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HomeMy WebLinkAboutWQ0002376_Residual Annual Report 2020_20210228Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0002376 Applicant/Permittee City of Reidsville Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Brent Collins Email Address* brent.collins@emaresourcesinc.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... ....................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3367511441 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00002376 Fbs Current Existing permt number Applicant/Permittee Address* 1100 Vance Street, Reidsville, NC 27320 Facility Name * City of Reidsville RLAP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) 2020 Reidsville Annual Report - WQ0002376.pdf 14.7MB Upload only 1 FLFdocurrent (less than 250 NB). NLRiple documents rust be corrbined into one FDFfile unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature ff &kgw Submission Date 2/28/2021 February 28, 2021 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2020 Annual Report - Reidsville Treatment and Land Application of Residuals Permit No. WQ0002376 Dear Sir or Madam: Enclosed is one copy of the 2020 Annual Report for the above referenced land application permit. During 2020 EMA Resources, Inc. land applied 291.08 dry tons of wastewater residuals to 306.45 acres of private farmland. Lime was ordered in October to be applied to the fields that had a pH under 6.0, even though it is no longer a requirement in their permit. Site conditions have been too wet to apply the lime. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Brent Collins Director of Technical Services brent.collins2emaresourcesinc.com Phone 336.751.1441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 ,EMA ---Resources, Inc. City of Reidsville 2020 Annual Report Residuals Land Application Permit No. WQ0002376 Prepared By: EMA Resources, Inc. Phone 336.751.1441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0002376 County: Rockingham County Year: 2020 Facility Name (as shown on permit): City of Reidsville Land Application Operator: Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes C] No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part _A_- Residuals Anplication Summarv! EMA Resources Inc. Total number of application fields in thepermit: 56 Total number of fields utilized for land application during the year: 22 Total amount of dry tons applied during the year for all application sites:1 291.08 Total number of acres utilizes for land application during the year: 306.45 rarr 15- Annual Comniance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes CU No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the pennitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I 1 I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Chuck Smith - Public Works Director Per&ee I^4me and "Title (type or print) to Signature om i•er* Date (if different from`Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T lei 100Z1 Signature of Permitte Date 2/8/2021 Signature of Land Applier Date (if different from Permittee and Preparer) 1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0002376 Facility Name: City of Reidsville Residual Source WQ # or NPDES #: WWTP Name: Residual Analvsis Data NCO024881 Reidsville WWTP Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Conic. Limit (mg/kg) Sam le or Composite Date 1/9/20 4/2/20 7/21/20 10/1/20 Percent Solids (%) NA 0.56 2.18 0.779 0.988 Arsenic 75 69.8 20 30 24 Cadmium 85 8.25 2.36 2.5 2.91 Copper 4,300 54.8 179 38.8 268 Chromium NA 31.7 36.7 29.5 55.9 Lead 840 24.8 45.1 22.5 58.3 Mercury 57 0.528 0.814 0.399 0.337 Molybdenum 75 21.7 6.19 16.9 13.5 Nickel 420 27.5 12.5 15 22.3 Selenium 100 81.7 23.3 40 32 Zinc 7,500 217 643 101 963 Total Phosphorus NA 12900 17000 12600 29500 TKN NA 63000 12000 27800 27900 Ammonia -Nitrogen NA 27000 10600 15300 24400 Nitrate and Nitrite NA 833 234 625 582 or surface disposal facilities the ceding concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen Ities f submitting false information, including the possibility of fines and imprisonment for knowing violations." JA "' Z 10 ZdL I Signature o er * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 IO2 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0002376 Facility Name: City of Reidsville Residual Source NPDES # or WQ#: NCO024881 WWTP Name: Reidsville WWTP Residual Analvsis Data Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Sample or Com osite Date 1/9/20 4/2/20 7/21/20 10/l/20 Aluminum 3470 14500 2990 27100 Calcium 6320 9670 4890 19000 Magnesium 3330 3300 2290 4640 pH 6.8 6.9 7.4 7.7 Potassium 9770 3840 6640 6190 Sodium 24500 5190 8800 6750 PAN 25133 5954 12025 13832 SAR 4.63 1.71 2.29 1.13 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." A�A— Z to I ZM1 Signature o r * to *Preparer is defin in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 12.05 Operator: Ronnie Marshall Owner: James Albert Predominant Soil Series: CgB2 Acres Used: 15.41 Acres Permitted: 15.41 Site #: RC005 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.78 Arsenic 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.419 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.419 Chromiuni 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 Lead 0.091 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.091 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Selenium 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Zinc 1.506 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.506 Total Phos- 46.138 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 46.138 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville James Albert Operator: Ronnie Marshall Crop 1 Name: Fescue -Hay WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 12.05 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 15.41 RC005 Acres Permitted: 15.41 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 11/4 110500 0.988 0.295 Reidsville WWTP Dry <.5" S 0.5 1 0.3 27900 24400 582 8.173 NA Fescue 11/5 117000 0.988 0.313 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 8.653 NA Fescue 11/6 65000 0.988 0.174 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 4.807 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 21.634 o.000 Lime Applied Annuallbs/acre 0.038 0.005 0.419 0.087 0.091 0.001 0.021 0.035 0.050 1.506 46.138 5.172 6.678 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.04 0.023 1.949 0.552 0.503 0.02 0.062 0.303 0.063 2000 Current Cumulative lbs/ac 0.078 0.028 2.368 0.639 0.594 0.021 0.083 0.338 0.113 Permitted C. P. L. R. * * * * 1 3 1 34 1 1338 1 267 15 1 1 374 89 Permit PAN Limit 1 st/2nd Crop 1 209 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 2.41 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: James Albert Predominant Soil Series: FrD2 Acres Used: 14.79 Acres Permitted: 14.79 Site #: RC005 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.16 Arsenic 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 Chromiuni 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Lead 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 denum Nickel 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Selenium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Zinc 0.314 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.314 Total Phos- 9.617 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 9.617 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville James Albert Operator: Ronnie Marshall WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 2.41 Site #: Predominant Soil Series: FrD2 Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 115 Crop 2 Name: Acres Utilized: 14.79 RC005 Acres Permitted: 14.79 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 11/6 58500 0.988 0.163 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 1 582 4.508 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o SsSoo As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 4.508 o.000 Lime Applied Annuallbs/acre 0.008 0.001 0.087 0.018 0.019 0.000 0.004 0.007 0.010 0.314 9.617 0.008 0.004 0.312 0.076 0.057 0.001 0.011 0.04 0.013 0.809 0.016 0.005 0.399 0.094 0.076 0.001 0.015 0.047 0.023 1.123 36 1 34 1 1338 1 267 15 1 1 374 89 1 2498 1 1 115 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 8.57 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: James Albert Predominant Soil Series: NaB Acres Used: 10.7 Acres Permitted: 10.7 Site #: RC005 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.80 Arsenic 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.429 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.429 Chromium 0.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090 Lead 0.093 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 denum Nickel 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Selenium 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Zinc 1.543 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.543 Total Phos- 47.259 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 47.259 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville James Albert Operator: Ronnie Marshall WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 8.57 Site #: Predominant Soil Series: NaB Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 178 Crop 2 Name: Acres Utilized: 10.7 RC005 Acres Permitted: 10.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/7 117000 0.988 0.451 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 1 582 12.463 NA Fescue 10/8 91000 0.988 0.350 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 9.693 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 2os000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 22.156 0.000 Lime Applied Annuallbs/acre 0.038 0.005 0.429 0.090 0.093 0.001 0.022 0.036 0.051 1.543 47.259 5.172 6.715 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.04 0.023 1.949 0.552 0.503 0.02 0.062 0.303 0.063 2000 Current Cumulative lbs/ac 0.078 0.028 2.378 0.642 0.596 0.021 0.084 0.339 0.114 Permitted C. P. L. R. * * * * 1 3 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 178 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Auman French Owner: Dan Stocks Predominant Soil Series: 8.49 Acres Permitted: 8.49 Site #: RC010 Field #: 2.89 RnD Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.34 Arsenic 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Chromium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Lead 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 denum Nickel 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Selenium 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056 Zinc 0.148 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.148 Total Phos- 8.772 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.772 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Dan Stocks Operator: Auman French WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 2.89 Site #: Predominant Soil Series: RnD Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 141 Crop 2 Name: Acres Utilized: 8.49 RC010 Acres Permitted: 8.49 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 3/28 123500 0.56 0.340 Reidsville WWTP Dry <.5" S 0.5 0.3 63000 27000 1 833 17.075 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o t235oo As Cd Cu Cr Pb Hg Mo Ni Se Zn P 17.075 0.000 Lime Applied Annuallbs/acre 0.047 0.006 0.037 0.022 0.017 0.000 0.015 0.019 0.056 0.148 8.772 0.167 0.04 2.52 0.62 0.556 0.016 0.12 0.366 0.205 7.715 0.214 0.046 2.557 0.642 0.573 0.016 0.135 0.385 0.261 7.863 1 36 34 1 1338 267 1 15 374 1 89 1 2498 1 141 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 27.62 Operator: Harry Sharpe Owner: Daisy Purgason Predominant Soil Series: NaB Acres Used: 20.67 Acres Permitted: 20.67 Site #: RC011 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date ENE MENEM mammon Non no 0 Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 1 C 11 12 DT/Ac./ App. Event 0.57 0.76 Arsenic 0.023 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Cadmium 0.003 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.205 0.410 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.614 Chromiuni 0.042 0.085 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.127 Lead 0.052 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.141 Mercury 0.001 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 denum Nickel 0.014 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Selenium 0.027 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.076 Zinc 0.736 1.471 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.207 Total Phos- 19.448 45.076 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 64.524 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Daisy Purgason Operator: Harry Sharpe WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 27.62 Site #: Predominant Soil Series: NaB Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 178 Crop 2 Name: Acres Utilized: 20.67 RCOl l Acres Permitted: 20.67 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)�• Precip. Past 24 His. inches F '5 w o 7� co * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/4 130000 2.18 0.572 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 1 234 6.808 NA Fescue 10/19 143000 0.988 0.285 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 7.885 NA Fescue 10/20 91000 0.988 0.181 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 5.018 NA Fescue 10/21 58500 0.988 0.117 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 3.226 NA Fescue 10/22 91000 0.988 0.181 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 5.018 NA Fescue 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 513500 As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 27.954 o.000 Lime Applied Annuallbs/acre 0.060 0.007 0.614 0.127 0.141 0.001 0.028 0.048 0.076 2.207 64.524 0.153 0.036 2.609 0.65 0.489 0.008 0.109 0.387 0.163 6.178 0.213 0.043 3.223 0.777 0.630 0.009 0.137 0.435 0.239 8.385 36 34 1 1338 267 15 374 89 1 2498 1 1 178 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Harry Sharpe Owner: Iris Sharpe Predominant Soil Series: NaB Acres Used: 9.34 Acres Permitted: 9.34 Site #: RCO11 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.76 0.52 Arsenic 0.030 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Cadmium 0.004 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.272 0.277 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.548 Chromium 0.056 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.113 Lead 0.068 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.009 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 denum Nickel 0.019 0.023 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Selenium 0.035 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.068 Zinc 0.976 0.994 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.970 Total Phos- 25.806 30.444 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 56.250 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Iris Sharpe Operator: Harry Sharpe WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 11.91 Site #: Predominant Soil Series: NaB Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 178 Crop 2 Name: Acres Utilized: 9.34 RCO11 Acres Permitted: 9.34 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)�• Precip. Past 24 His. inches F '5 w o 7� co * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/4 78000 2.18 0.759 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 1 234 9.040 NA Fescue 10/22 91000 0.988 0.401 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 11.105 NA Fescue 10/23 26000 0.988 0.115 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 3.173 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o t9s000 As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 23.318 0.00o Lime Applied Annuallbs/acre 0.055 0.007 0.548 0.113 0.129 0.002 0.023 0.042 0.068 1.970 56.250 0.007 0.004 0.29 0.073 0.049 0.001 0.012 0.039 0.009 0.656 0.062 0.011 0.838 0.186 0.178 0.003 0.035 0.081 0.077 2.626 36 34 1 1338 267 15 374 89 1 2498 1 1 178 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 9.91 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Harry Sharpe Owner: Lawrence McCollum Predominant Soil Series: CgB2 Acres Used: 8.95 Acres Permitted: 8.95 Site #: RC012 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.11 Arsenic 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.593 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.593 Chromiuni 0.124 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.124 Lead 0.129 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030 denum Nickel 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Selenium 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Zinc 2.132 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.132 Total Phos- 65.313 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 65.313 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Lawrence McCollum Operator: Harry Sharpe Crop 1 Name: Fescue -Hay WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 9.91 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 8.95 RC012 Acres Permitted: 8.95 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 His. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/23 104000 0.988 0.479 Reidsville WWTP Dry <.5" S 0.5 1 0.3 27900 24400 582 13.244 NA Fescue 10/24 136500 0.988 0.628 Reidsville WWTP Dry <.5" S 0.5 0.3 27900 24400 582 17.383 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 24050o As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 30.627 o.000 Lime Applied Annuallbs/acre 0.053 0.006 0.593 0.124 0.129 0.001 0.030 0.049 0.071 2.132 65.313 0.123 0.033 2.363 0.579 0.442 0.01 0.101 0.371 0.153 5.849 0.176 0.039 2.956 0.703 0.571 0.011 0.131 0.420 0.224 7.981 1 36 34 1 1338 267 15 374 89 1 2498 1 209 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: Acres Used: 11.09 Acres Permitted: 11.09 Site #: RC041 Field #: 14.18 CaD 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date M1111m mammon Non no 0 Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 1 C 11 12 DT/Ac./ App. Event 1.28 Arsenic 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.458 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.458 Chromium 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Lead 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 denum Nickel 0.032 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.032 Selenium 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.060 Zinc 1.645 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.645 Total Phos- 43.486 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 43.486 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: Lofton Lovelace Annual Dry Tons Applied: 14.18 Site #: RC041 Acres Permitted: Donald Lovelace Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 150 CaD Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 11.09 11.09 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/15 26000 2.18 0.213 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 2.538 NA Fescue 6/8 91000 2.18 0.746 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 8.883 NA Fescue 6/9 39000 2.18 0.320 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 3.807 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o is6000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 15.227 F 0. 000 Lime Applied Annuallbs/acre 0.051 0.006 0.458 0.094 0.115 0.002 0.016 0.032 0.060 1.645 43.486 20.215 21.860 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.283 0.253 10.586 1.36 2.32 0.05 0.52 1.526 0.383 Current Cumulative lbs/ac 0.334 0.259 11.044 1.454 2.435 0.052 0.536 1.558 0.443 Permitted C. P. L. R. * * * * 1 36 34 1 1338 267 1 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 1 150 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 34.86 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: CgB2 Acres Used: 17.2 Acres Permitted: 17.2 Site #: RC041 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 2.03 Arsenic 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.726 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.726 Chromiuni 0.149 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.149 Lead 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.183 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 denum Nickel 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Selenium 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Zinc 2.607 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.607 Total Phos- 68.918 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.918 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Lofton Lovelace Operator: Donald Lovelace Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 34.86 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 17.2 RC041 Acres Permitted: 17.2 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/14 149500 2.18 0.790 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 9.409 NA Fescue 5/15 13000 2.18 0.069 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 0.818 NA Fescue 6/9 91000 2.18 0.481 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 5.727 NA Fescue 6/10 130000 2.18 0.687 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 8.182 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 383500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 24.136 0.000 Lime Applied Annuallbs/acre 0.081 0.010 0.726 0.149 0.183 0.003 0.025 0.051 0.094 2.607 68.918 0.286 0.272 11.243 2.041 2.238 0.054 0.544 1.541 0.391 22.059 0.367 0.282 11.969 2.190 2.421 0.057 0.569 1.592 0.485 24.666 36 34 1338 1 267 15 1 1 374 1 89 1 2498 209 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 38.40 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 22.6 Acres Permitted: 22.6 Site #: RC 119 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.70 Arsenic 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.068 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.608 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.608 Chromiuni 0.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.125 Lead 0.153 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.153 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Selenium 0.079 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.079 Zinc 2.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.185 Total Phos- 57.766 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 57.766 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 38.40 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 22.6 RC119 Acres Permitted: 22.6 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/23 136500 2.18 0.549 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 6.538 NA Fescue 6/24 175500 2.18 0.706 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 8.406 NA Fescue 6/25 58500 2.18 0.235 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 2.802 NA Fescue 6/26 52000 2.18 0.209 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 2.491 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 422500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.237 0.000 Lime Applied Annuallbs/acre 0.068 0.008 0.608 0.125 0.153 0.003 0.021 0.042 0.079 2.185 57.766 43.619 45.804 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.451 0.381 25.548 1.304 4.551 0.141 1.051 4.008 0.653 Current Cumulative lbs/ac 0.519 0.389 26.156 1.429 4.704 0.144 1.072 4.050 0.732 Permitted C. P. L. R. * * * * 36 1 34 1338 1 267 15 1 1 374 1 89 Permit PAN Limit 1 st/2nd Crop 156 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 11.23 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 6.47 Acres Permitted: 6.47 Site #: RC119 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.74 Arsenic 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.069 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.621 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.621 Chromiuni 0.127 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.127 Lead 0.156 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.156 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043 Selenium 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Zinc 2.231 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.231 Total Phos- 58.990 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 58.990 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 11.23 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 6.47 RC119 Acres Permitted: 6.47 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/26 78000 2.18 1.096 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 13.050 NA Fescue 6/27 45500 2.18 0.639 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 7.613 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 123500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.663 FO.000 Lime Applied Annuallbs/acre 0.069 0.008 0.621 0.127 0.156 0.003 0.021 0.043 0.081 2.231 58.990 44.219 46.450 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.506 0.369 25.595 1.551 4.573 0.153 0.991 3.922 0.691 Current Cumulative lbs/ac 0.575 0.377 26.216 1.678 4.729 0.156 1.012 3.965 0.772 Permitted C. P. L. R. * * * * 36 1 34 1338 1 267 15 1 374 1 89 Permit PAN Limit 1 st/2nd Crop 156 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 9.79 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 20.14 Acres Permitted: 20.14 Site #: RC119 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.09 0.40 Arsenic 0.004 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Cadmium 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.032 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062 Chromiuni 0.006 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030 Lead 0.008 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.001 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 denum Nickel 0.002 0.012 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Selenium 0.004 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.036 Zinc 0.113 0.804 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.917 Total Phos- 2.992 10.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 13.022 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 9.79 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 20.14 RC119 Acres Permitted: 20.14 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)�• Precip. Past 24 Hrs. inches F '5 w o 7� co * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/12 19500 2.18 0.088 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 1.048 NA Fescue 7/2 84500 0.779 0.136 Reidsviile WWTP Dry <.5" S 0.5 0.3 27800 15300 625 3.278 NA Fescue 7/3 162500 0.779 0.262 Reidsviile WWTP Dry <.5" S 0.5 0.3 27800 15300 625 6.304 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 266500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 10.629T 0.000 Lime Applied Annuallbs/acre 0.027 0.002 0.062 0.030 0.026 0.000 0.015 0.014 0.036 0.917 13.022 0.373 0.336 22.678 0.98 3.932 0.14 0.901 3.627 0.581 38.368 0.400 0.338 22.740 1.010 3.958 0.140 0.916 3.641 0.617 39.285 36 1 34 1338 1 267 15 1 374 1 89 1 2498 156 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 6.97 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 9.29 Acres Permitted: 9.29 Site #: RC 119 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date 01111m mammon Non no 0 Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 1 C 11 12 DT/Ac./ App. Event 0.75 Arsenic 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Chromium 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Lead 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 denum Nickel 0.023 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.023 Selenium 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Zinc 1.515 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.515 Total Phos- 18.900 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 18.900 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 6.97 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 9.29 RC119 Acres Permitted: 9.29 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)*• Precip. Past 24 Hrs. inches F '5 w o 7� co * N o TKN mg/kg 27800 o mg/kg 1 15300 Nitrate and Nitrite mg/kg 625 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/1 214500 0.779 0.750 Reidsviile WWTP Dry <.5" S 0.5 0.3 18.038 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 214500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 18.038 0.000 Lime Applied Annuallbs/acre 0.045 0.004 0.058 0.044 0.034 0.001 0.025 0.023 0.060 1.515 18.900 0.463 0.32 16.336 2.193 3.144 0.095 0.681 2.15 0.587 34.641 0.508 0.324 16.394 2.237 3.178 0.096 0.706 2.173 0.647 36.156 1 36 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 1 1 156 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 11.22 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 9.81 Acres Permitted: 9.81 Site #: RC 119 Field #: 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.14 Arsenic 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.410 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.410 Chromiuni 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Lead 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Nickel 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Selenium 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Zinc 1.471 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.471 Total Phos- 38.896 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 38.896 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 11.22 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 9.81 RC119 Acres Permitted: 9.81 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5L C) w * o o' * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/16 123500 2.18 1.144 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 13.628 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 123500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 13.628 FO.000 Lime Applied Annuallbs/acre 0.046 0.005 0.410 0.084 0.103 0.002 0.014 0.029 0.053 1.471 38.896 0.188 0.087 6.023 1.407 1.05 0.034 0.234 0.819 0.236 13.363 0.234 0.092 6.433 1.491 1.153 0.036 0.248 0.848 0.289 14.834 36 1 34 1338 1 267 15 1 374 1 89 1 2498 1 156 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 5.49 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 6.52 Acres Permitted: 6.52 Site #: RC 119 Field #: 10 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Bonn MENWEEME NUMEMENOMEM Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.84 Arsenic 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Chromiuni 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Lead 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 denum Nickel 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Selenium 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Zinc 1.701 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.701 Total Phos- 21.218 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 21.218 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 5.49 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: 10 Acres Utilized: 6.52 RC119 Acres Permitted: 6.52 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)�• Precip. Past 24 Hrs. inches F '5 w o 7� co * N * w o TKN mg/kg 27800 o mg/kg 1 15300 Nitrate and Nitrite mg/kg 625 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/1 13000 0.779 0.065 Reidsviile WWTP Dry <.5" S 0.5 0.3 1.558 NA Fescue 7/2 156000 0.779 0.777 Reidsviile WWTP Dry <.5" S 0.5 0.3 27800 15300 625 18.692 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o i69000 As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 20.250 o.000 Lime Applied Annuallbs/acre 0.051 0.004 0.065 0.050 0.038 0.001 0.028 0.025 0.067 1.701 21.218 8.443 10.144 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.149 0.046 2.598 0.927 0.505 0.031 0.152 0.523 0.122 Current Cumulative lbs/ac 0.200 0.050 2.663 0.977 0.543 0.032 0.180 0.548 0.189 Permitted C. P. L. R. * * * * 1 3 1 34 1 1338 1 267 15 1 1 374 89 Permit PAN Limit 1 st/2nd Crop 1 156 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): 10.64 Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 19.92 Acres Permitted: 19.92 Site #: RC119 Field #: 11 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.53 Arsenic 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.191 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.191 Chromiuni 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 Lead 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 denum Nickel 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Zinc 0.687 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.687 Total Phos- 18.156 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 18.156 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Thomas Carter Operator: Thomas Carter Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 10.64 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 156 Crop 2 Name: 11 Acres Utilized: 19.92 RC119 Acres Permitted: 19.92 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/27 117000 2.18 0.534 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 6.358 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 117000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 6_3 5 8T 0.000 Lime Applied Annuallbs/acre 0.021 0.003 0.191 0.039 0.048 0.001 0.007 0.013 0.025 0.687 18.156 0.089 0.025 1.773 0.732 0.257 0.014 0.097 0.392 0.057 5.005 0.110 0.028 1.964 0.771 0.305 0.015 0.104 0.405 0.082 5.692 36 1 34 1338 1 267 15 1 374 1 89 1 2498 1 156 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 2.32 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: NaB Acres Used: 2.79 Acres Permitted: 2.79 Site #: RC119 Field #: 12 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Bonn MENWEEME NUMEMBEEMEM Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.83 Arsenic 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Chromium 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Lead 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 denum Nickel 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Selenium 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Zinc 1.681 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.681 Total Phos- 20.966 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.966 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville WQ Permit #: WQ0002376 Field #: 12 Acres Utilized: Thomas Carter Annual Dry Tons Applied: 2.32 Site #: RC119 Acres Permitted: Thomas Carter Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 133.5 NaB Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 2.79 2.79 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)*• Precip. Past 24 Hrs. inches a F '5 w o 7� co * N o TKN mg/kg 27800 o mg/kg 15300 Nitrate and Nitrite mg/kg 625 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/2 71500 0.779 0.832 Reidsviile WWTP Dry <.5" S 0.5 0.3 20.021 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 7t5oo As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.021 o.000 Lime Applied Annuallbs/acre 0.050 0.004 0.065 0.049 0.037 0.001 0.028 0.025 0.067 1.681 20.966 0.136 0.073 4.095 0.859 0.535 0.018 0.197 0.886 0.105 9.628 0.186 0.077 4.160 0.908 0.572 0.019 0.225 0.911 0.172 11.309 36 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 1 1 133.5 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 8.86 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Gene Small Owner: Harvery Albert Predominant Soil Series: NaB Acres Used: 9.24 Acres Permitted: 9.24 Site #: RC 125 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phoms Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.96 Arsenic 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.343 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.343 Chromium 0.070 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.070 Lead 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 denum Nickel 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Selenium 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Zinc 1.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.233 Total Phos- 32.606 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.606 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Harvery Albert Operator: Gene Small WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 8.86 Site #: Predominant Soil Series: NaB Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 178 Crop 2 Name: 4 Acres Utilized: 9.24 RC125 Acres Permitted: 9.24 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/13 97500 2.18 0.959 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 1 234 11.423 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 11.423 0.000 Lime Applied Annuallbs/acre 0.038 0.005 0.343 0.070 0.087 0.002 0.012 0.024 0.045 1.233 32.606 0.119 0.034 2.759 0.644 0.667 0.032 0.1 0.358 0.146 8 0.157 0.039 3.102 0.714 0.754 0.034 0.112 0.382 0.191 9.233 1 36 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 1 1 178 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 8.67 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Auman French Owner: State of N.C. Predominant Soil Series: CgB2 Acres Used: 18.33 Acres Permitted: 18.33 Site #: RC126 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.22 0.26 Arsenic 0.030 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Cadmium 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.024 0.092 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Chromiuni 0.014 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 Lead 0.011 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.009 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 denum Nickel 0.012 0.006 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Selenium 0.035 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.047 Zinc 0.093 0.332 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.425 Total Phos- 5.547 8.772 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.319 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville State of N.C. Operator: Auman French Crop 1 Name: Fescue -Hay WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 8.67 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 18.33 RC126 Acres Permitted: 18.33 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 3/29 39000 0.56 0.050 Reidsville WWTP Dry <.5" S 0.5 1 0.3 63000 27000 833 2.497 NA Fescue 3/30 104000 0.56 0.132 Reidsville WWTP Dry <.5" S 0.5 0.3 63000 27000 833 6.660 NA Fescue 3/31 26000 0.56 0.033 Reidsville WWTP Dry <.5" S 0.5 0.3 63000 27000 833 1.665 NA Fescue 4/2 52000 2.18 0.258 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 3.071 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 0 22t000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 13.893 0.000 Lime Applied Annuallbs/acre 0.040 0.005 0.116 0.033 0.034 0.001 0.013 0.018 0.047 0.425 14.319 11.863 12.288 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0.223 0.057 3.884 1.12 1.115 0.025 0.175 0.607 0.274 2000 Current Cumulative lbs/ac 0.263 0.062 4.000 1.153 1.149 0.026 0.188 0.625 0.321 Permitted C. P. L. R. * * * * 1 36 34 1 1338 267 1 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 209 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 11.82 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Auman French Owner: State of N.C. Predominant Soil Series: CgB2 Acres Used: 10.8 Acres Permitted: 10.8 Site #: RC 126 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.09 Arsenic 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.392 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.392 Chromiuni 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080 Lead 0.099 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Nickel 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Selenium 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Zinc 1.407 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.407 Total Phos- 37.196 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 37.196 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Reidsville Land Owner: State of N.C. Operator: Auman French Crop 1 Name: Coral WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 11.82 Site #: Predominant Soil Series: C:;B2 Crop 1 Max. PAN: 130 Crop 2 Name: Acres Utilized: 10.8 RC126 Acres Permitted: 10.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/2 65000 2.18 0.547 Reidsville WWTP Dry <.5" S 0.5 1 0.3 12000 10600 234 6.515 NA Corn 4/3 65000 2.18 0.547 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 6.515 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: o t30000 As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 13.030 o.000 Lime Applied Annuallbs/acre 0.044 0.005 0.392 0.080 0.099 0.002 0.014 0.027 0.051 1.407 37.196 0.223 0.057 3.884 1.12 1.115 0.025 0.175 0.607 0.274 11.863 0.267 0.062 4.276 1.200 1.214 0.027 0.189 0.634 0.325 13.270 1 36 34 1 1338 267 15 374 89 1 2498 1 130 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Dennis Williams Owner: Dennis Williams Predominant Soil Series: 14.66 Acres Permitted: 14.66 Site #: RC 128 Field #: 21.18 CdB2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 1.33 0.12 Arsenic 0.053 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 Cadmium 0.006 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.476 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.485 Chromiuni 0.098 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Lead 0.120 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.125 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.016 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Nickel 0.033 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Selenium 0.062 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Zinc 1.710 0.232 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.943 Total Phos- 45.220 2.898 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 48.118 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: Dennis Williams Annual Dry Tons Applied: 21.18 Site #: RC128 Acres Permitted: Dennis Williams Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 156 CdB2 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 14.66 14.66 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)�• Precip. Past 24 11rs. inches a F '5 w o 7� co * N * w o TKN mg/kg 12000 o mg/kg 10600 Nitrate and Nitrite mg/kg 234 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 6/30 214500 2.18 1.330 Reidsviile WWTP Dry <.5" S 0.5 0.3 15.839 NA Fescue 7/1 52000 0.779 0.115 Reidsviile WWTP Dry <.5" S 0.5 0.3 27800 15300 625 2.771 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 26650o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 18.610 o.000 Lime Applied Annuallbs/acre 0.060 0.007 0.485 0.104 0.125 0.002 0.020 0.037 0.071 1.943 48.118 0.027 0.012 0.771 0.165 0.114 0.005 0.039 0.113 0.027 2.231 0.087 0.019 1.256 0.269 0.239 0.007 0.059 0.150 0.098 4.174 36 34 1 1338 267 15 374 1 89 1 2498 1 1 156 Date lbs/ac Prior Years Cumulative lbs/ac 2000 Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Ken Martin Owner: Ken Martin Predominant Soil Series: Acres Used: 39.24 Acres Permitted: 39.24 Site #: RC130 Field #: 20.09 CmB 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.51 Arsenic 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.183 Chromiuni 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Lead 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.046 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 denum Nickel 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Selenium 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Zinc 0.658 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.658 Total Phos- 17.408 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 17.408 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 4; 2/8/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. City of Reidsville Ken Martin Operator: Ken Martin WQ Permit #: WQ0002376 Field #: Annual Dry Tons Applied: 20.09 Site #: Predominant Soil Series: CmB Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 146 Crop 2 Name: Acres Utilized: 39.24 RC130 Acres Permitted: 39.24 Cation Exchange Capacity (non 503): 0 Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/3 188500 2.18 0.437 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 1 234 5.200 NA Fescue 4/4 32500 2.18 0.075 Reidsville WWTP Dry <.5" S 0.5 0.3 12000 10600 234 0.897 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 22t000 As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 6.097 o.000 Lime Applied Annuallbs/acre 0.020 0.002 0.183 0.038 0.046 0.001 0.006 0.013 0.024 0.658 17.408 0.243 0.078 6.369 1.731 1.274 0.034 0.261 0.917 0.303 16.554 0.263 0.080 6.552 1.769 1.320 0.035 0.267 0.930 0.327 17.212 36 34 1 1338 267 15 374 89 1 2498 1 1 146 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/8/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Waypointo ANALYTICAL 1 /22/2020 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-010-0057 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TIN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 1/10/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Alabama #40750 Louisiana #04015 Mississippi California #2904 Kentucky #90047 Tennessee #TN02027 VA NELAP #460181 NC #415 EPA #TN00012 Texas #T104704180 Arkansas #88-0650 Oklahoma #9311 SC #84002 Kentucky UST #80215 PA DEP #68-03195 Page 1 of 7 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-010-0057 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 92901 Reidsville Solids 01/09/202011:30 01/10/2020 Page 2 of 7 Waypoint ANALYTICAL Client: EMA Resources Inc Project: Reidsville, NC Lab Report Number: 20-010-0057 Date: 1 /22/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 92916 Analyte: Aluminum QC Batch No: L472729 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 3 of 7 i Wa2790 Whitten Road, Memphis, TN 38133 ypoint.Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Mr. Brent Collins Project Reidsville, NC Report Date : 01/22/2020 755 Yadkinville Road Information : Received : 01/10/2020 Mocksville , NC 27028 Report Number : 20-010-0057 REPORT OFANALYSIS Danyale Love Project Manager Lab No : 92901 Matrix: Solids Sample ID : Reidsville Sampled: 1/9/2020 11:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 99.4 % 0.010 1 01/13/20 16:26 ADM SW-DRYWT Ammonia Nitrogen 27000 mg/Kg - dry 4170 1 01/21/20 14:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <833 mg/Kg - dry 833 833 1 01/20/20 16:09 ZBD 4500NO3F-2011 Organic N 36000 mg/Kg - dry 270.0 13530 1 01/14/20 16:15 CALCULATION pH 6.8 S.U. 1 01/21/20 05:24 JSL 9045D Total Solids 0.560 % 0.010 0.010 1 01/13/20 16:26 ADM 2540G-2011 Total Volatile Solids 66.3 % 0.010 0.010 1 01/13/20 16:26 ADM 2540G-2011 Total Kjeldahl Nitrogen 63000 mg/Kg - dry 270 13500 1 01/14/20 16:15 CLP 4500NORGD-2011 Phosphorus 12900 mg/Kg - dry 428 833 1 01/14/20 02:18 BKN 6010D Aluminum 3470 mg/Kg - dry 338 833 1 01/14/20 02:18 BKN 6010D Arsenic <69.8 mg/Kg - dry 69.8 83.3 1 01/14/20 02:18 BKN 6010D Cadmium <8.25 mg/Kg - dry 8.25 16.7 1 01/14/20 02:18 BKN 6010D Calcium 6320 mg/Kg - dry 2800 4170 1 01/14/20 02:18 BKN 6010D Chromium <31.7 mg/Kg - dry 31.7 41.7 1 01/14/20 02:18 BKN 6010D Copper 54.8 mg/Kg - dry 24.2 41.7 1 01/14/20 02:18 BKN 6010D Iron 2970 mg/Kg - dry 707 833 1 01/14/20 02:18 BKN 6010D Lead <24.8 mg/Kg - dry 24.8 50.0 1 01/14/20 02:18 BKN 6010D Magnesium 3330 mg/Kg - dry 370 833 1 01/14/20 02:18 BKN 6010D Manganese 172 mg/Kg - dry 30.5 83.3 1 01/14/20 02:18 BKN 6010D Mercury <0.528 mg/Kg - dry 0.528 2.40 1 01/15/20 16:17 TJS 7471A Molybdenum <21.7 mg/Kg - dry 21.7 41.7 1 01/14/20 02:18 BKN 6010D Nickel <27.5 mg/Kg - dry 27.5 41.7 1 01/14/20 02:18 BKN 6010D Potassium 9770 mg/Kg - dry 497 833 1 01/14/20 02:18 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 i Waypoint. ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville , NC 27028 Report Number : 20-010-0057 Lab No : 92901 Sample ID : Reidsville 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Project Reidsville, NC Information : REPORT OFANALYSIS Report Date : 01/22/2020 Received : 01/10/2020 Danyale Love Project Manager Matrix: Solids Sampled: 1/9/2020 11:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Selenium <81.7 mg/Kg - dry 81.7 83.3 1 01/14/20 02:18 BKN 6010D Sodium 24500 mg/Kg - dry 1290 4170 1 01/14/20 02:18 BKN 6010D Zinc 217 mg/Kg - dry 180 208 1 01/14/20 02:18 BKN 6010D Sulfur 1980 mg/Kg - dry 815 833 1 01/14/20 02:18 BKN 6010D Sodium Absorption Ratio 4.80 Ratio 2.22 5.00 1 01/14/20 02:18 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded Page 5 of 7 • WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 9fl1.213.2400 °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-010-0057 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: #70 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: rRory Phillips Date & Time: 01/10/2020 10:47:20 Page 6 of 7 Client Narne/Address Client Project Manager/Contact Billing Information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadklnville Rd Mocksville, NC 27028 Project Description Project/Site Location (City/State) RUSH — Additional charges apply Method of Shipment Matrix Key Special Detection Limit(s) Fed Ex nUPS OU5PS WW — Wastewater GW — Groundwater //UcOther Date Results Needed Courier 0 Client Drop off DW — Drinking Water S —Sail /Solid 0 — OF p - Product M - Misc Project Number Project Manager Phone # Project Manager Email Purchase Order Number Site/Facia" ID # 336-399-3646 brent-collins@emaresources.com W A coo! c IGC Na25203 {Micro only} a r a © CD C U 8 Cool <m 6c Waypoint T _ C gIu2 ANALYTICAL r c Y 2 as E CD to ❑ W None ❑ None Required E NaOH pH510 2790 Whitten Road Unless noted, all containers p w a is V7 Q Z T V J F HNO3 pHc2 G HCL pHQ Memphis. IN 38133 p H H3PO4 (901 ) 213.2400 per Table 11 of 40 CFR Part ; E x n m Q] Y ;_ Z O ••^L• Y..i. pii<2 ! Cool r- 6c NA25243 135- Date Time sample Identification Required Analysis / Preservative Comments/Notes Ig �I.3A r ds,,; If Metals:AI,As,Ca,Cd,Cr,Cu,Fe,Pb M n,M9, Mo, Hg, Ni,Se,Na, P,S, K,Zn 17 a-01"57 oz�5oz� Ill��1�111111�1�lllll�ltll111�111t�11ti1111� t���ll�tll�ll EMA f�esnurc+'s Inc Relds,ile. NC 11177 For Laboratory Use Only Sampled by (Name - Print) � Client Remarks/Comments Sludge Samples - Report Dry Weight ICE Custody lsLab Comments / N Rel9nqu d by: (SIGNATURE) Date Time Received by: [SIGNATUREI Date Time y ,/y x-,O-ear 131a Cooler Tem Relinquished by: (S$GNATURE) Date Time Reces d by: 61 NATUR£I Date Time U Relinquished by: [SIGNATURE) Date Time Rec ed (SIG URE) as e �TI 0(6: a Page 7 of 7 Waypointo ANALYTICAL 4/15/2020 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-094-0100 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 4/3/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 2/28/2021 Arizona State Program AZ0816 8/30/2020 Arkansas State Program 88-0650 2/7/2021 California State Program 2904 5/10/2020 Georgia State Program C044 2/18/2023 Georgia State Program 04015 6/30/2020 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 6/30/2020 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP 04015 6/30/2020 Mississippi State Program MS 5/10/2020 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 8/31/2020 Pennsylvania State Program - NELAP 68-03195 5/31/2020 South Carolina State Program 84002 5/10/2020 South Carolina State Program 84002 6/30/2020 Tennessee State Program 02027 2/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 9/30/2020 Virginia State Program - NELAP 460181 9/14/2020 Washington State Program C1018 7/31/2020 Page 1 of 1 00001/20-094-0100 Page 2 of 9 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-094-0100 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 86361 Reidsville Solids 04/02/2020 09:15 04/03/2020 Page 3 of 9 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Reidsville, NC Lab Report Number: 20-094-0100 Date: 4/15/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Analyte: Aluminum QC Batch No: L486301 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L486116 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Copper QC Batch No: L486116 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Iron QC Batch No: L486301 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L486116 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Potassium QC Batch No: L486301 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Manganese QC Batch No: L486301 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L486116 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Lead QC Batch No: L486116 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 4 of 9 Waypoint".0 - ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com Solids Total Mercury Analysis - CVAA Method 7471A Analyte: Mercury QC Batch No: L485965 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 WayP �'��' 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Mr. Brent Collins Project Reidsville, NC Report Date : 04/15/2020 755 Yadkinville Road Information : Received : 04/03/2020 Mocksville , NC 27028 Q�ln Report Number : 20-094-0100 REPORT OFANALYSIS Danyale Love Project Manager Lab No : 86361 Matrix: Solids Sample ID : Reidsville Sampled: 4/2/2020 9:15 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 97.9 % 1 04/06/2015:35 JDT SW-DRYWT Ammonia Nitrogen 10600 mg/Kg - dry 1190 1 04/15/20 12:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <234 mg/Kg - dry 234 234 1 04/07/20 13:22 ZBD 4500NO3F-2011 Organic N 1381 mg/Kg - dry 47.62 2381 1 04/13/20 16:38 CALCULATION pH 6.9 S.U. 1 04/13/20 05:39 JSL 9045D Total Solids 2.18 % 0.010 0.010 1 04/06/20 15:49 ADM 2540G-2011 Total Volatile Solids 74.2 % 0.010 0.010 1 04/06/20 15:49 ADM 2540G-2011 Total Kjeldahl Nitrogen 12000 mg/Kg - dry 47.6 2380 1 04/13/20 16:38 CLP 4500NORGD-2011 Phosphorus 17000 mg/Kg - dry 122 238 1 04/07/20 19:35 KKM 6010D Aluminum 14500 mg/Kg - dry 96.7 238 1 04/07/20 19:35 TJS 6010D Arsenic <20.0 mg/Kg - dry 20.0 23.8 1 04/07/20 19:35 KKM 6010D Cadmium <2.36 mg/Kg - dry 2.36 4.76 1 04/07/20 19:35 KKM 6010D Calcium 9670 mg/Kg - dry 800 1190 1 04/07/20 19:35 KKM 6010D Chromium 36.7 mg/Kg - dry 9.05 11.9 1 04/07/20 19:35 KKM 6010D Copper 179 mg/Kg - dry 6.90 11.9 1 04/07/20 19:35 KKM 6010D Iron 9710 mg/Kg - dry 202 238 1 04/07/20 19:35 TJS 6010D Lead 45.1 mg/Kg - dry 7.10 14.3 1 04/07/20 19:35 KKM 6010D Magnesium 3300 mg/Kg - dry 106 238 1 04/07/20 19:35 KKM 6010D Manganese 452 mg/Kg - dry 8.71 23.8 1 04/07/20 19:35 TJS 6010D Mercury 0.814 mg/Kg - dry 0.164 0.743 1 04/07/20 12:51 DDB 7471A Molybdenum <6.19 mg/Kg - dry 6.19 11.9 1 04/07/20 19:35 KKM 6010D Nickel 12.5 mg/Kg - dry 7.86 11.9 1 04/07/20 19:35 KKM 6010D Potassium 3840 mg/Kg - dry 142 238 1 04/07/20 19:35 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 6 of 9 waypANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville , NC 27028 Report Number : 20-094-0100 Lab No : 86361 Sample ID : Reidsville 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Project Reidsville, NC Information : REPORT OFANALYSIS Report Date : 04/15/2020 Received : 04/03/2020 Danyale Love Project Manager Matrix: Solids Sampled: 4/2/2020 9:15 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Selenium <23.3 mg/Kg - dry 23.3 23.8 1 04/07/20 19:35 KKM 6010D Sodium 5190 mg/Kg - dry 368 1190 1 04/07/20 19:35 KKM 6010D Zinc 643 mg/Kg - dry 51.4 59.5 1 04/07/20 19:35 KKM 6010D Sulfur 8480 mg/Kg - dry 233 238 1 04/07/20 19:35 KKM 6010D Sodium Absorption Ratio <2.22 Ratio 2.22 5.00 1 04/07/20 19:35 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded Page 7 of 9 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-094-0100 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: #56 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: ory Phillips Date & Time: 04/03/2020 12:36:24 Page 8 of 9 Client Name/Address Client Project Manager/Contact Bilking information For Laboratory Use Only EMA Resources Inc gent Collins Account #46245 755 Yadkii Rd Moi iilc. NC 27028 Project Description Project/Site Location (City/State) RUSH - Additional charges apply Method of Shipment Matrix Key Special Detection Limit(s) r_-41ed Ex UPS �USPS W W -Wastewater GW - Groundwater it, /vc Date Results Needed ❑ Courier B Client Drop Off aW - Drinking Water S -- Soil /Solid O-0a P - Product M - Misc J Other project Number Project Manager Phone !I Project Manager Email Purchase Order Nurnber Site/Faclllt:y ID 9 336-399-3646 Brent.coHins@emaresources.cc)ni N A Cool < IDC Na2SIO3 (micro Only) [[�� W Y CD r O C B Cool t= 6C C H25O4 i oin a O E o� ❑ ❑ None Required ANALYTICAL c $ EE ti o [J] W E HeOH p}tril] 2796 Whitten Road 11.1niess noted, all containers u a L `a �, � a M u F HNO3p}fs2 G H{t pHct Memphis. TN 38133 a Z � (901) 213-2400 Per Table €1 of 40 crR Part E i ^ H H3PO4 pi]36. I Caul c=6C NA25203 :Im L7 Hate riche Sample Identification RC WredAnalysis/Preservative Comments/Notes q1Z 9. ■�a„ JIG a ''Ix V�'- Meta1s:A1 As,Ca,Cd,Cr,Cu,Fe,Pb . d�v: Mn, Mg , Mo, Hg, N i, S e, N a . P,S, K, Zn '�lllltilllltilllll�ti111111ti11111ti11�111111�111111l11111111�It 1� o ��20 EMA Resources Inc Ill Reidsvd4e. NG For Laboratory Use Only Sampled by (Name - Print) Client RemarksJCornments Sludge Samples - Report Dry Weight Ice Custody Lab Comments 0 / N Seals F Z"-/ �II,�S Felinquls d by' [SlG TURF} Date Tune Received by: [SIGNATURE] Date Time �H� Y - `N . `1'/z 5. Blank/ onler T Relinquished by: (SIGNATURE) bate Time Rece4wA by: SIGNATURE) Date Time j� Relinquished by-. (SIGNATURE) Date Time R �edj: (5 IMIATUi Q it T me , t3 ; -c Q �L ul_�.a) Waypointo ANALYTICAL 7/31 /2020 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-204-0007 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 7/22/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arizona State Program AZ0816 08/30/2020 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 05/10/2020 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2020 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2020 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2020 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2020 Washington State Program C1018 07/31/2020 Page 1 of 1 00001/20-204-0007 Page 2 of 8 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-204-0007 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 93695 Reidsville Solids 07/21/202010:30 07/22/2020 Page 3 of 8 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Reidsville, NC Lab Report Number: 20-204-0007 Date: 7/31 /2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Solids Total Mercury Analysis - CVAA Method 7471A Sample 93987 Analyte: Mercury QC Batch No: L503343 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Waypointo ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-204-0007 Lab No : 93695 Sample ID : Reidsville Project Reidsville, NC Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 07/31/2020 Received : 07/22/2020 Danyale Love Project Manager Matrix: Solids Sampled: 7/21/2020 10:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 99.2 % 0.010 1 07/28/20 17:10 FMM SW-DRYWT Ammonia Nitrogen 15300 mg/Kg - dry 3130 3130 1 07/29/20 10:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <625 mg/Kg - dry 625 625 1 07/27/20 14:58 ZBD 4500NO3F-2011 Organic N 12500 mg/Kg - dry 6250 1 07/29/20 10:00 DH CALCULATION pH 7.4 S.U. 1 07/31/20 06:32 JSL 9045D Total Solids 0.779 % 0.010 0.010 1 07/28/20 17:10 FMM 2540G-2011 Total Volatile Solids 64.2 % 0.010 0.010 1 07/28/20 17:10 FMM 2540G-2011 Total Kjeldahl Nitrogen 27800 mg/Kg - dry 6250 1 07/30/20 15:31 CLP 4500NORGD-2011 Phosphorus 12600 mg/Kg - dry 345 625 1 07/24/20 00:22 TJS 6010D Aluminum 2990 mg/Kg - dry 578 625 1 07/24/20 16:29 TJS 6010D Arsenic <30.0 mg/Kg - dry 30.0 62.5 1 07/24/20 00:22 TJS 6010D Cadmium <2.50 mg/Kg - dry 2.50 12.5 1 07/24/20 00:22 TJS 6010D Calcium 48903 mg/Kg - dry 4840 6250 1 07/24/20 00:22 TJS 6010D Chromium <29.5 mg/Kg - dry 29.5 31.3 1 07/24/20 00:22 TJS 6010D Copper <38.8 mg/Kg - dry 38.8 62.5 1 07/24/20 00:22 TJS 6010D Iron 2760 mg/Kg - dry 1070 1250 1 07/24/20 16:29 TJS 6010D Lead <22.5 mg/Kg - dry 22.5 37.5 1 07/24/20 00:22 TJS 6010D Magnesium 2290 mg/Kg - dry 323 625 1 07/24/20 00:22 TJS 6010D Manganese 159 mg/Kg - dry 40.6 62.5 1 07/24/20 16:29 TJS 6010D Mercury <0.399 mg/Kg - dry 0.399 1.81 1 07/27/20 12:28 DDB 7471A Molybdenum <16.9 mg/Kg - dry 16.9 31.3 1 07/24/20 00:22 TJS 6010D Nickel <15.0 mg/Kg - dry 15.0 31.3 1 07/24/20 00:22 TJS 6010D Potassium 6640 mg/Kg - dry 773 1250 1 07/24/20 00:22 TJS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 5 of 8 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Reidsville, NC Brent Collins Report Date : 07/31/2020 755 Yadkinville Rd Information : Received : 07/22/2020 Mocksville , NC 27028 Danyale Love Report Number : 20-204-0007 REPORT OFANALYSIS Project Manager Lab No : 93695 Matrix: Solids Sample ID : Reidsville Sampled: 7/21/2020 10:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <40.0 mg/Kg - dry 40.0 62.5 1 07/24/20 00:22 TJS 6010D Sodium 8800 mg/Kg - dry 1630 3130 1 07/24/20 00:22 TJS 6010D Zinc <101 mg/Kg - dry 101 156 1 07/24/20 00:22 TJS 6010D Sulfur 1810 mg/Kg - dry 648 1250 1 07/24/20 00:22 TJS 6010D Sodium Absorption Ratio 2.323 Ratio 0.01 0.01 1 07/24/20 00:22 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 6 of 8 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-204-0007 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: #101 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: lKristinaA. McAdams Date & Time: 07/22/2020 10:53:35 Page 7 of 8 Client Name/Address Client Project Manager/Contact Billing Information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadkinville Rd Mocksville, NC 27028 Project Description Project/Site Location (city/State) RUSH - Additional charges apply Method of Shipment Matrix Key Special Detection Limits) EFed Ex F UPS OusPs WW - Wastewater GW- Groundwater Date Results Needed Courier M Client Drop off DW -- Drinking Water 5 -Soil /Solid O - oil P Product M - Misc other Project Number Project Manager Phone p Project Manager Email Purchase Order Number Site/Facility ID # 336-399-3646 Ixent.collins@emaresources.com 4:'I5,,, f 1e- ❑ 2 Z 0 -0 A Cool t 1OC Na252O3 (Micro Only) • C U B Cool t= 6C T - Q Q C u2 Waypo�nt a E m cm ❑ ❑ None Required None ANALYTICAL c E: E 0 W E WCH pH>10 2794 Whitten Read Memphis. TN 38133 P Unless n rioted, all containers LJ ° ` a oc u o v7 � Q Z - m — M V J F HNO3 pHc2 HCL (901) 213 2400 per Table II of 40 CFR Part y E x m Ia H H3Pp4 PH�2 Cool <= 6C NA25203 135. 2 m ^2 Date Vine Sample Identification Required Analysis J Preservative Comments/Notes 7/11 1 �f�rl�� s� '� a/ ✓ ,/ Meta Is: Al, As, Ca, Cid, Cr,Cu,Fe, Pb Mn,Mg,Mo, Hg, Ni,Se,Na,P,S,K,Zn 111111Illllill1111illllll1111i11114111111111111111111IIIII14 45 EMA Resources Inc 10:53 23 Reidsville. NC For Laboratory Use Only Sampled by (Name-- Print) �I�s Client Remarks/Comments Sludge Samples - Report Dry Weight Ice Custody Lab Comments Seals N Y �� ] Relinqui ed by: IGNATURE] Date Time Received by: (SIGNATURE) Date Time 7IZI H:+gpl►+ Blank/ ooler T mp Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time LRelinquished Date Time Received by: (SIGNATURE) pate Time r by: (SIGNATURE) Waypointo ANALYTICAL 10/14/2020 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-276-0058 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 10/2/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/20-276-0058 Page 2 of 8 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-276-0058 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 99029 Reidsville Solids 10/01/202013:15 10/02/2020 Page 3 of 8 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Reidsville, NC Lab Report Number: 20-276-0058 Date: 10/14/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Sample 87699 Analyte: Aluminum QC Batch No: L516416 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L516416 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L516150 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Manganese QC Batch No: L516416 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Molybdenum QC Batch No: L516150 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Selenium QC Batch No: L516150 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Selenium QC Batch No: 1-516150/1-515796 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Sample 99029 (Reidsville) Analyte: Selenium QC Batch No: 1-516150/1-515796 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Page 4 of 8 Waypointo ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Road Mocksville , NC 27028 Report Number : 20-276-0058 Lab No : 99029 Sample ID : Reidsville Project Reidsville, NC Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 10/14/2020 Received : 10/02/2020 Danyale Love Project Manager Matrix: Solids Sampled: 10/ 1/ 2020 13:15 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 99.0 % 0.010 1 10/08/20 16:06 FMM SW-DRYWT Ammonia Nitrogen 24400 mg/Kg - dry 2500 2500 1 10/13/20 14:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 582 mg/Kg - dry 485 485 1 10/13/20 13:46 ZBD 4500NO3F-2011 Organic N 3500 mg/Kg - dry 2500 2500 1 10/08/20 14:49 CALCULATION pH 7.7 S.U. 1 10/05/2013:00 ADM 9045D Total Solids 0.988 % 0.010 0.010 1 10/08/20 16:06 FMM 2540G-2011 Total Volatile Solids 63.2 % 0.010 0.010 1 10/08/20 16:06 FMM 2540G-2011 Total Kjeldahl Nitrogen 27900 mg/Kg - dry 5000 1 10/08/20 14:49 CLP 4500NORGD-2011 Phosphorus 29500 mg/Kg - dry 276 500 1 10/12/20 20:06 TJS 6010D Aluminum 27100 mg/Kg - dry 462 500 1 10/12/20 20:06 TJS 6010D Arsenic <24.0 mg/Kg - dry 24.0 50.0 1 10/12/20 20:06 TJS 6010D Cadmium 2.913 mg/Kg - dry 2.00 10.0 1 10/12/20 20:06 TJS 6010D Calcium 19000 mg/Kg - dry 3870 5000 1 10/13/20 18:19 TJS 6010D Chromium 55.9 mg/Kg - dry 23.6 25.0 1 10/13/20 18:19 TJS 6010D Copper 268 mg/Kg - dry 31.0 50.0 1 10/12/20 20:06 TJS 6010D Iron 21100 mg/Kg - dry 852 1000 1 10/12/20 20:06 DADS 6010D Lead 58.3 mg/Kg - dry 18.0 30.0 1 10/12/20 20:06 TJS 6010D Magnesium 4640 mg/Kg - dry 258 500 1 10/12/20 20:06 TJS 6010D Manganese 1080 mg/Kg - dry 32.5 50.0 1 10/12/20 20:06 DADS 6010D Mercury <0.337 mg/Kg - dry 0.337 1.53 1 10/05/20 12:22 DDB 7471A Molybdenum <13.5 mg/Kg - dry 13.5 25.0 1 10/12/20 20:06 TJS 6010D Nickel 22.33 mg/Kg - dry 12.0 25.0 1 10/12/20 20:06 TJS 6010D Potassium 6190 mg/Kg - dry 618 1000 1 10/12/20 20:06 TJS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 5 of 8 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Reidsville, NC Mr. Brent Collins Report Date : 10/14/2020 755 Yadkinville Road Information : Received : 10/02/2020 Mocksville , NC 27028 Danyale Love Report Number : 20-276-0058 REPORT OFANALYSIS Project Manager Lab No : 99029 Matrix: Solids Sample ID : Reidsville Sampled: 10/1/2020 13:15 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <32.0 mg/Kg - dry 32.0 50.0 1 10/12/20 20:06 TJS 6010D Sodium 6750 mg/Kg - dry 1300 2500 1 10/13/20 18:19 TJS 6010D Zinc 963 mg/Kg - dry 81.0 125 1 10/12/20 20:06 TJS 6010D Sulfur 11600 mg/Kg - dry 518 1000 1 10/13/20 18:19 TJS 6010D Sodium Absorption Ratio 1.13 Ratio 0.01 0.01 1 10/12/20 20:06 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 6 of 8 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-276-0058 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: #99 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: ory Phillips Date & Time: 10/02/2020 11:13:58 Page 7 of 8 Client Name/Address Client Project Manager/Contact Billing Information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadicinville Rd Mocksville, NC 27028 Project Description Project/Site location (City/State) RUSH - Additional charges apply Method of Shipment Matrix Key Special Detection Limit(s) ID -Fed Ex �USPS WW -Wastewater GW - Groundwater s f,L�fr ljc I �l_d5v� �rL�N(-- Date Results Needed ®UPS Courier Client Drop OffDW - Drinking Water S -Soil /Solid 0 - Oil P- Product M -Misc Other Project Number Project Manager Phone q Project Manager Email Purchase Order Number Site/Facility ID # 336-399-3646 brent.coil ins@emaresources.corn r:4,-,_ If, A Cool < 10C Na25203 {Micro Onlyj e ° U _0 B Coot [= 6C Wa- Yp�MI�yTt�ru x o CJ o E ❑ C H2So4 pH[2 D None Required = y E P 0 r� � E NaOH pHa30 2790 Whitten Road Unless noted, all containers " w `o N f6 Q Z @ V J r F HNQ3 pH[2 G HCL pH[2 Memphis, I'N 38133 > V (901) 2I3.2400 per Table EI of 40 CFR Fart xJ3 0 H CootH3P< 6C N Coot = 0.25243 Y3fi. � � `- Date Time Sample Identification Required Analysis / Preservative Comments/Notes roll I:lSf,., rCr: ds� r!c I � y� C tir V Meta1s:ALAs,Ca.Cd.Cr,CU.Fe.Pb Mn,Mg,Mo,Hg,Ni,Se,Na,P.S,K.Zn IIII II Ill ICI Illill Illll IIIII IIII Ilia I Ill IIIII 11141111 III �2�flg EMA Resaurcea Inc.. 11 1327 Reidsviile, NC 1::H For Laboratory Use Only Sampled by (Name - Print) r�n� /ks Client Remarks/Comments Sludge Samples - Report Dry Weight Ice Custody seals Lab Comments / N Vy Relin fished by: SIGNATUREy Date Time Received by: (SIGNATURE) Date Time Y/r�i i 1d I .1No'" Blank/C Relinquished by: (SIGNATURE) Date Time Receiv by: NATURE) Date Time - k Relinquished by: (SIGNATURE) Date Time Rece ed y: (SI ATURE) Ti e F _ `Dlatei 1 V Z z, 'r J 03�S5 aceAnalytical National Center for Testing & Innovation AW ANALYTICAL REPORT January 20, 2020 EMA Resources Sample Delivery Group: L11771O3 Samples Received: 01/08/2020 Project Number: Description: Sludge Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By JJwkC4V1-- Justin Carr Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 1 of 23 TABLE OF CONTENTS ONE LAB. NATIONWIDE. * Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results REDSVILLE L1177103-01 Qc: Quality Control Summary Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E GI: Glossary of Terms al: Accreditations & Locations Sc: Sample Chain of Custody 1 2 3 4 5 5 7 7 9 10 11 12 13 15 17 18 19 21 22 23 ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1177103 01/20/20 14:21 PAGE: 2 of 23 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time REDSVILLE L1177103-01 Waste Brent Collins 01/07/2008:30 01/08/2009:00 t C P Method Batch Dilution Preparation Analysis Analyst date/time date/time Preparation by Method 1311 WG1408214 1 01/09/20 08:50 01/09/20 08:50 BAA Preparation by Method 1311 WG1408380 1 01/09/2012:02 01/09/2012:02 CGD Wet Chemistry by Method 9012 B WG1408346 1 01/10/20 08:52 01/13/2012:46 JER Wet Chemistry by Method 9034-9030B WG1408079 1 01/09/20 22:00 01/09/20 22:00 LDT Wet Chemistry by Method 9045D WG1408459 1 01/10/2015:00 01/11/2018:00 MSP Wet Chemistry by Method D93/1010A WG1412116 1 01/20/2010:15 01/20/2010:15 MJA Mercury by Method 7470A WG1408995 1 01/10/2010:30 01/13/20 09:49 ABL Metals (ICP) by Method 6010D WG1409034 1 01/11/2012:29 01/12/2015:33 CCE Volatile Organic Compounds (GC/MS) by Method 8260D WG1409088 1 01/12/20 23:09 01/12/20 23:09 BMB Chlorinated Acid Herbicides (GC) by Method 8151A WG1411034 1 01/14/2018:22 01/16/20 02:35 LEL Pesticides (GC) by Method 8081B WG1409135 1 01/12/2016:58 01/13/2013:24 HMH Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1409132 1 01/12/2018:00 01/13/20 05:24 AO Location FC Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fn Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fr Mt. Juliet, TN Mt. Juliet, TN FC Mt. Juliet, TN Mt. Juliet, TN �GI SAI RC ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1177103 01/20/20 14:21 PAGE: 3 of 23 CASE NARRATIVE ONE LAB. NATIONWIDE. * All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr FC GI Justin Carr [Al Project Manager RC Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 4 of 23 REDSVILLE Collected date/time: 01/07/20 08:30 Preparation by Method 1311 SAMPLE RESULTS - 01 L1177103 Result Qualifier Prep Batch Analyte date / time TCLP Extraction 1/9/202012:02:38 PM WG1408380 TCLP ZHE Extraction - 1/9/2020 8:50:29 AM WG1408214 Fluid 1 1/9/202012:02:38 PM WG1408380 Initial pH 7.85 1/9/202012:02:38 PM WG1408380 Final pH 4.86 1/9/202012:02:38 PM WG1408380 Wet Chemistry by Method 9012 B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Cyanide ND 0.250 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Sulfide ND 25.0 Wet Chemistry by Method 9045D Dilution Analysis Batch date / time 1 01/13/202012:46 WG1408346 Dilution Analysis Batch date / time 1 01/09/2020 22:00 WG1408079 Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 7.10 T8 1 01/11/202018:00 WG1408459 Sample Narrative: L1177103-01 WG1408459: 7.1 at 23.7C Wet Chemistry by Method D93/1010A Result Analyte Deg. F Ignitability DNI at170 Mercury by Method 7470A Qualifier Dilution Analysis Batch date / time 1 01/20/202010:15 WG1412116 Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Mercury ND 0.0100 0.20 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Arsenic ND 0.100 5 Barium ND 0.100 100 Cadmium ND 0.100 1 Chromium ND 0.100 5 Lead ND 0.100 5 Selenium ND 0.100 1 Silver ND 0.100 5 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Benzene ND 0.0500 0.50 Carbon tetrachloride ND 0.0500 0.50 Chlorobenzene ND 0.0500 100 Chloroform ND 0.250 6 ACCOUNT: PROJECT: EMA Resources Dilution Analysis Batch date / time 1 01/13/2020 09:49 WG1408995 Dilution Analysis Batch date / time 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 1 01/12/202015:33 WG1409034 ONE LAB. NATIONWIDE. * Fp Fc FS Fn Fc �GI SAI Rc Dilution Analysis Batch date / time 1 01/12/2020 23:09 WG1409088 1 01/12/2020 23:09 WG1409088 1 01/12/2020 23:09 WG1409088 1 01/12/2020 23:09 WG1409088 SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 5 of 23 REDSVILLE SAMPLE RESULTS Collected date/time: 01/07/20 08:30 L1177103 Volatile Organic Compounds (GC/MS) by Method 8260D - 01 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND J4 0.0500 0.50 1 01/12/2020 23:09 WG1409088 1,1-Dichloroethene ND 0.0500 0.70 1 01/12/2020 23:09 WG1409088 2-Butanone (MEK) ND 0.500 200 1 01/12/2020 23:09 WG1409088 Tetrachloroethene ND 0.0500 0.70 1 01/12/2020 23:09 WG1409088 Trichloroethene ND 0.0500 0.50 1 01/12/2020 23:09 WG1409088 Vinyl chloride ND 0.0500 0.20 1 01/12/2020 23:09 WG1409088 (S) Toluene-dH 85.5 80.0-120 0111212020 23.09 WG1409088 (S) 4-Bromofluorobenzene 89.4 77.0-126 0111212020 23.09 WG1409088 (S) 1,2-Dichloroethane-d4 101 70.0-130 011121202023.09 WG1409088 Chlorinated Acid Herbicides (GC) by Method 8151A Result Analyte mg/I 2,4,5-TP (Silvex) ND 2,4-D ND (S)2,4-DichlorophenylAcetic Acid 65.8 Pesticides (GC) by Method 8081B Result Analyte mg/I Chlordane ND Endrin ND Heptachlor ND Lindane ND Methoxychlor ND Toxaphene ND (S) Decochlorobiphenyl 81.5 (S) Tetrochloro-m-xylene 70.2 Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I date / time 0.00200 1 1 01/16/2020 02:35 WG1411034 0.00200 10 1 01/16/2020 02:35 WG1411034 14.0-158 0111612020 02.35 WG1411034 Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I date / time 0.00500 0.03 1 01/13/202013:24 WG1409135 0.00500 0.02 1 01/13/202013:24 WG1409135 0.00500 0.0080 1 01/13/202013:24 WG1409135 0.00500 0.40 1 01/13/202013:24 WG1409135 0.00500 10 1 01/13/202013:24 WG1409135 0.0100 0.50 1 01/13/202013:24 WG1409135 10.0-128 011131202013.24 WG1409135 10.0-127 011131202013.24 WG1409135 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,4-Dichlorobenzene ND 0.100 7.50 1 01/13/2020 05:24 WG1409132 2,4-Dinitrotoluene ND 0.100 0.13 1 01/13/2020 05:24 WG1409132 Hexachlorobenzene ND 0.100 0.13 1 01/13/2020 05:24 WG1409132 Hexachloro-1,3-butadiene ND 0.100 0.50 1 01/13/2020 05:24 WG1409132 Hexachloroethane ND 0.100 3 1 01/13/2020 05:24 WG1409132 Nitrobenzene ND 0.100 2 1 01/13/2020 05:24 WG1409132 Pyridine ND 0.100 5 1 01/13/2020 05:24 WG1409132 3&4-Methyl Phenol ND 0.100 400 1 01/13/2020 05:24 WG1409132 2-Methylphenol ND 0.100 200 1 01/13/2020 05:24 WG1409132 Pentachlorophenol ND 0.100 100 1 01/13/2020 05:24 WG1409132 2,4,5-Trichlorophenol ND 0.100 400 1 01/13/2020 05:24 WG1409132 2,4,6-Trichlorophenol ND 0.100 2 1 01/13/2020 05:24 WG1409132 (S) 2-Fluorophenol 39.6 10.0-120 0111312020 05.24 WG1409132 (S) Phenol-d5 25.5 10.0-120 0111312020 05.24 WG1409132 (S) Nitrobenzene-d5 57.2 10.0-127 0111312020 05.24 WG1409132 (S) 2-Fluorobiphenyl 67.7 10.0-130 0111312020 05.24 WG1409132 (S) 2,4, 6-Tribromophenol 64.5 10.0-155 0111312020 05.24 WG1409132 (S) p-Terphenyl-d14 74.5 10.0-128 0111312020 05.24 WG1409132 ONE LAB. NATIONWIDE. Fp Fc FS Fn FA Fc F, SAI Rc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 6 of 23 WG1408346 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9012 B L1177103-01 Method Blank (MB) (MB) R3490255-1 01/13/201233 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Cyanide U 0.0390 0.250 L1177102-01 Original Sample (OS) • Duplicate (DUP) (OS) L1177102-01 01/13/2012:42 • (DUP) R3490255-5 01/13/2012:45 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg %_ Reactive Cyanide ND 0.000 1 0.000 20 L1177103-01 Original Sample (OS) • Duplicate (DUP) (OS) L1177103-01 01/13/2012:46 • (DUP) R3490255-6 01/13/2012:47 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide ND 0.000 1 0.000 20 Laboratory Control Sample (LCS) (LCS) R3490255-2 01/13/2012:34 Spike Amount LCS Result LCS Rec. Analyte mg/kg mg/kg Reactive Cyanide 2.50 2.51 100 Rec. Limits LCS Qualifier 50.0-150 L1176796-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. * (OS) L1176796-01 01/13/20 12:39 • (MS) R3490255-3 01/13/20 12:40 • (MSD) R3490255-4 01/13/20 12:41 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 1.67 ND 1.27 0.738 76.4 44.3 1 75.0-125 J3 J6 53.3 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 7 of 23 WG1408346 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9012 B L1177103-01 L1177424-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1177424-10 01/13/20 13:03 • (MS) R3490255-7 01/13/20 13:04 • (MSD) R3490255-8 01/13/20 13:05 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 2.15 2.27 3.87 3.89 74.3 75.4 Dilution Rec. Limits 75.0-125 MS Qualifier MSD Qualifier RPD J6 0.588 ONE LAB. NATIONWIDE. * RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 3 of 23 WG1408079 Wet Chemistry by Method 9034-9030B Method Blank (MB) (MB) R3439492-1 01/09/20 22:00 MB Result Analyte mg/kg Reactive Sulfide U MB Qualifier MB MDL MB RDL mg/kg mg/kg 7.63 25.0 L1177102-01 Original Sample (OS) • Duplicate (DUP) QUALITY CONTROL SUMMARY L1177103-01 (OS) L1177102-01 01/09/20 22:00 • (DUP) R3489492-3 01/09/20 22:00 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg %_ Reactive Sulfide ND ND 1 0.000 20 Laboratory Control Sample (LCS) (LCS) R3489492-2 01/09/20 22:00 Spike Amount LCS Result Analyte mg/kg mg/kg Reactive Sulfide 100 87.8 LCS Rec. Rec. Limits LCS Qualifier 87.8 70.0-130 ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 9 of 23 WG1408459 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9045D L1177103-01 L1177102-01 Original Sample (OS) • Duplicate (DUP) (OS) L1177102-01 01/11/20 13 00 • (DUP) R3439927-2 01/11/20 13 00 Original Result DUP Result Dilution DUP RPD Analyte su su Corrosivity by pH 7.42 7.46 1 0.538 Sample Narrative: OS: 7.42 at 23.8C DUP:7.46 at23.6C L1177123-01 Original Sample (OS) • Duplicate (DUP) (OS) L1177123-01 01/11/20 13 00 • (DUP) R3489927-3 01/11/20 13 00 Original Result DUP Result Dilution DUP RPD Analyte su su Corrosivity by pH 7.21 7.26 1 0.691 Sample Narrative: OS: 7.21 at 21.6C DUP:7.26 at21.5C Laboratory Control Sample (LCS) (LCS) R3489927-1 01/11/2018:00 Spike Amount LCS Result LCS Rec. Rec. Limits Analyte su su Corrosivity by pH 10.0 9.96 99.6 99.0-101 Sample Narrative: LCS: 9.96 at 20.2C DUP Qualifier DUP RPD Limits DUP Qualifier DUP RPD Limits 1 LCS Qualifier ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 10 of 23 WG1412116 QUALITY CONTROL SUMMARY Wet Chemistry by Method D93/1010A L1177103-01 L1177848-01 Original Sample (OS) • Duplicate (DUP) (OS) L1177343-01 01/20/2010:15 • (DUP) R3492211-3 01/20/2010:15 Original Result DUP Result Dilution DUP RPD Analyte Deg. F Deg. F Ignitability 149 148 1 0.674 DUP Qualifier DUP RPD Limits i 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3492211-1 01/20/2010:15 • (LCSD) R3492211-2 01/20/201015 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte Deg.F Deg.F Deg.F Ignitability 82.0 79.9 79.9 97.4 97.4 97.0-103 0.000 10 ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 11 of 23 WG1408995 QUALITY CONTROL SUMMARY Mercury by Method 7470A L1177103-01 Method Blank (MB) (MB) R3490165-1 01/13/20 0925 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Mercury U 0.00330 0.0100 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3490165-2 01/13/20 09:27 • (LCSD) R3490165-3 01/13/20 09:29 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I Mercury 0.0300 0.0300 0.0285 100 95.1 80.0-120 5.10 20 L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. * (OS) L1176194-01 01/13/20 09:35 • (MS) R3490165-4 01/13/20 09:37 • (MSD) R3490165-5 01/13/20 09:39 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0311 0.0290 104 96.5 1 75.0-125 6.99 20 L1177408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1177403-01 01/13/20 09:41 • (MS) R3490165-6 01/13/20 09:43 • (MSD) R3490165-7 01/13/20 09:45 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0307 0.0297 102 98.9 1 75.0-125 3.32 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 12 of 23 WG1409034 Metals (ICP) by Method 6010D Method Blank (MB) QUALITY CONTROL SUMMARY L1177103-01 (MB) R3490023-1 01/12/2015:00 MB Result Analyte mg/I MB Qualifier MB MDL mg/I MB RDL mg/I Arsenic 0.0600 J 0.0333 0.100 Barium U 0.0333 0.100 Cadmium U 0.0333 0.100 Chromium U 0.0333 0.100 Lead U 0.0333 0.100 Selenium U 0.0333 0.100 Silver U 0.0333 0.100 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3490028-2 01/12/2015:02 • (LCSD) R3490028-3 01/12/2015:05 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte mg/I mg/I mg/I Arsenic 10.0 9.91 9.89 99.1 98.9 80.0-120 Barium 10.0 9.87 9.87 98.7 98.7 80.0-120 Cadmium 10.0 9.63 9.61 96.3 96.1 80.0-120 Chromium 10.0 9.36 9.37 93.6 93.7 80.0-120 Lead 10.0 9.80 9.80 98.0 98.0 80.0-120 Selenium 10.0 10.2 10.1 102 101 80.0-120 Silver 2.00 1.72 1.72 86.1 86.1 80.0-120 L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1176194-01 01/12/20 15:07 • (MS) R3490023-5 01/12/20 15:12 • (MSD) R3490023-6 01/12/20 1515 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 9.40 9.51 94.0 95.1 Barium 10.0 ND 9.58 9.69 95.8 96.9 Cadmium 10.0 ND 9.43 9.54 94.3 95.4 Chromium 10.0 0.262 9.26 9.33 90.0 90.7 Lead 10.0 ND 8.81 8.88 88.1 88.8 Selenium 10.0 ND 9.69 9.83 96.9 98.3 Silver 2.00 ND 1.72 1.74 86.1 86.8 LCS Qualifier LCSD Qualifier RPD RPD Limits 0.210 20 0.0250 20 0.241 20 0.0285 20 0.00270 20 0.495 20 0.00651 20 Dilution Rec. Limits 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 MS Qualifier MSD Qualifier RPD 1.15 1.20 1.19 0.687 0.790 1.46 0.770 ONE LAB. NATIONWIDE. * RPD Limits 20 20 20 20 20 20 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 13 of 23 WG1409034 QUALITY CONTROL SUMMARY Metals (ICP) by Method 6010D L1177103-01 L1178016-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1173016-01 01/12/201517 • (MS) R3490023-7 01/12/20 15:20 • (MSD) R3490023-8 01/12/20 15:22 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 10.1 10.0 101 100 Barium 10.0 ND 9.99 10.0 99.5 99.7 Cadmium 10.0 ND 9.69 9.72 96.9 97.2 Chromium 10.0 ND 9.45 9.48 94.5 94.8 Lead 10.0 0.333 10.2 10.2 98.7 98.8 Selenium 10.0 ND 10.3 10.2 103 102 Silver 2.00 ND 1.75 1.75 87.3 87.6 ACCOUNT: EMA Resources PROJECT: ONE LAB. NATIONWIDE. * Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 75.0-125 0.664 20 1 75.0-125 0.157 20 1 75.0-125 0.282 20 1 75.0-125 0.302 20 1 75.0-125 0.153 20 1 75.0-125 0.965 20 1 75.0-125 0.310 20 SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 14 of 23 WG1409088 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260D L1177103-01 Method Blank (MB) (MB) R3490297-3 01/12/20 2150 MB Result MB Qualifier Analyte mg/I Benzene U Carbon tetrachloride U Chlorobenzene U Chloroform U 1,2-Dichloroethane U 1,1-Dichloroethene U 2-Butanone (MEK) U Tetrachloroethene U Trichloroethene U Vinyl chloride U (S) Toluene-dH 83.1 (S) 4-Bromofluorobenzene 89.6 (S) 1,2-Dichloroethane-d4 103 Laboratory Control Sample (LCS) (LCS) R3490297-1 01/12/20 18:53 Spike Amount LCS Result Analyte mg/I mg/I Benzene 0.250 0.250 Carbon tetrachloride 0.250 0.276 Chlorobenzene 0.250 0.226 Chloroform 0.250 0.260 1,2-Dichloroethane 0.250 0.334 1,1-Dichloroethene 0.250 0.232 2-Butanone (MEK) 1.25 1.91 Tetrachloroethene 0.250 0.207 Trichloroethene 0.250 0.259 Vinyl chloride 0.250 0.191 (S) Toluene-dH (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 MB MDL mg/I 0.0167 0.0167 0.0167 0.0833 0.0167 0.0167 0.167 0.0167 0.0167 0.0167 LCS Rec 100 110 90.4 104 134 92.8 153 82.8 104 76.4 85.9 91.0 116 MB RDL mg/I 0.0500 0.0500 0.0500 0.250 0.0500 0.0500 0.500 0.0500 0.0500 0.0500 80.0-120 77.0-126 70.0-130 Rec. Limits LCS Qualifier 70.0-123 68.0-126 80.0-121 73.0-120 70.0-128 71.0-124 44.0-160 72.0-132 78.0-124 67.0-131 80.0-120 77.0-126 70.0-130 J4 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 15 of 23 WG1409088 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1177103-01 ONE LAB. NATIONWIDE. * L1177408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1177403-01 01/13/20 02:06 • (MS) R3490297-4 01/13/20 03:05 • (MSD) R3490297-5 01/13/20 03:25 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Benzene 0.250 ND 0.283 0.296 113 118 Carbon tetrachloride 0.250 ND 0.309 0.348 124 139 Chlorobenzene 0.250 ND 0.251 0.269 100 108 Chloroform 0.250 ND 0.285 0.315 114 126 1,2-Dichloroethane 0.250 ND 0.331 0.357 132 143 1,1-Dichloroethene 0.250 ND 0.300 0.333 120 133 2-Butanone (MEK) 1.25 ND 1.65 1.97 132 158 Tetrachloroethene 0.250 ND 0.237 0.272 94.8 109 Trichloroethene 0.250 ND 0.295 0.308 118 123 Vinyl chloride 0.250 ND 0.251 0.260 100 104 (S) Toluene-dH 87.8 87.8 (S) 4-Bromofluorobenzene 89.9 90.8 (S) 1,2-Dichloroethane-d4 ill 118 ACCOUNT: EMA Resources PROJECT: Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 17.0-158 4.49 27 1 23.0-159 11.9 28 1 33.0-152 6.92 27 1 29.0-154 10.0 28 1 29.0-151 7.56 27 1 11.0-160 10.4 29 1 10.0-160 17.7 32 1 10.0-160 13.8 27 1 10.0-160 4.31 25 1 10.0-160 3.52 27 80.0-120 77.0-126 70.0-130 SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 16 of 23 WG1411034 Chlorinated Acid Herbicides (GC) by Method 8151A Method Blank (MB) QUALITY CONTROL SUMMARY L1177103-01 (MB) R3491211-1 01/16/20 0100 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 2,4-D U 0.000667 0.00200 2,4,5-TP (Silvex) U 0.000667 0.00200 (S) Z4-Dichlorophenyl Acetic 65.2 14.0-158 Acid Laboratory Control Sample (LCS) (LCS) R3491211-2 01/16/20 0113 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 2,4-D 0.0500 0.0447 89.4 50.0-120 2,4,5-TP (Silvex) 0.0500 0.0435 87.0 50.0-125 (S) Z4-Dichlorophenyl Acetic 79.2 14. 0-158 Acid L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1176194-01 01/16/20 0127 • (MS) R3491211-3 01/16/20 0141 • (MSD) R3491211-4 01/16/20 0155 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4-D 0.0500 ND 0.0411 0.0436 82.2 87.2 2,4,5-TP (Silvex) 0.0500 ND 0.0353 0.0382 70.6 76.4 (S) Z4-Dichlorophenyl Acetic 63.4 65.0 Acid ACCOUNT: EMA Resources PROJECT: ONE LAB. NATIONWIDE. * Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 50.0-120 5.90 20 1 50.0-125 7.89 20 14.0-158 SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 17 of 23 Cp ITC] Fs-s [Cn] 1-Sr El FAI 9 Sc WG1409135 Pesticides (GC) by Method 8081B Method Blank (MB) QUALITY CONTROL SUMMARY L1177103-01 (MB) R3490334-1 01/13/201210 MB Result Analyte mg/I MB Qualifier MB MDL mg/I MB RDL mg/I Gamma BHC U 0.00167 0.00500 Endrin U 0.00167 0.00500 Heptachlor U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 Chlordane U 0.00167 0.00500 Toxaphene U 0.00333 0.0100 (S) Decachlorobiphenyl 96.3 10.0-128 (S) Tetrochloro-m-xylene 69.2 10.0-127 Laboratory Control Sample (LCS) (LCS) R3490334-2 01/13/2012:22 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I Gamma BHC 0.0100 0.0101 101 55.0-129 Endrin 0.0100 0.00999 99.9 57.0-134 Heptachlor 0.0100 0.00997 99.7 27.0-132 Methoxychlor 0.0100 0.0113 113 54.0-155 (S) Decachlorobiphenyl 90.0 10.0-128 (S) Tetrochloro-m-xylene 75.4 10.0-127 L1177103-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1177103-01 01/13/20 13:24 • (MS) R3490334-3 01/13/20 13:37 • (MSD) R3490334-4 01/13/20 13:49 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits Analyte mg/I mg/I mg/I mg/I Gamma BHC 0.0100 ND 0.00956 0.00979 95.6 97.9 1 14.0-141 Endrin 0.0100 ND 0.0102 0.0102 102 102 1 10.0-160 Heptachlor 0.0100 ND 0.00970 0.00967 97.0 96.7 1 16.0-136 Methoxychlor 0.0100 ND 0.0114 0.0116 114 116 1 10.0-160 (S) Decachlorobiphenyl 78.1 80.9 10.0-128 (S) Tetrochloro-m-xylene 69.1 69.0 10.0-127 ONE LAB. NATIONWIDE. * MS Qualifier MSD Qualifier RPD RPD Limits 2.38 40 0.000 39 0.310 40 1.74 34 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 13 of 23 WG1409132 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1177103-01 Method Blank (MB) (MB) R3490117-2 01/13/20 0042 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 1,4-Dichlorobenzene U 0.0333 0.100 2,4-Dinitrotoluene U 0.0333 0.100 Hexachlorobenzene U 0.0333 0.100 Hexachloro-1,3-butadiene U 0.0333 0.100 Hexachloroethane U 0.0333 0.100 Nitrobenzene U 0.0333 0.100 Pyridine U 0.0333 0.100 2-Methylphenol U 0.0333 0.100 3&4-Methyl Phenol U 0.0333 0.100 Pentachlorophenol U 0.0333 0.100 2,4,5-Trichlorophenol U 0.0333 0.100 2,4,6-Trichlorophenol U 0.0333 0.100 (S) Nitrobenzene-d5 67.0 10.0-127 (S) 2-Fluorobiphenyl 76.9 10.0-130 (S) p-Terphenyl-d14 76.0 10.0-128 (S) Phenol-d5 24.9 10.0-120 (S) 2-Fluorophenol 37.E 10.0-120 (S) 2,4, 6-Tribromophenol 75.0 10. 0-155 Laboratory Control Sample (LCS) ONE LAB. NATIONWIDE. * (LCS) R3490117-1 01/13/20 0020 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 1,4-Dichlorobenzene 0.500 0.310 62.0 18.0-120 2,4-Dinitrotoluene 0.500 0.433 86.6 49.0-124 Hexachlorobenzene 0.500 0.392 78.4 44.0-120 Hexachloro-1,3-butadiene 0.500 0.299 59.8 19.0-120 Hexachloroethane 0.500 0.281 56.2 15.0-120 Nitrobenzene 0.500 0.318 63.6 27.0-120 Pyridine 0.500 0.151 30.2 10.0-120 2-Methylphenol 0.500 0.266 53.2 28.0-120 3&4-Methyl Phenol 0.500 0.281 56.2 31.0-120 Pentachlorophenol 0.500 0.415 83.0 23.0-120 2,4,5-Trichlorophenol 0.500 0.408 81.6 44.0-120 2,4,6-Trichlorophenol 0.500 0.380 76.0 42.0-120 (S) Nitrobenzene-d5 54.5 10.0-127 (S) 2-Fluorobiphenyl 77.5 10.0-130 (S) p-Terphenyl-d14 75.2 10.0-128 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1177103 01/20/20 14:21 19 of 23 WG1409132 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1177103-01 Laboratory Control Sample (LCS) (LCS) R3490117-1 01/13/20 0020 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I (S) Phenol-d5 277 10.0-120 (S) 2-Fluorophenol 42.1 10.0-120 (S) 2,4, 6-Tribromophenol 84.0 10. 0-155 L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1176194-01 01/13/20 03:36 • (MS) R3490117-3 01/13/20 03:57 • (MSD) R3490117-4 01/13/20 0419 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 1,4-Dichlorobenzene 0.500 ND 0.180 0.304 36.0 60.8 2,4-Dinitrotoluene 0.500 ND 0.237 0.420 47.4 84.0 Hexachlorobenzene 0.500 ND 0.195 0.372 39.0 74.4 Hexachloro-1,3-butadiene 0.500 ND 0.223 0.308 44.6 61.6 Hexachloroethane 0.500 ND 0.196 0.293 39.2 58.6 Nitrobenzene 0.500 ND 0.197 0.312 39.4 62.4 Pyridine 0.500 ND 0.0755 0.162 15.1 32.4 2-Methylphenol 0.500 ND 0.181 0.272 36.2 54.4 3&4-Methyl Phenol 0.500 ND 0.196 0.291 39.2 58.2 Pentachlorophenol 0.500 ND 0.184 0.343 36.8 68.6 2,4,5-Trichlorophenol 0.500 ND 0.252 0.409 50.4 81.8 2,4,6-Trichlorophenol 0.500 ND 0.226 0.378 45.2 75.6 (S) Nitrobenzene-d5 34.6 54.6 (S) 2-Fluorobiphenyl 44.5 76.5 (S) p-Terphenyl-d14 38.8 73.4 (S) Phenol-d5 23.3 30.5 (S) 2-Fluorophenol 30.3 46.9 (S) 2,4, 6-Tribromophenol 45.1 78.0 ONE LAB. NATIONWIDE. * Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 17.0-120 J3 51.2 40 1 39.0-125 J3 55.7 25 1 35.0-122 J3 62.4 24 1 12.0-120 32.0 34 1 10.0-120 39.7 40 1 12.0-120 J3 45.2 30 1 10.0-120 J3 72.8 37 1 10.0-120 J3 40.2 30 1 10.0-120 J3 39.0 36 1 10.0-128 J3 60.3 37 1 33.0-120 J3 47.5 31 1 26.0-120 J3 50.3 31 10.0-127 10.0-130 10.0-128 10.0-120 10.0-120 10.0-155 ACCOUNT: PROJECT: EMA Resources SDG: DATE/TIME: L1177103 01/20/20 14:21 PAGE: 20 of 23 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. * The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions u Fc FS (dry) Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. Fn ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Fr Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Fc Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. F Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the Rc result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. Case Narrative (Cn) Quality Control Summary (Qc) Sample Chain of Custody (Sc) Sample Results (Sr) Sample Summary (Ss) Qualifier J J3 J4 J6 T8 A brief discussion about the included sample results, including a discussion of any non -conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Description The identification ofthe analyte is acceptable, the reported value is an estimate. The associated batch QC was outside the established quality control range for precision. The associated batch QC was outside the established quality control range for accuracy. The sample matrix interfered with the ability to make any accurate determination, spike value is low. Sample(s) received past/too close to holding time expiration. ACCOUNT: EMA Resources PROJECT: SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 21 of 23 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing Cp turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Fc State Accreditations Alabama 40660 Nebraska NE-OS-15-05 FS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 Fn California 2932 New Mexico n/a Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Fr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Fc Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 7G1 Indiana C-TN-01 f Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'" 2006 Louisiana' LA180010 Texas T104704245-18-15 Rc Maine TN0002 Texas 5 LABO152 Maryland 324 Utah TN00003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2 LA Third Party Federal Accreditations A2LA— ISO17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 ' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT ND OR ID SD VWY ` NV T NE T UT CA co KS W o �AZ NM O� T TX AK � . b C, fo • B HI 4 S ACCOUNT: V PROJECT: EMA Resources ME MN WVI NY MI T IA T PA 4 OH Mo IL Ihi T T WV VAT KY N * r� AR Ms AL GA LA FL SDG: DATE/TIME: PAGE: L1177103 01/20/20 14:21 22 of 23 Billing Information: Aralvsis I Container I Pr servative Chain of Custody Page _of_ EMA Resources Mr. Brent Collins Pres 755 Yadkinville Road Chk C8Aq*ft• 755 Yadkinville Road Mocksville, NC 2702$ r - A%mwa 6ftrrQ TwmV s +.+avai Mocksville, NC 27028 12d65 tel Rd � Mount Juliet, TN 37322 1+ = r Phone: 615-758.5858 f�.: Phone: 8011a67.51 FaM: 615-758-5859 �I' Report to: Mr. Brent Collins Email To brent.collins@emaresourcesinc.com Project Description: Sludge Cit /State n / /f,/� Collected: K*;Q;li/�V `r Please C+rcle PT MT CT _7 Phone: 336-751-1441 Client Project p Lab Project R SDG # L1 I U 3 Fax: 336-751-1442 1193 Ti Coltected by {print): Site/Facility ID q P.O, a BYE+ i CI1•�s ` a a Acctnum: EMARES Tem Iate:T11413 P Collected by (signature): RUSK? (Lab MUST Be Notified) Quote # Same Day _ Five Day Next Day _ 5 Day (Rad Only) Date Results Needed ^_ C Z `'"{ Prelogin: P748414 PM. 807 - Justin Carr Immediately / .! Packed on Ice N _ Y _ Two Day _ 10 Day (Rad Only) Na. —Three Day of = J f-q l.7 4— CL u - , PB: , - Shipped Vla: FedEX Standard Remarks Sample ID Comp/Grab Matrix • Depth Date Time ntas z.� ss z X X i RRemarks: ' Matrix: s4mple Receipt COC Seal Present/intact:,/_NP Y _N SS -Soil AIR -Air F- Filter pH Temp GW- Groundwater 8-Binassay WW - wastewater DW • Drinking Water DT - Other Flow Other COC Signed/Accurate: _N Bottles arrive intact: t_N Correct bottles used: _N 5amp4esfetufned vea UPS Fe Ex Courier __ _ Tracking# �,� I YJ 6 / If Avglicable vOA Zero Headspace: Y N preservation Correct/Checked: N RAD Screen t0.5 ril Z__`J Relinquished by : (Signature) Date: Time: 11712070 09t) Received by: (Signature) TTip Blank Received: Yes / No HCLii TSR Relinquished by : (Signature) Date: Time: Received by {Signat��re) Temp: °C 63ttles Received: If preservation required by Login: Date/Time Relinquished by : (Signature) Date: Time oRec'ved f r lab bz"Sigturei Rate: Time: Hold: Condition: NCFq 0 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WWTP Name: Reidsville WWTP Monitoring Period: WQ Permit Number: WQ0002376 NPDES Number: NCO024881 From 1 / 1 /2020 To 3/31 /2020 Pathogen Reduction (15A NCAC 02T .1106)- Please indientP 1PvP1 ,ath.nvnil .,..a nl*-- Class A: Alt.A (time/temp) ❑ - ---- - ------ Alt B (Alk Treatment) [3 ..0 -. n uu 11 vG IJCI 11m IIICU. Alt. C (Prior Testing) ❑ Alt (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost F-I Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray LJ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density R1 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ 1Air Drying ❑ Composting ❑ JAerob1c Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level PathogenDensity tY Number o Excee- Frequency Sample Analytical Minimu m Geo. Mean aximu Unitsences in Sludge d of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 10510 14471 21251 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) . a.a.au■ Aald al.11ull 1%GuuGt1u11 t1JEii 1\l.L-lk- 1uL 1 .1lu / I - rlease lnnlcate alternative nPrfnrmoda Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 21 Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) J Alt. 9 (Injection) ❑ !'T7)mirii. A TT/ll►T 11T ♦ TT Alt. 10 (Incorporation) ❑ .--T— , No vector attraction reduction alternatives _ were performed 11r 1l.Li 1 ]MY114 a i ti 1 Ir'lViEN 1 tplease check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." J "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Bryan - WWTP Superintendent Brent Collins; Director of Technical Services Preparer N me and Title (type or print) Land Applier Name and Title(ifapplicable)(type or print) 2 to =( Z�G2/8/2021 Signature eparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) 1 Contact: Brent Collins Report Date: 1/Page Page 1 0 Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 1/7/2020 Meritech Work Order # 01072014 Sample: Reidsville #1 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.73 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 10510 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D Meritech Work Order # 01072015 Sample: Reidsville #2 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.74 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 13584 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D Meritech Work Order # 01072016 Sample: Reidsville #3 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.45 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 16928 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D Meritech Work Order # 01072017 Sample: Reidsville #4 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.52 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 11364 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D Meritech Work Order # 01072018 Sample: Reidsville #5 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.54 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 21251 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 01072019 Sample: Reidsville #6 Grab Parameters Result Analysis Date % Total Solids 1.39 % 1/7/20 Fecal Coliform (Sludge) 13081 col/g dry wt 1/7/20 Page 2 Report Date: 1/14/2020 Date Sample Rcvd: 1/7/2020 1/7/20 Reporting Limit Method 0-100 % SM 2540B 130 col/g dry wt SM 9222D Meritech Work Order # 01072020 Sample: Reidsville #7 Grab 1/7/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.41 % 1/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 17409 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5-9-2016 Chain of Custody Record (COC) NPDES#: ME RITECH INC. Client: EMA Resources Inc. Phone:_ 336-751-1441 0 1 Address:_ 755 Yadkinville Rd Fax: 336-751-1442 ENVIRONMENTAL LABORATORIES Mocksville NC 27028 Email: brent.collins(a)emaresourcesinc com 642 Tamco Rd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritechiabs.com Attention:_ Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. www.meritechlabs.com Circle all that apply: Email (preferred), Fax, Mail Std 10da s) 3-5 Days 24�48Hrs Sampling Dates & Times Person Taking Sample (Sign/Print): GD f Ib� f / Lab Use Only Sample Location and/or ID # Vr Start End Comp? #of Test(s) Required pH OK? Date Time Date Time Grab? Cont. s / �N No ? Reidsville #1 117ho `l 'i Fecal Coliform 1 Reidsville #2 Reidsville #3 Reidsville #4 Reidsville #5 Reidsville #6 Reidsville #7 V Temperature Upon Receipt: ,) 0 Method of *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** V ., , Shipment: Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg E�' ug/L ❑ ❑ Hand Delivery Relinquished by: /� r �� Date: Time: J , r Received by: Date: Time: (/ Y _-7-W ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rereived b ab: _ �$ Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Report Date: 2/5/2020 Date Sample Rcvd: 1/7/2020 Vector Attraction Reduction / Aerobically Digested Sludge 30 Day Test Meritech Work Order # 01072023 Sample: Reidsville Composite 1/7/20 Total Solids Volatile Solids % Volatile Solids Week 1 0.470 0.340 0.725 Week 2 0.470 0.350 0.738 Week 3 0.400 0.280 0.700 Week 4 0.410 0.290 0.702 Week 5 0.370 0.260 0.712 Van Kleek Reduction (%): 6.51 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass �Mm 14-1 n^ C-1'% i ) Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5-9-2016 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:_ 336-751-1441 Address:_ 755 Yadkinville Rd Fax: 336-751-1442 Mocksville NC 27028 Email:_ brent.collins(@emaresourcesinc.com Project: P.O.#: Attention:_ Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: Email (preferred), Fax, Mail Stcl 10days) 3-5 Days 24�48Hrs ME R ITE C H INC. 1 ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechiabs.com Sample Location and/or ID # Sampling Dates & Times Person Taking Sample (Sign/Print): Go B( � "J'5c f ) Lab Use Only Start End Comp? Grab? #of Cont. Test (s) Required On Ice? e�) / No pH OK? Cl OK? Date Time Date Time Reidsville 07/u 30 Day Bench Temperature Upon Receipt: / /7 Method of Shipment: *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes 2' No ❑ Report results in: mg/L ❑ mg/kg U ug/L ❑ ❑ Hand Delivery Relinquished by: Date: Time: _1 -26 Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Re ived kab� DdheC Tjme' ) i/ 1= ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WWTP Name: Reidsville WWTP WQ Permit Number: WQ0002376 NPDES Number: NCO024881 Monitoring Period: From 4/1/2020 To 6/30/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and altPrnativa ". wfn .A . Class A: Alt. A (time/temp) D Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs Cl If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost L i Heat Drying ❑ I Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density Rl Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑1 Air Drying ❑ Composting 0 JAeroble Digestion L7 Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level PathogenDensity tY Number o Excee- Frequency Sample Analytical Minimum Geo. Mean Maximum Units in Sludge g of Analysis Type Tech-nique n 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFu 7204 7834 9057 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) X7_ _--_ ♦ a. weight) - T 1 v ectur tittractron neauctlon tl:�A INUAU UZ l .1tU7) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) Q AIt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed L1 l r 1(1 lr 11;A I MIN N l Al E1VIUIN 1 (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Bryan - WWTP Superintendent Brent Collins; Director of Technical Services Preparer Narve and Title (type or print) Land Applier Name and 2 Title (if applicable)(type or print) io ` z�i 4u"2/8/2021 Signature parer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Page 1 Report Date: 4/14/2020 Date Sample Rcvd: 4/2/2020 Meritech Work Order # 04022004 Sample: Reidsville 1 Grab 4/2/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.45 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7792 col/g dry wt 4/2/20 130 col/g dry wt SM 9222D Meritech Work Order # 04022005 Sample: Reidsville 2 Grab 4/2/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.65 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7204 col/g dry wt 4/2/20 130 col/g dry wt SM 9222D Meritech Work Order # 04022006 Sample: Reidsville 3 Grab 4/2/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.54 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 8232 col/g dry wt 4/2/20 130 col/g dry wt SM 9222D Meritech Work Order # 04022007 Sample: Reidsville 4 Grab 4/2/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.43 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7856 col/g dry wt 4/2/20 130 col/g dry wt SM 9222D Meritech Work Order # 04022008 Sample: Reidsville 5 Grab 4/2/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 2.42 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7513 col/g dry wt 4/2/20 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 04022009 Sample: Reidsville 6 Grab Parameters Result Analysis Date % Total Solids 2.48 % 4/7/20 Fecal Coliform (Sludge) 7331 col/g dry wt 4/2/20 Meritech Work Order # 04022010 Sample: Reidsville 7 Grab Parameters Result Analysis Date % Total Solids 2.66 % 4/7/20 Fecal Coliform (Sludge) 9057 col/g dry wt 4/2/20 Page 2 Report Date: 4/14/2020 Date Sample Rcvd: 4/2/2020 4/2/20 Reporting Limit Method 0-100 % SM 2540B 130 col/g dry wt SM 9222D 4/2/20 Reporting Limit Method 0-100 % SM 2540B 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. aboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 59-2016 Chain of Custody Record (COC) . MERITECH, INC. ....................... . .................... . ............................................................................. ..... ... . . ... ... .... . ... . . .. .. .................. ..... .... .. .. ........... ENVIRONMENTAL LABORATORIES ..................... ... 64.21a mCo-Rd. . ................ — Phone: . ... 33 . 6 . -3 . 42 4748 .... . .... ....... . ........ ........ . ... .... .... . .. ... ***** ........... .... ... Reidsville .. NC . 27.320 7.32.0 ..... — .F . .a . . x . : ........ .. 3 . . 3 . ... 6-.34.... . . 2 . ... -1 .5..22.... ............ ........ Email: info@meritechlabs.com .................... . ..................... I .......................................... www.meritechiabs.com NPDES#: ............. . ........... ................................... ...................... I ...... I ................ . ................... . ................... Client: 1EIVIA Resources Inc. Phone: 1336-751-1441 ..... ­* .... .1 ................................ . ................................... I ................. -- -71 ............... ....... . ............. Address: 1755 Yadkinville Rd Fax: :336-751-1442 ................................ . ................................... ..................... ........................ . ................... . ....... ........... ...... - Wocksville NC 27028 Email.-. brent.coIIins@emaresourcesinc.coni ....... . ............................................ . ................................... ................ Project: ............. ............ ........... **"* ............ ..... ** ....... ......... ...... ............. . ........... ................................. P.OX: Attention: :Brent Collins Turn Around Time* *RUSH work needs prior approval. ... H.ow..w.ou.1clyou like your report sent? ............. . .. .. .. ... ... .... ... ...... . Circle all that apply: Email referred) Fax, Mail S s) s Sample Location and/or ID # Sampling Dates & Times Person Taking Sample (Sign/Print): Lab Use Only Start End Comp? Grab? Hof Cont. Test(s) Required On Ice? Yes No pH OK? CI OK? Date Time Date Time kip., is'i. I/ C 1 'Ilzbo co I �e e-,21 Ci 1'-4 01% If 7 Temperature Upon Receip 9') t E, Method of Shipment: Dechlorination (<0.5 ppm� of Ammonia, Canicle, Phenol and TKN samVles must be done in the field prior to preservation. Comments: .................................................. ....... ............................................. ........................................................... ....................... Compositor # E] UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L 0 mg/kg P""ug/L ❑ El Hand Delivery Relinquished by Date: /,/ 0 Time: 9 Received by: Date: Time: El Other ..................................... Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rece b�yl —7 9 FSTj) nle: i ci q-'r- W Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 5/5/2020 Date Sample Rcvd: 4/2/2020 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test Meritech Work Order # 04022001 Sample: Reidsville Composite 4/2/20 Total Solids Volatile Solids % Volatile Solids Week 1 0.940 0.700 0.748 Week 2 0.920 0.700 0.760 Week 3 0.870 0.640 0.737 Week 4 0.870 0.640 0.736 Week 5 0.830 0.610 0.735 Van Kleek Reduction (%): 6.70 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass �C�oeV2� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5 32016 Chain of Custody Record (COC) . MERITECH INC. .............. *"** ...... ......... . . . ....... * ........ONMENTAL LABORATORIES ENVIRONMENTAL .............. I ........ . ..................... ............................................................... .... . .... ....... .... . .... ... .... . ... ..... .... . .. ... 64.2..Ta . mco - Rd. ­Pho.ne.: ... 33 . 6 . -3 . 42- 47 4 . 8 Reidsville NC 27320 Fax: 336-342-1522 ....................... . .................... . ............................................................... Email: info@meritechiabs.com ............ I ..................... . .................... . ................................................................ www.meritechiabs.com NPDES#: ............. ........... ................................ ................................... ............................................. . .................... ................. ent: 1EMA Resources Inc. Phon 441 e: i336-751-1 ........... . .......... I ...................... I ......... . ................................... ........................................ I . ................... .................... Address: �755 Yadkinville Rd Fax: :336-751-1442 ......... . ........... ................................ . ................................... . I .................. .............. . .. I ................ . ................... Mocksville NC 27028 Email: brent.collins@emaresourcesinc.com ............. .......................................... . ................................... ..................... ......... Project: ......... ............ * .................... ' ....... * ... . ... ­ ......... ............ P.OX: ............. . ........... ................................ . .............................. ...................... .... Attention: !Brent Collins Turn Around Time* *RUSH work needs prior approval. How would you like your report sent? ............ . ............................................ . ......................................................... L__Jgass) �n Circle all that appl<E�>referrecl) , Fax, Mail S s Sample Location and/or ID # Sampling Dates & Times Person Taking Sample (Sign/Print) Lab Use Only Start Date Time End Date Time comp? Grab? # Of Cont. Test(s) Required On Ice? Yes No pH OK? Cl OK? vs y Temperature Upon Receipt- t Method of Shipment: Dechlorination (<0.5 ppm) of Ammonia, Canide, Phenol and TKN samRIes must be done in the field prior to preservation. Comments: ..................... ........................................... ............ ; ............................... ............. .................................................................................. lJUg Compositor # ❑ UPS # EJ Fed Ex Are these results for regulatory purposes? Yes �No ED Report results in: mg/L El mg/kg Q' ug/L E] El Hand Delivery Relinquished by: Date: f// a Time: zo Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received Date: Time: Relinquished by: Date: Time: Received �. lay, 0TeJ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WQ Permit Number: WQ0002376 WWTP Name: Reidsville WWTP NPDES Number: NCO024881 Monitoring Period: From 7/1/2020 To 9/30/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tithe/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic El Beta Ray❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIt. (1) Fecal Density R Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion 0 Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g �' umber o Excee- e Frequency of Analysis Sample Type Analytical Tech -pique MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 7315 13361 24515 col/ g 0 Quarterly Q y G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 0 IAIt. 4 (Spec. 02 uptake) J. Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) h1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Bryan - WWTP Superintendent Brent Collins; Director of Technical Services �Zv Title (type or print) Land Applier Name and Title (if applicable)(type or print) t�i 2/8/2021 * Signature o arer Date Signature of Land Applter (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client. EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Page 1 Report Date: 7/28/2020 Date Sample Rcvd: 7/21/2020 Meritech Work Order # 07212005 Sample: Reidsville 1 Grab 7/21/20 Parameters Result Analysis Date Reporting; Limit Method % Total Solids 0.87 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7315 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D Meritech Work Order # 07212006 Sample: Reidsville 2 Grab 7/21/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.84 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 12987 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D Meritech Work Order # 07212007 Sample: Reidsville 3 Grab 7/21/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.84 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 7576 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D Meritech Work Order # 07212008 Sample: Reidsville 4 Grab 7/21/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.85 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 12834 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D Meritech Work Order # 07212009 Sample: Reidsville 5 Grab 7/21/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.89 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 24515 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 07212010 Sample: Reidsville 6 Grab Parameters Result Analysis Date Page 2 Report Date: 7/28/2020 Date Sample Rcvd: 7/21/2020 7/21/20 Reporting Limit Method % Total Solids 0.83 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 16429 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D Meritech Work Order # 07212011 Sample: Reidsville 7 Grab 7/21/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.89 % 7/22/20 0-100 % SM 2540B Fecal Coliform (Sludge) 20429 col/g dry wt 7/21/20 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. z2z" �& — Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5.4.z�6 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:_336-751-1441 Address:_ 755 Yadkinville Rd Fax: —336-751-1442 Mocksville NC 27028 Email: brent.collinspemaresourcesinc.com Project: P.O.#: Attention:_ Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: mail referred), Fax, Mail St loda s) 3 5 D 2 MERITECH INC. / ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or 1D # Sampling Dates & Times Person Taking Sampie �� f Lab Use Only Start End Comp? Grab? # of Cont, Tests } Required e? es No pH OI<7 CIOK? Date Time Date Time 7/Zr 3 I? yAa s �A 7 v Temperature Upon Receipt: L Method of Shipment: *** Dechlorination <D.S m of Ammonia, Cyanide, Phenol and TKN sam les must be done in the field prior to preservation.*** Comments: Compositor # ❑ U PS Ijug # ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg Pl' ug/L ❑ Hand Delivery/ Relinquished by; Date: Time: /I: as o,N Received by: date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by; Date: Time; R eived b' ,), Date: ITV't- Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 8/20/2020 Date Sample Revd: 7/21/2020 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 07212012 Sample: Reidsville Composite 7/21/20 Total Solids Volatile Solids % Volatile Solids Week 1 0.710 0.460 0.648 Week 2 0.640 0.430 0.667 Week 3 0.470 0.310 0.657 Week 4 8.53 0.510 0.059 Week S 0.540 0.370 0.683 Van Kleek Reduction (%): -17.23 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 13-2011 B - A x I00 = % TOTAL SOLIDS 1313=D x I00 = % VOLATILE SOLIDS C / C WO # ] 1f C A 13 122110 Dry Wt Diff DATE SAMPLE USED DISH 4 TARP WT, Isf Dry Wt Fina! Dr Wt Gnal-initial TIME f 1 Z. 11 ANALYST F f D DATE TIME ANALYST DATE TrMR 4NALYST (initial ignition 550°C for 1 hour) BY: (repeat iginition 550°C for 30 minutes) AMPLE USED DISH # TARC 11523 2.7 . (initial ignition 550°C for I liour) BY: (repeat iginition 550°C for 30 minutes) SAMPLE g USED DISI-I t! I TART' (initial ignition 550°C for I hour) REP RTl D BY: (reiginition 550°C for 30 minutes) Ist Ignition Wt (g) Final Ignite Wt (g) Ignite Wt Diff (final -initial) % VOL SOLIDS 1Vt W I Final tion Wt (g) ' Final Ignite Wt (g) Dry Wt (g) I I+ Dry Wt Diff * TOT SOLIDS nitial) I % VOL SOLIDS inal DryWt Dry Wt Diff find -initial % TOT SOLIDS0.71 Ignite Wt Diff Ignite Wt Diff Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS {{//Ignition 4 pp D •5- DATE I SAMPLE U5ED I DISH # TARE 4VT. Dr Wt F' TIME 15131 .9 L �! 1NALYST `7 anal Dr FVt Dry Wt Diff * tinal-initial % TOT SOLIDS 11� (initial ignition 550°C for I hour) Ignition WI (g) Final Ignite Wt REPORTED BY: (repent iginition 550°C for 30 min) / l Accepfance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight most not change >4%or >50mg (0,0500g), whichever is less. (final -initial) I %VOL SOLIDS PERCENT TOTAL SOLIDS l PERCENT VOLATILE SOLIDS SM 2540 B-2011 B - A x 100 = % TOTAL SOLIDS B - DD x 100 = % VOLATILE SOLIDS C wed � Z C A B DATE Dry W t Diff SAMPLE U51 D 1D7SII # TARE WT. G�1st Dr Wt Final Dr Wt lino! -initial) I %TOT TIME 3 3 1 1• i0 . Q I ANALYST yarn 9• D Ignite Wt (initial ignition 550°C for 1 hour) 1st Ignition 4Vt (g) Final Ignite Wt (g) (final -in REP RTED BY: (repeat iginition 550°C fm• 30 minutes) 9 DATE SA PLE USED DISH # T'ARE 4VT. Dr Wt Final Dr '1Vl TIME l �� • Ala a � �� �' � ANALYST (initial ignition 550°C for I hour) Ignition Wt (g) Final Ignite Wt (g REP RTED BY: (repeat iginition 550°C for 30 minutes) Z DATE SAI IPLE g USED DISH # TARE WT. Dr W TIME .1 • t L41. ,a ANALYST % VOL SOLIDS Vt Diff -initia[) % TOT al-lnitial) I % VOL SOLIDS t Final Dr Wt Dry Wt Diff * final -initial % TOT SOLIDS 1. Ignite Wt Diff (initial ignition 550°C for 1 hour) Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS REP RTED BY: (repeat iginition 550°C for 30 minutes) 10 DATE SA LE g USED DISH # TARE WT. Dr TIME � }�5 3. . q it �y ANALYST WtW Final Dry Wt Dry Wt Diff * Cnal-initial %TOT SOLIDS c (initial ignition 5500C for I hour) Ignition Wt (g) Final Ignite Wt (g) REPORTED BY: (repeat iginition 5500C for 30 min) * Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change>4% or>50mg (0.0500g), whichever is less. at -initial) I % VOL PERCENT TOTAL SOLIDS 1 PERCENT VOLATILE SOLIDS SM 2540 B-2011 B - A x 100 = % TOTAL SOLIDS H - DD x 100 = % VOLATILE SOLIDS c \ C (initial ignition 550°C for I hour) (repeat iginition 550°C for 30 minutes) (initial ignition 55VC for I hour) (repeat iginition 550°C for 30 minutes) (initial ignition 550°C for I hour) (repeat iginition 550°C for 30 minutes) 1st Ignition Wt (g) Ignite Wt Diff * Final Ignite Wt (g) (final -initial) % VOL SOLIDS 3 •5741 D 0/. Ignition Wt (g) Mont Ignite Wt (g) Ignite Wt Diff * (final -initial) % VOL SOLIDS Sao. a5�04 3-+.95e:�r o o,/. Ignition Wt (g) Final Ignite Wt (g) Ignite Wt Diff * (final -initial) % VOL SOLIDS LA 1. QlLk+ - aF- `-L '1- U D - 3 0L -/- Ignite Wt Diff (initial ignition 550°C for 1 hour) Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS REPORTED BY: (repeat iginition 550°C for 30 min) tA1. a g Liy 'it. A SKy 3y' % Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less. PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 13 - A x 100 = % TOTAL SOLIDS C 13D x 100 = % VOLATILE SOLIDS C Ist Ignition Wt (g) Final Ignite Wt (g) fgnite AV Diff (final -initial) % VOL SOLIDS Ignition Wt (g) Final Ignite Wt (g) Ignite Wt Diff * (final -initial) % VOL SOLIDS Z!J Ignition Wt (g) Final Ignite Wt (g) Ignite 1Vt Diff * (final -initial) % VOL SOLIDS 9 Ignite Wt Diff * (initial ignition 5500C for 1 horn') Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS REPORTED BY: (repeat iginition 550°C for 30 min) * Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight most not change>4%or>50rng (0.0500g), whichever is less. WB484 PERCENT TOTAL SOLIDS 1 PERCENT VOLATILE SOLIDS GSM 2540 B-2011 I3 - A x 100 = % TOTAL SOLIDS C B - DD x 100 = % VOLATILE SOLIDS r C (initial ignition 550°C for I hour) (repeat iginitinn 5500C for 30 minutes) (initial ignition 550°C for I hour) (repent iginitinn 550°C for 30 minutes) (initial ignition 550°C for I hour) (repeat iginitinn 550C for 30 minutes) (initial iguitian 550°C for 1 hour) Ignition Wt lgntte Wt Diff REPORTED BY: (g) rival Ignite Wt (g) (final -initial) % VOL SOLIDS (repeat iginitinn 550°C for 30 min) � � L� � .� * Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat drylignife cycle, weight must not change >4% or>50mg (OA5UUg), whichever is less. 5-9.20M Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:336-751-1441 Address-.—755 Yadkinville Rd Fax: 336-751-1442 Mocksville NC 27028 Email: brent.collins@emaresourcesinc.com Project: P.Q.#: Attention:_ Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: mai referred), Fax, Mail Std 10da s) 3 5 D 24-48His p M ERITECH INC. 1 ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechiabs.com Sample Location and/or ID # Sampling Dates & Times person Taking e(Si n/Print): ��, f �a%nf Lab UseOnly Start End comp? Grab? #of Cont. Test(s) Required on lee? No pH OK? Cl QK? Date Time Date Time IQi �IsW�kr 7121 Temperature Upon Receipt: 1 S Method of Shipment: *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field pricir to preservation, *** Comments: Compositor # ❑ UPS Jug# ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg lnir ug/L ❑ Hand Delivery Relinquished by: Date: ]��( Time: Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received b : Date: Time: Relinquished by: Date; Time: eceive —) -) I y:y TirpQ�y AAIN UAL rA 1 HUhh:1N A1N V V hJU I UK A 1 I KACIIUN REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WWTP Name: Reidsville WWTP WQ Permit Number: WQ0002376 NPDES Number: NCO024881 Monitoring Period: From 10/1/2020 To 12/31 /2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermoplulic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIt. (1) Fecal Density 0 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ 1 Air Drying ❑ Composting ❑ JAerob1c Digestion ❑ Anaerobic Digestion 17 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g tY Number o Excee- dences Frequency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 812 1037 1699 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l VS reduction ❑ ( ) Alt. 2 40-day bench " ( y ) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O uptake) e.l (p z Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Bryan - WWTP Superintendent Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if (if applicable)(type or print) 2/8/2021 Signature eparer* ate Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact. Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Page 1 Report Date: 10/12/2020 Date Sample Rcvd: 10/5/2020 Meritech Work Order # 10052004 Sample: Reidsville 1 Grab 10/5/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.12 % 10/6/20 0-100 % SM 2540B Fecal Coliform (Sludge) 812 col/g dry wt 10/5/20 130 col/g dry wt SM 9222D Meritech Work Order # 10052005 Sample: Reidsville 2 Grab 10/5/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.06 % 10/6/20 0-100 % SM 2540B Fecal Coliform (Sludge) <858 col/g dry wt 10/5/20 858 col/g dry wt SM 9222D Meritech Work Order # 10052006 Sample: Reidsville 3 Grab 10/5/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.04 % 10/6/20 0-100 % SM 2540B Fecal Coliform (Sludge) 874 col/g dry wt 10/5/20 130 col/g dry wt SM 9222D Meritech Work Order # 10OS2007 Sample: Reidsville 4 Grab 10/5/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.05 % 10/6/20 0-100 % SM 2540B Fecal Coliform (Sludge) <866 col/g dry wt 10/5/20 866 col/g dry wt SM 9222D Meritech Work Order # 10052008 Sample: Reidsville 5 Grab 10/5/20 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.07 % 10/6/20 0-100 % SM 2540B Fecal Coliform (Sludge) <850 cal/g dry wt 10/5/20 850 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc, Environmental Laboratory Laboratory Certification No. 165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 10052009 Sample: Reidsville 6 Grab Parameters Result Analysis Date % Total Solids 1.07 % 10/6/20 Fecal Coliform (Sludge) 1699 col/g dry wt 10/5/20 Meritech Work Order # 10052010 Sample: Reidsville 7 Grab Parameters Result Analysis Date % Total Solids 1.07 % 10/6/20 Fecal Coliform (SIudge] 1699 col/g dry wt 10/5/20 Page 2 Report Date: 10/12/2020 Date Sample Rcvd: 10/5/2020 10/5/20 Reporting Limit Method 0-100 % SM 254013 130 col/g dry wt SM 9222D 10/5/20 Reporting Limit Method 0-100 % SM 2540B 130 col/gdry wt SM9222D I hereby certify that I have reviewed and approve these data. AMJEd(� Ha rv" L Laboratory Repr sentative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 ❑ ❑❑❑� a V o�rD�� w ��CL� lb X � Q O r C� G fD r"� � {� � .0 r`h / C S C S C Q � a a n n rD O S T7 Q1 C m N �. r 0- -s m o \� {� V'1 -•C w N - C rb3 rD m rD O rn ro rD o Z n a p o a CD QI O O m fa O 3 n a HTrn o D(DCq M �.n X o O 3 3 �• n n rp O ° v O n r+ W °' a, D `^ � N O Q Q O N Q rD a fD N fD- M 3 3 m ° 3 D C� �. o ° ❑ a v O m p CD r-F Z n 0 m < on Z3U rD Hof rt co m rro rD m 3 S p N O � D m a m a Q N A ul N C - C V+ v rb C o rr C �. a _ 7 C C O O _ tU 3. O fD o rpLn [� 1 T j c y n ► V 3 p ufDi N rD Oo to i Q Z3 rt O p T � V v+ fD X CD - p o x o o Ln �r � CL W W l to w [7 m ro va o S a Ul U r OP a Y Y C � rb 4:� 4�- n r ro w a N Y 3 r Ln C y 3 3 O fD a r p a c ro rD = Z ti �1 ❑ L; O 0 O d T� -� N - Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 11/5/2020 Date Sample Rcvd: 10/5/2020 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 10052003 Sample: Reidsville Composite 10/5/20 Total Solids Volatile Solids % Volatile Solids Week 1 1.31 0.810 0.619 Week 2 1.24 0.790 0.638 Week 3 1.25 0.810 0.648 Week 4 1.10 0.700 0.635 Week 5 1.00 0.650 0.651 Van Kleek Reduction (%): -14.74 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass =-In4 4K /-, LaboraioryR resentative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 59ze,6 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:_ 336-751-1441 Address:_ 755 Yadkinville Rd Fax: 336-751-1442 Mocksville NC 27028 Email:_ t)reni.colfinso emaresourcesinc.com Project; Attention:_ Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval, Std l0da s) 3_ 5 pays 24�49"rS Circle all that apply: Ema' preferred) , Fax, Mail M E R I T E C H INC. 1 ENVIRONMENTAL LABORATORIES ti 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com WWW.I'Y eritechIabS.com - - Sample Location and/or ID # Sampling Dates & Times Person Taking S pie (Si n/Prin i � I Lab Use Only Start End Camp? Grab? Hof cant, Test(s) Required Yes es N / IVa pH ? CI OK? Date Time Date Time oa 5 i 9. Temperature Upon Recelpt: �L Method of *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TO samples must be done in the field prior to preservation. *** Comments: /��,yFs �/�f� Compositor #Shipment: ❑ UPS # ❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ ,—,Juug Report results in: mg/L ❑ mg/kg L ug/L ❑ [� Hand Delivery Relinquished by: Date: Time: IQ/� `%Yla,,, Received by: Date: Time: EJ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: j ec ive jGT�ryq:f IA NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL012709 �5{i �141..tiL Client: James Albert Advisor: Brent Collins Predictive 381 Green Acres Dr EMA Resources Inc ;• Stokesdale, NC 27357 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 465896 Advisor ID: 405413 Sampled: Received: 11/09/2020 Completed: 11/24/2020 Farm: RC005 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 1.3 120-200 70 90 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.18 1.12 3.8 48 2.0 4.8 27 23 29 16 68 76 63 34 34 58 0.1 3 Sample ID: 00002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.7 120-200 130 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.18 1.15 3.5 60 1.4 5.4 7 34 33 22 50 218 148 47 47 49 0.1 3 Sample ID: 00003 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.8 120-200 100 60 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.13 1.13 5.2 71 1.5 5.3 16 40 43 24 82 49 46 33 33 34 0.1 2 Noah 0, olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL012709 James Albert Page 2 of 3 Sample ID: 00005 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.5 120-200 100 70 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.18 1.08 6.1 78 1.4 5.7 16 33 45 30 75 53 49 197 197 67 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032078 �5{i �141..tiL Client: Dan Stocks Advisor: Brent Collins Predictive 1612 Crutchfield Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 450848 Advisor ID: 405413 Sampled: Received: 06/11/2020 Completed: 06/18/2020 Farm: RC010 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 60 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 0.90 13.2 96 0.5 6.8 87 38 67 28 45 838 507 371 371 161 0.3 2 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032077 �5{i �141..tiL Client: Daisy Purgason Advisor: Brent Collins Predictive 6079 NC Hwy 65 EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 465895 Advisor ID: 405413 Sampled: Received: 06/11/2020 Completed: 06/18/2020 Farm: RC011 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 60 100 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 1.02 7.8 93 0.6 6.5 31 20 71 20 48 141 94 193 193 60 0.3 4 Noah 0' olina i I Awl' Futacii frum fuWCurnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032076 �5{i �141..tiL Client: Iris Sharpe Advisor: Brent Collins Predictive 913 Onslow Dr EMA Resources Inc ;• Greensboro, NC 27408 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 509177 Advisor ID: 405413 Sampled: Received: 06/11/2020 Completed: 06/18/2020 Farm: RC011 Sample ID: 00002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.6 120-200 0 20 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.13 1.05 4.7 74 1.2 5.4 76 66 41 27 55 79 64 187 187 30 0.1 2 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL016042 �5{i �141..tiL Client: Lawrence McCollum Advisor: Brent Collins Predictive 434 Truman Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 289332 Advisor ID: 405413 Sampled: Received: 11/20/2020 Completed: 12/18/2020 Farm: RC012 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 110 120 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 1.10 4.9 79 1.0 5.9 15 13 49 28 41 99 76 121 121 67 0.1 2 Noah 0' olina i I Awl' Futacii frum fuWCurnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL031359 �5{i �141..tiL Client: Lofton Lovelace Advisor: Brent Collins Predictive 3575 NC Hwy 150 EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 219281 Advisor ID: 405413 Sampled: Received: 05/27/2020 Completed: 06/03/2020 Farm: RC041 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 0.91 20.5 92 1.7 6.3 240 100 61 28 48 310 198 537 537 264 0.1 0 Sample ID: 00004 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 0.95 12.6 86 1.8 6.0 530 57 74 10 46 248 165 602 602 289 0.1 1 Noah 0' olina i I Awl' fotciW frum fuWCurnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL002213 �5{i �141..tiL Client: Thomas / Tommy Carter Advisor: Brent Collins Predictive 381 King Carter Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 480518 Advisor ID: 405413 Sampled: Received: 08/11/2020 Completed: 08/19/2020 Farm: RC119 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.05 16.6 92 1.4 6.3 411 250 59 25 70 400 252 701 701 400 0.1 1 Sample ID: 00002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.09 13.4 97 0.4 7.0 137 53 62 33 39 452 273 463 463 207 0.1 1 Sample ID: 00005 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.6 120-200 0 40 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.15 9.4 82 1.7 5.7 202 53 61 18 55 312 204 490 490 202 0.1 1 Noah 0' olina I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL002213 Thomas / Tommy Carter Page 2 of 4 Sample ID: 00006 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 100 0 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 1.09 8.2 84 1.3 6.1 16 129 51 26 43 1493 912 80 80 139 0.1 1 Sample ID: 00008 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.24 5.5 79 1.2 5.9 100 31 58 19 52 1009 622 148 148 93 0.1 2 Sample ID: 00010 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.13 8.4 88 1.0 6.2 108 224 51 24 60 447 282 179 179 67 0.0 Sample ID: 00011 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.5 120-200 70 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.15 8.1 80 1.6 5.7 30 44 52 25 56 784 487 119 119 104 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL002213 Thomas / Tommy Carter Page 3 of 4 Sample ID: 00012 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.9 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.11 7.2 73 1.9 5.5 109 89 48 19 54 789 490 146 146 121 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032544 �5{i �141..tiL Client: Thomas / Tommy Carter Advisor: Brent Collins Predictive 381 King Carter Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 480518 Advisor ID: 405413 Sampled: Received: 06/23/2020 Completed: 07/01/2020 Farm: RC119 Sample ID: 00004 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.98 9.1 86 1.3 5.9 380 28 72 12 72 160 113 296 296 353 0.2 2 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO32544 Thomas / Tommy Carter Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-1 zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL031365 �5{i �141..tiL Client: Thomas / Tommy Carter Advisor: Brent Collins Predictive 381 King Carter Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 480518 Advisor ID: 405413 Sampled: Received: 05/27/2020 Completed: 06/03/2020 Farm: RCr119 Sample ID: 00009 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.91 14.3 91 1.3 6.4 319 47 62 27 46 190 124 321 321 216 0.1 1 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032079 �5{i �141..tiL Client: James Jones Advisor: Brent Collins Predictive 210 Griffin Rd. EMA Resources Inc ;• Stokesdale, NC 27357 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 384685 Advisor ID: 405413 Sampled: Received: 06/11/2020 Completed: 06/18/2020 Farm: RC125 Sample ID: 00004 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 50 70 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 0.85 9.8 93 0.7 6.6 39 34 62 30 41 233 148 286 286 105 0.1 1 Noah 0, olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032543 �5{i �141..tiL Client: State of NC Advisor: Brent Collins Predictive 1612 Crutchfield Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. +_ Soil Report Mehlich-3 Extraction Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 442976 Advisor ID: 405413 Sampled: Received: 06/23/2020 Completed: 07/01/2020 Farm: RC126 Sample ID: 0002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.3 120-200 0 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 1.06 6.1 84 1.0 5.8 94 42 62 19 39 180 125 151 151 ill 0.1 2 Sample ID: 0005 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.3 120 - 160 0 50 0 0 0 0 0 0 Note: 3 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 1.12 6.1 84 1.0 5.8 98 44 61 19 37 183 127 156 156 100 0.1 2 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL002212 �5{i �141..tiL Client: Dennis Williams Advisor: Brent Collins Predictive 140 Andy Trail EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 441122 Advisor ID: 405413 Sampled: Received: 08/11/2020 Completed: 08/19/2020 Farm: RC128 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.7 120-200 110 60 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 1.03 11.7 86 1.6 5.5 14 41 47 37 38 132 96 64 64 93 0.1 1 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL032075 �5{i �141..tiL Client: Ken Martin Advisor: Brent Collins Predictive 551 Bakers Cross Rd EMA Resources Inc ;• Reidsville, NC 27320 755 Yadkinville Rd f'. Soil Report Mehlich-3 Extraction +_ Mocksville, NC27028 Sampled County : Rockingham Links to Helpful Information Client ID: 329325 Advisor ID: 405413 Sampled: Received: 06/11/2020 Completed: 06/18/2020 Farm: RC130 Sample ID: 00001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.16 6.0 83 1.0 6.0 182 33 69 11 61 195 134 144 144 94 0.2 3 Noah 0' olina i I Awl' Futaw frum FwW Curnml5skm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture