WQ0030998_Residual Annual Report 2020_20210226

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?*
Annual Report Year*
Permit Number (IR)*
Applicant/Permittee
Email Notifications
.......................................................... .............
Does this need review by the hydrogeologist?*
Regional Office
CO Reviewer
Admin Reviewer
* Annual Report
* Residual Annual Report
r Additional Information
r Other
2020
W00030998
Triple S Farms and Cleaning, Inc.
0 Yes r No
Wilmington

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Robert T. Branch
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ..........................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363129007
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0030998
Fbs Current Existing perrrit number
Applicant/Permittee Address* PO Box709 Beulaville, NC 28518
Facility Name * Triple S Farms and Cleaning RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
ar_2020_SSS-Final.pdf 10.22MB
Upload only 1 PCF document (less than 250 fvB). Miltiple documents rust be combined into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/26/2021

2020 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2021

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 26, 2021
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2020 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2020 Application Summary Table, and 11) 2020 Application Condition Summaries.
A total of 4,090,018 gallons (411.46 dry tons) of Class B lime -stabilized biosolids or Class B fecal and
injected/incorporated biosolids were land applied to 116.4 acres in 2020. This material was divided as follows:
• 230,000 gallons (19.85 dry tons) from Beulaville WWTP,
• 1,707,480 gallons (167.32 dry tons) from Clayton Little Creek WRF,
• 66,038 gallons (1.40 dry tons) from Kenansville WWTP,
• 0 gallons (0 dry tons) from Rose Hill WWTP,
• 406,300 gallons (63.34 dry tons) from Warsaw WWTP,
• 60,000 gallons (6.36 dry tons) from Southwest Plantation WWTP, and
• 1,566,200 gallons (153.18 dry tons) from Wallace WWTP.
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Sincer
v
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville
Town of Rose Hill Town of Warsaw
Southwest Plantation Town of Wallace
Town of Clayton

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2020 Application Summary Table
XI 2020 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County: Duplin Year: 2020
Facility Name (as shown on permit): Triple S Farms & Cleaning
Land Application Operator: Triple S Farms & Cleaning Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
A Yes El No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A Residuals Application Summary:
Total number of application fields in thepermit:
9
Total number of fields utilized for land application during the year:
8
Total amount of dry tons applied during the year for all application sites:
411.46
Total number of acres utilizes for land application during the year:
1116.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Cl Yes El No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print)
Signature of Permittee Date
See Attached
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (1212006)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part B - Annual Comulance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1.13 below) issued by the Division of Water Quality. U Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permlt.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CPR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Pen -nit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signat a Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF CLAYTON
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. i Yes U No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Si�grtature of Preparer* Date
(if different from Perrnittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF KENANSVILLE
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 10 Yes U No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the pennit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
rw R a-aL •a
Signature f Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTHWEST PLANTATION
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. -,: Yes O No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) 1'he facility did not exceed any of the Pollutant Concentration Limits in I SA NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations arc
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13)-Mi baffc-, , ui=ment""pecifiedron•the"permit were -maintained -during -each application -of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility 9fAges pad hnprisonment for knowing violations."
of
ZC/
Date
fferent from Permittee)
parer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WALLACE
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. j Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
�1 ; �f i J 2/-YoZl
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Ll Yes L3 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the pennit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached,
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in I5A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in l5A NCAC 02T .I I05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general reyuirelients in as specified in the Land Application Permit were complied with (applicable to* CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations,
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
rgrt C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
JZ-/— ty- &2/1
Signat a of Pr parer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998 Laboratory: 1) Environmental Chemists
Facility Name: Triple S Farms & Cleaning 2)
Residual Source WQ # or NCO026018 3)
NPDES #: 4)
W WTP Name: Town of Beulaville VIW 1'P
5)
PaT=eter
11 g g
Ceiling
Cone.
Limit
Sample or Composite Date
BE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false inPrmation, including the possibility of fines and imprisonment for Imowing violations."
Signature of PrFpar r
*Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26)
C�r --2G-2I
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0023178 Laboratory: 1) Waypoint Analytical
Facility Name: Town of Clayton 2)
Residual Source WQ # or
NPDFS #:
NCO025453
WWTP Name: Little Creek Water Reclamation Facility
i?ne'Au.ni Annlveie nata
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m
Sample or Composite
Date
2/zon_02o
Percent Solids (%)
NA
2.35
Arsenic
75
<20.8
Cadmium
85
<4.1 7
Copper
4,300
164.00
Chromium
NA
16.40
Lead
840
<12.5
Mercury
57
<0.625
Molybdenum
75
<10.4
Nickel
420
11.60
Selenium
100
<20.8
"Zinc
7,500
492.00
Total Phosphorus
NA
28,400
TKN
NA
59,600
Ammonia- Nitrogen
NA
10,200
Nitrate and Nitrite
NA
642
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalQt;4;,:,4
ies for submitting false information, including the possibility of fines and imprisonment for knowing violations."
.
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCA.0 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL .RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
NCO036668
WWTP Name: Town of Kenansville WWTP
Dave ival An'luele 7late
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sam le or Composite Date
6/10/2020
Percent Solids (%)
NA
0.51
Arsenic
75
57.50
Cadmium
85
<48.00
Copper
4,300
353.00
Chromium
NA
<48.00
Lead
840
<48.00
Mercury
57
<3.28
Molybdenum
75
<48.00
Nickel
420
<48.00
Selenium
100
<48.00
Zinc
7,500
763.00
Total Phosphorus
NA
9,050
TKN
NA
33,200
Ammonia -Nitrogen
NA
<19.60
Nitrate and Nitrite
NA
81
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." '
Signature oTPreparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

I
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
WWTP Name:
R 'd I A 1' D to
WQ0029601
W Southwest Plantation WTP
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
est ua na sts
Parameter
(mgtkg)
a
Ceiling
Conc.
Limit
Sample or Compopite Date
3/4l2020
Percent Solids (° o)
NA
254
Arsenic
75
1 965
Cadmium
85
•=9,65
I
Copper
4,300
15800
Chromium
NA
1280
,
Lead
840
<9.65
Mercury
57
<0.614
Molybdenum
75
<9.65
Nickel
420
<9.65
Selenium
100
<9.65
Zinc
7,500
85400
Total Phosphorus
NA
16.200
TKN
NA
77.200
Ammonia -Nitrogen
NA
4.130
f
Nitrate and Nitrite
NA
64
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure tha uali d personnel properly gathered and evaluated the information submitted. I am aware that there a
Signal re of Prepare '
•Ilr arer is derined in 40 CFR Part 503.9(r) and i 5A NCAC 2T .1102 (26)
Z.M-Zi
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S .Farms & Cleaning
Residual Source WQ # or
NPDES #:
WWTP Name:
NC0003450
Town of Wallace WWTP
Laboratory: 1) Environmental Chemists, Inc.
2)
3)
4)
5)
Residual Analysis Data
Parameter
(mg/kg)
Ceiling
Cone.
Limit
Sam
le or Com
osite
Date
4/20/2020
2.84
7nzl2ozo
2.44
11/30/2020
2.05
1/6/2020
1.74
Percent Solids (%)
NA
<17.30
<17.30
35.20
<19.70
<24.10
<24.10
Arsenic
Cadmium
75
85
<t 1.70
<11.70
669.00
27.10
754.00
33.90
795.00
35.70
Copper
Chromium
4,300
NA
989.00
32.50
47.20
3.46
<17.30
<17.30
<17.30
1110.00
21,300
45.60
1.20
<19.70
25.60
<19.70
1310.00
21,300
48.00
0.96
<24.10
<24.10
13 440.0
13.00
1,950
Lead
840
64.90
Mercury
Molybdenum
57
75
1.97
<I 1.70
22.10
<11.70
1400.00
24,400
Nickel
420
100
7,500
NA
Selenium
Zinc
Total Phosphorus
17,800
54,300
34,300
,j KN
NA
35,000
4,130
8,460
<4.88
ia-Nitrogen
[�N!it!mEte
NA
<5.75
1 sec
1
Al P K
and pN. Values
from
3
the previous
4/20/20
were used
in the calcuations.
4,650
Envirochem
and Nitrite
NA
3,050
f 11
* For this sample. Envirochem did not perform the o osmg ana y , , ,
rting period. Discussion with Envirochem are continuing
exported the data late to have another sample performed during the correct repo
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed_ The parameters can be reported in FORM RSSF- B
WQ Permit Number. WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
NCO021903
VVVVTP Name: Town of Warsaw WWTP
Laboratory: 1) Environmental Cbemists
2)
3)
4)
5)
Parameter
(mg&g)
Ceiling
Conc.
Limit
Sample or Composite Date
-
�kvjnf Mir,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assJ�e that qial"ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
oen�flties fod;jj mitting false information, including the possibility of fines and imprisonment for knowing violations."
�' 0 3 "IM-5
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 105.86
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series NoA
Acres Used: 34.2 Acres Permitted: 34.2 Site #: 1 Field #: i
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
BL 2020-076461-2020-1-28 CL 20-055-0 WL-3-2020- WL-3-2020. BL 2020-07 KV 2020-0t
Sample
or Com-
posite
Date
5/7/20
1/6/20
2/20/20
7/22/20
7/22/20
5/7/20
6/10/20
% Solids
2.07
1.74
2.35
2.44
2.44
2.07
0.51
Arsenic
30.70
11.70
20.80
35.20
35.20
30.70
57.50
Cadmium
23.20
11.70
4.17
19.70
19.70
23.20
48.00
Chromium
23.20
32.50
16.40
33.90
33.90
23.20
48.00
Copper
436.00
989.00
164.00
754.00
754.00
436.00
353.00
Lead
29.60
64.90
12.50
45.60
45.60
29.60
48.00
Mercury
2.02
1.97
0.63
1.20
1.20
2.02
3.28
Molyb-
denum
23.20
11.70
10.40
19.70
19.70
23.20
48.00
Nickel
23.20
22.10
11.60
25.60
25.60
23.20
48.00
Selenium
23.20
11.70
20.80
19.70
19.70
23.20
48.00
Zinc
1880.00
1400.00
492.00
1310.00
1310.00
1880.001
763.00
Total
Phos-
horus
14,400
24,400
28,400
21,300
21,300
14,400
9,050
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�o
O
a
0.18
0.19
1.12
fl.80
0.59
0.18
0.04
s,
Arsenic
0.01
0.00
0.05
0.06
0.04
0.01
0.00
0.18
Cadmium
0.01
0.00
0.01
0.03
0.02
0.01
0.00
0.09
Chromiurr
0.01
0.01
0.04
0.05
0.04
0.01
0.00
0.16
Copper
0.15
0.38
0.37
1.21
0.89
0.15
0.03
3.18
Lead
1 0.01
0.02
0.03
0.07
1 0.05
0.01
0.00
0.20
Mercury
0.00
0.00
1 0.00
0.00
0.00
0.00
0.00
1
0.01
Molyb-
0.01
0.00
0.02
0.03
0.02
0.01
0.00
0.10
denum
Nickel
0.01
0.01
0.03
0.04
0.03
0.01
0.00
0.13
enium
0.01
0.00
0.05
0.03
0.02
0.01
0.00
0.13
0.66
0.53
1.10
2.10
1.54
0.66
0.06
6.67
[hf
5.09
9.32
63.47
34.22
25.09
5.09
0.74
143.02
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
Information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
74--%� - -_
Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series
8.48
Acres Permitted: 8.48 Site #:
Field #:
47.92
n/a
FoA
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WR 2020-076451-202GA-30 CL 20-055-0 WL-3-2020• CL 20-0554
Sample
or Com-
posite
Date
5/7/20
4/20/20
2/20/20
7122/20
2/20/20
Solids
3.30
2.84
2.35
2.44
2.35
Arsenic
30.10
17.30
20.80
35.20
20.80
Cadmium
14.90
17.30
4.17
19.70
4.17
Chromium
21.20
27.10
16.40
33.90
16.40
Copper
258.00
669.00
164.00
754.00
164.00
Lead
26.80
47.20
12.50
45.60
12.50
Mercury
0.85
3.46
0.63
1.20
0.63
Molyb-
denum
17.30
17.30
10.40
19.70
10.40
Nickel
14.90
17.30
11.60
25.60
11.60
Selenium
14.90
17.30
20.80
19.70
20.80
Zinc
748.00
1110.00
492.00
1310.00
492.00
Total
Phos-
horus
16,500
21,300
28,400
21,300
28,400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�o
r.1 >
O
a ?. 0
" w�
0.88
1.62
1.52
0.51
1.11
a
iA
Arsenic
0.05
0.06
0.06
0.04
0.05
0.25
Cadmium
0.03
0.06
0.01
0.02
0.01
0:12
Chrorniurr
0.04
0.09
0.05
0.03
0.04
0.25
Copper
0.45
2.17
0.50
0.78
0.36
4.26
Lead
0.05
0.15
0.04
0.05
0.03
0.31
Mercury
0.00
0.01
0.00
0.00
0.00
0.02
Molyb-
denum
0.03
0.06
0.03
0.02
0.02
0.16
Nickel
0.03
0.06
0.04
0.03
0.03
0.17
Selenium
0.03
0.06
0.06
0.02
0.05
0.21
Zinc
1.31
3.60
1.50
1.35
1.09
8.86
Total
Phos-
28.92
69.13
86.58
21.93
63.20
269.76
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possi ility of fines and imprisonment for knowing violations"
�e- ,� ' - Qa Q
Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual):
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only):
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series
59.93
n/a
FoA
Acres Used: 21 Acres Permitted: 21 Site #: 1 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WR 2020.07645 2020-07646 CL 20.055-0 WL-3-2020 CL 20.0554
Sample
Com-
orite
posite
Date
5/7/20
5/7/20
2/20/20
7/22120
2/20/20
7/6 Solids
3.30
2.07
2.35
2A4
2.35
Arsenic
30.10
30.70
20.80
35.20
20.80
Cadmium
I4.90
23.20
4.17
19.70
4.17
Chromium
21.20
23.20
16.40
33.90
16.40
Co per
258.00
436.00
164.00
754.00
164.00
Lead
26.80
29.60
12.50
45.60
12.50
Mercury
0.85
2.02
0.63
1.20
0.63
Molyb-
denum
17.30
23.20
10.40
19.70
10.40
Nickel
14.90
23.20
11.60
25.60
11.60
Selenium
14.90
23.20
20.80
19.70
20.80
Zinc
748.00
1880.00
492.00
1310.00
492.00
Total
Phos-
horus
16,500
14,400
28,400
21,300
28,400
Annual Heavy Metal Field Loadings (Calculated in ibs/acre):
o
m d
e
9 0
0.16
0.20
1.02
0.49
0.99
in
Arsenic
0.01
0.01
0.04
0.03
0.04
0.14
Cadmium
0.00
0.01
0.01
0.02
0.01
0.05
Chromium
0.01
0.01
0.03
0.03
0.03
0.11
Copper
0.08
0.17
0.33
0.74
0.32
1.65
Lead
1 0.01
0.01
1 0.03
0.04
0.02
1
0.12
Mercury
0.00
0.00
1 0.00
0.00
0.00
0.00
Molyb-
denum
0.01
0.01
0.02
0.02
0.02
0.08
Nickel
0.00
0.01
0.02
0.03
0.02
0.09
Selenium
0.00
0.01
0.04
0.02
0.04
0.12
Zinc
0.23
0.74
1.00
1.29
0.97
4.24
Total
Phos-
5.15
5.68
57.89
20.91
56.28
145.90
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
,�; - e
Signature of Land Applier Date
Author Darvl D Merritt nFNR Ft•1RM eeFl cG 17mnrnn

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 7.37
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 4.14 Acres Permitted: 4.14 Site #: 1 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
we imn.MKea n.nac_nnnl CUID 'min.,
Sample
or Com-
posite
Date
5/7/20
2120/20
314/20
% Solids
3.30
2.35
2.54
Arsenic
30.10
20.80
9.65
Cadmium
14.90
4.17
9.65
Chromium
21.20
16.40
12.80
Copper
258.00
164.00
158.00
Lead
26.80
12.50
9.65
Mercury
0.85
0.63
0.61
Molyb-
denum
17.30
10.40
9.65
Nickel
14.90
11.60
9.65
Selenium
14.90
20.80
9.65
Zinc
748.00
492.00
854.00
Total
Phos-
horus
16,500
28,400
16,200
Annual Heavy Metal Field Loadinus (Caleulated in Ihs/aerel-
m°
1.31
0.16
0.31
c
0
w �
�
o n
••
Arsenic
0.08
0.01
0.01
0.09
Cadmium
0.04
0.00
0.01
0.05
Chromium
0.06
0.01
0.01
0.07
Copper
0.68
0.05
0.10
0.83
Lead
0.07
0.00
0.01
0.08
Mercury
0.00
0.00
0.00
0.00
Molyb-
denum
denum
0.05
0.00
0.01
0.05
Nickel
0.04
0.00
0.01
0.05
Selenium
0.04
0.01
0.01
0.05
Zinc
1.96
0.16
0.52
2.65
Total
Phos-
43.33
9.14
9.95
62.42
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 34.75
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 11.2 Acres Permitted: 11.2 Site #: I Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WL 2-2020-4-302020-076a5 CL 20-055-0
Sample
Com-
orite
posite
Date
4/20/20
5/7/20
2/20/20
% Solids
2.84
3.30
2.35
Arsenic
17.30
30.10
20.80
Cadmium
17.30
14.90
4.17
Chromium
27.10
21.20
16.40
Copper
669.00
258.00
164.00
Lead
47.20
26.80
12.50
Mercury
3.46
0.85
1 0.63
Molyb-
denum
17.30
17.30
10.40
Nickel
17.30
14.90
11.60
_
Selenium
17.30
14.90
20.80
Zinc
1110.00
748.00
492.00
a
Total
Phos-
horus
21,300
16,500
28,400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
A�+
y
1.63
1.31
0.16
�a
y
a�
Arsenic
0.06
0.08
0.01
0.14
Cadmium
0.06
0.04
0.00
0.10
Chromium
0.09
0.06
0.01
0.15
Copper
2.18
0.68
0.05
2.91
Lead
0.15
0.07
0.00
0.23
Mercury
0.01
0.00
0.00
0.01
Molyb-
0.06
0.05
0.00
0.11
denum
Nickel
0.06
0.04
0.00
0.10
Selenium
0.06
0.04
0.01
0.10
Zinc
3.61
1,97
0.16
5.74
Total
Phos-
69.28
43.38
9.19
121.86
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibilitv of fines and imprisonment for knowing violations"
Signature of Land Applier Author Darvl D. Merritt Date nFNR FORM RAFI RF r7/*)nn9i

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual): 13.21
WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Eric Smith Owner: Eric Smith Predominant Soil Series GoA
13.95 Acres Permitted: 13.95 Site #: 1 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WR 2020-07645
1
low
®
By, 1 i
. s
Annual Heavy Metal Field Loadings Calculated In lbs/acre :
1�
VIM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
Information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual):
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only):
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series
111.00
n/a
FoA
Acres Used: 14.5 Acres Permuted: 14.5 Site #: 1 Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WL 1-2020-1-28 P 2020 4-13 WL-3-2020-1CL20-055-1 WL-3-2020 C1-20-035-1
Sample
or Com-
posite
Date
1/6/20
314/20
7/22/20
2/20/20
7/22/20
2/20/20
% Solids
1.74
2.54
2.44
2.35
2.44
2.35
Arsenic
11.70
9.65
35.20
20.80
35.20
20.80
Cadmium
11.70
9.65
19.70
4.17
19.70
4.17
Chromium
32.50
12.80
33.90
16.40
33.90
16.40
Copper
989.00
158.00
754.00
164.00
754.00
164.00
Lead
64.90
9.65
45.60
12.50
45.60
12.50
Mercury
1.97
0.61
1.20
0.63
1.20
0.63
Molyb-
denum
11.70
9.65
19.70
10.40
19.70
10.40
Nickel
22.10
9.65
25.60
11.60
25.60
11.60
Selenium
11.70
9.65
19.70
20.80
19.70
20.80
Zinc
1400.00
854.00
1310.00
492.00
1310.00
492.00
Total
Phos-
horns
24,400
16,200
21,300
28,400
21,300
28,400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
< 9,
1.38
0.09
1.68
2.90
0.55
1.06
Y
N
7
Arsenic
0.03
0.00
0.12
0.12
0.04
0.04
Q.36
Cadmium
0.03
0.00
0.07
0.02
0.02
0.01
0.15
Chromiurr
0.09
0.00
0.11
0.10
0.04
0.03
0.37
Copper
2.73
0.03
2.54
0.95
0.83
0.35
7.42
Lead
0.18
0.00
1 0.15
0.07 1
0.05
0.03
0.48
Mercury
0.01
0.00
0.00
0.00
0.00
0.00
0.02
Molyb-
denum
0.03
0.00
0.07
0.06
0.02
0.02
0.20
Nickel
0.06
0.00
0.09
0.07
0.03
0.02
0.27
Selenium
0.03
0.00
0.07
0.12
0.02
0.04
0.29
Zinc
3.87
0.15
4.41
2.85
1.43
1.04
13.75
Total
Phas-
67.40
2.84
71.74
164.68
23.32
59.97
389.95
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibili of fines and imprisonment for knowing violations"
�[��{
Signature of Land Applier Date
Authr►r I�arvl n 11Aarritt r1CK10 CI'1DI1A KACI or n1nnnn%

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 31.41
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 8.93 Acres Permitted: 8.93 Site #: 1 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
SWP 2020 4-13 P 2020 4-13 BL 202M7E CL 20-055-1 WR 2020-0 CL 20.0554 sure 202f),
Sample
or Com-
posite
Date
3/4/20
3/4/20
5/7/20
2/20/20
5/7/20
2/20/20
3/4/20
% Solids
2.54
2.54
2.07
2.35
3.30
2.35
2.54
Arsenic
9.65
9.65
30.70
20.80
30.10
20.80
9.65
Cadmium
9.65
9.65
23.20
4.17
14.90
4.17
9.65
Chromium
12.80
12.80
23.20
16.40
21.20
16.40
12.80
Copper
158.00
158.00
436.00
164.00
258.00
164.00
158.00
Lead
1 9.65
9.65
1 29.60
12.50
26.80
12.50
9.65
Mercury
0.61
0.61
2.02
0.63
0.85
0.63
0.61
Molyb-
denum
9.65
9.65
23.20
10.40
17.30
10.40
9.65
Nickel
9.65
9.65
23.20
11.60
14.90
11.60
9.65
Selenium
9.65
9.65
23.20
20.80
14.90
20.80
9.65
Zinc
854.00
854.00
11880.00
492.00
748.00
492.00
854.00
Total
Phos-
horus
16,200
16,200
14,400
28,400
16,500
28,400
16,200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
-<o
�! 0
0.14
0.14
0.41
0.33
2.16
0.20
0.14
y
Arsenic
0.00
0.00
0.02
0.01
0.13
0.01
0.00
0.18
Cadmium
0.00
0.00
0.02
0.00
0.06
0.00
0.00
0.10
Chromium
0.00
0.00
0.02
0.01
0.09
0.01
0.00
0.14
Copper
0.04
0.04
0.35
0.11
1.11
0.06
0.04
1.78
Lead
0.00
0.00
0.02
0.01
0.12
0.00
0.00
0.16
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
enum
denum
0.00
0.00
0.02
0.01
0.07
0.00
0.00
0.11
Nickel
0.00
0.00
0.02
0.01
0.06
0.00
0.00
0.10
Selenium
0.00
0.00
0.02
0.01
0.06
0.01
0.00
0.11
Zinc
0.24
0.24
1.53
0.32
3.23
0.19
0.24
6.00
Total
Phos-
4.61
4.61
11.69
18.70
71.19
11.24
4.61
126.66
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including thss' ity of fines and imprisonment for knowing violations"
Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu — Copper
Pb —
Lead
Hg — Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #:
Owner: Eric Smith nnual Dry Tons Applied: 105.86 Site #:
Operator: Eric Smith Predominat Soil Series NoA
Crop 1 Name: Bermudagrass Crop 1 Max PAN: 299.00 Crop 2 Name:
1 Acres Utilized: 34.20
Acres Permitted: 34.20
Cation Exchange Capacity (non 503): NA
#NIA
Crop 2 Max. PAN
#N/A
_ 0
CD
� o
`�
Specify
Totals
Per Acre
o, o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
1=1,s
v
3 •o
re
Q
<
e
X _
� -
Co
>'
� n
F �
t
+
o'
TKN
a
z 0
o �
g
m
Nitrate
and
Nitrite
mtVkr
PAN Applied
(Ib,/acre)
Must Select
CropI or Crop
p
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop I
Crop 2
Mar-20
70,000
2,047
2.07
0.18
Beulavik - WWTP
S
0.50
0.30
55,600
5
7,740
8.63
X
Mar-20
90,000
2,632
1.74
0.19
Wallace wwTP
INC
1.00
0.30
35,000
6
3,050
5.18
X
Jul-20
390,000
11,404
2.35
1.12
Little Creek WRF
S
0.50
0.30
59,600
10,200
642
45.96
X
Jul-20
270,000
7,895
2.44
0.80
Wallace WWTP
INC
1,00
0.30
54,300
8,460
3
35.69
X
Aug-20
198,000
5,789
2.44
0.59
walbm wwrP
INC
1.00
1 0.30
54,300
8,460
3
26.17
X
Sep-20
70,000
2,047
2.07
0.18
Beulaville WWTP
S
0.50
0.30
55,600
5
7,740
8.63
X
Oct-20
66,038
1,931
0.51
0.04
Kenansville WWTP
S
0.50
0.30
33,200
20
81
0.82
X
TOTALS:
33,744
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.18
0.09
0.16
3.18
0.20
0.01
0.10
0.13
0.13
6.67
143.02
131.08
0.00
Date
lbs/ac
Current Cumulative lbs/acre
.. ............. .
0.94 0.83 NA J 47.62 4.46 0.09 NA 1.64 1.04 96.21
0.77 0.74 NA 44.44 4.25 0.08 NA 1.51 0.92 89.53
36 34 NA 1,338 267 15 NA 374 89 2,498
299 #N!A
Prior Years Cumulative Ibslacre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
-� *Application Method: S - Surface, IN - injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0,2,
Date Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rat
UENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner:
Operator:
Eric Smith
Eric Smith
Crop I Name: Betmudasrass
WQ Permit #:
nnual Dry Tons Applied:
WQ0030998 Field #:
47.92 Site #:
Acres Utilized:
Acres Permitted:
Predominat Soil Series FoA Cation Exchange Capacity (non 503):
Crop 1 Max PAN: 276.00 Crop 2 Name: Wheat Crop 2 Max. PAN
8.48
8.48
NA
50.00
:'::
o K
Specify
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DT;Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(may
Wet,
Moist)
Precip.
Past 24
Hrs.
tomes
s =
e m
a o.
'
<
;y a
ti w
* N
+ w
3
7d
w
; �
o
TKN
m A
z 3
�o c
R.
o c
Nitrate
and
Nitrite
PAN Applied
(Ibs/acre)
Must Select
Clop 1 or Crop
2
Gal.
Cu-Yd.
Report
Tot''
in Gal.
Crap I
Crop 2
Crop I
Crop 2
Mar-20
5400
6,368
3.30
0.88
Warsaw WwTP
S
0.50
0.30
39,700
3
1,910
24.22
X
Jun-20
116,200
13,703
2.84
1.62
Wallace WWTP
INC
1.00
0.30
17,800
4,130
1
26.72
X
Jul-20
131,900
15,554
2.35
1.52
Link Cmek WRr•
S
0.50
0.30
59,600
10,20D
642
62.68
X
Aug-20
42,900
5,059
2.44
0.51
Wallace WWTP
INC
1.D0
0.30
1 54,300
8,460
3
22.87
X
Nov-20
96,290
11,355
2.35
1.11
Little Cmek WRF
S
0.50
0.30
59,600
10,200
642
45.76
X
#52,
TOTALS:
0=39
.•
As
Cd
Cr
Cu
Pb
He
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
Annuallbs/acre
0.25
0.12
0.25
4.26
0.31
0.02
0.16
0.17
0.21
8.86
269.76
136.49
45.76
Date
lbs/ac
Current Cumulative lbs/acre
0.94 0.80 NA 40.56 3.89 0.09 NA 1.50 0.96 78.77 . • . •
0.69 J 0.67 NAa 36.29 3.58 0.07 NA 133 1 0.75 69.91
36 34 NA 1 1,338 267 15 NA 374 89 2,498
276 50.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R-****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
jJhT4/� J _3-/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
oz�**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier
Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading R t
17ENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner:
Operator:
Eric Smith
Eric Smith
Crop 1 Name: Bermadagmss
WQ Permit #: WQ0030998 Field #:
nnual Dry Tons Applied: 59.93 Site #:
Predominat Soil Series FoA
Crop 1 Max PAN: 276.00 Crop 2 Name:
Acres Utilized: 21.00
Acres Permitted: 21.00
Cation Exchange Capacity (non 503): NA
Wheat
Crop 2 Max. PAN
50.00
a
.. a
Specify
Totals
Per Acre
,,
o Solids
As
Decimal
Volume
Applied per
Acre
DT]Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(
Wet,
Moist)
Precip.
Past 24
Hrs.
lnclars
fl
K o
� _.
L
a m
_
?
; ^:
�. m
0
?
7d �'
�'
:3k
I
Z 3
an c
`; =
m
Nitrate
and
Nitrite
PAN Applied
(lbs/acre)
Must Select
Crop I or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Mar-20
23,800
1,133
3.30
0.16
Watsaw WWTP
S
0.50
0.30
39,700
3
1,910
4.31
X
May-20
48,000
2,286
2.07
0.20
Beulaville wwrP
S
0.50
0.30
55,600
5
7,740
9.64
X
Jun-20
218,400
10,400
2.35
1.02
LitlkCmek WRF
S
0.50
0.30
59,600
10,200
642
41.91
X
Aug-20
101,300
4,824
244
0.49
Wsitace WWTP
INC
1.00
0.30
54,300
8,460
3
21.81
X
Nov-20
212,330
10,111
2.35
0.99
Little Cmek WRF
S
0.50
030
59,600
10,200
642
40.75
X
TOTALS:
28,754
As
Cd
Cr
Cu
Pb
H2
Mo
Ni
Se
Zn
P
PAN i
PAN 21
Lime Applied
Annual lbs/acre
0.14
0.05
0.11
1.65
0.12
0.00
0.08
0.09
0.12
4.24
145.90
77.67
40.75
Date
lbs/ac
Current Cumulative lbs/acre
0.51 0.38 NA 19.92 1.74 0.05 NA 0.70 0.55 40.98
0.37 0.33 NA 18.27 1.62 0.04 NA 0.61 0.43 36.74
36 34 NA 1,338 267 15 NA 374 89 2,498
276 50.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R****
Permit PAN Limit I st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations."
?-)*Application Method: S - Surface, IN - Injection, INC - Incorporation
Le-. � ��� � I **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rai
DENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
WQ Permit #: W00030998
Field #:
Owner: Eric Smith nnual Dry Tons Applied: 7.37 Site #:
Operator: Eric Smith Predominat Soil Series FoA
Crop 1 Name: Feseue Crop 1 Max PAN: 207.00 Crop 2 Name: awn
Acres Utilized: 4.14
Acres Permitted: 4.14
Cation Exchange Capacity (non 503): NA
Crop 2 Max. PAN
#NIA
O
o
o
SpeciN
Totals
Per Acre
a a Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(�•
Wet,
Moist)
Precip.
Past24
Hrs.
inches
�
!. _.
d
a
'
<
e
a
R
•
91 ro
- a
:
;'
TKN
a
a
w a
f9
' G
Nitrate
and
Nitrite
m /k ,
PAN Applied
(lbs/aere)
Must Select
Crop l or Crop
2
Gal.
Cu.Yd.
Report
�o
Totals
in Gal.
Crop 1
Crop 2
Crop I
Crop 2
Jun-20
39,500
9,541
3.30
1.31
Warsaw WWTP
S
0.50
1 0.30
39,700
3
1,910
36.29
X
Jun-20
6,800
1,643
2.35
0.16
Linte Creek WRF
S
0.50
030
59,600
10200
642
6.62
X
Jun-20
12,000
2.899
2.54
0.31
Southwest Plantation
S
0.50
0.30
77,200
4.130
64
14.77
X
TOTALS:
14,U82
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.09
0.05
0.07
0.83
0.08
0.00
0.05
0.05
0.05
2.65
62.42
57.68
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.28 0.21 NA 11.90 0.85 0.02 NA 0.62 0.29 33.86
0.18 0.17 NA 11.07 0.76 0.02 NA 0.57 0.24 31.21
36 34 NA 1,338 267 15 NA 374 89 1 2A98 ...... ....
207 #NIA
Prior Years Cumulative lbsi acre
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, AnaerobleaIly Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rat
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #: 1 Acres Utilized: 11.20
Owner: Eric Smith nnual Dry Tons Applied: 34.75 Site #: 5 Acres Permitted: 11.20
Operator: Eric Smith
Crop 1 Name: Fescue
Predominat Soil Series
FoA Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 207.00 Crop 2 Name: aNlA Crop 2 Max. PAN
#N/A
C7
?
Specify
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DTlAc
Residual Sources
(NPDES #, WQ#,
Fert., At ma! Waste,
Site
Cond.
(Dry
Wet
Moist)
Precip.
Past 24
Hrs.
tnenes
K d
a _.
Q
]
<
o
w
t
gi CD I-
ry d
TKN
m
z >
m a
g W.
m •
Nitrate
and
Nitrite
PAN Applied
(lbs/acre)
Must Select
CfOp) or Crop
2
Gal.
Cu.Yd.
ToC uls
in Gal.
Crop I
Crop 2
Crop 1
Crop 2
Jun-20
153,800
13,732
2.84
1.63
Wallace WWTP
INC
1.00
0.30
17,800
4,130
1
26.77
X
Jun-20
107,000
9,554
3.30
1.31
Warsaw WWTP
S
0.50
0.30
39,700
3
1,910
36.34
X
Jun-20
18,500
1,652
2.35
0.16
Little Creek WRF
S
0.50
0.30
59,600
10,200
642
6.66
X
TOTALS.
24,939
As
Cd
Cr
Cu
Pb
HR
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
Annual lbs/acre
0.14
0.10
0.15
2.91
0.23
0.01
0.11
0. 10
0.10
5.74
121.86
69.77
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.61 0.53 NA 23.82 2.24 0.07 NA 0.93 0.61 45.05
0.47 0.44 NA 20.91 2.01 0.05 NA 0.83 0.51 39.31
36 34 NA 1,338 1 267 1 IS 1 NA 374 89 2.498
1 207 #N/A
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
Ami�-J*Application Method: S - Surface, IN - Injection, INC - Incorporation
C/►�C_ � �C)Q _ **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading R t
TENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SJMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SJBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: W00030998 Field #: I Acres Utilized: 13.95
Owner: Eric Smith nnual Dry Tons Applied:
Operator: Eric Smith
Crop 1 Name: Forest
Acres Permitted: 13.95
Predominat Soil Series GoA Cation Exchange Capacity (non 503): NA
13.21 Site #:
Crop 1 Max PAN: 60.00 Crop 2 Name: NN/A
Crop 2 Max. PAN #N/A
C7
Specify
Totals
Per Acre
o.
.o Solids
As
Decimal
Volume
Applied per
Acre
DTIAc
Residual Sources
(NPDES #, WQ#.
Fert., Animal Waste,
etc.)Wet,
Site
Cond.
(Dry,
Moist)
Precip.
Past 24
Hrs.
tnetm
7 M
I �
..
C m
°+ c
_
<
� �
* N
`
�
3'
x a
� m
: n
;
TKN
molke
z �'
9
oS o
?
�,
m
Nitrate
and
Nitrite
PAN A lied
pp
(lbs/acre)
Must Select
Crop 1 or Crop
p p
2
Gal.
Cu.Yd.
Report
T
in Gal.
Crop 1
Crop 2
Crop I
Crop 2
Mar-20
96,000
6,882
3.30
0.95
Warsaw WWTP
S
0.50
0.30
39,700
1 3
1,910
26.18
X
TOTALS:
6,982
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.06
0.03
0.04
0.49
0.05
0.00
0.03
0.03
0.03
1.42
31.25
26.18 1
0.00
Date 1.lbs/ac
Current Cumulative lbs/acre
0.10 0.08 NA 0.78 0.10 0.00 NA 0.09 0.08 2.90
0.05 0.05 NA 0.29 0.05 0.00 NA 0.06 0.05 1.48
36 34 NA 1,338 267 15 NA 374 89 2,498
60 #N/A
Prior Years Cumulative Ibs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�^ *Application Method: S - Surface, IN - Injection, INC - Incorporation
v' zov-Ca al **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier
Date
***Mineralization Rates: Compost - 0.1, Annerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rt �t
DENR FORM FSF (12/2008)

ANNUAL LAND APPLICATION FIELD 9JMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND 9JBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:
Owner:
Triple S Farms
Eric Smith
Operator: Eric Smith
Crop 1 Name: Bennudagrass
WQ Permit #: WQ0030998
nnual Dry Tons Applied: 111.00
Field #:
Acres Utilized: 14.50
Site #: 7 Acres Permitted: 14.50
Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 276.00 Crop 2 Name: Wheat Crop 2 Max. PAN 50.00
0
o ?:
fD
Specify
Totals
Per Acre
o o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fed., Animal Waste,
etc.)
Site
Cond.
(Dry'
Wa'
Moist)
Precip.
Past 24
Hrs.
tact�es
X o
^ _.
m
' ?
<
?
_:
p SIP"
N
* o
ii
:
* ^
TKN
z
2 c
a 'w'
Nitrate
and
Nitrite
k,
PAN Applied
(Ibs/acre)
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Mar-20
276,000
19,0341
1.74
1.38
Wallace W WTP
INC
1 1.00
0.30
35,000
6
1 3,050
37.44
X
Mar-20
12,000
828
2.54
0.09
Sotahwest Plantation
S
0.50
0.30
77,200
4,130
64
4.22
X
Jul-20
240,000
16,552
2.44
1.68
Wallace WWTP
INC
I.00
0.30
54,300
8,460
3
74.82
X
Jul-20
429,000
29,586
2.35
2.90
U(teCreek WRF
S
0.50
0.30
59,600
10,200
642
119.23
X
Aug-20
78,000
5,379
2.44
0.55
Wallace WWTP
INC
1.00
0.30
54,300
8,460
3
24.32
X
Nov-20
156,220
10,774
2.35
1.06
Little Creek WRF
S
0.50
0.30
59,600
10,200
642
43.42
X
TOTALS:
82,1531.
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.36
0.15
0.37
7.42
0.48
0.02
0.20
0.27
0.29
13.75
389.95
260.03
43.42
Date
Ibs/ac
Current Cumulative Ibs/acre
0.37 0.17 NA 7.84 0.51 0.02 NA 0.28 0.30 15.27
0.01 0.01 NA 0.42 0.03 0.00 NA 0.01 0.01 1.52 ......
36 34 NA 1,338 267 T 15 NA 374 89 2,498
276 50.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
r� *Application Method: S - Surface, IN - Injection, INC - Incorporation
a( **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rat
DENR FORM FSF (12/2008)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner:
Operator:
Eric Smith
Eric Smith
Crop 1 Name: Wheat (Grain)
WQ Permit #: WQ0030998 Field #: I
nnual Dry Tons Applied: 31.41 Site #: 9
Acres Utilized: 8.93
Acres Permitted: 8.93
Predominat Soil Series GoA Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 136.00 Crop 2 Name: Millets Crop 2 Max. PAN 50.00
�U
s °
SDecify
Totals
Per Acre
o ro Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fort., Animal Waste,
etc 1
Site
Cond.
D
( ry'
Wes)
Moist)
Precip.
Past 24
Hrs.
Inches
-o
�,
_ a
Q m
o
<
S.
X _.
R m
; »
o'
'
3
M
91ry
n �
:
o
TKN
m k
2 b
.; a
o� c
a
Nitrate
and
Nitrite
mWko
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Jan-20
12,000
1,344
2.54
0.14
Southwest Plantation
S
0.50
0.30
77,200
4,130
64
6.85
X
Apr-20
12,000
1.344
2.54
0.14
souillwestPlamation
S
0.50
0.30
77,200
4,130
64
6.85
X
May-20
42,000
4,703
2.07
0.41
6eutaville WWTP
S
0.50
0.30
55,600
5
7,740
19.83
X
Aug-20
30,000
3,359
2.35
0.33
Little Creek WRF
S
0.50
0.30
59,600
10,200
642
13.54
X
Nov-20
140,000
15,677
3.30
2.16
Warsaw WWTP
S
0.50
0.30
39,700
3
1,910
59.63
X
Nov-20
18,040
2,020
2.35
0.20
L•gtleCreek WRF
S
0.50
0.30
59,600
10,200
642
8.14
X
Nov-20
12,000
1,344
2.54
0.14
Southwest Pluntation
S
0.50
0.30
77,200
4,130
64
6.85
X
TOTALS:
29,792
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.18
0.10
0.14
1.78
0.16
0.01
0.11
0.10
0.11
6.OD
126.66
91.47
40.21
Date I
Ibs/ac
Current Cumulative lbs/acre
0.35 0.35 NA 5.97 0.52 0.02 NA 0.35 0.36 14.57
0.16 0.25 NA 4.20 0.36 0.01 NA 0.25 0.25 8.57
36 34 NA 1,338 267 15 NA 374 89 2,498
136 50.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop1
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
ul � �'eD I **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 03, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loadinge.
DtENR FORM FSF (1212006)

RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Beulaville
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
2020-07646
5/7/2020 Type of Stabilization: Lime
6/2/2020
Annual 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.070
Nitrogen (TKN)*
5.560
55,600.00
Phosphorus
1.440
14,400.00
Potassium
0.384
3,840.00
Sulfur
0.000
0.00
Calcium
1.970
19,700.00
Magnesium
0.205
2,050.00
Sodium
0.389
3,890.00
Iron
---
Aluminum
---
6,280.000
Manganese
---
Copper
---
436.000
1,500
Zinc
---
1,880.000
2,800
Ammonia Nitrogen*
0.000
4.830
Nitrate N / Nitrite N*
---
7,740.000
Cadmium
---
23.200
39
Chromium
---
23.200
1,200
Nickel
---
23.200
420
Lead
---
29.600
300
Arsenic
---
30.700
41
Mercury
---
2.020
17
Selenium
---
23.200
100
pH
4.650
Calcium Carbonate Eq. (es
t)
0.000
Organic Nitrogen
5.560
Molybdenum
---
23.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2020
Date Reported: 6/2/2020 Report No: BL 2020-07646
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
48.842
PAN Inj.
48.847
P
28.800
K
7.680
Lime (estimated)
0.000
Secondary Nutrients
Calcium
39.400
Magnesium
4.100
Sodium
7.780
SAR
1.012
Chloride
0.000
Iron
0.000
Alumium
12.560
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.07
pH
4.650
Min Rate
0.300
Metals
Arsenic
0.061
Cadmium
0.046
Chromium
0.046
Copper
0.872
Lead
0.059
Mercury
0.004
Molybdenum
0.046
Nickel
0.046
Seleniun
0.046
Zinc
3.760

F77-*'- --711
Environmental Chemists,
Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ° 910.392.4424
Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS
info(cenvironmentalchemists.com
Town of Beulaville
Date of Report: Jun 02, 2020
PO Box 7085
Customer PO #:
Greenville NC 27835
Customer ID: 08100015
Attention: Angie Miller
Report #: 2020-07646
Project ID: Sludge
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/13/2020
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/13/2020
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
05/13/2020
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/13/2020
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/13/2020
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/13/2020
RCI
Cyanide
EPA 335.4
0.145 mg/kg
05/12/2020
Sulfide SM 4500 S D
Reporting limit elevated due to matrix interference.
<0.50 mg/kg
05/11 /2020
Ignitability
SW 846 method 1010
>200 °F
05/20/2020
pH
SW 846 Method 9045D
4.65 units
05/13/2020
Sludge Residuals
Aluminum
EPA 200.7
6280 mg/kg
05/13/2020
Arsenic
EPA 200.7
30.7 mg/kg
05/13/2020
Cadmium
EPA 200.7
<23.2mg/kg
05/13/2020
Calcium
EPA 200.7
19700 mg/kg
05/13/2020
Chromium
EPA 200.7
23.2mg/kg
05/13/2020
Copper
EPA 200.7
436 mg/kg
05/13/2020
Lead
EPA 200.7
29.6mg/kg
05/13/2020
Magnesium
EPA 200.7
2050mg/kg
05/13/2020
Molybdenum
EPA 200.7
<23.2mg/kg
05/13/2020
Nickel
EPA 200.7
<23.2 mg/kg
05/13/2020
Potassium
EPA 200.7
3840 mg/kg
05/21 /2020
Selenium
EPA 200.7
<23.2mg/kg
05/13/2020
Sodium
EPA 200.7
3890mg/kg
05/13/2020
Zinc
EPA 200.7
1880 mg/kg
05/13/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
7740 mg/kg
05/13/2020
Total Solids (%)
SM 2540 s
2.07 %
05/12/2020
Ammonia Nitrogen
SM 4500 NH3 C
<4.83 mg/kg
05/08/2020
Report #:: 2020-07646
P- , ,F 7

e:n�rochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax
[e-mail]
Town of Beulaville Date of Report: Jun 02, 2020
PO Box 7085 Customer PO #:
Greenville NC 27835 Customer ID: 08100015
Attention: Angie Miller Report #: 2020-07646
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 org B 55600 mg/kg 05/08/2020
Total Phosphorus SM 4500 P F 14400 mg/kg 05/13/2020
Mercury SW8467471B 2.02mg/kg 05/19/2020
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
05/14/2020
Barium
EPA 200.7
<1.0 mg/L
05/14/2020
Cadmium
EPA 200.7
<1.0 mg/L
05/14/2020
Chromium
EPA 200.7
<1.0 mg/L
05/14/2020
Lead
EPA 200.7
<1.0 mg/L
05/14/2020
Selenium
EPA 200.7
<1.0 mg/L
05/14/2020
Silver
EPA 200.7
<1.0 mg/L
05/14/2020
Mercury
EPA 245.1
<0.0002 mg/L
05/19/2020
Comment:
Sludge residual results reported on a dry weight basis.
Reviewed by:
Report #. 2020-07646 Paae 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: ("�. i ., iC�'/ { �t Date: i� J� I I.�' ReportNumber:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Receipt of sample:
Delivered UPS ❑ FeclEx ❑ Other ❑
❑ YES IONO
N/A 1. Were custody seals present on the cooler?
❑ YES I ❑ NO
N/A 12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt;} °C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank Against Bottles
I Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
IT NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
D NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
51 YES
❑ NO
7. Were collection date and time listed on the COC?
JX YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
Of YES
❑ NO
YES
❑ NO
1>0' YES ❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? "*
❑ YES D NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
' TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
'* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
HZSOa HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately
for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002

L�
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
910.392.0223 252.473.5702
Info®environmentalchemists.com
CLIENT: Town of Beulaville
PROJECT NAME: Annual Sludge
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled Bv: C i� SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
r
01
a
E
a
E
0
2
C o
c a
" `
c CM
V E
m m
g=
z
PRESERVATION
ANALYSIS REDUESTED
D e
Time
Temp
W
_
o
-'
'
$
H
"�
o
z
=
=
0
a
z
o
w
o
7-Sludge
t k L.
9'_" r1-
C
P
QQI�
X
Full TCLP
G
G
C
P
X
Nutrients/Metals
G
G
C
P
X
RCI
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/rime
1.
2.
o
Temperature when Received: L- T Accepted: IRejected: Resample
Delivered By: Received By: Date:_
Time: J1-c2

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Clayton
Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
CL 20-055-0007
2/20/2020
3/4/2020
Annual 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.350
Nitrogen (TKN)*
5.960
59,600.000
Phosphorus *
2.840
28,400.000
Potassium
0.954
9,540.000
Sulfur
0.000
0.000
Calcium
1.370
13,700.000
Magnesium
0.521
5,210.000
Sodium
0.389
3,890.000
Iron
---�
Aluminum
---
10,600.000
Manganese
---
Copper
---
164.000
1,500
Zinc
---
492.000
2,800
Ammonia Nitrogen*
1.020
10,200.000
Nitrate N / Nitrite N*
---
642.000
Cadmium
---
4.170
39
Chromium
---
16.400
1,200
Nickel
---
11.600
420
Lead
---
12.500
300
Arsenic
---
20.800
41
Mercury
---
0.625
17
Selenium
---
20.800
100
pH
6.400
Calcium Carbonate Eq. (es,t
0.000
Organic Nitrogen
4.940
Molybdenum
---
10.400
75
Chloride
---
Boron
ailable P2O5ecific
F
Gravity
8.340

Wastewater Treatment Plant
Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2020
Date Reported: 3/4/2020 Report No: CL 20-055-0007
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
41.124
PAN Inj.
51.324
P
56.800
K
19.080
Lime (estimated)
500.000
Secondary Nutrients
Calcium
27.400
Magnesium
10.420
Sodium
7.780
SAR
1.096
Chloride
0.000
Iron
0.000
Alumium
21.200
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.35
pH
6.400
Min Rate
0.300
Metals
Arsenic
0.042
Cadmium
0.008
Chromium
0.033
Copper
0.328
Lead
0.025
Mercury
0.001
Molybdenum
0.021
Nickel
0.023
Seleniun
0.042
Zinc
0.984

Waypoint
ANALYTICAL
3/4/2020
Town Of Clayton
POB 879
Clayton, NC. 27528
7621 Whiteoine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
wvvw,v-jaypointa n,310cal.com
Ref: Analytical Testing
Report Number: 20-055-0007
Project Description Holding Tank #1
Waypoint Analytical Virginia, Inc. received sample(s) on 2/24/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen sulfite...) are required to be analyzed within 15 minutes of
sampling Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding tirne compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely.
?_., r 5"7-
Pauric McGroary
Agronomist
Laboratory's Lability in any claim relating to analyses performed shall be limited to. at laboratory's option. repeating the
analysis in question at laboratory's expense. or the refund of the charges paid for performance of said analysis

a
'
Way
7521 vehit807
Read, Richmond,
V7
PANALY
,vtah,
804-733.94Q1 "Fax iSO4•771-64dG
-6446
i ICAO
V1:NLv.waypoii?:allalytical.com
Sample Summary Table
Report Number: 20-055-0007
Client Project Description: Holding Tank
#1
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
70553
Holcino Tank :1
Solids
02/20/2020 11:00
02/2412020
70553
Holdina Tank 1!
Solids
02j-0/2020 11:00
02;'241:2020
SM-4500-NH3C
:^IP h1TN
70553
Holring lank #1
Solids
02/20/2020 11:015
02/24/2020
9045D
'.,!JP MTN
70553
Holding Tank 11
Solids
02/20/2020 11.00
02124/2020
4500NO3F-2011
NIP MIN
70553
Holding Tank 41
Solids
01/20j7020 11.:00
021"24/2020
6010D
V/P hITN
70553
Holding Tank a 1
Solids
02/20/2020 11:00
021!24/2020
SN/-74716
NIP MTN
70553
Holding Tank 1
Solids
02/20/2020 11:00
02/24/2020
SM-4500-NH3C-rKN
NIP hl T N
70553
Holding Tank 1
Solids
02/20/2020 11:00
02/24/2020
SM-254GG
',"JP P17N
1MP MTN - Meirphis, TN: N- aypoint Analytical - TN, Memphis, TN
P.jq:' 2 E

` 1
Waypoint'.
t
7Whitnnine Road, Richmond. VA 23237
Main 80' 4-743-9dOT ° rax 804 271 G446
ANALYTICAL
www.waypointarialytitai.com
46546
Torn Of Clayton
FOB 879
Project
Holding Tank r:. 1
Report Date : 03/04/2020
Informaton :
Received : 02/24!2020
Clayton , NC 27528
Pam« me G��
Fzunc ivtcGroar,+
Report Number : 20-055-0007
REPORT OFANAL YSIS
Agronomist
Lab No 70553
Matrix:
Solids
Sample ID : Holding Tank #1
Sampled:
2/20/2020 11:00
Test
Results
Units
MOIL
DF Date Time
By Analytical
Analyzed
Method
Moisture
97.6
`I"j
0.010
1 02,126,20 17:01
ADM Sh1-2W(—,
Test
Results
Units
MQL
DF Date: Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
10200
mg/Kg - dry
4170
1 03,02/20 13:00
1133 SM-4500-NH3C
Nitrate:Nitrite-N
642
mg/Kg - dry
208
1 03i02120 14:10
ZED 4500NO3F-2011
Organ-c N
49600
mg/Kg - dry
104Di1
1 03102 j?0 10:00
DH CALCULATION
pH
6.4
s.u.
1 03j02/20 05:41
JSL 9045D
Total Solids
2.35
%4,
0.010
1 02/26/20 17:01
ADM SM-2540G
Total Kleldahl Nitrogen
59600
mg/Kg - dry
10400
1 03!02/20 10:00
1F) ;h1-4500-NH3C-TK"
FhosphORis
28400
mg/Kg dy
208
1 021/26/2016:46
JTR 6010D
Aluminum
10600
mg/ Kg dry
208
1, 02/ 26/20 16:46
TTR 6010D
Arsenic
: 20.8
mg.,Kg - dry
20.8
1 02126!20 16 46
JTR 6010D
Calcium
13700
mg/K9 - dry
1040
1 021:26120 16:46
JTR 6010D
Cadmium
<4.17
mg/Kg - dry
4.17
1 02/26/20 16:46
Ti R 60101?
Chromium
16.4
mg/Kg - dry
10.4
1 02,/26!20 16:46
JTR 601OD
Copper
164
mg/Kg - dry
10.4
1 02/26!20 16:46
JTR 60101)
Lead
<12.5
ntg/Kg - dry
12.5
1 02/26/20 16:46
JTR 601UD
Magnesium
5210
mg/Kg - dry
208
1 02/26.20 16:46
JTR 6010D
Mercury
<0.625
mg/Kg - dry
0.625
1 02r26/20 12:51
NS SW-7471B
Molybdenum
<10.4
mg/Kg - dry
10.4
1 02/260.0 16:46
JTR 6010D
Qualifiers/ DF Dilution Factor
L Limit Fxreeded
Definitions h1Q- Method Ouantitation Limit
_ 5

rr �
Wayposint .
NAMICAL
46-r4
Town Or Clayton
FOB 879
Clayton , NC 27528
Report Number : 20-055-0007
Lab No • 70553
Sample ID : Holding Tank #1
7621 Whitepine Road. Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
wrr,v.waypoi,itanalytical.corn
Project Holding Tank w 1
Informa;ion :
REPORT OPANAL YSIS
Report Date : 03/04/2020
Received : 02/24/2020
Pam« tv 60wr
Paunc McGroary
Agronornist
Matrix: Solids
Sampled. 2/ 20/ 2020 11:00
Test
Results
Units
MOL
DF Date Time
Analyzed
By
Analytical
Method
Nickel
11.6
nigi Kg - dry
10A
1 022%26!20 16:46
JTR
60107
Potassium
9540
mg,'K9 - dry
208
1 02,•'26/20 16:46
JTR
6010D
Selenium
<20.8
mg,'Kg - dry
'20,8
1 02/ 26/20 16:46
JTR
6010D
Silver
< 10.4
mg/Kg - dry
10.4
1 0.-1/26/20 16:46
JI P.
6010U
Sotl urn
3890
mg/Kq - dry
1040
1 02/26/20 16:46
JTR
6010D
Zinc
492
mg/Kg - dry
52A
1 02/26/20 16:46
JTR
6010D
Sodium Absorption Patio
1.11
1
CALCULATION
Qualifiers/ D- Dilution Factor L Lrrrrt Exceeded
Definitions NQL Method Quanf tat.,:,n Umrt

if yPoi nt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
jNbin 804-743-9401 'Fax [phone]
w:1v:v.bvcy nointa+idly:ica i.co•n
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number-. 20-055-0007
Shipping Method
Fed Ex US Postal Lab
Other
I] UPS Client Courier
Thermometer ID:
Shipping container.!cooler uncompromised?
Yes
No
Nurnber of coolers/boxes received
Custody seals intact on shipping container cooler?
Yes
No • Not Present
Custody seals intact on sample bottles?
Yes
No 40 Not Present
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
* Yes
No
COC properly completed
Yes
No
Samples in proper containers?
* Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time? _
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
Yes
No
No
N-A
Water - VOA vials free of headspace
Trip Blanks received with VOAs
Yes
Yes
No
No
NIA
NA
Soil VOA method 5035 — compliance criteria met
Yes
No
NA
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? Yes No
Comments:
Signature Brandi Watson
Date & Time: 02 24-2020 10:11.21

WASTE' 1 E' �'lrri I .' i? :�?1'!'� Il�j�li!Illl I I Y,t !�j' !—
' I� .I'ii
Submitted By Charge Tr.
1_
., ryts
or;} ,
Project
Sample Information
.KT'.
• rl 1 ,
._. .... . �_.... ....... ...... ...
i
I
PIS
t'n`r •,nc "� r.' ':�•, r^ I tea; � _ r.;. ., „ . � - r ----
TEat A.� lab e 5�r'°ua! ;r-tnrrhGn ; rr F:,'n'j1_5
N :rp;)n� tiN:r±t .....�i K;r.Uf..h A�:r*r • , �� ^! ,. rr' 3 G±q.;o�c "5,.,,yon
en r r ,i 7: If r f , r I : r 5 r for At, r
t.l;.^r 9 - e -b r r r - 8 tt C., t e n -. 6!•_ , . t� r -y __ _.__--y..-2.
>1" < fi i. i )h.. i ..I r� r. ,t" , 1•r. ., —_'_s .�. _T.
';, .1.,l:Yr ..' ,. r -, ,r : .rr I r.. ... n.,. Ir. t., r. . t ., F1•: t

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Kenansville
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
2020-09561
6/10/2020 Type of Stabilization: time
7/15/2020
Annual 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
0.510
Nitrogen (TKN)*
3.320
33,200.00
Phosphorus
0.905
9,050.00
Potassium
0.304
3,040.00
Sulfur
0.00
Calcium
1.750
17,500.00
Magnesium
0.167
1,670.00
Sodium
1.190
11,900.00
Iron
---
Aluminum
---
4,040.000
Manganese
---
Copper
---
353.000
1,500
Zinc
---
763.000
2,800
Ammonia Nitrogen*
0.002
19.600
Nitrate N / Nitrite N*
---
80.800
Cadmium
---
48.000
39
Chromium
---
48.000
1,200
Nickel
---
48.000
420
Lead
---
48.000
300
Arsenic
---
57.500
41
Mercury
---
3.280
17
Selenium
---
48.000
100
H
6.790
Calcium Carbonate E . (es
t)
0.000
Organic Nitrogen
3.318
Molybdenum
---
48.000
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Wastewater Treatment Plant
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2020
Date Reported: 7/15/2020 Report No: KV 2020-09561
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
20.089
PAN Inj.
20.109
P
18.100
K
6.080
Lime (estimated)
0.000
Secondary Nutrients
Calcium
35.000
Magnesium
3.340
Sodium
23.800
SAR
1.641
Chloride
0.000
Iron
0.000
Alumium
8.080
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
0.51
pH
6.790
Min Rate
0.300
Metals
Arsenic
0.115
Cadmium
0.096
Chromium
0.096
Copper
0.706
Lead
0.096
Mercury
0.007
Molybdenum
0.096
Nickel
0.096
Seleniun
0.096
Zinc
1.526

Environments Chemists,
Inc.
i 4
ara'
6602 Windmill Wvav, WVilrnin tun, NC 28405 ��
8 - 910.392.0223 Lab
710 Bocvsertown Road, klanteo, NC
: 91.0.392.4,24 Fax
2:15-A. Wilmington
27954 o 252.417
,3,5702 Lab/Fax
Highway, Jacksonville, INC 2854-0 • 910.347.58-13 Lab; Fax
ANAL.' T iCAL & CONSULTING CHEMISTS
is iolnenvironmentalcheraists.com
Town of Kenansviile
PO Box 370
Date of Report: Jul 15, 2020
Kenansville NC 28349
Customer PO #:
Attention:
Customer ID: 09020018
Report #: 2020-09561
Project ID: Sludge
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
Chlorobenzene (TCLP)
SW846 Method 826015030
<0.01 mg/L
06/25/2020
Chloroform (TCLP)
SW846 Method 8280/5030
40.01 mg/L
06/25/2020
Methyl ethyl ketone (TCLP)
SW848 Method 8260/5030
<0.01 mg/L
06/25/2020
Tetrachloroethylene (TCLP)
swsas Method 826015030
<0.05 mg/L
06/25/2020
Trichloroethylene (TCLP)
SW846 Method 826015030
<0.01 mg/L
06/25/2020
Vinyl Chloride (TCLP)
SW846 Method 826015030
<0.01 mg/L
06/25/2020
RCI
<0.01 mg/L
06/25/2020
Cyanide
Reporting limit elevated due to matrix
EPA 335 4
Interference.
<0.05 mg/kg
06/29/2020
Sulfide
SM 4500 S D
1 nitability
9
sw 64s method Coto
0.81 mg/kg
06/16/2020
pH
>195°F
06/26/2020
Sludge Residuals
SNl046 Method 8045D
6.79 units
07/06/2020
Aluminum
EPA 200 7
Arsenic
4040 mg/kg
06/16/2020
Cadmium
EPA 200 7
57.5 mg/kg
06/16/2020
Calcium
EPA 200.7
<48.0 mg/kg
06/16/2020
Chromium
EPA 200.7
17500 mg/kg
06/16/2020
Copper
EPA 200.7
<48.0 mglkg
06/16/2020
EPA 200.7
Lead
353 mg/kg
06/16/2020
EPA 200.7
Magnesium
EPA 200.7
<48.0 mg/kg
06/16/2020
Molybdenum
EPA 20D.7
1670 mg/kg
06/16/2020
Nickel
<48.0 mg/kg
06/16/2020
EPA 200.7
Potassium
<48.0 mg/kg
06/16/2020
Selenium
EPA 200.7
3040 mg/kg
06/16/2020
EPA 200.7
Sodium
EPA 200.7
<48.0 mg/kg
06/16/2020
Zinc
11900 mg/kg
06/16/2020
EPA 200.7
Nitrate+Nitrite-Nitrogen
EPA 353.2
763 mg/kg
06/19/2020
Ammonia Nitrogen
SM 4500 NH3 C
80.8 mg/kg
06/20/2020
<19.6 mglkg
06/11/2020
Report A`:: 2020-CS561
Page 2 of 3

}R `•_ ' _ 4E Vironamen-tal Chemises, Ine.
8 3 ! co{ 2 drnill VVI , I- iimirmon, NC 23405 a 9105. ' 022> La! 6 910,3924-LN F'av
— 71.0 E-Owse:toWn Road, NIanteo, INC 2795:1 i 252.473 570' Lab/Faxsni
'_55-_lLViin in�ttn=lighway. jacksunville, N-C 285-_10 • 910.34 S43 Lawi-1 ax.
ANALYnCAL & CONSULTING CHEMISTS in lchemismcorn
Town of Kenansville
Date of Report: Jul 15, 2020
PO Box 370
Customer PO #:
Kenansville NC 28349
Customer ID: 09020018
Attention-
Report #: 2020-09561
Project ID. Sludge
Total Kjeldahl Nitrogen (TKN ) SM 4500 Org S
33200 mg/kg 06/11/2020
Total Phosphorus SM 450C P F
9050 mg/kg 06/19/2020
Mercury SW846 7471E
<3.28 mg/kg 06/15/2020
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
06/25/2020
Barium
EPA200.7
<1.0mg/L
06/25/2020
Cadmium
EPA 200.7
<1.0 mg/L
06/25/2020
Chromium
EPA 200.7
<1.0 mg/L
06/25/2020
Lead
EPA 200.7
<1.0 mg/L
06/25/2020
Selenium
EPA 200.7
<1.Omg/L
06/25/2020
Silver
EPA 2G0.7
<1.0 mg/L
06/25/2-020
Mercury
EPA 245 1
<0.0002 mg/L
06/25/2020
Comment:
Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received
basis.
Reviewed by:
Reccrt ::: 2020-0951a 1
Pape 3 of 3

Enviranimentai Chemist, Inc.,'IMIrnington, NC Lab #94
6602 Windmill Way
'Wilmington. i4C 28405'
Sample Receipt Checklist 910.352.0223
1 , ,
Client: �`�5�1 I
Date i Report Number:C)
Receipt of sample:
J YES ❑ NO
Delivered I
fedEx ❑ Other ❑
C] YES
❑ NO
N/A
N/A
1. Were custody seals present on the cooler?
Original temperature upon
eceipt
2. If custody seals were present, were they intact/unbroken?
?
T
How temperature taken: ❑ Temperature Blank Corrected temperature upon receipt 'C
tR Gun ID: Thomas Traceable S/N 192511657 Against Bottles
C7 YES
❑ ryO
p IR Gun Correction Factor'C: 0.0
3. If temperature of cooler exceeded 6'C,
YES
YES
❑ NO
was Project M r./QA notified?
4. Were pro per custody, rocedures(relinquished/received)followed?
❑ NO
S. Were sample ID's listed on the CQC?
I YES
YES
❑ NO
❑ NO
6. Were sam les ID's listed on sample containers?
YES
❑ NO
7. Were c1! in'tbn date and time listed on the CDC?
YES
❑ NO
S. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
❑ NO
10. Did samples arrive in good condition for each test?
EYES
E5
❑
11. Was adequate sample volume available?'
❑ YES
NO
❑ NO
12. Were samples received within propholding time for requested tests?
13. Were acid er preserved samples
F❑ YES
13 YES
❑ NO
ANO
received at a pH of <2?
14. Were cyanide samples received at a pH >127
i
© YES
❑
❑
15. Were sulfide samples received at a pH >9?
O YES
NO
❑ NO
16, Were NH3JUN/Phenol received at a chlorine residual of <0.5 m/L? ab
ere Sulfide/Cyanide received
17:N-
❑ YES
❑ NO _
at a chlorine residual of <0.5 m/L?
1l3,ere orlhpRb °sidesamples illtemd-i"#te
field raithi"5-minutes3--• - - —
° TOC/volatiies are pH checked at time of analysis and recorded on the benchsheet.
o a Bacteria
samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly
y preserved or with headspace)
by adding (circle one):
were received incorrectly preserved and were adjusted accordingly
1-12SO, HNO,
Time of preservation:
HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain
a new sample or
notiry the state lab if directed to analyzed by the customer. who was notified, date and time;
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Jacksonville WWTP
SWP 2019 1-19
3/4/2020
4/13/2020
Annual 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.54
Nitrogen (TKN)*
7.720
77,200.000
Phosphorus
1.620
16,200.000
Potassium
0.409
4,090.000
Sulfur
0.000
Calcium
1.510
15,100.000
Magnesium
0.246
2,460.000
Sodium
0.020
200.000
Iron
---
Aluminum
---
2,970.000
Manganese
---
Copper
---
158.000
1,500
Zinc
---
854.000
2,800
Ammonia Nitrogen*
0.413
4,130.000
Nitrate N / Nitrite N*
---
64.200
Cadmium
---
9.650
39
Chromium
---
12.800
1,200
Nickel
---
9.650
420
Lead
---
9.650
300
Arsenic
---
9.650
41
Mercury
---
0.614
17
Selenium
---
9.650
100
pH
7.070
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
7.307
Molybdenum
---
9.650
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Jacksonville WWTP
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Annual 2020
Date Reported: 4/13/2020 Report No:
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
48.100
PAN Inj.
52.230
P
32.400
K
8.180
Lime (estimated)
0.000
Secondary Nutrients
Calcium
30.200
Magnesium
4.920
Sodium
0.400
SAR
0.063
Chloride
0.000
Iron
0.000
Alumium
5.940
Manganese
0.000
Boron
0.000
Sulfur
0.000
SWP 2020 4-13
Physical Characteristics
% Solids
2.54
pH
7.070
Min Rate
0.300
Metals
Arsenic
0.019
Cadmium
0.019
Chromium
0.026
Copper
0.316
Lead
0.019
Mercury
0.001
Molybdenum
0.019
Nickel
0.019
Seleniun
0.019
Zinc
1.708

envirochem
s
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Wav, Wilmington, INC 25405 • 910.392.0223 Lab • 910392.-4z24 Fa%
710 Bowsertotcn Road, Manfoo, NC 2795$ • 252.�473.57O2 Lab/Far
255-A Wilmington Hi ;hwav, Jacksonville, NC 285.40 • 910.3-47.5843 Lab/Fax
intu(a ens uonmentalchemist;.ccnn
Environmental Services
Date of Report: Apr 13, 2020
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2020-03793
Project ID: Bear Trail Golf Course
pH
SW 846 Method 90450 7.07 units
04/02/2020
Sludge Residuals
Aluminum
EPA 200 7
2970 mg/kg
03/12/2020
Arsenic
EPA 200 7
<9.65 mg/kg
03/12/2020
Cadmium
EPA 2007
<9.65mg/kg
03/12/2020
Calcium
EPA 200 7
15100 mg/kg
03/12/2020
Chromium
EPA 200 7
12.8 mg/kg
03/12/2020
Copper
EPA 200 7
158 mg/kg
03/12/2020
Lead
EPA 200 7
<9.65 mg/kg
03/12/2020
Magnesium
EPA 200 7
2460 mg/kg
03/12/2020
Molybdenum
EPA 200 7
<9.65 mg/kg
03/12/2020
Nickel
EPA 200 7
<9.65 mg/kg
03/12/2020
Potassium
EPA 200 7
4090 mg/kg
03/24/2020
Selenium
EPA 200 7
<9.65 mg/kg
03/12/2020
Sodium
EPA 200 7
200 mg/kg
03/16/2020
Zinc
EPA 200 7
854 mg/kg
03/12/2020
Nitrate+Nitrite-Nitrogen
EPA 3532
64.2mg/kg
03/11/2020
Total Solids (%)
SM 2540 B
2.54 %
03/09/2020
Ammonia Nitrogen
SM 4500 NH3 C
4130 mg/kg
03/10/2020
Total Kjeldahl Nitrogen (TKN)
SM 4500 org B
77200 mg/kg
03/11/2020
Total Phosphorus
SM 4500 P F
16200 mg/kg
03/19/2020
Mercury
SW84e 7471E
<0.614 mg/kg
03/13/2020
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
03/19/2020
Barium
EPA 200.7
<1.0 mg/L
03/19/2020
Cadmium
EPA 200.7
<1.0 mg/L
03/19/2020
Chromium
EPA 200.7
<1.0 mg/L
03/19/2020
Lead
EPA 200 7
<1.0 mg/L
03/19/2020
Selenium
EPA 200 7
<1.0 mg/L
03/19/2020
Silver
EPA 200 7
<1.0 mg/L
03/19/2020
Report # 2020-03793
Page 2 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: £C\V - it F �� \/ (f �' �� Date: f J' 5 iLD Report Number: .2 (-)
_Receipt of sample: Delivered UPS ■ FedEx • Other 0
■ YES
• NO
N/A
1. Were custody seals present on the cooler?
• YES
0 NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt la.T ?C Corrected temperature upon receipt 9C
How temperature taken: 0 Temperature Blank 1 Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor 6C: 0.0
■ YES
• NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
cit YES
0 NO
4. Were proper custody procedures (relinquished/received) followed?
cg YES
0 NO
5. Were sample ID's listed on the COC?
YES
• NO
6. Were samples ID's listed on sample containers?
YES
0 NO
7. Were collection date and time listed on the COC?
4 YES
• NO
8. Were tests to be performed listed on the COC?
YES
0 NO
9. Did samples arrive in proper containers for each test?
IX YES
0 NO
10. Did samples arrive in good condition for each test?
YES
0 NO
11. Was adequate sample volume available?'
Nf YES
• NO
12. Were samples received within proper holding time for requested tests?
■ YES
0 NO
13. Were acid preserved samples received at a pH of <2? *
• YES
• NO
14. Were cyanide samples received at a pH >12?
• YES
0 NO
15. Were sulfide samples received at a pH >9?
❑ YES
• NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ••
❑ YES
0 NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
• TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
• • Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note Notify customer service .mmediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) Nere received with headspace
COMMENTS:
JUL Q.A.UO2

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT:
ENVIRONMENTAL SERVICES
PROJECT NAME:
BEAR TRAIL GOLF COURSE
REPORT NO: 'LTD — D /-(7 .,
ADDRESS:
PO BOX 1054
CONTACT NAME:
SONNY SCOZZARI
PO NO:
JACKSONVILLE, NC 28541
REPORT TO:
PHONE/FAX: [phone]
COPY TO:
email: [e-mail]
Sampled By:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
E.
Composite
or
Grab
Container
(P or G)
W
cam'
L E
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
.
a
z
_
.
$
2
8
=
0
Z
0
5
o
Effluent
C
P
X
BOD, TSS, NO2
Effluent
C
P
X
NO3, NH3, TKN, TP
Effluent - Grab
P
X
Fecal Coliform
G
Effluent - Triannuals
(March, July, November)
C
P
X
TDS, Chloride
/
a
CcL\12
J. L.EC‘ C '��
71—c P
Transfer
Aelinqulshed1By
Date/Time
Received By:
Date/Time
.�,),7::s%
1.
•• ..'_,-.) ,' -I
'f,;''(:: c".. 145-)zc,
2.
f
''
emperature wnen Iiecelvea:
Delivered By:
Comments:
Z_ I b .1 ygccepted: ( R)jected: Resample Requested: 1 _
_Received By. :rDate: 51LL
TURNAROUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Wallace
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WL 1-2020-1-28
1/6/2020
1/28/2020
1st Quarter 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.740
Nitrogen (TKN)*
3.500
35,000.000
Phosphorus *
2.440
24,400.000
Potassium
0.460
4,600.000
Sulfur
0.000
0.000
Calcium
2.800
28,000.000
Magnesium
0.339
3,390.000
Sodium
0.655
6,550.000
Iron
---
'`�
Aluminum
---
13,400.000
Manganese
---
Copper
---
989.000
1,500
Zinc
---
1,400.000
2,800
Ammonia Nitrogen*
0.001
5.750
Nitrate N / Nitrite N*
---
3,050.000
Cadmium
---
11.700
39
Chromium
---
32.500
1,200
Nickel
---
22.100
420
Lead
---
64.900
300
Arsenic
---
11.700
41
Mercury
---
1.970
17
Selenium
---
11.700
100
pH
5.920
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.499
Molybdenum
---
11.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
1st Quarter 2020
1/28/2020 Report No: WL 1-2020-1-28
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
27.102
PAN Inj.
27.108
P
48.800
K
9.200
Lime (estimated)
500.000
Secondary Nutrients
Calcium
56.000
Magnesium
6.780
Sodium
13.100
SAR
1.295
Chloride
0.000
Iron
0.000
Alumium
26.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
1.74
pH
5.920
Min Rate
0.300
Metals
Arsenic
0.023
Cadmium
0.023
Chromium
0.065
Copper
1.978
Lead
0.130
Mercury
0.004
Molybdenum
0.023
Nickel
0.044
Seleniun
0.023
Zinc
2.800

Environmental Chemists, Inc.
h6('2 Windmill Wilmington, NC 2 405 * 910.392.0223 Lab • 910.392 4424 Fri,
710 L1c ser tow n Road, \lank0, NC 27954 • 2;2 473.57 (12 Lab; Fay
255-A Wilmington Highway, \C 2S540 • 91t1-3475i443 I_al ; Fii
ANALYTICAL & CONSULTING CHEMISTS info �r em ironmentakhemi;t>. om
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
RCI
Cyanide EPA 335.4
Reporting limit elevated due to matrix interference.
Sulfide
Ignitability
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
SM 4500 S D
SW 845 method 1010
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 2007
EPA 2007
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 2CC 7
EPA 353 2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
0.06 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.125 mg/kg 01/08/2020
0.32 mg/kg 01/10/2020
>205 °F 01/10/2020
13400 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
28000 mg/kg 01/07/2020
32.5 mg/kg 01/07/2020
989 mg/kg 01/07/2020
64.9 mg/kg 01/07/2020
3390 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
22.1 mg/kg 01/07/2020
4600 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
6550 mg/kg 01/13/2020
1400 mg/kg 01/07/2020
3050 mg/kg 01/13/2020
1.74 % 01/06/2020
5.92 units 01/20/2020
<5.75 mg/kg 01/08/2020
Pace 2 of 4
Report # 202C•00150

Environmental Chemists, Inc.
nf,02 Windmill Way, �Viltnington, NC 28403 • 910.392.0223 Lab • 910.392.4424 Fa\
7111 &ows€.rtown Road, \tante °, NBC 27934 • 252.473.5702 Lab/Fat
255- 28340 • 910.347 5843Lab/Fa \
_� .l1,Vilmin:�tan Highway, Jacksonville, _c, NC
ANALYTICAL& CONSULTING CHEMISTS in!b a en ironni_ntalcixnti,t,.rom
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 Org B
SM 4500 P F
SW846 7471B
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 2007
EPA 200 7
EPA 245 1
35000 mg/kg 01/08/2020
24400 mg/kg 01/10/2020
1.97 mg/kg 01/17/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<0.0002 mg/L 01/20/2020
Lab ID
20-00346
Test
Sample ID:
Site: 001
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.91 % 01/06/2020
<943 MPN/g 01/06/2020
Lab ID
20-00348
Sample ID:
Site: 002
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM92210EMPN 24hr503
1.57 % 01/06/2020
<1147 MPN/g 01/06/2020
Lab ID
20-00349
Test
Sample ID:
Site: 003
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10 50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.91 % 01/06/2020
<943 MPN/g 01/06/2020
Report 4 2020-00160
Page 3of4

Analytical F ContiHung f.pamist
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification tf94 NHCDHHS: DLS certification 437729
tion and Chain of Custod
6602 Windmill Way. Wilmington. NC 75405
Office 910-942.02) t l a>t 910.392 4424
[e-mail]
Branch Residuals Bob Branch
Projectname: WWTP LTMP-sludge samples
./
Report No: -,t; .- I( t.W
Client.
CC Town of Wallace
Contact name:
PO No:
Address
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to:Brent Dean, [e-mail]
Email: [e-mail]
�j
by rt?..tft tip h G Z? e,V
SAMPLE TYPE: 1= Influent, Er Effluent, W=Well, ST= stream, S0= Soil, SL=Sludge, Other.
Sampled 1'tSa
l
ISQ
a,
a
a
Preservation
collection
Y JD
Identification
date
time
temp
a
E
co
"'
p
E
E
0 o
c
°
c
° `o
c
r M
u c
p a
E
z
v
c
0
z
v
i
0
v,
NI
=
m
O
Z
x
S
0
z
O
=
t—
w
1
t—
O
Analysis required
Sample
X
nutrients/metals
full TCI P
RCI
1 —02—2%aD
ID
G
P
399
udge-(Quarterly)
G
P
; �r
t I`,
X
Fecal Density,% TS
1. sludge
X
�„
Fecal Density,% TS
G
P
�`l
2 sludge
G
P
)si tj
X
Fecal Density,%TS
3. sludge
.�
X
Fecal Density,% TS
)
G
P
, •,
4 sludge
G
P
- `; j
X
Fecal Density,%'IS
5. sludge
-z,e ;?
X
Fecal Density,% TS
G
P
6 sludge
G
P
3,; 5
X
Fecal Density,% TS
/ Sludge
V/
3/week
June 1- Sept 30; 1/week Octoberl- May 31 Cronic toxicity due in an, Apr,Jul Oct
Up/dawn stream samples:
'shed B Y
Relin fi
Date/time
Rec ived y:41
Date/time
Transfer
f
/
LI _/
I/Gi/td
-,----)
21
t
--i Accepted: v Rejected: ---- i ; Resample:
`71.'.L!
temp when received-
Received by: t—`—� +.c — date/time / jC' 1i •J
By ''C,
delivered
Comments' ( turnaround: / •-
I

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
WL 2-2020-4-30
4/20/2020
4/30/2020
2nd Quarter 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.84
Nitrogen (TKN)*
1.780
17,800.000
Phosphorus *
2.130
21,300.000
Potassium
0.370
3,700.000
Sulfur
0.000
Calcium
2.150
21,500.000
Magnesium
0.276
2,760.000
Sodium
0.337
3,370.000
Iron
---
-
Aluminum
---
11,400.000
Manganese
---
Copper
---
669.000
1,500
Zinc
---
1,110.000
2,800
Ammonia Nitrogen*
0.413
4,130.000
Nitrate N / Nitrite N*
---
0.960
Cadmium
---
17.300
39
Chromium
---
27.100
1,200
Nickel
---
17.300
420
Lead
---
47.200
300
Arsenic
---
17.300
41
Mercury
---
3.460
17
Selenium
---
17.300
100
pH
7.250
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
1.367
Molybdenum
---
17.300
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
2nd Quarter 2020
4/30/2020 Report No: WL 2-2020-4-30
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
12.334
PAN Inj.
16.464
P
42.600
K
7.400
Lime (estimated)
500.000
Secondary Nutrients
Calcium
43.000
Magnesium
5.520
Sodium
6.740
SAR
0.967
Chloride
0.000
Iron
0.000
Alumium
22.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.84
pH
7.250
Min Rate
0.300
Metals
Arsenic
0.035
Cadmium
0.035
Chromium
0.054
Copper
1.338
Lead
0.094
Mercury
0.007
Molybdenum
0.035
Nickel
0.035
Seleniun
0.035
Zinc
2.220

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.3924424 Fax
710 Bo vscrtnwn Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fa
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Apr 30, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-06497
Project ID: WWTP Sludge
Lab ID
20-16001
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Solid/Sludge
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
N itrate+N itrite-Nitrogen
Total Solids (°/o)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
EPA 200 7
EPA 200 7
EPA 2007
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 2007
EPA 353 2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 City 0
SM 4500 P F
SW846 7471 B
11400 mg/kg 04/22/2020
<17.3 mg/kg 04/22/2020
<17.3 mg/kg 04/22/2020
21500 mg/kg 04/22/2020
27.1 mg/kg 04/22/2020
669 mg/kg 04/22/2020
47.2 mg/kg 04/22/2020
2760 mg/kg 04/22/2020
<17.3 mg/kg 04/22/2020
<17.3 mg/kg 04/22/2020
3700 mg/kg 04/22/2020
<17.3 mg/kg 04/22/2020
3370 mg/kg 04/28/2020
1110 mg/kg 04/22/2020
0.96 mg/kg 04/24/2020
2.84 % 04/21/2020
7.25 units 04/29/2020
4130 mg/kg 04/21/2020
17800 mg/kg 04/22/2020
21300 mg/kg 04/29/2020
3.46 mg/kg 04/21/2020
Report # 2020-0649T Paae 1 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client 1k 1 tAc,i:
Receipt of sample
O YES
❑ NO
Delivere
Sample Receipt Checklist
Date41
OZ O /cb?U Report Number:
.i
6602 W.ndmill Way
Wilmington, NC 28405
910.392 0223
Other
1 Were custody seals present on the cooler?
10 YES ❑ NO 2 If custody seals were present, were they intact/unbroken?
!Original temperature upon receipt 9). 6 4C
Corrected temperature upon receipt
N/A
N/A
How temperature taken. ❑ Temperature Blank
IR Gun ID: Thomas Traceable S/N 192511657
O YES 0 NO
tte YES
YES
YES
YES
YES
I$ YES
it YES
tE YES
IS YES
O YES
O YES
O YES
O YES
O YES
❑ NO
D NO
❑ NO
NO
O NO
O NO
D NO
O NO
D NO
O NO
❑ NO
❑ NO
D NO
UPS ❑ FedEx ❑
Against Bottles
❑
IR Gun Correction Factor 6C: 0.0
3 If temperature of cooler exceeded 66C, was Project Mgr,/CIA notified"
4 Were proper custody procedures (relinquished/received) followed'
5• Were sample ID's listed on the COC'
6 Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC
8 Were tests to be performed listed on the COC'
9 Did samples arrive in proper containers for each test
10. Did samples arrive in good condition for each test'
11. Was adequate sample volume available'
12. Were samples received within proper holding time for requested tests 0 NO 13. Were acid preserved samples received at a pH of c27'
14. Were cyanide samples received at a pH >127
15. Were sulfide samples received at a pH >97
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? • •
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L7
' TOCNolatiles are pH checked at time of analysts and recorded on the benchsheet
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
sample(s)
oy adding (circle one)
Time of preservation
Note Notify customer service
notify the state lab A directed
Volatiles Samples)
COMMENTS
(Must be completed for any sample(s) incorrectly preserved or with headspace,
were received incorrectly preserved and were adjusted accordingl,
H2SO4 HNO3 HCI NaOH
If more than one preservative is needed, notate in comments belov.
immediately for incorrectly preserved samples Obtain a new
RiOK
to analyzed by the custoe' Who was notified, date and time
inor
were received with headspace
r>nr n • nn,
vv�.. 4r,-VVc

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28 405 • 910.392.0223 Lab • 910.392.4424 Fa\
710 Bowsertown Road, Manteo, NC 27954 • 252. 473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a emironmentalchemish.com
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Apr 30, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-06497
Project ID: WWTP Sludge
Lab ID
20-16003
Test
Sample ID:
Site: 001
Method
Collect Date/Time Matrix Sampled by
4/20/2020 10:20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.62%
49619 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16004
Test
Sample ID:
Site: 002
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.78%
28418 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16005
Test
Sample ID:
Site: 003
Method
Collect DatelTime Matrix Sampled by
4/20/2020 10:20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.78%
28418 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16006
Test
Sample ID:
Site: 004
Method
Collect Date/Time Matrix Sampled by
4/20/2020 10:20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.67 %
29589 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16007
Test
Sample ID:
Site: 005
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.96%
43919 MPN/g
04/21/2020
04/20/2020
Report # 2020.06497 Page 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Wimimill Wat. Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fa\
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington I lighway, Jacksonville, N.0 28540 • 910.347.5843 Lab/Fat
in focmenvironmenta1ehemi ts.com
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Apr 30, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-06497
Project ID: WWTP Sludge
Lab ID
20-16008
Test
Sample ID:
Site: 006
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.71 %
339484 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16009
Test
Sample ID:
Site: 007
Method
Collect Date/Time Matrix
4/20/2020 10.20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
3.03
115512 MPN/g
04/21/2020
04/20/2020
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: IC 10 k Ol '
Report # 2020-06497 Page 3 of 3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQcertification #94 NHCDHHS: DLS certification #37729
Collection and Chain of Custody
6602. Windmill Way, Wilmington. NC 25405
Office. 910-392,0223 Fax [phone]•1
[e-mail]
Client: Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: ) - (..5 , 14 rj.3"
Address: 316 E Murray St
Contact name:
PO No:
Wallace, NC 284b6
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to: Brent Dean, [e-mail]
Email: [e-mail]
J1
Sampled by (l�"1 powt\ ,..,.i Sc (t� /R
SAMPLE TYPE: 1= Influent, E= Effluent, W=Well, ST= stream, S0= Soil, SL=Sludge, Other:
Sample Identification
1
J collection
o-
°'
ETi
composite
or grab
a`i
S
c l7
° o`
a,
0--
u E
Lab ID
Number
Preservation
Analysis required
date
time
temp
v
z°
i
v
,
N
rn
O
Z
x
o
z
O
F
w
_
o
Sludge -(Quarterly)
(-{-;0-;0
1o, ao
G
P
l:�f -6i: \
�
X
X
X
CN
Ag,As,Cd,Cr,Cu,Hg,Mo,Ni,Pb,Se,Zn
Total N
1. sludge
G
P
ft.900 -')
X
Fecal Density,% TS
2. sludge
G
P
S,i,;)G'C Li
X
Fecal Density,% TS
3. sludge
G
P
Ilt,005-
X
Fecal Density,% TS
4. sludgei
/
G
P
i1,2 DO Lc
X
Fecal Density,% TS
5. sludge
G
P
ltvl)t '
X
Fecal Density,% TS
6. sludge
G
P
( LU '
X
Fecal Density,% TS
7. sludge
G
P
I L9 mCi
X
Fecal Density,% TS
sluge (annual)
TCLP,RCI
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
NO3+NO2,P, K,Na, TKN,
Transfer
R quished By:
Date/time
Receive By-
Date/time
1
/
4t -a0 --1 ° )0
!-\j'
!/'-•
-1\%11( V
2
/
ternp when received: / , rj `.., Accepted: v` Rejected: Resample:
delivered By ;
\ply> Received by: On date/time 0/4.0 ')1- col
Comments: turnaround:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Wallace
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WL-3-2020-8-25
7/22/2020
8/25/2020
3rd Quarter 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
2.440
Nitrogen (TKN)
5.430
54,300.000
Phosphorus *
2.130
21,300.000
Potassium*
0.370
3,700.000
Sulfur
0.000
0.000
Calcium
2.440
24,400.000
Magnesium
0.339
3,390.000
Sodium
0.440
4,400.000
Iron
---
Aluminum*
---
11,400.000
Manganese
---
Copper
---
754.000
1,500
Zinc
---
1,310.000
2,800
Ammonia Nitrogen
0.846
8,460.000
Nitrate N / Nitrite N
---
2.830
Cadmium
---
19.700
39
Chromium
---
33.900
1,200
Nickel
---
25.600
420
Lead
---
45.600
300
Arsenic
---
35.200
41
Mercury
---
1.200
17
Selenium
---
19.700
100
pH*
7.250
Calcium Carbonate Eq. (est
0.000
Organic Nitrogen
4.584
Molybdenum
---
19.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
* Parameters were not analyzed on 8/25/20 sample. Results from 4/30/20 are reported.

Date Reported:
Wastewater Treatment Plant
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
3rd Quarter 2020
8/25/2020 Report No: WL-3-2020-8-25
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
35.970
PAN Inj.
44.430
P
42.600
K
7.400
Lime (estimated)
0.000
Secondary Nutrients
Calcium
48.800
Magnesium
6.780
Sodium
8.800
SAR
1.090
Chloride
0.000
Iron
0.000
Alumium
22.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.44
pH
7.250
Min Rate
0.300
Metals
Arsenic
0.070
Cadmium
0.039
Chromium
0.068
Copper
1.508
Lead
0.091
Mercury
0.002
Molybdenum
0.039
Nickel
0.051
Seleniun
0.039
Zinc
2.620

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Aug 25, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-12250
Project ID: WWTP Sludge
Lab ID
20-30921
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
7/22/2020 9:30 AM
Matrix
Solid/Sludge
Results
Sampled by
Lisa Cottle
Date Analyzed
PAN
Used 30% Mineralization Rate
SAR
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Selenium
Silver
Sodium
Zinc
Cyanide
Total Solids (%)
Ammonia Nitrogen
Mercury
Total Nitrogen (calc)
Total Kjeldahl Nitrogen (TKN)
Nitrate+Nitrite-Nitrogen
Total Nitrogen
Calculat on
Calculat on
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 335.4
SM 2540 B
SM 4500 NH3 C
SW846 7471B
EPA 351 2
EPA 353 2
Total Nitrogen
439 mg/kg 08/14/2020
0.820 08/17/2020
35.2 mg/kg 07/30/2020
<19.7 mg/kg 07/29/2020
24400 mg/kg 08/13/2020
33.9 mg/kg 07/29/2020
754 mg/kg 07/29/2020
45.9 mg/kg 07/29/2020
3390 mg/kg 08/13/2020
<19.7 mg/kg 07/29/2020
25.6 mg/kg 07/29/2020
<19.7 mg/kg 07/29/2020
<19.7 mg/kg 07/29/2020
4400 mg/kg 08/13/2020
1310 mg/kg 07/29/2020
<2.05 mg/kg 07/24/2020
2.44 % 08/18/2020
8460 mg/kg 08/09/2020
1.20 mg/kg 08/06/2020
54300 mg/kg 07/30/2020
2.83 mg/kg 07/30/2020
54300 mg/kg 08/14/2020
Report if 2020-12250 Page 1 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-30922
Test
Date of Report: Aug 25, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-12250
Project ID: WWTP Sludge
Sample ID:
Site: 001
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-30923 Site: 002
Test
Total Solids (%)
Fecal Density
Collect Date/Time
7/22/2020 9:30 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr503
Collect Date/Time Matrix Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
Method Results Date Analyzed
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results Date Analyzed
2.28%
1009 MPN/g
07/23/2020
07/22/2020
Lab ID
20-30924
Test
Sample ID:
Site: 003
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-30925
Test
Site: 004
Total Solids (%)
Fecal Density
Lab ID
20-30926
Test
Total Solids (%)
Fecal Density
Sample ID:
Site: 005
SM 2540 B
SM 9221C E MPN 24 hr 503
Collect Date/Time
7/22/2020 9:30 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Method
2.46 % 07/23/2020
935 MPN/g 07/22/2020
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results Date Analyzed
Collect Date/Time
7/22/2020 9:30 AM
2.33%
558 MPN/g
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results
SM 2540 B
SM 9221C E MPN 24 hr 503
Collect Date/Time Matrix
Method
SM 2540 B
2.28 %
1009 MPN/g
07/23/2020
07/22/2020
Date Analyzed
07/23/2020
07/22/2020
Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
SM 9221C E MPN 24 hr 503
3.16%
412 MPN/g
07/23/2020
07/22/2020
Report # : 2020-12250
Page 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-30927
Test
Sample ID:
Site: 006
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-30928 Site: 007
Test
Total Solids (%)
Fecal Density
Comment:
Reviewed by:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Aug 25, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-12250
Project ID: VVWTP Sludge
Collect DatelTime
7/22/2020 9:30 AM
Method
SM2540B
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results Date Analyzed
2.53 % 07/23/2020
SM 9221C E MPN 24 hr 503 910 MPN/g 07/22/2020
Collect Date/Time Matrix Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
c'tkoia-)
2.46
935 MPN/g
07/23/2020
07/22/2020
Report #:: 2020-12250
Page 3of3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client:IA) Q-ei -mum
Sample Receipt Checklist
Date 7 /ca/Its 0 Report Number -^
!Receipt of sample Delivered-2i UPS 0 FedEx 0 Other 0
❑ YES 'O NO N/A 11 Were custody seals present on the cooler?
,❑ YES 10 NO N/A
`t
Or�inal temperature upon receipt itr
'How temperature taken.
LIR Gun ID
'0 YES
O
t❑
0 YES ❑ NO
YES
2 if custody seals were present, were they intact/unbroken
0 Temperature Blank
Thomas Traceable S/N 192511657
❑ No
O NO
YES !❑ NO
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
O
.❑
❑
t❑
To
NO
NO
❑ NO
❑ NO
❑ NO
O NO
❑ NO
NO
NO
NO
NO
YES I❑ NO
'C Corrected temperature upon receipt
1},' Against Bottles
R Gun Correction Factor 'C: 0 0
3 If temperature of cooler exceeded 6'C, was Project Mgr /O,A notified?
4. Were proper custody procedures (relinquished/received) followed
5 Were sample ID's listed on the COC'
6 Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
8 Were tests to be performed listed on the COCA
9 Did samples arrive in proper containers for each test?
10 Did samples arrive in good condition for each test?
11 Was adequate sample volume available?'
7
12. Were samples received within proper holding time for requested tests
13. Were acid preserved samples received at a pH of <2? "
14. Were cyanide samples received at a pH >121
15. Were sulfide samples received at a pH >9'
16 Were NH3/TKN/Phenol received at a chlorine residual of <0 5 m/L?
17. Were Sulfide/Cyanide received at a chlorine residual of <0 5 m/L'
18. Were orthophosphate samples filtered to the field within 15 minutes?
TOC/,Io at es are pH checked at time of ana ysis and recorded ors the benchsheet
° Bacter a samples are checked for Chlorine at time of analysis and recorded on the oenchsheet
Sample Preservation:
Sample{s,
by adding Icirce one)
Time of preservation
Must oe completed for any sampie(s) incorrectly preserved or with headspacei
were received incorrectly preserved and were adjusted accordinglF
H:504 HNO, HCI NaOH
f more than one preservative is needed, notate in comments below
Note Notify c.,stomer se-v ce m^,ed ate'y for incorrectly preserved undies Octa n a 'sew sa-nc e o'
"ct'fy t^e state 'at+ if d rested to a^a.rted py t^e c.rstome' No was notified date and time
volatiles Sarno e s
COMMENTS:
were received with headsoace
6602 Windmill Way
tlmtrtgton, NC 284D5
910 392 0223
'C
JOC QA 002

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification #94 NHCDHHS: DLS certification #37729
Collection and Chain of Custod
6602 Windmill Way, Wilmington, NC 25405
office: 910-392-0223 Fax: [phone]
[e-mail]
Client: Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: z.t3 — / ZZ 5.-0
Address: 316 E Murray St
Contact name:
PO No:
Wallace, NC 28466
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to: Brent Dean, [e-mail]
Email: [e-mail]
Sampled by: L; 5 A. co. -{e
SAMPLE TYPE: 1= Influent, E= Effluent, W=Well, ST= stream, SO= Soil, SL=Sludge, Other:
collection
a
T
0)
-aE
composite
or grab
a
01
C
Y
° o`
0)
C
Q '=
u E
Lab ID
Number
Preservation
Analysis required
Sample Identification
date
time
temp
C
Z
J
=
. -
in o
1
O
i
o
z
O
cc
=
o
Sludge -(Quarterly)
7- 22-ZD
q, 3 0
G
P
3D5 .1
X
X
X
CN
Ag,As,Cd,Cr,Cu,Hg,Mo,Ni,Pb,Se,Zn
Total N
1. sludge
G
P
3O L 2_
X
Fecal Density,% TS
2. sludge
G
P
105 1..5j
X
Fecal Density,%TS
3. sludge
G
P
30i 1-4X
Fecal Density,% TS
4. sludge
G
P
3r)S �5
X
Fecal Density,% TS
5. sludge
G
P
30rj t6
X
Fecal Density,%TS
6. sludge
{
G
P
3CS 4'7
X
Fecal Density,% TS
7. sludge
G
P
Z,C�j L$
X
Fecal Density,%TS
sluge (annual)
TCLP,RC1
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
NO3+NO2,P, K,Na, TKN,
Transfer
Reli wished By:
Date/time
Received By: f 17
Date/time
(-('')\14
7-2 Z -2O�
1.--_. / ,�,' f
-?-22- C /33
3
z +
—1Q /
t
�_
temp when received:( Accepted: Rejected: Re%ample:
t
delivered By: E... Received by: .--. date/time 7/ 4
,
Comment. t"� turnaround:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Wallace
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WL 4-2020-11-30
11/30/2020
1/21/2021
4th Quarter 2020
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.050
Nitrogen (TKN)*
3.430
34,300.000
Phosphorus *
0.195
1,950.000
Potassium
0.361
3,610.000
Sulfur
0.000
Calcium
2.630
26,300.000
Magnesium
0.311
3,110.000
Sodium
0.373
3,730.000
Iron
---
Aluminum
---
13,500.000
Manganese
---
Copper
---
795.000
1,500
Zinc
---
1,340.000
2,800
Ammonia Nitrogen*
0.000
4.880
Nitrate N / Nitrite N*
---
4,650.000
Cadmium
---
24.100
39
Chromium
---
35.700
1,200
Nickel
---
24.100
420
Lead
---
48.000
300
Arsenic
---
24.100
41
Mercury
---
0.961
17
Selenium
---
24.100
100
pH
IL 5.180
Calcium Carbonate Eq. (esTnii.
0.000
Organic Nitrogen
3.430
Molybdenum
---
24.100
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Wallace WWTP
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
4th Quarter 2020
1/21/2021 Report No: WL 4-2020-11-3
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
29.882
PAN Inj.
29.887
P
3.900
K
7.220
Lime (estimated)
500.000
Secondary Nutrients
Calcium
52.600
Magnesium
6.220
Sodium
7.460
SAR
0.828
Chloride
0.000
Iron
0.000
Alumium
27.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.05
pH
5.180
Min Rate
0.300
Metals
Arsenic
0.048
Cadmium
0.048
Chromium
0.071
Copper
1.590
Lead
0.096
Mercury
0.002
Molybdenum
0.048
Nickel
0.048
Seleniun
0.048
Zinc
2.680

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Lab ID
20-51474
Test
Sample ID:
Site: Sludge 1
Method
Collect Date/Time
11/30/2020 9:50 AM
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
Lab ID Sample ID:
20-51475 Site: Sludge 2
Test
Method
Collect Date/Time
11/30/2020 9:50 AM
2.46%
<732 MPN/g
11/30/2020
11/30/2020
Matrix Sampled by
Solid/Sludge Sean Pistorice
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
Results Date Analyzed
2.71 %
<665 MPN/g
11/30/2020
11/30/2020
Lab ID Sample ID:
20-51476 Site: Sludge 3
Test
Total Solids (%)
Fecal Density
Sample ID:
Site: Sludge 4
Lab ID
20-51477
Test
Total Solids (%)
Fecal Density
Lab ID
20-51478
Test
Collect Date/Time
11/30/2020 9:50 AM
Method
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results Date Analyzed
SM 2540 B
SM 9221C E MPN 24 hr 503
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221 C E MPN 24 hr 503
1.86 %
<968MPN/g
11/30/2020
11/30/2020
Matrix
Solid/Sludge
Results
Sampled by
Sean Pistorice
Date Analyzed
2.35%
<766 MPN/g
Sample ID:
Site: Sludge 5
Total Solids (%)
Fecal Density
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Matrix
Solid/Sludge
Results
11/30/2020
11/30/2020
Sampled by
Sean Pistorice
Date Analyzed
1.97
<914 MPN/g
11/30/2020
11/30/2020
Report #: 2020-20206 Page 1 of 5

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention. Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Lab ID
20-51479
Test
Sample ID:
Site: Sludge 6
Total Solids (%)
Fecal Density
Lab ID
20-51480
Test
Method
SM 2540 B
Collect Date/Time Matrix Sampled by
11/30/2020 9:50 AM Solid/Sludge Sean Pistorice
Results Date Analyzed
SM 9221 C E MPN 24 hr 503
2.10%
<858 MPN/g
11/30/2020
11/30/2020
Sample ID:
Site: Sludge 7
Method
Collect Date/Time
11/30/2020 9:50 AM
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
1.85 %
<973 MPN/g
11/30/2020
11/30/2020
Report #:: 2020-20206 Page 2 of 5

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-51483A
Test
Sample ID:
Site: Sludge
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
Method
[e-mail]
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Collect Date/Time
11/30/2020 1:38 PM
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results
Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 846 Method 8081B/3510
SW 846 Method 80818/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 848 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/351 -
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
<0.02 mg/L 12/08/2020
<0.0005 mg/L 12/08/2020
<0.0005 mg/L 12/08/2020
<0.0005 mg/L 12/08/2020
<0.0005 mg/L 12/08/2020
<0.0005 mg/L 12/08/2020
<0.05 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.250 mg/L 12/08/2020
<0.050 mg/L 12/08/2020
<0.0003 mg/L 12/09/2020
<0.0003 mg/L 12/09/2020
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
Report*: 2020-20206 Page 3 of 5

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info r. environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Mercury
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
TCLP Metals
Arsenic
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
EPA 200.7
EPA 200 7
EPA 200.7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
EPA 200 7
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
<0.05 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
<0.01 mg/L 12/08/2020
13500 mg/kg 12/03/2020
<24.1 mg/kg 12/03/2020
<24.1 mg/kg 12/03/2020
26300 mg/kg 12/03/2020
35.7 mg/kg 12/03/2020
795 mg/kg 12/03/2020
48.0 mg/kg 12/03/2020
3110 mg/kg 12/03/2020
<24.1 mg/kg 12/03/2020
<24.1 mg/kg 12/03/2020
3610 mg/kg 12/03/2020
<24.1 mg/kg 12/03/2020
3730 mg/kg 12/03/2020
1340 mg/kg 12/03/2020
0.961 mg/kg 12/03/2020
4650 mg/kg 12/08/2020
2.05 % 12/08/2020
5.18 units 12/23/2020
<4.88 mg/kg 12/06/2020
34300 mg/kg 12/06/2020
1950 mg/kg 12/09/2020
<1.0 mg/L 12/11/2020
Report #:. 2020-20206 Page 4 of 5

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
12/11/2020
12/11/2020
12/11/2020
12/11/2020
12/11/2020
12/15/2020
12/10/2020
Comment:
Reviewed by:
*Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as
basis.
KaA-uokl, ookil'araJ
received
Report #:. 2020-20206
Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: t • \iLfC.IIaLe,
6602 Windmill Vv
Wilmington, NC 284
910.392.02,
Sample Receipt Checklist
Date: ill30 2) Report Number: O_ f %�(.0
Receipt of sample: ECHEM Pickup
Client Delivery 0 jUPS 0 FedEx 0 Other 0
O YES 0 NO N/A . Were custody seals present on the cooler?
❑ YES 0 NO 1` N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
0 Temperature Blank LA Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 IR Gun Correction Factor °C: 0.0
0 YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES 0 NO 4. Were proper custody procedures (relinquished/received) followed?
YES 0 NO 5. Were sample ID's listed on the COC?
YES 0 NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
YES 0 NO 10. Did samples arrive in good condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of <2? *
r❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES 0 II NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* IOC/Volatiles 1rr pH ciY2cked at time of analyse ;acid roam -led on [tieberich.lit-['t
s
Bacteria; samples are checked fur Chlorine a: time of analysis and recorded on the benchs�teet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H,2SO, HNO; HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
t» ibfy customer service irnmedia'.e1y for ir:corre:tiy preserved samples 0btain a r.ew sample or
notify the state 13b i' directed t r analyzed C;`, the customer. `4as G-_t.f!ed, date and time ^--'
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: D4ocertification t$94 NHCDHHS: DLS certification U37729
Collection and Chain of Custod
6602 Wmdmdl Way, Wilmington, NC 25405
Office: 910-392-0223 Fax: [phone]
[e-mail]
Client: Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: U .-.4 tJ i P
Address: 316 E Murray St
Contact name:
PO No:
Wallace, NC 28466
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to: Brent Dean, [e-mail]
Email: [e-mail]
Sampled by: 54)07A P".54br
SAMPLE TYPE: 1= In luent, E= Effluent, W=Well, ST= stream, SO= Soil, SL=Sludge, Other:
collection
o-
a)
composite
or grab
a
a
c
ro _
c t7
o
y
t E
Lab ID
Number
Preservation
Analysis required
Sample Identification
date
time
temp
c
'
i
a-LLI
0
=
0
=
0
z
O
t-z
ccE
i
O
Sludge -(Quarterly)
G
P
X
X
X
CN
Ag,As,Cd,Cr,Cu,Hg,Ma,Ni,Pb,Se,Zn
Total N
1. sludge
11-36'Lb
or 50
G
P
`1w
1 t
X
Fecal Density,%TS
2. sludge
1
G
P
chi (
X
Fecal Density,% TS
3. sludge
I
j
G
P
j�'1I
X
Fecal Density,% TS
4. sludge
jjj
G
P
I'1`!
X
Fecal Density,%TS
5. sludgei.
G
P
tr�1 I
X
Fecal Density,%TS
6. sludge
1r
G
P
c1•- 1
X
Fecal Density,%TS
7. sludge
G
P
..)\-1\ii0
X
Fecal Density,%TS
sluge (annual}
TCLP,RCI
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
NO3+NO2,P, K,Na, TKN,
Transfer
Relinquished By:
Date/time
Recetvec+y8y: .
Date/ime .
2
temp when received: `�-'\ ," , . Accepted: V Rejected: ,..---"Th Resample:
delivered By: , n Received b t ` i— 1 / f^ date/time '5 3_.
_
Comments: turnaround:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Warsaw
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
2020-07645
5/7/2020
6/2/2020
Annual 2020
Type of Stabilization:Lime
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
3.300
Nitrogen (TKN)*
3.970
39,700.00
Phosphorus
1.650
16,500.00
Potassium
0.294
2,940.00
Sulfur
0.00
Calcium
2.180
21,800.00
Magnesium
0.147
1,470.00
Sodium
0.149
1,490.00
Iron
---
Aluminum
---
8,550.000
Manganese
---
Copper
---
258.000
1,500
Zinc
---
748.000
2,800
Ammonia Nitrogen*
0.000
3.030
Nitrate N / Nitrite N*
---
1,910.000
Cadmium
---
14.900
39
Chromium
---
21.200
1,200
Nickel
---
14.900
420
Lead
---
26.800
300
Arsenic
---
30.100
41
Mercury
---
0.845
17
Selenium
---
14.900
100
pH
6.560
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.970
Molybdenum
---
17.300
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2020
6/2/2020 Report No: WR 2020-07645
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
27.641
PAN Inj.
27.644
P
33.000
K
5.880
Lime (estimated)
0.000
Secondary Nutrients
Calcium
43.600
Magnesium
2.940
Sodium
2.980
SAR
0.478
Chloride
0.000
Iron
0.000
Alumium
17.100
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
3.30
pH
6.560
Min Rate
0.300
Metals
Arsenic
0.060
Cadmium
0.030
Chromium
0.042
Copper
0.516
Lead
0.054
Mercury
0.002
Molybdenum
0.035
Nickel
0.030
Seleniun
0.030
Zinc
1.496

I
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fri
710 B. syscrtowr Road, Nianteo, NC 27954 ° 252.473.5702 L ab/ Fa:,.
255-A Wilmington Highway, Jacksonville, NC 265-10 • cJ i ; b /
ANALYTICAL & CONSULTING CHEMISTS into rt environmentalcnemras.cnm
Town of Warsaw
P.O. Box 464
Warsaw
Attention: Greg Hughes
NC 28398
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide
Sulfide
Ignitability
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
EPA 335.4
SM 4500 S D
SW 640 method 1010
SW 846 Method 90450
EPA 200.7
EPA 203.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 353.2
SM 2540 B
SM 4500 NH3 C
SM 4500 Oro B
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 09070029
Report #: 2020-07645
Project 1D: Sludge
<0.01 mg/L
<0.01 mg/L
<0.05 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
05113/2020
05/13/2020
05/13/2020
05/13/2020
05/13/2020
05/13/2020
0.142 mg/kg 05/12/2020
0.73 mg/kg 05/11/2020
>185 °F 05/21/2020
6.56 units 05/13/2020
8550 mg/kg 05/13/2020
30.1 mg/kg 05/13/2020
<14.9 mg/kg 05/13/2020
21800 mg/kg 05/13/2020
21.2 mg/kg 05/13/2020
258 mg/kg 05/13/2020
26.8 mg/kg 05/13/2020
1470 mg/kg 05/13/2020
17.3 mg/kg 05/13/2020
<14.9 mg/kg 05/13/2020
2940 mg/kg 05/21/2020
<14.9 mg/kg 05/13/2020
1490 mg/kg 05/13/2020
748 mg/kg 05/13/2020
1910 mg/kg 05/13/202G
3.30 % 05/12/2020
<3.03 mg/kg 05/08/2020
39700 mg/kg 05/08/2020
R_per 4 2020-07645

A71AL ' ti AL fz COrISITI Ip1E:i
Town of Warsaw
P.O. Box 464
Warsaw
NC 28398
Attention Greg Hughes
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Environmental Chemists, Ine.
SI:7 4500 P F
SW840 7471 P.
rli• i1K-..2Ct•.".S'il 1':0h1(1:
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 09070029
Report #: 2020-07645
Project ID: Sludge
16500 mg/kg
0.8450 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 rng/l.
<1.0 mg/L
<1.0mg/•_
05/13/2020
05/19/2020
05/14/2020
05/14/2020
05/ 14/2020
05/14/2020
06(14/202 0
0514 /2020
<1.0 mq/L 05114/2020
Mercury EPA 245.'
�___ ........ ____..__ _ _ .-_ �._ _ _ .._._._.___....._.-_-_,... _ ,,. w. __ - G.O./r
0.. mgll 05!1:1/2020
Comment: .:sludge residual results reported on a dry weight basis.
Reviewed by: ti 1 .-� _ ', / -- .
EPA 200.7
EPA 200.7
EPA 20r,
EPA 2007
EPA 2C0 7
EPA 200
LPA 200.7

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

enviroehem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Beulaville
PO Box 7085
Greenville NC 27835
Attention: Angie Miller
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 08100015
Report #: 2020-07646
Project ID: Sludge
Lab ID
20-18820
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
5/7/2020 9:10 AM
Matrix Sampled by
Solid/Sludge client
Results
Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
<0.02 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.05 mg/L 05/18/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.250 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.003 mg/L 05/19/2020
<0.003 mg/L 05/19/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
Report it 2020-07646 Pane 1 of

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax
[e-mail]
Town of Beulaville
PO Box 7085
Greenville NC 27835
Attention: Angie Miller
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 08100015
Report #: 2020-07646
Project ID: Sludge
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
Cyanide EPA 335.4
Sulfide SM 4500 S D
Reporting limit elevated due to matrix Interference.
Ignitability
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
SW 846 method 1010
SW 848 Method 9045D
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 NH3 C
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.05 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
0.145 mg/kg 05/12/2020
<0.50 mg/kg 05/11/2020
>200 °F 05/20/2020
4.65 units 05/13/2020
6280 mg/kg 05/13/2020
30.7 mg/kg 05/13/2020
<23.2 mg/kg 05/13/2020
19700 mg/kg 05/13/2020
23.2 mg/kg 05/13/2020
436 mg/kg 05/13/2020
29.6 mg/kg 05/13/2020
2050 mg/kg 05/13/2020
<23.2 mg/kg 05/13/2020
<23.2 mg/kg 05/13/2020
3840 mg/kg 05/21/2020
<23.2 mg/kg 05/13/2020
3890 mg/kg 05/13/2020
1880 mg/kg 05/13/2020
7740 mg/kg 05/13/2020
2.07 % 05/12/2020
<4.83 mg/kg 05/08/2020
Report #:: 2020-07646
Porno . n/ 7

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmentalchemists.com
Town of Beulaville
PO Box 7085
Greenville NC 27835
Attention: Angie Miller
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 08100015
Report #: 2020-07646
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 Org B
SM 4500 P F
SW846 7471B
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
55600 mg/kg
14400 mg/kg
2.02 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
05/08/2020
05/13/2020
05/19/2020
05/14/2020
05/14/2020
05/14/2020
05/14/2020
05/14/2020
05/14/2020
05/14/2020
05/19/2020
Comment: Sludge residual results reported on a dry weight basis.
Reviewed by: - (.
A...
Report #. 2020-07646
Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: . f'.(' ii �C Vt 1 i.-t
Receipt of sample:
O YES
❑ YES
Sample Receipt Checklist
Date: '1 2 L' Report Number:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
to 1
❑ NO
❑ NO
Delivered
P N/A
;181 N/A
UPS 0 FedEx ❑ Other 0
1. Were custody seals present on the cooler?
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt .4 °C Corrected temperature upon receipt
0 Temperature Blank Dii Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ NO 3. If temperature of cooler exceeded 6"C, was Project Mgr./CIA notified?
❑ NO 4. Were proper custody procedures (relinquished/received) followed?
a' YES 5. Were sample ID's listed on the COC?
How temperature taken:
CIYES
cif YES
Fir YES
tit YES
YES
(4 YES
1ir YES
X YES
X YES
O YES
O YES
O YES
O YES
O YES
O YES
❑ NO
❑ NO
❑ NO
❑ NO
O NO
❑ NO
❑ NO
❑ NO
❑ NO
0 NO
O NO
O NO
O NO
O NO
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2? *
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
Time of preservation:
H2504 HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. CIA.002

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
N OF CUSTODY
910.392.0223 252.473.5702
[e-mail]
CLIENT: Town of Beulaville
PROJECT NAME: Annual Sludge
REPORT NO: AI — �f elf
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
•
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
Semple Type
s
a 8o
Container
(P or G)
d
f
"
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
D e
Time
Temp
_
z
3
3
o
_
o
w
o
Sludge
i )72.
9 1-- A
C
P
�Q��
X
Full TCLP
G
G
C
P
X
Nutrients/Metals
G
G
P
i
X
RCI
G
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
o
Temperature when Received: L .-'f Accepted: Rejected: Resample R e ted:
Delivered By: Received By: Date: -/ k. Time: 9-i
Comments: " TU OUND:

Waypoi nt
ANALYTICAL
10/8/2020
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number 20-268-0013
Project Description Holding Tank 2
Waypoint Analytical Virginia, Inc. received sample(s) on 9/24/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices,are reported on en es -
received basis unless otherwise indicated. This report shall not be reproduced except in full anc relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely.
t24.4eit wy/
Paunc McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option. repeating the
analysis in question at laboratory's expense. or the refund of the charges paid for performance of said analysis.
Page 1 of 10

Waypoint
ANALYTICAL
Report Number: 20-268-0013
Client Project Description: Holding Tank 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticaLcom
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 SW-1311 WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 8081A WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 SW-1311 (ZHE) .A/P MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 8151A WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 6010D WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 82608 WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 8270C WP MTN
73774 Holding Tank 2 TCLP 09/23/2020 13:00 09/24/2020 7470A WP MTN
73775 Holding Tank 2 Solids 09/23/2020 13:00 09/24/2020 SW-9045C WP MTN
73775 Holding Tank 2 Solids 09/23/2020 13:00 09/24/2020 SW-7.3.4 WP MTN
73775 Holding Tank 2 Solids 09/23/2020 13:00 09/24/2020 SW-7.3.3 WP MTN
73775 Holding Tank 2 Solids 09/23/2020 13:00 09/24/2020 ASTM D93-80 WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 1

Waypoint.
ANALYTICAL
46546
Town 0f Clayton
P08 879
Clayton , NC 27528
Report Number : 20-268-0013
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypointanalyticaLcom
Project Holding Tank 2
Information
REPORT Of ANALYSIS
Report Date : 10/08/2020
Received : 09/24/2020
/r. ('l &er,; /
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73774 Matrix: TCLP
Sample ID : Holding Tank 2 Sampled: 9/23/2020 13:00
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
LCLP Herb ode Extraction Combined 1 09/29/20 15:19 RMW SW-1311
1 CL P Metals Extraction Combined 1 09/29/20 15:19 RMW SW-1311
TCLP Pesticide Extraction Combined 1 09/29/20 15:19 RMW SW-1311
TCLP SVOC Extraction Combined 1 09/29/20 15:19 RMW SW-1311
TCLP VOC ZHE Extract on Combined 1 09/29/20 15:02 RMW SW-1311 (ZHE)
Analytical Method: 6010D Prep Batch(es): L5140O1 09/30/20 09:22
Prep Method: 3015A
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
TCLP Arsenic <0.750 rng/L 0.250 1 10/01/20 08:04 DADS L514304
TCLP Barium <0.250 mg/L 0.250 1 10/01/20 08:04 DADS L514304
TCLP Cadmium <0.0500 rng/L 0.0500 1 10/01/20 08:04 DADS 1514304
TCLP Chromium <0.100 mg/1 0.100 1 10/01/20 08:04 DADS L514304
TCLP Lead <0.100 mg/L 0.100 1 10/01/20 08:04 DADS L514304
TCLP Selenium <0.500 mg/1 0.500 1 10/01/20 08:04 DADS L514304
TCLP Silver <0.0500 mg/L 0.0500 1 10/01/20 08:04 JADS L514304
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 10

Waypoint.
ANALYTICAL
46546
Town 0f Clayton
P0B 879
Clayton , NC 27528
Report Number:20-268-0013
Lab No : 73774
Sample ID : Holding Tank 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.com
Project Holding Tank 2
Information •
REPORT OF ANALYSIS
Report Date : 10/08/2020
Received : 09/24/2020
Paunc Mc Groary Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 9 / 23 / 2020 13:00
Analytical Method: 7470A Prep Batch(es): L515414 10/08/20 07:30
Prep Method: 7470A
Test
Results
Units
MQL
DF
Date i Time
Analyzed
By Analytical
Batch
TCLP Mercury
<0.0200
mg/L
0.0200 1 10/08/20 14:57 DOB L515563
Analytical Method: 8081A Prep Batch(es): L514155 09/30/20 16:40
Prep Method: 3510C
Test Results Units MQL
DF Date / Time By
Analyzed
Analytical
Batch
TCLP Endrin
TCLP gamma-BHC
TCLP Methoxychlor
TCLP Toxaphene
TCLP Chlordane
TCLP Heptachlor Epoxide
TCLP Heptachlor
Surrogate. Decachlorobiphenyl
Surrogate: Tetrechloro-m-xylene
Analytical Method: 8151A
Prep Method: 8151A
Test
<0.001600
<0.001600
<0.001600
<0.01200
<0.008000
<0.001600
<0.001600
Results
mg/L
mg/L
mg/L
mg/L
nig/L
mg/ L
mg/L
0.001600
0.001600
0.001600
0.01200
0.008000
0.001600
0.001600
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
10 10/01/20 02:20 VIC L514318
90.92 Limits: 36-116% 10 10/01/20 02:20 VIC L514318
98.08 Limits: 25-123% 10 10/01/20 02:20 VIC L514318
Prep Batch(es): L514409 10/01/20 17:40
Units
MQL
DF Date / Time By
Analyzed
Analytical
Batch
TCLP 2,4-D
TCLP 2,4,5-TP (Silvex)
Surrogate: DCAA
<0.0200
<0.0020
40.80
mg/L
mg/L
0.0200
0.0020
Limits: 20-120%
1 10/02/20 21:34 VIC
1 10/02/20 21:34 VIC
1 10/02/20 21:34 VIC
L514792
L514792
1.514792
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
Pace 4 et. 10

Waypoint
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number:20-268-0013
Lab No : 73774
Sample ID : Holding Tank 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank 2
Information :
REPORT OF ANALYSIS
Report Date : 10/08/2020
Received : 09/24/20 .0
ri
I)C1411.6- 1 (,rQOWtJ
Pauric Mc Groarj Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 9/ 23/ 2020 13:00
Analytical Method: 82606
Prep Method: 5030B
Test Results
Prep Batch(es): L514230 09/30/20 09:21
Units
MQL
DF Date / Time
Analyzed
By Analytical
Batch
TCLP Benzene
TCLP Carbon Tetrachloride
•TCLP Chlorobenzene
TCLP Chloroform
TCLP 1,4-Dichlorobenzene
TCLP 1,2-Dichloroetha;le
TCLP 1,1-Dichloroethene
TCLP Methyl Ethyl Ketone (MEK)
TCl P Tetrachloroethene
TCLP Trichloroethene
TCLP Vinyl Chloride
Surrogate: 4-Bromofluorobenzene
Surrogate: Dibromofluorometharie
Surrogate: 1,2-Dichlorcetnane - d4
Surrogate: Toluene-d8
Analytical Method: 8270C
Prep Method: 3510C
Test
0.0116
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
<0.200
<0.0100
<0.0100
<0.0100
Results
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.0100
0.0100
0.0100
0.0100
0.0100
0.0100
0.0100
0.200
0.0100
0.0100
0.0100
91.2 Limits: 71-137%
86.2 Limits: 70-128%
95.2 Limits: 63-136%
80.6 Limits: 70-130%
Prep Batch(es): L514571 10/02/20 12.10
Units
MQL
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
09/30/20
18:04
18:04
18:04
18:04
16:04
18:04
18:04
18:04
18:04
18:04
18:04
MKD
MKD
MKD
MKD
MKD
MKD
MKD
MKD
MKD
MKD
MKD
1 09/30/20 18:04 MKD
1 09/30/20 18:04 MKD
1 09/30/20 18:04 MKD
1 09/30/20 18:04 MKD
L514248
L514248
L514248
L514248
L514248
1514248
L514243
L514248
L514248
L514248
L514248
L514248
L514248
L514248
L514248
DF Date / Time By Analytical
Analyzed Batch
TCLP 2-Methylphenol
TCLP 3&4 Methylphenol
TCLP 2,4-Dmitrotoluene
<0.100
<0.200
<0.100
mg/L
mg/L
mg/L
0.100
0.200
0.100
5 10/05/20 16:38 CCB
5 10/05/20 16:38 CCB
5 10/05/20 16:38 CCB
L514730
L514730
L514730
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
Page 5 of 10

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number : 20-268-0013
Lab No : 73774
Sample ID : Holding Tank 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401° Fax [phone]
www.waypointanalytical.com
Project Holding Tank 2
Information :
REPORT OF ANALYSIS
Report Date : 10/08/2020
Received : 09/24/2020 M
L Yep c,/ /
Paunc Mc Groary Ph.D., CPA
Agronomist
Matrix: TCLP
Sampled: 9/ 23/2020 13:00
Analytical Method:
8270C Prep Batch(es): L514571 10/02/20 12:10
Prep Method: 3510C
Test
Results
Units
MOL
DF Date r Time
Analyzed
By Analytical
Batch
TCLP Hexachlorobencene
TCLP Hexachlorobutadiene
TCLP Hexachlorcethane
TCLP Nitrobenzene
TCLP Pentachlorophenol
TCLP Pyridine
TCLP 2,4,5-Trichlorophencl
TCI P 2,4,6-Trichlorophencl
Surrogate: TCLP 2,4,6-Tribromophenol
Surrogate: TCLP 2-Fluorobiphenyl
Surrogate: TCLP 2-Huorophenol
Surrogate: TCLP 4-1erphenyl-d14
Surrogate: TCLP Nitrobenzene-d5
Surrogate: TCLP Phenol-d6
<0.100 mg/L
<0.100 mg/1
<0.100 mg/L
<0.100 mg/L
<0.200 mg/L
<0.100 mg/L
<0.100 mg/L
<0.100 mg/L
56.3
45.0
18.0
64.5
45.0
12.5
0.100
0.100
0.100
0.100
0.200
0.100
0.100
0.100
Limits: 42-102%
Limits: 24-860/
Limits: 13-37%
Limits: 30-122%
Limits: 25-78%
Limits: 9-27%
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
CCB
CCB
CCB
CCB
CC0
CCD
CCB
CCB
5 10/05/20 16.38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16:38
5 10/05/20 16;38
5 10/05/20 16:38
CCB
CCB
CCB
CCB
CCB
CCB
L514730
L514730
L514730
1514730
L514730
L514730
L514730
1514730
L514730
L514730
1514730
L514730
L514730
L514730
Qualifiers/
Definitions
DF Dilution Factor
MQL
Method Quantitation Limit
Page 6 cf 10

Waypoint.
ANALYTICAL
46546
Town Of Clayton
P0B 879
Clayton , NC 27528
7621.Whitepine Road, Richmond, VA 23237
Main 804-743-9401° Fax [phone]
www.waypointanalytical.com
Project Holding Tank 2
Information :
Report Number :20-268-0013 REPORT OF ANALYSIS
Lab No : 73775
Sample ID : Holding Tank 2
Report Date : 10/08/2020
Received : 09/24/2020
'a4411.f. m ( 6+6 pty
Paunc Mc Groat)/ Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 9/ 23/ 2020 13:00
Test Results Units MQL DF Date i Time By Analytical
Analyzed Method
Cyanide (Reactivity) <0.125 mg/Kg 0.125 1 10/06/20 10:45 FMh1 SW-7.3.3
Ignitability >96 degrees C 1 10/06/20 08:39 JDT ASTM D93-80
pH 6.7 s.u. 1 10/05/20 13:00 ADM SW-9045C
Sulfide (Reactivity) <25.0 mg/Kg 25.0 1 10/06/20 10:45 FMM SW-7.3.4
Qualifiers/
Definitions
DF Dilution Factor 1 Limit Exceeded
MQL Method Quantitation Limit
Pace 7 of 10

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton
Project: Holding Tank 2
Lab Report Number: 20-268-0013
Date: 10/8/2020
CASE NARRATIVE
Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D
Sample 73774 (Holding Tank 2)
QC Batch No L514730/L514571
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 8 of 2.0

Waypoint
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 20-268-0013
G Fed Ex
• UPS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Shipping Method
CD US Postal 0 Lab
O Client 0 Courier
J Other:
Thermometer ID: i
Shipping containericooler uncompromised?
• Yes Q No
Number of coolers/boxes received 1 1
Custody seals intact on shipping container/cooler? (s) Yes
L.) No • Not Present
Custody seals intact on sample bottles? 0 Yes
J' No
Not Present
Chain of Custody (COC) present?
• Yes 0 No
COC agrees with sample label(s)?
• Yes 0 No
COC properly completed
Samples in proper containers?
• Yes
40 Yes
O No
O No
Sample containers intact?
• Yes 0No
Sufficient sample volume for indicated test(s)? • Yes
O No
All samples received within holding time?
• Yes 0No
Cooler temperature in compliance?
• Yes (ThNo
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes 0No
Water - Sample containers properly preserved 0 Yes
Water - VOA vials free of headspace 0 Yes
O No
n No
• •
NIA
NIA
Trip Blanks received with VOAs
0 Yes 0 No • N/A
Soil VOA method 5035 — compliance criteria met r) Yes
O No • N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes
• No
Signature Samantha Clarke Date & Time. 09.24/2020 10:5442
Page 9 of 10

WASTEWATER SAMPLE TRs1NSMITTAI. FORM/CHAIN OF CUSTODY
\V'a).point Analytical
'i Nlr rlu.R !tP I+,..1%\)Ct- ICI t.1'4I-•un1 l,r. U-1' 1,41
wu.I -yap n1• J .“,! p.mrt.el.11s Its .I ,au
.AcrOunt
Customer Information
Submlttod Ely
Charge To
CopyTo
�J'� •
2Lt/Ny arcra yfAN
sag (
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PO Boer g ?9
c",4774ew, A)c 2?f2.
Protect (
P^une.gt9-S,S3-/536 Fa' 9i4-SS3-/9/j. Ema 6L r ray etaA)..i.z cI/ z`GAiVC.G,
Sample Information
F.:,.,),. : ID
Litt cer
Let. L'S2
C. • nrt.! leforn3! dl
Ccnt3ne: 1 Iamat an
Pe• % Y.,'tt De!. el Tests
t,T.e
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0 'e
T. a
Hac!nv e!7 B' ISIgr‘alure+
Dtle
(,me
Test Available
Special Instructions or Remarks
`1rtr<.fy Se e, T M31 Kyekiat"I Ammonium rI tr8te 8 0,-conic Natogre1
Ph(-sn^'rys. lr ta, - rr.or) oclt;slum Shcidt•_ Salfur Calcium MilUnoclt;rp S.*;:(0n Ir)n Alnm:!11:m
!-1.t--piEC? LGCT Of Z.ne Afier11C Bar'•i.rl Cd']'n..:n• Crinrl+Urn Cubait 7!olyCaer:ur-1 ).19rrt:r'} Lelr!
=oIen,Jm Sll'.er rie. Rel Acx-ty (To1ar) Allit,iI' T?I4ll Stor hernic.31 D. yr)r:n laemann; tr, dey'l Bctc.•
=. rr 4,31 O• rgen De' land Ch cnde C:.1d..te1 int.e (Stec. I t) 4e.a ,itle-t Chrpn,tu' + I. and C_=rea5e (EPA 1
t.H Phenol SGIIus (Dissolved Suspe rdt:tl Otill vulat:lt'I
O
limo
I! 1-\ C O\' v .i

Waypoi nt
ANALYTICAL
4/30/2020
Town Of Clayton
POB 879
Clayton, NC. 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 20-112-0006
Project Description: Holding Tank
Waypoint Analytical Virginia, Inc. received sample(s) on 4/21/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance
Tne results are shown on the attached Report of Analysists). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
7
Paunc McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to. at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the chares paid for performance of said analysis.

Waypoint"
��1
ANALYTICAL
Report Number: 20-112-0006
Client Project Description: Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
/1113 Holding Tank Solids 04/20/2020 1G:30 04/21/2020 SM-2540G WP M IN
/1113 Holding lank Solids 04/20/7020 10:30 04/21/2020 SW-7.3.3 WP MTN
71113 Holding Tank Solids 04/20/2020 10:30 04/21/2020 SW-7.3.4 WP MTN
71113 Holding Tank Solids 04120/2023 10:30 04/21.12020 SW-90-45C ,..VP MTN
71113 Holding Tank Solids 0420/2020 10:30 04/21/2020 ASTM D93-80 WP MTN
WP MTN - Memphis, TN: W1ypoint Analytical -TN, Memphis, TN

Waypoint.
ANALYTICAL
465-16
Town 0f Clayton
P0B 879
Clayton , NC 27528
Submitted By : James Warren
Report Number : 20-112-0006
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
James Warren
Project Holding Tank
Information :
REPORT OF ANALYSIS
Report Date : 04/30/2020
Receved : 04/21/2020
Pam. Inc Gel`'
Paunc McGroary
Agronomist
Lab No : 71113 Matrix: Solids
Samp:e ID : Holding Tank Sampled: 4/20/2020 10:30
Test Results Units MOL DF Date Time By Analytical
Analyzed Method
Moisture 97.7 0.010 1 04/24/20 16:46 CJR SM-2540G
Tall Results Units MOL DF Date Time By Analytical
Analyzed Method
Cyanide (Reactivity) <5.43 mg/Kg - dry 5.43 1 04/ 28/ 20 10:55 FMM SW-7.3.3
ignitability >96 degrees C 1 04/23/20 08:24 JDT ASTM D93-80
pH 6.3 s.u. 1 04/30/20 06:11 JSL SW-9045C
Total Solids 2.29 `%'c 0.010 1 04/24/20 16:46 CJR SM-2540G
Sulfide (Reactivity) <1090 mg/Kg - dry 1090 1 0-4/28/20 10:00 FMN1 SW-/.3.4
Qualifiers/
Definitions
D Nut on Factor L Limit Exceeded
MQL Method Quant:tation Limit

Waypoi nt(
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 20-112-0006
Fed Ex
• UPS
O US Postal
O Client
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Shipping Method
() Lab
J Courier
0 Other:
Thermometer ID: I
Shipping container/cooler uncompromised?
• Yes 0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
) Yes () N• o • Not Present
Yes f No • Not Present
Chain of Custody (COC) present?
• Yes ( No
COC agrees with sample label(s)?
• Yes c) No
COC properly completed • Yes
▪ No
Samples in proper containers? • Yes
N• o
Sample containers intact? • Yes
N• o
Sufficient sample volume for indicated test(s)? • Yes
0 No
All samples received within holding time?
• Yes C.No
Cooler temperature in compliance?
• Yes (:: No
CoolerrSamples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
r.• No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
I'; Yes 0 No • WA
Yes `: No • N/A
Trip Blanks received with VOAs
Yes
No
�NPA
Soil VOA method 5035 — compliance criteria met i,_; Yes
0 No • N/A
High concentration container (48 hi.) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes
• No
Signature: Brandi Watson Date & Time: 04'21/2020 13:33:26
'aae _ ,.i

Project
\VASTEWATLR SAM11'I.h I RANSMI I -I Al. FORM CIIAIN OF CUSTOD1"
WAN. p. in. ti .11
411u:. p.u: N.vd N,.I:,a,,..c 1 \ c_+ 1 . • •4 I' 3 t , • . III I •ie•.i n1Y^ u1., . a•p, mt :,:,:7. t.. •, ., m
Customer Information
Submitted By
Charge To
opt To
_ 'Ar1'•,f Lr.
('•;r;fr;•
/1
1?L
r i,,t:,'c.,
r.•matl�• •- ^ : },.. `` :. ,::
•
Sari,-:e IU
Lit
: t:,L' t,"e
Ord,
Sample Information
(,ynL.r @• tr!tr+n:y �r . '?.3G? t^: rn.• In De;.roa t !:n
ir-
N'pr0<r
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•
•
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Test Available
I.7Tt. i t•i••.
2Y:t' .r j icy
2II 29
Soectai Instrvatc.ns pr Nirnerts
T.Mal Ao;rt;:nly i. NNr:ne C'!:)a' tb!,,,qtri
Ph:KC'�gr) i1i 6ti, !;rt7a:rt PU+i4b, o St!late•Sullu Cd1C'ylr, 7...to 'C+1.lIDi 7utl1 '+ of:.n A:il^,u tiCl
!i'.j.d^tse {:Upt?•:: Zll.: A15C,.,C Si' in Catirn,urt Ch+_, j'+ i'pbrll) 7.7UIilrl.:r;,r.• i.7rr,�Ylrq i_efal
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r? rn�1cd Scinls it.isy v oa S '4r -:ger. Toy.; nt.1t11_•'
r•: itrit r( . , /ri. .Prrtr, i ) . 1 •/ y 4, -
? g_ _. v.. 7

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC _84. 5 i '3i0.392.02_23 Lab 910.392. 24 Fa
710 Buwsertowr. Road, iVlanteo, NC 27954 2524735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NiC 28.540 s 910 347.5843 Lab/cat;
into(5)enviroilmentuichetmsts.com
Town of Kenansville
PO Box 370
Kenansville
Attention:
NC 28349
Date of Report: Jul 15, 2020
Customer PO #:
Customer ID: 09020018
Report #: 2020-09561
Project ID: Sludge
Lab ID
20-23843
Test
Sample ID:
Site: sludge
Method
Collect Date/Time Matrix Sampled by
6/10/2020 10:00 AM Solid/Sludge Garry Benson
Results Date Analyzed
Total Solids (%)
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1.1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
SM 2540 B
SW 846 Method 8081B/3510
SW 846 Method 80818/3510
SW 846 Method 8081B/3510
SW 846 Method B06113/3510
SW 846 Method 8081B/3510
SW 846 Method B0818/3510
SW 845 Method 80618/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method B270/3510
SW 845 method 8270;3510
SW 846 method 8270/3510
SW846 method 8270i3510
SW B46 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270:3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW646 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW646 Method 8260/5030
SW346 Method 8262/5030
0.51 %
<0.02 mg/L
<0.0005 ma/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.05 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0 050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg,'L
<0.250 mg/L
<0.050 mg1L
<0.003 mg/L
<0.003 mg/L
<0.01 ma/L
<0.01 mg!L
<0.01 mg/L
06/11/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/23/2020
06/24/2020
06/24/2020
06/25/2020
06/25/2020
06/25/2020
Report 2020.09561
Page 1 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc..
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Mlanteo, NC 27954 G 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab /Fax
iniorgena i ronmenta lcnemists.com
Town of Kenansviife
PO Box 370
Kenansville NC 28349
Attention:
Carbon Tetrachloride (TCLP)
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Date of Report: Jul 15, 2020
Customer PO #:
Customer ID: 09020018
Report #: 2020-09561
Project ID: Sludge
SWB4B Method 8260/5030
SW846 Methcd B260/5030
SW846 Method 8260/5030
SW848 Method B260/5030
SWB48 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
<0.01 mg/L 06/25/2020
<0.01 mg/L 06/25/2020
<0.01 mg/L 06/25/2020
<0.05 mg/L 06/25/2020
<0.01 mg/L 06/25/2020
<0.01 mg/L 06/25/2020
<0.01 mg/L 06/25/2020
Cyanide EPA 335 4
Reporting limit elevated due to matrix interference. <0.05 mg/kg 06/29/2020
Sulfide SM 4500 s 0
lgnit bility
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Ammonia Nitrogen
SW 848 method 1010
SW 846 Method 9045D
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 4500 NH3 C
0.81 mg/kg 06/16/2020
> 195 °F 06/26/2020
6.79 units 07/06/2020
4040 mg/kg 06/16/2020
57.5 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
17500 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
353 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
1670 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
3040 mg/kg 06/16/2020
<48.0 mg/kg 06/16/2020
11900 mg/kg 06/16/2020
763 mg/kg 06/19/2020
80.8 mg/kg 06/20/2020
<19.6 mg/kg 06/11/2020
Page 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
CoJ2 Windmill Way, Wilmington, \C 28405 • 910. (42.0223 Lab • 910.399.44.)4 Fax
710 Bowsertvwn Road. Manteo, NC 27954 • 252.47 3.5702 Lab/Fax
255-A Wilm -tgton fighwav, Jacksonville, NC 28540 ; 910.34; .5,943 Lab /Fax
in foi:Lenvironmen taIchenusts.c0m
Town of Kenansville
PO Box 370
Kenansville
Attention -
NC 28349
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 Org B
SM 450C P F
SW846 7471B
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200.7
EPA 2C0.7
EPA 245 1
Customer ID:
Report #:
Project ID: Sludge
Date of Report: Jul 15, 2020
Customer PO #:
09020018
2020-09561
33200 mg/kg
9050 mg/kg
<3.28 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
06/11/2020
06/19/2020
06/15/2020
06/25/2020
06/25/2020
06/25/2020
06/25/2020
06/25/2020
06/25/2020
06/25/2020
06/25/2020
Comment: Sludge residual results, except pH, reported on a dry weight basispH reported on an as received
basis.
Reviewed by: ok OJ.j, Ottinx,t3
ReOcrt 0:: 202C-0956.•
Page 3 a' 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client:
Receipt of sample:
O YES
O YES
Vim
Delivered
N/A
N/A
Ori inat temperature upon eceipt
How temperature taken:
❑ NO
❑ NO
se
Sample Receipt Checklist
Date
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Report Number:c
UPS ❑ FedEx O Other ❑
1. Were custody seals present on the cooler?
2. If custodyseals were present, were they intact/unbroken?
'C
❑ Temperature Blank
IR Gun ID: Thomas Traceable S/N 192511657
O YES
r'
YES
YES
YES
YES
O YES
0
YES
YES
O YES
O YES
O YES
Corrected temperature upon receipt
Against Bottles 'C
IR Gun Correction Factor 'C: 0.0
❑ NO 3. If temperature of cooler exceeded 6'C, was Project M: r./QA notified?
❑ NO 4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
6. Were samples Vs listed on sample containers?
0 NO 7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
9. Did samples arrive in proper containers for each test?
10. Did samples arrive In good condition for each test?
11. Was adequate sample volume available?'
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2? e
14. Were cyanide samples received at a pH >12?
❑ NO 15. Were sulfide samples received at a pH >9.
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
❑ NO
❑ NO
O NO
❑ NO
CINO
❑ NO
O NO
❑ NO
❑ NO
❑ NO
CINO
NO._ 18. Were c, r ophospbate_sacapies.f lterr ge ithirr15 minutes ---
e TOC/Volatiies are pH checked at time of analysis and recorded on the benchsheet.
° o Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservatio
n:
(Must be completed for any samples} incorrectly
Y preserved or with headspace)
SO
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H
z ° HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time;
Volatiles Sample(s)
were received with headspace
COMMENTS: -
DOC. QA.002

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill ‘Vav, Wilmington, NC 28405 • 910.392.02211 ab • 911).392.4424 Fai
710 Bowsertnwn Road, Manteo, NC 27954 • 252.473.571)2 Lab/Fa\
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.58.43 Lab/Fax
inlu/u em ironmentalchemists.com
Environmental Services
PO Box 1054
Jacksonville NC 28541
Attention: Sonny Scozzari
Date of Report: Apr 13, 2020
Customer PO #:
Customer ID: 14110017
Report #: 2020-03793
Project ID: Bear Trail Golf Course
Lab ID
20-09213
Test
Sample ID:
Site: Sludge
Method
3/4/2020
Collect Date/Time Matrix Sampled by
Solid/Sludge Sonny Scozzari
Results Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
RCI
Cyanide
Sulfide
Ignitability
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 80818/3510
SW 846 Method 8081B/3510
SW 846 Method 80818/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
EPA 335.4
SM 4500 S D
SW 846 method 1010
<0.02 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.05 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
0.400 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
0.400 mg/L
<0.050 mg/L
<0.050 mg/L
<0.250 mg/L
<0.050 mg/L
<0.003 mg/L
<0.003 mg/L
0.077 mg/kg
0.49 mg/kg
>210°F
03/19/2020
03/19/2020
03/19/2020
03/19/2020
03/19/2020
03/19/2020
03/19/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/20/2020
03/16/2020
03/31/2020
03/12/2020
Report # 2020-03793 Page 1 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 25405 • 910.392.0223 Lab • 91(1.192.4424 Fax
710 Bowsertotvn Road, Mantes. NC 27934 • 252.473 5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 26'540 • 91(1.347.5843 Lab/Fax
inturu en.tronntentaIchemisRcom
Environmental Services
PO Box 1054
Jacksonville NC 28541
Attention: Sonny Scozzari
Date of Report: Apr 13, 2020
Customer PO #:
Customer ID: 14110017
Report #: 2020-03793
Project ID: Bear Trail Golf Course
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+N itrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
SW 846 Method 9045D
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 353 2
SM 2540 B
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
S W 846 7471B
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
7.07 units 04/02/2020
2970 mg/kg 03/12/2020
<9.65 mg/kg 03/12/2020
<9.65 mg/kg 03/12/2020
15100 mg/kg 03/12/2020
12.8 mg/kg 03/12/2020
158 mg/kg 03/12/2020
<9.65 mg/kg 03/12/2020
2460 mg/kg 03/12/2020
<9.65 mg/kg 03/12/2020
<9.65 mg/kg 03/12/2020
4090 mg/kg 03/24/2020
<9.65 mg/kg 03/12/2020
200 mg/kg 03/16/2020
854 mg/kg 03/12/2020
64.2 mg/kg 03/11/2020
2.54 % 03/09/2020
4130 mg/kg 03/10/2020
77200 mg/kg 03/11/2020
16200 mg/kg 03/19/2020
<0.614 mg/kg 03/13/2020
<1.0 mg/L 03/19/2020
<1.0 mg/L 03/19/2020
<1.0 mg/L 03/19/2020
<1.0 mg/L 03/19/2020
<1 0 mg/L 03/19/2020
<1.0 mg/L 03/19/2020
<1.0 mg/L 03/19/2020
Report # 2020 03793 Page 2 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Wav, 4Vilrnin;gti n, NC 28405 • 910.392.0223 Lab • 910.392.4-124 fra\
710 Bowser own Road, Monteo, NC 27954 • 252.473.5702 Lab/ l-a\
25=+-A Wilmington Highway, Jacksonville, NC 28540 • 910.347 5843 Lab/Fa\
infoiu.en irunmentalchcmi;tt.com
Environmental Services
PO Box 1054
Jacksonville NC
Attention: Sonny Scozzari
Date of Report: Apr 13, 2020
Customer PO #:
28541 Customer ID: 14110017
Report #: 2020-03793
Project ID: Bear Trail Golf Course
Mercury
EPA 245 1
<0.0002 mg/L
03/19/2020
Comment: Sludge residual results reported on dry weight basis.
Reviewed by:
kvActuziil, OQAOIUL
Report # 2020-03793 Page 3 of 3

Client:JG\Vf -{( (-2C
Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
-1 2a-If s- y j _
Date: y� 3 15t=U Report Number:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Receipt of sample: Delivered UPS 0 FedEx ■ Other •
• YES
• NO
N/A
1. Were custody seals present on the cooler?
• YES
• NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt (v.l) 9C Corrected temperature upon receipt 9C
How temperature taken: • Temperature Blank 4 Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
• YES
• NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./GA notified?
EX YES
0 NO
4. Were proper custody procedures (relinquished/received) followed?
cir YES
• NO
5. Were sample ID's listed on the COC?
I ' YES
0 NO
6. Were samples ID's listed on sample containers?
YES
0 NO
7. Were collection date and time listed on the COC?
YES
• NO
8. Were tests to be performed listed on the COC?
Pe YES
0 NO
9. Did samples arrive in proper containers for each test?
IX YES
• NO
10. Did samples arrive in good condition for each test?
XYES
• NO
11. Was adequate sample volume available?
t4f YES
• NO
12. Were samples received within proper holding time for requested tests?
❑ YES
• NO
13. Were acid preserved samples received at a pH of <2? •
• YES
• NO
14. Were cyanide samples received at a pH >12?
• YES
• NO
15. Were sulfide samples received at a pH >9?
• YES
0 NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ••
❑ YES
• NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
• TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
'''• Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Samples) Nere received with headspace
COMMENTS:
JUC - CA.UO2

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT:
ENVIRONMENTAL SERVICES
PROJECT NAME:
BEAR TRAIL GOLF COURSE
REPORT NO: jr — C`---) f `/ a]
ADDRESS:
PO BOX 1054
CONTACT NAME:
SONNY SCOZZARI
PO NO:
JACKSONVILLE, NC 28541
REPORT TO:
PHONE/FAX: [phone]
COPY TO:
email: [e-mail]
Sampled B1r: , �,•
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
Sample Type
Composite
or
Grab
Container
(P or G)
c
Q E
"
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
c
=
,,
y
g
z
=
a
Z
o
5
o
Effluent
C
P
X
BOD, TSS, NO2
Effluent
C
P
X
NO3, NH3, TKN, TP
Effluent - Grab
P
X
Fecal Coliform
G
Effluent - Triannuals
(March, July, November)
C
P
X
TDS, Chloride
7
• /
••
l
0\t\
`' ,uclkci.0
7tcP
Transfer
RelinquishedtBy:
Date/Time
Received By:
Date/Time
;13/5
2.
r
Temperature when Received:
Delivered By:.
Comments:_
-z _ b W LAccepted: r/ Rejected: Resample Requested:
Received By. �� 11, c <r ;� - :_ `- -- C, Date: =) `T(Ll: Time: i q �' ?
4 TURNAROUND:

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Oral. Wilmington, NC 28405 • 910.392.1)223 Lab • 910.392.4424 Far
710 Bowscrtown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.58 43 Lab/Fax
n1fo rf em•ironnlen talchemtsts.com
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Lab ID
20-00344
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
1/6/2020 10:50 AM
Matrix
Solid/Sludge
Results
Sampled by
Lisa Cottle
Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dtchloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 846 Method 8081/3/3510
SW 846 Method 80818/3510
SW 846 Method 80816/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 80816/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
<0.02 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0 0005 mg/L
<0.05 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.250 mg/L
<0.050 mg/L
<0.003 mg/L
<0.003 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
01/10/2020
01/10/2020
01/10/2020
01/10/2020
01/10/2020
01/10/2020
01/10/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/08/2020
01/09/2020
01/09/2020
01/09/2020
01/09/2020
01/09/2020
01/09/2020
Report # 2020-0C160 Page 1 of 4

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
7 1013owsertown Road, Manteo, NC 27954 • 252.473.57(12 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info'u em ironmcntalchemists.com
Branch Residuals/Bob Branch
Attention
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide EPA 335 4
Reporting limit elevated due to matrix interference
Sulfide
Ignitability
Sludge Residuals
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SM 4500 S D
SW 846 method 1010
Aluminum EPA 200 7
Arsenic EPA 200.7
Cadmium EPA 200 7
Calcium EPA 200 7
Chromium EPA 200 7
Copper EPA 200 7
Lead EPA 200 7
Magnesium EPA 200 7
Molybdenum EPA 200 7
Nickel EPA 200 7
Potassium EPA 200 7
Selenium EPA 200 7
Sodium EPA2007
Zinc EPA 200 7
Nitrate+Nitrite-Nitrogen EPA 353 2
Total Solids (%) SM 2540 B
pH SM 4500 H B
Ammonia Nitrogen SM 4500 NH3 C
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
0.06 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.01 mg/L 01/09/2020
<0.125 mg/kg 01/08/2020
0.32 mg/kg 01/10/2020
>205 °F 01/10/2020
13400 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
28000 mg/kg 01/07/2020
32.5 mg/kg 01/07/2020
989 mg/kg 01/07/2020
64.9 mg/kg 01/07/2020
3390 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
22.1 mg/kg 01/07/2020
4600 mg/kg 01/07/2020
<11.7 mg/kg 01/07/2020
6550 mg/kg 01/13/2020
1400 mg/kg 01/07/2020
3050 mg/kg 01/13/2020
1.74 % 01/06/2020
5.92units 01/20/2020
<5.75 mg/kg 01/08/2020
Report # 2020-00160
Page 2 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Wad, Wilmington, NC 28405 • 91.0.392.0223 Lab • 910.392.-1424 Fa\
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fat
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fay
inlur'(i em rronmentalchcmists.com
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 Org B
SM 4500 P F
S W 646 7471B
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 245 1
35000 mg/kg 01/08/2020
24400 mg/kg 01/10/2020
1.97 mg/kg 01/17/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<0.0002 mg/L 01/20/2020
Lab ID
20-00346
Sample ID:
Site: 001
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.91% 01/06/2020
<943 MPN/g 01/06/2020
Lab ID
20-00348
Sample ID:
Site: 002
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.57 % 01/06/2020
<1147 MPN/g 01/06/2020
Lab ID
20-00349
Test
Sample ID:
Site: 003
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.91 % 01/06/2020
<943 MPN/g 01/06/2020
Report # 2020-00160
Page 3 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway; Jackson ille, NC 28540 • 910.347.5843 Lab/Fat
mfour environmentalchemists.cum
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Lab ID
20-00350
Test
Sample ID:
Site: 004
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.86 % 01/06/2020
<968 MPN/g 01/06/2020
Lab ID
20-00351
Test
Sample ID:
Site: 005
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.81 % 01/06/2020
<995 MPN/g 01/06/2020
Lab ID
20-00352
Test
Sample ID:
Site: 006
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.83 % 01/06/2020
<984 MPN/g 01/06/2020
Lab ID
20-00353
Sample ID:
Site: 007
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.61 % 01/06/2020
<1119MPN/g 01/06/2020
Comment: Sludge residuals reported on a dry weight basis.
Reviewed by:
Report # 2020-00160 Page 4 of 4

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification 494 NHCDHHS: DLS certification #37729
Collection and Chain of Custody
G&02 Windmill Way, Wilmington, NC 25405
Office: 91(1-392-0773 Fax: [phone]
[e-mail]
Client: Branch Residuals Bob Branch
Address: CC: Town of Wallace
Project name: WWTP LTMP-sludge samples
Contact name:
Report No:
PO No:-
Sampled bv. Y-1a i�O 4 k Rta lc h G- zz e 11
collection
Sample Identification
Sludge -(Quarterly)
1. sludge
2. sludge
3. sludge
4. sludge
5. sludge
6. sludge
7 sludge
date
time
temp
Report To: Lisa Cottle, ORC
Copy to:Brent Dean, [e-mail]
n
n
E
4)
%./� G ryl
Phone/Fax: Lisa 910-285-5927
Email: [e-mail]
SAMPLE TYPE: 1= Influent, E= Effluent, W=Well, ST= stream, SO= Soil, SL=Sludge, Other:
c
0
u c
v
o
7
ro
Preservation
0
Z
u
0
sri
O
z
2
x
0
Z
cc
x
1—
O
Analysis required
10 : 5D
G
G
P
X
X
nutrients/metals
full TCI.P
RCI
Fecal Density,% TS
P
P
X
X
Fecal Density,% TS
Fecal Density,%TS
G
P
P
G
G
P
P
3� I
X
X
Fecal Density,% TS
Fecal Density,%TS
X
X
Fecal Density,% TS
Fecal Density,% TS
Up/down stream samples: 3/week June 1- Sept 30; 1/week Octoberl- May 31
Transfer
1
2
temp when received:
delivered By
Date/time
Relinq, ished By:
} t
,.� Accepted: Rejected:
Received by:
1 -G-2o / I 0
Cronic toxicity due in Jan, Apr,Jul Oct
Received�pyE
Resample:
date/time
Comments.
Date/time
turnaround:
-7t,�

ANALYTICAL & CONSULTING CHEMISTS
t;b02 tvinurnnill Way, i';iiminglon, NC 28405 ° 910.392.0223 Lab ' 910.392.1424. Fa:•.
710 Bowsertown Rood, Manteo, NC 27954 ° 252 47 35702 Lab/ Fa
255-A Wilmirlgion Highway, Jacksonville, NC 2:y540 910.347.5843 Lab; i-a:.
rotor em9ronmentalchemists.corn
Town of Warsaw
P.O. Box 464
Warsaw NC 28398
Attention: Greg Hughes
Date of Report: Jun 02. 2020
Customer PO #:
Customer ID: 09070029
Report #: 2020-07645
Project ID: Sludge .
Lab ID
20-18819
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
5/7/2020 8:00 AM
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychior (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 846 Method 8081/3/3510
SW 846 Method 80818/3510
SW 846 Method 5081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 80818/3510
SW 646 Method 80818/3510
SW 846 Method 8081 B/3510
SW 846 method 5270/3510
SW 846 method 8270135'10
SW 846 method 8270/3510
SW 846 method 827013510
SW 646 rrathod 8270/3510
SW 846 method 827013510
SW 846 method 8270/3510
SW 845 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 646 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
5W646 Method 8151A
SW846 Method 8260/5030
SW846 Methcd 8260/5030
SW846 Methcd 8260/5030
SW846 Melhed 8260/5030
Matrix Sampled by
Solid/Sludge Greg Hughes
Results Date Analyzed
<0.02 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.0005 mg/L 05/18/2020
<0.05 mg/L 05/18/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.250 mg/L 05/14/2020
<0.050 mg/L 05/14/2020
<0.003 mg/L 05/19/2020
<0.003 mg/L 05/19/2020
<0.01 mg/L 05/13/2020
<0 01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
<0.01 mg/L 05/13/2020
Repo:: 2020-07645

.6 . 6 _ 0 ..
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ° 910.392.4424 Fa-,
710'3owsertown Road, Mantco, NC 27954 252.473.5702 Lab/Fay:
255-,\ l Alrnington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ a •.
ANALYTICAL & CONSULTING CHEMISTS info(r rerviro7ment xlcnemr,r;x„m
Town of Warsaw
P.O. Box 464
Warsaw
NC 28398
Attention: Greg Hughes
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 09070029
Report #: 2020-07645
Project ID: Sludge
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide
Sulfide
Ignitability
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8250/5030
SW846 Method 8260/5030
EPA 335.4
SM 4500 S D
SW 646 method 1010
SW 846 Method 9045D
EPA 200.7
EPA 203.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 NH3 C
Total Kjeldahl Nitrogen (TKN) SM 4500 erg 8
<0.01 mg/L
<0.01 mg/L
<0.05 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
05/13/2020
05/13/2020
05/13/2020
05/13/2020
05/13/2020
05/13/2020
0.142 mg/kg 05/12/2020
0.73 mg/kg 05/11/2020
>185 °F 05/21/2020
6.56 units 05/13/2020
8550 mg/kg 05/13/2020
30.1 mg/kg 05/13/2020
<14.9 mg/kg 05/13/2020
21800 mg/kg 05/13/2020
21.2 mg/kg 05/13/2020
258 mg/kg 05/13/2020
26.8 mg/kg 05/13/2020
1470 mg/kg 05/13/2020
17.3 mg/kg 05/13/2020
<14.9 mg/kg 05/13/2020
2940 mg/kg 05/21/2020
<14.9 mg/kg 05/13/2020
1490 mg/kg 05/13/2020
748 mg/kg 05/13/2020
1910 mg/kg 05/13/2020
3.30 % 05/12/2020
<3.03 mg/ kg 05/08/2020
39700 mg/kg 05/08/2020

Ai 1A1 Y ; ti;:,1_ F; corli:U; 1 i?1i;i CH NI1S i S
Town of Warsaw
P.O. Box 484
Warsaw
NC 28398
Attention Greg Hughes
Environmental Chemists, Inc.
GGra'_ y`:ili i a1i .. �` tl', .: `c4 1 ; . :LJ_ i+? 0;2.3 1 d4i �' E 1 ::
10 1i;ttti_ !'r 'rs's Rt'a, :l t ,i i �.it r ) a ?:)_1":i �ii%_ l.Qi./Fe
(-1.4 ' :I'. J i:Gsur..'i3:..." lii! ,.1.-��,1:
1.11.1,14� Li'ii',itiN•1, 11:; i.'l;i'G;.o,..:42i1
Date of Report: Jun 02, 2020
Customer PO #:
Customer ID: 09070029
Report #: 2020-07645
Protect ID: Sludge
Total Phosphorus SM 4500 P F 16500 mg/kg 05/13/2020
Mercury SN1846 7471E 0.8450 mg/kg 05/19/2020
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L. 05/14/2020
Barium EPA 200 : <1.0 mg/L 05/14/2020
Cadmium EPA 2cO' <1.0 mg/L 05/14/2020
Chromium EPA 200 ' <1.0 rng/l. 05/14/2020
Lead EPA ?CO 7 «1.0 rng/! 05/14/2020
Selenium
EPA 200 7 <t.0mg,•'l. 05.11=1r2020
Silver CPA 2f.O ; <1.0 rrlq/L 05/ 14/2020
Mercury '= _ ti 245 •• <0.0002 mg/L 05/19/2020
________.._ _ .. _ _
Comment' Sludge retsldual reSultS repafted on a dry weight basis
Reviewed by: ;;" t t `'j - ;y
2r2,1-07e.:4

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Beulaville, Town of Clayton, Town of Kenansville, Town of Warsaw, and Southwest
Plantation meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection or incorporation.
The forms for these facilities are marked appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town ofBeulaville WWTP
Monitoring Period: From 1/1/2020
WQ Permit Number: WQ0030998
NPDES Number: NC0026018
To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed•
Class A:
Alt. A (time/temp) ■
Alt B (Alk Treatment) Ll
Alt, C (Prior Testin) U
..... . .... ::
Alt.D (No Prior Test) 0
Process to Further Reduce Pathogengs U
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ■
Heat Drying Cl
Heat Treatment ,.-1
Thenuophilic U
::::::::::;
Beta Ray •
Gamma Ray
•
Pasteurization ; .I
Class B: 'Alt (1) Fecal Density ❑
Alt. (2) Process to Significantly
Reduce Pathogens C7
..
If applicable to alternative performed
(Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
v
Air Drying
•
Composting Ll I_Aerobic
Digestion •
Anaerobic Digestion
•
.'::.-. .
•
If applicable to alternativeperformed (Class A or Class B) complete the followin
monitor'ng data:
Parameter
Allowable Level
in Sludge
Pathogen DensityFrequency
Number 0
Excee-
dences
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2x 10tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
conform)
3 MPN per 4 grams
total solid (dry
weight)
r Attraction Reduction (15A NCAC 02T .1107) - Please indicate a
Alt.1 (VS reduction)
ER
•
Alt. 2 (40-day bench) •
Alt. 3 (30-day bench)
❑
Alt. 4 (Spec. 02 uptake)
I ,
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable)
0
Alt. 8 (Drying - Unstable)
i
Alt. 9 (Injection)
row.
El
Alt. 10 (Incorporation) •
No vector attraction reduction alternatives were performed
0
FICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Stanley Miller, WWTP ORC
Preparer Name end Title (type or print)
Signatureeparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
r1PNR r=r1RriA pkir= n79- till',nnn%

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Clayton Little Creek WRF
tiVQ Permit Number: WQ0030998
NPDES Number: NC0025453
Monitoring Period: From 1 1 2020 To 12/31/2020
1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) •
Alt B (Alk Treatment) ■
Alt. C (Prior Testing) 0
AMID (No Prior Test) •
Process to Further Reduce Pathogengs 0
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ■
Heat Drying •
Heat Treatment 0
Thertnophilic 1-1
Beta Ray •
Gamma Ray 0
Pasteurization ■
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens v.
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization v
Air Drying
•
Composting
•
Aerobic Dige,tion
•
Anaerobic Digestion • (
If applicable to alternative performed
(Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dence,
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nione
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
conform)
3 MPN per 4 grams
total solid (dry
weight)
- Please indicate alternative performed:
Alt. 1 (VS reduction)
l...l
Alt. 2 (40-day bench) ill
Alt. 3 (30-day bench) 1J
Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic)
0
Alt. 6 (Alk. Stabilization's
Alt 7 (Drying - Stable) ..
Alt. 8 (Drying - Unstable)
F.'
Alt. 9 (Injection)
0
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
i7
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
0 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. James O. Warren, WRF ORC
Preparer Name and Title (type or print)
S/igt lure of Preparer*
*Preparer is defined in 40 CFR Part 503.9(r)
Land Applier Name and Title (if applicable)(type or print)
Date PP
Signature of Land Applier (if applicable) Date
$
and 15A NCAC 2'T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Kenansville WWTP
Monitoring Period: From 1/1/2020
WQ Permit Number: WQ0030998
NPDES Number: NC0036668
To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ■
r Alt B (Ask Treatment) ■ '
Alt. C (Prior Testing) U
Alt.D (No Prior Test) 0 (
Process to Further Reduce Pathogens
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Drying •
Heat Treatment 0
Therinophilic U
f
Beta Ra •
Gamma Ra
■
Pasteurization ■
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly
Reduce Pathogens n
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
o
Air Drying
•
Composting 0 'Aerobic
Digestion u
Anaerobic Digestion 0
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
in (Minimum
Pathogen Density
Number of
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niauA
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to theMP
6th power
per grans of
total solids
CRT
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wcight)
ector Attraction Reduction (1SA NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench) D
Alt. 3 (30-day bench) •
Alt. 4 (Spec. O: uptake)
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Ask. StabilizationCl
Alt 7 (Drying - Stable) D
Alt. 8 (Drying - Unstable)
0
Alt. 9 (Injection)
t-D
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed
U
El
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
CATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement In 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Garry Benson, WWTP ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature oTPreparer*
a-a4-a
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

d Title (type or print)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Southwest Plantation WWTP
Monitoring Period: From 1°'1,2020
WQ Permit Number: WQ0030998
NPDES Number: W00029601
To 12 31 2020
eduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tune/temp) 0 I Alt B (Alk Treatment) 0 I
Alt. C (Prior Testing)
A1t.D (No Prior Test) 0 I
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying •
Heat Treatment 0
Thermoplulic I
Beta Ray •
Gamma Ray •
Pasteurization 0
Class B:
Alt. (1) Fecal Density 0
Alt (2) Process to Sigitfican ly Reduce Pathogens ." I.
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization v
Air Drying 0 I Composting • 'Aerobic Digestion 0
Anaerobic Digestion •
1
If applicable to alternative performed (('lass A or Class B) complete the following monitoring data:
Parameter
Allowable Le%el
in Sludge
g
Pathogen Density
lVulnber Or
Excee-
gre
drnr«
Frequency
y
ofAnal AnalysisTypenin
Sample
Analytical
Tech -
e
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2x10tothe
6th power
per gram of
total solids
MPv
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Attraction Reduction (15A NCAC 02T .1107) - Please iadicnte niternntive performe l:
Alt.1 (VS reduction)
0
Alt. 2 (40-day bench) •
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. O: uptake)
0
Alt. 5 (14-Day Aerobic)
0
Alt. 6 (Alk. Stabilization0
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
J
Alt. 10 (Incorporation) La
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vectomttaction' retlatrtlon-requlremvtttln-15A-NC'AC 021'71107 havrbeenmeeL
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Sonn Scozzari, WWTP ORC
Preparer
Land Applier Name and Title (if applicable)(type or print)
• Z ZIA I
Signa ire of Preparer* Date Signature of Land Applier (if applicable) Date
*P eparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 1/1/2020 To 3/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ElI
Alt B (Alk Treatment) • I Alt. C (Prior Testin g) 0
'
r---
•
Alt.D (No Prior Test) ■ 1 Process to Further Reduce Pathogengs Li
_ - . - , . ,
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Heat Drying ❑
Heat Treatment Q
Thennophilic f.3
Compost ■
Beta Ray 0
Gamma Ray 0
__ Pasteurization 0
.. •
Class B:
Alt. (1) Fecal Density C]
Alt. (2) Process to Significantly Reduce Patho ens s 0 '
If applicable to alternative performed (Class B onlr) indicate "Process to Significantly Reduce
Pathogens":
Lime Stabilization • I Air Dryin$ Ill T
ComestinF ❑
Aerobic Digestion LI
Anaerobic Digestion © i
...
if applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen
Density
nber of Number
` c
Frequency
ofAnalysis
Sample
Type
,�rtaiytieai
nZ,
lvlinimun,Geo.
Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
943
1,011
1,147
MPN/
Gram
0
Quarterly
Grab
SM E 1 C
M
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
conform)
3 MPN per4 grams
total solid (dry
weight)
Veetnr Attraction
Reduction
(15A
NCACb2T
.1107) - Please indicate alternative pe or d:
Alt.1(VS reduction) 0 it. 2 (40-day bench) ❑
Alt. 5 (14-Day Aerobic) ❑ )Alt. 6 (Alk. Stabilization❑
Alt. 3 (30-day bench) ❑
Alt 7 (Drying - Stable) 0
Alt. 4 (Spec. 02 uptake) ❑
Alt. 8 (Drying - Unstable) E,1
No vector attraction reduction alternatives were performed E3
Alt. 9 (Injection) C] lAlt. 10 (incorporation) 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
u
Ms. Lisa Cottle, WWTP ORC
Prcparer Name and Title (type or print)
LI1 L. LP
Signature of Preparer*
Mr. Eric R. Smith, Land Applier ORC
Land Applier Nameind Title (if applicable)(type or
20V,
ate Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
rint)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 4/1/2020 To 6/30/2020
06) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 5 I
Alt B (Alk Treatment) 0 1
Alt. C (Prior Testing) 01 •
Alt.D (No Prior Test) • I Process to Further Reduce Pathogengs
. . . . .. . .....0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ■
Heat Drying ❑
Heat Treatment 0
?hemophilic iJ I
•
Beta Ray 0
Gamma Raj 0
Pasteurization ■
F Class B;
Alt. (1) Fecal Density a
Alt. (2) Process to Sieui.ficantly Reduce Pathogens 0 f '
If applicable to alternative performed ipass B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying as
Composting b „Aerobic.Digestion
U
Anaerobic Dilation 0 I ' .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Allowable Level
Pathogen
Density
nmmerr of
u
Frequency
Sample
Anel}mcal
Th-
Parameter
in Sludge
Minimum
Geo. Mean
Maximum
Units
' maExcep,
of Analysis
Type
nea e
—2
x 10 to the
6th power
MPN
28,418
57,356
339,484
MPN/
Gram
0
Quarterly
Grab
SM 9221 C
E
Fecal Coliform
per gram of
total solids
CFU
_
_
r _
1000 mpn per gram
of total solid (dry
wei rht)
.
Salmonella bacteria
(in lieu of fecal
3 MPN per 4 grams
total solid (dry
weight)
r coiiform)
Vector Attraction
Alt I (VS reduction)
Alt. 5 (14-Day Aerobic)
Alt. 9 (Injection)
Reduction
•
■
l)
(15A
Alt. 2
Alt. 6
Alt. 10
NCAC
(40-day bench)
(Alk. StabilizationO
(Incorporation)
b2T .1107)
0
Cl
- iindicate
Alt. 3 (30-day
Alt 7 (Drying
No vector
alternative
bench)
- Stable)
attraction
0 _
0
reduction alternatives
performed:
Alt. 4 (Spec. 02 uptake) El
Alt. 8 (Drying - Unstable) 0
were performed ■
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 1SA NCAC 02T .1107 have not been met." (Please note
if you cheek this statement attach an explanation why you have not met one or both of the
ll
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC
Preparer Name and Title (type or print)
Signature Gof Preparer*
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name and Title (if applicable)(type orrprint)
20 z l �-c�c. _
(2- ... J/Y7
ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP
NPDES Number: NC0003450
Monitoring Period: From 7/1/2020 To 9/30/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tetnp) ❑ ]
Alt B (Alk Treatment) C] I
Alt. C (Prior Testing) U
.
•
Alt.D (No Prior Test) 0 I
Process to Further Reduce Pathogengs L)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying U
Heat Treatment • '
Thertnophilic U
Beta Ray 0
Gamma Ray
is
Pasteurization 0
Class B:
Alt. (1) Fecal Density ZJ
Alt. (2) Process to Significantly Reduce Pathogeni:3
If applicable to alternative performed (Class B only) indkate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑
Composting •
[Aerobic Digestion 0
Anaerobic Digestion 0
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in SludgeMinimum
Pathogen DensityFrequency
Number of
Excess
d��s
of Analysis
Sample
Type
Anafytleal
Tech-
ninuc
S1vt 9221
C E
Geo, Mcar�Maximum
Units
Fecal Coliform
2 x to w the
6th power
per gram of
total solids
MPN
412
787
1,009
MIN/0
gram
Quarterly
Grab
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weft)
uction (15A NCAC 02T .11 - Please indicate alternative performed:
Alt1 (VS reduction) 0
Alt. 2 (40-day bench) 0
Alt 3 (30-day bench) $ `Alt.
4 (Spec. 02 uptake) U
Alt. 5 (14-Day Aerobic) 0
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) 0
Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) El
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement hi 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you cheek this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Prep Name and Title (type or print)
Signature of Preparers`
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name an Title (if applicable)(type or print)
z
ate Signature of Land Applier (if applicable) Da e
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Monitoring Period: From 10/1/2020 To
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: I Alt. A (time/temp) C] Alt B (Alk Treatment) 0 Alt. C (Prior Testing) 0
AID o Prior Test 0
� ) I Process to Further Reduce Psthogengs L:,1
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
,�st ❑ -
Beta Ray 0 f
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ0030998
WWTP Name: Town of Wallace WWTP N00003450
Heat Drying O Heat Treatment O
Gamma Ray 0 Pasteurization
Fecal Density p Alt. Process to Si ificEut
•Lime Stabilization ❑ {
Anaerobic Digestion 0
Class B: Alt, (1)
(2)gt tlx Reduce Pathogens D
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Air Drying 0 I Composting 0 IAerobic Digestion. 0
Thermophilic i_.l
If applicable to alternative performed (Class A or Glass B) complete the following monitorin =; data:
Number of
L•xcee-
drne-rs
Parameter
Fecal Coliform
Salmonella bacteria
(in lieu of fecal
califorml
Allowable Level Pathogen Density
in Sludge Minimum Geo. Mean Maximum Units
2x10totlbe
6th power
per gram of
total solids
1000 mpn per gram
of total solid (dry
wcishti
MPN
CPU
3 INPN per 4 grmns
total solid (dry
weight)
665
832
973
MPN/
Gram
0
Frequency
of Analysis
r
Quarterly
Vector Attraction Reduction (1afA NCAC OIT .1107) - please in cute alternative rformed
Alt.1 (VS reduction)
0
Alt. 5 (14-Darr Aerobic) 0
Alt. 9 (injection) O
e
0 Alt. 4 (Spec. 02 uptake) 0
Alt 7 (Drying - Stable) 0 Alt. 8 (Drying - Unstable) 0
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements hi 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check thls statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Sample
Type
Grab
AnaiyncliT
Tech-
nin
SM 9221
CE
0
WQ Permit Number:
NPDES Number:
12/31/2020
Alt. 2 (40-day bench) ❑ '
Alt. 6 (Alk Stabilization❑
_Alt. 10 (incorporation) l7
Ms. Lisa Cottle, WWTP ORC
PreparerJame and Title (type or print)
n;
Signature of Preparer*
tli
Alt. 3 (30-day bench)
Mr. Eric R. Smith, Land Applier ORC
Land Applier Nmoz anil Title e (if� plicable)(type or print)
1 ate Signature of Land Applier (if applicable) a
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Warsaw WWTP
Monitoring Period: From 1 /1 /2020
WQ Permit Number: WQ0030998
NPDES Number: WQ0021903
To 12131/2020
Pathogen Redaction (15A NCAC 02T .1106) - Please indicate level achieved and alternative perfo
Class A:
Alt. A (time/temp) 0 I
Alt B (Alk Treatment) • I
Alt. C (Prior Testing) J
Alt.D (No Prior Test) LJ
Process to Further Reduce Pathogcngs ■
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying Li
Heat Treatment •
Thermophilic ■
1
Beta Ray 1-sl
Gamma Ray 0
Pasteurization •
Class B: (Alt. (1) Fecal Density Ll I
Alt. (2) Process to Significantly Reduce Pathogens
v
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ci
Air Drying 0
Composting • 'Aerobic Digestion �.3
Anaerobic Digestion 0 I
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
deuces
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
nimie
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2x 10tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
ector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
■
Alt. 2 (40-day bench) •
Alt. 3 (30-day bench) ■
Alt. 4 (Spec. 02 uptake)
0
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. StabilizationC1
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
LJ
Alt. 9 (Injection)
1-1
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed
L 1
TATEMENT (please check the appropriate statement)
tJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
L I "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Greg Hughes, WWTP ORC
arer Ne and Title (type or print)
w 21/z1
Sign ture f Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Land Applier Name and Title (if applicable)(type or print)
hFA1R PrIR&A DVRC n T tilmnru t

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Beulaville, Town of Clayton, Town of Kenansville, Town of Warsaw, and Southwest
Plantation meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection or incorporation.
Documentation of these activities are found in the following section.

Facility Name Town offeulaville
Triple SFarn s WQ0030998
Line Stabilization Documentation
Month
4k,. c it ,: z
D
Date
T
Tla.
App+Wmate
CmYmnr
time
/Adaged
Prior to Lime Addition
>12 pH
2 Hours After >12 pH
24 Hears After >12 pH
Outgo)
Temp
T
pll
s.art
Tani
Carr
Time
1111
o.
T
Tema
pH
wan
Tomo.
Car
Mae
— pH
...mud
QA
amnion,
Tamp
—
pH
wage
Tray.
Cu?
-
'rate
- pH
ooruW
— IPA
Sordoni
Temp
pH
watt
T.
Carr
Tyre
pH
congeal
17A
nods.+
Hauled
3
0
1
1B.xa0
.1
1r5
y,7)
'242
9.c 6
44
%/.0
'2 f!
o 42,
10;15
/�;e:7
12.00
jet ,5'/.1r4
d
et -!Z
41, / '
12,Di
12.00
/75/Pkt
=,raj
/b.AO
//43
n.so
i--3-016
tlAtikk
Signature of Operator
• EPA 40 CFR Part 503 for Iime stabilization requites lute muted with sewage sludge to have a pH of 12 or greater after 2 hours and maintain a pH of 11.5 for the following 22 bans.
pH umol = actual pH values that have not beat temperature corrected
pH eeneied m pH values have ban temperature corrected
Aft temperature units are in Celsius.
=
It
Imo u
ti
h
a
O •
C11
M
C
.O
C0)
O
-
Ce
M
G`
O
M
O
CV
O
CV
G
C
00
O
- -
Wt
r-
C
Cr
O
\p
O
O
M
0
C
o
0
O
rn
0
9
t
\O
0
9
t
O.
0.
a
t
I'ot
9
t
.--+
6
r
0
i
N
0
t
N
0
t
N
N
6
e
O
M
O
t
M
C
t
M
C
m
M
O
t
N
't
O
r
`t
C
t
IJ
E
m
H
-4
M
M
M
M
in
It
e
en
en
en
en
M
N
N
(f`d
N
! 251
N
e.4
N
tV
e`a
-.
oo
...
-
.M-4
,--4
O

Facility Name Town of Beulaville
Yma 1 Ate' Uve
Prior to Lime Addition
Triple SFarms WQ0038998
Lime Stabilization Documentation
>12p8
21Hair Afiler >t2 p11
Month
24 Hours After >12
DaMa
Dane
Non
GMiwr
Added
Temp
nraru
Garr
Time
a eon
Temp
r•.
•Wy.
Carr
psi
.rrea.a
IPA
uww
harp
pas
saw
'HIM.
Car
abe
pH.-
avenge
---IVw
m.rwa
—
Ybnp
pH
Mud
'Hop
Leer
pH
c+/n w
EPA
ae.aeti
Harried
Si) t
1
ieboo
"3t#o-
//: j
/
,3,54
✓..).7
/6: ft
C
3L5
/ 5
L'•
£Zr.'S
-c r8
q'ne�e
i w i40•%
ad-1
12.00
.10
/ze�'
' i)41
JS
/` 1N
12.00
/ e
i zJS
1
1HON
41-5 )
1 I
11.50
S %� Xi
/,
Signature of 944;-
Operator
EPA 40 CFR Part S03 for lime stabilization requires Time mixed with sewage sludge to have a pH of 12 or greater alter 2 hows and marntain a pH of 11.5 for the following 22 hours.
pH semi = actual pH values that have not been temperature corrected
pH aann.d a pH values have been temperature corrected.
AO temperance units am in Celsius.
ICorrectlonl
Factor
./'r
N'
O
N
Nr
C
O.1
on
O
10
M
O
re)
on
a
O
M
6
t —
N
6
d'
N
6
•—r
N
6
00
•--u
6
•rl
.—,
6
N
......
6
IT
p
O
\0
O
d
0.03
•
, O
O
o
en
C
6
11.1111111.111.1
l0
O
6
O\
C
6
N
•. -,
6
In
•—a
6
00
r-a
6
..r
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6
ct
t41
6
t�
N
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on
6
M
M
6
'.O
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7"
6
ar'1
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Ga
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on
1`
on
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on
arty
on
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on
M
M
tit
on
—.
on
O
on
ON
N
00
N
t+
N
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N
an
IN
N
M
N
N
N
—+
N
CO
CV
Chl�
•—u
Is i
co
--1
"
•-+
,1-
..r
en
.—a
N
,...1.—u
11
O

TripleS Fanws WQ0030998
Lime Stabilization Documentation
Fealty Name Town ofBeulaville
Month fC 1a4e< atokli
Doe
Murk
Na
Apperdiame
Gilirur
Lim
Mid
Prior to Lime Addition
> 12 pH
2 Hours After Az pH
24 Hears After>12 eH
Date(s)
Ta.p
pH
.a.i
—Taw
(kn
Thar
PH
mnrr.1
Tmp
pH
r.W
Tina.
Car
Taws
01
.miners
era
magma
Tamp
pH
'dal
Tarp.
Carr
71re
PH
m
a.we
vA
mM
Temp
pH
.art
Tem.
Corr
Mow
pH
MUM'
[PA
stall
Hauled
9-iqtd
/
7D,Ce'�
24'
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• EPA 90 CFR Part 503 for lime stabilisation requires lime mixed with sewage sludge to have a pH of' 12 or greater alter 2 hours and maintain a pH of 11.5 for the following 22 hours.
pH mew a actual pH values that have not been temperature corrected.
pH ...wee a pH values have beau temperature corrected.
All temperature units are in Celsius.
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Sludge Stal(ilizaiiorn itceord
own cif Clayton
tittle i:n ecl. \V iter fterliirilintion F:n;'ililt
L) * : �:.':C:% Lr:,cittion: j o/d '?.%-T'4#i1 #1
\'otunii: 1 rented: �t;! ,I`•/?/i tll;i�ii l:st•d:_C CO3
Volume Used: _T_pj. 50 L6s•
liiitlfil
.-Ater Addition
12.O0 alter temp.
i`o.rreetiou i
Two I-1rS, After Addition
s> == 12.00 ti ftcr temp.
correction )
lime Gait` p11 i Col-f-c.crionn_.I_ I.in;nl r Ienrli.
r
1,S `?SL -�h/' t, 4? .,, ; .J -o, C!t_�.c—.-s' —--- i—
v ''
.,,, -cc -
'.L_; '0US
L:-
iz
y" z . 2 3
il,P +•t1.its
t 1Ii s_ after Addition
11.50 alter temp.
correction
Pi parer:
Date/ Tinsel C;uffei' 1 Readina
_.,I 5 i',e .J 32_ 3.5
Iris ..'ef r _SI0pi• ,: i '- .-7,-t4.
-''y' I.' tZr`
Fitt" Time 1 Buffer Readin`,
iC,
/ 2 , t••/ r G'•• U',i
Nly
-- / 77_`: ; 7
T-3
1nt: ' Sloe 4 ,�r ,�l,
•

Burnett Lime Company, Inc.
Y'7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
5
0
L
T
0
3.ytsr"t
H 11,.,13 . r t?i t
P
hi 4. ".5 5'Y[ ilk.+;l ._`�:..r;�;R :?7s�'; ..
T
0
CUSTOMER NO.
.r
. (Alias!.
BLC ORDER LOT NO.
<
SHIPP'ELX "--
•
w
4 1
PROTECT NO.
CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER.
DELIVERY TICKET NO.
�_:
- .ram .� ;:
4 4
SHIPMENT WEIGHTS
O
cC
C7
w
CC
BILL FREIGHT CHARGES TO:
❑ BURNETT LIME Et CONSIGNEE
SHIPPED VIA TERMS
DESCRIPTION
1 Tanker CAL' FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE
CUSTOMER SIGNATURE
FT
r,
ClAL-�-FLQ
S Y S r E H S L U R R Y
�Ay+M
•a "'xi'
CAL -PLO' slurry
Drinking Water Treatment Additive
Tested in accordance with
Standard ANSI/NSF60
Calcium Hydroxide
650 mg/L Maximum Use Level
DRIVER NAME
TANKER NO.

Sludge Stabilization Re:-.(tict
o))n of Cla) ton
idle Cre.e1-. kVatei Reclamation Focilit)
Date: it-/ 2/.:94) 1:ocation:_/-/a_b1/,,, 14 ,,,,k .7 ' i j
I oix
1" otumv Ili iti...0: 3 (ISO°c) ,91.5. Alkali 1..cd: C 157CG) 3
. .. _.
V olume II sert...5).171.110 ZA65.
i litK7 Tillie I Dr-
ak I pH Correction 1 . Final
1 Facto' i
T emp.
1 ,
Initial
After Addition
12.00 after temp.
correction )
-1%5 Ci11 rs. After Addition
V- 12.00 after temp.
correction )
24 firs. after Addition
(>--- 11.5( after temp.
correction )
7-
as 2.c)
Li-/ /
I.2
12.
(f-/g/.0,16
/2.
J/ Li'
, pH
25-2./. if. 3.4.
3? I 3•9' ek.03:-. • 7' 73 21j*
11,5* -21 br-
.1148!3•9 k .03 IA- 303 Z. 2-
= .2;
5*-2.3.,rx
35 / -r I 2... j.gs.
1.33- 23.5'
--------
Time
Prep alvf :_pc,
Buffer
41/ w .2.0 7 . 0
! i
Reading___
7.OG
i1 -a .9 !
/a , o /
I a • 6 .A. 1- 32/.6
lnt: p./..n__ Slope --.371.3Er ??
Reading
1 2.00
I 1 / A vo- 1 r 2- • 5. 7
Int: DIA
TI)4inicoliBtif.foer
• a-
l-173.1
3204
Slope -Sg;
99

Burnett Lime Company, Inc.
O 7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S
0
L
D
0
ttu. . Count' n-
Qavt»-1. : �?_'•.''.i.
s Clayton WiTP
H Lithe avek VA
000 ti1iaiiY s1Tl%f t C
Claytotis ?T` ,5.}52O
T
0
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
56393
SHIPMENT WEIGHTS
GROSS
w
cc
PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER NO.
ORDERED
BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO.
SHIPPED
SHIPPED VIA
DESCRIPTION
1 Tanker CAL—FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE
SPECIAL INSTRUCTIONS
TERMS
CAL -~FLO
3 7 S T° N & SLURRY
�4'9 R'y� Drinking Water Treatment Additive
WQA _j Tested in accordance with
Standard ANSI/NSF60
6
/ Calcium Hydroxide
'oto� 50 mg/I. Maximum Use level
DRIVER NAME TANKER ND.
VIN #
CUSTOMER SIGNATURE
Z
ill l`;TCl v'IFR COPY

Sludge Sia1•lilir:alion Record
Ion it of C•1.a` ttalr
1.it11;' t._rei 1, Water Rot. 1':arilrti
Date:
/
Volume L reined: i ed:
lime
Initial
after Addition
(' 12.00 after temp.
correction ) _ -
1 \Sff 1-1vs. After Addition
�- - 12.00 after temp.
correction )
Lution: _ '
�.Ilt:i li I, s d.
C r✓
y ♦1
Volumei!c'c.1:-'�^'� T6,5td
1 into ' 11:11e I p
C.)
( or rectit.n Final
1 actor 1,fi
L• X•o3= .072 +7441-.
3 X • 03 =
E Temp.
�3/Zo 1125 /Z. oq
z cX
124 Hrs. alter Addition
( 11.50 after temp.
Correction )
12.39
017•111
17:72-
Z'zo
2 , 7 z i z. 3 3 1P 7
17'20 Z7• w
? /.
Date' Time i Buffer I Reading My
(t3/.c )-,/17 'l L,/ I. 'Lc / -Ca.1 I
:l /• /(.,t/ I io, L!r 1 ^lLZ. e I
1 1/ /
tnt:_i t.f: Slope._S %^ _
Date' Time Buffer I Reading
1nt: l.,;l �: ,Slope -570., Ll 1
m j

Burnett Lime Company, Inc
1 .'7095 Hwy 11, Campobello, SC 29322
5200 US Hwy 17 S, Bartow, FL 33830
0 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S
0
L
D
T
0
S
H
P
T
0
ainyto91Accounts Crovir
cl 55 jj
Attn: Psyat- '
P.O.-
- 3-v grgi
Clayton, i'' 27520
Clayton. 'WITI-'
Clvtlk
100Q ani greet t at
Clayton, : 27520
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
'57522
SHIPMENT WEIGHTS
to
tit
0
t7
x
W
cc
a O
C7
PROJECT NO.
BILL FREIGHT CHARGES TO:
❑ BURNETT LIME
CONSIGNEE
CUSTOMER NO.
C008
ORDERED' •
CAR Y
BLC ORDER LOT NO.
� l
CUSTOMER PURCHASE ORDER NO.
SHIPPED VIA
e
•
fir(+
1 0 (rt—
SHIPPED DESCRIPTION
1 Tanker CAL"FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
ANAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE b*.E.."
SPECIAL INSTRUCTIONS
� I
DRIVER NAME
r
I -
FT
TERMS
t 3i
CAL--=FLO
SYSTEM 5 SLURRY -�
R ?� SFq � CALILO• Slurry
7y�' ' Drinking Water Treatment Additive
(� WQ ht - Tested In accordance with
Standard ANSI/NSF60
Calcium Hydroxide
650 mg/L Maximum Use Level
TANKER NO.
x r
VIN #
1J i •
CUSTOMER SIGNATURE
w
z
nI In-reN.ar-rs ..

Date: �'yl Zo ZG3
Volume Treated: $.O(1, ()(L)
Tine
Sludge Stabilization Record
Town of Clay ton
tittle Creek 1Vater Reclamation Facility
Location: /lr`i t:`rr/ /
Alkali used: Ct / G' :3
olunte Used: `VC,/
rime / Date pll
Correction Final 1 Temp.
Factor
Initial
After Addition
(>= 12.0(1 after temp.
correction )
Two Hrs. After Addition
(>= 12.00 after temp.
correction )
24 lirs. after Addition
(>= 11.50 after temp.
correction )
pH
-
. I .z •5 j. r
`1 C:
/2. 6 E
12 s/
Prcparer:
4/, C= {` - I ,;)) / 7 57)
Date/Tine 1 Buffer 1 Reacting 11Iv
rr•C, I •Lt, !0c7.'7
Int: .PJ Slope • '� ;,
Date/ Time
• ic.
4)
Buffer j Reading J NI
l,_.. I i , c: f
-/vt.G
—3rit.i
Int: j:,%,3 Slope s

Burnett Lime
( 7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S
0
L
D
T
0
S
H
F
T
0
•
opanyg Inc.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
' Qa 4 f
SHIPMENT WEIGHTS
PROJECT NO
BILL FREIGHT CHARGES TO:
BURNETT LIME ri CONSIGNEE
CUSTOMER NO
:ORDERED ; ,
•
BLC ORDER LOT NO.
SHIPPE`[S
1
CUSTOMER PURCHASE ORDER NO.
Tanker CAL—FLO® Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
SHIPPED VIA
FT
TERMS
(CALEFLO.
5 Y 7 Y E M x S L U R R Y
C{�• CAL'ILCHI Murry
ttilDrinking Water Treatment Additive
r"` Tested In accordance with
Standard ANSI/NSF60
Calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE ` ark%'' 650 malt Maximum Use Level
VIN #
w
Z
CUSTOMER SIGNATURE

‘.H
I
t 1•1.1....i.1 Alt L
= T 305- /00
en -cos 630,'
. 9..4; ...C. 'o
I il!!. 1•11 ,4•
1
c1/23 b.') -
.7, 1 c) - I), / :5
---- -
9/e3/Zou'
9:0 / /2..56 --
9/z3/2.a20
/2.Cz — "9
/7.0 z
9/2y.
5-•12,4.7 7 12..3g 2 .2
1 it t! I WI
11
iL,94- Z3 °
/Z.L13 ZI•F
,
1):41t: nillt. ! 11111fet 1 ii(iiii', N I •
;-• . . : 7 4.");,-
i- -
le), o IF .__. _ ....11.0, 422' _' -16,f-' 27
1 e...},!rilr.
Daic, Ftme ; 1,411-1,x I Ntailiwz.
ft 9 7
. r6f
r I
1'Z . • Y I-1.
int: La14--

Burnett Lime Company, Inc.
7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 5, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S Clayton (Town L )
0 .'iith: aciionsit ia.`y':.11e
T
0
S
H
F'
0
(lay#oti, - 15-2. '
ti 1�Iff�7'i �4sx.1°
Little &eAlis. Mkt
1000 11.t at}I eet Lr 1
Clay-4-m, ; ',' 75?0
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
t, 8i 9 8 4
SHIPMENT WEIGHTS
Le)
0
w
cc
PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMERNO:
"-CIRDFRED
BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO.
SHIPPED VIA
SHIPPED `^ - DESCRIPTION
1 Tanker CAL—FLO° Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
Calcium
Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE °F%e�oE�� 650 mgjL Maximum Use Level
TERMS
i423t
LLi
b
GAL
SYSTEM & SLURRY
SPECIAL IN§TRUCTIONS
FT
CAL-FL0" Slurry
ti" r C:: Drinking Water Treatment Additive
/.�: Tested in accordance with
�'• WQA�� Standard ANSI/NSF60
DRIVER NAME
VIN #
w
Z
CUSTOMER SIGN TTtJRE

Pennitee: '�, ry?5
Land Application Permit No: j,J Q 00 3 qqg
ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Batch Size (gallons)
000
Lbs. of Lime t C`+
Date
Initial pH
>12 11
p
2 Hour pH
{
24 Hour pH
Operator
Initials
pH
Temp °C
Corr.
Factor+/
Corrected
pHTime
pHTemp
°C
Corr.
Faclor+/
Corrected
p11
Time
Temp °C
Corr.
Factor+/
Corrected
pH
pH
Temp °C
Corr.
Faclor+/
Factor
Corrected
pH
Time
ff.+-i
f.7W
��t,J
ii4
r7 G
S::3L`
Ij.`hat./-7.c1.
- .q�
j:.)ci•,s
"i:o-t-,
Roo
7�Tr �f
I'
~ ,2f
12,Ar1
tt•,/o
f, ,.6n
'ik.•4
Fa )
JrEt';S
9,16
%fi
,
Comments:
a
Csi
V
O
O
vs
O
M
Ci
w
Co.
w
O
a
a
d
a
Date ) ti •• )' -
w
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0
9
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0

Triple S I'urnrs tf Q01130993
Lime Stabilisation Documentation
Facility Name Southwest Plantation/ Bear "Frail
i02D
Dale
-
Tan,
No.
'Approeimare
Gallo.,
Lime
Added
Prior to Line Addition
>12 pll
2.11ourshfter>12
pll
24 flours After>12 p 1
niacin)
1louletl
Temp
pll _.
.tad
Temp.
Carr
lime
p11
eanaW
Temp
pl1
.tad
Temp.
Corr
Moe
pli
rerreaN
EPA
sawaimi
Temp
pll
u+.+t
Temp..
Carr
That
pll .
rwreared
rrA
Swd.nt
Temp
pH
woad
Temp.
Corr
Time
pfl
mmned
Wet
S>.eWard
1/
,j�
(Zr,a,
Y�r,�
1I<•�
.
�7
�?uU
�,9Y
f .)
j�,
i1 1/
-.2 1
n -
�_ (re
1E.Ly
lz.xtl
(..
! �(
i2. $2
-.2`i
j.fi�E
i[. 8
2
1_.MI
(i+•9
11.i.
. IS
t�
Crit>��i
it.tD
S
lto
11
3j5'
I
J ,pro
1156
IL.ti
1•J1.
-- 2(r
fR o
2 q
12.0
r3.141
3(o
f 2t5
/2:rr;
I�.LI
12.)
-,3L
ILj 15
iz.43
13.i
{1
'•314
1215
(1.41
/4
`ll`S
1
12,Loi)
':Sn
11•1
1.1`i
;zq
t)t,.. G
1'i5
1SLf
17,47
-.zt
£ ?)1
12. (
•
i'./
12,-IN
7.11
loll
12.0
ii•it,
11.A
`-p`1
t81 i
I\•t%'
V.zy
e;/Z `
i
112. Ga:.,
q5z.
a7,A
70
•fr6
o'Qo
1.53
1.4
13.03
. ;
CG 1 ,
13-D
)1.1
I2•'T'
•c'
1 115
t
I1•`io
-t'
o& 0
11-93
4.125
ra 2
JL5
1
t =t L47t7
�' SL'
my.a0
,
?•��
`rY
i?R 2.�
,ls I
g 1 L1
z.
! .`]�
' �
Ufs't
5.t�
3
r{
r'ir3
S2 �
3.
.1:3.b1
1
1 DI 1
0 .51,
i
?,,�}.t
{.i Y
•• ol%
F
%b1B
g
'jTs
Signaturc.oaVerator
• EPA 40 CFK Part 503 for link stabilization acquires lime mixed with sewage 51lulge to Itatie a oil of 12 or _Beater (r 2 hours and maintain a pi i oP 1 I far the tolle>in
Iol I a.wi - actual pl I values that have not Wen tcntperuure corrected.
pl l m-ntot = pl 1 values have been temperature corrected.
Alt temperature units are in Celsius.
2_ hour,
Correctkin
Factor
'n
^t
N
'1"
C".
en
ti:
en
t ri
e'':
0,30 1
t -
N
'1
N
—t
N
00
r,-1
N
—
^
M
Q^
^
rn
O
C.',
O
t
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tr-,
r
OG
—
N
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. •
N
e
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re:
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r
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c^.
r
ri
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t
er)
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E
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oN
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r';
t--
t'7
sso
r*:
in
en
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enre;
rn
N
r^n
r--
rr
O
re;
t7N
N
OG
N
C`-
N
r4
rr:
N
24
I 23
N
ele•-t
21
20
cA
00
t�
r-+
rrt
—
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^
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.--�
.--.
r-.

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Jan-20
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
pergram. =:..
Log
1
1/6/20
943
2.975
2
1/6/20
1,147
3.060
3
1/6/20
943
2.975
4
1/6/20
968
2.986
5
1/6/20
995
2.998
6
1/6/20
984
2.993
7
1/6/20
1,119
3.049
Most Probable Number / Gram
Total
Average
21034
3.005
1,011
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
61i02 Windmill \Vav, Wilmington, NC 28405 • 9111.392.11223 Lab • 910.392.4424 Fa;
710 Biw.v.;t.rt n Road, lan`.ei , NC 27934 • 252 473 5702 Labi Fay
255-.A 6Vilmington Highway, Jacksonville, NC 28540 • 910.347 5843 Lab/ Fa\
inluur en: ironnientaichenti,t,.cun1
Branch Residuals/Bob Branch
Attention:
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 Org B
SM 4500 P F
S W 846 7471 B
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 2007
EPA 200 7
EPA 245 1
35000 mg/kg 01/08/2020
24400 mg/kg 01/10/2020
1.97 mg/kg 01/17/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<1.0 mg/L 01/13/2020
<0.0002 mg/L 01/20/2020
Lab ID
20-00346
Test
Sample ID:
Site: 001
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
1.91 % 01/06/2020
<943 MPN/g 01/06/2020
Lab ID
20-00348
Sample ID:
Site: 002
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM92210EMPN 24hr503
1.57 % 01/06/2020
<1147 MPN/g 01/06/2020
Lab ID
20-00349
Test
Sample ID:
Site: 003
Method
Collect DatelTime Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 8
SM 9221C E MPN 24 hr 503
1.91 % 01/06/2020
<943 MPN/g 01/06/2020
Report # 2020-00160
Pace 3 of 4

Environmental Chemists, Inc.
f.-L2 V:3‘. Wilmington, \C 2S4t15 • 910.392 0223 i ah • g111.3 )2 4424 Fit
10 Bol,\ sertuwn Road, Manteo, NC 27g5-4 • 252 473.3702 Lab/Fa:
. 5 i k. ilmingtun Highway, Jackson \ il!e, \C 2S540 • L110 347.5S4.3 I_ab%RI\
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention:
1 L, em unnnlentalrhe1111SIs.Con1
Date of Report: Jan 28, 2020
Customer PO #:
Customer ID: 15060009
Report #: 2020-00160
Project ID: WWTP LTMP
Lab ID
20-00350
Test
Sample ID:
Site: 004
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10.50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.86 % 01/06/2020
<968 MPN/g 01/06/2020
Lab ID
20-00351
Test
Sample ID:
Site: 005
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10:50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.81% 01/06/2020
<995 MPN/g 01/06/2020
Lab ID
20-00352
Test
Sample ID:
Site: 006
Method
Collect Date/Time Matrix Sampled by
1/6/2020 10'50 AM Solid/Sludge Lisa Cottle
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.83% 01/06/2020
<984 MPN/g 01/06/2020
Lab ID
20-00353
Sample ID:
Site: 007
Collect Date/Time Matrix Sampled by
1/6/2020 10 50 AM Solid/Sludge Lisa Cottle
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.61 % 01/06/2020
<1119 MPN/g 01/06/2020
Comment: Sludge residuals reported on a dry weight basis.
Reviewed by:
P.eoor, t 202C-00150
Page 4of4

49 l
• 4 -4: -
Analytiiai & Consulting CIi ins is
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification tf94 NHCDHHS: DLS certification #37729
tod
6b02. Windmill Way, Wilmington, NC 2940S
Office' 910-392-0)21 I'ax• 910-392-4424
[e-mail]
•
Client. Branch Residuals Bob Branch
Project name: WWTP LTMP-sludge samples
Report No: •�1rt % • %,�),' j.i{. ,'
Address' CC: Town of Wallace
Contact name:
PO No:
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to:Brent Dean, [e-mail]
Email: [e-mail]
Sampled by: L •, CD Ole 1 k E zz ell
SAMPLE TYPE: 1= Influent, E= Eff uent, W=Well, ST= stream, S0= Soil, SL=Sludge, Other:
sq i
f collection
sample_ type
composite
or grab
container (P
or G)
Chlorine
mg/L
Lab ID
Number
Preservation
Analysis required
ai
z
=
0
_
M
O
=
1
Q
z
O
1-
W
2
p
Sample Identification
date
time
temp
G
P
�1
`1c!/-1
X
nutrients/metals
full TCIP
RCI
Sludge
J-(p 20a7
10 . �
-(Quarterly)
1. sludget
G
P
; Lr
if
X
Fecal Density,%TS
G
P
"-
L
X
Fecal Density,%TS
2. sludge
3. sludge
G
P
- cl
�
X
Fecal Density,%TS
G
P
,
•� tJ
X
Fecal Density,`/ TS
4.
sludge
5. sludge
G
P
•}r_i
X
Fecal Density,%'IS
G
P
•,
- > 2-
X
Fecal Density,/ TS
6. sludge
7. sludge
\✓'
G
P
2,
X
Fecal Density,% TS
__.
Up/down stream samples 3/week
June 1- Sept
30; 1/week Octoberl- May 31 Cronic toxicity due in Jan, Apr,Jul Oct
I
Relinq, ished By: ,
Date/time
Received y:
Date/time
ransfer
J
i '5
/ -G -.2 e / / 0s
fi
1(072d
2
3 /
."--._i
temp received:
i-A.� )./ Accepted: Rejected: ,/ '., _..-�' . Resarnple:
when
delivered By: Received by: r "-- `_. „. „----- date/time / -(: - t)
7
Comments' ( turnaround: / •'-('N,

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Apr-20
Environmental Chemists, Inc.
Lab #
Date Analyzed ,
Most Probable Number
per gram
Log
1
4/20/20
49,619
4.696
2
4/20/20
28,418
4.454
3
4/20/20
28,418
4.454
4
4/20/20
29,589
4.471
5
4/20/20
43,919
4.643
6
4/20/20
339,484
5.531
7
4/20/20
115,512
5.063
Most Probable Number / Gram
Total
Average
. • 13310
4.759
57,356 :.........
Fecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Environmental Chemists, Inc.
t ,2 Windmill 1,:_av, Wilmington, NC 2S4N1= • 910.392,0223 Lab • 910392 4424 Fa,
71(3 Bi,w ertcwn Road, Mante , NC 27'434 • 232.473.5702 Lab; Fa\
253-A Wilmington Highway, Jacksonville. NC 2S349 • 910.347.541 [ ab
ANALYTICAL & CONSULTING CHEMISTS
inli .r n�ironn:er:talcil2nt!Sh.corn
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Apr 30, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-06497
Project ID: WWTP Sludge
Lab ID
20-16003
Test
Sample ID:
Site: 001
Method
Collect Date/Time Matrix
4/20/2020 10.20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.62%
49619 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16004
Test
Sample ID:
Site: 002
Method
Collect Date/Time Matrix Sampled by
4/20/2020 10:20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.78 %
28418 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16005
Test
Sample ID:
Site: 003
Method
Collect Date/Time Matrix Sampled by
4/20/2020 10.20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.78%
28418 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16006
Test
Sample ID:
Site: 004
Method
Collect Date/Time Matrix Sampled by
4/20/2020 10 20 AM Water Grayson Powell/ Lisa Cottle
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.67 %
29589 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16007
Test
Sample ID:
Site: 005
Method
Collect Date/Time Matrix
4/20/2020 10 20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 254G B
SM 9221C E MPN 24 hr 503
2.96 %
43919 MPN/g
04/21/2020
04/20/2020
Report # 202C•C649' mace 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill W'a‘. Wilmin t, m, NC 2640; • 910 3='2.0223 Lab • '410'392.4424 Foss
710 Bow ertur;n Road, Nlanteo, `.0 27954 • 252.-17 3.97(2 Lab/Fax
235-A Wilmington I lighwav, Jacksonville, NC • glo 3-1 .5i43 Lab/Fat
irlu ri en s iromncr,talrhem!a.cum
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Apr 30, 2020
Customer PO #:
09010063
2020-06497
Customer ID:
Report #:
Project ID: WWTP Sludge
Lab ID
20-16008
Test
Sample ID:
Site: 006
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.71 %
339484 MPN/g
04/21/2020
04/20/2020
Lab ID
20-16009
Test
Sample ID:
Site: 007
Method
Collect Date/Time Matrix
4/20/2020 10:20 AM Water
Results
Sampled by
Grayson Powell/ Lisa Cottle
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
3.03%
115512 MPN/g
04/21/2020
04/20/2020
Comment: Sludge residuals, except pH, reported on a dry weight basispH reported on an as received basis_
Reviewed by: fkk.LOW.vXL Oki�
Repor. rt 202C-0549• Page 3 of 3

MalyOml •
& Cunsullmg Cheroots
•
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification ft94 NHCDHHS: DLS certification ff37729
Collection and Chain of Custody
660? Windmill Way, Wilmington, N(. 2540',
(Mice: 910-392-0223 Fax: [phone]? 1
[e-mail]
Client. Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: ; %(} - j (4,:, i-l.e-) •.
Address: 116 E Murray St
Contact name
PO No:
Wallace, NC 28466
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to: Brent Dean, [e-mail]
Email: [e-mail]
t'
Sampled by 6vrh' j01 Powt,\
I I ' Sc.1 (Ik
SAMPLE TYPE: 1= Influent, L= Effluent, W=Well, ST= stream, S0= Soil, SL=Sludge, Other:
1
Sample Identification
collection
cii
a
aJ
v
composite
or grab
E.
41
c
° o
y
c
o0
u
Lab ID
Number
Preservation
Analysis required
z
U
•V
i
rn
0
z
1-
cc
Lu
o
date
time
temp
Sludge -(Quarterly)
t.{_;0_0
1Q; a0
G
P
1l',,i:, t
X
X
X
CN
Ag,As,Cd,Cr,Cu,Hg,Mo,Ni,Pb,Se,Zn
Total N
1. sludge
G
P
IL, CC 7
X
Fecal Density,%TS
G
P
it:, I.; C `I
X
Fecal Density,% T5
2. sludge
3. sludge
'
G
P
tU,0(..)'f
X
Fecal Density,%TS
G
P
/i. DO ‘4
X
Fecal Density,% TS
4. sludge
5. sludge
G
P
LL0t' 1-
X
Fecal Density,% TS
G
P
LID CU' '
X
Fecal Density,% TS
6 sludge
7. sludge
\✓
G
2
I. L;, Ct:I
X
Fecal Density,% TS
singe (annual)
TCI.P,RCI
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
NO3+NO2,P, K,Na, TKN,
'Transfer
R • quashed By:
Date/time
Received Byi
Date/time
1.
%'�`Cj .
,-1 -a10-i 0
Iry tv.i./...—
"-VV.?fit
2
ternp when received: Accepted: Rejected: Resample:
delivered Ry• Received by. i ,r\;",, date/time -\I 1O" Ol '1/% ' n
Comments. turnaround:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Aug-20
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
7/22/20
1,009
3.004
2
7/22/20
935
2.971
3
7/22/20
558
2.747
4
7/22/20
1,009
3.004
5
7/22/20
412
2.615
6
7/22/20
910
2.959
7
7/22/20
935
2.971
1Vlost Probable Number / Gram
Total
Average
20.270
2.89€
787.
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Lab ID
20-30926
Test
Lab ID
20-30925
Test
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-30922
Test
Sample ID:
Site: 001
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-30923 Site: 002
Test
Total Solids (%)
Fecal Density
Lab ID
20-30924
Test
Sample ID:
Site: 003
Total Solids (%)
Fecal Density
Sample ID:
Site: 004
Total Solids (%)
Fecal Density
Sample ID:
Site: 005
Total Solids (%)
Fecal Density
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Aug 25, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-12250
Project ID: WWTP Sludge
Collect Date/Time
7/22/2020 9:30 AM
Method
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results Date Analyzed
SM 2540 B
SM 9221 C E MPN 24 hr 503
Collect Date/Time Matrix
7/22/2020 9:30 AM Solid/Sludge
2.28%
1009 MPN/g
Sampled by
Lisa Cottle
Method Results
SM 2540 B
SM 9221 C E MPN 24 hr 503
Collect Date/Time Matrix Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
Method Results
07/23/2020
07/22/2020
Date Analyzed
SM 2540 B
2.46 %
935 MPN/g
2.33 %
SM 9221 C E MPN 24 hr 503 558 M PN/g
Collect Date/Time Matrix Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
07/23/2020
07/22/2020
Date Analyzed
Method
07/23/2020
07/22/2020
Results Date Analyzed
SM 2540 B
SM92210EMPN 24hr503
Collect Date/Time Matrix
7/22/2020 9:30 AM Solid/Sludge
Method Results
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.28 %
1009 MPN/g
07/23/2020
07/22/2020
Sampled by
Lisa Cottle
Date Analyzed
3.16%
412 MPN/g
07/23/2020
07/22/2020
Report # 2020-12250
Page 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-30927
Test
Sample ID:
Site: 006
Total Solids (%)
Fecal Density
Lab ID
20-30928
Test
Total Solids (%)
Fecal Density
Comment:
Reviewed by:
Sample ID:
Site: 007
!tcoldi),
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
Method
SM 2540
[e-mail]
Date of Report: Aug 25, 2020
Customer PO #:
Customer ID: 09010063
Report #: 2020-12250
Project ID: WWTP Sludge
Collect Date/Time
7/22/2020 9:30 AM
Matrix Sampled by
Solid/Sludge Lisa Cottle
Results Date Analyzed
2.53 %
SM 9221C E MPN 24 hr 503 910 MPN/g
Collect Date/Time Matrix Sampled by
7/22/2020 9:30 AM Solid/Sludge Lisa Cottle
Method
SM 2540 B
SM 9221 C E MPN 24 hr 503
07/23/2020
07/22/2020
Results Date Analyzed
2.46 %
935 MPN/g
07/23/2020
07/22/2020
Report # 2020-12250
Page 3of3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ certification #94 NHCDHHS: DLS certification #37729
Collection and Chain of Custody
6602 Windmill Way, Wilmington, NC 25405
Office: 910-392-0223 Fax: [phone]
[e-mail]
Client: Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: 2:,C] .- 1 2,0 5 {,/
Address: 316 E Murray St
Contact name:
PO No:
Wallace, NC 28466
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910-285-5927
Copy to: Brent Dean, [e-mail]
Email: [e-mail]
Sampled by. 1-, A C.L)+ -{
SAMPLE TYPE: I= Influent, E- Effluent, W=Well, ST= stream, SO= Soil, SL=Sludge, Other:
collection
o_
E
composite
or grab
`—`
m
c L7
o o`
01
0-
E
o f AD
3 z
Preservation
Analysis required
Sample Identification
date
time
temp
c
z
i
cr
i
m0
Z
p
z
Q
1
cc
LIJ
p
Sludge-(Quarterly)
-7-22-ZD
Cj-
G
P
3�'7 1
x
X
X
CN
Ag,As,Cd,Cr,Cu,tlg,Mo,Ni,Pb,Se,Zn
Total N
1. sludge
G
P
SOS
X
Fecal Density,% TS
2. sludge
I
G
P
1c5 1_ 1)
X
Fecal Density,% TS
3. sludge
I
G
P
770'3 yy
X
Fecal Density,% TS
4. sludge
(
G
P
3Ci
X
Fecal Density,".•a TS
5. sludge
i)
G
P
30ti Lt,
X
Fecal Density,°61'S
6. sludge
G
P
3C.5 Li
X
Fecal Density,%TS
7. sludge
(
G
P
1,C7 L.
X
Fecal Density,%TS
sluge (annual)
TCLP,RCI
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
No3+NO2,P, K,Na, TKN,
Transfer
Relirsuished By:
Date/time
Received By: j. a �.�
Date/time
4J c
*-2' ZL'
..-.-_. ,%
`, 22-zc '3);
l
��[j
(��
j.
�.%-
temp when received: ,. Accepted:4"" Rejected: Reample:
delivered By: � r` Received by: date/time 7/ „�-/-3 ci
p
Comment. turnaround:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Jan-21
Environmental Chemists, Inc.
Lab #
Date Analyzed
1Vlost:Fr ibable Number
er gram
Log
1
11/30/20
732
2.865
2
11/30/20
665
2.823
3
11/30/20
968
2.986
4
11/30/20
766
2.884
5
11/30/20
914
2.961
6
11/30/20
858
2.933
7
11/30/20
973
2.988
Most Probable Number / Gram
Total
Average
20.440
2.920
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Lab ID
20-51474
Test
Sample ID:
Site: Sludge 1
Total Solids (%)
Fecal Density
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Lab ID
20-51475
Test
Sample ID:
Site: Sludge 2
Total Solids (%)
Fecal Density
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results
Date Analyzed
2.46 % 11/30/2020
<732 MPN/g 11/30/2020
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results
2.71 %
<665 MPN/g
Date Analyzed
11/30/2020
11/30/2020
Lab ID Sample ID:
20-51476 Site: Sludge 3
Test
Total Solids (%)
Fecal Density
Lab ID Av Sample ID:
20-51477 Site: Sludge 4
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-51478
Test
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Site: Sludge 5
Total Solids (%)
Fecal Density
Method
SM 2540 B
Matrix Sampled by
Solid/Sludge Sean Pistorice
Results
Date Analyzed
1.86 % 11/30/2020
<968 MPN/g 11/30/2020
Collect Date/Time Matrix
11/30/2020 9:50 AM Solid/Sludge
Results
SM 9221C EMPN 24 hr 503
Method
SM 2540 B
Sampled by
Sean Pistorice
Date Analyzed
2.35 % 11/30/2020
<766 MPN/g 11/30/2020
Collect Date/Time Matrix Sampled by
11/30/2020 9:50 AM Solid/Sludge Sean Pistorice
Results Date Analyzed
SM 9221C E MPN 24 hr 503
1.97 %
<914 MPN/g
11/30/2020
11/30/2020
Report # 2020-20206 Page 1 of 5

ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention. Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info .. environmentalchemists.com
Date of Report: Jan 21, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2020-20206
Project ID: WWTP Sludge
Lab ID
20-51479
Test
Sample ID:
Site: Sludge 6
Total Solids (%)
Fecal Density
Lab ID Sample ID:
20-51480
Test
Site: Sludge 7
Total Solids (%)
Fecal Density
Collect Date/Time
11/30/2020 9:50 AM
Method
SM 2540 B
SM 9221C E MPN 24 hr 503
Matrix
Solid/Sludge
Results
Method
SM 2540 B
Sampled by
Sean Pistorice
Date Analyzed
2.10 % 11/30/2020
<858 MPN/g 11/30/2020
Collect Date/Time Matrix Sampled by
11/30/2020 9:50 AM Solid/Sludge Sean Pistorice
Results Date Analyzed
SM 9221C E MPN 24 hr 503
1.85 %
<973 MPN/g
11/30/2020
11/30/2020
Report #:: 2020-20206 Page 2 of 5

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: D1 Q certification t194 NHCDHHS: DLS certification 1137729
Collection and Chain of Custod
6602 Windmill Way, Wilmington, NC 25405
Office: 910-392-0223 Fax: [phone]
[e-mail]
Client. "Town of Wallace WWTP
Protect name• WWTP LTMP-sludge samples
Report No: ::' ,t ._-- Li./ r.4J `o
Address 316 F Murray St
Contact name'
PO No:
Wallace NC '28466
Report To: Lisa Cottle, ORC
Phone/Fax: Lisa 910.285-5927
Copy to• Brent Dean [e-mail]
Email: [e-mail]
Sarnpled hy: ,4.01.i e .5 r.:Y„t7
SAMPLE TYPE: 1= In luent, E= Eff'ue nt, W=Well, ST- stream, SO= Soil, SL=Sludge, Other:
collection
cl•
w
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composite
or grab
� i
tc
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a
c
m .
li
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date
time
temp
C
ak
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T
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=
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=
0
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=
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G
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Total N
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2. sludge
,
1
G
P
C., : ";"{ ,
X
Fecal Density,% TS
3. sludge
'
6
P
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X
Fecal Density,%TS
4 sludge
G
P
ti I ''-?-'1')
X
Fecal Density,', TS
5, sludge
1
G
P
(,1'--1'j f,
X
Fecal Density,% TS
6. sludge
G
P
=; ti'It 1 Mi
X
Fecal Densit y,S'6 TS
I. sludge
6
P
t 1'.15(n
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X
Fetal Derisity,9 TS
S H,r?
sluge (annual)
TCLP,RCI
Al
NH3-N,Mg,Ph,plant aval. N,Ca, SAR
N034.NO2,P, K,Na, TKN,
Transfer
Relinquished By:
Date/time
Receive di.,f3y:„ 1
Date%time/
i ->c (--ci
1
3,-,,".. (l i��f'.l� i ilT._"—'
1,
i 1: .- J i� ?�
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f � � �e ��. /ti..�' ti"
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delivered By: Received bye} ' -, - x. ,_ / j .1t : , )'
. ,` _�*`i ,�i .. . '.,.._n_ ..- date time • j �j. ,.C,
Comments: turnaround:

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SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Beulaville, the Town of Warsaw, the Town of Clayton, the Town of Kenansville and
Southwest Plantation met pathogen reduction and vector attraction reduction requirements through
lime stabilization. The soil pH will continue to be raised through the continued application of lime
stabilized biosolids to these application fields.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
"I nip rav&no-Ci rowth� ..
IV i Science;
HARVEYS-BEULAVILLE [60126]
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Grower: TRIPLE S FARMS Page 3
Farm: TRIPLE S FARM / FIELD 1
LID: D2FF3088107 Target pH: 6
Test Method: Mehlich III Received: 11/2/2020 Processed: 11/4/2020
Sample ID
Lab ID
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
15
836648PW
68
122
14
32
5.5
2.8
20
132
132
28
26
60
6.2
55
2.85
Min
16
836649PW
336
42
10
68
5.4
1.6
33
1326
1326
62
47
678
8.4
81
1.47
Min
17
836650PW
391
40
9
67
5.3
2.2
38
2011
2011
56
43
792
10.2
78
0.70
Min
18
836651PW
285
14
8
90
6.1
0.2
31
2211
2211
41
40
785
9.3
98
0.86
Min
19
836652PW
268
12
7
84
6.0
0.8
33
1925
1925
47
45
700
9.0
91
1.08
Min
20
836653PW
354
24
7
86
6.2
0.6
42
1374
1374
38
37
630
9.7
94
0.87
Min
21
836654PW
263
11
5
78
5.7
1.4
45
1071
1071
41
34
615
8.9
84
1.52
Min
22
836655PW
259
11
6
80
5.5
0.8
34
954
954
47
38
535
6.1
87
0.72
Min
23
836656PW
234
11
5
75
5.7
1.6
44
1028
1028
41
34
518
8.4
81
0.85
Min
i
.- 24 836657PW
223 13
7
69
5.3
1.2
41
745
745
41
34
455
5.3
77
0.63
Min 1
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID
15
Crop
BERMUDA PASTURE M
NCDA
Lime
Tons/Acre
Soil Fertility
Recommendations (Ibs/A)
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
1.3
220
20
12
16
BERMUDA PASTURE M
0.8
220
140
12
17
BERMUDA PASTURE M
1.2
220
140
12
18
BERMUDA PASTURE M
220
200
12
19
BERMUDA PASTURE M
220
220
12
20
BERMUDA PASTURE M
220
180
12
21
BERMUDA PASTURE M
0.5
220
220
25
12
22
BERMUDA PASTURE M
0.4
220
220
25
12
23
BERMUDA PASTURE M
0.5
220
220
25
12
24
BERMUDA PASTURE M
0.6
220
200
25
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the tee assessed on the referenced sample.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
cc�1npray %7rowdy.. .
W i Scie.n cef
HARVEYS-BEULAVILLE [60126] Grower: TRIPLE S FARMS
Farm: TRIPLE S FARM
1060 S NC 41 & 111 LID: D2FF3088107
BEULAVILLE, NC 28518 Test Method: Mehlich III
/ FIELD 1
Received:
Page 4
Target pH: 6
11/2/2020 Processed: 11/4/2020
Sample ID
25
Lab ID
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
836658PW
239
16
6
74
5.8
1.4
40
908
908
34
30
465
7.4
81
0.73
Min
26
836659PW
412
44
8
85
5.7
0.4
26
1940
1940
38
32
718
8.5
95
0.42
Min
27
836660PW
322
27
7
77
5.8
1.4
27
1756
1756
47
38
722
9.4
85
0.54
Min
Explanation of Symbols - % (percent), -I Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID Crop
25
BERMUDA PASTURE M
26
NCDA Soil Fertility Recommendations (Ibs/A)
Lime
TonslAcre
0.4
N
Nitrogen
P205 K20 Mg
Phosphate Potash Magnesium
220
200
25
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
12
BERMUDA PASTURE M
27
0.3
220
120
12
BERMUDA PASTURE M
0.4
220
180
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in Its entirety Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
"1 n'lpprc viAtto,Grcr th,...
Wi Sc L&vtGt'�'
HARVEYS-BEULAVILLE [60126]
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Grower:
Farm:
Test Method:
TRIPLE S FARMS
TRIPLE S FARM
LID: D2FF3088105
Mehlich III
/ FIELD
2
Received:
Target
11/2/2020 Processed:
Page 5
pH:
6
11/4/2020
Sample ID
28
Lab ID
836661PW
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
231
10
6
79
5.9
1.2
25
1072
1072
34
30
615
8.6
86
0.70
Min
29
836662PW
188
8
5
80
6.0
1.0
29
654
654
34
37
428
7.2
86
0.94
Min
30
836663PW
204
7
6
84
5.9
0.6
25
762
762
31
28
568
6.5
91
0.53
Min
31
836664PW
198
12
6
81
5.8
1.0
31
760
760
34
30
550
7.8
87
1.02
Min
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID
28
Crop
BERMUDA PASTURE M
NCDA
Lime
Tons/Acre
Soil Fertility Recommendations (Ibs/A)
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
0.3
220
220
12
29
BERMUDA PASTURE M
220
220
25
12
30
BERMUDA PASTURE M
0.3
220
230
25
12
31
BERMUDA PASTURE M
0.3
220
220
25
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis Is based solely on the sample as received. Laboratory liability is limited to the tee assessed on the referenced sampie.

HARVEYS-BEULAVILLE [60126]
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
Grower: TRIPLE S FARMS
Farm: TRIPLE S FARM / FIELD 3A
LID: D2FF3088103
Test Method: Mehlich III
I mil ray G row . .
1LUii'S'
Received: 11/2/2020
Page 6
Target pH: 6
Processed: 11/4/2020
Sample ID
32
Lab ID
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
836665PW
229
10
9
87
6.5
0.4
31
956
956
44
36
572
9.8
96
0.97
Min
33
836666PW
265
16
10
86
6.6
0.4
34
1110
1110
50
38
545
10.9
96
1.30
Min
34
836667PW
295
9
8
90
6.2
0.2
32
1076
1076
41
39
602
8.9
98
0.90
Min
35
836668PW
300
9
7
75
5.6
1.4
25
1328
1328
38
32
680
8.0
82
0.65
Min
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID
32
Crop
BERMUDA PASTURE M
NCDA
Lime
Tons/Acre
Soil Fertility Recommendations (Ibs/A)
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
220
220
pH$
12
33
BERMUDA PASTURE M
220
200
pH$
12
34
BERMUDA PASTURE M
220
220
12
35
BERMUDA PASTURE M
0.6
220
220
12
Explanation of Symbols - Ibs/A (pounds p •-•-mo)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability Is limited to the lee assessed wr the referenced sample.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
cr� / np rCrt/ lAttidx i7rowtY'...
W i S ci,e4w&"
HARVEYS-BEULAVILLE [60126]
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Grower: TRIPLE S FARMS Page 7
Farm: TRIPLE S FARM / FIELD 3B
LID: D2FF3088104 Target pH: 6
Test Method: Mehlich 111 Received: 11/2/2020 Processed: 11/4/2020
Sample ID
36
Lab ID
•
Ca (%)
pHw
Zn-AI
Mn-AI
Cu-I
Soil Class
79
6.2
685
31
368
0.83
Min
37
r
r
74
6.6
0.6
24
682
682
31
26
318
9.2
94
1.41
Min
38
836671PW
236
38
13
82
6.4
0
618
31
30
302
:0
Min
Explanation of Symbols - % (percent), -I Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID Crop
36
BERMUDA PASTURE M
37
NCDA Soil Fertility Recommendations (lbs/A)
Lime
TonslAcre
N
Nitrogen
P205 K20 Mg
Phosphate Potash Magnesium
220
180
BERMUDA PASTURE M
38
220
20
s
Sulfur
B
Boron
Zn
Zinc
20
Mn
Manganese
pH$
Cu
Copper
See Note
12
12
BERMUDA PASTURE M
220
140
20
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in Its entirety. Waters Agricutural Laboratories has no control over the manner In which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed nn the referenced sarnple.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
"I flip v.ay im,l / {'J YCTW th/.. .
I4 i SG%�,rtu�i'
HARVEYS-BEULAVILLE [601261
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Grower:
Farm:
Test Method:
TRIPLE S FARMS
TRIPLE S FARM
LID: D2FF3088110
Mehlich III
Page 8
/ FIELD 4
Target pH:
Received: 11/2/2020 Processed:
6
11/4/2020
Sample ID
39
Lab ID
836672PW
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
153
142
13
52
5.9
1.6
20
410
410
44
36
200
6.7
76
1.61
Min
40
836673PW
140
74
14
56
5.9
0.8
12
325
325
31
28
155
3.9
79
0.46
Min
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID Crop
39
BERMUDA PASTURE M
40
NCDA Soil Fertility Recommendations (Ibs/A)
Lime
Tons/Acre
0.3
N
Nitrogen
P205 K20 Mg
Phosphate Potash Magnesium
220
BERMUDA PASTURE M
0.3
220
60
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
20
20
Cu
Copper
See Note
12
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in Its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis Is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
a I ni,prayivt. 'Gio-wth'..
With Sae/Ace"
HARVEYS-BEULAVILLE [60126]
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Grower: TRIPLE S FARMS Page 9
Farm: TRIPLE S FARM / FIELD 5
LID: D2FF3088106 Target pH: 6
Test Method: Mehlich III Received: 11/2/2020 Processed: 11/4/2020
Sample ID
41
Lab ID
836674PW
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
284
320
13
58
5.9
1.8
21
1185
1185
34
30
548
11.7
85
0.70
Min
42
836675PW
295
238
12
68
6.6
0.2
23
745
745
38
31
412
6.8
97
0.57
Min
43
836676PW
268
146
10
68
6.1
0.8
22
710
710
47
44
408
6.9
88
2.01
Min
44
836677PW
276
147
10
68
6.2
0.8
19
816
816
28
31
388
6.9
88
0.80
Min
45
836678PW
273
121
22
48
6.2
1.2
22
1051
1051
56
48
765
5.9
80
0.75
Min
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID
41
Crop
BERMUDA PASTURE M
NCDA
Lime
TonslAcre
0.3
Soil Fertility Recommendations (Ibs/A)
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn 1
Manganese
Cu
Copper
See Note
220
20
12
42
BERMUDA PASTURE M
220
20
pH$
12
43
BERMUDA PASTURE M
220
20
12
44
BERMUDA PASTURE M
220
20
12
45
BERMUDA PASTURE M
220
20
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is Ilndled to the tee assessed on the referenced sample.

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
rcrrnpr 'i'vt +7ro-w 11,...
1 W ith, SG%e,nce "
HARVEYS-BEULAVILLE
1060 S NC 41 & 111
BEULAVILLE, NC 28518
Sample ID
7
[60126]
Lab ID
836640PW
P-I
K-I
Mg (%)
Grower:
Farm:
Test Method:
Ca (%)
TRIPLE S FARMS
TRIPLE S FARM / FIELD 7
LID: D2FF3088109
Mehlich III Received: 11/2/2020
Target
Processed:
Page 10
pH: 6
11/4/2020
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
171
127
12
55
5.6
1.8
. 32
392
392
34
30
255
7.3
75
1.40
Min
8
836641PW
107
76
12
37
5.1
2.2
26
208
208
19
21
150
5.0
56
1.76
Min
9
836642PW
81
79
12
41
5.1
3.0
38
171
171
16
19
78
7.2
58
3.26
Min
10
836643PW
150
49
14
62
5.5
1.4
29
258
258
25
24
95
6.7
79
2.08
Min
11
836644PW
120
52
10
58
5.6
1.8
32
306
306
25
24
145
6.5
72
1.84
Min
12
836645PW
136
67
11
62
5.8
1.0
28
301
301
22
23
158
5.1
80
0.99
Min
13
836646PW
150
131
12
62
5.9
1.0
27
409
409
38
32
210
6.3
84
1.11
Min
14
836647PW
142
146
15
53
5.6
1.0
24
331
331
31
28
168
5.3
81
1.14
Min
Explanation of Symbols - % (percent), -I Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID Crop
8
9
BERMUDA PASTURE M
BERMUDA PASTURE M
BERMUDA PASTURE M
NCDA Soil Fertility Recommendations (Ibs/A)
Lime
Tons/Acre
0.7
N
Nitrogen
P205
Phosphate
220
K20
Potash
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
1.3
1.8
220
220
60
50
Cu
Copper
See Note
12
12
12
10
BERMUDA PASTURE M
0.6
220
110
12
11
BERMUDA PASTURE M
0.7
220
110
12
12
BERMUDA PASTURE M
0.3
220
80
12
13
BERMUDA PASTURE M
0.3
220
12
14
BERMUDA PASTURE M
0.4
220
20
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability Is limited to the fee assessed on the referenced swipe.

WA RS r 1. RAL
.A L=OR : NC..
HARVEYS-BEULAVILLE [60126]
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive i Warsaw, NC 28398- i Phone [phone]
Grower: TRIPLE S FARMS
Farm: TRIPLE S FARM / HELD 9
"1n't ?rOv 4'-<rowt�L..
lit) C ScCe'vu e"
Page 11
Tar et nH: 6
UM J I'& rt"I & I I I 1.11.F. ULUVJVVV IVV -
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 11/2/2020 Processed: 11/4/2020
Sample ID
1
Lab ID
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
836634PW
233
88
15
64
5.7
1.2
24
452
452
41
34
265
7.8
84
1.47
Min
2
836635PW
194
36
14
74
5.7
0.4
17
385
385
38
32
218
4.8
92
0.58
Min
3
836636PW
270
50
14
70
5.9
1.0
20
521
521
44
36
275
7.7
87
0.91
Min
4
836637PW
208
62
15
71
6.0
0.6
21
452
452
41
42
250
6.3
90
1.01
Min
5
836638PW
250
77
12
75
6.1
0.6
25
694
694
47
44
368
7.9
92
0.83
Min
6
836639PW
357
80
8
88
6.3
0.2
31
1270
1270
41
37
672
13.1
99
0.90
Min
Explanation of Symbols - % (percent), -I (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID
1
Crop
BERMUDA PASTURE M
NCDA
Lime
Tons/Acre
0.4
Soil Fertility Recommendations
(lbs/A)
Mg
Magnesium
N
Nitrogen
P205
Phosphate
K20
Potash
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
220
40
20
12
2
BERMUDA PASTURE M
0.3
220
150
20
12
3
BERMUDA PASTURE M
0.3
220
110
20
12
4
BERMUDA PASTURE M
220
90
20
12
5
BERMUDA PASTURE M
220
60
12
6
BERMUDA PASTURE M
220
50
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in Its entirety. Waters Agricutural Laboratories has rio control over the manner in which samples are taken, therefore, analysis Is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

4,1
Farm Sample ID Map
Tnple S Farms

2020 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2020 APPLICATION SUMMARY
. . . . ..
.:.**......
• •• ••••••••
::47aiiiier:'::
TrUki
•• •.•. .
::litO:
:.:.:.:.:.
*Oil:
•. . . . . .
.:.:.:•:.:•:.
. . . ...
::A.00.:
. . . . .
:::::MW::
. . .
:::Sad:
:•:.:::.::::::::::
:041i0k.:.:
•. . . . . .
••.• • " " "
Pk T0.P.
::):A0*:::
.•. . . . ... .
" " " "
:-:----:-:-:
:Or.y:*r.i:
. . . . . . .
" ' "•"•"•"•"••••••••••••••••••••••••••••••
..:.:.:::::::::::::::::::
:-:.:.:.:.:.::::::ci.o.0..:.:.:.:.:.:•:.:.:
Source
:PAN
: (lbs/oe) :
Eric Smith
1
1
34.2
Mar-20
70000
0.18
6.04
Bermudagrass
Beulaville WWTP
131.08
Mar-20
90000
0.19
6.53
Bermudagrass
Wallace WWTP
Jul-20
270000
0.80
27.47
Bermudagrass
Wallace WWTP
390000
1.12
38.22
Bermudagrass
Little Creek WRF
Aug-20
198000
0.59
20.15
Bermudagrass
Wallace WWTP
Sep-20
70000
0.18
6.04
Bermudagrass
Beulaville WWTP
Oct-20
66038
0.04
1.40
Bermudagrass
Kenansville WWTP
2
8.48
Mar-20
54000
0.88
7.43
Bermudagrass
Warsaw WWTP
182.25
Jun-20
116200
1.62
13.76
Bermudagrass
Wallace WWTP
Jul-20
131900
1.52
12.93
Bermudagrass
Little Creek WRF
Aug-20
42900
0.51
4.36
Bermudagrass
Wallace WWTP
Nov-20
96290
1.11
9.44
Wheat
Little Creek WRF
3
21
Mar-20
23800
0.16
3.28
Bermudagrass
Warsaw WWTP
118.41
May-20
48000
0.20
4.14
Bermudagrass
Beulaville WWTP
Jun-20
218400
1.02
21.40
Bermudagrass
Little Creek WRF
Aug-20
101300
0.49
10.31
Bermudagrass
Wallace WWTP
Nov-20
212330
0.99
20.81
Wheat
Little Creek WRF
4
4.14
Jun-20
39500
1.31
5.44
Fescue
Warsaw WWTP
57.68
Jun-20
12000
0.31
1.27
Fescue
Southwest Plantation
6800
0.16
0.67
Fescue
Little Creek WRF
5
11.2
Jun-20
153800
1.63
18.21
Fescue
Wallace WWTP
69.77
Jun-20
107000
1.31
14.72
Fescue
Warsaw WWTP
Jun-20
18500
0.16
1.81
Fescue
Little Creek WRF
6
14
Mar-20
96000
0.95
13.21
Trees
Warsaw WWTP
26.18
7
14.5
Mar-20
276000
1.38
20.03
Bermudagrass
Wallace WWTP
303.45
Mar-20
12000
0.09
1.27
Bermudagrass
Southwest Plantation
Jul-20
240000
1.68
24.42
Bermudagrass
Wallace WWTP
Jul-20
429000
2.90
42.04
Bermudagrass
Little Creek WRF
Aug-20
78000
0.55
7.94
Bermudagrass
Wallace WWTP
Nov-20
156220
1.06
15.31
Wheat
Little Creek WRF
9
8.93
Jan-20
12000
0.14
1.27
Wheat
Southwest Plantation
121.68
Apr-20
12000
0.14
1.27
Millett
Southwest Plantation
May-20
42000
0.41
3.63
Millett
Beulaville WWTP
Aug-20
30000
0.33
2.94
Millett
Little Creek WRF
Nov-20
140000
2.16
19.27
Wheat
Warsaw WWTP
Nov-20
18040
0.20
1.77
Wheat
Little Creek WRF
Nov-20
12000
0.14
1.27
Wheat
Southwest Plantation
Fields App ied to: 8 116.4
Total
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Town of Rose Hill
Southwest Plantation
Town of Wallace
Town of Warsaw
Gallons
Dry Tons
Metric
Tons
Permit Limit Dry Tons
4,090,018
411.46
374.05
NA
230,000
19.85
18.05
38
1,707,480
167.32
152.11
80
66,038
1.40
1.28
38
0
0.00
0.00
38
60,000
636
5.78
5
1,566,200
153.18
139.25
330
460,300
6334
57.58
38
Branch Residuals Soils, LLC Confidential
2/13/2021
Page 1

2020 APPLICATION CONDITION SUMMARIES

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.07
Residual Report No.: BL 2020-07646
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3 4/20
1
70,000.0
Dry
Cool,Clear
0.00
Total Gallons
70,000.0=

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.07
Residual Report No.: BL 2020-07646
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/16/20
1
70,000.0
Dry
Warm,Cloudy
0.01
Total Gallons
70,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Beulaville WWTP
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.07
Residual Report No.: BL 2020-07646
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/13/20
3
48,000.0
Dry
Warm,Clear
0.00
Total Gallons
48,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Beulaville WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.07
Residual Report No.: BL 2020-07646
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5 12 20
9
42,000.0
Dry
Cool,Clear
0.00
Total Gallons
42,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/23/20
1
30,000.0
Dry
Hot,Cloudy
0.24
7/24/20
1
12,000.0
Moist
Hot,Cloudy
0.48
7/27/20
1
36,000.0
Dry
Hot,Clear
0.00
7/28/20
1
36,000.0
Dry
Hot,Cloudy
0.08
8/27/20
1
18,000.0
Dry
Hot,Clear
0.00
8/31/20
1
30,000.0
Dry
Hot,Clear
0.00
9/1/20
1
30,000.0
Dry
Hot,Clear
0.00
9/2/20
1
30,000.0
Dry
Hot,Cloudy
0.01
9/3/20
1
30,000.0
Dry
Hot,Clear
0.00
9/4/20
1
18,000.0
Dry
Hot,Clear
0.00
9/8/20
1
24,000.0
Dry
Warm,Cloudy
T
9/11/20
1
12,000.0
Dry
Hot,Cloudy
0.45
9/22/20
1
36,000.0
Dry
Warm,Clear
0.00
9/23/20
1
36,000.0
Dry
Warm,Clear
0.00
9/24/20
1
12,000.0
Dry
Warm,Cloudy
T
Total Gallons
390,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/21/20
2
36,000.0
Dry
Hot,Clear
0.00
7/22/20
2
36,000.0
Dry
Hot,Clear
0.00
7/29/20
2
14,000.0
Dry
Hot,Clear
0.00
7/30/20
2
12,100.0
Dry
Hot,Cloudy
0.01
8/10/20
2
3,500.0
Dry
Hot,Cloudy
0.16
8/12/20
2
3,500.0
Dry
Hot,Clear
0.00
8/13/20
2
8,700.0
Dry
Hot,Cloudy
0.01
8/14/20
2
6,900.0
Dry
Warm,Clear
0.00
8/19/20
2
5,200.0
Dry
Warm,Cloudy
0.00
8/24/20
2
6,000.0
Dry
Warm,Cloudy
0.20
Total Gallons
131,900.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/6/20
2
30,130.0
Dry
Warm,Clear
0.00
12/10/20
2
36,100.0
Dry
Cool,Clear
0.00
12/11/20
2
30,060.0
Dry
Cool,Clear
0.00
Total Gallons
96,290.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/20
3
10,400.0
Moist
Hot,Clear
0.00
6/30/20
3
24,300.0
Dry
Hot,Cloudy
0.01
7/2/20
3
24,000.0
Dry
Hot,Clear
0.00
7/6/20
3
24,000.0
Moist
Hot,Clear
0.00
7/7/20
3
3,600.0
Dry
Warm,Cloudy
0.00
7/29/20
3
34,000.0
Dry
Hot,Clear
0.00
7/30/20
3
29,900.0
Dry
Hot,Cloudy
0.01
8/10/20
3
8,500.0
Dry
Hot,Cloudy
0.16
8/12/20
3
8,500.0
Dry
Hot,Clear
0.00
8/13/20
3
21,300.0
Dry
Hot,Cloudy
0.01
8/14/20
3
17,100.0
Dry
Warm,Clear
0.00
8/19/20
3
12,800.0
Dry
Warm,Cloudy
0.00
Total Gallons
218,400.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/23/20
3
47,190.0
Dry
Cool,Cloudy
0.02
11/24/20
3
54,000.0
Dry
Cool,Clear
0.00
11/25/20
3
63,010.0
Dry
Warm,Cloudy
0.00
12/7/20
3
12,010.0
Dry
Cool,Cloudy
0.19
12/9/20
3
36,120.0
Dry
Cool,Clear
0.00
Total Gallons
212,330.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/20
4
2,000.0
Moist
Hot,Clear
0.00
6/30/20
4
4,800.0
Dry
Hot,Cloudy
0.01
Total Gallons
6,800.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/20
5
5,600.0
Moist
Hot,Clear
0.00
6/30/20
5
12,900.0
Dry
Hot,Cloudy
0.01
Total Gallons
18,500.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/13/20
7
36,000.0
Dry
Hot,Cloudy
0.24
7/15/20
7
30,000.0
Dry
Hot,Clear
0.00
7/16/20
7
30,000.0
Dry
Hot,Clear
0.00
7/17/20
7
12,000.0
Dry
Hot,Cloudy
0.14
7/20/20
7
12,000.0
Dry
Hot,Cloudy
0.02
10/6/20
7
18,000.0
Dry
Warm,Clear
0.00
10/8/20
7
36,000.0
Dry
Warm,Clear
0.00
10/9/20
7
24,000.0
Dry
Warm,Cloudy
0.00
10/19/20
7
54,000.0
Dry
Warm,Clear
0.00
10/20/20
7
54,000.0
Dry
Warm,Clear
0.00
10/21/20
7
54,000.0
Dry
Warm,Clear
0.00
10/22/20
7
63,000.0
Dry
Warm,Clear
0.00
10/23/20
7
6,000.0
Dry
Warm,Clear
0.00
Total Gallons
429,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/3/20
7
48,000.0
Dry
Cool,Clear
0.00
11/4/20
7
54,000.0
Dry
Warm,Clear
0.00
11/5/20
7
54,220.0
Dry
Warm,Clear
0.00
Total Gallons
156,220.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/20/20
9
18,000.0
Moist
Warm,Cloudy
0.22
8/21/20
9
12,000.0
Moist
Warm,Cloudy
0.08
Total Gallons
30,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Little Creek WRF
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.35
Residual Report No.: CL 20-055-0007
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/10/20
9
18,040.0
Dry
Warm,Clear
0.00
Total Gallons
18,040.0

Town of Kenansville
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Kenansville WWTP
Farmer:
Eric Smith
Acres:
34.2
Site/Tract:
1
Application Method:
Surface
Field:
1
Percent Solids:
0.51
Residual Report No.:
KV 2020-09561
Crop:
Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/22/20
1
18,900.0
Dry
Warm,Clear
0.00
10/23/20
1
47,138.0
Dry
Warm,Clear
0.00
ifi6.44)38.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2020
Southwest Plantation
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 2.54
Residual Report No.: SWP 2020 4-13
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/20
4
12,000.0
Moist
Hot,Clear
0.00
Total Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2020
Southwest Plantation
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.54
Residual Report No.: SWP 2020 4-13
Crop: Bennudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/23/20
7
12,000.0
Dry
Cool,Cloudy
0.06
Total Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2020
Southwest Plantation
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.54
Residual Report No.: SWP 2020 4-13
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/17/20
9
12,000.0
Dry
Cool,Clear
0.00
Total Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2020
Southwest Plantation
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.54
Residual Report No.: SWP 2020 4-13
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/25/20
9
12,000.0
Dry
Cool,Clear
0.00
Total Gallons
1
12;00Q.0.

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2020
Southwest Plantation
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.54
Residual Report No.: SWP 2020 4-13
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/30/20
9
12,000.0
Moist
Warm,Cloudy
0.52
Total Gallons
12,000.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 1.74
Residual Report No.: WL 1-2020-1-28
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/24/20
1
30,000.0
Dry
Cool,Cloudy
0.07
3/27/20
1
60,000.0
Dry
Warm,Clear
0.00
Total Gallons
90,000.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 1.74
Residual Report No.: WL 1-2020-1-28
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/19/20
7
108,000.0
Dry
Warm,Cloudy
0.07
3/20/20
7
108,000.0
Dry
Warm,Clear
0.00
3/24/20
7
60,000.0
Dry
Cool,Cloudy
0.07
Total Gallons
276,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Incorporated
Field: 2
Percent Solids: 2.84
Residual Report No.: WL 2-2020-4-30
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/8/20
2
31,000.0
Dry
Warm,Clear
0.00
6/9/20
2
33,500.0
Dry
Hot,Cloudy
0.01
6/25/20
2
31,000.0
Dry
Warm,Cloudy
0.42
6/26/20
2
7,800.0
Moist
Hot,Clear
0.00
6/29/20
2
12,900.0
Moist
Hot,Clear
0.00
Total Gallons
116,200..0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Incorporated
Field: 5
Percent Solids: 2.84
Residual Report No.: WL 2-2020-4-30
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/8/20
5
41,000.0
Dry
Warm,Clear
0.00
6/9/20
5
44,500.0
Dry
Hot,Cloudy
0.01
6/25/20
5
41,000.0
Dry
Warm,Cloudy
0.42
6/26/20
5
10,200.0
Moist
Hot,Clear
0.00
6/29/20
5
17,100.0
Moist
Hot,Clear
0.00
Total Gailous
153,800..0.

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/23/20
1
66,000.0
Dry
Hot,Cloudy
0.24
7/24/20
1
48,000.0
Moist
Hot,Cloudy
0.48
7/27/20
1
72,000.0
Dry
Hot,Clear
0.00
7/28/20
1
72,000.0
Dry
Hot,Cloudy
0.08
7/29/20
1
12,000.0
Dry
Hot,Cloudy
0.20
Total Gallons
270,000.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/27/20
1
36,000.0
Dry
Hot,Clear
0.00
8/28/20
1
30,000.0
Dry
Hot,Clear
0.00
8/31/20
1
42,000.0
Dry
Hot,Clear
0.00
9/1/20
1
36,000.0
Dry
Hot,Clear
0.00
9/2/20
1
30,000.0
Dry
Hot,Cloudy
0.01
9/3/20
1
24,000.0
Dry
Hot,Clear
0.00
Total Gallons
198,000.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Incorporated
Field: 2
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/10/20
2
5,200.0
Dry
Hot,Cloudy
0.16
8/12/20
2
7,000.0
Dry
Hot,Clear
0.00
8/13/20
2
11,000.0
Dry
Hot,Cloudy
0.01
8/14/20
2
8,700.0
Dry
Warm,Clear
0.00
8/19/20
2
11,000.0
Dry
Warm,Clear
0.00
Total Gallons
42,900.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Incorporated
Field: 3
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/10/20
3
12,800.0
Dry
Hot,Cloudy
0.16
8/12/20
3
17,000.0
Dry
Hot,Clear
0.00
8/13/20
3
25,000.0
Dry
Hot,Cloudy
0.01
8/14/20
3
21,500.0
Dry
Warm,Clear
0.00
8/19/20
3
25,000.0
Dry
Warm,Clear
0.00
Total Gallons
101,300.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/6/20
7
6,000.0
Moist
Hot,Clear
0.00
7/13/20
7
96,000.0
Dry
Hot,Cloudy
0.24
7/15/20
7
108,000.0
Dry
Hot,Clear
0.00
7/16/20
7
30,000.0
Dry
Hot,Clear
0.00
Total Gallons
240,000.0

Town of Wallace
Wallace, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2020
Wallace WWTP
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 2.44
Residual Report No.: WL-3-2020-8-25
Crop: Bermudagrass
Date
Field No.
Suffield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/20/20
7
36,000.0
Dry
Warm,Cloudy
0.22
8/21/20
7
42,000.0
Moist
Warm,Cloudy
0.08
Total Gallons
78,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 3.30
Residual Report No.: WR 2020-07645
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3 2/20
2
54,000.0
Dry
Warm,Clear
0.00
Total Gallons
54,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 3.30
Residual Report No.: WR 2020-07645
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/12/20
3
23,800.0
Dry
Warm,Clear
0.00
Total Gallons
23.,800.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 3.30
Residual Report No.: WR 2020-07645
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/23/20
4
39,500.0
Dry
Warm,Cloudy
0.18
Total Gallons
39,50:0.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres:
11.2
Site/Tract:
1
Application Method: Surface
Field:
5
Percent Solids: 3.30
Residual Report No.:
WR 2020-07645
Crop:
Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/23 20
5
107,000.0
Dry
Warm,Cloudy
0.18
•:•:-:•:-
:•:•:•:•:

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres: 13.95
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 3.30
Residual Report No.: WR 2020-07645
Crop: Trees
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/1120
6
96,000.0
Dry
Warm,Cloudy
0.05
Total Gallons
96,00.0.0.

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2020
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 3.30
Residual Report No.: WR 2020-07645
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/9/20
9
69,300.0
Dry
Warm,Cloudy
0.06
11 /10'20
9
70,700.0
Dry
Warm,Clear
0.00
Total Gallons
140,000.0