HomeMy WebLinkAbout20081199 Ver 2_Monitoring Report_20120712July 13 2012
Ms Coleen H Sullins
NCDENR DWQ
401 Oversight/Express Review Perinitting Unit
1650 Mail Service Center
Raleigh NC 27699 1650
girl scouts r
Girl Scouts Hornets Nest Council
7007 Idlewild Road
Charlotte NC 28212
T 704/731 6500 / 800 868 0528
F 704/567 0598
www hngirlscouts org
Re Girl Scout Academy at Oak Springs, Iredell County (DWQ #20081199)
Preconstruchon Water Quality Monitoring Report (late winter /early spring and summer
2012 penods)
Dear Ms Sullms
Attached hereto is the late winter /early spring and summer 2012 preconstruction water quality
monitoring summaries associated with the proposed reservoir at the Girl Scouts Hornets Nest Council
Oak Springs Academy This information is provided based on the requirements and conditions of the
section 401 water quality certification DWQ #20081199
The attached information includes water quality sampling data from the unnamed tributaries of the
Yadkin River that will be inundated and will provide the input for the proposed reservoir This
information includes both analytical laboratory summary reports (March 2012 and July 2012) and
monthly average temperature data from four sampling sites (i a one site downstream of the proposed
discharge and three sites within the proposed reservoir middle upstream 1 and upstream 2)
If you have any questions or require additional information please feel free to contact me at 704 731 6552
or sdaley@hngirlscouts org
42: Smc ly
Sally aley JUL 1 2 2012
Chief Executive Officer
Girl Scouts Hornets Nest Council
Encl Pre - construction water quality monitoring summary (spring 2012)
Average Monthly temperature data summary (winter/spring 2011 2012)
Analytical water quality lab results (spring 2012)
Pre - construction water quality monitoring summary (summer 2012)
Average Monthly temperature data summary (May June 2012)
Analytical water quality lab results (summer 2012)
cc Bryan Tompkins USFWS Asheville
Amanda Jones USACE Asheville
Girl Scout Camp at Oak Springs
Statesville, NC
LATE WINTER /EARLY SPRING 2012
PRE-CONSTRUCTION WATER QUALITY MONITORING DATA
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SUMMER 2012
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Analytical Laboratory
13339 Hagers Ferry Road
Huntereviile NC 2807 8-7929
McGuire Nuclear Complex MG03A2
Phone 980. 875 -5245 Fax 980-875-4349
Order Summary Report
Order Number
J12060295
Pnact Name
WA
Customer Nam(s$
Scott Fletcher
Customer Address. Operations
Lab Contact Jason C Perkins phone 980 -US -5348
1 n a
Report Authorised e� 702012
Islgrreture)
Program Comments
Please contact the Program Manager (Jason C Perkins) with any questions regarding this report
Date Flags & Calculations
Page, of 23
Any analytical tests or individual analytes within a test flagged with a Qualifier Indicate a deviation from the method quality
system or quality control requirement The qualifier description Is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading All results are reported on a dry weight basis unless otherwise noted
Data Package
This data package includes analytical results that are applicable only to the samples described In this narrative An estimation of
the uncertainty of measurement for the results in the report Is available upon request This report shall not be reproduced except
In full without the written consent of the Analytical Laboratory Please contact the Analytical laboratory with any questions The
order of Individual sections within this report is as follows
Job Summary Report Sample /denNgcaBon Technk al Validation of Data Package AnaWal Laboratory CertMcate ofAna"s
Analytical Laboratory QC Reports Sub- oontractsd Laboratory Results Customer Specillc Date Sheets Reports 6
Documentation Customer Database Entries Teat Case Narratives Chain of Custody (COC)
Certification
The Analytical Laboratory holds the following State Certifications North Carolina (DENR) Certificate 0248 South Carolina
(OHEC) Laboratory ID # 99005 Contact the Analytical Laboratory for definitive information about the certification status of
specific methods
Sample ID's & Descriptions
Pon 2 of 23
Sample 10
Collection
PlwdMation Date and Time Colieeted By Semple Description
2012013382
Operation 20,Jun -12 1030 AM GENE VAUGHAN DAM SITE
2012013384
Operation 20- Jun-12 11 50 AM GENE VAUGHAN MANS LAND
2 Total Samples
Technical Validation Review
Checklist
COC and pW report are in agreement with sample totals ® Yes U No
and analyses (compliance programs and procedures)
All Results are less than the laboratory reporting limits p Yes g No
All laboratory QA/QC requirements are acceptable ® Yes 0 No
The Vendor Laboratories have been qualified by the
Analytical Laboratory Yes
Report Sections Included
® Job summary Report
® Sample Idemiflaetion
® Technhntl Vaildatton of Date Package
® Ane"cal Laboratory CartUie to of NWysls
❑ Analocal Laboratory QC Report
Page 3 01 23
❑ sub-contracted Laboratory Results
❑ Custaner Specific Date Sheets Reports & Documentarlon
❑ Customer Debase Erk W
® Chain of Custody
® Electronic Date Deliverable (EDD) Sent Separaft
Reviewed By DataBase Administrator Date 7/3/2012
Page 4 of 23
Certificate of Laboratory Analysis
This report shall not be reproduced except In full
Order # J12060295
Site DAM SITE Sample #' 2012013382
Collection Date 20- Jun-12 10 30 AM Matrbc OTHER
Analyse
ALKALINITY (FIXED END POINT
Result
4.111
Units flualHiere
RDL
DF
Method
Analysis Date/Time
Analyst
Al wW* (mg(L CeCO3)
32
mg/t.
01
1
SM2320B
22-Jun-12 08 37
TJA7067
(Ca=)
AMMONIA (COLOMMETRIC)
Anlmonle (Cob dnu trlc)
011
mg44L
002
1
EPA 3501
26-Jun-12 12-34
BGN0034
NITRITE + NITRATE (COLORIMETfticl
NMrite + NfbIft (Colodmeblo)
0.29
mg-NIL
001
1
EPA 3532
25Jun -12 12.34
BGNWN
GA MOSPHATE WAWMIMETWO
O- PHOSPHATE (Coladmetrlc)
00106
mg•PIL N1
0 005
1
EPA 3851
21 Jun -12 0939
7uNN
Total Jgdd c l Nitrogen
0 n
mg-W
015
1
EPA 3512
28%km -12 1313
BGN9034
TOTAL PHOSPHORUS (COLORIM
Total Phosphans (CaWknotrtc)
rC)
0 019
mg-PIL
0 005
1
EPA 385 1
03-Jul-12 *31
SGN9034
FECAL COMFORM
Vendor Parameter
complete
1
V PACE
SPECIFIC CONDUCTANCE
Vendor Parameter
PM IN
Complete
1
V PACE
WATER (NON.G. P IANCn
Vendor Parameter
TURSIOM
ANA yS181
Complete
1
V PACE
Vendor Parameter
complete
1
V PACE
Site MANS LAND
Sample #
2012013384
Collection Date 20-Jun-12 1150
AM
Matrbc
OTHER
Analyte
MJWJNITY BWQ END PONT 4,111
Result
Units Waliflers
RDL
DF
Method
Analysis DaWTlme
Analyst
AlhelinMy (mglL CGW3)
23
mglL
01
1
SM23208
22-Jun-12 08 37
TJA7057
(CeCO3)
AMMONIA (COLORIM"RiCi
Ammonia (CoWmetrlc)
012
mg-N&
002
1
EPA 3501
26-Jun-12 12:35
BGN3034
Certificate of Laboratory Analysis Page 5 of 23
Th/s report shall not be reproduced except In full
Order # J12NO295
Side MANS LAND Sample 0 2012013384
Collection Date 20- Jun-12 11 50 AM Matrix OTHER
Ana" Result Units Qualifiers ROL OF Method Analysis DataMme Analyst
NffRrrE + NITRATE (COLORIMETRICI
NIMte + Nitrate (Colorimetric) 014 mg+ A. 001 1 EPA 353 2 28,1un -12 12:35 SM9034
O-PHOSPHATE (COLORIMETRICI
O- PHOSPHATE (C tic)
000870 mg-PA. NI 0 005
u� Nitrogen
0.22 mg-NIL 015
(
TOM PHOSPHORUS MLDMMEMC)
Total Phosphorus (Calorknetdc)
00098 Wit. 0 005
FECAL COMFORM
Vendor Parameter
Complete
SPECIFIC CONDUCTANCE
Vendor Parameter
Complete
PH IN WATER (NONSOMPL!ANCn
Vendor Parameter
ANALYSIS)
Complete
IWIMM
Vendor Parameter
complete
1 EPA 3851 21-Jun-12 0942 TLINN
i EPA 3512 28,hm -12 1314 aGNWU
1 EPA 3851 03,tu1 -12 10.32 SON9034
1 V PACE
1 V PACE
1 V PACE
1 % PACE
Qualifiers
N1 See additional Infonnallon listed below
Samples were not filtered within the required time upon collection All results should be considered as estimates
(�IceMaocale
wewtoom
June 29 2012
Program Manager
Duke Energy
Pena AnWylial Services, Ina
408 Fast Meadow Road suite A
Eden NC 27288
RE Project- J12000295
Pace Project No 92121949
(818)438921
Pane Ana*ftW Servim Ina
2228 Riverside Dr
AshwAs NC 288114
(828)264.7178
Pans AnWyftW 8ervWM Irm
fieff f as suite 100
Hunh svft NC 28078
(704739092
Dear Program Manager
Enclosed are the analytical results for sample(s) received by the laboratory on June 20 2012 The
results relate only to the samples Included in this report Results reported herein conform to the
most current TNI standards and the laboratory s Quality Assurance Manual where applicable unless
otherwise noted in the body of the report
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted
If you have any questions concerning this report please feel free to contact me
Sincerely
Kevin Godwin for
Kevin Herring
kevin herring@pacelabs com
Project Manager
Erudowes
ca. I& Jay Pokm Duke Energy
�fq9' � REPORT OF LABORATORY ANALYSIS Page i of 17
��) This mW shall not be reproduced mroep in full
TN without the wd8en consent of Pace A"yftd SeMma Inc
45
IceAnalftcal"'
Poe Analydi l Ber4ft% Ina
208 East Meadow Road Sub A
Edon NO 27288
(33SX23-M1
PM AnaVftal SerAm Ina
2226 RW"de Or
Aehow0a NO 28604
(828)264 -7178
SAMPLE ANALYTE COUNT
Paee Armly W ServkM Ina
fftWd*Me Sucre 108
HunWWAe NO 28078
(704)875.9092
Protect.
J12M MOS
Pepe Project No
92121949
Amdytea
Lab ID
Sample ID
Method
Analysts
Rep.
Labors"
92121949001
DAM SITE
SM 9222D
KDF
1
PA
EPA 1201
AES
1
PASI,A
EPA 1801
SAE
1
PAST -A
EPA 9040
AES
1
PASI,A
92121949002
MANS LAND
SM 9222D
KDF
1
PASIC
EPA 12D 1
AES
1
PASHA
EPA 1801
SAE
1
PASI -A
EPA 9040
AES
1
PASHA
REPORT OF LABORATORY ANALYSIS Page 3 of 17
Thla report shall not be nwoduoed exoW in fidl
wilhoul the wrinen owment of Pepe Analybral Sww a Ine
aceAmOcal
�omn
Pace Analytical Services, Inc.
205 Fast Meador Road &MA
Eden NO 27258
(338)823.8921
HITS ONLY
Pace Analytical Services Inc.
2228 Rhmelde Or
Adwvffie NO 28804
(828M4 -7178
Pace Analytical SeMees, Inc
M91iWM9 Suds 100
HuNasvllle NO 28078
(704)076.9082
Project
J12060M
Pace Project No
92121949
Lab Semple ID
CUM Semple ID
Method
Parameters
Read Units
Report Lund
Ar aWW
QuaUfiers
92121949001
DAN SITE
SM 0222D
Fecal CoMmis
58 0 CF 9100 ml.
10
OSM1218 28
N2
EPA 1201
Spedflc ConducWm
781 unhoslan
100
08/21112 0950
N2
EPA 1801
Turbidity
55 NTU
10
08/2?112 09 50
EPA 9040
pH
71 Std Units
010
08/2711213 32
H1 HS
92121949002
MANS LAND
SM 0222D
Fwal Coltfonns
14 0 CF1.11100 ml.
10
08/20/1218 28
N2 u1
EPA 1201
Specific Condudanoe
851 unlhoalan
100
08021/12 09 50
N2
EPA 1801
Tuft*
17 NTU
10
08/22!12 09 50
EPA 9040
PH
8 8 Std Units
010
0=7 /1213 32
H1 H8
REPORT OF LABORATORY ANALYSIS Page 4 of 17
The repel shall not be reproduced, except in ha
wdhmd ere wrleen oonsem of Pete Anetyaeal Senolm Inc
ceAnalAcal
Paso Analytical Services, Irre
205 Fast Meadow Road Suite A
Eden, NC 27288
(338)825-8821
Pace Anaytical Services, Ine.
2228 Wverelde Or
AstwAls NC 28804
PROJECT NARRATIVE
Protect J12000205
Papa Protect No 92121949
Megrod SM 9222D
Desorlptlon MBIO O222D Fecal CoHform CHT
Clieft Duke Erier99
Date June 29 2012
(SM284.7178
General Information
2 samples were analyzed for SM 92220 All samples were reoelved In acceptable condition with any exceptions noted below
Mold Tuna•
The samples were anayzed within the method required hold times with any exceptions noted below
IMtlai Calibrations (Including MS Tune as applicable)
AD criteria were within method requirements with any exceptions now below
Continuing Capbradon
All criteria were within method requirements with any exceptions noted below
Internal Standards
AD Internal standards were within QC limits with any exceptions noted below
Surrogates
All surrogates were within OC Omb with any exceptions noted below
Method BlanL
A9 analytes were below the report tindt In the method (dank with any exceptions noted below
Laboratory Control Spike
All laboratory control spike compounds were within OC limits with any exceptions noted below
IWabix Spires
All percent recoveries and relative percent dUbrences (RPDs) were within acceptance aiterle with any exceptions noted below
Duplicate Sample
A I duplicate sample results were within method acceptance alterla with any exceptions noted below
Additional Conarherrle
Anelyte Comments
OC Batch MBCH14214
N2 The lab does not hold TNI aaxeditatlon for this parameter
BLANK (Lab ID 783491)
Fecal Coliforms
DAM SITE (Lob ID 92121949001)
Fecal Col forms
DUP (Lab ID 783493)
Fecal Collforms
MANS LAND (Lab ID 92121949002)
Fetal Cotifoms
REPORT OF LABORATORY ANALYSIS
Tire report shall not be reproduced, axoW in full
wtthad tib written consent of Pace Analytical Services, Inc.
Pave ArAWal Services, Ina,
11111"0 tas, suite loo
Flutter v$e NC 28078
(7o4)87f►9092
Page 5 of 17
lceftlft,
►rexAaoefabs
Project A
Pace Project No 92
M tftod SM 8222
Deeelfpow MB10 9222
also,~ Duke Energy
Data June 29
Analyte Comments
QC Batch MBCHM4214
e
Poe Analytical Servlees lna Pave AnalMal Services Inc.
Pace An@WU W Bervkee Ina
!
208 Eed Meadow Road SWteA 2225 Rivmdds Dr
"Me Suits loo
Qom
Eden NC 27288 AehevNe NC 28804
HuMusYRe NC 28078
(336)OMI-8821 (828)254.7176
(704)87 &8092
PROJECT NARRATIVE
000205
121949
D
D Fecal CoUfmm CHT
2012
u1 Results based upon cc" courts outslde acceptable range
MANS LAND (Lab ID 92121949002)
Fecal Collforms
REPORT OF LABORATORY ANALYSIS Page 6 of 17
The repot shall not be reproduced except in hill
wtMoul Ore wn ten OVUM of Pace Analytical SerAM Inc
I
a
/�,��'J
Pece Anallr" Series Inc. Peon Analytical Services, Inc.
Pass Analytical Semless, Inc
C @I`U a cQ1
•'
20S East Avow Road &ftA 2226 Rhmmids Dr
11110m4me &ft 100
Eden NC 27268 Asheville NO 28804
Hurb sWle NC 28078
(886)9258921 (OW)284.7176
(704W84M
PROJECT NARRATIVE
Project, J1208M
POW Project No 92121949
Msthod EPA 1201
Description 1201 Specific Conductance
Client: Duke Energy
Date June 29 2012
General information
2 samples were analyzed for EPA 1201 AD samples were received In ecxeptable condition with any exceptions noted bear
Hold Thm
The samples were analyzed wlttln the method required hold Ow with any exceptions noted below
Method Blank
All anslytes were below the report nmlt In the method blank with any exceptions noted below
Lr ConM spike
AD laboratory control spike carlpounds were waft OC Dndte wkh any exceptlorre noted below
Makh spikes
All percent recovertes and relative percent dtiferertoes (RPOs) were within aoosptence crtterte with any exceptions noted below
Dupik de Semple
All dupacete sample results were within method acceptance criteria with any exceptions noted below
Additional Coeumnts
OC Batch WET/21324
N2 The lob does rot hold TNI accreditation for this parameter
BLANK (Lab ID 752800)
Specific Conductance
DAM SITE (Lab ID 02121949001)
Specific Conductance
DL P (Lob ID 782802)
Specific Conductance
Specific Conductance
LOS (Lab ID 782801)
SpedBc Corxbrctance
MANS LAND (Lab ID 92121949002)
Specific Conductance
REPORT OF LABORATORY ANALYSIS Page 7 of 17
no report shell not be reproduced except in full
wh td the wdtlen eoesont of Pace Ansocal Semen Inc
ceAnalytica!
awrxpea�6soam
Project: J12080298
1`80e Project No 92121949
Illetitod EPA 1801
Description 1801 Turbidity
Client: Duke Energy
Date• June 29 2012
Pace Arayaoal serAces, Ina
208 Fad Meadow Road sulte A
Eden NO 27288
(338)8288921
Paw Aray" SerAmm Its.
2718 Rkwelde Or
AeherBle NC 28804
PROJECT NARRATIVE
(828)284.7178
General Intormatlon
2 samples wee analyzed for EPA 1801 AO samples was received In acceptable condition with any exceptions noted below
Hold Tim
The samples were analyzed witidn the meftd retpdred hold tines with any exceptions noted below
Mod d Blank
All anaytes were below the report Omit In the me#W blank with any exceptions noted below
Laboratory Control Spike:
AO laboratory control spike compounds were within QC limits with any eicepllons noted below
lisldrbt spikes
All percent recoverles and relative percent differences (RPDs) were wOtdn acceptance criteria with any exceptions toted below
Duplicate sample
All duplicate sample results were within me0rod acceptance alma with any exceptions noted below
Additional Comments.
Pane Anay" 8srrlces, Inc.
Moore 8udte 100
HredderavIDe NC 28078
(704)0784092
REPORT OF LABORATORY ANALYSIS Page 8 Of 17
TW report slap not be reproduced except in full
withad the wftn arm" of Pare k ylpcal sew"a, Inc
CeAl1�1J�lCal a Pace Analytical Services Ina PaceAnaytloal Services, Inc. Paos Analy" services Ina
{�G 208 Eael Meadow Road Suke A 2225 Rhwide Dr Suite too
y Edam NC 27288 Ashedle NC 28804 HurdervAs NC 28078
(336)8238821 (e28)264 -7178 (704)875.9092
PROJECT NARRATIVE
Project- J1206MO
Pace Project No 92121949
111119111W EPA9040
DescrIp9llon 9040 pH
Client DAG Energy
Date June 29 2012
GeneralIn10114 on
2 samples were analyzed for EPA 9040 All samples were received In acceptable condition with any exceptions noted below
Hold Tlme
The samples were andiysed within the method required hold tlmes with any exceptions noted below
H1 Analysis conducted oukdde the EPA method holding time
DAM SITE (Lab ID 92121949001)
MANS LAND (Lab ID 92121949002)
H5 Aneysts Initiated outside of the 15 minute EPA nwomncended holding tine.
DAM SITE (Lab la 92121949001)
MANS LAND (Lab la 92121949002)
Wlefhod Blank
AN analytes were below the report 11m11 In the method blank with any exceptions noted below
Laboratory ConbW Spike
AD labonit" 00001 5131118 compotaxle were within OC timtlo with any exceptions noted below
MaNx Spikes
All Percent mcxwerles and relative percent dktelence5 (RPDs) were **M acceptance k nUft with tiny excepbons noted balm
Dupilcatd Sample
A11 duplicate sample resuks were w M methM aeoaptanoe a bda with any exceptions noted below
Additional Comments
This date package has been reviewed for quality and comptetsneas and Is approved for release
REPORT OF LABORATORY ANALYSIS Page 9 of 17
Tine raPort shall not be reproduced axoept m Nit
worm the woen consent of Pecs Analywal Servloae Inc
Velll a"ca/ a
wwwp bmwm
Peas Analytical Sowlce% Inc
208 Eem Meadow Road Sufte A
Eden, NC 27288
(3181623-8921
Pane Analytical Services Inc
2225 Riv mft Dr
AshevOW NC 28804
(0n)2U -7178
ANALYTICAL RESULTS
Pace And"cel SorvicM Inc.
11MAIIAR& 8ufla 100
Fume, NC 28078
(704 )875.9092
Project. J1206MG
Pace Project No 92121949
Semple GAM SITE
Lab ID 92121949001 Collected 08/20/1210 30
Reoehred 0111=1215 55 Matrix Water
Parameters
Results Units
Report Lbnfi
DF
Prepared Analyzed CAS No Qua]
111111310 8?J:2D Fecal Conform CMT
Analytical Method SM 92220
Fecal CoMimms
SU CFU/100 ml.
10
1
08120/121828 N2
1201 SpeclNa Conductance
Analytical Method EPA 1201
Specific Conductance
781 umhoalcm
100
1
08/21/12 0850 N2
1801 Turbidity
Analytical Method EPA 1801
Turbidity
55 NTU
10
1
08/22/12 09 50
9040 pH
Analytical Method EPA 9040
pH
71 Std Units
010
1
08/27/1213 32 H1 H8
Date 08J2M12 02 25 PM REPORT OF LABORATORY ANALYSIS Page 10 of 17
This report shell not be mproduoed except m bull.
vr&W the MOM aonseM of Pace Analytical 6ervioss Inc
lCeA1720cal"'
Pane Analytcal Services tno.
208 East Meadow Road &die A
Eden NO 27250
(336)623.8921
Pans Analypeet Gamin% Ina.
2225 Rivmeide Or
AdWAID NO 26M
(826)254.7176
ANALYTICAL RESULTS
Pace Analytical 8sfvtcea Inc,
tGdy?Qm sake 100
FdoaerWWWe NC 28078
(704)0766082
Projecl J12080298
Pepe Project No 92121949
Sample MANS LAND
Lab ID 92121949002 Collected 08/20/1211 50
Received 08/20/1215 55 Metrbr Whter
Parameters
Results Units
Repot Lbrdt
OF
Prepared AnaWW CAS No Qual
MBIO 9222D Pecel Coftirm CHT
Ane"cel Method SM 9222D
Fecal Co6torrrm
14.0 CFU/100 mL
10
1
0INW121&28 N2 ul
1201 Speaft Conduounce
Ana"cei Me0rod EPA 1201
Spedft Comae
881 umhoslan
100
1
0821 /12 0850 N2
1801 Turbidity
Analytcat Method EPA 1801
Turbidky
17 NTU
10
1
0822/12 0980
9040 pH
Analytical Method EPA 9040
pH
8.8 Std Units
010
1
0827/1213 32 H1 Hs
Date 08W=12 02 26 PM REPORT OF LABORATORY ANALYSIS Page 11 of 17
TMs repot dud not be reproduced, except in M
without the wmen cone of Pace Analytical Sam= Inc
(� 2eftlytcalo
Pace Arraytical Services Irm
208 East Meadow Road Stilts A
Eden NO 27288
(338)8238921
Pace Analyeeal Servleee Inc.
2228 RWaralde Or
AshaM NO 28804
(828)284.7178
QUALITY CONTROL DATA
Project J1208MB
Pepe Project No 92121949
QC Be" MBCW4214 Analysis Method SM 9222D
QC Batch Method SM 9222D Analysts Descr"m 9222D MBIO Fecal Collform CHT
Associated Lab Samples 92121949001 92121949002
METHOD BLANK 783491 Malt Water
A880deted Let) Samples 92121949001 92121949002
Blank Reporting
Parameter Units Result LImN Analyzed Qualifiers
Fecal CclffOrms CFW100 mt. ND 10 0201121828 N2
SAMPLE DUPLICATE 783493
92121981001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal CoUbms CFUf100 ml 100 ND (2
Pave Analyeeal BeMces, Inc
liAue Suftsloo
Hw to vAle NC 28078
(704)076 -9092
Date 08/M012 02 28 PM REPORT OF LABORATORY ANALYSIS Page 12 of 17
The mW slid not be reproduced. exoW in fall
wdh&A the wMMn consent of Pave And Semmes. Inc
COAWW
swerpeosiebaaoer
Project J12060205
Pace Project No 92121949
Pace AnsyftlServices Inc
208 Easi Usedow Road Suite A
Eden, NO 27288
(338)8238921
Pace Analy" Servtoes, Ina.
2225 Riverside Dr
Asheville NO 28804
(828)254-7178
QUALITY CONTROL DATA
QC Batch WET/21324 Analysis Method EPA 1201
QC Batch Method EPA 1201 Analysis Description 1201 SpedNc Conductance
Associated Lab Samples 92121949001 92121949002
METHOD BLANK 782800 Matrbc Water
Associated Lab Samples 92121949001 92121040
Blank RepoAktg
Parameter units Result Limit AnaWsd Qualifiers
Specific Conductance umhosla n NO 10 0 08121112 09 50 N2
LABORATORY CONTROL SAMPLE 782801
Pace AnaWas!BeMces Inc.
id*W3a sufte 100
HunWrsvlDe NO 28078
(704)8769092
Spike LCS LOS % Rec
Parameter Unite Conc. Result % Roo Limits Quawlers
Specific Conductance umhoa/an 1410 1420 101 90-110 N2
SAMPLE DUPLICATE 782802
92121598002 Dup
Parameter Untie Result Result RPD Quaillkers
Spook Conductance tdnhoslam 474 478 1 N2
SAMPLE DUPLICATE 782848
92121949001 Dup
Parameter Units Result Result RPD Quefiflers
Specific Cortdu cw= umhoslan 781 788 1 N2
Date 08n =12 02 28 PM REPORT OF LABORATORY ANALYSIS Page 13 of 17
This reW ehd not be reproduced swept in fun
wkhout sire written consent d Pace Anarytlesi Oavbes, Ina
COAna Vmle
Project. J12060296
Pepe Project No 92121949
Pow Analytical8eMeM Inc.
208 Feat Meadow Road Suite A
Eden, NC 27288
(330MM921
Paw Anaytleal Services Ina
2228 Riverside Dr
Ae WAG NC 28804
(828)264.7178
QUALITY CONTROL DATA
QC Batch WET/21341 Analysis Method EPA 1801
QC Batch Method EPA 1801 Analysis Description 1801 Turbidity
ASSOtiated Lab samples 92121949001 92121940002
METHOD BLANK. 783585 Matrbc Water
Assodated Lab samples 92121949001 92121949002
Blank Reporting
Parameter Units Result Wnit Anayed Qualfiers
Turbidly NTU ND 10 WWI 2 0980
LABORATORY CONTROL SAMPLE 783585
Pace Anti" Services Inc,
irue subs 100
HurftrGVft NC 28078
M111768092
spice LCS LCS % Rec
Parameter Urals Conr_ Result % Rea Limits Qualifiers
Turbidity NTU 10 100 100 90.110
SAMPLE DUPUCATE 783587
92121949001 Dup
Parameter Urdta Result Resd RPD Qualifiers
Turbidly NTU 55 65 1
Data 08/29/2012 02 28 PM REPORT OF LABORATORY ANALYSIS Page 14 of 17
TMs report"not be reproduced except in I d
wf0rout the wften correent of Pace Andy ind Services Inc
ceAnaocal
www.perem0aoosr
Pans AnaVftal SeMoes Inc
205 East Meadow Road Buns A
Eden NC 27258
(x1SM4921
Pace Analyttaal Services, Inc
2225 Rhrerelde Or
AsteWle NC 28804
(828)254-7178
QUALITY CONTROL DATA
Project J12050295
Pepe Project No 92121949
QC Batch WET121408 Analysis Method EPA 9040
QC Batch Method EPA 9040 Analysis Desalptlon 9040 pH
Associated Lab Samples 92121949001 92121949002
SAMPLE DUPLICATE 785938
92121887001 Dup
Parameter Units Result Re" RPD Qualdlers
pH Std Units 89 69 0 HI H8
SAMPLE DUPLICATE 788939
92122384003 Dup
Parameter Units Resort Result RPD QualHiers
pH Std Units 70 70 1 H1 HS
Paee AnelyttaN Semites, Inc.
SmiSwas suns 100
HwftrWft NC 28078
(704)876.9082
Date 08129/2012 02 28 PM REPORT OF LABORATORY ANALYSIS Page 15 of 17
Ttds report 00 riot be reproduced except in full
wkhotd the written ommenl of ParsAnelybcel 8mvlces Inc
ne /� �� a Pace Analyhot 9ervkm Irm Pane Ansly6otl Servlm Ina Pace Ansydeal 8srvkss Ina
A a � 205 Eeet Meadow Read SAM 2228 Rivwdde Dr 151100448 Suits 100
Eden NC 27286 Asheville NC 28004 Hwfersvfffe, NC 29018
(339)823-8821 (828)284 -7178 (704)8764092
QUALIFIERS
Project: J12060205
Pace Projed No 92121949
DEFINITIONS
OF Dilution Factor H reported represents the factor applied to the reported data due to changes In sample preparation dilution of
the sample aliquot, or moisture content.
NO Not Detected at or above adjusted reporting Omit
J Estimated concentration above the adjusted method detection ibnft and below the adjusted reporting emit
MOL Adjusted Method won Umft
PRL Pace Reporting Umft
RL Reporting Umft
S Surrogate
1 2aownylhydrazlre (8270 listed analyte) decomposes toAzobeozene
Consistent with EPA guldellnes, unrounded date are displayed and have been used to calculate % recovery and RPD values
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
OUP Semple Duplicate
RPD Relative Percent Dftrence
NC Not Calculable
80 Silica Gel Clean -Up
U Indicates the compound was aria" for but not detected
each eeelyte Ids lWWn9 de concentration
cannot be �e�ed Oan DOhenylandne usbO Method 8270 The result reported for
Add preservation may not be appropdste fo 2- ChbmetiryMnyl efher Styrene and VI" chloride
Pace Ans"01 Is TNI nom edited Corded your Pace PM for the MMOM fist of accredited analytes
TNI The NELAC bmft to
LABORATOWES
PASI -A Pace Analytical Services Asheville
PASI-C Pace Analytical Services Charlotte
ANALYTE aUALIFIERS
H1 Analysis conducted outsde the EFA method hokWV time
H8 Analysis initiated outside of the 15 minute EPA recommended holding Irme
N2 The lab does not hold TNI accreditation for this paraneter
III Results based upon colony counts outside acceptable ramp
Date 00/20012 02 28 PM REPORT OF LABORATORY ANALYSIS Page 18 of 17
This report ehd not be reproduced except In full
wtthout the vn Mm co cant of Pace Analylxwl Sendoes Inc.
ceft"Cal
Pace AnaVWW 9om1c , Inc
208 Eesl Meadow Road SuBe A
Eden, NC 27288
(338)8238821
Pace Anslytlal SeMces, Ina
2228 Rhwside Dr
Adrevsie NC 28804
(8287178
QUAUTY CONTROL DATA CROSS REFERENCE TABLE
Pao Ana0dool SorAcm ins
Iriliitie sine 100
Ifiaderwft NC 28078
(704)8784092
Protect
J12080295
Pace Pf*d No
92121949
Lab ID
Sample ID
QC Batch Method
Analytkal
QC Batch Analydeal Method Balch
92121949001
DAM BITE
SM 92220
MSCH14214
92121948002
MANS LAND
SM 9222D
MSCW4214
92121949001
DAM SITE
EPA 1201
WET/21324
92121949002
MANS LAND
EPA 1201
WET/21324
92121949001
DAM SITE
EPA 1801
WET/21341
92121949002
MANS LAND
EPA 1801
WET/21341
92121949001
DAM SITE
EPA 9040
WET121408
92121949002
MANS LAND
EPA 9040
WET21408
Date 0829/2012 02 28 PM REPORT OF LABORATORY ANALYSIS Page 17 of 17
Thin report shall not be reproduced a mpl in lull.
wbhwA are wrl0en ecnwd of Palle Anelyucal SeM M Inc
R
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