D. R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 5 of 12 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. 0.Bias 339 Valdese. N.C. 28690 Attention: Mr. C. Bortnick j Date Received: 1 I-Dec-17 Report Date: 26-3an-18 Sample Date: 11-Dec-17 BRL#: BRL-201 7-0999 Lab Sample ID: LSID-2017-03951 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivih,as CN * I mg/kg SW-846-7.3.3 16:25 12118/2017 KCJ Reactivity as Sulfide * 5 mgikg SW-846-7.3.3 15:10 12/18/2017 KCJ Reported By: StJn9oon,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 6 of 12 1. a Analytical Report N les:5!n.in; (ollectill Date: i_ t ; - ,r: Project: lieeet 1aoPkplr ID .., \u:elytrs It PQi Qu:P! l Hits DF Date Sualyzed METALS ANALMS(6010) SVV6010® SMOSOB nn0:y5t KrAS mgiK 01 Page 11 of 29 Blue Ridge Labs, Inc. � P.O. Box 2940 Lenoir,NC 28645 Telephone(828) 728-0149 Fax(928) 728-0131 Chain of Custody NPDS Re rtin Po Groundwater Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/Trust Fund Reporting Report To Bill To: L ci wn, V.4�,i s 4F Project Name: w PO Number: Ice Present: Y N C-Composite Field Preservatives Lab:Check G-Grab Tithe& Field Raid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested . Type HR:MM Check Removed Chlor °C Initials. °C JNY N Y N Y N P or A I .�, a -F G 1�,11,<� web �Co C f- R+, A$, C% , a, c�, 1< F K �r ,ayti b,5 :2.h t 14 M14% N.0 PAS Na,.v 3 t TIcN I p, y I ' Relin ' It d BY: Date: Time: [2 1 t 2 i 7 slued BY: Date: Tithe: :lptnt st+bmisslon ofsamples,cliou ag+t:cs that invoices,ta:duc ut the time wark 14 catn h.ted, saniplesp ' Open nccttunls ttr4.duc.t1 days Pitllowiug invoice date. A iitttuta ehMae of 1.SA pef month will he imptmed on all padta:aceounls. +Vhcn n thefiighiug deny do to nitre Ridge Lnh {ARL),buyer atah��rires BRI.to ptvftwm lolly the analysis indimed uboae and alm agrees to pay c0114elinn tN►d tutw,x y fees if the uaxeunt hcrottuh delitxluent. Aloe Ridge I.att4 esen•tl the right 4t it is he c client's for any w�n1t where pttyntt m has tort lush Hardy.in t:lfi�ct rendering that data uttsapptnt��d for regulatory purprrius. IiRI.cuutxtt gutttvnlw that any regu{warn tuuluttity will attiecpt tray work ttthmiticd.Ihereliirc it is the client's nwptv's"lity to r�llucst an this l'imu altprolxiatc tests. NC'DrNR Ccrtirted l.ah#271 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelaWenoirOgmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr, C. Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: IOXIOCOIF BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03061 Client Sample ID: ftM—PUSR Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Hg by Cold Vapor AAS *%10.005 mg/I 7470A 1994 10/17/2017 Summit TCLP Extraction Metals extracted SW-846-1311 Summit Ag */ 1.25 mg/l SW-846-6010 10/17/2017 Summit As *V 1.25 mg/1 SW-846-6010 10/17/2017 Summit Ba *✓ 12.5 mg/l SW-846-6010 10/17/2017 Summit Cd 0.25 mg/l SW-846-6010 10/17/2017 Summit 'Cr *✓ 0.5 mg/l SW-846-6010 10/17/2017 Summit Pb * ✓ 1.25 mg/l SW-846-6010 10/17/2017 Summit Se •r0.125 mg/l SW-846-6010 10/17/2017 Summit Reported By: S.I son,D.R.Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 7 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N, C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03062 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP ZHE Volatiles Extraction extracted SW-846-1311 Summit Benzene * ✓ 0.1 mall SW846-8260 10/19/2017 Summit Carbon Tetrachloride * ✓ 0.1 mg/l SW846-8260 10/19/2017 Summit Chlorobenzene *✓ 0.1 mg/1 SW846-8260 10/19,12017 Summit Chloroform *✓ 0.1 mg/I SW846-8260 10/19,12017 Summit Dichloroethane, 1,2- *V 0.1 mg/l SW846-8260 10/19/2017 Summit Dichloroethene, 1,1- *✓ 0.1 mg/l SW846-8260 10/19/2017 Summit MEK * ✓ 2 mg/l SW846-8260 10/19/2017 Summit Tetrachloroethene * ✓ 0.1 mg/l SW846-8260 10/19C017 Summit Trichloroethene * 0.1 mg/l SW846-8260 10/19/2017 Summit Vinyl Chloride * ✓ ii S 846-9260 10/19I2017 Summit Reported By: S.I son,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.275 Page 8 of 20 - _-- ----ter-- - - -- - Blue Ridge Labs P4 Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O.Box 339 Valdese,N.C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct 17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03063 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP Semi-VOC Extraction extracted SW-846-1311 Summit Cresols(Total) 4 mg/1 SW-846-8270 10/17/2017 Summit Dichlorobenzene, 1A * 0.08 mg/I SW-846-8270 I0/17,"1017 Summit Dinitrotoluene,2,4- 0.1 mg/1 SW-846-8270 10/17/2017 Summit Hexachloro-1,3-Butadiene *✓ 0.1 mg/l SW-846-8270 10,117/2017 Summit Hexachlorobenzene 0.1 mg/l SW-846-8270 10/17/2017 Summit Hexachloroethane *✓ 0.08 mg/I SW-846-8270 10/17/2017 Summit Nitrobenzene * 0,08 mg/1 SW-846-8270 10/17/2017 Summit Pentachlorophenol • 0.2 mg/I SW-846-8270 10,17/2017 Summit Pyridine *✓ 0.2 mg/1 SW-846-8270 10,11712017 Summit Trichlorophenol,2,4,5- * ✓ 0.2 mg/1 SW-846-8270 10/17/2017 Summit Trichlorophenol,2,4,6- * ✓ 0.2 mg/1 SW-846-8270 10/17/2017 Summit Reported By: S.it Vhson�,D.R.Wessinger *Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No.215 Page 9 of 20 Blue Ridge Labs PO Box 2940 Lenoir,NC 28645 828-728-0149 blueridgelabslenoirOgmail.com Client: Town of Valdese P.0.Box 339 Valdese,N. C.28690 Attention: Mr.C.Bortnick Date Received: 09-Oct-17 Report Date: 02-Nov-17 Sample Date: 09-Oct-17 BRL#: BRL-2017-0802 Lab Sample ID: LSID-2017-03064 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP Semi-VOC Extraction extracted / SW-846-1311 Summit 2,4,5-TP(Siivex) 0.5 mg/1 SW-846-8080 10/21/2017 Summit 2,4-1) *✓ 1 mg/l SW-846-8080 10/21/2017 Summit Chlordane «V/ 0.01 mg/1 SW-846-8080 10121/2017 Summit Endrin *`/ 0.001 mg/l SW-846-8080 10/21/2017 Summit Heptachlor *V' 0.001 mg/l SW-846-8080 10/21/2017 Summit Heptachlor Epoxide * `'0.001 mg/I SW 846-8080 10/21/2017 Summit Lindane *✓0.001 mg/l SW-846-8080 10/21/2017 Summit Methoxychlor * ✓0.001 mg/l SW-846-8080 10/21/2017 Summit Toxaphene * V 0.02 mg/l SW-846-8080 1012 U2017 Summit Reported By: S.J.Vo ,D.R Wessinger Concentrations are below Minimum Quantiflcation Limit except where noted. NC Laboratory Certificate No.275 Page 10 of 20 Analytical Report 11141-34 lilleeth)ij IjjjIV; jl`9'(117 1 A N I I'm ect: J f ut I Lab ID.. i 7 io 7', �i i INij lictif"millple 11):3o45 3(!(,1 3(tt", 31",4 ®nshsts PQJI Qual I nit. D11, Dare Affahzell METALS ANALYSIS(6010)B SW6010C SW3050B Analyst KMS 2 26 2-4 pm Irlinnid Page 11 of 27 Analytical Report I-I ItO"34 17 A\1 T 17 1',-t7.;4—, Matrix: ',l. i)(.!I. 'Iienl SAMI)IC 11):110b.; ; Z;l-'_;.17.; %na 1.1 st, Eiewlt PQI Qual I nit, I)i Date Anahiwd METALS ANALYSIS(6010)8 SVV6010C SVV30SOB Analyst MAS Page 12 of 27 Couil.pam !)jL;Q %rite Box Lam NC 2=5 F"2 30 7 T(IY (IienT ID4 Ulf)ll)� Cullec(�d.%n;l4tr Rep hut Result I nit, Nl;tlri% Niethtut I)F Regl_%I. 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C.7 SUrr :Rec S%xz.:? EPA 82ao 13 T 0; T"J":'0 1 TM &'9;2t'A 7 SL,f- T.,Iueri��F 9-,C� ;4-Rec 51itjq4 EPA 62.C-1)E r T M NOTES, Page 9 of 27 c , \ - .., I�Cia\tit{ {%1 1 :(Ij 7 1'(I:f'�eani-\'nitat{Ie�Anal vsk(S"1311 827,11) Client 11).= Lab ID# ('01lected Anahte Rep Lma Risott (nits M:alria ilethnd 1)F Reel e; Run lnalvst 5;:.�GE• — C r� r• n 17 -. T EPA U7,0,C Z ^G SJH �} 2 ?4 .S+r•Z1 - +. _ _ !dJ >:g:L S!tdz EPA E:-?C <L." .7 v Sim q --•t� ''^7::YJ ,COWrot „G.p�r.;rp;.,._ np t.• - _ ,^.'L EP..:,aca .Aae',]G 2 SJH ;2v75 C__ tr:;y�,=�. .aasw_ T NO' L S;•Jac EPA__"DG :r vl7 SJN NZI 3 . bL:�,z2�n_ S:L::Z-a EP:_.'GC 5N 2Ct' aai '- ZW <1•{:J� EPA E.7,31. _ U f 01 2 , SJH 1}r '! - 2;3t773 8f3: tae ..7:_ _,.L+._ <.: W%L S•u4;u_ E P A 3 7 ,v QC 2 ., I,:, . SJH 7 Naroaenzene T?L... '_C.13LIO tier'fJ'S. SFU'-'C-? EP:._c'C,C c _ , f -ti _ _ .. G.1H -C--S;W7I;;C1172130 7..CC, G:9r�. !30i-. _�:. Pzr.�., _ wrvi _? NO -yi S'i:-_ EPA+27:C ? sG� ,,. 7.[U:. 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Bra 3J,a _P.9a7 -.y r.iac y} T9 L C,vtt,� _ A 9C.r:•g 3i. r6 61%3.i4, -xix-.LL'" aj,L r ,Ar, t,Y.7r1y .. 3C5?J3„713!» v`3<v!7 ,w;"�fsi'3 Stsn G'C5 "G \ a ulge _.PA&:h 8 Page 5 of 27 E,5:1�5-I L-LJ t-ompam i'MUL RI&C 1-flls-111C fio),20-1,1 Lenoir\V 12. es?mv T 'I Y Herbicides Amill isis(SAVI 3 11.115)1 Client lD# I ab ILU Cullected Ajml,6 re Rep Lint Result I flits Nlatri% %fethud DF RoL21.$l Run Anabst Nma Si�ae EP -21A 00 5.,X UID myii Sw-gre E PA a I--,1 A 1 JBN lmr4 I CLT N(Ilatilex Client IM I'a If I I)q Callecled fla 4 Ic Reif Lull Result I nits 'llatrix Method OF Rtgl.%i Rull w, N,-)—ail, 82E., Ci I r-1, N,D!nzt Slt- Ce EPA Kp"6 1 t�-;-I 19: C,I T",j Z'S;20 NIEK ND g;; S!.cce E p 5;W.,B 20o, FV, -.:iL EPA 82F-0 B 1 0,500' 1,M T xn, 16 i9,2 C 7 Ca,c-c�n. D t��a?L $iucae EPA.a26r,8 !3r,x,4 0::DS rC!',5r-D!- TM Q,L Sr:cc-= EPA.P:=0 a I -ct,,s42 c 7.,. --ef,B I ND 7%3IL E P�,p-, X� 0;it C; N T) Sl,.zge EPA 9215k,B -LI0 7h1 CC, N,Dw mgk Shacx EPA 82F�3 S 1 500 TM D-o. r-7 D vmji 200 NP cjL S!,Ics EPA KZKD 9 Sur, ";GE4 Siwlcre EP;,.E';260 B '0;*i20117 TPA .3 C.re,-.oc'.. 10--'9 2 017 Sorr 7,-, vRet S 1 wC e EPA 526C'B ?U19,QG17 7 M1,j C ��-I 'Y-Rec SIV199 'EPA 52 60 0 1 E't NOTES: mn?4r, -Cv qAle- Page 6 of 27 I'I MV?34 LA !C i orim,NC I IT scmi-A olatiles %nak'is sx%1311 isr111 Client ID-- I all Ills Collected Im.111%le Rep 1-mi Result [nits Matrix Method DF Regf-0 Run Analyst NE, stu:��n EPA.K-70,C 2 �-i2o, 1--.D:cnvc,,en,- ne 7 E,a 131 BjH :SG if3t Lai, O01 17 24 CII .14 U, SILC, EPA CZ-1,+C L117 6JN .irC NO SiAri: EPA 82 TO,C 2 Qlo "Y f3Q.54 10 9i2O Q'- ND EPA C.C 2 1310 12 C;1 T SJH ci9.2 G 17 clesois -1val 4 Oc ND ::L S,ucge EPA 927C C L 2U' 1',1-1712017 SJH co-, Nr rcfl, S',z;z CPA 6:70 C z SX: 'a"7,20 17 UJI 1 A 5t EPA 6-73 C 2 7 tj C, -n,7 SJH :i055j3mIIl305z?--r-3 Oc I 1 0'7 0 c;;11.v-I ND mq L S ,ye EPA 8270.C 0' C., C� �'20*7 a 0�3n-" r4 rj .L STu^;a EPA a�-743 G 2 2 Q 1 Bih 05E;3%- IK62;3-30933 Gut IQI» 17 Nc, 5;,cce EPA a2-0 C 2 jaj7TZC,!- BJH R.!t- 7 Star 2%Fiuotc4pr.vci OzS -7 t' -,yRsc 5,.ac.e EPA C n.!1 7,.O 17 Sjfj l Lei 0,1'j�2-I 7 Sx-, Pt1e—. J-ic.9 S�uaze EPA K-I.;C 2 BJH FIK,16,30-621'C-S-. Ii Re, S-I EPA 4�7 0:C 7 5JVi i3r.)5-: Sur. 2 a Tj- E- SILrp EPA A-,-Q C', 0 17 BJH 00 S:xxp EPA iZ'27Cj C az 2,C,I BjkI E P L 7r�C. Page 7 of 27 Blue Ridge Labs Inc. P.O. Box 2940 Lenoir,NC 28645 Telephone(828)728-0149 Fax(828)728.013) Chain of Custody NPDS Reporting Groundwater Sanitary Landfill Hazardous Waste Industrial or C Non n State Reporting— UST/Trust Fund Reporting Report To: Bill To: Town of Vladese Chris Bortale Project Name: PO Number: Ice Present: Y N Field Preservatives Lab Check Time& Field Resid Temp Field Sulfide Chlor Field Sample ID Sample Date Time Sulfide Present/ Field Dechlorination pH Resid Temp Sampler Analysis Requested Type HR:MM Check Removed heck I Chlor °C Initials i OC Y N Y N Y N Y N PorA ac-szA•�� 5 �,., his A4, Cam, U fit,, N., Ks ham. ► Cakt c�•�� 'ho,Se z� .At,^ay1C1; 9; �I' . l i oil�YV i 1514 l� Z5ni*,Ab:1.+yt CArr•Us,d:*y t I -T-c t— i ish y: Date: Time: R Date: Time: !� 9 0 7 C/A Upon submission of samples,client agrees that invoices are due at the time wodr is completed.P Open accounts are due 20 days following invoice date. A finance charge of l.5%per month will be imposed on all paslue accounts. When relinquishing samples to blue Ridge Labs(BRL),buyer audtorrcos BRL to perform onlythe anal reserves the right to deny documentation for an work whore analysis indicated died above and also agrees to pay purposes. and attomey feel Ute account becomes delinquent. Aluc Ridge Labs Y payment has not been made,in effect tendering that data unsupported for regulatory purposes, ORL submitted,tberefbre it is the client's responsibility to request on this Form appropriate tests. NC I�NR Certified Lab 927S cannot guarantee that any regulatory authority will accept any work ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: Town of Valdese WQ Permit Number: 1990 WWTP Name: Lake Rhodhiss Wastewater Treatment Facility NPDES Number: NCO041696 Monitoring Period: From 1/1/2017 To 12/31/2017 Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) El Alt B (Alk Treatment)D Alt. C(Prior Testing)® A1t.D(No Prior Test) F Process to Further Reduce Pathogengs p If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost El Heat Drying D Heat Treatment D Thermophilic D ?` Beta Ray D Gamma Ray D Pasteurization D Class B: Alt. (1)Fecal Density D Alt. (2)Process to Significantly Reduce Pathogens D If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization D Air Drying D Composting D Aerobic Digestion D Anaerobic Digestion D .:::.:.......::._: ..._.::.:: ::;.. :;- i If applicable to.alternative performed(Class A or Class B)complete the following monitoring data: Allowable Level Pathogen.Density um er o equency SampleAnal caParameter in Slud a Excee-enceq11OFr fnal sis Tech- g imu Geo. Mean axim Unitsy Type nigue 2 x 10 to the WN 6th power per gram of . Fecal Coliform total solids CFU Q 1000 mpn per gram of total solid (dry < 1 277 MPN/g 0 Monthly Grab Vulti tube weight) Salmonella bacteria 3 WN per 4 grams (in lieu of fecal total solid(dry coliform) I weight) Vector Attraction Redaction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.I (VS reduction) D Alt.2(40-day bench) D Alt.3 (30-day bench) D jAlt.4(Spec.OZ uptake) D Alt.5(14-Day Aerobic) D Alt.6(Alk.Stabilization D Alt 7(Drying-Stable) ® jAlt. 8(Drying-Unstable) D Alt.9(Injection) D Alt. 10(Incorporation) D No vector attraction reduction alternatives were performed D CERTIFICATION STATEMENT(please check the appropriate statement) El "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." El "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Christopher L Bortnick N/A arer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print) Signature of repkrer Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T(12/2006) FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: �A LL- Q I Sample Date: T Dry Incubator Water Bath Sample Time: : Ll Time In : ,�.7 ,,l�,,, j; 1 7 �/,,� Sampler: / w Time Out : ( 7 QM_ Test Date: - i 17 Test Analyst: ;/YZ Tube # Broth Sample Confirmation Total Stren th Dilution Positive 1 + _ 2 A + _ 3 Double + - 4 (1ml ) + _ 5 + 6 + _ 7 A + _ 8 Single + /1 9 (0.1ml) + _ �J 10 + _ 11 + _ 12 B + _ 13 Double + _ CD 14 (0.01MI) + 15 + 16 + - 17 B + - 18 Single + - 19 (0.001ml) + - 20 I I + SterilitZ Control: MPN Index: Q Single - Strength Broth: Double - Strength Broth: Single - Strength Buffer Water: Index #: Double - Strength Buffer Water: 10 X MPN Index/ 100ml Iv x A-1 Broth Lot#: 3 0;�q MPN /g Largest Volume x % Dry Solids x, 3 Incubation Times: Dry Incubator: 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM '/ } PERCENT SOLIDS FOR COMPOST MpN aAT : •_ ' 1 . I „�..,,. AN +IL'YST: DISH WEIGHT. � 4aRAMS U(SH WEIGHT & WILT SOLIDS: ����® GwS ()ISM HT & OILY SOLIDS: ' WEIQ L GIBS , NISI"{ WEIGHT & Wes' 86LIDS DISH WEIGHT m WEIGHT OF MET SOLIDS VA'.'t6hWe++bAa c�MLf T.atC•.AEar4.. ' '� VS i 1 DISH WEIGHT DRY SOLIDS - DISK WEIGHT WEIGHT OF DI Y SOLIDS m CALCUL AT101ii11: 96 SOLIDS 4 WRIGHT OF bFtY SOLIDS � x 100 % WEIGHT OF WET.SOLIDS x i©a % V6 BOU08 � 1 L{ 3 � FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: E,6L L_ C? - 1(a t�vP _ Sample Date: Dry Incubator Water Bath Sample Time: Time In L - I 1 An— , 1 pn1 Sampler: Time out 3,z .A%, Test Date: r _ 1 Test Analyst:. Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + 4 (1 ml) + _ v 5 + 6 + _ 7 A + _ 8 Single + _ 9 (0.1ml) + _ 10 + 11 + _ 12 B + _ 13 Double + - 14 (0.01 ml) + 15 + 16 + _ 17 B + _ 18 Single + _ r1 19 ( 0.001 ml) + - �D 20 + - Sterility Control: MPN Index: Single- Strength Broth: Double - Strength Broth: -- Single - Strength Buffer Water: __12� Index #: Double - Strength Buffer Water: 10 X MPN Index/ 100ml A-1 Broth Lot#: 50 MPN /g = _ I o'� � _ < a Largest Volume x % Dry Solids x 3�a.y Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOU FOR COMP06T MPN . � I DISH MIGHT: ..,. 01.8" WRIGHT & W r SOLIgS: GRAMS w"^.aLl u.Ewa':+LTG".+u..fc74"•Y.CS'TT._�.17'• i..r.,wGw�'$�'.Q�^.��P.tm�vimx.s.cw....:Rne -aw.._.. , Fmp�p/►gip g+p�p n, ,.i«:u`�:�vw«.�o...'k�C,'��wo�.s-.�:+':�fG1R&It1,�2tt» �,, hAbs�IVAY'!�I I�I�I��Iq�n° �='�idr..:}J�J1;r�x+�'u:'�}fi1C .::�,��L::'ti6t.•":.'�:�ww1Gw""�,":6:��:i.M«"°L'•'iJ II I I , I ICr�IS 4 Ut1 IGW�" A W 'SCraLft I. , DISH WEIGHT WEIGHT OF W, ET SOLIDS ��y aaMVYC W�.wm,aetwdpp4,�t„y,,,yli NaiPctuHn,•L mxNfal+heati7.�:tu�ad:.y � � f es..+ ..,any-vl•..ec:�m;r �['�11(( arNwTv�tlroaitr�, - DISH MOW : DRY SOLIDS �ol DISH 4A4cIGHT WEIGI�i I OF'DRy SOLIDS MaRj1•e/faMM/GVME'�Me.1WGLL:i.VfypyKi�'•.ML SOWN weatr OF bRYBOLIDS 1 HCt1Rllr=:1<1 itrANNLL 12•TYAa✓.ivf .� ' . (v1y wst � ��fMuuAnON� wA'41.rwnKisrltw.NP4cyN ' ' ...�'1.i+.w...��i�'i.vWu4.�'nL\ �.M.-�N4�.+:.I�u......r•W+w�".�' 1Li'�iCZt. � .' \. °..._.�•,�•�,,;_, x 100 % MIGHT OF NEST BONDS lb BOWS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C 4i E) Sample ID: FA L-L - I Sample Date: I - l 7 Dry Incubator Water Bath Sample Time: : 4 cd A v. Time In : 11 A-,n I a ', r I Pn, Sampler: G �,j Time out fry: I I p 9 fs4-01,. Test Date: f - S - 1-7 Test Analyst: Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1 ml) + _ 5 + 6 + _ 7 A + _ 8 Single + 9 (0.1 ml) + _ V 10 + 11 + 12 B + _ 13 Double + _ 14 (0.01 ml) + 15 + 16 + _ 17 18 Single + - 19 (0.001 ml) + - 20 + _ Sterility Control. MPN Index: - Single - Strength Broth: Double - Strength Broth: -< Single - Strength Buffer Water: Index #: Double - Strength Buffer Water: _ 10 X MPN Index/ 100ml �� x �� A-1 Broth Lot#: j v 3 O'q 11 �'` MPN /g = __ — _ 02< Largest Volume x % Dry Solids [ x 3,0,� 3 Incubation Times: , Dry Incubator. 3 hours Water Bath: 21 +l- 2 hrs. MPN FECAL COLIFORM / GRAM < WN DAM . 1 ANXYST: , DiSi i Wf tGHT. , GRAMS DISH MIGHT & WET SOLIDS: d, ��a> 3 GRAMS DISH WEI Hlr & DRY SOLIDS: Q GRAMS ppooppes`�su.�; h,7bdp/�7��+p .p p�®�Q{ 117IFI 1 A6'I4iM9.9 a • CJIS MIGHT A WE`D' �5bLIDS DISH WEIGHT WEIGHT OF W. SOLIDS .M?.YMa•Y.�..+.M`"r^^.^wvJr.rrtMwa,N.n11N..p.P�,F�i:atww. - .Hvss.+tlT�iGR>-=.'�Zyy�41SANA , � .. • .'KtVl��•I..H1..IIR•ANllpy�¢y�y�.�.YytaY WSue:.um.-Wsanwr.��ei��ECltu�aom.tnxwwun �'l. � C/� �2\ ����` •sa..�wJ..xw DISH VOIGHT a DRY SOLIDS DISH WEIGHT WEIGHT OF'DRY SOLIDS '�.n-�r.:.v,p.."rto.w.wuweY.•w..xwa¢r� '' wa,.=a�.n..Y.•sn, ++..e-ise+..+®ca,ncY.�uu„�wrcvmNeaY „e,.,�,rn,,,,+r . '� Sf��liJS wellw OF bR SUDS � MOW OF WET 801jDS J FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: 1. Sample Date: o� - I -7 Dry Incubator Water Bath Sample Time: ? A, Time In 5-, I., ,S`Q loom Sampler: ,�= Time out Test Date: Test Analyst: . Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1 ml) + _ 5 + 6 + 7 A + _ 8 Single + _ 9 (0.1 ml) + _ 10 + 11 + _ 12 B + _ f 13 Double + 14 (0.01.MI) + 15 + 16 + 17 B + 18 Single + - 19 (0.001 ml) + - 20 + Sterility Control: MPN Index: 0 - 1 Single - Strength Broth: --. Double - Strength Broth: Single - Strength Buffer Water: Index A Double - Strength Buffer Water: 10 X MPN Index/ 100ml j�x� A-1 Broth Lot#: ��,3®mil� � MPN /g = = _ � Largest Volume x % Dry Solids a -9 Incubation Times: Dry Incubator: 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM 6 GRAM PERCENT SOLIDS FOR 60"Mppo �p DISH WegGHT-1 a a.._ = ' aRAMB DIM W01O r & WET SOLIDS: GRAMS �n DISH WF—IQN ' A DRY OWN: ;. � O. I'S «�1"w.°`.�Sr�.Y�..•`�T�f4"i.;�:Gt�1�W��.ila'�' "'b1.Q:«.:ate P PISH MIGHT A WET �SbUDS DISH WEIGHT WEIGHT Or- WET SOLIDS "•�++auc�sw+._.:.,�//,--``+Wmv�+,.. v:MeYr<W—nnmsnMw+.+��.wn,uw.�•.� ' Wv;w::,a5n;:wz.aronJar °a DISH MftT 8, DRY 80Ia,I08 n., DISH WEIGHT IIUEIGI1T OF DRY SOLIDS •�Q•.iY PNI�}.�Im IN/mcvaevae�\u�4,u:=.\�fnN�3'�.n:.•.V� CALCULATION +Warivtu�.I�..NJr��er,.Qgsery�,p. Cfi�nV/.\K:LnTa�AMt4Wr�yjy,Swr • ' �l Cb � e'• j' 1 .wn°v�uanG'v.`''+.v'°.^"q' •mY'Liw+nvcs-vbr.ro ! /\�lnl l+fm+,+.t,*.r.can rrwtyy •Mi��iY,fy� �7i ' • a Nei 80=9 WeIGHT OF C]RY SOMAS p)�g ,,{00 �{D,, � 5• V d'G +WW �j(f IGHT OF WEI'SOLIDS mm°y"'°'•"a^ww..a.uv..�..e+,r..+.c.uroa•.c,.eruo • � • It OWN FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: ,.�-►�� Sample Date: ;� - e)- r 7 Dry Incubator Water Bath Sample Time: _q : q 7 ,gM Time In ®: o ,a : 50 A-,i Sampler: C: ,��. ✓ - �J�n•.. " ��� Time out Test Date: J . C)- r Test Analyst: CA, Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1 MI) + _ 5 + _ 6 + _ 7 A + _ 8 Single + _ 9 (0.1m1) + _ t 10 + 11 + _ 12 B + _ 13 Double + - 14 (0.01MI) + - 15 + 16 + 17 B + _ 18 Single + 19 (0.001 MI) + - 20 + - Sterility Control: MPN Index: c0 Single- Strength Broth: Double-Strength Broth: Single- Strength Buffer Water: sa' Index #: Double - Strength Buffer Water: _ 10 X MPN Index/ 100ml I� A-1 Broth Lot#: �,�� MPN /g = Largest Volume x % Dry Solids dv,y ,2 e.k Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. / MPN FECAL COLIFORM / GRAM C t PERCENT SOLIDS FOR COMPOST MPN l 7 AWL'YST: CASH VWIGNT WET SOUN: GRAMS GRAMS '•'�'"u7^u:J7}�Y.IrIa:C"it:�r n�,, -,---' �:.= DISH WgldH " A WE r '8bLlD8 DISH WEIGHT wElaI•'T or.. V. ET SOLIDS a + W�.fL::1:41a:.fyf.bAV'R-Slfi 'tiiuGf ' �` C�� RbFtNibNM/fdy , .r1—..AW ' • h.MIIMycyRi�syy. V DISH WVGHT 8, DRY 801.108 DISH WEIGHT WEIGHT OF'DRY SOLIDS ", +Mmuv+mC'7a1mJc'.sry.�q�y nmMe.:+rha+mmYnbMf*+acaa r1M1.MY a.tT/�w ixi* Msy ��//p�•L 3 ' • �Yf.�nlavK�11.Y "— V ".+5;`� .Ty::;,y,_,aT�s�!T;_s"+,_]:elC.G1'..r^... `'�$t'ilE:.��^'.iLir•:.f^.r�ilt-'Tr..;.�.:�'t�.,:JiSsl'.E'�:n'�t"..:1T:—j^'�4t>�--...^-�y...: ..n.-,W„nw,un ' CALCULATIONS: x 100 WEIGHT OF WETSOUDS ?� 100 °,A f J FECAL COLIFORM - -MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: Sample Date: ,� - i i '7 Dry Incubator Water Bath Sample Time: q :...� o Time In G': -A,,— ('4 ; Sampler: (?� �,„r.z cZ< Time out (a ; 1 PM-Ll - , Test Date: 3 - 3 1 7 Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation positive 1 + _ 2 A + _ 3 Double + 4 (1 MI) + _ �) 5 + 6 + _ 7 A + _ 8 Single + _ 9 (0.1m1) + _ 10 + _ 11 + _ 12 B + _ 13 Double + - 14 (0.01 ml) + _ 15 + _ 16 + _ 17 B + _ 18 Single + _ 19 (0.001 mi) + - 20 + - Sterility Control: MPN Index: Single- Strength Broth: _112f Double- Strength Broth: --42L Single - Strength Buffer Water: = Index #: < Double - Strength Buffer Water: 10 X MPN Index/ 100ml A-1 Broth Lot MPN /g = - f- ,,2q Incubation Times: Largest Volume x % Dry Solids I �� Dry Incubator. 3 hours Water Bath: 21 +1- 2 hrs. MPN FECAL COLIFORM / GRAM � l PERCENT SOLID FOR C' POST MPN DISH MIGHT., c s- �Na ' NAN MIGHT WET SOLIDS: ..3 j,�7 GRP+m6 018H WEPHT DIY SOLIDS: ' I S �a�'����'1'd�'�'it�P1SA •..�.�..-:,. �rra�:t�� �,r .�:s ��:;��'..�s�:::� a � ^�[��:�Ff:N:r.73d:-,;.:*�rdcL�«�^,�.s:�UC^.ai,'.4 •;;� , ..: rilsH W91611T 8, WET 'S6LIDS DISH WEIGHT om WEIGHT(fir' WrT SOLIDS .'wn>awvr...,•�n.w....w.xw.,.,,•+uY.,mmno..ww..n+:=5n.... . ' E CW�nnmcrvgw.e.wgrrw,,.eu 1 .aw `rya k,SfiC:,}aq.a.l,.tlr.V•cY.:pN .R:;ry1L'�V•1'. ' • 11,5MIF.y..�M1�J Sln ,�y� A..P'/YOTRYIOdQA{ DISH MIGHT 8 DRY 801.09. 45tl1 DISH WEIGHT •m WEIGH OF'DRY 59OLIDS Yr.laply./p:dV+•rcavM4-+ar.YWtU4;>'=.5..4pyru�•Y.R•�sel. . 1 ,�C���RiMn\+NWY nAger_•:esSx.OnteV.y�trG.eYC �CVIa• ,a.l+•.na+.+n. .VN� FCALCULATIONs: 11�IY Q.�7ira.'n..•+�i ' • I • % SOMS WaIow OF bR Y BOLIDS c� WEIGHT OF WEI'SOURS 73 ), -j ?'� FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C 8z`E) Sample ID: Ti---P, 1�7 Sample Date: j f r 7 . Dry Incubator Water Bath Sample Time: 9; Oki Time In Sampler: C a� Ns-c Time Out Date: if- Test PM Test Analyst: Cx�l Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double _ 4 (1 ml) + 5 + 6 + _ 7 A + - 8 Single +. _ 9 (0.1m1) + _ 10 + 11 + _ 12 B + _ 13 Double + _ 14 (0.01ml) + _ 15 + 16 + _ 17 B + 18 tingle + _ 19 (0.001 ml) + 20 + _ Sterility Control: MPN Index: Single- Strength Broth: Ice Double - Strength Broth: Single - Strength Buffer Water: Index Double - Strength Buffer Water: �6` 10 X MPN Index 1100ml lI X A-1 Broth Lot#: p 1 MPN /g = = J� Largest Volume x % Dry Solids Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR 00 B O IT MP'N GRAMq a. "'m 3:�.Iw11w^:.�"i7�..5. 4:Gi3'.�A'd�•"�i�.. 1 �w..i. ;rLo:,...".""��'�.' i�'1�,:.'�:^.�+.a.�'.C(�t�t :.a�'^..'°3tL:�.7+�i+�itr:�l�sl;rax�'t..:nra! �.�s , II • 1 1 PISH MIGHT WET 'SbLID DISH WEIGHT r3 WEIGHT OF WET SOLIDS ...-ti p a.^••le���w.c am m..r�.iiaumaw.inxa�,�/I ,..im.,,,.r..Pw I , DISH W010-HT 8, DRY SOLIDS nl,H WEIGHT m WEIGHT OF'DRY SOLIDS '�W.Pr+.wclYrpl MrawnG�.enlwtla.i::\n6aH�L:?'++..C.'Mt iMFiraCwiFgyaNwCi"R.a]i�1iSY..ysRliaietV '1 wal.iK'avr.ViR9laM�q�.�aa;yf4a'✓t 1 tl.m.,neP�t+rt+nCN .iPrrV��.MC 7i�W.iw.f4oMMa I • L.m�'.«i4'FPy;i.;.•'`"a��?'�J7i�a{L7.�dw':.::^_°"^.1'"�.."..�...�.�Pii1�:.'LSi.7`-�'11i.-t..&'•.'.:.�i tC'i71C''Li=:i:3�]���'ii�'.y'1773."i.,t� �pT_�ww., . CALCULATIONS,: A' SMIDS MIGHT OF bRY SOLIDS ,. " MIGHT OF WST SOLIM f 1 x 100 % FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: W..., Sample Date: y - I Y- I-) Dry Incubator Water Bath Sample Time: Time In 3, I Sampler: Cam-- Time out Test Date: Test Analyst: Tube# Broth Sample Confirmation Total Stren th Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1 ml) + _ 5 + .6 + _ 7 A + _ 8 Single + _ o 9 (0.1 ml) + _ 10 + 11 + _ 12 B + _ 13 Double + - 14 (0.01MI) + _ r16 85 + +7 B + _ Single + 19 (0.001 ml) + - 20 + Sterility Control: MPN Index: Ll _ Single - Strength Broth: — Double-Strength Broth: -4 Single- Strength Buffer Water: Index A Double - Strength Buffer Water: ' _ 10 X MPN Index! 100m1 A-1 Broth Lot#: .S a ���� 5- [VipR1 /g - _ Largest Volume x % Dry Solids I a�• �2 s,�' Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM 1 GRAM PERCENT SOLIDS FOR COMPOST MPN t DISW WEIGHT.- 02 <�, QQtAMS DIAN U I(aWr & WET SOLIDS: DISH WEIGHT 9 DRY SOLIDS., , m L•17a��q{:A,�".yp�g�uQ��d`T�K.{«C.•Z733aA.^,;T3,�i' ' .mot+{..:, r pp``ryryrr��++��,w'1tY714i1gC3o° -�'.�''�qk.'.'J".TOL:nrr.uw..�:�'1'USI 'dC9.:k°"t—..%lt�':+ 7 �:.�`t� uCf"..�al"...'•v'^�;,�"S:iR6C.1"1.:. --rn M.. {I t ,1 rJISH MIGHT A WET (SOLIDS DISH WEIQHT WF.IQHT OF WET SOLIDS . 'MMN•rwa,.W.ww.weuM..ntyyvnyFlellty.PMh�:•:'-�^•e'1 - wrbrvtPwy�s.tS.i�1.NNhy'?MpA e , E hflM='1I1{M•-sa0an'w.aNt { I �< I 9 I '1Wi:fk:tu*i':W�:a+Wav2fi�NafhN^11��urt ' • YMaRi1+fN.nV�+aW.GWIiA ,.CgaMIHloaWtsri�tnlw,SOu.{cs 1 1 DISH VfflGHT a MY 801.108 aal DISH WEIGHT We OGHT OF 1DRY SOLIDS ''aOabOi.I:awiyy,Ipl.MVrtypHQ.n1Wt{�5:=.:..WIW�-e•`•C�aCI IrCtCM1st'JGHehyglm,•y • � .nntfe..9tzc6Tl/Ma! Mt,:C'+f'+RSI?av 1 �'Oeie'1"�w.�.C1MmVCtVi*+.�a+AxMe. ' '.eG_•ifi�.:iYiry'..•.�y'^�G�!l;r�"u�..�l!e•..+.+F.:.,i^'°.�..��nesY`--C�`udf'i'»LCx..^'.uM.�.�T:'-�',�T'.P.ri.�'�.�l�i`»l:�+i'INYr�StlM"'^al*" —.,va1*,-.•.,,�,rm,m„r..n...,, •� . BMW IiNMe der OF bRY BOLIDS x 0 � WEIGHT OF WB I'SOURS GA .t. FECAL COLIFORM MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample.ID: WZ.•i ►� - 4 f 7 h wP, Sample Date: _ 1;Y, 17 Dry Incubator Water Bath Sample Time: 7: Time In ,,,_ Sampler: Time Out Test Date: 3 ® ` Test Analyst: Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 + 7 A + _ 8 Single + _ 9 (0.1 ml) + - 10 + 11 + 12 B + - 13 Double + - 14 (0.01MI) + _ 15 + 16 + 17 B + _ 18 Single + - 19 (0.001 ml) + - 20 + Sterility Control: MPN Index: Lq _ _ Single - Strength Broth: _ Double - Strength Broth: - Single - Strength Buffer Water: Index #: Double - Strength Buffer Water: 10 X MPN Index/ 100ml A-1 Broth Lot#: J Q MPN /g Incubation Times: Largest Volume x % Dry Solids Dry Incubator. 3 hours Water Bath: 21 +1- 2 hrs. d MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR C' MPOW MPN CIS DISH WEIGHT.,. GRAMS. 1 01814 WEIGHT 9 DRY SOLIDS: RAMS ��r��'^�;,� a�as��'�t wr+a�uu�" e., :..n..,, ,...,.,,,x,�• , ' MUM�+p,a.�1 p�® u.tW.,...Qa4 .Q&{l�;p�'f:..'PRC"—�i'I.�.S:)`.1Rt77�'11: i.1• •,--•r 4nbdlVd�e�I ATICIM4.9 .1 1 1,gISH MIGHT A WET 'SbLIDS DISH WEIGHT t o WEIGHT OF WE'r SOLIDS ..rw..rn.xw..»•w......�*�.w.n..uu..a•w�.*�:xe+w...r+w - e..wn+*w>�..asw.c,:.-.a.n+ayew,,., . vsMtYa�.�.lniim<r-aruv�,omsr+«.�.atsvrm�� �j ' " �•- `p eta ,.a�,.,�4>ea.. '�/ .�f u•,n<,:.,a-.,tr.•n,�l.r�n.nr,>�-;-.�,r�a„d"a:�.,.o.m.,.aw„ DISH WEIGHT 8: DRY SOLIDS DISH VV IGHT WEIGHT OF1 URY SOLIDS •�'.�.,+M1�^tnlave�ppeMWlgyr.a.rpr.\4JIaLL��}lnppy..;y�i...{•;sp! y, ��,��,�� . 1 ,�ttmV+gte.V ,vA.Nc�.aw'n(un6M+�*=+WYfi . 1 �.;:.c.:..--,�ra:�,:a_�e :max-=:'�".xc•�1e�t��^r_r'k.:. •�.-�.l;�xc.�:�„n�.�:c� r,,. ' WEIGIAT OF W81'BOUDS i�0p 0% 4$ SOWS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: S PO .,rG — ��y -7 Sample,Date: _ _ / Dry Incubator Water Bath Sample Time: 00 A Time In Sampler: �. Ua�,; 'Time out. 1 9 Test Date: I _ Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive 1 + - 2 A . + _ 3 Double + _ 4 {1 ml) + _ 5 + - 6 + _ 7 A + _ 8 Single + _ 9 (0.1ml) + _ 10 11 U++ 12 B13 Double _ 14 (0.01 mi) + _ 15 + 16 + . 17 13 + _ 18 Single + _ 19 (0.001 ml) + _ 20 + Ste Y Con trot MPN Index: Single - Strength Broth: Double - Strength Broth: Single —Strength Buffer Water: Index #' Double - Strength. Buffer Water: 10 X MPN Index/ 100ml A-1 Broth Lot �3 c1 cI 57 MPN /g Largest Volume x % Dry Solids Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +1- 2 hrs. / MPN FECAL COLIFORM / GRAM ' PERCENT SOLIDS FOR CO POU MPN DION WEIGHT., GRAMS w mnyJw rv.ac•::.e7 DISH WEIQNT DRY SOLIDS: lit 1 , �n�:b�44�6a1�7°�1'1��11�0 :�rsatr�z�+asr.�:.;�,xr.�;,�.,a.�;�:�,:a ��:c:;�a� r.�;. �;�•::�1. ;�A.��• ;:� PISH WFIGH1" A W ' 'SbLIDS la,. DISH WEIQOP T ax WEIGHT OF W. SOLIDS '1:.W,�.�M^�mMeMt.No.w,M1.+NN..O�w•h+R�,�..t1f.t.,, • , mPmrrCw.wlm.�m✓„rr..os>�..�.>ltwv�- WT•ta.::tJ,axG:Wnab+Y,evw•lkt.auN.•a`:IM1�it�4+.i"wwn .lwK'lAa%surnnWV. �vOd�,Wu>L� ' • bf+IN1.T1i DISH U DC-I"'IT 8 DRY SOLIDS 4 P, DISH VVE1 HT WEIGHT OF,D.RY v9OLIDS Pn'uy¢�yyplNW.a.aetaWey4WaYL�lnanit.i�'+.R•..e1 , IMmMagIN�fPvtR�.xay.�gV+41i'W • • 1 I INw4rc'.�9jxml+.TaYµgrcY.<'�Cv,�yaa 1 ' • Ll '+w�PGVl,.wmttarsiw.nre+cay LAN:=���iu8'u.+i.tw'���lc�"�dfii��,;.7i aZC7�lw.:,w. • ��{-«�n M ! � ."'°M•"��.�" ^��rl�:.La'1�"i.7'r�',Ylli.;.a 'a�y'* w�.�F�it".�YwQ.:''w•,•,y��^.t =^1cw,en y^va.o.wu1�.T,i�14xt=. S ' WEIGHT OF MT SOURS x 100 % aeap� FECAL COLIFORM MULTIPLE TUBE FERMENTATION (SM 9221 C 8< E) Sample ID: 17 Sample Date: _ t-(— ( -� Dry Incubator Water Bath Sample Time: = 02 q Time In �� ' I Sampler: � �. �c17��caC /�� �I y Time Out If : 1 (3 A,, ," n1 Test Date: �- : _ t Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive 1 D+++ 2 A _ 3 Double _ 4 (1 ml)� _ 5 _ 6 + _ 7 A + _ 8 Single + _ 9 (04 MI) + _ 10 + _ 11 + _ 12 B + _ 13 . Double + _ O 14 (0.01 mi.) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001 mi), + _ 20 + Sterility Control: MPN Index: Single - Strength Broth: -(�' O Double-Strength.Broth: -ate Single - Strength Buffer Water: Index A J Q Double - Strength Buffer Water: A-1 .Broth Lot#: MPN /g 10 X MPN Index/ 100ml I®a x 5 g ® � = Incubation Times: _ _ V Largest Volume x % Dry Solids 1 x o2U- Dry Incubator: 3 hours Water Bath: 21 +l- 2 hrs. MPN FECAL COLIFORM / GRAM 19 PERCENT SOLIDS FOR CO POU MPN 1 ` 1 • 1 DATE. . _ cal 1 14� AWLYST; . DISH WEIGHT.- �`._� GRAMS ' MAN WEIGNT & WET- SOWS: GRAMS DISH WF.IQHlr & DRY 80I.„I68m � .a�a� GRAMS a""^'L•wE:'+Y�•a`;�l::b.:'T�y�Gi3`�39�R'�T�iJ?al' 1 sunn+ ' map nn ��vgp p�p� �'r372A:«I.m��we"'�"t•1.�' 'fG14'3�1 ..:it°"....�{"S1"--"'�+T+1�•4:-T.fd'.N:ISY.4�H':�1:J aa7"^..�".�"..""-uwS�R�n'^14."��'•7ti'�'C:swf.'"..Cit�:i�'i::.'°i;.'2.".1 s�+�b�{UA�191 h1�ll4ilq�o , 1 IDISH VV IGHT A WET 'SbLIDS Ifi, DISH WEIQHT M3 WEIGHT OF W,Eff SOLIDS .Kph+aw.n.Y.•.w..�e+w+nwa*+..Iwayyy�tl,M1u1♦v�weq A=-.www+w� • 1 0.•�♦^+�vme„94a4*+=.`�o wStWtKY1+N11IIItl'.YI'IWu+c1e1*+.rvva/a r 1 rsra a �•y7 wrt+te:aw:.+Vv.ammmrem•wavha:.�r_..,v.Lw _�'�Y x _ NN.LiY• C� 1 DISH WE10 8, DRY SOLIDS Ltel 1� ' qIS�j WFIt��IT m W�II��I�' � DAY SOLIDS ��q,♦q/�//'��'yypp.Hiq��pi6lin��ulYa�y:arlJ..'ai�.i a11`�7iw��.wNii� �.�.�1 • 1 �+/">'Vi�.P•L —'"^�.°�C'I+:ntT+w`.�.��'.�T3�1Fi:L �+'�"�''>�4L:'I.C.'•�L'�`a.'.L"Pr<iLl:nr.AV:►LTtf�w�w.rylx-..°j .•��r�.rl��..c+•�t.w�•i r a - ATIONSS. ,. WEIGHT- WET SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample 1D: _ PQ1 Af �® ) -7 Sample Date: (®- A'_ - Dry Incubator Water Bath Sample Time: o; a c Time In Sampler: 6.A-r�ri-ter. �rz<L , Time Out Test Date: � ,� �.� Test Analyst: U T ube# Broth Sample Total Strength Dilution Confirmation Positive 1 + _ 2 A + _ 3 Double. + _ 4 (1 ml) + _ 5 + 6 + - 7 A + _ 8 Single + 9 (0.1ml) + _ 10 + 11 + 12 B + _ 13 Double + _ 14 (0.01 MI) + 15 + 16 + - 17 B + _ 18 Single + 19 (0.001ml) '+ _ 20 UNIC + Sterility Control.- MPN Index: <-,3 Single- Strength Broth: _ Double -Strength Broth: -- Single - Strength Buffer Water: Index #.' Double - Strength Buffer Water: 10 X MPN Index/ 100ml A-1 Broth Lot MPN /g Largest Volume x % Dry Solids Incubation Times: I X 30 -� Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. / MPN FECAL COL.IFORM I GRAM I • t PERCENT SOLIDS FOR C' MP06T MPN. DISH WEIGHT: .,�, GPM$ ' f 1, 4yl IGt�I�I° "T SOLIDS: v.�.��:� GRAMS DIN W IQHT A DRY SOLIDS: �� � GRAMS . . GUNFU'9' � '� '��,�..•.. r ,. .�u� tre�s�ac�.ter:.--�::�r. x�:�:�r :s:: ,—..,,,.. 17'I RM4 ,. laii.WvlGHT Ili ET 'BbLIDS 131811 WEIQHT 0 WEIGHT OF W. SOLIDS . w"^+woc.�ta4rt+::..—.S�waCttavw nnu:rl:,a..nnmrmAtwR.vm,*•owna:.wJ«+n m r �:G�:4A�.Wf.ahvxda�Napyxy;�:�vv.�'+Wn fbM+.M4'�.Wt141 4yM+aa.NTi+IDvtnyr:�7� . I j I : DISH ,W00HT DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS ., '"QPbwir.:m.c�ygo��'�..monrc+oaawtw:=.+nspvra:+w•:.s'm vneaiWwJr_xtnasWWetf vmkc:.naw<rtNnupre'�GjR , . '..M:=�n�I11.�i+�+'r+�+c"�'S�.t a'' �Ii�o�Cl'r.S+..aO..T%'w.1'^^C.C'^•�".�y1C'�E:.'7YS�Li:—$.f"r..�,:P;•��-•su'i�.:�'13iY�°iC'�L1�w�4 Ya S CALCULATIONS: NS: ' WEIGHT OF WET BOUDS f FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: oLC�I"7 gyp. Sample Date: _ G Sample Time: . _ Dry Incubator Water Bath ®;Sampler: Time In � ; �= p^ti '�rz �. tr.�.�c ,.5 Time Out P l Am,' Test Date: Test Analyst: Q Tube# Broth Sample Total Stren th Dilution Confirmation Positive 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 + - 7 A + _ 8 Single + _ 9 (0.1 ml) + _ 10 + 11 + 12 B + _ 13 Double + _ 14 (0.01 MI) + _ 15 + 16 + - 17 t _. B _ + _ 18 Single + _ 19 (0.001 ml) + _ 20 + _ SterffitZ Control: MPN Index: Single- Strength Broth: Double - Strength Broth: Single - Strength Buffer Water: Index A Double - Strength Buffer Water: 10 X MPN Index 1100ml A-1 Broth Lot#: 6_0 3 O MPN 1 g x <12- < aq Incubation Times: Largest Volume x % Dry Solids Dry Incubator. 3 hours / Water Bath: 21 +/- 2 hrs. / vvv MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN I P ' DI,SH V IGWr & !NET SOLIDS: DISH WEIQNT & DRY SOUDS � • . Q RAMS ��w.' wG�S:tm+`virtmlla.a•.» - - y �5.+7:9L409.. J� ��'�RfdR�p��'I��l�4 .....P..: ..,..,.,..,.5::�«a ��s.r:.ss�:rasr_��,�.:�,•� '_::��. r �::,1�:~.;�:� 'I DISH WFIG"OT A IIUU ISOLIDS DISH WEIGHT va weaI"•IT o wrT SOLIDS aLLNh7+�J.w111111ttav/„pMaaaV'a.�•�a.P,aYJM E ,�2-cz 7 02®F. W.lt4::t:Rm.-W.'Oh,o tgPbVaah.O��.�i G.+•�-'W M++aawa�laaa'N•vn�lav I ;nartMRWAtgvltl�naaasma.�y I 1 DISH VUUGHT 9 DRY COLIN u15 DISH VVE19HT •� WEIG14T OF DRY SOLIDS �7OpbP.I:q[iyypOeMefgents•We.1YWIaLL:—IV.FPH�: 'i'LL•�4'.sYl 1 •Vaw��MMmrt fV.C.AIvlC.lYv'1'AW�YIL' , a.m522naamx+wla�x P I • ::e-:'G1.`jiu''�'•:±::.. '_.x"i,_la�dltTt":.'..'.�..".�.GZ,T�;r."SvlGllEbi�i^:,iµ„�.C..'.'.'•"�SC�i2'C:La'.�•'t`.di�s::lFtt:z'lLZ3:air' .+.... ,....a �t�,�'P�J�„�Td®Ilea ��••• ,,...��� .�...�� ,, r.�.-�••� SOWDS V4/aiwr of bRY SOLIDS 100 la Vim. WEIGHT OF WETSOUDS X 100 % 1$ SOURS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (S.M.9221 C 8< E) Sample ID: ® l- Sample Date: Cn_ - '7_ ( '7 Dry Incubator Water Bath Sample Time: Time In Sampler: Time out 1zP A Test Date: Test Analyst: Tube# Broth Sample Total Stren th Dilution I , Confirmation Positive 1 + _ 2 A .+ _ 3 Double + _ 4 (1 ml) + _ 5 + 6 + _ 7 A + _ 8 Single + _ 9 (0.1ml) + 10 + 11 + _ 12 B + _ 13 Double + Q 14 (0.01ml) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001MI) + 20 1 + _ Single- Strength Control. MPN Index: gth Broth � Double -Strength Broth: _;�2L Single- Strength Buffer Water: Index A •C Double - Strength Buffer Water: 10 X MPN Index/ 100ml I x { A-1 Broth Lot#: �j O 30 9�� MPN /g = Largest Volume x % Dry Solids I a Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. / MPN FECAL COLIFORM / GRAM l PERCENT SOLIDS FOR 'MPO T MPN DIAH WEIGHT & �V�"°I' ��➢ILL,1��: �. � �-_ GRAMS DISH I HT & DRY SOLIDS: � r 1 � 1 . ORAM$ �a'p"mp�L•'u",F���p,,:%3Jq"R`.,w..(L�7epfi.S,^�'�Jw'u•'Cr37I3�,7�J�i., � ,�+. � R tliNV��l1 i�GI��®U�a° �1�'71V:, :..�:,.,.:a'.�if�RII[1�2rS'i'•....,!''tCC:."�•,�ili:;?,x7:51:rJa.i;.:'�rtcL•::;cw:•'.��Y.s:Cct9L"al.'�,�:�.i .�•'^"S�:P:1 ..DISH MIGHT tic W r '86UDq DISH WEIMM WEIGH` Or WET SOLIDS . ."+'•M•+na•..w.w^^,n•.w+aa.,•.r+tMwsawv,giboy.++r�a:a.»....ww 7uv.www..m+.,aar�3vwn,�.�.»aadttkswe+w OSM,7cbb-nn.nrrvlt a ,w..r.,>cv-xm,c.yy.we vtsewum:.w".v.Na.0 „h`•,11• r.+a=,�u ia...0..an:„s§nc—.m, c_ `/� �DISH WOGS IT d. DRY COU DS ool DISH WEIGHT •m WEIGH°T O r�1 DRY SOLIDS ' iN:mrs�•e♦'pf,YWMruPe�'WR§W.tISLLYi§K•AI,iL':?'•.,ML•.6f0i.• .�PWfcY.f9w,-a1Vla,4�'N9JYA • . S Y,id�f.,glLb' a1lK:'"'n�'.amfnfNnt�rY,h=.Y.'Ou 1 f r > ® 3 ' % BOLIDS 11Ve{effr of bRY BOLIDS i®o o MIGHT OF WEI'SOTS FECAL COLIFORM - -MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: S Pry— c2 \J-7 Sample Date: (p -a 7- ('7 Dry Incubator Water Bath Sample Time: a 7 A v-- Time In Av, r ; Qi Sampler: g,, Time Out Test Date: Test Analyst: Tube# Broth Sample Confirmation Total Stren th Dilution Positive 1 U+, _ 2 A 3 Double _ , 4 ( 1ml) + _ 5 + 6 + _ 7 A + _ 8 Single + _ 9 (0.1 ml) + _ r1 10 + 11 + 12 B + _ 3 Double + _ 14 (0.01 ml) + 15 + 16 + _ 17 B + _ 18 Single + - 0 19 (0.001ml) + - 20 + _ Steritit Co trot: MPN Index: Single - Strength Broth: Double - Strength Broth: - 4,f Single - Strength Buffer Water: Index #: Double - Strength Buffer Water: -- a__ 10 X MPN Index/ 100ml rcx ( I A-1 Broth Lot#: 58 3 C�q MPN /g = Largest Volume x % Dry Solids l � yJ `l , Incubation Times: Dry Incubator: 3 hours Water Bath: 21 +1- 2 hrs. ✓ MPN FECAL COLIFORM 1 GRAM - I PERCENT SOLIDS FOR COMPOST MPN DISH wSlGHr. � 43RAMS ' DISH WEIGHT & WET SOLIDS: GRAMS DISCI WEIQHT A DRY SOLIDS: f '7 ' CRAMS , DISCI WFIGHT WET '196LIOS DISH WEIGHT WEIGHT OF W. ET SOLIDS �:veua.,;,vrno»,rn.adW+watamis .w•.�++..+r ' � `� ! W LPN^�� DISH WEIGHT & DRY SOLIDS DISCI WEIGHT WEIGHT OF DRY SOLIDS VOfSAlnCU .n.,�.�,•.-,:Lp.�,xr.W„�,,�,c.•ea,a3amr�.•:.n�.,o-�...-:--•s- •.��..�''".'.2°�' TIolgs % SOMDS = WEIGHT OF DFt'Y SOLIDS x 900 °e6 WEIGHT OF WET SOLIDS • 16 SOUDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: �l P����� 1-7 Sample Date: (Q - Dry Incubator Water Bath Sample Time: &N Time In l �; ,, Sampler: Time Out �,�:3�i ;� Test Date: I .7 Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive, 1 + 2 A + _ 3 Double + _ 4 (1 MI) + r8 5 + 6 + _ 7 A + _ Single + _ o 9 (0.1 ml) + _ 10 + 11 + 12 B + _ 13 Double +. _ Q 14 (0.01 ml) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001 ml) + 20 1 + _ Sterility Control_- MPN Index: Single- Strength Broth: g� Double- Strength Broth: _ Single - Strength Buffer Water: Index A Double - Strength Buffer Water: -, , 10 X MPN Index/ 100ml A-1 Broth Lot#: J< 3 Q 9'q 5� MPN /g Incubation Times: Largest Volume x % Dry Solids Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: / / ANALYST: , DISH WEIGHT: re). GRAMS DISH WEIGHT & WET SOLIDS: 3 C6_ GRAMS DISH WEIGHT & DRY SOLIDS: r a GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS of DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: SOLIDS = WEIGHT OF DRY SOLIDS % WEIGHT OF WET SOLIDS X 100 X 100% %SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION .(SM $221 C & E) Sample ID: S7PA Sample Date: '7 _a y_t 7 Dry Incubator Water Bath Sample Time: I Time In Sampler: (a . fNa LN z t.*G 7 ,,)Time Out Test-Date: o2 - (-7 Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive 1 + _ 2 A + _ 3 Double + _ 4 (1mI) + _ 5 + 6 + 7 A + _ 8 Single + _ 9 (0.1 ml) + _ 10 + 11 + 12 B + _ 13 Double + _ 14 (0.01 ml) + _ 15 + 16 + 17 B + _ 18 Single + _ 19 (0.001 ml) + _ 20 + _ mud Sterilit Con roll MPN Index) Single- Strength Broth: Double-Strength Broth- Single - Strength Buffer Water: Index #:. Double - Strength Buffer Water: 10 X MPN Index] 100ml A-1 Broth Lot#: J Q 3,4 ct cl �— MPN /g Largest Volume x % Dry Solids I x Incubation Times: � � 3 y" 7 Dry Incubator: 3 hours Water Bath: 21 +1- 2 hrs. d MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: / / r ANALYST: DISH WEIGHT: �c'� GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DRY SOLIDS: 13 •, a GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS = WEIGHT OF DRY SOLIDS X 100% WEIGHT OF WET SOLIDS �� X 100 % %SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: Sample Date: '7 - 0 y .l7 Dry Incubator Water Bath Sample Time: : �34a Time In :, fAl- : 13 Sampler: - ��;,.ram c�c , ti✓sc4�„M� Time Out �.� Test Date: c _ ( Test Analyst: Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + _ 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 + 7 A + _ 8 Single + _ 9 (0.1ml) + 10 +. s 11 + _ 12 B + _ 13 , Double + _ 14 (0.01ml) + 15 + _ 16 + _ 17 B + _ 18 Single + _ 19 (0.001 ml) + - 20 L + _ Ste .it Control: MPN Index: Single - Strength Broth: " Double- Strength Broth: _ Single- Strength Buffer Water: Index #: - Double - Strength Buffer Water. 10 X MPN Index/ 100m1 A-1 Broth Lo j ei�$- MPN /g t#: ay Largest Volume. x % Dry Solids t. x 3G-v 3(�a Incubation Times: ., Dry Incubator. 3 hours Water Bath: 21 +1- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: 7 /_ / ANALYST: DISH WEIGHT:. 7 GRAMS DISH WEIGHT & WET SOLIDS: � GRAMS DISH WEIGHT & DRY SOLIDS: GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: SOLIDS = WEIGHT OF DRY SOLIDS o WEIGHT OF WET SOLIDS X 100 X 100 % %SOLIDS 3 o FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: 17 Sample Date: '7 - 02 Dry Incubator Water Bath Sample Time: : S .- Time In ej: :►.I lyL Sampler: �ic,� � Time Out J� �io� Test Date: Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive 1 + 2 A + _ 3 Double + _ 4 (1 MI) + _ 5 + _ 6 + _ 7 A + _ 8 Single + _ 9 (0.1 ml) + 10 + 11 + _ 12 B + _ 13 Double + _ 14 (0.01MI) + 15 + 16 + 17 B + _ 18 Single + 19 (0.001 ml) + _ �J 20 + _ Sterility Control: MPN Index: Single- Strength Broth: Ix Double - Strength Broth: Single- Strength Buffer Water: Index A < Double - Strength Buffer Water. 10 X MPN Index/ 100ml A4 Broth Lot M ��) 3,Z)l TS- MPN /g OL ��l< Largest Volume x % Dry Solids t x ag rf Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: / ' cLE / ANALYST: . DISH WEIGHT: CCi GRAMS DISH WEIGHT & WET SOLIDS: 3&. GRAMS DISH WEIGHT & DRY SOLIDS: GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: SOLIDS = WEIGHT OF DRY SOLIDS X 100 WEIGHT OF WET SOLIDS 1�� X 100 % %SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: Sample Date: -J -n-7 Dry Incubator Water Bath Sample Time: ® ,q. ' Time In Sampler: (�4, t .,�;,v; Time out 0 Sa p n c Test Date: -7 _ _ 1 -7 Test Analyst: Tube# Broth Sample _ Total Strength Dilution Confirmation Positive 1 + _ 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 + _ r"7 A + 8 Single + 10 + 12 B + 13 Double + 14 (0.01 ml) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001ml) + _ 20 + _ _Stei&_tv Control., MPN Index: Single:- Strength Broth: Double- Strength Broth: - Single - Strength Buffer Water: Index A Double.- Strength Buffer Water: 10 X MPN Index-/ 100ml A-1 Broth Lot#: E6 3,a d MPN /g Largest Volume x % Dry Solids I 'x 31.Ll. Incubation Times: Dry Incubator. 3 hours Water.Bath: 21 +/- 2 hrs. / MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: / / ANALYST: Ci DISH WEIGHT: - GRAMS DISH WEIGHT & WET SOLIDS: J GRAMS DISH WEIGHT & DRY SOLIDS: I GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS 3 o? dE3t , 9 -1 DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: SOLIDS = WEIGHT OF DRY SOLIDS �( 100 % WEIGHT OF WET SOLIDS t , X 100 % %SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: Sample Date: 7 , _ l 7 Dry Incubator Water Bath Sample Time: Time In Sampler: _ ;,v-Z<v, Time Out Test Date: -7 - Test Analyst: Tube# Broth Sample Confirmation Total Stren th Dilution Positive 2 A + _ 3 Double + _ 4 1 ml + 5 + 6 + _ 7. A + _ 8 Single + _ 9 (0.1 ml) + 10 + 11 + 12 B + 13 Double + _ 14 (0.01 ml) + _ 15 +' 16 + 17 B + _ 18 Single + _ 19 (U01 ml) + _ 20 + _ Steri it Control: MPN Index d Single - Strength Broth: v Double - Strength Broth: a—" Single - Strength Buffer Water: Index #: -� Double - Strength Buffer Water. 10 X MPN Index/ 100ml f x < .4 A-1 Broth Lot#: 4.� MPN /g = _ Largest Volume x % Dry Solids -I ')(3 To-o 3 7 Incubation Times: Dry Incubator. 3 hours Water,Bath:- 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM '� PERCENT SOLIDS FOR COMPOST MPN DATE: / / 1 -7 ANALYST: _C6 DISH WEIGHT: off- GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DRY SOLIDS: _.L7-� GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS L e ( i / . 3 CALCULATIONS: SOLIDS = WEIGHT OF DRY SOLIDS WEIGHT OF WET SOLIDS X 100 o c X 100 % %SOLIDS J FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C. & E) Sample ID: Sample Date: (� ( � _ -7 Dry.Incubator Water Bath Sample Time: i o : Time In t ►:4 w Sampler: �- Time Out Test Date: Test Analyst: Tube# Broth Sample Total Stren th Dilution Confirmation Positive - + 2 A + 3 Double + _ 4 (1mi ) + _ 5 + 6 + _ 7 A + 8 Single + d 9 (0.1 ml) + _ 10 + 11 + - 12 B + 13 Double + _ 14 (0.01 MI) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001 mi) + _ 20 + Sterility Control.- MPN Index. a d Single- Strength Broth: 42L Double- Strength Broth: Single - Strength Buffer Water: Index #.• < Double - Strength'Buffer Water: 10 X MPN Index/ 100ml l F { A-1 Broth Lot#: S® 3�g� S MPN /g = - _ Largest Volume x % Dry Solids J 7<d-c- 1- a(- Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +1- 2 hrs. / 4 V MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: /� /�� / ANALYST: DISH WEIGHT: o�6 GRAMS DISH WEIGHT & WET SOLIDS: _�2 GRAMS DISH WEIGHT & DRY SOLIDS: _w�- GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT =. WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS = WEIGHT OF DRY SOLIDS j( 100 % WEIGHT OF WET SOLIDS �- X 100 % %SOLIDS FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: S F_r Sample Date: �`C� ( �; . ( � Dry Incubator Water Bath Sample Time: A-,,,` Time In L LI A,,,,- 1 0 LI LI 101Y, Sampler: err` Time Out :°�i �. - i t �;d/ ,,, Test Date: Test Analyst: QA Tube# Broth Sample Confirmation Total Strength Dilution Positive 1 + 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 + - 7 A + _ 8 Single + _ 9 (0.1 ml) + _ 10 + 11 + _ 12 B + _ 13 Double + _ 14 15 + 16 + _ 17 B + 18 Single + _ 19 (0.001MI) + - 20 + Sterfl—ftv Control., MPN Index: o. - (o Single= Strength Broth: Double Strength Broth: -- Single - Strength Buffer Water: Index.#. Double Strength Buffer Water: _ 10 X MPN Index/ 100ml I A-1 Broth Lot#:. ��4 ® � y MPN /g = r _ Largest Volume x % Dry Solids Incubation Times:' Dry Incubator. 3 hours Water Bath: 21 +!- 2 hrs. / MPN FECAL COLIFORM 1 GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: 1 / S4 / ANALYST: DISH WEIGHT:. GRAMS DISH WEIGHT & WET SOLIDS: 3 L4 • GRAMS DISH WEIGHT & DRY SOLIDS: GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS WEIGHT OF DRY SOLIDS X 100 % WEIGHT OF WET SOLIDS X 100% %SOLIDS [., � • i FECAL_COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: um_eweA r o�_Cy E`7 Sample Date: O 4 - f - Dry Incubator Water Bath• Sample Time: : ► i �,�,�, Time In Sampler: ^,-z Time out 44° 3 On Ic.-c Test Date: (c� - P ) _ 1'7 Test Analyst: Tube# Broth Sample Confirmation Total Stren th Dilution Positive. 1 + _ 2 A + _ 3 Double + _ 4 (1 MI) + _ 5 + 6 + _ 7 A + _ 8 Single + _ 9 (0.1 mi) + 10 + 11 + _ 12 B + _ 13 Double + _ 14 (0.01ml) + _ 15 + 16 + 17 B + _ 18 Single + _ 19 (0.001mi) + 20 + Sterility Control: MPN Index: c� - Single - Strength Broth: 0 Double'-Strength.Broth: Single - Strength Buffer Water: Index #: Double - Strength Buffer Water: 10 X MPN Index/ 100ml I� A*1 Broth Lot#: cl r/ram- MPN/g = 12- Largest Volume x % Dry Solids _ ` Incubation Times: 3�r� Dry Incubator. 3 hours Water Bath: 21 +I- 2 hrs. MPN FECAL COLIFORM / GRAM 3 PERCENT SOLIDS FOR COMPOST MPN DATE: A-Z / / ANALYST: DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: Q o-GRAMS DISH WEIGHT & DRY SOLIDS: _-GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS � (A CALCULATIONS: WEIGHT OF DRY SOLIDS SOLIDS = X 100 % • WEIGHT OF WET SOLIDS %SOLIDS � ` . X 100% .3 Q , FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: ,�,,,� Sample Date: -r Dry Incubator Water Bath. Sample Time: 9 : -, Time In Sampler. /L�Ns to Time out Test Date: Test Analyst: CA Tube# Broth Sample Confirmation Total Strength Dilution Positive 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 6 7 + _ 7 A + _ 3 Single + _ 9 (0.1ml) + _ 10 + 11 + 12 B + _ 13 Double + _ 14 (0.01 ml) + 15 + 16 + _ 17 B + _ 16 Single + - 19 (0.001 ml) + 20 + _ Sfed—Ift Co trol: MPN Index: Single- Strength Broth: Double- Strength Broth: C Single - Strength Buffer Water: Index #: Double - Strength Buffer Water. 10 X MPN Index/ 100ml I x < A-1 Broth Lot#: �Q 3 V 99,5 iVIPN /g = _ 02 Largest Volume x % Dry Solids Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. -- MPN FECAL COILIFORM f CRAM < PERCENT SOLIDS FOR COMPOST MPN DATE: ANALYST: CA DISH WEIGHT: cu GRAMS DISH WEIGHT & WET SOLIDS: _IRS, GRAMS DISH WEIGHT & DRY SOLIDS: 10 - GRAMS COMPUTATIONS: DISH WEIGHT &, WET SOLIDS - DISH WEIGHT — WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT WEIGHT OF DRY SOLIDS © � , e �. a- CALCULATIONS: WEIGHT OF DRY SOLIDS 100 SOLIDS = WEIGHT OF WET SOLIDS SOLIDS X 100 FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) _ j Sample ID: f A Sample Date: I a y _ ( ? I Dry Incubator Water Bath Sample Time: 1 � - Time In Sampler: r -2, &- Time Out. , `_ ,3 al AP �?: P Test Date: ( r 7 Test Analyst: QA Tube# Broth Sample Total Stren th Dilution Confirmation Positive 1 + _ 2 A + _ 3 Double + 4 (1 MI) + _ �J 5 + _ 6 + _ 7 A + _ 8 Single + _ 9 (0.1m1) + _ 10 + 11 - + _ 12 + _ 13 Double + _ 14 (0.01 ml) + _ 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001 ml) + _ Q 20 + _ Stedlit Control: MPN Index: ®3 - Single- Strength Broth: Double - Strength Broth: -, Single- Strength Buffer Water: _ Qr' Index A C �L Double - Strength Buffer Water. A-1 Broth Lot#: SO 3®cj s- MPN /g 10 X MPN Index/ 100m1 Largest Volume x % Dry Solids ( Or.s a Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. / MPN FECAL COLIFORM / CRAM l PERCENT SOLIDS FOR COMPOST MPN DATE:�,�. / / ANALYST: DISH WEIGHT: _ GRAMS DISH WEIGHT & WET SOLIDS: c'7. GRAMS DISH WEIGHT & DRY SOLIDS: - GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT - WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: . WEIGHT OF DRY SOLIDS �( 100 °Y SOLIDS = WEIGHT OF WET SOLIDS SOLIDS X 100% o C �v6-A7� FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: J=��1_ [ - �>26 17 i� ,A� Sample Date: 1-4 Dry incubator Water Bath. Sample Time: o °Sk ti Time In f 1 : 3 3 A a?: 33 R Sampler: t� �� , � 1 G- W.T-"" _X Time Out a 3 P . Test Date: Test Analyst: Tube# Broth Sample Total Strength Dilution Confirmation Positive 1 + _ 2 A + _ 3 Double + _ 4 (1 ml) + _ 5 + 6 + _ 7 A + _ .8 Single + _ 9 (0.1 ml) + _ 10 + 11 + _ 12 B + _ 13 Double + 14 (0.01 ml) + _ 15 + . 16 + _ 17 B + _ 18 Single + _ 19 (0.001 ml) + _ 20 + Sterility Control: MPN Index: Single- Strength Broth: _0 Double-Strength Broth: Single- Strength Buffer Water: -10— Index #' Double - Strength Buffer Water: �- 10 X MPN Index/ 100ml A-1 Broth Lot#: 63(37�7)4a MPN/g <av Largest Volume x % Dry Solids I Xc�?•zf Incubation Times: Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM 1 GRAM a PERCENT SOLIDS FOR COMPOST MPN DATE: oZ- / L / ANALYST: DISH WEIGHT: ` -r-- GRAMS DISH WEIGHT & WET SOLIDS: e�.'��• GRAMS DISH WEIGHT & DRY SOLIDS: l - d GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT - WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS �t - 7 3 CALCULATIONS: SOLIDS WEIGHT OF DRY SOLIDS X 100 WEIGHT OF WET SOLIDS %SOLIDS X 100% � `r. L�' ®2 3 a J FECAL COLIFORM - MULTIPLE TUBE FERMENTATION (SM 9221 C & E) Sample ID: r Ct -� Sample Date: /o2 - .S- [ -7 Dry Incubator Water Bath. Sample Time: . Time In ; ;a I Sampler. G -,,� ,. �, �r s Time out i a ; P. p,vj 9 ; 3 A. Test Date: I - _ 1 -7 Test Analyst: Tube## Broth Sample Confirmation Total Strength Dilution Positive + _ 2 A + _ 3 Double + _ 4 (1ml) + _ 5 + 7 A + - 8 Single + } 9 (0.1 ml) + _ I 10 + 11 + _ 12 B + _ 13 Double + 14 (0.01ml) + _ v 15 + 16 + _ 17 B + _ 18 Single + _ 19 (0.001 ml) + _ 20 + _ Sterility Control., MPN Index: _ Single- Strength Broth: _s Double - Strength Broth: Single- Strength Buffer Water: g Index #: Double - Strength Buffer Water: --,,i2r 10 X MPN Index/ 100ml x .� A-1 Broth Lot#: -5 d 3 c S MPN /g = _ _ Incubation Times: Largest Volume x % Dry Solids ..I x'a(�•d� -� Dry Incubator. 3 hours Water Bath: 21 +/- 2 hrs. MPN FECAL COLIFORM / GRAM PERCENT SOLIDS FOR COMPOST MPN DATE:�_ / � � ANALYST: . DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DRY SOLIDS: GRAMS COMPUTATIONS: DISH WEIGHT & WET SOLIDS - DISH WEIGHT - WEIGHT OF WET SOLIDS 3 7, Q DISH WEIGHT & DRY SOLIDS - DISH WEIGHT m WEIGHT OF DRY SOLIDS 3 � - CALCULATIONS: SOLIDS WEIGHT OF DRY SOLIDS x 100 % = WEIGHT OF WET SOLIDS V %SOLIDS COMPOST PAD TEMPERATURES WINDROW PAD # : �j 2-— 2 017 DATE BUILT: t)--9-7-w/7 DATE FINISHED TEMPING: h-d ki i DATE FRONT MIDDLE BACK INITIALS Lq sl sa 2 i 3 (- t G CA 4 5-1075 Z 6 1`ts '' �W `✓ 7La-,q� 4> Ai") -D^l� 8 1l ao Cc:' 10 (D Q 12 It/ 6� U Gs 15 16 17 18 19 20 21 .22 23 24 25 26 27 28 TEMPS COMPLETE (Y/N): FECAL MPN (PASS/FAIL): IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : A L-;__ -- -7 DATE BUILT: - ,� � -Z7 DATE FINISHED TEMPING: ( � ✓ �a DATE FRONT MIDDLE BACK INITIALS / 1 1 G � a V 4 CA 6 3t - Li 5 53 5 (0 cc 7 55 5q cc sSIR 9 10 11 - S 12 '�� 11►- la- ems" ,'� .� 15 16 17 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): FECAL MPN (PASS/FAIL): /A *' IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : jv o261- DATE BUILT: _ 4\- .T-- DATE FINISHED TEMPING: ► - DATE FRONT MIDDLE BACK INITIALS Lk CA 2 - L1� C,na 4 -a , ' V/ 5 3 o 6 7 fZZ�-2 6 8 - 3 7 r a-'- 9 0 � � su ! 10 to; iL 11 �_ t.o Ff 12 G - O 13 LO v. 15 16 17 18 19 20 21 22 . 23 24 25 26 27 28 � t�rAla TEMPS COMPLETE (YIN): . Y4��--5_ FECAL MPN (PASSIFAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD Ll DATE BUILT: - o -17 ✓ DATE FINISHED TEMPING: DATE FRONT MIDDLE BACK INITIALS 1 __,ll)- ✓ 5 3 ? 4 - i 3 c 5 4' 72- 71 5 i,;/ 7 1- 7 L=s 9 - f 0 6 y �✓ 10 4-7 5 6 11 (A- G 12 13 71 15 16 17 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): �� FECAL MPN (PASS/FAIL): S5`� " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : .nnn�+�►2 ,j o2(zs 1 "7 DATE BUILT: P-- DATE FINISHED TEMPING: I-7 DATE FRONT MIDDLE BACK INITIALS 1 - (a CA2 S-1171 C4 3 $` s ? 13 3 ��P,35 4 �` 6 T Sv cl 5 - - 73 7 2- 6 - Cv 3 (0 7 7 -`� % `� `�. cam' 9 - l Cos c 11 -73 12 — J G T J- CA 13 d Ca 1 61 ,7 Sd- 3 15 16 17 18 19 20 21 22 23 24 25 26 27 28 r` TEMPS COMPLETE (YIN): r�� FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : � ,,, _ l ✓ DATE BUILT: tip' 1. 17 DATE FINISHED TEMPING: DATE FRONT MIDDLE BACK INITIALS 2 - f 1 CR 3 -r _ -� - - 3 SAYS CA 5 -7— d" ( /Pn s 7 - r7 (0 — 10 - 12 -1, -I C' 13 '1 t ' 15 16 1.7 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): _ FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : �++�.roti`,rL - cl �j DATE BUILT: 7- 3 -- 1 ? DATE FINISHED TEMPING: - o2 3-1 -7 DATE FRONT MIDDLE BACK INITIALS U �- a 2 ~ 1 - - G7 a ✓ 3 - 1 CA 4 -- -7- 13 t�© Co G c. 3 �Ay; 5 ' W &9 Cy 55" Cr 6 - & c I C. f 7 -3 �, D- l AS' 8 ` 3 c4) 10 11 7-2-0 7 12 co 6- (a'7 13 t� 7 15 16 17 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): )eS FECAL MPN (PASS/FAIL): Nss �7^G�S 1-7 ' IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : &aawU- F— DATE BUILT: --TT- 1 - � DATE FINISHED TEMPING: ::Z - L) - ( 7 'm �C" DATE FRONT MIDDLE BACK INITIALS 2 CA 3 4 Z' 7 D 5 2-5 — L.r 6 - cl CA 7 -7 8 9 -ac G_ 10 11 '7 1 1; e�] it -7 12 ! i 5 13 15 16 17 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): 1 FECAL MPN (PASSIFAIL): R 5 �'^ I 11 '* IF PILE DOES NOT MEET THE TIME I TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : DATE BUILT: DATE FINISHED TEMPING: I ,/ DATE FRONT MIDDLE BACK INITIALS 1 C- V- 0 50 4�( 5L 2 (-o..I -IT si 411 5* 4 5 C3 —I� �v �c:y C�6 7 -a - / &v 8 AA-1-7 c. 9 -z� -17 z- 11 —c2p CA 12 13 - O 15 16 17 18 19 20 21 22 23 24 25 26 27 28 -7 TEMPS COMPLETE (YIN): �I� 5 FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : ..s �A-r.^rv- Co oZ d DATE BUILT: _ Ca - -7 - I DATE FINISHED TEMPING: DATE FRONT MIDDLE BACK INITIALS 1 � _1 ,� .> HE CIA 2 L rb `a' , 5 - 6 W Jr) C- L 10 -To 11 ( - ( -7 S 12 -a -! C ` k/ 13 15 16 17 18 19 20 21 .22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): 1 FECAL MPN {PASS/FAIL): S " ** IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : DATE BUILT: G _ j,2 r 7 DATE FINISHED TEMPING: Lp I DATE FRONT MIDDLE BACK INITIALS 1 G3 CA 2- Qf" 3 4 c� (oi 5 CA 6 9 - -1 �S 11 G-15•-11 G C ` O a2S 12 13 -1:1- -4- (d s !v•2 t� 164 4 15 16 17 18 19 20 21 .22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): FECAL MPN (PASS/FAIL): '* IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST ' PAD TEMPERATURES WINDROW PAD # : P NZ-Al t - cZ© -7 DATE BUILT: _ ,�- IT- (7 DATE FINISHED TEMPING: �,- - ) ✓ 40 DATE FRONT MIDDLE BACK INITIALS 1 - I q Jr-c)- 2 ` 2,� `' 3 d/u 4 a 5 r�3 t; T,7r/ cx 8 9 . 5 -17 Is C 6 <^3 5 10 5.. -2,% � " `9 6,3 2.5 ` AYS 12 - 3 C 13 _ n 15 G 7 (D C 16 17 18 19 20 21 22 23 24 25 26 27 28 b -'-t I TEMPS COMPLETE (YIN): E FECAL MPN (PASSIFAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES r WINDROW PAD# : p t„� C- ,�j - c2<i i -7 DATE BUILT: _ S-- /i- ['7 DATE FINISHED TEMPING: D t DATE FRONT MIDDLE BACK INITIALS 2 _7 3 �-AYS 3 �aL �? 4 L 6 60 o67 7 s -Z ; -7 8 -72 7 9 - 02 10 . L 13 &0 &q '7 6 t- 4 _ Gc2cak - 15 16 17 18 19 20 21 -22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): _ FECAL MPN (PASS/FAIL): (,C:h " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : -YPIA_Z f DATE BUILT. 3 - 3,4� - f� DATE FINISHED TEMPING: L) - ( o - 1 -7 �ll DATE FRONT MIDDLE BACK INITIALS 1 CA 2 5 C 3 `i - `5 ,� ✓ 4 4- ,5 bAY 5 5 L4d -7a f 7 Li C 6 s -- t 9 lo - lllp 13 104- (0r U 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): Y4i-5 FECAL MPN (PASS/FAIL): C� *` IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : S Pl! Z'f DATE BUILT: > -n ) - t L DATE FINISHED TEMPING: ''� - I ► - 1 - �0 DATE FRONT MIDDLE BACK INITIALS 1 3 2--3_ Ia L1 H L1 3 _3 1 .5 o ?/ ,f �j � 5 `-J- Z Csr S� LI Lt LJ G,Cl 69 — -5-1 9 .5 7 L 12 �-i'�1 F� O ©Ally 13 Q. 15 16 17 18 19 20 21 .22 23 24 25 26 27 . 28 TEMPS COMPLETE (YIN): 0 FECAL MPN (PASS/FAIL): 5 " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD DATE BUILT: _ 3- -zv►� DATE FINISHED TEMPING: - a2a ( -7 DATE FRONT MIDDLE BACK INITIALS 1 3"-o S b 6 I 5L 2 3-41; S 3 t _ a "p 7 4 7 ]Lc; —7 0 6 q Ls 1 CiO 7 3l lY" r, 7 C 5 L 8 - G3 10 :3 - 3 C 11 "3 --,,A 3 .1)-- 7( 3 12 (z -- -7-2 - 71 -70 15 16 17 18 19 20 21 .22 23 24 25 26 27 28 l 1 TEMPS COMPLETE (YIN): YEN FECAL MPN (PASSIFAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD It c�,1-\ DATE BUILT: 19- -1 DATE FINISHED TEMPING: V qll v DATE FRONT MIDDLE BACK INITIALS 5 j 4-1 % C`� Ic ` (2�5' 6 C --� $ , 1 -7 C 1102,3 cf 12 Q. cl IL {� 13 G 15 16 17 18 19 20 21 .22 23 24 25 26 27 28 TEMPS COMPLETE (YIN): 5 FECAL MPN (PASS/FAIL): �i 7�� ,�{ 7 IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES, RE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : i„ram: a - 0-Q 1 DATE BUILT: - G, - ( "7 DATE FINISHED TEMPING: DATE FRONT MIDDLE BACK INITIALS L _ 3 --) Z -- 0 � n, Ll" G, 7 — l- C 6 C� 8 - G cl Q! -- 10 - i 5S, GJ V- 11 1 61 CA 12 13 15 16 17 18' 19 20 21 22 23 24 25 26 27 28 TEMPS COMPLETE � F `' 17 (YIN): _� FECAL MPN (PASSIFAIL). 55�_ '= IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD# : F—AL,L- oZ6 lei DATE BUILT: 11 - ! Y- 6 e DATE FINISHED TEMPING: ( ?- cl 16 a DATE FRONT' MIDDLE BACK INITIALS to ; C� -- 5 —tn cel m. fa-(-Imo► � �i a ,. ' r J - 2 . -7, ja- - �Hco i �,�. G -7)TEMPS COMPLETE (YIN): _lam FECAL MPN (PASS/FAIL): ?A 55 c.�4 " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : FIA DATE BUILT: S H'?— Oo DATE FINISHED TEMPING: DATET FRONT MIDDLE BACK INITIALS ��z2—pIG v $C� C ✓ 4.0 S 3mY5 S — 1 CA to - r—Itio S�Ss C� 9- v ' L 1 1 t� S` • G S—J� • � �-- �`� Cn r71 TEMPS COMPLETE (YIN): FECAL MPN (PASSIFAIL): " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER,READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : '�..� -r��- J — a�t c 7 DATE BUILT. - '7 DATE FINISHED TEMPING: d - `7-r'7 y�0 DATE FRONT MIDDLE BACK INITIALS S' �t i . _ � ' �LJ 3o x S7 � � - � 5 5 6 � s� 60 5-9 2- /4- U, 1 - _d' I " TEMPS COMPLETE (YIN): . FECAL MPN (PASSIFAIL): ?ASS " IF PILE DOES NOT MEET THE TIME/TEMP.STANDARDS,CONTINUE ON SEPARATE TEMP.SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS