WQ0001953_Resiudals Annual Report 2020_20210218

2020
Town of Spindale
Wastewater Treatment Plant
2020 Annual Report
Land Application Program
Permit No. WQ0001953
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001953 County: Rutherford Year: 2020
Facility Name (as shown on permit): Town of Spindale
Land Application Operator: US Biosolids, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
A Yes C3 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit: 1 6
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 1 10.2
Total number of acres utilizes for land application during the year: 58.3
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
including but not limited to items 1-13 below) issued by the Division of Water Resources. R1 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .l I l I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (type or print)
Signature of Preparer*
if different from Permittee)
Preparer is defined in 40 CFR Part 503.9 (r) and
1 412 t
Date
Signature of Permittee Date
Signature of Land Atelier
9-$. 2p a
Date
if different from Permittee and Preparer)
15A NCAC 02T .1 102 (26) DENR FORM ACF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001953
Facility Name: Town of Spindale
Residual Source WQ # or
WQ0001953
NPDES #:
WWTP Name: Town of Spindale WWTP
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
Parameter
mg/kg)
Conc.
Limit
m k a
Sample or Composite Date
6-5-2020
Percent Solids (%) NA 0.38
Arsenic 75 25
Cadmium 85 " 25
Copper 4,300 131
Chromium NA 62.5
Lead 840 75
Mercury 57 3.83
Molybdenum 75 62.5
Nickel 420 62.5
Selenium 100 12
Zinc 7,500 313
Total Phosphorus NA 9330
TKN NA 129000
Ammonia -Nitrogen NA 31800
Nitrate and Nitrite NA 1700
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
211,1121
Date
Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0001953 Laboratory: 1)
Facility Name: Town of Spindale 2)
Residual Source
WQ0001953
3)
NPDES # or WQ#: 4)
WWTP Name: Town of Spindale WWTP 5)
Residual Analvsis Data
Waypoint Analytical
Sample or Composite Date
Parameter
mg/kg)
6-5-2020
Organic N 97000
pH 6:3
Aluminum 6230
Calcium 12500
Iron 9730
Magnesium 17000
Maganese 255
Poatassium 6250
Sodium 23500
Sulfur 2950
PAN 46760
SAR 3.29
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
i6/L /
Date
DENR FORM RSSF - B (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 2.05
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used: 15.1 Acres Permitted: 15.1 Site #: M Field #: I
Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg. %, Solids use Raw Percent ffl:
Sample of
Com-
posite
Date
1
6/5/20
2 3 4 5 6 7 8 9 10 11 12
Solids 0.38
Arsenic 25
Cadmiuml 25
Copper 131
Chromium 62.5
Lead 75
Mercury 3.83
Molyb-
denum
62.5
Nickel 62.5
Selenium 12
Zinc 313
Total
Phos-
horns
9330
Annual Heavy Metal Meld Loadines (Calculated in Ibs/acre):
Event 1
1 11 1 111 1 111 1 111 1 111 1 111 1 tll 1 111 1 111 1 111 1 111 1 111 1 11
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 1 •
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1
1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1: 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1
rotal
1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111
1 ceruly, unuer penalty of jaw, tnat tnis document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applter
a-J jo-%,
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale
Land Owner: John McFadden
Operator: John McFadden
Crop 1 Name: Fescue
WQ Permit #: WQ0001953 Field #: M1
Annual Dry Tons Applied: 2.0600 Site #: M1
Predominant Soil Series: PaC2
Crop 1 Max. PAN: 158 Crop 2 Name:
Acres Utilized: 15.1
Acres Permitted: 15.1
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
I
c
Volume appliedPP
enter one) Solids/
Liquid9
Cu. Yds Gallons
Solids
Volume
Applied per
Acre
Dry TonslAc)
Residual Sources
NPDES #. WQ#.
Fert.. Animal
Waste. etc)
Soil
Cond.
Dry'
Moit. st)
Precip.
Past 24
Hrs.
nches
D
K - a
c Fa _
o
N'
R
K
N
TKN
mg/kg
z D
q
73
3 '
mg/kg
Nitrate
and
Nitrite
mg/kg
Ibs/acre )
Name of Crop Type
Receiving Residual
Application
Crop 1 Crop 2 Crop 1 Crop 2
4-2020 130000 0.38 0.136 WQ0001953 dry 0 s 0.5 0.3 129000 31800 1700 12.758 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
101 A LSI 01 130000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 12.758 0.000 Lime Applied
Annuallbs/acre 0.007 0.007 0.036 0.017 0.020 0.001 0.017 0.017 0.003 0.085 2.538 1 Date lbs/ac
Prior Years Cumulative lbs/ac 0.054 0.047 21.504 2.665 0.962 0.027 0.137 3.004 0.566 22.76 12-20 1000
Current Cumulative lbs/ac 0.061 0.054 21.540 2.682 0.982 0.028 0.154 3.021 0.569 22.845
Permitted C. P. L. R.**** 36 1 34 1338 1 NA 1 267 15 1 NA 1 374 1 89 1 2498
Permit PAN Limit 1st/2nd Crop F 158
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
1. B-
Date
Application Method: S - Surface, IN - Injection, INC - Incorporation
Z'1 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale
WQ0001953
John McFadden Owner:
15.5 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
John McFadden Predominant Soil Series:
15.5 Site #: M Field #:
2.17
PaC2
3
Residual Analysis Data (lieavv Metals and Total Phosnhorus use mg/kg- "/a Solids use Raw Percent til-
Sample or
Com-
posite
Date 6/5/20
2 ( J..31 4,' S 6 7 ' 8
v v
9. 10 ' 11 12
Solids 0.38
Arsenic 25
Cadmium 25
Copper 131
ChrorniLlrnj 62.5
Lead 75
Mercury 3.83
Molyb-
denum
62.5
Nickel 62.5
Selenium 12
Zinc 313
Total
Phos-
horns
9330
wuuual rteavy ivietai r lclu L,oaatn2s 1l.aicuiatea In Ins/aerel:
p•
Event
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 '
1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 1
1 1 : 1 111 1 111 1 111 1 111 1 Ilt 1 111 1 111 1 111 1 111 1 111 1 111 1 1
1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11
1 1:: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1::
otal
Phos- 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111
y, uuucl [,cushy 01 iaw, uiat tuts uocument was prepares under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale
Land Owner: John McFadden
Operator: John McFadden
Crop 1 Name: Fescue
WQ Permit #: WQ0001953 Field #: M3
Annual Dry Tons Applied: 2.1630 Site #: M3
Predominant Soil Series: PaC2
Crop 1 Max. PAN: 158 Crop 2 Name:
Acres Utilized: 15.5
Acres Permitted: 15.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o L
p
Volume applied
enter one) Solids/
Liquid
Cu. Yds Gallons
Solids
Volume
Applied per
Acre
Dry Tons/Ac)
Residual Sources
NPDES #, WQ#.
Fert.. Animal
Waste, etc)
Soi1
Cond.
Dry,
Wet.
Moist)
Precip.
Past 24
Hrs.
inches
D
3: -0
C, '0
0 ?
c
N
TKN
mg/kg
z D
3 •
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1 Crop 2 Crop 1 Crop 2
4-2020 136500 0.38 0.140 W00001953 dry 0 s 0.5 0.3 129000 31800 1700 13.050 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
71 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 01 1365001 As Cd Cu Cr Pb Fig Mo Ni Se Zn P 13.050 0.000 Lime Applied
Annuallbs/acre 0.007 0.007 0.037 0.018 0.021 0.001 0.018 0.018 0.003 0.088 2.612 Date I lbs/ac
Prior Years Cumulative lbs/ac 0.061 0.054 21.54 2.682 0.982 0.028 0.154 3.021 0.569 22.845 12-20 1000
Current Cumulative Ibs/ac 0.068 0.061 21.577 2.700 1.003 0.029 0.172 3.039 0.572 22.933
Permitted C. P. L. R.**** 36 1 34 1338 1 NA 1 267 1 15 1 NA 1 374 1 89 1 2498
Permit PAN Limit 1 st/2nd Crop 158
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
2-A.
Date
Application Method: S - Surface, IN - Injection, INC - Incorporation
ak **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual):
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 17.1 Acres Permitted: 17.1 Site #: M Field #:
3.71
PaC2
4
Residual Analvsis Data (Heavv Metals and Total Phosnhorus use mg/kg. o % Solids use Raw Percent #L•
Sample or
Com-
posite
Date 6/5/20
2 3 4 i J. 6 7 8 9 10 11 . 12
Solids 0.38
Arsenic 25
Cadmium 25
Copper 131
Chromium 62.5
Lead 75
Mercury 3.83
Molyb-
denum
62.5
Nickel 62.5
Selenium 12
Zinc 313
Total
Phos-
horus
9330
Annual neavy tv etal rieta Loaaines lUalculated in lbs/acrel:
Total 1 L21 3 4 5 L6, L7J L81 9 10 11 12
DT/Ac./ c
App. a
Event 0.22
Arsenic 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
Cadmiuml 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
Copper 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057
Chromium 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Lead 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb-
denum
0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Nickel 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Selenium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Zinc 0:136 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.136
Total
Phos- 4.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.049
horus
y, U11UU1 Nc1141Ly U, law, tHat uus uocumen[ was preparea unaer my airection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1 I---
Signature of Land Applier
a4?01
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale
Land Owner: John McFadden
Operator: John McFadden
Crop 1 Name: Fescue
WQ Permit #: WQ0001953 Field #: M4
Annual Dry Tons Applied: 3.7080 Site #: M4
Predominant Soil Series: PaC2
Crop 1 Max. PAN: 158 Crop 2 Name:
Acres Utilized: 17.1
Acres Permitted: 17.1
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p
p
Volume applied
enter one) Solids/
Liquid
Cu. Yds Gallons
o
Solids
Volume
Applied per
Acre
DryTons/Ac)
Residual Sources
NPDES #, WQ#.
Fert.. Animal
Waste, etc)
Soil
Cond.
Dn.
Moist)
Precip.
Past 24
Hrs.
ncnes
D
3 -
a
o P
a -
C N'
iv
0
TKN
mg/kg
z D
S
rM o
a w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre)
Name of Crop Type
Receiving Residua'.
Application
Crop 1 Crop 2 Crop 1 Crop 2
3-2020 156000 0.38 0.145 W00001953 dry 0 s 0.5 0.3 129000 31800 1700 13.519 NA Fescue
4-2020 78000 0.38 0.072 W00001953 dry 0 s 0.5 0.3 129000 31800 1700 6.760 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 01 234000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.279 0,wo Lime A lied
Annual lbs/acre 0.011 0.011 0.057 0.027 0.033 0.002 0.027 0.027 0.005 0.136 4.049 Date lbs/ac
Prior Years Cumulative lbs/ac 0.047 0.037 15.469 1.929 0.754 0.018 0.099 1.968 0.469 18.362 12-20 1000
Current Cumulative lbs/ac 0.058 0.048 15.526 1.956 0.787 0.020 0.126 1.995 0.474 18.498
Permitted C. P. L. R.**** 36 34 1338 NA 267 15 NA 374 89 2498
Permit PAN Limit Ist/2nd Crop I 158
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
N
Signature of Land Applier
I•Jl.30
Date
Application Method: S - Surface, IN - Injection, INC - Incorporation
Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of SDindale
WQ0001953
John McFadden Owner:
10.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
John McFadden Predominant Soil Series:
10.6 Site #: M Field #:
2.27
CaB2
5
Residual Analvsis Data (Heavv Metals and Total Phosphorus use m0kE, % Solids use Raw Percent #):
Sample or:.._1_
Com-
posite
Date 6/5/20
2; 3 4 5 6 7.1 8 9. 10 1 11 12
Solids 0.38
Arsenic 25
Cadmium 25
Copper 131
Chromium 62.5
Lead 75
Mercury 3.83
Molyb-
denum
62.5
Nickel 62.5
Selenium 12
Zinc 313
Total
Phos-
phorus
9330
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 3 4; 5 6 7j 8 9 10 11'; 12i
H
DT/Ac./ c
App.
Event 0.21
Arsenic 1 0.011 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.011
Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
Copper 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
Chromium 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Lead 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb-
0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
denum
Nickel 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027
Selenium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Zinc 0.134 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.134
Total
Phos- 3.993 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.993
horus
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land App ier Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale WQ Permit #: WQ0001953 Field #: M5 Acres Utilized: 10.6
Land Owner: John McFadden Annual Dry Tons Applied: 2.2660 Site #: M5 Acres Permitted: 10.6
Operator: John McFadden. Predominant Soil Series: CaB2 Cation Exchange Capacity (non 503):
I'-- 1 Na,.,n• PPQrIla Crnn t Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
Volume applied Volume Residual Sources
Soil
Precip. D c
Z Y
5 Nitrate
PAN Applied
Name of Crop Type
Y enter one) Solids/ Applied per NPDES #, WQ#,
Cond. Past 24 TKN ao o and
Ibs/acre)
Receiving Residual
o Liquidq Solids Acre Fert., Animal
Dry, Hrs. 0
o m N
ry '
c Nitritec'd
Application
Cu. Yds Gallons Dry TcnslAc)
Waste, etc)
Wet.
Moist) inches
o z
0 3 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
4-2020 143000 0.38 0.214 WQ0001953 dry 0 s 0.5 0.3 129000 31800 1700 19.992 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 1 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS1 01 1430001 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 19.992 0.000 Lime Applied
Annuallbs/acre 0.011 0.011 0.056 0.027 0.032 0.002 0.027 0.027 0.005 0.134 3.993 Date lbs/ac
Prior Years Cumulative lbs/ac 0.064 0.05 1 21.773 2.711 1.055 0.025 0.139 2.789 0.259 25.642 12-20 1000
Current Cumulative lbs/ac 0.075 0.061 21.829 2.738 1.087 0.027 0.166 2.816 0.264 25.776
Permitted C. P. L. R.**** 36 34 1338 NA 267 15 NA 3741 89 2498
Permit PAN Limit 1 st/2nd Crop 209
I certify, under penalty of law, that this document was prepared under my direction or supervision in accoruaDCC wit„ a syMC111 UV51g==CU lV aaau= ===a=
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Application Method: S - Surface, IN - Injection, INC - Incorporation
9211 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
ignature of Land Applier Date ***
Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale WQ Permit Number:
WWTP Name: Town of Spindale WWTP NPDES Number:
Monitoring Period: From 1/1/2020 To 12/31/2020
WQ0001953
NCO020664
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time,/temp) Alt B (Alk Treatment) F Alt. C (Prior Testing)l
A1t.D (No Prior Test) p Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost LIT Heat Drying Heat Treatment Thermophilic
Beta Ray Ll Garnm!E2L2 Pasteurization Ll
Class B: jAlt. (1) Fecal Density Yj Alt. (2) Process to Significantly Reduce Pathogens 1
If applicable to alternative performed (glass B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization C: AirDrying CompostingR Aerobic Digestion El Anaerobic
Digestior. Q If
applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter
Allowable
Level in
Sludge Pathogen
Density Number ot Excee-
encesY
Frequency
of
Analysis Sample
Type
Analytical
Tech -
nioue
MinimuGeo. Mean Maximum Units Fecal
Coliform 2
x 10 to the 6th
power per
gram of total
solids MPN
7692 8195 8696 MPN/g 0 7 grab sm9221 CFU
1000
mpn per gram of
total solid (dry weight)
Salmonella
bacteria in
lieu of fecal coliform)
3
MPN per 4 grams total
solid (dry weight)
Vector
Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.
I (VS reduction) 0 Alt. 2 (40-day bench) Alt. 3 (30-day bench) 2) jAlt. 4 (Spec. OZ uptake) J Alt.
5 (14-Day Aerobic) CI Alt. 6 (Alk. Stabilization Alt 7 (Drying - Stable) Q 1 Alt. 8 (Drying - Unstable) Alt.
9 (Injection) LI Alt. 10 (Incorporation) p No vector attraction reduction alternatives were performed 11 CERTIFICATION
STATEMENT (please check the appropriate statement) 21 "
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector
attraction reduction requirement in 15A NCAC 02T .1107 have been met." Li "
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector
attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the requirements.)
This
determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that
the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment." 6 ,. &
e.n„ or © A L Dennis Key US Biosolids, Inc. Preparer
Name and Title (type or print) land Applier Name and Title (if applicable)(type or print) 1••
01 Signature
of Preparer* Date Signa ure of Land Applier (if applicable) Date Preparer
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR
FORM PVRF 02T (12/2006)
Waypoint,
ANALYTICAL
i 46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-155-0004
Lab No: 72556
Sample ID : Spindale
Test
Moisture
Test
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytical.com
Project Spindale
Information :
REPORT Of ANAL YSIS
Results Units
99.6
Results Units
MOL
0.010
MOL
Report Date: 06/11/2020
Received : 06/03/2020
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 6/ 1 / 2020 10:00
DF Date / Time By Analytical
Analyzed Method
1 06/05/2016:47 FMM SM-2540G
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 31800 mg/Kg - dry 62SO 1 06/10/20 14:00 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 1700 mg/Kg - dry 1210 1 06/09/20 15:40 ZBD 4SOONO3F-2011
Organic N 97000 mg/Kg - dry 62500 1 06/10/20 10:00 CALCULATION
pH 6.3 S.U. 1 06/09/20 05:20 JSL 9045D
Total Solids 0.380 0.010 1 06/05/20 16:47 FMM SM-2540G
Total Kjeldahl Nitrogen 129000 mg/Kg - dry 62500 1 06/10/20 10:00 PI M-4500-NH3C-TKF
Phosphorus 9330 mg/Kg - dry 1250 1 06/09/20 22:09 KKM 60100
Aluminum 6230 mg/Kg - dry 1250 1 06/09/20 22:09 KKM 6010D
Arsenic 25 mg/Kg - dry 125 1 06/09/20 22:09 KKM 6010D
Calcium 12500 mg/Kg - dry 12500 1 06/09/20 22:09 KKM 6010D
Cadmium 2S.0 mg/Kg - dry 25.0 1 06/09/20 22:09 KKM 6010D
Chromium 62.5 mg/Kg - dry 62.5 1 06/09/20 22:09 KKM 6010D
Copper 131 mg/Kg - dry 12S 1 06/09/20 22:09 KKM 6010D
Iron 9730 mg/Kg - dry 2500 1 06/09/20 22:09 KKM 6010D
Lead 75.0 mg/Kg - dry 75.0 1 06/09/20 22:09 KKM 6010D
Magnesium 1700 mg/Kg - dry 12SO 1 06/09/20 22:09 KKM 6010D
Manganese 255 mg/Kg - dry 125 1 06/09/20 22:09 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions
M LQ Method Quantitation Limit
Page 3 cf 6
Waypointo
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-155-0004
Lab No : 72556
Sample ID : Spindale
Test
Project Spindale
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 1 Fax [phone]
www.waypointanalytical.com
REPORT Of ANAL YSIS
Results Units MOL
Report Date : 06/11/2020
Received : 06/03/2020
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 6/ 1/2020 10:00
DF Date 1 Time By Analytical
Analyzed Method
Mercury 3.83 mg/Kg - dry 3.83 1 06/09/20 11:59 DD8 SW-7471B
Molybdenum 62.S mq/Kg - dry 62.5 1 06/09/20 22:09 KKM 6010D
Nickel 62.5 mg/Kg - dry 62.5 1 06/09/20 22:09 KKM 6010D
Potassium 6250 mg/Kg - dry 2500 1 06/09/20 22:09 KKM 6010D
Selenium 12 mg/Kg - dry 12S 1 06/09/20 22:09 KKM 6010D
Sodium 23500 mg/Kg - dry 6250 1 06/09/20 22:09 KKM 6010D
Zinc 313 mg/Kg - dry 313 1 06/09/20 22:09 KKM 60100
Sulfur 2950 mg/Kg -dry 2500 1 06/09/20 2.2:09 KKM 60100
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantization Limit
L Limit Exceeded
Page 4 of 6
SAR
Sodium Absorption Ratio
Na : Sodium (Mg/L) Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L / Equivalent weight
Na M /L Ca(M /L) M M /L
89.3 1 47.5 1 6.46
Na..._(ME) I Ca,.„WEI I M.g,..(ME.),
3.8826091 2.375 10.538333
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 3.216944 (From Mg/L entered above)
SAR= 3.296102 (From ME entered below)
Na (ME) Ca (ME) Mg (ME)
3.9 1 2.3 1 0.5
The amour
amount of E
Permitting
PAN
Mineralization as decimal Total dry
tons/year
Acres
Applied onRate
0.3 1 TKN
129000
NH3
31800
NO3
1700
NO210
Solids
0.0038
PAN Surface
46760 mg/kg 93.52 lbs/dry ton
0 Ibs total PAN
DIV/0! jibs PAN/acre
PAN Injection
62660 mg/kgmg/kg 125.32 lbs/dry ton 0
1 lbs total PAN DIV/
0! jibs PAN/acre Dry
Tons/1000 gal. 0.
015846 1st
year PAN Surface
lbs. 0
1st
year PAN Injected
lbs. 0
lbs./
acre Surface
DIV/
0! lbs./
acre Injected
DIV/
0! MR(
TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg mg/
kg x .002 =Ibs/dry ton MR(
TKN-NH3) + l(NH3)+NO3+NO2 mg/
kg x .002 mg/
kg Ibs/
dry ton 1000
X 8.34 X %solids X sp. gravity "=dry tons/1000gal." 2000
Analytical Results'
U.S. Biosolids Inc 4K
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/24/2020
Reported: 04/30/2020
For: Spindale
Comments:
Sample Number Parameter Sample ID Result
200324-25-01 2 30 Day Benchscale Spindale <1
Unit Method Analyzed Analyst
ova EPA625-R.92JLI 03/24/2020 WC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 38
30 Day Bench Worksheet
WEEK 1
Sample ID #2 (A. 225
Samples TotatSpIld]s Volatile Solids Volatile Fraction
12 i tQ35 I
Avera e• 2 401
WEEK 2
Samples Total Solids Volatile Solids Volatile Fraction
1 n. rag 0. 30 D. 5 `7
2 1. 06 1J
3 O. I p
Average: 0-161 0.42 7 V
WEEK 3
Samples Total Solids Volatile Solids Volatile Fraction
1 2 0 - 2-2 2
2 3 l
3 Q
Average: 3 i 7 q
WEEK 4
Samples I atile Solids Volatile Fraction
1 1 2
2 WO-320-M 6i33i r. 261 Average:
11 0.1% 0 . 153q p WEEK
5 Samples
I Total Solids Volatile Solids Volatile Fraction I
C. 27 0.14 0-51S6 2
0.26 1 --- 3
Q 2 3 Average:
3 5 WEEK
6 Samples
I Total Sq-
7olatile
Solids Volatile Fraction 1
I. 5"T 2
G. O. 1 S 6 3
2- 1 Average:
2 p• 5 7 Van
Kleeck Reduction: Initial % Vol. Frac. - Final % Vol. Frac. X 100 = % Initial %
Vol. Frac. — ( Initial % Vol. Frac. X Final % Vol. Frac.) FINAL
RESULT ( % 1
Client: US u S u L c -.
STATFSYIIA-F
ANALYI ICAL
122 Court Strout • P.
O. Box 229
Address: Q c '
r
Smicsvillc, NC 29697
7041872-4697
Chain of
Custody Record
Contact Person:
t
Phone N 336 )w 089 FAXN
PO It Requisitioned by: lT1me Dale)
Customer - --
SampleIDM
Lah ID a
Time Sampled
Grob Only)
Dale Sampled7
Grob Onty) T I
Matrix
x rvW
hrunclrn mueare i for arolyxi.
Relinquished by:
Il
Received by -
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date
Time end____ am, pm Date _ / -j_
Composite Sampling .
Time begin am, pm Date
Time end am, pm Date
Time 1- / 5 am, (/ D Date LJ u Sampled by: %r/r
Time IQ amDate 70 Transported
by: Time
am, pm Date //_ Holding times met: Time
am, pm Date _ / —/_ Compliance
work: Non-
compliance work: Lab
Comments _T SamplesTransported On Ice _ Inilials.
r\
rn
CO
CO
N
p N00
0
m O '
O a
r`
00
00
N
U
Z
11i
aJ
V)
00
N
N
X
O
co
0
a
ce*al ical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Swte 100
Huntersville. NC 28078
1704)875-9092
Project: US. Bio. Spindale
Pace Project No.: 92470995
ANALYTICAL RESULTS
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12:45 Received: 03/25/20 11:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Comments: • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311, 03/28/20 15:06 Initial pH: 6.98; Final pH: 4.96
Pace National - Mt. Juliet
2,4,5-TP (Silvex)
2,4-D
ND ni 0.00200 1 03/31/20 21:16 04/02/20 01:47 93-72-1
Surrogates
ND ni 0.00200 1 03/31/20 21:16 04/02/20 01:47 94-75-7
2,4-DCAA (S) 89.8 % 14.0-158 1 03/31/20 21:16 04/02/20 01:47 19719-28-9
8081 TCLP Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311: 03/26/20 16:12
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
Chlordane (Technical)
NO ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 58-89-9
Endrin
NO ug/L 3.0 1 03/30/20 17:06 04/01/20 17:21 57-74-9
Heptachlor
ND ug/L 0.50 1 03/30/20 17:06 04/0112017:21 72-20-8
Heptachlor epoxide
NO ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 76-44-8
Methoxychlor
ND ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 1024-57-3
Toxaphene
ND ug/L 1000 1 03/30/20 17:06 04101/2017:21 72-43-5
Surrogates
NO ug/L 3.0 1 03/30/20 17:06 04/01/20 17:21 8001-35-2
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
78 % 10-138 1 03/30/20 17:06 04/01/20 17:21 2051-24-3
86 % 10-110 1 03/30/20 17:06 04/01/20 17:21 877-09-8
8082 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 03/26/20 16:12
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 12674-11-2PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
NO ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11104-28-2
PCB-1242 (Aroclor 1242)
ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11141-16-5
PCB-1248 (Aroclor 1248)
NO ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 53469-21-9
PCB-1254 (Aroclor 1254)
NO ug/L 1000 1
ND
03/30/20 17:41 04/01/20 00:25 12672-29-6
PCB-1260 (Aroclor 1260)
ug/L 1000 1
NO
03/30/20 17:41 04/01/20 00:25 11097-69-1
Surrogates ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11096-82-5
Decachlorobiphenyl(S) 91 % 10-132 1 03/30/20 17:41 04/0112000:25 2051-24-3
6010 MET ICP, TCLP Analytical Method. EPA 601OD Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/05/20 1629 Initial pH: 7.79; Final pH: 4.5
Pace Analytical Services - Asheville
Arsenic
Barium
NO ni 0.050 1 04/06/20 12:15 04/07/20 02:52 7440-38-2
Cadmium
ND ri 0.25 1 04/06/20 12:15 04/07/20 02:52 7440-39-3
Chromium
NO ni 0.0050 1 04/06/20 12:15 04/07/20 02:52 744043-9
Lead
NO mg/L 0.050 1 04/06/20 1215 04/07/20 02:52 7440-47-3
Selenium
NO ni 0.025 1 04/06/20 12:15 04/07/20 02:52 7439-92-1
Silver
NO mg/L 0.10 1 04/06/20 12:15 04/07/20 02:52 7782-49-2
NO mg/L 0,025 1 04/06/20 1215 04/07/20 02:52 7440-22-4
REPORT OF LABORATORY ANALYSIS
Date: 04/07/2020 04:48 PM
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28
PO Box 228 e Statesville, NC 28687 e 704/872/4697
Page 15 of 38
xo2aceAnal ical
www.pacalabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
704)875-9092
Project: US. Bio. Spindale
Pace Project No.: 92470995
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12:45 Received: 03/25/20 11:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No Qual
7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311, 04/05/20 16:29 Initial pH: 7.79:: Final pH: 4.5
Pace Analytical Services - Asheville
Mercury NO mg/L 0.00020 1 04107/2010:46 04/0712014:07 7439-97-6
8270E TCLP RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
1.4-Dichlorobenzene NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 106-46-7
2,4-Dinitrotoluene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 121-14-2
Hexachloro- 1, 3-butadiene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 87-68-3
Hexachlorobenzene NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 118-74-1
Hexachloroethane NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 67-72-1
2-Methylphenol(o-Cresol) NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 9548-7
3&4-Methylphenol(m&p Cresol) NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 15831-10-4
Nitrobenzene NO ug/L 50.0 1 03130/2020:50 03131/2017:10 98-95-3
Pentachlorophenol NO ug/L 100 1 03130/2020:50 03131/2017:10 87-86-5
Pyridine NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 110-86-1
2,4,5-Trichlorophenol NO ug/L 50.0 1 03/30/20 20:50 03131/2017:10 95-954
2,4.6-Trichlorophenol NO ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 88-06-2
Surrogates
Nitrobenzene-d5 (S) 65 12-102 1 03/30/20 20:50 03/31/20 17:10 4165-60-0
2-Fluorobiphenyl (S) 58 13-107 1 03/30/20 20:50 03/31/20 17:10 321-60-8
Terphenyl-d14 (S) 80 21-132 1 03/30/20 20:50 03/31/20 17:10 1718-51-0
Phenol-d6 (S) 30 10-110 1 03/30/20 20:50 03/31/20 17:10 13127-88-3
2-Fluorophenal (S) 20 10-110 1 03/30/20 20:50 03/31/20 17:10 367-12-4
2,4,6-Tribromophenol(S) 33 27-108 1 03/30/20 20:50 03/31/20 17:10 118-79-6
8260D MSV TCLP Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Benzene NO ug/L 100 20 04/04/20 08:20 71-43-2
2-Butanone (MEK) NO ug/L 200 20 04/04/20 0820 78-93-3
Carbon tetrachloride NO ug/L 100 20 04/04/20 08 20 56-23-5
Chlorobenzene NO ug/L 100 20 04/04/20 08:20 108-90-7
Chloroform NO ug/L 100 20 04/04/20 08:20 67-66-3
1.4-Dichlorobenzene NO ug/L 100 20 04/04/20 08:20 106-46-7
1.2-Dlchloroethane NO ug/L 100 20 04/04/20 08:20 107-06-2
1.1-Dichloroethene NO ug/L 100 20 04/04/20 08:20 75-35-4
Tetrachloroethene NO ug/L 100 20 04/04/20 08.20 127-18-4
Trichloroethene NO ug/L 100 20 04/04/20 08:20 79-01-6
Vinyl chloride NO ug/L 100 20 04/04/20 08:20 75-01-4
Surrogates
1,2-Dichloroethane-d4 (S) 99 70-130 20 04/04/20 08:20 17060-07-0
Toluene-d8 (S) 105 67-135 20 04/04/20 08:20 2037-26-5
4-BromoOuorobenzene (S) 97 70-130 20 04/04/20 08:20 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 04/07/2020 04:48 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 16 of 38
Pace Analytical Services, LLC
9800 Kincey Ave. Swte 100
ce Analyti l Hunterswlle. NC 28078
Clli li
www. paceelabsl.coolm [phone]
ANALYTICAL RESULTS
Project: US. Bid. Spindale
Pace Protect No.. 92470995
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12 45 Received 03/25/20 11 32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 99.6 % 0.10 1 04/01/20 16:15
1010 Flashpoint,Closed Cup Analytical Method: EPA 1010A
Pace Analytical Services - Asheville
Flashpoint 200 deg F 70.0 1 04106/20 15:09
9045 pH Soil Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C 7.3 Std. Units 0.10 1 04/06/20 14:04 H3
9095 Paint Filter Liquid Test Analytical Method: EPA 90958
Pace Analytical Services - Asheville
Free Liquids Fail 1.0 1 03/27/20 18A0
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide. Reactive ND mg/kg 248 1 03/30/20 15.18 03/30/20 15:50
734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive NO mg/kg 2480 1 03/30/20 15:18 03/30/20 15:23
Sample: 200324.25.01 Lab ID: 92470995002 Collected. 03/24/20 12:45 Received: 03/25/20 11:32 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016) NO ug/L 1.0 1 03/31/20 15:55 04/0212020:28 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11104-28-2
PCB-1232 (Aroclor 1232) NO ugiL 1.0 1 03/31/20 15:55 04/02/20 20:28 11141-16-5
PCB-1242 (Aroclor 1242) NO ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 53469-21-9
PCB-1248 (Aroclor 1248) NO ug/L 1.0 1 03/31/20 15:55 04/02/20 2028 12672-29-6
PCB-1254 (Aroclor 1254) NO ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11097-69-1
PCB-1260 (Aroclor 1260) NO ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11096-82-5
Surrogates
10-130 1 03/31/20 15:55 04/02/20 20:28 2051-24-3
Decachlorobiphenyl(S) 64
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 04/07/2020 04:48 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 28
PO Box 228 a Statesville, NC 28687 e 704/872/4697
Page 17 of 38
Client: ().
Address: P0 a8o,
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122
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Cotut Street - P.O. Box 228
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Statesville, NC 2MR7
7(g) 972-4697
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Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/24/2020
Reported: 03/26/2020
For: Spindale
Comments: GM 8,195 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200324-26-01 Fecal Coliforms 1 8696 MPN/g SM92210E-2006 03/25/2020 WC
2.00324-26-01 Percent Solids 1 0.23 SM254OB-2011 03/25/2020 WC
200324-26-02 Fecal Coliforms 2 8000 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-02 Percent Solids 2 0.25 SM25406-2011 03/25/2020 WC
200324-26-03 Fecal Coliforms 3 8333 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-03 Percent Solids 3 0.24 SM254OB-2011 03/25/2020 WC
200324-26-04 Fecal Coliforms 4 8696 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-04 Percent Solids 4 0.23 SM254OB-2011 03/25/2020 WC
200324-26-05 Fecal Coliforms 5 8000 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-05 Percent Solids 5 0.25 SM25406-2011 03/25/2020 WC
200324-26-06 Fecal Coliforms 6 8000 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-06 Percent Solids 6 0.25 SM2540B 2011 03/25/2020 WC
200324-26-07 Fecal Coliforms 7 7692 MPN/g SM92210E-2006 03/25/2020 WC
200324-26-07 Percent Solids 7 0.26 SM254OB-2011 03/25/2020 WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4
Condition of Receipt
Sample Number 200324-26-01 Temp on Arrival. -
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-02 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-03 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-04 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-05 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-06 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-07 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4
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Staresvillc, NC 28687
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NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL020227
ti
Predictive
Client: John McFadden
345 McFadden Rd.
Advisor: Zach Key
Southern Soil Builders
I1, _
Forest City, NC 28043 958 Hoots Rd
1 ;
j Mehlich-3SoilReport Extraction Roaring River, NC 28669
Sampled County : Rutherford
Links to Helpful Information
Client ID: 442899 Advisord ID: 231531
Sampled: 11/23/2020 Received: 11/30/2020 Completed: 01/29/2021 Farm:
Sample ID: M1 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.3 120-200 0 80 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.41 0.93 10.5 83 1.8 5.9 95 30 66 15 45 207 141 385 385 575 0.1 1
Sample ID: M3 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Fescue/OGrass/Tim, M 0.8 120-200 0 110 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.46 1.02 6.5 71 1.9 5.6 100 16 56 14 44 342 222 205 205 426 0.1 2 i
Sample ID: M4 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Fescue/OGrass/Tim, M 0.7 120-200 0 100 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N
I 0.46 1.02 5.9 70 1.8 5.6 77 21 52 16 45 447 285 212 212 398 0.1 2
North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler. Commissioner of Acrriculture
NCDABCS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL020227
John McFadden Page 2 of 3
Sample ID: M5 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Fescue/OGrass/Tim, M 0.5 120-200 0 70 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N
0.46 1.03 8.2 79 1.8 5.8 150 34 61 16 50 328 214 501 501 727 0.1 1
Sample ID: M6 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.46 0.98 9.9 85 1.4 6.1 123 82 62 20 45 372 239 354 354 346 0.1 1
NCDABCS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO20227
John McFadden Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1 copper index
ESP exchangeable sodium percent
Fertilizer
HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies I K2o potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they i Mg% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN mineral soil class
an excellent source; 175 to 250 lb, per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples. Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-O mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htrMl#sfind information that P-1 phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.) P205 phosphate
S-I sulfur index
Test Results
SS-1 soluble salt index
WN weight per volume
Zn-AI zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-1, SS-1, Na, ESP, SS-1, NO3-N (not routinely
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm