WQ0037135_2020 Residual Annual Report_20210226

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00037135
Applicant/Permittee U.S. Biosolids, Inc
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Zach Key
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ .....................................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3369577871
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00037135
Fbs Current Existing permt number
Applicant/Permittee Address* 958 Foots Road Roaring River, NC 28669
Facility Name * U.S. Biosolids RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Annual Report -US Biosolids B.pdf 5.11 MB
Upload only 1 FLFdocurrent (less than 250 `VB). Miltiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature ]]
Submission Date 2/26/2021

2020
U.S. Biosolids, Inc.
Class B Permit
2020 Annual Report
Land Application Program
Permit No. WQ0037105

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0037135 County: Wilkes Year: 2020
Facility Name (as shown on permit):
Land Application Operator:
U.S. Biosolids. Inc.
U.S. Biosolids, Inc.
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit-1
49
Total number of fields utilized for land application during the year:1
22
Total amount of dry tons applied during the year for all application sites:
578.02
Total number of acres utilizes for land application during the year:
271.18
Part B - Annual Com fiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-113 below) issued by the Division of Water Resources. Q Yes D No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T, I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 1 1 I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Zach Key President
Permittee Name and Title (type or print)
Sii4nafure of
9. -2A,JI
Sig tune of rmittee Date
Date Sign4rure of Land Applier
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135
Facility Name: U.S. Biosolids, Inc.
Residual Source WQ # or
NPDES #:
NCO025984
WWTP Name: Forest City WWTP
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
5)
Statesville Analytical
Parameter
(mg/kg)
Conc.
Limit
m a
Sample or Composite Date
1-23-20
Percent Solids (%)
NA
15.5
Arsenic
75
3.11
Cadmium
85
2.9
Copper
4,300
233
Chromium
NA
NA
Lead
840
47.1
Mercury
57
0.187
Molybdenum
75
5.03
Nickel
420
9.55
Selenium
100
3.63
Zinc
7,500
1123
Total Phosphorus
NA
832.2
TKN
NA
47112
Ammonia-NitrogenE
NA
14452
Nitrate and Nitrite I
NA
722.58
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting
f�lsc information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer'* ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0037135 Laboratory: 1) Statesville Analytical
Facility Name:
Residual Source
NPDES # or WQ#:
U.S. Biosolids, Inc.
WQ0037135
WWTP Name: Forest City WWTP
Residual Analvsis Data
3)
4)
5)
Sample or C mposite Date
Parameter
(mpg)
I -23-20
H
5.67
Aluminum
7400
Calcium
9970
Potassium
2920
Magnesium
2700
PAN
17745.5
SAR
0.929
Sodium
1032.26
KI certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. l am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer' ate
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135
Facility Name: U.S. Biosolids, Inc.
Residual Source WQ # or NCO020664
NPDES #:
WWTP Name: Town of Spindale WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)(mg/kg
Conc.
Limit
)a
Sample or Composite Date
6-5-2020
Percent Solids (%)
NA
0.38
Arsenic
75
25
Cadmium
85
25
Copper
4,300
131
Chromium
NA
62.5
Lead
840
75
Mercury
57
3.83
Molybdenum
75
62.5
N ickel
420
62.5
Selenium
100
12
Zinc
7,500
313
Total Phosphorus
NA
9330
TKN
NA
129000
Ammonia -Nitrogen
Nitrate and Nitrite
NA
NA
31800
1700
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Keterence the ►naivuluai permit for metals itmns.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WO0037135 Laboratory: 1) Waypoint Analytical
Facility Name: U.S. Biosolids, Inc. 2)
Residual Source NCO020664 3)
NPDES # or WQ#: 4)
WWTP Name: Town of Spindale WWTP 5)
Residual Analvsis Data
-----
Parameter
Poatassium
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the passibility of fines and imprisonment for knowing violations."
Signature of Preparer
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135 Laboratory: 1)
Facility Name: US Biosolids, Inc. 2)
Residual Source WQ # or 3)
NPDES #: NC0021181 4
WWTP Name: City of Belmont 5)
Residual Analvsis Data
Waypoint Analytical
Parameter
(mg/kg)(mg/kg)d
Conc.
Limit
Sample or Composite Date
8-18-20
Percent Solids (%)
NA
395
Arsenic
75
12.5
Cadmium
85
2.5
Copper
4,300
343
Chromium
NA
91.8
Lead
840
31.3
Mercury
57
0.973
Molybdenum
75
6.25
Nickel
420
23.2
Selenium
100
12.5
Zinc
7,500
1610
Total Phosphorus
NA
22200
TKN
NA
44000
Ammonia -Nitrogen
NA
3330
Nitrate and Nitrite
NA
355
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
�t' xr •2l
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0037135
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvcic Data
US Biosolids, Inc.
NCO021181
City of Belmont
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
BEEMEEMEMEMEN
Manganese
----------
------------
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135
Facility Name: US Biosolids, Inc.
Residual Source WQ # or NCO020567
NPDES #:
WWTP Name: Yadkin Valley Sewer Authority
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
h
(m Ik r)
Sample or Composite Date
10-5-20
Percent Solids (%)
NA
2.91
Arsenic
75
17.2
Cadmium
85
3.45
Copper
4,300
614
Chromium
NA
3 2. 9
Lead
840
23.7
Mercury
57
0.717
Molybdenum
75
8.62
Nickel
420
17.2
Selenium
100
17.2
Zinc
7,500
614
Total Phosphorus
NA
33900
TKN
NA
65200
Ammonia -Nitrogen
NA
2690
Nitrate and Nitrite
NA
167
" For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0037135 Laboratory: 1) Waypoint Analytical
Facility Name: US Biosolids, Inc. 2)
Residual Source N00020567 3)
NPDES # or WQ#: 4
WWTP Name: Yadkin Valley Sewer Authority 5)
Residual Analvsis Data
Parameter
(mg/kg)
Sample or Composite Date
10-5-20
pH
6.1
Aluminum
52800
Calcium
3.45
Iron
27300
Magnesium
3660
Maganese
486
Potassium
4760
Sodium
2030
Sulfur
5930
PAN
20265
SAR
0.417
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature oT Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135 Laboratory: 1)
Facility Name: Town of North Wilkesboro 2)
Residual Source WQ # or NCO020761 3)
NPDES #: 4)
WWTP Name: Thurman Street WWTP 5)
Residual Analysis Data
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/kg}'
Sample or Composite Date
6-1-2020
Percent Solids (%}
NA
3.22
Arsenic
Cadmium
75
85
15.6
3.13
Copper
4,300
569
Chromium
NA
93.4
Lead
840
55.6
Mercury
57
2.73
Molybdenum
Nickel
75
420
11.5
33.8
Selenium
100
15.6
Zinc
Total Phosphorus
TKN
7,500
NA
NA
1660
22900
58400
Atnrnonia-Nitrogen
NA
9560
Nitrate and Nitrite
NA
263
For surface disposal facilities the ceiling concentration limits fisted in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for Knowing violations."
1)A.,
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ00037135
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
Town of North Wilkesboro
NCO020761
Thurmond Street W WTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
1 1
--
Organic N
Manganese
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signatufe of Preparer *
�, -;Q-;7- 1
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037135 Laboratory: 1)
Facility Name: U.S. Biosolids, Inc. 2)
Residual Source WQ # or N00025909 3)
NPDES #: 4)
WWTP Name: Town of Rutherfordton WWTP 5)
Residual Analvsis Data
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
m /k )a
Sample or Composite Date
4-30-20
Percent Solids (%)
NA
1.45
Arsenic
75
33.3
Cadmium
85
6.67
Copper
4,300
588
Chromium
NA
3 5. 2
Lead
840
26.9
Mercury
57
0.933
Molybdenum
75
16.7
Nickel
420
18.6
Selenium
100
313
Zinc
7,500
1050
Total Phosphorus
NA
14800
TKN
NA
91300
Ammonia -Nitrogen
NA
17100
Nitrate and Nitrite
NA
408
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signa6ke of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0037135
Facility Name: U.S. Biosolids, Inc.
Residual Source NCO025909
NPDES # or WQ#:
WWTP Name: Town of Rutherfordton WWTP
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
Magnesium
Potassium
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 25.24
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Dennis Key Owner: Dennis Key Predominant Soil Series: PbB2
Acres Used: 6.36 Acres Permitted: 6.36 Site #: NC-WK-DK Field #: 1
Residual Analysis Data (H
Sample or ? . ? f 3
Com-
posite
Date 10/5/20
Solids
2.91
Arsenic
17.2
Cadmium
3.45
Copper
614
�hrorniumj
32.9
Lead
23.7
Mercury
0.717
8.62
denum
Nickel
17.2
Selenium
17.2
Zinc
614
Total
Phos-
33900
Metals and Total Phosphorus use m
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
% Solids use Raw Percent #):
ota I
Ll
1 3 4]
5
61
7
8
9
70�
11°
12
DT/Ac./
Wl
APp,
0
as
L:vent
3.97
y
Arsenic
0.136
10.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.136
Cadmium
0.027
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Copper
4.873
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.873
--hromium
0.261
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.261
Lead
0.188
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.188
Mercury
0.006
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
denum
0.068
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.06$
Nickel
0.136
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.136
Selenium
0.136
0.000
0.000T 0.000
u00
0.000
0.0-00
0.000
0.000
0.000 1
0.000
0.000
0.136
Zinc
4,873
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.873
Total
Phos- 1269.030
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
269.03f
Dhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of lines and
imprisonment for knowing violations".
SignaPofnd Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-DK Acres Utilized. 6.36
Land Owner: Dennis Key Annual Dry Tons Applied. 25.2402 Site #: 1 Acres Permitted: 6.36
Operator: Dennis Key Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop I Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN:
L s
Volume applied
Volume
Residual Sources
soil
Precip.
a
<
c
z D
Nitrate
(enter one) Solids/
%
Applied PP per
(NPDES #, WQ#,
Cond.
past 24
n b
z
ry
l KN
and
Liquid
Solids
Acre
Fert.. Animal
(Dry.
Hrs,
o w
ti'
Nitrite
Cu. Yds Gallons
(DryTonslAc)
Waste. etc)
Wet.
Moist)
inches
Q
*
mg/kg
mglkg
mg/kg
3-2020
78000
2.91
1.488
NCO020567
dry
0
s
0.5
0.3
65200
2690
167
6-2020
78000
2.91
1.488
NCO020567
dry
0
s
0.5
0.3
65200
2690
167
9-2020
52000
2.91
0.992
NCO020567
dry
p
s 0.5 0.3 65200 2690 167
0.000
0.000
0.000
0.000
0.000
0.000
a.000
0.000
0.000
Residuals
Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS: 01 2080001
As
Cd
Cu
Cr
Pb
HR
Mo
Ni
Se
Zn I P
Annual lbs/acre
0.136
0.027
4.873
0.261
0.189
0.006
0.068
0.136
0.136
4.873 1269.0301
Prior Years Cumulative Ibs/ac
1.225
0.087
25.975
50.563
6.553
0.739
1.178
5.3
0.981
94.76
Current Cumulative lbs/ac
1.361
) 114
30.848
50.824
6.741
0.744
1.246
5,436
1.117
999N3
Permitted C. P. L. R.****
36
34
1338
1 NA
267
15
NA
374
89
2498
Permit PAN Limit I st/2nd Crop
lL
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I Crop 2
60.317 NA
60.317 NA
40.212 NA
0,000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0,000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
160,847 0.000
Crop 1
Crop 2
Fescue
Fescue
Fescue
Lime
Date
A lied
Ibs/ac
12-20
3000
194
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Q �y *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Cdigested -0.2
Signature of Land Applier Date Compost -0.1, anaerobiall y
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loadima Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Lee Walker Owner:
14.05 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Lee Walker Predominant Soil Series:
14.05 Site #: NC-WK-LW Field #:
32.50
FeB2-Fairview
I
Residual Analysis Data (Heavy Metals and Total Phosphorus use mt?/k2, % Solids use Raw Percent 9):
Com-
posite
DateTotal
Phos•11
'11
Annual heavy Nletal l+ield Loadln2s ICalculated in lbs/acre):
Total
1
21
3
4
5
5;
7�
8!
9
10 f
11
12 i
DT/Ac./
o
App.
rt
W.
Event
0.45
1.86
14
Arsenic
0.015
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Cadmium
0.003
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
0.551
2.121
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.673
Chromium
0.030
0.348
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.378
Lead
0.021
0.207
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.229
Mercury
0.001
0.010
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Molyb-
0.008
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.051
denum
Nickel
0.015
0.126
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.141
Selenium
0.015
1 0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Zinc
0.551
6.188
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.740
Total
Phos-
30.442
85.371
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
115.813
horus
ceruty, uuuer penalty of law, rnat ints aocumeni was prepares under my sirection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signatur of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc.
Land Owner: Lee Walker
Operator: Lee Walker
Crop I Name: Fescue
WQ Permit #: WQ0037135 Field #: NC-WK-LW
Annual Dry Tons Applied: 32.4935 Site #: 1
Predominant Soil Series: FeB2-Fairview
Crop I Max. PAN: 188 Crop 2 Name:
Acres Utilized: 14.05
Acres Permitted: 14.05
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
°
«� o
0
Volume applied
enter one Solids/
( )
Liquid
Cu, Yds GaIlOt15
o
/„
Solids
Volume
A lied cr
pp p'
Acre
D TonslAc
rY )
Residual Sources
(NPDES 4, V6 Q4.
Fert.. Animal
Waste. etc)
Soil
Cond.
(Dry,
wet
Moist)
Precip.
Past 24
11rs.
inches
,>
K �
� F,
* '
o
7� sv
v -
°
a
�
°i
F
TKN
m Ik
9 9
z D
3
o 3
�.
m 1k
9 9
Nitrate
and
Nitrite
m Ik
9 9
PAN Applied
( lbslacre)
Name of Crop IV
Receiving Residual
Application
Crop 1
p
Crop 2
p
Crop I
P
Crop 2
P
3-2020
45500
3.22
0.435
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
17.128
NA
Fescue
6-2020
149500
3.22
1.429
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
56.279
NA
Fescue
9.2020
52000
2.91
0.449
NCO020567
dry
0
s
0.5
0.3
65200
2690
167
18.203
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTAI.S:
01
247000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
1 P
91.609
0.000
Lime Applied
Annual lbslacre
0.074 0.015 2.673 0.378 0.229 0.011 0.051 0.141 0.074 6.740 115.913
0.047 0.012 3.217 0.633 0.281 0M08 0.051 0.234 0.044 9.144
0.121 0.027 5.890 1.011 0.510 0.019 0.102 0.375 0.118 15.884
36 34 1 1338 1 NA 267 15 NA 374 89 1 2498
F 188
Date
Ibs/ac
Prior Years Cumulative lbs/ac
0
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crap I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
)•-).C-:25
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 37.14
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Lee Walker Owner: Lee Walker Predominant Soil Series: FeB2-F2irview
Acres Used: 8.16 Acres Permitted: 8.16 Site #: NC-WK-LW Field #: 2
Residual
Com-
posite
Date
% Solids
Arsenic
Cadmium
Copper
-hromiurr
Lead
10/5/20
2.91
17.2
3.45
614
32.9
23.7
0.717
is Data
6/2/20
3.22
15.6
3.13
569
93.4
55.6
2.73
Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
8.62
11.5
denum
Nickel 17.2
33.8
Selenium 17.2
15.6
Zinc 614
1660
Total
Phos- 3390
222900
Dhorus
Annual Heavv Metal Field LoadinLys (Calculated in lh0avrol-
[otal 1'
2
3 4
5
6!
7
8
9°
1 D
11_
12I
DT/Ac.I
y
App.
a�
Event 1.45
3.10
Arsenic 0.050
0.097
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.147
Cadmium 0.010
0.019
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Copper 1.781
3.529
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.310
Chromium 0.095
0.579
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.675
Lead 1 0.069
0.345
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.414
Mercury 0.002
0.017
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.019
Molyb-
0.025
denum
0.071
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0 .000
a.oao
0.000
0.096
Nickel 0.050
0.210
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.260
Selenium 0.050
0.097
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.147
Zinc 1.781
10.295
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.200
0.000
0.000
12.076
Total
Mhos- 98.310
142.026
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
240.336
horus
1
"I rPrtifv Ilndi r
na l", ..F
i-, ♦l...a a6:,.
---- _
,µ...me... -- 11.'1'". a "I] %;[ uiy u I Vutlurl Ur supervision in accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sign ure of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-LW Acres Utilized: 8.16
Land Owner: Lee Walker Annual Dry Tons Applied: 37.1420 Site #: 2 Acres Permitted: 8.16
Operator: Lee Walker Predominant Soil Series: FeB2-Fairview Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 188 Crop 2 Name: Crop 2 Max. PAN:
y o
Volume applied
AP
enter one Solids/
{ )
Liquid
Cu. Yds Gallons
/o
Solids
Volume
Applied cr
pp p'
Acre
(Dry TonslAc)
Residual Sources
{NPDES #, WQ#,
Fert.. Animal
Wa te, etc)
Soil
Cond.
(Dry,
WeL.
Moist)
Precip.
Past 24
Hrs,
nches
>
K
rq
c �'
o
-
o'
v
TKN
mg/kg
Z a
o 3
ro o
w.
mg/kg
Nitrate
and
Nitrite
mglkg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3-2020
1
84500
3.22
1.390
NCO020761
dry
0
s
0.5
033
1 58400
9560
1 263
54.770
NA
Fescue
6-2020
104000
3.22
1.711
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
67.409
NA
Fescue
9-2020
97500
2.91
1.450
NCO020567
dry
0
s
0.5
0.3
65200
2690
167
58.765
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
o.000
0.000
0,000
0,000
0.000
0,000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTA1,S
0
28600o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
180.945T
0,000
Lime Applied
Annuallbs/acre
0.147
0.047
0.194
36
0,029
0.009
0.038
34
5.310
2.711
8.021
1 1338
0.675
0.574
1.249
1 NA 1
0.414
0.26
0.674
267 1
0.019
0,007
0,026
15
0.096
0.044
0.140
NA 1
0.260
0.227
0.487
374
0.147
0.043
0.190
1 89
12.076
6.372
18,448
2499
240.336
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
Current Cumulative lbs/ac
Permitted C. P. L. R,****
Permit PAN Limit I st/2nd Crop
18$
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
/j *Application Method: S - Surface, IN - Injection, INC - Incorporation
/ **Volatilization Rate: Surface- 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Lee Walker Owner:
17.7 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Lee Walker Predominant Soil Series:
17.7 Site #: NC-WK-LW Field #:
64.62
Fe62-Fairview
3
mestuuat A.natysts Data
(Heavy Metals and 'Total Phosphorus
use mg/kg,
% Solids use
Raw Percent #):
Sample or L 11
2
L31
L.4j
I6 E
7
8:
9
10
11
12
Com-
posite
Date 10/5/20
6/2/20
% Solids 2.91
3.22
Arsenic 17.2
15.6
Cadmium 3.45
3.13
Copper 614
569
Chromium 32.9
93.4
Lead 23.7
55.6
Mercury 0.717
2.73
Molyb-
8.62
denum
11.5
Nickel 17.2
33.8
Selenium 17.2
15.6
Zinc 614
1660
Total
Phos- 33900
22900
horus
Annual Heavy
Metal Field
Loadings
(Calculated
in Ibs7acre):
Total 1
2
3
4
5
6
7
8 1
9
10
11
12
DT/Ac./
App.
Event 0.45
3.21
Arsenic 0.015
0.100
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.115
Cadmium 0.003
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Copper 0.548
3.647
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.195
Chromium 0.029
0.599
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.628
Lead 0.021
0.356
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.378
Mercury 0.001
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Molyb0.008
denurn
denum
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Nickel 0.015
0.217
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.232
Selenium 0.015
0.100
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.115
Zinc 0.548
10.641
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.188
Total
Phos- 30.239
146.789
0,000
0.000
0.000
O.Ooo
0.000
0.000
0.000
0.000
0.000
0,000
177.028
horus
tli cP rfifi■, nrl av r.
..IL...,
1'1,.... aL.,a
�L__ ., _
_
- --- -- V- ----- %, "- 7 • •- r.aa t/1 Opal V unucl illy ulrecuon or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sign re of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-LW Acres Utilized: 17.7
Land Owner: Lee Walker Annual Dry Tons Applied: 64.6183 Site #: 3 Acres Permitted: 17.7
Operator: Lee Walker Predominant Soil Series: FcB2_Fairview Cation Exchange Capacity (non 503):
Crop I Name: Fescue Crop I Max. PAN: 188 Crop 2 Name: Crop 2 Max. PAN:
Volume applied
Volume
Residual Sources
Soil
a
o<
>o
Nitrate
� >=
(enter one) Solids/
%
Applied per
p
(Nf DF-.S #, WQ#.
Cond.
2
Past _4
�
a
v
TKN
c E
and
Liquid
Solids
Acre
Fert.. Animal
(Dry.
lirs.
c w
Nitrite
Cu. Yds Gallons
(Dry Tons/Ac)
Waste. etc)
Wet.
MoIS1)
nches0
Q
o
mg/kg
mglkg
mg/kg
3-2020
195000
3.22
1.479
NCO020761
drn
0
s
0.5
0.3
58400
9560
263
6-2020
227500
3.22
1.726
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
9-2020
65000
2.91
0 446
NCO020567
A",
0
. s 0.� 0.3 65200 2690 167
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals
Applications totals
on FORM FSF
supp ( attach
FORM
FSF supp to this form):
TOTALS: 0 487500
As
Cd
Cu Cr
Pb Hg
Mo
Ni
Se Zn P
Annual Ibs/acre
0.115
0.023
4.195 0.628
0.378 0.018
0.081
0.232
0.115 11.188 17T028
Prior Years Cumulative Ibs/ac
0.05
0.013
3.501 0.669
0.3 0.009
0.054
0.247
0.048 10.037
Current Cumulative lbs/ac
0.165
0.036
7.696 1.297
0.678 0.027
0.135
0.479
0.163 21.225
Permitted C. P. L. R.****
36
34
1338
NA
267
15
NA
374
89
1 2498
Permit PAN Limit 1st/2nd Crop
LL
PAN Applied
Name of Crop Type
{ lbs/acre)
Receiving Residual
Application
Crop 1 Crop 2
Crop 1
Crop 2
58.269 NA
Fescue
6T981 NA
Fescue
18.061 NA
Fescue
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
144.31 f 0.000
Lime
Applied
Date
lbs/ac
0
188
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
- *Application Method: S - Surface, 1N - Injection, INC - Incorporation
�� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
William Porter Owner:
29.35 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
William Porter Predominant Soil Series:
29.35 Site #: NC-WK-BP Field #:
66.89
FeB2-Fairview
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mR/kii, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 i
10/5/20
2
6/2/20
3
4
5
6
7
$ l
9a
10
l
12
% Solids
2.91
3.22
Arsenic
17.2
15.6
Cadmium
3.45
3.13
Copper
614
569
Chromium
32.9
93.4
Lead
23.7
55.6
Mercury
0.717
2.73
Molyb-
denum
8.62
11.5
Nickel
I T2
33.8
Selenium
17.2
15.6
Zinc
614
1660
Total
Phos-
horus
33900
22900
Annual Heavy Metal hield Loadintrs (Calculated in lbs/acre):
Total
L1'
2
3
L 4
5
6_
7
$i
9
10
11
12;
DT/Ac./
o
App.
rt
Event
0.94
1.34
"
Arsenic
1 0.032
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Cadmium
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
1,156
1.523
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.678
Chromium
0.062
0.250
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.312
1_ead
0.045
0.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.193
Mercury
0.001
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.016
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
denum
Nickel
0.032
0.090
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.123
Selenium
0.032
0.042
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.074
Zinc
1.156
4.442
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 5.598
Total
Phos-
63.800
61.280
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
125.080
horus
-1 certify, under penalty of iaw, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
a- 3.4-; 1
Signatur of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-BP Acres Utilized: 29.35
Land Owner: William Porter Annual Dry Tons Applied: 66.8816 Site #: 2 Acres Permitted: 29.35
Operator: William Porter Predominant Soil Series: FeB2-Fairview Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 188 Crop 2 Name: Crop 2 Max. PAN:
o
N
u °
p
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
D TonS1AC
( )
ResiduaI Sources
(NPDES #, 1k'Q#,
Fort., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet.
Moisl)
Precip.
Past 24
Hrs.
inches
>
�» v
Q W
o
o
d
4
_
0
;0
w
*
w
'lKN
m !k
9 9
=
�'
�o o
a �.
m Ik
9 9
Nitrate
and
Nitrite
rn !k
9 9
PAN Applied
pp
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
P
Crop 2
P
Crop 1
p
Crop 2
P
3-2020
227500
2.91
0.941
NCO020567
dry
0
s
0.5
0.3
65200
2690
167
38.122
NA
Fescue
6-2020
292500
3.22
1.338
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
52.710
NA
Fescue
0.000
0,000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0,000
0.000
0.000
0,000
0,000
0.000
0.00a 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
520000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
90.833 1
0.000
Lime Applied
Annuallbs/acre
0.074
0.015
2.678
0.312
0.193
0.009
0.047
0.123
0.074
5,598
125.080
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.144
0.218
36
0.029
1 0.044
34
7.032
9.710
1 1338
1.109
1.421
NA
0.586
0.779
1 267
0.021
0.030
15
0.099
0.146
NA
2.506
2.629
374
0.081
0.155
89
15.516
21.114
2498
12-2020
2000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PANT Limit 1 st/2nd Crop
1
188
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
eJA1r *Application Method: S - Surface, IN - Injection, INC - Incorporation
?�-�� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date k** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
W Q003 713 5
W i I I iam Porter Owner
13.36 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
William Porter Predominant Soil Series:
13.36 Site #: NC-WK-BP Field #:
31.74
FeB2-Fairview
3
Residual Analvsis Data (Heavv Metals and 'Total Phosphorus use mg/kg. % Solids use Raw Percent HI!
Com-
posite
-.-Date1
Total
' .
�+
•11
•11
Annual rieav_v Metal Vield Loadings (Ualeulated in lbs/acre):
Total
1?
21
3
4
5
6
7
8
9
10
l l
12
DT/Ac./
o
App.
Event
1.00
1.37
Arsenic
0.035
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.077
Cadmium
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
1.233
1.561
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.794
Chromium
0.066
0.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.322
Lead
0.048
0.153
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.200
Mercury
0.001
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.017
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
denum
Nickel
0.035
0.093
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.127
Selenium
0.035
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.077
Zinc
1.233
4.555
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.788
"Total
Phos-
68.071
62.838
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
130.909
horus
I ceriuy, under penany of iaw, may ims aocumen[ was preparea under my airection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
_ V �� -
Sig ure of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-BP Acres Utilized: 13.36
Land Owner: William Porter Annual Dry Tons Applied: 31.7372 Site #: 3 Acres Permitted: 13.36
Operator: William Porter
Crop 1 Name: Fescue
Predominant Soil Series: FeB2-Fairview
Crop 1 Max. PAN: 188 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
ce O
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry TonslAc)
Residual Sources
(NPDES #. WQ#•
Fert., Animal
Waste, etc)
Soil
(Dry..
Moist)
Precip.
Past 24
Hrs•
iriches
D
T
� n
?
o
m °
r^n -
� w
a
TKN
mg/kg
z
c
rt �
a
rngtkg
Nitrate
and
Nitrite
mgikg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
3-2020
110500
2.91
1.004
NCO020567
dry
0
s
0.5
0.3
65200
1 2690
167
40.678
NA
Fescue
6-2020
136500
3.22
1.372
NCO020761
dry
0
s
0.5 1
0.3
58400
9560
263
54.039
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
247000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
94.717
0.000
Lime Applied
Annuallbs/acre
0,077
0.016
2.794
0.322
0.200
0.009
0.049
0.127
0.077
5.788
130.9091 1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.053
0.008
2,113
0.206
0.192
0.008
0.028
0.93
0.023
4.229
12-2020
1000
Current Cumulative lbs/ac
0.130
0.024
4.907
0.528
0.382
0.017
0.077
1.057
0.100
10.016
Permitted C. P. L. R.****
36
34
1338
1 NA
267
15
1 NA
1 374
89
2498
Permit PAN Limit 1st/2nd Crop
188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, 1N - Injection, INC - Incorporation
Jl _Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc. Total Dry Tons Applied (Annual):
WQ0037135 Cation Exchange Capacity (non 503 only):
William Porter Owner:
26.6 Acres Permitted:
26.17
William Porter Predominant Soil Series: FeB2-Fairview
26.6 Site #: NC-WK-BP )Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1?
6/2/20
2 j
3j
5
6
7j
81
9
10
11
121
Solids
3.22
Arsenic
15.6
Cadmium
3.13
Copper
569
Chromium
93.4
Lead
55.6
Mercury
2.73
Molyb-
denum
1 ! 5
Nickel
33.8
Selenium
15.6
Zinc
1600
Total
Phos-
horus
22900
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1;
21
3
4
5;
6 j
7
S
9
10
11
12 I
0
DT/Ac./
0
App.
Event
0.98
Arsenic
0.031
0.000
0.000
1 0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.031
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.120
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.120
Chromium
0.184
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.184
Lead
0.109
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.109
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
denum
Nickel
0.067
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Selenium
0.031
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.031
Zinc
3.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.149
Total
Phos-
45.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
45.067
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zj �� -
Signal re of Land Applie
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: LDS Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-WK-BP Acres Utilized., 26.6
Land Owner: William Porter Annual Dry Tons Applied: 26.1834 Site #: 4 Acres Permitted: 26.6
Operator: William Porter Predominant Soil Series: FeB2-Fairview Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max, PAN: 188 Crop 2 Name: Crop 2 Max. PAN:
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
ado
Solids
Volume
Applied per
Acre
(Dry TonslAc)
Residual Sources
(NPDES #, WQ#,
Fert., Anima]
Waste, etc)
Soil
Cond.
(Dry'
Wet.
Moist)
Precip.
Past 24
Firs.
inches
Y
K a
f �
a �
o
o
K.
� =
;v
�,
o'
0
1'KN
mglkg
D
q'
o 3
(M o
-'
mglkg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
6-2020
195000
3.22
0.984
NCO020761
dry
0
s
0.5
0.3
58400
9560
263
38.773
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
IUFAL.S:
01
195000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
38.773
0.000
Lime Applied
Annual Ibs/acre
0.031
0.006
1.120
0.184
0.109
0.005
0.023
0.067
0.031
3.149
45.067
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.206
0.039
8.96
1.669
0.755
0.028
0.134
3.361
0.115
17.329
12-2020
2000
Current Cumulative lbslac
0.237
0.045
9.980
1.853
0.864
0.033
0.157
3.428
0.146
20.477
Permitted C. P. L. R.****
36
34
1338
NA
267
15
1 NA
374
89
2498
Permit PAN Limit 1st/2nd Crop
1 1 188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, 1N - Injection, INC - Incorporation
1 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
14
%* Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobialIy digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Charles Killian Owner:
4.3 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Charles Killian Predominant Soil Series:
4.3 Site #: NC-GA-MH Field #:
6.42
CeB2
0204
Residual Analvsis Data (Heavv Metals and Total Phosphorus use mtJke. % Solids use Raw Percent #1:
Sample or
Com-
posite
Date
_i
8/18/20
2
3
4
5
6
7
8
9
1C
11 '
12
% Solids
3.95
Arsenic
12.5
Cadmium
2.5
Copper
343
Chromium
91.8
Lead
31.3
Mercury
0.973
Molyb-
denum
6.25
Nickel
23.2
Selenium
12.5
Zinc
1610
Total
Phos-
horus
22200
Annual Heavv ivietal viela Loacltnes t( alculated in lbslacrel:
Total
1 ':
2 i
3
4;
5
6
7
8
9 i
10
11
12
DTIAc.I
a
App.
m
Event
1.49
Arsenic
0.037
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.037
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.025
Chromium
0,274
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.274
Lead
0,094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Mercury
0,003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
denum
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Nickel
0.069
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 j
0.000
0.000
0.000
0.069
Selenium
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Zinc
4.811
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.811
Total
Phos-
66.334
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
66.334
horus
■ LGl tuy, UtIUCE- PCHUlly to law, teal tnt9 uocument was preparea unaer my atreetlon or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sign?reofnd ApplierinDate
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc.
Land Owner: Charles Killian
Operator: Charles Killian
Crop 1 Name: Fescue
WQ Permit #: WQ0037135 Field 4: NC-GA-MH-2
Annual Dry Tons Applied: 6.4239 Site ##: 4
Predominant Soil Series: CeR2
Crop I Max. PAN: 209 Crop 2 Name:
Acres Utilized: 4.3
Acres Permitted: 4.3
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
❑
Volume applied
(enter one) Solids/
Liquid
q
Cu, Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry TonslAc)
Residual Sources
(NPDES 4. WQ4.
Fert.. Animal
Waste_ etc)
Soil
Cond.
(Dry,
Wet.
Moist)
Precip.
Past 24
11rs.
inches
>
K �
a
o
a =
o
N
# ?
K
z
i;
*
TKN
mgrkg
z >
= 9
o
'
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10-2020
39000
3.95
1.494
NCO021181
dry
0
s
0.5
0.3 1
44000
3330
355
42.490
NA
Fescue
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
o.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
39000
As
Cd
Cu
Cr
Pb
H F
Mo
Ni
Se
Zn
P
I 42.490
0.000
Lime Applied
Annuallbs/acre
0.037
0.007
1.025
0.274
0.094
0.003
0.019
0.069
0.037
4.811
66.334_1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.014
0.007
2.382
1.219
0.119
0.004
0.055
0.145
0.024
3.924
12-20
2000
Current Cumulative Ibs/ac
0.051
0.014
3.407
1.493
0.213
0.007
0.074
0.214
0.061
8.735
Permitted C. P. L. R.****
36
34
1338
1 NA
1 267
15
1 NA
374
1 89
2498
Permit PAN Limit 1st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Charles Killian Owner:
24.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Charles Killian Predominant Soil Series:
24.6 Site #: NC-GA-MH Field #:
34.27
CeB2
0205
Residual Analvsis Data (Heavy Metals and Total Phosahorus use mg/k2, % Solids use Raw Percent #):
Com-
posite
Date:
t
Total
phorusPhos-
M
ENNEEMENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibslacre):
Total
1
2J
3 1
L 4
LIJ
S 1
9
10
11
12
DT/Ac./
c
App.
Event
1.39
Arsenic
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.956
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.956
Chromium
0.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.256
Lead
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0A00
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
morn ]enum
Nickel
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Selenium
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Zinc
4.485
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.485
Total
Phos-
61.849
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
61.849
horus
"f certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
9- Is'Z1
Signa re of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-GA-MH-2 Acres Utilized: 24.6
Land Owner: Charles Killian Annual Dry Tons Applied: 34.2607 Site #: 5 Acres Permitted: 24.6
Operator: Charles Killian
Predominant Soil Series: CeB2
Crop I Name: Fescue Crop I Max. PAN: 209 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o -
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
ova
Solids
Volume
Applied per
Acre
D Tons1AC
(Dry )
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste_ etc)
Soil
Cond.
(Dr,'
Wet.
Moist)
Precip.
Past 24
Hrs.
inches
D
0
°
S
m w
N
TKN
m Ik
9 9
z n
o3
o
2.
m !k
9 9
Nitrate
and
Nitrite
m Ik
9 9
PAN Applied
( Ibslacre)
Name of Crop Type
Receiving Residual
Application
crop1
crop2
Crop 1
P
Crop 2
P
10-2020
208000
1 3.95
1.393
NCO021181
dry
0
s
0.5
0.3
44000
3330
1 355
39.612
NA
Fescue
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
0
208000
As
Cd
Cu
Cr
Pb
Rg
Mo
Ni
Se
7.,n
P
39.612
0,000
Lime Applied
Annuallbs/acre
0.035
1.379
1.414
36
0.007
0.16
0.167
34
0956
24.022
24,978
1338
0.256
7.038
7,294
1 NA
0.087
3.174
3,261
267
0.003
0.111
0.114
15
0.017
0.637
0.654
NA
0.065
15.203
15.268
374
0.035
0.179
0.214
89
4.485
65.867
70.352
2498
61.849
Date
Ibs/ac
Prior Years Cumulative lbslac
12-20
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.**** 1
Permit PAN Limit Ist/2nd Crop 1
209
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
41 . -24- ?
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 0.72
Permit #:
Operator:
Acres Used:
WQ0037135
Norman McDaniel
4.3
Cation Exchange Capacity (non 503 only):
Owner: Evelyn Davis Predominant Soil Series:
CaB2
Acres Permitted: 4.3 Site #: NC-RU-RD Field #: IA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
615120
L21
3j
4€
5_
6,
7
B;
9
10
11
12
% Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium.62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
horus
9330
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total1
41
5
6
L7J
S,
L9l
10,`
111
12!
DT/Ac./
o
App-
in
Event
0.17
"
Arsenic
1 0.008
0.000
0.000
1 0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.008
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Chromium
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Lead
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
enum
Nickel
0.021
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Selenium
0.004
1 0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Zinc
0.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.105
Total
Phos-
3.135
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.135
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signat e of Land Applier
?•:).r► a1
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-RD Acres Utilized: 4.3
Land Owner: Evelyn Davis Annual Dry Tons Applied: 0.7210 Site #: 1A Acres Permitted: 4.3
Operator: Norman McDaniel Predominant Soil Series: CaB2 Cation Exchange Capacity (non 503):'
Crop 1 Name: Fescue Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
° s
° °
Volume applied
Pp
(enter one) Solids/
Liquid
Yds Gallons
%
Solids
Volume
Applied per
Acre
o ronslAc
( ry 1
Residual Sources
(NPDES 4, WQ#.
Fert.. Animal
waste. etc)
Soil
Coed_
(Dry.
Wei.Cu.
Moist)
Precip.
Past 24
Hrs.
ncnes
>
a -
a FS'
o �
=
a
R
r. _
TKN
m !k
9 9
z
c
m �k
9 9
Nitrate7PANAppliedName
andReceiving
NitriteApplication
m �k
9 9P
of Crop Type
Residual
2
Cro I
p
Cro 2
P
8-2020
45500
0.38
0.168
NCO020664
dry
0
s
0.5
0.3
129000
31800
1700
15.681
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTAt.S-
01
45500
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
15.681
0.000
Lime Applied
Annual Ibslacre
0.008
0.008
0.044
0.021
0.025
0.001
0.021
0.021
0.004
0.105
3.135
1
Date
lbslac
Prior Years Cumulative ibs/ac
0
0.009
36
0
0.008
34
0
0.044
1338
0
0.021
NA
0
0.025
267
0
0.001
15 1
0
0.021
NA
0
0.021
374 J
0
0.004
89
0
0.105
2498
12-2020
2000
Current Cumulative lbslac
Permitted C. P. L. R.****
Permit PAN Limit Istl2nd Crop
1 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applies! (Annual): 31.18
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Norman McDaniel Owner: Evelyn Davis Predominant Soil Series:
Acres Used: 29.3 Acres Permitted: 29.3 Site #: NC-RU-RD Field #:
CaB2
1B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
615120
2
4/30/20
3
a
5
S
7
8
9
10
11j
12
%Solids
0.38
1.45
Arsenic
25
33.3
Cadmium
25
6.67
Copper
131
588
Chromium
62.5
35.2
Lead
75
26.9
Mercury
3.83
0.933
Molyb-
denum
62.5
16.7
Nickel
62.5
18.6
Selenium
12
33.3
Zinc
313
1050
Total
Phos-
horus
9330
14800
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3 j
5
6i
7
SJ
9
10 J,11
12
DT/Ac./
0
App.
y
Event
0.31
0.75
Arsenic
0.016
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Cadmium
0.016
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Copper
0.082
0.883
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.965
Chromium
0.039
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Lead
0.047
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
Mercury
0.002
0.001
0.000
0.000 11
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.039
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
denum
Nickel
0.039
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Selenium
0.008
1 0.050
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.058
Zinc
0.196
1.577
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.773
Total
Phos-
5.841
22.230
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
28.070
norus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
V. zeal
Signatur f Land Appi er Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc.
Land Owner: Evelyn Davis
Operator: Norman McDaniel
WQ Permit #: WQ0037135 Field #: NC-RU-RD
Annual Dry Tons Applied: 31,1682 Site #: 1B
Predominant Soil Series: CaB2
Crop 1 Name: Fescue Crop I Max. PAN:
209
Crop 2 Name:
Acres Utilized: 29.3
Acres Permitted: 29.3
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
L r
°y
0
Volume applied
(enter one) Solids/
l,ipuid
Cu. Yds Gallons
%
Solids
Volume
pe
Applied per
Acre
(Dry TGns/Ac)
Residual Sources
(NPDES #, WQ##,
Pert.. Animal
Waste. etc)
Soil
Cond.
Wei''
Moist)
Precip.
past 24
Hrs.
inches
D
w
o
w
„ _
* ^'
0
* R
'TKN
mg/kg
z n
"'
a o
w
mglkg
Nitrate
and
Nitrite
mglkg
PAN Applied
(]bs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
4-2020
364000
1.45
0.751
NCO025909
dry
0
s
0.5
0.3
91300
17100
408
46.900
NA
Fescue
8-2020
338000
0.38
0.183
NCO020664
dry
0
s
0.5
0.3
129000
31800
1700
17.095
NA
Fescue
9-2020
240000
0.38
0.130
NCO020664
dry
0
s
0.5
0.3
129000
31800
1700
12.139
NA
Fescue
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
94200ol
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
76.134
0.000
Lime Applied
Annuallbs/acre
0.066
0.026
0.965
0.092
0.087
0.004
0.064
0.067
0.058
1.773
28.070
Date
lbs/ac
Prior Years Cumulative Ibs/ac
0
0
0
t)
0
0
0
0
0
0
12-2020
2000
Current Cumulative ]bs/ac
0.066
0.026
0.965
0.092
0.087
0.004
0.064
0.067
0.058
1.773
Permitted C. P. L. K.****
36
34
1 1338
1 NA 1
267
1 15
1 NA 1
374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
�Z- 7.6`21
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total pry Tons Applied (Annual): 7.19
Permit #:
Operator:
Acres Used:
WQ0037135
Norman McDaniel
19.6
Cation Exchange Capacity (non 503 only):
Owner: Evelyn Davis
Acres Permitted: 19.6 Site #:
Predominant Soil Series:
NC-RU-RD Field #:
CaB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
6/5/20
2 !
3
4
5
6
7
8!
9_
10 ;
11 ;
12
% Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium
62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
horus
9330
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
L9
10
11
12
DT/Ac./
o
App.
Event
0.37
Arsenic
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Cadmium
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Copper
0.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Chromium
0.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Lead
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
denum
0.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Nickel
0.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Selenium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Zinc
0.230
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.230
Total
Phos-
6.848
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.848
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
-.;.,C'd I
Sign re of Land Applier
Date
DFNR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-RD Acres Utilized., 19.6
Land Owner: Evelyn Davis Annual Dry Tons Applied: 7.2099 Site #: 2 Acres Permitted: 19.6
Operator: Norman McDaniel Predominant Soil Series. CaB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
i
G
Q
Volume applied
enter one) Solids/
( ) �
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied r
pp per
Acre
(Dry Tons/AC)
Residual Sources
(NPDES 4, WQ4.
Fert., Animal
Waste. etc)
SOil
Cond.
(Dry.
Wet.
Moist)
Precip.
Past 24
Hrs,
tnehes
>
K b
n'
p
°
o
t7 -
w
-
a0
K
z
�`
TKN
mg/kg
z >
� D
E o
n w.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
(Ibs/acre}
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
4-2020
214500
0.38
0.173
NCO020664
dry
0
s
0.5
0.3
129000
31800
1700
16.218
1 NA
Fescue
9-2020
240500
0.38
0.194
NCO020664
dry
0
s
0.5
0.3
129000
31800
1700
18.184
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
T--45-5000l
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
34.402
0.000
Lime Applied
Annuallbs/acre
0.018
0
0.018
36
0.018
0
0.018
34
0.096
0
0.096
1338
0,046
0
0.046
NA
0.055
0
0.055
267
0.003
0
0.003
15
0.046
0
0.046
NA
0.046
0
0.046
374
0.009
0
0.009
89
0.230
0
0.230
2498
6.848
Date
lbs/ac
Prior Years Cumulative lbs/ac
12-2020
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
209
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
Total Dry Tons Applied (Annual): 25.84
WQ0037135 Cation Exchange Capacity (non 503 only):
Larry Bailey Owner: Larry Bailey Predominant Soil Series:
$ Acres Permitted: 8 Site #: NC-RU-LB
Field #:
PbB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1 /23/20
2
3j
4j
5
6,
11
9<
10
11
12
% Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1 123
Total
Phos-
horus
832.2
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4i
5
6!
8
9;
10
Ill',
12
DTIAc.I
_7j
c
APp-
W.
Event
3.23
14
Arsenic
0.020
1 0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.020
Cadmium
0.019
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Copper
1.505
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.000
0.000
1.505
Chromium
######
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
#####gii
Lead
0.304
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.304
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Nickel
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Selenium
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Zinc
7.255
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.255
Total
Phos-
5.376
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.376
horus
-1 ceruly, under penatry of Eaw, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
9. 74- ar
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-LB Acres Utilized: 8
Land Owner: Larry Bailey Annual Dry Tons Applied: 25.8463 Site ##: 1 Acres Permitted: 8
Operator: Larry Bailey
Crop I Name: Fescue
Predominant Soil Series: PbB2
Crop 1 Max. PAN: 178
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
°
:3
cd °
❑
2-2020
Volume applied
(enter one) Solids/
Li Liquid
9
Cu. Yds Gallons
77
%
Solids
15.5
Volume
Applied er
p
Acre
(Dry TonslAcj
1.256
Residual Sources
(NPllES #. WQ#.
Fert... Animal
Waste. etc)
NCO025984
Soil
Cond.
(Dry.
Wet,
]Moist)
dry
Precip.
Past 24
Itrs.
inches
0
Y
K
o �
"•
s
o
v -
-
* N"
0.5
z
D
b
0.3
TKN
mglkg
47112
z Y
o �
a I"
mgAg
14452
Nitrate
and
Nitrite
mgtkg
72258
PAN Applied
(lbslacre)
Name of CropType
yp
Receiving Residual
Application
Crop I
44.594
Crop 2
NA
Crop 1
fescue
Crop 2
4-2020
55
15.5
0.897
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
31.853
NA
Fescue
10-2020
66
15,5
1.077
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
38.224
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
OAOo
0.000
0.000
0.000
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 c�rALS:
1ys
0
As
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form)-
Cd Cu Cr Pb H Mo Ni Se Zn P
I14.671
0.000
Lime Applied
Annuallbs/acre
0.020
0.019
1.505
#######
0.304
0.001
0.032
0.062
0.023
7.255
5.376
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.063
0.083
36
0.052
0.071
34
3.379
4.884
1338
0.487
#######
NA
0.952
1.256
267
0.005
0.006
15 1
0.101
0.133
NA
0.208
0.270
374 1
0.4
0.423
89
13.22
20.475
2498
12-2020
1000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
178
--i certify, unaer penalty of law, tnat tnis document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - incorporation
V- ;Lr 2 **Volatilization Rate: Surface- 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 47.39
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series: PbB2
Acres Used: 11.7 Acres Permitted: 11.7 Site #: NC-RU-LB Field #: 2
Residual Analvsis Data (Heavv Metals and Total Phn.cnhnriur, lisp mo/kn_ 0/,, cnlirle t,eP Raw PPMnPnt fdl•
Sample or
Com-
posite
Date
1;
1 /23/20
2
3
4 i
5!
6 1
7
8;
V 9
10�
11
12
% Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1123
Total
Phos-
horus
832.2
Hunuai rxeavy ivietai rxem i,oaotn2s tt,afcuiatea in ins/acrel:
Total
L 1
2
3
4
5
6!
7
8
9
10E
11
12
DTIAc.I
--
-
App.
Event
4.05
Arsenic
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.025
Cadmium
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Copper
1.887
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.887
Chromium
######
0.000
0.000
0.000
0.000
0.000
o.000
0.000
0.000
0.000
0.000
0.000
######
Lead
0.382
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.382
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.000
0.000
0.000
0.002
Molyb-
denum
0,041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Nickel
0.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.077
Selenium
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
"Zinc
9.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.000
o.000
0.000
0.000
9.096
Total
Phos-
6.741
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.741
horus
IWLA aiy, UNKAVI 11VINtrty M inw, tnat ims uocument was preparea unaer my airectton or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
SignPeofandApplier
Date
DENR FORM MFLSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-LB Acres Utilized: 11.7
Land Owner. Larry Bailey Annual Dry Tons Applied: 47.3849 Site #: 2 Acres Permitted: 11.7
Operator: Larry Bailey Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop l Name: Fescue Crop I Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
:3 c
�CL
Volume applied
Pp
(enter one) Solids/
Liquid
3
Cu. Yds Gallons
��a
Solids
Volume
A 1�� d cr
PP ie p'
Acre
(Dry TonslAc)
Residua] Sources
(NPDES #, WQ#.
Fert.. Animal
Waste, etc}
Soil
Cond•
(Dry,
5
Wet
Moist)
Precip.
Past 24
lirs.
inches
-a
K -e
_
� n'
o
o
_
�, -
-��.
�
N
TKN
mglkg
�_ ?
o E
Ro °
m
mglkg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lhs/acre)
Name o!'Crop �1'ype
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
3-2020
220
15.5
2.455
NCO025984
dry
0
s
1 0.5
0.3
1 47112
14452
722,58
87.119
NA
Fescue
4-2020
77
15.5
0.859
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
30.492
NA
Fescue
11-2020
66
15.5
0.736
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
26,136
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
3631
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
143.7471
0.000
Lime A lied
Annuallbs/acre
0.025
0.023
1.887
#######
0.382
0.002
0.041
0.077
0.029
9.096
6.741
Date
Ibs/ac
Prior Years Cumulative lbs/ac
0.068
0.093
36
0.054
0.077
34
3.564
5.451
1338
0.52
#######
NA
0.996
1.378
267
0.005
0.007
15
0.105
0.146
NA
0.215
0.292
374
0.408
0.437
89
€4.009
23.105
2498
0
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit ] st/2nd Crop
17S
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
9. 24 f
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.. Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 11.49
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series:
Acres Used: 4.4 Acres Permitted: 4A Site #: NC-RU-LB Field #:
PbB2
3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1 /23/20
2
L3J
L_4E
5
6�
7
S
9'
10
11
12
Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1123
Total
Phos-
horus
832.2
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
L1
2
3
a
5'
6'
7,
8'
9'
1fl;
11'
12'.
13TIAcJ
_.
�
_..
-
y
0
App.
Event
2.61
Arsenic
1 0.016
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0,000
1 0.000
0.016
Cadmium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
1.217
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.217
Chromium
######
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Lead
0.246
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.001
Molyb-
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
denum
Nickel
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Selenium
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
5.864
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.864
Total
Phos-
4.346
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.346
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
9- 2.c- a N
Signate re of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-LB Acres Utilized: 4.4
Land Owner: Larry Bailey Annual Dry Tons Applied: 11.4872 Site #: 3 Acres Permitted: 4.4
Operator: Larry Bailey Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop i Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
L
v
Q°
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry1ons/AC)
Residual Sources
(NPDES #, WQ#,
Fert., Anima]
Waste, etc)
Soil
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
11rs.
inches
D
� �
F 1G
o w
a "
o
w
N
�'
w
N
7
`hKN
mglkg
z Y
�'
°
w•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
f Ihs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
7-2020
88
15.5
2.611
NC0025984
dry
0
s
0.5
0.3
47112
14452
722.58
92.663
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
88
0
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
92.663 1
0.000
Lime App lied
Annuallbs/acre
0.016
0.048
0.064
36
0.015
0.031
0.046
34
1.217
2.508
3.725
1338
#######
0.398
#######
NA
0.246
0.649
0.895
267
0.001
0.005
0,006
15
0.026
0.064
0.090
NA
0.050
0.122
0,172
374
0.019
0.202
0.221
89
5.864
10.283
16.147
2498
4,346
Date
lbs/ac
Prior Years Cumulative lbs/ac
12-2020
1000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit i st/2nd Crop I
E�
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
1-1
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 21.54
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series: PbB2
Acres Used: 5.4 Acres Permitted: 5.4 Site #: NC-RU-LB Field #: 4
Residual
Analysis
Data (Heavy
Metals and Total Phosphorus
use mg/kg,
% Solids
use
Raw Percent #):
Sample or
1
2
4
5'
6'
7
8;
9
10
11 ,
12
Com-
posite
Date
1/23/20
% Solids
15.5
Arsenic
3,11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
5.03
denum
Nickel
9.55
Selenium
3.63
Zinc
1123
Total
Phos-
832.2
horus
Annual
Heavy
Metal Field
Loadings (Calculated
in Ibs/acre):
Total
2
3 41
5
6 E
7 j
8 z
9.
90..E
11 °
12
DT/Ac./
°
App-
r4
Event
3.99
Arsenic
1 0.025
0,000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Cadmium
0.023
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Copper
1.858
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.858
Chromium
###4##
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
#4#94#
Lead
0.376
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.376
Mercury
0.001
0.000
0.000 0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.00.1
Molyb-
0.040
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
denum
Nickel
0.076
0.000
0,000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
Selenium
0.029
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Zinc
8957
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.957
Total
Phos-
6.638
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6,638
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
__ 4W4 *�
Signiure of Land Applier
Date
DFzNR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc.
Land Owner: Larry Bailey
Operator: Larry Bailey
Crop 1 Name: Fescue
WQ Permit #: WQ0037135 Field #: NC-RU-LB
Annual Dry Tons Applied: 21.5386 Site #: 4
Predominant Soil Series: PbB2
Crop 1 Max. PAN:
178
Crop 2 Name:
Acres Utilized: 5.4
Acres Permitted: 5.4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 o
❑
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert.. Animal
Waste. etc)
Soi1
(Dry
Wet,�.
Moist)
Precip.
Past 24
Hrs.
inehes
a
�
o
w m
77
q
�'
TKN
mglkg
z D
mglkg
Nitrate
and
Nitrite
mg/kg
PAN A lied
(lbslacpe )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
4-2020
77
15.5
1.861
NC0025984
dry
0
s
0.5
0.3
47112
14452
722.58
66.066
NA
Fescue
7-2020
88
15.5
2.127
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
75.503
NA
Fescue
0.000
0.000
0.000
0.000
0,000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-4
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
165
01
As
Cd
Cu
Cr
Pb
I l l
Mo
Ni
Se
Zn
P
141.569
0,000
Lime Applied
Annual Ibs/acre
0.025
0.023
1.858
#######
0.376
0,001
0.040
0.076
0.029
8.957
6.638
Date
Ibs/ac
Prior Years Cumulative lbs/ac
0.051
0.033
2.64
0.419
0.683
0.005
0,068
0.128
0.212
10.822
12-2020
1000
Current Cumulative Ibs/ac
0.076
0.056
4.498
#######
1.059
0.006
0.108
0.204
0.241
19.779
Permitted C. P. L. R.****
36
34
1 1338
1 NA
267
15
NA
1 374
89
2498
Permit PAN Limit ist/2nd Crop
178
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Forth to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 1292
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series: PbB2
Acres Used: 4.6 Acres Permitted: 4.6 Site #: NC-RU-LB Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1_
1 /23/20
?J
L3Ja
i
5
6
7 j
8 I
9 s
14
11
12
% Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1123
Total
Phos-
horus
832.2
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1
2
3
4;
5 1
6;
71
8�
9
1 Q
11
12
D'f/Ac./
o
App.
Event
2.81
Arsenic
0.017
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.017
Cadmium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
1.309
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.309
Chromium
4#4#9#
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000#
Lead
0.265
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.265
Mercury
1 0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
denum
Nickel
0.054
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.054
Selenium
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Zinc
6.309
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
6.309
Total
Phos-
4.675
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.675
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signatu of Land Applier
�.;?C. j �
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-LB Acres Utilized: 4.6
Land Owner: Larry Bailey Annual Dry Tons Applied: 12.9231 Site #: 5 Acres Permitted: 4.6
Operator: Larry Bailey
Crop I Name: Fescue
Predominant Soil Series: PbB2
Crop 1 Max. PAN: 178
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
�
❑
Volume applied
enter one Solids/
( ) -�
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp •' P'
Acre
(Dry Tons/Ac)
Residual Sources
(NP1�1�S #. 1� Q#.
Feri., Animal
uv asLe, etc)
Soil
Cond.
ADD'
Moist)
Precip.
Past 24
Firs.
inches
>
�_ t?
� _
a
N
*
TKN
mg/kg
z 3
o �
r1°c
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibslacre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
3-2020
99
15.5
2.809
NCO025984
dry
0
s
0.5
0.3
47112
1 14452
722.58
99.714
NA
Fescue
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0,000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TO"I-ALs:
99
0
As
Cd
CU
Cr
Pb
H g
Mo
Ni
Se
Zn
P
99.714
0.000
Lime Applied
Annual lbs/acre
0.017
0.033
0.050
36
0.016
0.021
0.037
34
1.309
1.714
3.023
1338
#######
0.272
#######
1 NA
0.265
0.443
0.708
1 267
0.001
0.004
0.005
15
0.028
0.044
0.072
1 NA
0.054
0.083
0.137
1 374
0.020
0.138
0.158
1 89
6.309
7.026
13.335
1 2498
4.675
Date
lbs/ac
Prior Years Cumulative Ibs/ac
0
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
1 178
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, annerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
Total Dry Tons Applied (Annual): 14.36
WQ0037135 Cation Exchange Capacity (non 503 only):
Larry Bailey Owner: Larry Bailey Predominant Soil Series:
3.3 Acres Permitted: 3.3 Site #: NC-RU-1-13 Field #:
PbB2
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use ma/ka. % Solids use Raw Percent 91:
Sample or
Com-
posite
Date
Lij
1 /23/20
L2j3
J
4
5
L61
7
81
9
10 a
11 ;
1
% Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
d enum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1 123
Total
Phos-
horus
832.2
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
21
L3j
4
5'
63
7(
8
9'
10I
11
12;
DTIAc./
_
-9
0
App.
m
Event
4.35
Arsenic
0.027
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.027
Cadmium
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Copper
2.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
2.028
Chromiu
######
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Lead
0.410
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.410
Mercury
0.002
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.00 0
0.000
0.000
0.044
Nickel
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Selenium
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.032
Zinc
9.772
A000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.772
Total
Phos-
7.242
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.242
horus
i certtiy, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
0- d.r-,�L 4
Sign re of Land Appher
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-LB Acres Utilized: 3.3
Land Owner: Larry Bailey Annual Dry Tons Applied: 14.3591 Site #: 6 Acres Permitted: 3.3
Operator: Larry Bailey Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
`
o
Q2
Volume applied
(enter one) Solids/
liquid
Cu. Yds Gallons
ova
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#_
Fert.. Animal
Waste. etc)
Soil
Cond.
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
a
K a
a o
a
°
d
w °=
w'
:
w
N'
TKN
mglkg
3
o �
`��° w'
mg/kg
Nitrate
and
Nitrite
mglkg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
3-2020
110
1 15.5
4.351
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
154.439
NA
Fescue
0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0M00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
POT777A1s:
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
tto
o
As
Cd
Cu
Cr
Pb
H,
Mo
Ni
Se
Zn
P
154.439
0.000
Lime A lied
Annual lbs/acre
0.027
0.025
2.028
#######
0.410
0.002
0.044
0.083
0.032
9,772
7,242
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.34
0,367
36
0.022
0,047
34
1.767
3.795
1338
0.28
#######
NA 1
0.457
0,867
267
0.004
0.006
15
0.045
0.089
NA
0.086
0.169
374
0.142
0.174
89
7.246
17.018
2498
0
Current Cumulative lbslac
Permitted C. P. L. R.****
Hermit PAN Limit Ist/2nd Crop
178
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
` *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ' Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Frank Lawson Owner:
16.7 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Frank Lawson Predominant Soil Series:
16.7 Site #: NC-RU-FLB Field #:
30.16
PbB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use to&ka, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEEMENEENE
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1
2
3 j
4 3
5
S
7
8
9
1 p
DT/Ac.l
_
a
App.
Event
1.81
"
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
0.842
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.842
Chromium
######
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Lead
0.170
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.170
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denum
enum
Nickel
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Selenium
0.013
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.013
Zinc
4.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.056
"rota)
Phos-
3.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.006
horus
"1 cernIy, unaer penalty of iaw, tnat tnts document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�� ��l
Sign ture of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-FLR Acres Utilized: 16.7
Land Owner: Frank Lawson Annual Dry Tons Applied. 30.1540 Site #: 2 Acres Permitted: 16.7
Operator: Frank Lawson Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
o r
y
❑
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
A lied per
pp P
Acre
(Dry Tons1Ac)
Residua] Sources
(NPDES #, WQ#,
Pert., Animal
Waste, etc)
Soi]Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
� ,�
ro -a
_.
o a
�-
o
w
'�
N'
* w
� �
�,•
TKN
mgtkg
z �
o 3
� _2
a
mgtkg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
(lhslacre}
Name of Crop Type
Receiving Residual
t
Application
Crop 1
Crop 2
Crop 1
Crop 2
8-2020
154
15.5
1.204
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
42.725
NA
Fescue
9-2020
77
15.5
0.602
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
21.362
NA
Fescue
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
2311
0
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
64.087
0.000
Lime Applied
Annuallbs/acre
0.011
0.057
0.068
36
0.010
0.029
0.039
34
0.842
3.134
3.976
1338
#######
0.45
#######
NA
0.170
0.915
1,085
267
0.001
0.01
0.01 1
15
0.018
0.081
0.099
NA
0.034
0.169
0.203
374
0.013
0.37
0.383
89
4.056
11.893
15.949
2498
3.006
Date
lbs/ac
Prior Years Cumulative lbs/ac
!1
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
1 178
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loadiniz Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Norman McDaniel Owner:
9 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Norman McDaniel Predominant Soil Series:
9 Site #: NC-RU-NM Field #:
15.80
CaB2
C
i] ..7,...1 A.,..I.,c;� ".,+a rupa.,., X4,-tala aril 'rntnl Phnsnhorus use mg/ke. % Solids use Raw Percent #):
2
3
5'
6
7
8'
9
1p
11
12Ta
Sample or 1
4...
Com-
posite
Date 1/23/20
% Solids 15.5
Arsenic 3.11
Cadmium 2.9
Copper 233
Chromium NA
Lead 47.1
Mercury 0.187
Molyb- 5.03
denum
Nickel 9.55
Selenium 3.63
Zinc 1123
Total
Phos- 832.2
horus
Aetn,ial 4-1oQxrw Ma+al Vipid 1 .nadincrc It 'nieiilntedl In Insiacrel:
Total 1 v
2
3
4 V
5
6
7
8'
9
10
11
121
DT/Ac./
°
App.
sv
Event 1.76
Arsenic 0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium 0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper 0.818
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.818
Chromium ####4#
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Lead 0.165
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.165
Mercury 0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0-000
0.001
Molyb- 0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denum
Nickel 0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Selenium 0.013
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.013
Zinc 3.942
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.942
Total
Phos- 2.921
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.921
horus
"I certify, under penalty of law, that this document was preparea unaer my alrectlon or supervision In accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
01
1�/ 7�� -2. 24,
Sign re of Land pplier Date
DENR FORM MFLSF (12/2006)
I

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc.
WQ Permit #: WQ0037135
Field #: NC-RU-NM Acres Utilized: 9
Land Owner: Norman McDaniel
Annual Dry Tons Applied: 15.7950
Site #: C Acres Permitted: 9
Operator: Norman McDaniel
Predominant Soil Series: CaB2
Cation Exchange Capacity (non 503):
Crop I Name: Fescue
Crop 1 Max. PAN: 209
Crop 2 Name: Crop 2 Max. PAN:
Volume applied Volume
Soil ,
Residual Sources I recip.
Cond. K -ZSb
C z > Nitrate Name of Crop Type
o PAN Applied
w Receiving Residual
o o
(enter one} Solids/ /o Applied per
Past 24
(NPDES #, WQ#, _.
�
TKN o and
?4 no ( lbslacre)
" Application
a>
OLiquid Solids Acre
(Dry,
Fert., Animal Wet Hrs. a
Nitrite
w w
Cu. Yds Gallons (Dry TonslAc)
Waste, etc) Moist} inches
} mg/kg mglkg mglkg Crop I Crop 2 Crop I Crop 2
5-2020 121 15.5 1.755
NCO025984 dry 0 s
0.5 0.3 47 112 14452 722.58 62.290 NA Fescue
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0,000
0.000 0.000
0.000
0,000 O.000
0.000
0.000 0,000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
To'1al tzl 0 As
Cd Cu Cr Pb H
Mo Ni 5e Z.n P 62.290 0.000 Lime A lied
Annuallbslacre 0,011
0.010 0,918 ####### 0.165 0.001
0.018 0.034 0.013 3.942 2.921 Date I Ibslac
Prior Years Cumulative lbs/ac 0.046
0.043 2.473 0.332 0.736 0.003
0.081 0.175 0.356 9.357 0
Current Cumulative Ibslac 0.057
0.053 3.291 ####### 0.901 0.004
0.099 0.209 0.369 13.299
Permitted C. P_ L. R.**** 36
34 1338 NA 267 15
NA 374 89 2498
Permit PAN Limit 1st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction
or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and
evaluated the information submitted.
i am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, 1N - Injection, INC - Incorporation
�•'�l'%y
**Volatilization Rate: Surface -0.5, Injectionllncorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier
Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loadintr Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 17.24
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Norman McDanief Owner: Norman McDaniel Predominant Soil Series: PbB2
Acres Used: 6.2 Acres Permitted: 6.2 Site #; NC-RU-NM Field #: 1
Residual Analvsis Data (Heavy Metals and Total Phosohorus use ma/ki!, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/23/20
2
3
4'
6
6 1
7
$
9
10
11
12�
% Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1 123
Total
Phos-
horus
832.2
Annual Heavv Metal Held Loadintss IC.'alculatecl in lbslacrel:
Total
_1
2,
31
4;
5
61
7
8
9
10
11',
12
DTIAc.I
O
.w
App.
U
Lvent
2.78
Arsenic
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.017
Cadmium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
1.295
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.295
Chromium
# #
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
444#4#
Lead
0.262
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.262
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
denum
Nickel
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.053
Selenium
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Zinc
6.244
0.000
0.000
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.000
6.244
Total
Phos-
4.627
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.627
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sign ure of Land Applier
a-�.0
Date
DENR FORM MFLSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-NM Acres Utilized: 6.2
Land Owner: Norman McDaniel Annual Dry Tons Applied: 17.2309 Site #: 1 Acres Permitted: 6.2
Operator: Norman McDaniel Predominant Soil Series: PbB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I. Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
o =
�? o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
oho
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
( NPDES #, WQ#,
Fert., Animal
Waste. etc)
Soil
Cond.
(Dry.
Mist)
Precip.
Past 24
Hrs.
inches
a
K �
,5 -
o�
o
�, -
*
°
z
?
* 0
TKN
mg/kg
n
o
m
mg/kg
Nitrate
and
Nitrite
mgtkg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
6-2020
66
15.5
L390
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
49.321
NA
Fescue
9-2020
66
15.5
1,390
NCO025984
dry
0
s
0.5
0.3
47112
14452
722.58
49.321
NA
Fescue
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
132
0
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
98.6421
0.000
Lime Applied
Annual lbs/acre
0.017
0.016
1.295
#######
0.262
0.001
0.028
0.053
0.020
6.244
4.627
Date
lbs/ac
Prior Years Cumulative lbslac
0.59
0.05
3.139
0.449
0.893
0.005
0.096
0.199
0.386
12.207
0
Current Cumulative lbslac
0.607
0.066
4.434
#######
1.155
0.006
0.124
0.252
0.406
18.451
Permitted C. P. L. R.****1
36
34
1338
1 NA
267
15
1 NA
374
1 89
2498
Permit PAN Limit 1 st/2nd Crop
I F 178
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
^ `Application Method: S - Surface, IN - Injection, INC - Incorporation
"Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
""C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM`
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc. Total Dry Tons Applied (Annual):
WQ0037135 Cation Exchange Capacity (non 503 only):
Norman McDaniel Owner: Norman McDaniel Predominant Soil Series:
4.2 Acres Permitted: 4.2 Site #: NC-RU-NM Field #:
17.23
PaC2
2
Recirinal Analvsis nata (Heavv Metals and Total Phosnhorus use mlAL,. % Solids use Raw Percent #):
Sample or
Com-
posite
Date
LIJ
1/23/20
21
3
4 l
5
6
7
81
9
10
11
12
%Solids
15.5
Arsenic
3.11
Cadmium
2.9
Copper
233
Chromium
NA
Lead
47.1
Mercury
0.187
Molyb-
denum
5.03
Nickel
9.55
Selenium
3.63
Zinc
1123
Total
Phos-
horus
832.2
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
21
3
15
6
7
8;
9
10
11
12
__4F
DT/Ac./
c
App•
Event
4.10
Arsenic
0.026
0.000
0.000
1 0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.026
Cadmium
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Copper
1.912
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.912
Chromium
####4#
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Lead
0.386
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.386
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
denum
Nickel
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Selenium
0.030
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.030
Zinc
9.213
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.213
Total
Phos-
6.827
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.827
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
14 oe__
Sign re of Land Applier
C� -;.c-a4
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: US Biosolids, Inc. WQ Permit #: WQ0037135 Field #: NC-RU-NM Acres Utilized: 4.2
Land Owner: Norman McDaniel Annual Dry Tons Applied: 17.2309 Site ##: 2 Acres Permitted: 4.2
Operator: Norman McDaniel Predominant Soil Series: PaC2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN:
Volume applied
Volume
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - lA
Date "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loadinp_ Rate
DENR FORM FSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION NORM (02T Rules)
Facility Name: U.S. Biosolids, Inc.
WWTP Name: Forest City WWTP
Monitoring Period: From
WQ Permit Number:
NPDES Number:
111 /2020 To 12/31/2020
WQ0037135
NCO025984
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (tirneitemp) C
Alt B (Alk Treatnent) ®
Alt. C (Prior Testing)®
Alt.0 (No Prior Test) 0 1
Process to Further Reduce Pathogengs 0
If applicable to alternative performed (Class A only) indicate "Process to Fuirther Reduce Pathogens":
Compost ® I
Heat Drying J
Heat Treatment LJ
Thennophilic C,
Beta Ray o
Garnnia Ray D
Pasteurization
Class B:
jAlt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
.C7
Lime Stabilization ®
Air Drying
Composting L1 jAerobic
Digestion 1
Anaerobic Digestior. Lj
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Number o
Allowable Level Pathogen Density um Frequency Sample Analytical
Tech -
Fences
Parameter e- of Analysis Type maue
in Sludge MinimumGeo. Mean Maximurn Units
2 x 10 to the
MPN
21538
46466.8
70866
MPNIg
0
7
grab
sm9221
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) t-j
Alt. 2 (40-day bench)
Alt. 3 (30-day bench)
Alt. 4 (Spec. O, uptake) i
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) L1
JAIt. 8 (Drying - Unstable)
Alt. 9 (injection) j
Alt. 10 (incorporation) Lj
No vector attraction reduction alternatives were performed Il
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
Ll "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1 t07 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
&Aq411y &, C Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DE=NR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. Biosolids. Inc.
W WTP Name: Town of Spindale W WTP
Monitoring Period: From 1/1/2020 To
WQ Permit Number:
NPDES Number:
12/31 /2020
WQ0037135
NCO020664
u.,+h,...o., u114ZA N11—Af MT 11(161 - PIPacP indicate level achieved and alternative performed:
Class A:
Alt. A (tinte/tenip) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑ I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
I l.eat Treatment ❑
Thermophilic ❑
Beta Ray ❑ I
Gattltna Ray ❑
Pasteurization LJ
Class B: I
Alt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Coinposting ❑
jAerobic Digestion ❑
Anaerobic Digestior ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
o
NumberFrequency
Excee- encesof
Anal ysis
Sample
Typenioue
Analytical
Tech -
MinimumGeo.
Mean
Maximu
Units
1=ecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
7692
8195
8696
MPN/g
0
7
grab
sm9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vnrtnr Attrartian WPrinetlnn 1 ! 1A IN( :At 1!L 1 . i lu 1 i - rlease 1nuicate aituriiativc tifn im invu.
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) L:3
Alt. 3 (30-day bench) 21
Alt. 4 (Spec. O, uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (incorporation) Lj
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0,11 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
G;,y 0`4.,, e?. dA,L Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Pre arer* -Date Signature of Land pplier (if applicable) Date
i~ p
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: U.S. Biosolids, Inc,
WWTP Name: Town of Rutherfordton WWTP
Monitoring Period: From 1/1/2020
WQ Permit Number:
NPDES Number:
To 12/31 /2020
WQ0037135
NCO025909
PathnaPn Ri-tNetinn ill ;A NCAC 62T _11061 - Please indicate level achieved and alternative nerformed:
Class A:
Alt. A (tine/temp) ❑
Alt B (Alk Treattuent)❑
Alt. C (Prior Testing)❑
AIt.D (No Prior Test) J I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
1-teat Drying ❑
Heat Treatment $l
Therniophilic G
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density 211
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestior ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Number o
Allowable Level Pathogen Density Excee-
Analytical
Frequency Sample Tech -
Parameter in Sludge
g Minimum Geo. Mean Maximu Units encesType
of Analysis
Y T enigue
2 x 10 to the
MPN
1250
1361
1527
MPN/g
0
7
grab
sm9221
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
Vnnfnr Affr.aefinn Itarinetinn (IS A NI'AI nLI _I lil-/l - rieaCe innicare airernaiive Derlormeo:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) R1
Alt. 4 (Spec. O, uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
Ll "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Ap lier Name and Title (if applicabie)(type or print)
_ A 24.0i
Signature of Preparer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 C1•R Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM PVRF 02T (1212006)

YADKIN VALLEY SEWER AUTHORITY
NC0020567

Waypoint,
ANALYTICAL
46381
Southern Sail Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-280-0003
Lab No : 73889
Sample ID: YUSA
Test
Moisture
Test
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
Project US Biosolids Inc
Information :
REPORT OFANAI PSIS
Results Units
97.1
Results Units
MQL
0.010
MOL
Report Date : 10/14/2020
Received : 10/rr0,,6/2020
i� QO Cd
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10/5/2020 11.00
DF Date ITime By Analytical
Analyzed Method
1 10/12/2017:50 FMM SM-2540G
DF Date lTime By Analytical
Analyzed Method
Ammonia Nitrogen
2690
mg/Kg - dry
862
1
10/13/20 14,00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
167
mg/Kg - dry
165
1
10/13/20 13:51
713D
450ONO3F-2011
Organic. N
62400
mg/Kg - dry
8620
1
10/13/20 10:00
CALCULATION
J)"
6.1
S.J.
1
10/12/2016:30
ADM
9045D
Total Solids
2.91
%
0.010
1
10/12/20 17:50
FMM
SM-2540G
Total Kjeldahl Nitrogen
65200
mq/Kg - dry
8620
1
10/13/20 10:00
JPJ ;M-4S00-NH3C-TKP
Phosphorus
33900
mg/Kg - dry
172
1
10/10/20 03:34
]ADS
601.0D
Aluminum
52800
mg/Kg - dry
172
1
10/10/20 03:34
]ADS
6010D
Arsenic
<11.2
mg/Kg - dry
17.2
1
10/10/20 03:34
]ADS
601.01)
Calcium
10200
mg/Kg - dry
172.0
1
10/10/20 03:34
DADS
6010D
Cadmium
<3.45
mg/Kg - dry
3.45
1
10/10/20 03:34
]ADS
6010D
Chromium
32.9
mg/Kg - dry
8.62
1
10/10/20 03:34
]ADS
6010D
Copper
614
mg/Kq - dry
17.2
1
10/10/20 03:34
JADS
60100
Iron
27300
mg/Kg - dry
345
1
10/10/20 03:34
.LADS
6010D
Lead
23.7
mg/Kg - dry
103
1
10/10/20 03:34
]ADS
6010D
Magnesium
3660
mg/Kg - dry
172
1
10/10/20 03:34
DADS
6010D
Manganese
486
mg/Kg - dry
17.2
1
].D/10/20 03:34
JARS
601.01)
Qualifiers/ DF
Dilution Factor
Definitions
MQL
Method Quantitatian Limit
L
Limit
Exceeded
Page 3 of 7

Waypoint(!D
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-280-0003
Lab No : 73889
Sample ID: YUSA
Test
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypointanalytical.com
Project US Biosolids Inc
Information :
REPORT OFANAL PSIS
Results Units MQ1-
Report Date : 10/14/2020
Received : 10/06/2020
C L7 o w
Pauric Mc Groary Ph.O., CPA
Agronomist
Matrix: Solids
Sampled: 10 / 5 / 2020 11: 00
DF Date / Time By Analytical
Analyzed Method
Mercury
0.717
mg/Kg - dry n`
0.507
1
10/13/2013:20
DDB
SW-74713
Molybdenum
<8,62
mg/Kg - dry
8.62
1
10/10/20 03:34
]ADS
6010D
Nickel
17.2
mg/Kg - dry
8.62
1
10/10/20 03:34
]ADS
6010D
Potassium
4760
mg/Kg - dry
345
1
10/10/20 03:34
)ADS
6010D
Selenium
<17.2
mg/Kg - dry
17.2
1
10/10/20 03:34
]ADS
6010D
Sodium
2030
mg/Kg - dry
862
1
10/10/20 03:34
]ADS
6010D
Zinc
614
mg/Kg - dry
43.1
1
10/10/20 03:34
]ADS
60100
Sulfur
5930
mg/Kg - dry
345
1
10/13/20 00:08
]ADS
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions
MQt. Method Quantitation Limit
Page 4 of 7

Y11501
SAMPLE '1 I\AN I1E1R1t11111111111]i111 �1ki!#N�I�JR€I�z86.a003 ��J AC�csuni�
C�7
SUU1fWrri S;il 6uilrk:r;' 2`t`0 46381
"f'2i �i"ttit:�i:,cI.r,�si;;ci:n�rr;±t?4',12"2? tlsB insina: 1412:04
E
Submitted try Charge 1 a
ropy To
US Biosolids, Inc. US Biosolids, Inc. US Biosolids Inc.
958 Hoots Road 958 Hoots Road I 95$ Hoots Road
Roaring River, NC 28669 Roaring River, NC 28669 #oarirg River, NC 286fz9
'roject \f i el v1
Lab \u^i4er
Sample Id (Lab Use
Only, 1 Type
,w:,raw
_;e
Grab
Sam le Information
GOliec€lon Information Conlaine[ Informatw Please Check Des;red Tests
Date ;,me N;mber i T Sn3 tJisage� tdala::le
of 3att€esi Type tiolume 8Lt SL2 ?vleiaLs Se ies �� ` CC- ag C:
i sntids
1ff` i isiaS5 �"_-07� e
las`Fc I
GiassCZ i
j I _ Mastic
07
Gass
I
Pl
estI—
�
G;355 j- �.r• i i � I e i I
Oate e ! Received 8Y (Si nalure) Dwe Tine
I
Test Package Details
5€33 Metals: -SPn�c 2C :u �^ �:;
� �, .,ri r".7e"CGS{. ,I:OIYb^'L�6.�.'�.CrtEI.
� u:
€s9riper $ Zinc T-nduced 'r' S-2i
Si1ro�- a
CCE: C;ai,:u'n Carbc:iate � G:-OivafEn' Cr rW;,:fi neutral±za:io, `Ja:t:e'i,: os ! ;
eclal instructiGns or Remarks
uL`ters
r-

PAN
Mineralization
Rate TKN NH3 NO3
0.3 65200 2690 167
PAN Surface
20265 mglkg
40.53 lbsldry ton
0 Ibs total PAN
#DlV/0i Ibs PANlacre
PAN Injection
21610 mglkg
43.22 lbsldry ton
0
Ibs total PAN
#DIV101
Ibs PANlaere
Dry Tons11000 gal
0.121347
1st year PAN
Surface lbs.
0
1st year PAN
Injected Ibs.
0
lbs./acre
Surface
#DIWO!
I bs.la c re
Injected
#DIV/0!
NO2 % Solids tonslyear Applied on
0 0.0291
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =lbsldry tors
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =lbsldry ton
1000 X 8.34 X %solids X sp. gravitV
2000
"=dry tons/1000gal."

SAR
Sodium Absorption Ratio
Na M /L
Ca M IL
MqIhArill
Na : Sodium (MgIL) Equivalent weight: 23
L59.07
296.82
106.5
Ca : Calcium (MgIL) Equivalent weight: 20
Mg: Magnesium (MgIL) Equivalent weight: 12
Na..(ME.).
CajMg
M„(ME}
Milli Equivalent = MgIL / Equivalent weight
2.568261
14.841
8.875
The amour
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power amount of
t
SAR = 0.745819 (From MgIL entered above) Permitting
SAR= 0.417061 (From ME entered below)
Na (ME)
Ca(ME)
Mg
0.29
0.328
161ME
39

Analytical Results
U.S. BlosoildS Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/17/2020
Reported: 03/19/2020
For: YVSA
Comments: GM 68,115 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
200317-37-01
Fecal Coliforms
1
68966
MPN/g
SM92210E-2006
03/18/2020
WC
200317-37-01
Percent Solids
1
3.48
%
SM2540B-2011
03/18/2020
WC
200317-37-02
Fecal Coliforms
2
69565
MPN/g
SM92210E-2006
03/18/2020
WC
200317-37-02
Percent Solids
2
3.45
%
SM2540B-2011
03/18/2020
WC
200317-37-03
Fecal Coliforms
3
66667
MPN/g
SM92210E-20M
03/18/2020
WC
200317-37-03
Percent Solids
3
3.60
%
SM25408-2011
03/18/2020
WC
200317-37-04
Fecal Coliforms
4
67989
MPN/g
SM92210E-2006
03/18/2020
WC
200317-37-04
Percent Solids
4
3.53
%
SM25408-2011
03/18/2020
WC
200317-37-05
Fecal Coliforms
5
70175
MPN/g
SM92210E-2006
03/18/2020
WC
200317-37-05
Percent Solids
5
3.42
%
SM2540B-2011
03/18/2020
WC
200317-37-06
Fecal Coliforms
6
67989
MPN/g
SM9221CF-2006
03/18/2020
WC
200317-37-06
Percent Solids
6
3.53
%
SM2540B-2011
03/18/2020
WC
200317-37-07
Fecal Coliforms
7
65573
MPN/g
SM92210E-2006
03/18/2020
WC
200317-37-07
Percent Solids
7
3.66
%
SM25403-2011
03/18/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 + Statesville, NC 28687 • 704/872/4697
Page I of 2

n
m
xn
N
Client:
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r� O
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DD �
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a
Address: �d rq
___
rl". TFSVILLf"
no
t7
�Qr`_..�ir•--�C7Q
._......�.�.__
s �iNAL7 f ICAL
122 Court Stma • P.Q. Box 228
`l SFwlesvitic, NC 3RfiA7
.
00
Contact Person:
— k�
Phone A
33��77�-s
oq—
FAXN
_ /
i7W 1 072-407
00
Op
Po N
Requisitioned by:
_
Imo—
Data) _
Chain or
Custody Record
�
z
IN Lab40 P (Ora Only)
(Gnh QN)
W ww
Pwwaes mqw xcd !or a:tiJY-
01
��s I 2003i7.37. r
x
xC4
r
2
X
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Pi-
N
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CD
_
_____
Relinquished by: Time d am, pm Date � / �� / DO Sampled by:
Received by: Time Mao, pm Date �/�?I
Transported by:
/% �
Relinquished by:---... Time am, pm Date _!/_ f
Holding times met:
Received by. Time am, pm Date ..._I/. f
...._. Compliance work:
•-• Si �xr.lK�._�
Time begin am, pm Date / /­ Non-compliance work:
Time end am, pm Date _..._._...._�_
Lab Comments:
Samples Transported on ICB:
Time begin am, pm Date 1 I
Time end am, pm Date

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 07/30/2020
Reported: 09/08/2020
For: YVSA
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200730-22-01 30 Day Benchscale YVSA <1 % EPA525-R-s210 07/30/2020 WC
Respectfully submitted,
,gyp -Woo JY'h-f ,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Condition of Receipt
MENNEN
Sample Number 200730-22-01 Temp on Arrival: 4,5
Parameter Schedule:
Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

M1C �. J
8:osal:ds{ x�
cress:
ltact Person: -
�r
a
x idb-16 M Time Sam,
lie IDf (Grab Oml
- . PIIMPOTI t OR.,
Phone # 314-'JAB.
Requisitioned by:
jOrab Only)
7 3o-.7 Ira v
V
FAX!#
Dom)
ST.A7£SVIt_LF
i ANALT7tCAL
122 Court Stmel • P.O. Boc 228
Sud—ilk, NC 28687
Y w '°- QW) 872-"97
Chain of
Custody Record
+�.
r
Maroc
w
�
Panme-.as Rqucxcd for �mlysis
Relinquished by: Time 3:/ �V am, rr Date Su / 2- 9)
Received by: Time t 5l0 am V�Date -7/3q ZJ
Relinquished by:
Received by:
m t+
r.,ttq....,.
Time begin
am, pm Date
Time and
am, pm Date
Composite SampII
ng #2:
Time begin
am, pm Date ,/ /
Time end
am, pm Date _/-1�
Time am, pm Date _/_/—
Time am, pm Date —J_/
Lob Comments:
Sampled by „1
Transported by: -
Holding times met:
Compliance work:
Non-compliance work:
Samples Transported On Ice:
Initials:
h
rn
N o
00 h �
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Q a.
h
h
00
v,
00
N
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Q7
7
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a-

aceftlXical •
+rrw.p+crlgt.rnn
ANALYTICAL RESULTS
Pace Analytical Srrvlcea, LLC
9800 KinceyAve. suite 100
Hurtersvilla, NC 28078
[phone]
Project: YVSAIUS BI0
Pace Project No.: 9241D434
Sample: 200317.36,01
Lab ID: 92470434001 Collected: 03M7120 13:00 Received: 03/20120 09:30 Matrix: Solid
Results reported on a 'dry weigh!'
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS Na. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
96.5 % 0,10 1 03123120 15:25
1010 Flashpolnt,C lased Cup
Analytical Method: EPA 1010A
Pace Analytical Services -Asheville
Flashpoint
a200 deg F 70.0 1 03)31120 10:48
9045 pH Solt
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
8.7 Std. Units 0.10 1 0313012014:27 H3
9095 Paint Filter Liquid Test
Analytical Method: EPA 9095E
Pace Analytical Services - Asheville
Free Liquids
Fail 1.0 1 03/26120 15:08
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
ND mg/kg 28.8 1 03/23/20 15:02 03/23120 16:36
734S Reactive Sulfide
Analytical Method: SM 450052F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
NO mglkg 288 1 03123120 15:02 03123/20 15:03
Sample: 200317.36.01 PCB
Lab ID: 92470434002 Collected: 03/17/20 13:00 Received- 03/20120 09:30 Matrix: Water
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No. Quaff
8082 GCS PCB RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 12211
NO ugX 2.5 1 03131120 15:55 04101120 22A3 12674-11-2
PCB-1232 (Aroclor 1232)
ND ugiL 2.5 1 03/31120 15:55 04101120 22:13 11104.28-2
NO uglL 2,5
PCB-1242 (Aroclor 1242)
1 03/31120 15:55 04/01/20 22:13 11141-16-5
NO
PCB-1248 (Aroclor 1246)
ug1L 2.5 1 03131/20 15:55 04)01120 2213 53469-21-9
NO
PCB-1254 (Aroclor 1254)
ug1L 2.5 1 03131120 15:55 04101120 22:13 12672.29-6
ND
PCB-1260 (Aroclor 1260)
ug1L 2.5 1 03131/20 15:55 04101120 22:13 11097.69-1
NO ugiL
Surrogates
2,5 1 03/31/20 15:55 04/01120 22:13 11096-82-5
Decach€oroblphenyl (S)
35 % 10.130 1 03131I20 15:55 04101/20 22:13 2051.24-3
REPORT OF LABORATORY ANALYSIS
Date: 04/03/2020 04,55 PM
This report shall not be reproeviced. except in lull,
wilhoul the wrRien consent of Pace AnalyVcal Services, LLC,
Page 7 of 27
PO Box 228 • Statesville, NC 28687 e 704/872/4697
Page 16 of 38

I eAnaIXical
xrlr.�oassxcan
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvills, NC 28078
[phone]
ANALYTICAL ReSULTS
Project: YVSAIUS BIO
Pace Project No.'. 92470434
Sample: 200317.36.01
L fD: 92470434001 Collected: 03/17120 13:00 Received: 03120/20 09:30 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture,
sample
size and any dilutions.
Parameters
Results
Units Report Limit
OF
Prepared Analyzed CAS No.
1470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
`
Leachate Method/Date: EPA 1311; 04/01/20 16:10 Inftial pH: 7.76; Final pH: 4.5
Pace Analytical Services - Asheville
Mercury
ND
mglL
0.00020
1
0410212011:35 04102Q015:57 7439-97-6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
2,4-01nitrotcluene
ND
uglL
250
5
03/31/2015:03 04/0112012:27 106-46-7
Hexachloro-1,3-butadlene
NO
NO
ug1L
ug1L
250
250
5
03131/2015:03 04/01/2012:27 121-14-2
M1
Hexachlorobenzens
ND
uglL
5
0313V2015:03 0410112012:27 87-68-3
Hexachloroethane
250
5
0313112015:03 0410112012:27 118-74.1
2-Mothylphenol(o-Cresol)
NO
NO
uglL
ug1L
250
250
5
0313112015:03 04/01/201227 67-72-1
3&4-Mathytphenol(m&p Cresol)
1090
uglL
5
03/31120 15:03 04101/2012:27 95-48.7
Nitrobenzene
250
5
03/31/20 15:03 04/01/20 12:27 16831-10-4
Pentechlorophenol
NO
NO
uglL
250
5
03131120 15:03 04/01/20 12:27 98-95-3
Pyridine
uglL
500
5
03131/2015:03 04101/2012:27 87-86-5
M1
2,4,5-Trichlorophanol
ND
ug1L
250
5
03131/2015:03 041011201227 110-86-1
2,4,6-Trlchlorophenol
ND
NO
ug1L
250
5
03/31/2015:03 04101/2012:27 95-95-4
M1
Surrogates
uglL
250
5
03131/2015:03 0410V2012:27 88-06-2
M1
Nitrobenzene-d5 (S)
2-Fluorobiphemyl(8)
413
%
12.102
5
03/31120 15:03 04101/20 12:27 4165-60-0
D3
Terphenyi-d14 (S)
40
43
%
13.107
5
03/31/20 15:03 04/01/20 12:27 321.60-8
Phenol-06 (S)
%
21.132
5
03/31120 15:03 04/01/20 12:27 1718-51-0
2-Fluorophenol (S)
27
29
%
10-110
5
03/31/20 15:03 04/01120 12:27 13127.88-3
2,4,6-Tribromophenol (8)
38
%
10.110
5
03131)20 15:03 04/01/20 12:27 367-12-4
%
27-108
5
03131120 15703 04101120 12:27 118-79-6
8260D MSV TCLP
Analytical Method:
EPA8260D
Pace Analytical
Services - Charlotte
Benzene
2-Butanone (MEK)
NO
NO
ug1L
100
20
03/31/20 04:28 71.43-2
Carbon tetrachloride
ND
ug1L
ugll-
200
100
20
03131120 04:28 78-93-3
Chlorobenzene
ND
ug1L
20
03/31120 04:28 56-23.5
Chloroform
NO
uglL
100
20
03/31/20 04:28 108.90.7
1,4-Dichlorobenzene
NO
uglL
100
100
20
03/31/20 04:28 67.66.3
1,2-Dichlofoelhene
NO
ug1L
100
20
03/31120 04:28 106-46-7
1,1-Dichloroothene
NO
uglL
100
20
20
03/31/20 04:28 107-06-2
Tetrachtoroethene
ND
uglL
100
20
03131/2004:28 75-35-4
Trichtoroethone
NO
ug/L
100
20
03/31120 04:28 127-18-4
Vinyl chloride
NO
uglL
100
20
03/31/20 04:28 79-01-6
Surrogates
03131/20 04:28 75-01-4
1,2-Dichioroethane-d4 (S)
Toluene-d8 (S)
102
%
70-130
20
03/31120 04:28 17060.07-0
4-BromoBucrobenzene(S)
107
105
%
%
67-135
20
03/31/20 04:28 2037-26-5
70.130
20
03131/20 04:28 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shelf not he reproduced, except In full,
Date: 04103/2020 04:56 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 6 of 27
PO Box 228 s Statesville, NC 28687 s 704/872/4697
Page 15 of 38

aceAnalXical
rinr.pateYsli.esn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville. NC 25078
[phone]
Project: YVSAIUS BIO
Pace Project No.: 92470434
Sample: 200317.36.01 Lab lb: 92470434001 Collected: 03/17/20 13:00 Received: 03/20/20 09:30 Matrix: Solid
Results reported on a `dry weight` basis and are adjusted for percent molature, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A
2,4,5-TP (Sllvex)
2,4-D
Surrogates
2,4-DCAA (S)
8081 TCLP Pesticides RVE
gamma-BHC (Lindene)
Chlordane (Technical)
Enddn
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachl0m-m-xytena (S)
8082 TCLP PCBs RVE
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 {Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Vitt MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date: 04/0312020 04:55 PM
Analytical Method: EPAS151A Preparation Method: 8151A
Leachate Method/Date: 1311; 03/26/20 10:33 Initial pH: 6.33; Final pH: 4.94
Pace National - Mt. Juliet
NO mg1L 0 OD200 1 OW27120 08:22 03127/20 16:37 93.72-1
ND mgll 0.00200 1 03/27/20 08:22 03127/20 16:37 94-75-7
67.8 %
14.0-158 1
03127/20 08:22 03/27/20 16:37 19719-28-9
Analytical Method: EPA 8081B Preparation Method:
EPA 351OC
Leachate Method/Date: EPA 1311; 03126)20 16:12
Pace Analytical Services - Chadotle
ND ug1L
0.50 1
03/30/20 17:D6 04/01/20 1539 58-89-9
ND ug1L
NO
3.0 1
03/30/2017:06 0410112015:39 57-74-9
ug1L
NO
0.50 1
03/3012017:06 0410112015:39 72-20-8
trglL
0.50 1
03130/2017:06 0410112015:39 76.44-8
ND ug/L
0.50 1
0313012017:06 0410112015:39 1024.57-3
ND uglL
1000 1
03130120 17:06 04/0112D 15:39 72-43.5
ND ug/L
3.0 1
03/3012017:06 04/0112016:39 8001-35.2
78 %
10-138 1
03130)2017:06 0410112015:39 2051-24-3
13 %
10-110 1
03/3012017:06 0410112015:39 877-09-8
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Osle; EPA 1311; 03/26120 16:12
Pace Analytical Services- Charlotte
NO ug/L
ND ug1L
1000 1
03130120 17:41 03/31/20 23:26 12674-11-2
1000 1
03/30/20 17:41 03/31/20 23:26 11104-28-2
ND ug1L
1000 1
03/30120 17A1 03/31/20 23:26 11141-16-5
NO u91L
ND ug1L
1000 1
03130/20 17:41 03/31120 23:26 53469-21-9
NO uglL
1000 1
03/30/20 17:41 03/31120 23:26 12672-29-6
ND
1000 1
03/30/20 17:41 OW31/20 23;26 11097-69-1
ug1L
1000 1
03130/20 17A1 03/31120 23:26 11096-82-5
39 %
10.132 1
03/3012017:41 0313112023:26 2051.24-3
Analytical Method: EPA 6010D Preparation
Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/01/20 16:10 Initial pH: 7.76; Final pH: 4.5
Pace Analytical Services -Asheville
ND mg1L
0.37 mg1L
0,050 1
0410212011:11 04102/2017:46 7440.38-2
ND mg1L
0.25 1
0.0050 1
0410212011:11 041021201746 7440-39-3
04/02120 11:11 0410212G 17:46 7440-43-9
NO mg/L
ND
0.050 1
04102/2011:11 0410212017:46 7440-47-3
mg1L
NO
0.025 1
0410212011:11 0410212017:46 7439-92-1
mg1L
ND mg/L
0.10 1
04102/2011:11 04/0212017:46 7782.49-2
0.025 1
04/0212011:11 0410212017:46 7440-22-4
REPORT OF LABORATORY ANALYSIS
This raped shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 27
PO Box 228 ° Statesville, NC: 28687 ° 704/872/4697
Page 14 of 38

TOWN OF SPINDALE
NC0020664

Way
Point.
ANALYTICAL
46381
Southern Sail Builders
DenrliS Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-1SS-0004
Lab No: 72556
Sample ID : Spirldale
7621 Whitepine Road, Rithmond, VA 23237
Main 804-743.9401 ° Fax B04-271-6446
www.waypointanalytical.com
Proyect Spindale
Information :
REPORT Of ANAL PSIS
Report Date: 06/1 t/2020
Received : 06/03/2020
Pry, m` 69wr
Paint MCGroary
Agronomist
Matrix: Solids
Sampled: 6/ 11202010:00
Test Results Units MOL Of Date / Time By Analytical
Analyzed Method
Moisture
Test
99.6 %
Results Units
0.010 1 06/05/20 t6.47 FMM SM-2540G
MOL DF Date i Time By Anatyllcal
Analyzed Method
Ammonia Nitrogen
31800
mg/K4 - dry
6250
1 06/10/20 14:00
JPJ
5M-4500-Ntt3C
Nitrate+Nitrite-N
1700
mg/Kg - dry
1210
1 06/09/20 15:40
ZSD
450ONO3F-2011
Or9armc N
97000
mg/Kg - dry
62500
1 06/10/20 10:00
CALCULATION
pH
6.3
S.U.
1 D6/09/20 05:20
JSL
9D45D
Total Solids
0.390
%
0.010
1 06/05/20 16:47
FMM
SM-254OG
Total Kjddahl Nitrogen
1290M
mg/Kg - dry
62500
€ 06/10/20 10:00
JPJ
N-4500-111-13C-TKO
Phosphorus
9330
mg/Kg - dry
1250
1 05/09/20 22:09
KKM
60101)
Aluminum
6230
mg/Kg - dry
1250
1 06/09/20 22:09
KKM
6010D
Arsenic
25
mg/K9 • dry
125
1 06/09/20 22:09
KKM
60100
Calcium
c 12500
mg/Kg - dry
12500
1 06/09/20 22:09
KKM
60100
Cadmium
<25.0
mg/Kg - dry
25.0
1 06/09/20 22:09
KKM
6010D
Chromium
c62.5
mg/Kg - dry
625
I. 06/09/20 22:09
KKM
6010n
Copper
131
mg/Kg - dry
125
1 (16/09170 22:D9
KKM
60100
Iron
9730
mg/Kg - dry
2500
1 06/09/20 22:09
KKM
60LOD
Lead
c75.0
mg/)(g - dry
75.0
1 06/09/20 22:09
KKM
601OD
Magnesium
1700
mg/Kg - dry
1250
1 06/D9/20 22:09
KKM
60101)
Manganese
255
mg/Kg - dry
125
1 06/09/20 22:09
KKM
6010D
Qwlrfiers/ DF
Oilutnon Factor
L
Limit Exceeded
Oerrnitiana
MQL
Method Quantild4on Limit
Page 3 cf 6

Waypoint-0
ANALYTICAL
46381
Southern Soil eUilders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-155-0004
Lab No: 72556
Sample ID: Spindale
Test
Project Spindale
Information
7621 Whitepine Road, Richmond, VA 23237
Main804-743-9401 "Fax [phone]
www.waypointenalyticsl.com
REPORT Of ANAL PSIS
Results Units MOL
Report Date : 06/11/202(1
Received : 06/03/2020
P6 mF 607'
Pauric McGroary
Agronomist
Matrix: Sdids
Sampled: 6111202010:00
OF Date / Time By Analytical
Analyzed Method
Mercury
<3.83
m9/Kg - dry
3.83
1 06/09/20 11:59
DOB
SW-74718
Mdybdenum
<62.5
m9/Kg - dry
62.5
1 06/09/20 22:09
KKM
60100
Mckel
<62.5
rng/Kg - dry
62.5
1 06/09/20 22:09
KKM
6010D
Potassium
62SO
mg/Kg - dry
2500
1 06/09/20 22:09
KKM
60100
Selenium
12
m9/Kg - dry
125
1 06/09/Z0 22:D9
KKM
6010D
Sodiuvn
23SOO
rng/Kg - dry
6250
1 06/09/20 22:09
KKM
6010D
Zinc
-313
mg/Kg - dry
313
1 06/09/20 22:D9
KKM
6010D
Sulfur
2950
mg/Kg - dry
?500
1 06/04/20 22:09
KKM
60100
Qualifiers/ OF Dilution Factor L Limit Exceeded
Definitions M L Method Q Quantization Limit
Page 4 01 6

SAR
Sodium Absorption Ratio
Na : Sodium (MgIL) Equivalent weight. 23
Ca : Calcium (Mglt_) Equivalent weight: 20
Mg: Magnesium (MgIL) Equivalent weight: 12
Milli Equivalent = MgIL 1 Equivalent weight
Na M !L Ca M IL M M IL
89.3 47.5 6.46
i [@ (ME} I Ca (ME) MAC (ME)
3.882609 2.375 1 0.538333
SAR= Na Milli Equivalentl(0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 3.216944 (From MgIL entered above)
SAR= 3,296102 (From ME entered below)
Na (ME
I Ca (ME)
Mg (ME)
3.9
2.3
0.5
The amour
amount of E
Permitting I

Rate
TKN
NH3 NO3
0.3
129000
31B00 1700
PAN Surface
46760 m /k
93.52 lbs/dry ton
0 Ibs total PAN
#D1V10! Ilbs PAN/acre
PAN Injection
626601 mgIkg
125.32 lbs/dry ton
0 ibs total PAN
#DIVIO! Ilbs, PAN/acre
Dry Tons11000 gal.
0,015846
1st year PAN
lbs./acre
Surface lbs.
Surface
01
#DIV/0!
1st year PAN
lbs./acre
Injected lbs.
Injected
01
#DiVIO!
as decimal ITotal dry lAcres
02 % Solids tons ear Applied on
0 0.0038
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mg/kg
mg/kg x .DD2 =Ibs/dry ton
1000 X S.34 X %solids X sp. gravity
2000
"=dry tons/ 1000gal."

Analytical Results
U.S, Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive bate: 03/24/2020
Reported: 0413012020
For: Spindale
Comments:
A Ni LY1ICAL.
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200324-25-01 2 30 Day Benchscale Spindale <1 % EPA625-n-nA 03/24/2020 WC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 38

30 Day Bench Worksheet Sample Ill # 200,5ZU , 2 5
WEEK 1
Samples
' Total Solids
Volatile Solids
% Volatile Fraction
t
2
1
cD
3
�J zi
Avers e:J.
0 . 2
7 '
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
X
"-'
S
2
1 1 05
LO
3
G.
_
I
n
Avera e:
Z
e
WEEK 3
Sam les
Total Solids
Volatile Solids
I % Volatile fraction
I
0,22
2
2
.3
61
12.
3
Avers e:
�j
_0
0 -j 99
5
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
b
2
3
- 3;—)
I�
i
5 1 3
2
Average:
3G' Cj
WEEK S
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
. 2 `7
_�
51 S 5
2
0.2
5i
3
0.
_.
Average:
3 5
WEEK b
Samples
Total Solids
Volatile Solids
% Volatile Fraction
AOC
_ 2
0.
0- 14
5 5
3
.2Ci
O a
r
Average:
0-2-7
Van Kleeck Reduction: Initial% Vol. Frac. __Final % Vol. Frac. X 100 = %
Initial /o Vol- Frac. - (Initial % Vol. Frac. X Final % Vol. Frac.)
FINAL RESULT L _%LC_ D,

Client:
VS
-I3.0sor:dr �"��.
T
RTATcGVII.! f
�, ANALYIICAL
122Cnw(1trod • PO.baa229
Smtewfil4 NC 296RT
f7Ekf872-4697
Chain of
Custody Record
Address: jµ�' -
._._ ........
ContadPerson: �7 PhoneM 3,•;� �74 ���� �FAXA
G — --
Po RequWfionedply. MWO i"
Cueroew
s.�ple IDe
fee•ro a
rime Sampled
lamb owyl
aw Sampled
hrerMlen "meow ror Mrlyur.
Raiinquiehad by: - - _
Received by: _ 1!�
Relinquished by:
Received by.
Compowto s.magns n:
Time begin am, pm Data --J_/_
Time end am, pm Date —J _J_-.
Time begin am, pm Date —J_J—
Time and am, pm Date
Time 9: !S am, �rt1} mate .1"_ILIJ-20 Sampled by:
7i %�
Tne u1N "� Date / !^` Transported by: 7
Time am, pm Date _l�fielding times met'
Time am, pm Dais _!�_
Compliance work:
Non-compliance work:
Lab Comnwws- sarnow rrensportod on lam:
n
00
W
rat
U
z
a
w
00
rN
r4
x
0
m
O
0-

rraleor.eeewe
ANALYTICAL RESULTS
Pace Mwytiral SeMcr. LLC
9e0o I(inray Ave. Sine 100
lirreerev". NC 26076
(704)8754092
Project: US. Bic. Spindele
Pace Project No.: 92470M
Sample: 280324,25.01 Lab 13: 9247099MOI Catfectad: 0312412012:45 Recaived: 03f25f20 11:32 Maf7itt: Solid
Raauhs reported on a dry w&Vht' baste and am a4ustad for percent nwfstrrat sampin afse and any d1hroorm
Comments: • $temples requiring VwmiW preservatkm wrote fo:oK-ad outside of recommended tamperstwe limits of 0-0 degrees Celsius.
Parameters ReSuOa Unit Report Llrni OF Prepared Analyzed CAS No. Quail
ChloMM"Hwb.(GC)8161A Analytical Method: EPA 8151APreparationMeOwd:0151A
Leachate McCiodtData: 1311: 03r28/20 15-06 Initial pH: 6.98; Final pH: 4.96
Pace National - ML Jullet
2,4,5-TP (SWait) ND myL 0.00200 1 03131120 21:16 04/02/26 01:47 93.72-1
2,4-0 NO r119/L 0.00200 1 0313V20 21;16 04IC2120 01:47 94-75-7
Sunoyatu
2,44OCAA (S) 59.8 % 14.0-158 1 03/31/20 21:16 D4/02/20 01:47 19719.2&9
5081 TCLPPesticidas RYE
Analytical Method: EPASNIB Preparation Method: EPA3510C
Laachale Method/Date: EPA 1311; 03/2&20 16.12
Pace Anatybcat Servioes - Charlotte
gamma-BHC (Lindane)
NO u9iL
0.50 1
0313012D 17:06 04101120 1711 5849-9
Chlordane (Tedmical)
NO ug/L
3.0 1
03IW20 11:06 04MV2017:21 57-74.9
Endrin
NO u9R
0.50 1
03r3Ur2017:06 D"WO1T21 72.20-8
Heptachlor
NO u9+L
0.50 1
031301201T06 041011201721 7644-8
Heptachlor epoxide
NO ug&
0.50 1
0313012017:06 0410112D 17:24 1024-67-3
Methoxyahlor
NO ug/L
1000 1
0313012017:06 0410112017:21 72-43-5
Toxapheae
NO ugR
3.0 1
03130M1T06 D410112017:21 $001-35-2
Surrogates
De iphenyl (S)
78 %
10-138 1
0313=01T06 04101120 17:21 2051.24.3
Teraddow4wxylene (S)
86 %
10-110 1
0313012017:06 WWI() 17;21 577-09-6
0082 TCLP PCBs RYE
Analytical Method: E PA W82A Preparation Method: EPA 351 DC
Leachate MathodfDale: EPA 1311: 03/26QO 16:12
Pace Analytical Services - Charlotte
PCB-1016 (Aroebr 1016)
NO u91L
1000 1
Or30120 17:41 04/01/20 DO:25 12674.11.2
PCB-1221 (ArOCW 1221)
NO ug/L
1000 1
03/30120 17:41 04101120 00:25 11104.2&2
PCB-12321Aroclor 1232)
NO ug1L
10DO 1
03/30/20 17:41 04101/2000:25 11141-1&5
PCB-1242 (Amclor 1242)
NO ug/L
1000 1
03/30/20 17:41 04/01R000725 53469.21-9
PCB-1248 (Aroclor 1248)
NO ug/L
1000 1
03/30120 17:41 04/0112000:25 12672.29.E
PCB-1254 (Arodor 1254)
ND uglL
1000 1
03130/20 17:41 0"V20 OC:25 11097- i9.1
PCB-1260 (Arbclor 1260)
NO uQ&
1000 1
03130M 17:41 04M 20 00:25 11 OW62.5
Su►rogates
DecacNgrpbiphenyl(S)
91 %
10-132 1
D3130120 17AI 04/01r2C OC:25 2051-24-3
"ll0 MET ICP, TCLP
Analytcal Method: EPA 60100 Preparation Method: EPA 301 DA
Leachate Ma9m4tiate: EPA 1311; 04J05120 16:29 Initial pH: 7.79: final pH: 4.5
Pace Analytical Services - Ashevf0a
Arsenic
NO M91L
0.050 1
04106r20 12:15 04/07/20 U2:52 7440-38-2
Barium
NO mg1L
0.25 1
04108120 1215 D4107120 02:52 7440.39-3
Cadmium
NO m9/L
0-0050 1
04/08/20 12A5 04107/2D 02:52 744043-9
Chromium
NO mgrL
0.050 1
04106/20 12:15 04/D7/20 02:52 7440-47-3
Lead
NO m91L
0,025 1
04106/20 12:15 D4107120 02:52 7439-92-1
Selenium
NO m91L
0.10 1
04106I2012:15 0410712002:52 778249.2
Silver
NO nuyL
0.025 1
MM201215 0410712002:52 7440-224
REPORT OF LABORATORY ANALYSIS
Thin re" Shell not be reprnaucea, except
in h A.
Date: 04/07/2020 04:48 PM
r.:thrr.4 the wnftn taneanl o1P" Anaytlr:ai Services. LLC.
Page 5 of 28
PO Box 228 a Statesville, NC 28687 a 704/972/4697
Page 15 of 38

sear�eariaau
ANALYTICAL RESULTS
Projecr US. Bio. Spindale
Pace Project No.. 92470996
Pau Anaiytlur Services, LLC
91100 Kincey Me. Suha 100
Hunleravlle. NC 2E07a
1704R175.9092
Sample: 2M324.Y5.01 Lab ID: 92470906001 CONBCted: 0324/20 12'45 Received: 03125120 1132 Maf : Sold
Raaalb r,PoAert' an a 'dry wslyhe basis and an &#ustad farptult:snt -*!stars, rrampfs stra and any offilw Ions.
Corrawts: - Samples +squiring thermal preservation were recelved outside of recommended temperature limits of 0-0 degrees Celsius_
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. dual
7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Daw EPA 1311; 04/05120 15:29 Initial pH: 7.79; Final pH: 4.5
Pace Analytical Services, Asheville
Mercury NO m1171- 0.110020 1 04107/2010:46 04/07/2014:07 7439-97-6
8270E TCLP RVE
Analytical Method: EPA 6270E PreparaWn Method: EPA 35TOG
Pace Analytical Services - Charlotte
1,4-Dichlombenune
NO
ug1L
50.0
1
03130120M50 03r312017:10 106-46-7
2,4-Dini0rotoq,ene
NO
ug/L
50.0
1
03r302020:50 03/3u20171a 121.14-2
Hexadittiml,34Mwiene
NO
ug/L
50.0
1
03/30I20 20:50 03r3120 17:10 87.68.3
HexacNorobenzene
NO
ug1L
50.0
1
03/30/2020:50 031312017:10 118.74-1
lasadlbroetherle
NO
ug/L
50.o
1
03/3Qr2(120:50 0313112017:10 67-72-1
2-Methylpherwl(o-Creaof)
NO
uOrL
WO
1
1113ld M 20.50 0313112017:10 954&7
3&4-MerhyIptw o(m&p Creed)
NO
u911-
50.0
1
03r3OM 20:50 0313112017:10 15831-10A
Nwobenzens
NO
uglL
50.0
1
03fd M 20:50 03I3112D 17:10 9&95-3
Pentachimophenol
ND
u91L
100
1
03/ WO 20:50 03131/20 1710 87-M-5
Pyridine
NO
ug/L
50.0
1
03r30/20 20:50 03/31/20 17A0 110416-1
2,4,5-Trichlornphenol
NO
ug/L
50.0
1
03/30120 20:50 03/31/20 17:10 95-95.4
2,4,6-Trichbrapheno
ND
ug/L
50-0
1
03130/2020-50 0313112017:10 88-06-2
swropatsa
NRtoberizene-E5 (S)
65
%
12-102
1
03131 120 20:50 03/31120 17:10 416560-0
2-Fluotoblphenyl (S)
58
%
13-107
1
03/30/20 20:50 D3131120 17:10 321-6D-8
T-phenyl-014 (S)
80
%
21-132
1
03/30/20 20:50 03131120 17:10 1718-51-0
Phenol-d8 (S)
30
%
10-110
1
DY30M 20:50 03731/20 1710 13127-88-3
2-FIuorophorloF(S)
20
%
10-110
1
D313GI2020:50 0"1/2017:10 367.12-4
2.4.6-Tdbromophand (S)
33
%
27.106
1
0MMI) 20,50 033120 17:10 116-7M
82601D MSV TCLP
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Benzene
NO
ug/L
1DO
20
04/0412008:20 71-43.2
2-Butwone(MEK)
NO
ug&
200
20
04104/2008:20 78-93-3
Carbon tetrachloride
NO
ug/L
100
20
041042008:20 56-23-5
Chkwobenzene
NO
ug/L
100
20
04104M 06:20 108-90-7
Chlorolwm
NO
ug/L
100
20
04/04170 D8720 67.6&3
1,4-Dkhitxobensana
NO
ug1L
100
20
04/0420 08:20 106-46-7
1,2-DichIocmtKane
NO
trg2
10C
20
04/0420 138:20 107-06-2
1.1-Dldtlorowduna
N0
ug/L
10C
20
04M412008:20 75M-4
Tetradloroelherle
No
ug/L
100
20
04/0420 08:20 127-18-4
Trilhene
NO
ug/L
100
20
04/0408:20 79-01-6
12(I
Vinyl chloride
ND
uglL
100
20
04IW20 08:20 75-01-4
Sunnpallas
1,2-Didllorceils-0-04 (S)
99
%
70-130
20
04/04120 08720 1706M7.0
Tduene-d8 (S)
105
%
67.135
20
041041'20 08:20 2037-26-5
4-arwno8uorobenzene (S)
97
%
70-130
20
040420 08:20 4604)0 4
REPORT OF LABORATORY
ANALYSIS
This report erred not b4 w odwed. esospt in
tua.
Data: 04M72020 04:48 PM
wtthout Iha redden Consent of Pace Anaryar�l Se kes. LLC. Page 6 of 28
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 16 of 38

Pace Anehytlral 1kMow, LLC
4600 Kinsey Ave. Su4e 100
Hurrertviee. NC 25079
(704)375.9W2
Prolett US. 9kx Spindale
Pace Prged No.: 92470995
ANALYTICAL RESULTS
Sample: 20324.25.01
Lab 10: 224711996901 Co(lacted: 0324f20 12;45 Received: 0325M 11:32 Matrix: Solid
Results reporpd on a 'dry ~t' haa/a avid are a*iatad for limmot molserrs, sample she and any dlludoms
Comments: • Samples raWring thermal Preservation were recNved outside of recommended temperature limits of" degrees Celsius.
Parameters
ResuRt Units Report Limp OF Prepared Analyzed CAS No. Ouaf
Percent voistlw
Analytical Method: ASTM D2974.87
Pace Analytical Services - Charlotte
Percent Moohn
9919 % 0.10 1 0410120 16:15
1016 Flashpolyd.Closed Cup
Analytical McMod: EPA 1010A
Pace Analyical Services - Asheville
Flashpoird
�200 dog F 70.0 1 0410620 15:09
9"s PH son
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
PH at 25 Degrees C
7.3 Std. Unts 0.10 1 W1D620 14:D4 H3
911N Faint Flier Llquld Teat
Analytcal Method: EPA 90958
Para Analytical Services - Asheville
Free Liquids
Fall 1.0 1 03/27/20 18.40
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3,3.2
Paco Analytical Services - Greensburg
Cyanide, Reactive
NO mg4cg 248 1 0313020 15:18 03/30720 15:50
734E Reactive Sultlde
Analytical Method: SM 45M2F-2011 Preparation A1eth04 SW-846 7.3.4.2
Pace Analytical Services - Greensburg
SuWe, Reactive
NO m9 9 2480 1 0313012015:18 0313020 15:23
Sample: 2003U25.01
Lab I0: 9247099l002
"acted: 03242012AS
Received: 03I26t20 11:32 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared Analyzed CAS No. Cual
0093 GCS PC6 RYE
Analytical Method: EPA8062A Preparation Method: EPA 3510C
Pace ArWylicat
Services -
Charlotte
PCB-1016(Aroclor1016)
ND
ug1L
1.0
1
03131 f2l) 15,55 0410212020:28 12674-11-2
PCB-1221 (Arodpr 1221)
ND
u91L
1.0
1
03/3112015:55 04/0220 20:28 11104-26-2
PC13-1232 (Afodor 1232)
ND
1497L
1.0
1
03/31120 15:55 04/0220 2026 t 1141.16.5
PCB-1242 (Arocbr 1242)
ND
ug/L
1-0
1
0313112015:55 64/02120 20:28 53469.21-9
PCB-1248 (Amdor 1248)
ND
uWL
1.0
1
03131/20 15:55 041OV20 2028 12672-29-E
PC8-1254 (Arocior 1254)
NO
u91L
1.0
1
0313120 15:55 04/0220 20:28 11097.6go
PCB-1260(Aroclur 1260)
NO
ug/L
1.0
1
03131/20 15:55 04/02/20 20:28 1109&625
strnogaree
Decanhloroblphenyl (5)
64
%
10.130
1
03131M 1515 041022020:28 2051.24.3
REPORT OF LABORATORY ANALYSIS
This report shall nor he mpivduced, except in full,
Date: 04M712020 04:48 PM rvima4"TWOM Consent d Paoa Analyt GW Servroes. LLC. Page 7 0128
PO Box 228 a Statesville, NC 28687. 704/872/4697
Page 17 of 38

Analytical Results
U.S. Blosolid5 Inc
958 Moots Road
Roaring River, NC 28669
Receive Date: 03/24/2020
Reported: 03/26/2020
For: Spindale
Comments: GM 8,195 MPNIg
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200324-26-01
Fecal Coliforms
1
8696
MPNIg
SM92210E-20os
03/25/2020
WC
200324-26-01
Percent Solids
1
0.23
%
sM254W-2011
03/2512020
WC
200324-26-02
Fecal Coliforms
2
8000
MPN/g
SM92210E-2006
03/25/2020
WC
200324-26-02
Percent Solids
2
0.25
%
SM2540a.2011
03/25/2020
WC
200324-26-03
Fecal Coliforms
3
8333
MPNIg
5M92210E-2006
03/25/2020
WC
200324-26-03
Percent Solids
3
0.24
%
SWrAOa-2011
03/25/2020
WC
200324-26-04
Fecal Coliforms
4
8696
MPN/g
SM9221CF-2006
03/25/2020
WC
200324-26-04
Percent Solids
4
0.23
%
SM25406.2011
03/25/2020
WC
200324-26-05
Fecal Coliforms
5
8000
MPN/g
sM92210E-20os
0312512020
WC
200324-26-05
Percent Solids
5
0.25
%
SM2540B-2011
03/25/2020
WC
200324-26-06
Fecal Coliforms
6
8000
MPNIg
S"22'CE-2006
03/25/2020
WC
200324-25-06
Percent Solids
6
0.26
%
SM2540B 201,
03/25/2020
WC
200324-26-07
Fecal Coliforms
7
7692
MPN/g
SM92210E-2006
03/25/2020
WC
200324-26-07
Percent Solids
7
0.26
%
SM25408-2011
03/25/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/8-72/4697
Page I or 4

TOWN OF FOREST CITY
N CO025984

U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
Reported:
For:
Comments:
Analytical Results
01 /23/2020
03/24/2020
FOREST CITY
Sample Number Parameter
Sample ID
Result
200123-30.01
30 Day Benchscale FC
Unit
Method
Analyzed
Analyst
200123-30-01
Aluminum
FC
3.4
a/o
EPAszs.R-szro
Oi123/2020
WC
200123-30-01
Ammonia Nitrogen
FC
7400
mg/kg
Erin 200.7 re�4.4 1994 01/30/2020
MD
200123-30-01
Arsenic -Solid
FC
14451.8
mg/kg
sM4500r4r13BE-1997
01/28/2020
CJE
200123-30-01
Cadmium ICP
FC
e3.11
mg/kg
SM3113 B.2004
02/03/2020
MT
200123-30-01
Calcium
FC
2.9
mg/kg
EPA 200.7
01l3012020
MD
200123-30-01
Copper
FC
9970
mg/kg
EPA 2oa7
01I3012020
MD
200123-30-01
Corrosivity
FC
233
mg/kg
EPA 2oo.7
01129/2020
MD
200123-30-01
Ignitability
FC
See Attached
sw-34s
01/24/2020
PACE
200123-30-01
Lead -Solid
FC
See Attached
1010M
01/24/2020
PACE
200123-30-01
Magnesium
FC
47.10
mg/kg
SM311313
Oi131/202p
MD
200123-30-01
Mercury Solid
1=C
2700
mg/kg
EPA200.1
01/30/2020
MD
200123-30-01
Nickel
0.187
mg/kg
SM3112B-2011'
02/05/2020
MD
200123-30-01
Nitrate/Nitrite -
FC
FC
9.55
mg/kg
EPA207
01/29/2020
MD
Solids
722.581
mg/kg
SM450arrn
02/06/2020
CL
240123-30-01
pH
FC
200123-30-01
Potassium - Solid
FC
5.67
Std. Units
SM45COHB-2011
01/23/2020
CL
200123-30-01
Reactivity
FC
2920
mg/kg
EPnzoo 7
02/03/2020
M'l-
200123-30-01
Selenium Solid
FC
See Attached
sw-aas
01/24/2020
PACE
200123-30-01
T. Phosphorus Solid
FC
3.63
mg/kg
sM3113e
02/03/2020
MT
200123-30-01
TCLP
FC
832.2
mg/kg
SM4500PE-2011
01l3112020
CL
200123-30-01
TKN
See Attached
as Noietl
01/24/2020
FACE
200123-30-01
Zinc
FC
47112.3
mg/kg
g g
sMo�g B-2o1, aSaoN
01/29/2020 CL
FC
1123
mg/kg
Elan 200.7
01/29/2020 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 39

SAR
Sodium Absorption Ratio Na M /L Ca M IL M MIL
Na: Sodium (MgIL) Equivalent weight: 23 160.05 1545.35 1 418.5
Ca : Calcium (MgIL) Equivalent weighty 20
Mg : Magnesium (MgIL) Equivalent weight: 12 6.958fi96 77.2675 34.87]
ME)
Milli Equivalent = MgIL 1 Equivalent weight The amour
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power amount of (
SAR = 0.929304 (From MgIL entered above)
SAR= 0.92924 (From ME entered below)
Na (ME) Ca (ME) Mg (ME} 16
6.96 1 77.3 34.9
Permitting �

Sample #- 200123-30-ol
Client: Southern Sod Builders
30 Day Bench Test- Aerobic Sample Name: FC
EPA625-R-92/0 Sl� 5 0 Collect Di: Jan 23 2020 12�1 5pM
0
Tests: 30 Day
Date began: Digester Dimensions:
knalvst:
Volume of Sample in digester: MIS
Started: C.
rime Sta Tnitial DO reading of sampi 7
rted: 7
Initial Dal DO- '4'13(>2)'re mP: 0,01C DaY6 DO: 4"7()(>2)TCrnP:'�&'ZC
Date: Time-
il L—� Arl Date:
% Total Solids
Dish #:
NO
% Total Solids
-)ry Wt. + Dish Wt.:
Dish Wt.:
•
Dish #:
Dry Wt. + Dish Wt,:
4�.—T701
Sample Wt.:
Wish Wt.:
2-75-
% Total Solids;.
6.6' —
Sample Wt.!
%'rotal Solids:
'/a Volatile Solids
-)TY Wt.& Dish Wt,:
4+ 37 5
% Volatile Solids
Dry WU Dish
Q(��
Ash Wt,-
Wt.:
--". -7
Sample Wt.:
Ash Wt--
Sample Wt-
3, .&
—4 1
� - ----
% Vol. Solids.
% Vol. Solids:5—
Yo Total Solids 2 % Total Solids
Dish #: Dish H:
Dry Wt. + Dish Wt.: Dry Wt, 4 Dish Wt,:
Dish Wt.: Dish Wt,:
Sample Wt.::
LO
% Total Solids: Sample Wt.: %Total Solids;2-
Yo Volatile Solids
DrY Wt.& Dish Wt.: -14- (,020(,�? % Volatile Solids
D
Ash Wu pry Wt.& Dish Wt,: Q 5
-7 7 T
Sample Wt, Ash Wt.:
Sample Wt.:
% Vol. Solids:
% VOL Solids:
Xo Total Solids %Total Solids
Dish #: Dish 4-
)rY Wt, 4 Dish Wt.: l<ODry Wt. + Dish Wt,�,
Dish Wt,:
Sample Wt.: Dish M' wZ5
---
% Total Solids; Sample Wt.: 2 CS
% Total Solids:
Ya Volatile Solids % Volatile Solids
XY Wt.& Dish Wt.: Dry Wt.& Dish Wt.:
Ash Wt.: U,
Sample Wt,:
Sample Wt.: Ash Wt.:
% Vol. Solids:
% Vol, Solids:
(Type here)
PO Box 228 10 Statesville, NC 28687 - 704/872/4697
Page 35 of 39

LaL12 DO. 4-71 (>2) Tem . S c
Date- ! MLL
Yo Total Solids
Dish 4,
Try Wt. + Dish Wt."
Dish Wt.:
Sample wt_'
% Total Solids:
'/o Volatile Solids
3ry Wt.& Dish Wt,:
Ash Wt.: EY
Sample Wt.:
% Vol. Solids:
A Total Solids
Try Wt Dish #:
f Dish Wt,: J4-J
Dish Wt.:
Sample Wt
%"I'Otal Solids:
YE? volatile solids
Dry WU Dish Wt.: )44,
Ash Wt,: _41Ylslqm
Sample Wt.:
% Vol. Solids:
YG Total Solids
Dish
Dry Wt. � Dish Wt.:
Dish Wt.:
Sample Wt.:
% Total Solids:
Yo Volatile Solids
Dry WU Dish Wt.: 4CO, 3761-7
Ash Wt.:
Sample Wt,
% Vol. Solids: —.
[Type here]
Sample JD# 2 0 )/ 2,3, �0. ()I
Dav 18 Do: 4. (>2)Temp:Z.'9C
Date: Time:
% Total Solids
Dish 0:
Dry Wt. + Dish Wt.:
Dish Wt.:
Sample Wt,:
% Total Solids:
% Volatile Solids
Dry WU Dish Wt.:
Ash Wt.:
,Sample Wt.:
% Vol. Solids:
%Total Solids
Dish #:
Dry Wt. + Dish Wt,: dgy
Dish Wt,: CL
Sample Wt,:
% Total Solids:
% Volatile Solids
Dry WU Dish Wt.:
Asti Wt,: 'f' 7
Sample Wt.:
% Vol. Solids:
% Total Solids
Dish 4:
Dry Wt. + Dish Wt,:
Dish Wt.:
Sample Wt.:
%Total Solids:
% Volatile Solids
Dry WL& Dish Wt.: ;LJ _6717
Ash Wu Iq7
Sample Wt.:
% Vol. Solids:
PO Box 228 0 Statesville, NC 28687 v 704/872/4697
Page 36 of 39

2ILLI DO. ' (>2) Temp. �49
Date-- 2 Time /a 14
YcoTotal Solids
Dish #: U.
Dry Wt. 4- Dish Wt.:
Dish Wt.:
Sample Wt.:
'/'u Total Solids:
Yo Volatile Solids
Xy Wt.& Dish
76
Ash Wt.:__
Sample Wt,:
% Vol. Solids:
YaTotal Solids
Dish
Dry Wt. r Dish Wt.:
Dish Wt.: "Ig
Sample Wt.:
..--
% Total Solids;
'/a Volatile Solids
Dry Wt. & Dish Wt,: /71-g
Ash Wt.:
Sample Wt,:
% Vol, Solids:
XoTotal Solids
Dish 4: 10
Dry Wt. + Dish Wt,:
Dish Wt.:
Sample Wt.:
%Total Solids:
Ma Volatile Solids
Dry Wt. & Dish Wt.:, to 12, !UJ4
Ash Wt.:
Sample Wt.:
% Vol. Solids:
[Type here]
Sample I D# 9 0.,-17 3 _-.,; C?-
Day 30 DO - (>2) Temp.- C
% Total Solids
Dish#:
Dry Wt. + Dish Wt: 1/9,
Dish Wt:
Sample Wt:
% Total Solids:
% Volatile Solids
Dry Wt. & Dish Wt:
Ash Wt: _Ir kq
Sample Wt:
% Vol Solids: 0 Ve
Total Solids
Dish#:
Dry Wt. + Dish Wt:
Dish Wt:
Sample Wt:
% Total Solids:
% Volatile Solids
Dry Wt. & Dish Wt:
Ash Wt:
Sample Wt:
% Vol Solids:
% Total Solids
Dish#:
Dry Wt. + Dish Wt:
Dish Wt:
Sample Wt:
% Total Solids:
7—
!�!f' rz
Z
% Volatile Solids
Dry Wt, & Dish Wt:
Ash Wt:
Sample Wt:
% Vol Solids: L2 eg
PO Box 228 * Statesville, NC 28687 0 704/872/4697
Page 37 of 39

VOTE. oil/particle free air was supplied to the bottom of the Digester via a porous stone at a rate sufficient to mix the
;ample
10 day bench checklist —COMPLETE DAILY Sample ID# 20 1 '2 3,30 - of
i**n(,% MFTPD !'AZ TIM0AT1rllAt**i
Water
Sample
Serape
DO Meter
DO Meter^
TDO Meter
Da
I level
Temp 2 C
Solids
_
%
Temp°C
C aI m I,
Comments
I
_
21 11
_. .
3
q
2
g
4 1 ji
'6 1
7
_.. _._
�1..
.1D.
2 2. 5
I_-2
5
5
22•irl
6.5o
10 �,
tI
_�
22 •c
22•�0
I 12 2
`1
�.
[
23. IG
13
10
14
It
15
IZ
17 1
2 3 .
$— + --
'z la --
--_..
_ -
z�._
f
20
20 Iq
_R'7.7
21
23 2 20
242
26 7 2-7
. ✓ ..
/
u
ZZ_
_ ..
27
28
,T^
—
29
30
—
[Type here]
PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 38 of 39

'30 Day Bench Worksheet
WEEK I
Sample I.D # O() 12 3 - -C 01
Samples
Total Solids
Volatile Solids
% Volatile Fraction
�15
2
UI
------------
C�.U3�
S
3
7
1
[.Average:
(;
WEEK 2
Sam Ies
Tntal Solids
Volatile Solids
% Volatile Fraction
5
I
3
tra
D.
Avera e:
C'
Cj ,
WEEK 3
Samples
'Total Solids
Volatile Solids
% Volatile Fraction
1
U. 1-
2
[p
SC
-1
3
Avera e:
LP
U .
WEEK 4
Sampies
Total Solids
Volatile Solids
% Volatile Fraction
1
.t0
2
1,0
;4
3
-7 '51U
Average:
-7 Z
WEEK 5
Sam fes
' Total Solids
Volatile Solids
% Volatile Fraction
1
U
7_ I
z
. 7��
' Avera c;
(} .
0- y
WEEK 6
Samples Total Solids
Volatile Solids
% Volatile Fraction
D , �
Average: [(�'Z
Q
p.�q�)U- G.-1 30 x i GO
I-rap
Van Kleeck Reduction: Initial % Vol. Frac - Final % Vol Frac. X 100 = % Cb� 1
Initial % Vol. Frac. - ( Initial % Vol. Frac. X Final % Vol. Frac) �
FINAL RESULT � • "f a/o l Ot.
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 39 of 39

U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
Reported
For:
Comments:
Analytical Results
01 /2 3/2020
05/08/2020
FOREST CITY
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
200123-33-01
Fecal Coliforms
FC1
70866
MPNIg
SM92210E-2006
01/24/2020
WC
200123-33-01
Percent Solids
FC1
12.7
%
SM2540132011
01/24/2020
WC
200123-33-02
Fecal Coliforms
FC2
67670
MPNIg
SM92210E-2006
01/24/2020
WC
200123-33-02
Percent Solids
FC2
13.3
%
SM25408.2011
01/24/2020
WC
200123-33-03
Fecal Coliforms
FC3
21538
MPN/q
9V92210E-2006
01/24/2020
WC
200123-33-03
Percent Solids
FC3
13
%
srnzfi4oa-zo11
01124/2020
WC
200123-33-04
Fecal Coliforms
FC4
60000
MPNIg
SM92210EE2006
01/24/2020
WC
200123-33-04
Percent Solids
FC4
15
%
SM25406-2a11
01/24/2020
WC
200123-33-05
Fecaf Coliforms
FC5
34483
MPNIg
SM9221Cr-206
01/24/2020
WC
200123-33-05
Percent Solids
FC5
14.5
%
SM2540-2a11
01/24/2020
WC
200123-33-06
Fecal Coliforms
FC6
68182
MPN/g
SM92210E-2006
01/24/2020
WC
200123-33-06
Percent Solids
FC6
13.2
%
SM25403-2011
01/24/2020
WC
200123-33-07
Fecal Coliforms
FC7
34247
MPNIg
SM92210E-2006
01/24/2020
WC
200123-33-07
Percent Solids
FC7
14.6
aka
sM25406-2011
01/24/2020
WC
Respectfully submitted,
Dona Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

,.�aceAnal ical
� wnw.prcds6y.wm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: FOREST CITY
Pace Project No.: 92462234
Semple: Samples-200123.30.01
Results reported on a "dry weight"
Lab ID: 92462234001 Collected: 01/23120 12:15 Received. 01124120 08:54 Matrix: Solid
basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No. pual
Chlorinated Herb. (GC) 8151A
Analylical Method: EPA8151A Preparalion Method: 8151A
Leachale Melhod/Date: 1311:01130120 20:25 fnitiai PH: 6.3; Final pH: 4,87
2A,5-TP (Silvex)
2,4 D
NO mg/L 0.00200 1 02/03720 07:10 02/03120 19:38 93.72-1
Surrogates
NO mgrL 0.00200 1 02103120 07:10 D210312D 19,38 94-75-7
2.4-DCAA(S)
102 % 14.0-158 1 02/03120 07 10 02W2019,38 19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 80818 Preparation Method: EPA 3510C
Leachale MelhodlDate: EPA 1311 01/26120 15:49 Inilial pH; 7.71: First pH: 4
gamma-BHC (Lirdane)
Chlordane (Technical)
ND uglL 0.50 1 01129/20 11:34 01130120 18A2 58--9
NO
Endrin
uglL 3,0 i 0112972011:34 0173012018:02 57-7474-9
NO
Heptachlor
ag1L 0,50 1 01129/2011:34 01/3012018:02 72.20-8
NO
Heptachlor epoxide
ug/L 0.50 1 01129/20 11:34 01/30120 16:02 76.44-8
NO uglL
Methoxychlar
Methoxene
0.50 1 01129/2011:34 0113012018:02 1024-57.3
NO ug1L
1000 1 01129/2D 11:34 01130/20 18:02 72-43-5
NO
Surrogates
ug;L 3.0 1 Ot129120113a 0113012018:02 8001-35-2
Decechlorobiphenyl (S)
Tetrachforo-m•xylene {S)
65 % 10-138 1 01/29/20 11:34 D1l3012018:02 2051-24-3
a2
� 0-110 1 0112912011:34 01/3012018:02 877-09-8
9082 GCS PCB
Analytical Method: EPA 8082A Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 122i}
NO uglkg 261 1 01127120 11:32 0112912000a5 12674.11.2
PCB-221 (Aroclor1221)
NO uglkg 261 1 01127/20 11:32 01129120 00:15 111D4-28-2
ND ugAg
PCB-1242 (Aroclor 1232)
261 1 01/27120 11:32 01/29/20 00:15 11141-16.5
NO uglkg
PCB-1248 (Aroclor 1248
261 1 01127l20 11:32 01129/20 00:15 53469-21-9
NO uglkg
PCB-1248 (Aroclor 1254)
261 1 01127/20 11:32 01/29/20 00:15 12672.29-6
NO uglkg
PCB- 1260 (Arocior 1260)
261 1 0112712011,32 011291200q:15 11097-G9-1
ND uglk9
Surrogates
261 1 01127/20 11 32 01129i20 00:15 11096.82.5
Decachlarobiphenyl(S)
27 %
10-130 1 01127f20 11 32 01/29/20 00:15 2051-24-3
8082 TCLP PCBs RVE
Analylical Melhod: EPA 8082A Preparation Melhud: EPA 351CC
Leachale MelhodlDate: EPA 1311: 01/28/20 15:49 Initial pH: 7,71: Filial pH. 4
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
NO uglL 10DO 1 01129/20 11:34 D120120 15,35 12674-11-2
ND
PCB-1232 (Aroclor 1232)
ug1L 1000 i
uglL
NO OV2912011:34 01130/20 15:35 11141-16.2
PC8.1242(Aroclori242)
1000 1 01129l2011:34 0173012015:35 11141-1G•5
uglL
PCB-1248 (Aroclor 1242)
1000 1 01129120 11:34 01/30/20 15:35 53469-21-9
ND ugll-
PCB-1248 (Aroclor 1248)
1000 1 0112912D 11:34 01130/20 15-35 12672.29-6
NO
PCB-1254 (Aroclor 1254)
uglL 1000 1 01/29120 11:34 0113012D 15:35 11097-69.1
NO
Surrogates
u91L 1000 1 017297201134 OSl3012015:35 1109682-5
Oecachlombiphenyl (5)
61 %,
10.132 1 01129120 11:34 01130120 15:35 2051.24-3
6010 MET ICP, TCLP
Analytical Method; EPA 60100 Preparalion MethodEPA 3010A
Leachale MelhodlDate: EPA 1311: 02103120 17.10 hlitial pH:8.12: Final pH: 4,5
Arsenic
Barium
ND o 911- 0.050 1 021M4120 12:00 02/05120 16:35 7440.38-2
NO
1L
9 0 25 1 02104/20 12:00 02105/20 1635 7440-39-3
REPORT OF LABORATORY ANALYSIS
Dale: 0270712020 04:50 PM
This relowl shall not be rewaducee, except in lull,
without the written Consent of Pace Analytical Services. LLC.
Page 5 of 26
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 13 of 39

/ .;aWnalyfica(
www.pec�A67.tam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kinsey Ave, Suit, 100
HUP11MV111e, NC 28078
(704)875-909z
Project: FOREST CITY
Pace Project No.: 92462234
Sample; Samples-20Q123.30.01 Lab ID: 92462234001 Collected: 01/23/20 12:15 Received: 01124/20 08:54 Matrix: Solid
Results reported on a "dry weight" basis and are adJusted for percent moisture, sample size and any dilutions.
Parameters Results U6ts Report Limit OF Prepared Analyzed CAS No, 0'w
6010 MET ICR TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Dale: EPA 1311.
02143f20 17:10 Initial
pH: 8.12; Final pl-], 4.5
Cadmium
Chromium
NO 111gIL
N
0.0050 1
0210412012:00 02I0512016:35 T440.43.9
Lead
mglL
NCO mglL
0.050 1
02104/2012:00 0210512016:35 7440-47-3
Selenium
NO
0.025 1
02/0412012:00 02/0512016:35 7439-92-1
Silver
rrgNO mgIL
010 1
02/04/2012:00 0210512016:35 7752-49-2
7470 Mercury, TCLP
0.025 1
0210412012:00 02/05/2016:35 7440-22-4
Analytical Method: EPA 7470A Preparation
Method:
EPA 7470A
Leachate MethedlDate: EPA 1311:
02103/20 17:10 Initial pH: 8.12; Final pH: 4.5
Mercury
8270E MSSV TCLP Sep Funnel
ND mglL
0.00020 1
02f04120 13:30 02106120 1209 7439-97-6
Analytical Method: EPA8270E Preparation
Method: EPA 351DC
1,4-Dichlorobenzene
2.4-DlchJo nben a
NO uglL
NO
50.0 1
02104/20 08:07 0210,5120 12:26 106-46-7
HexDinitr o-1,3-butadiene
ug1L
NO uglL
50.0 1
D2104120 08:07 02/05720 12:26 121-14-2
Hexachlorobenzene
NO ug1L
50.0 1
02104/20 08:07 02/05/20 12:26 87-68-3
Hexachloroelhane
NO ug1L
50.1) 1
02/04/20 08:07 0210512D 12:26 118-74-1
2-Methylphenoi(o-Cresol)
NO
50.0 1
02104120 08:07 02105120 12:26 67-72-1
3&4-Melhylphenol(m&p Cresol)
NO ug1L
uglL
50.0 1
02104120 06:07 02105/20 12:26 95-48-7
Nitrobenzene
NO uglL
50.0 1
02/04/20 Q8:07 02/05120 12:26 10831-10.4
Penlachlorophenol
NO ug/L
50.0 1
02/04120 08:07 02/05120 12,26 98-95.3
Pyridine
NO ug1L
100 1
0210412006:07 02f0512012;26 87-86-5
2,4,5-7richloraphenol
NO
50.0 1
02/04120 08:07 02/05120 12:26 110-86-1
2,4, -Trichlorophenot
ug
NO ug/L lL
SQO i
0270412008:47 02105720 1226 95.95.4
Surrogates
50.0 1
02104120 08:07 02105/20 12:26 88-06-2
Nitrodenzene-d5 (S)
37 °o
2-Flucrohiphenyl (S)
33 �0
12-102 1
0210412D 08:07 02/05/20 12:26 4165-60-0
Terpheobiph4 (
40
13-107 1
02104/20 08:07 02105/20 12:26 321-60-8
Phenol-d6 (S)
12 �0
21-132 1
02l04120 05'07 02105120 12:28 1716-51-0
2-Fluorophenoi(S)
18 %
10-11D 1
02104/2008:07 02/0512012:26 13127-88.3
2,4,6-Tribromophenot (S)
4$
10-110 1
02104120 08.07 02105120 12:26 367-124
8260D MSV TCLP
27-108 1
02/04120 08:07 02/05120 12:26 118-79-6
Analytical Method: EPA 8260b
Benzene
2-Butanone (MEK)
ND ug1L
NO
100 20
02/06/20 20:09 71-43.2
Carbon tetrachloride
ug1L
NO ugll-
200 20
D21D6120 20:09 78-93-3
Chlorobenzene
NO uglL
100 20
02106/20 20.09 56.23.5
Chloroform
ND uglL
100 20
0210612D 20:09 108-90-7
1.4-Dichlorobenzene
NO uglL
100 20
02106/20 20:09 E7-66-:3
142-Dichloroethane
ND uglL
100 20
0210612020:09 106-46.7
1,1-Dichloroethene
ND uglL
100 20
02roG120 20:49 107-06-2
Telrachloreethene
NO uglL
100 20
02105120 20:09 75-35-4
Trichloraethene
N D ugfL
100 20
100
02106720 2009 12 T• 18-q
Viny! chloride
Surrogates
ND u01L
20
100 20
02/06120 20:09 79-01-6
1,2-Dichloroethane-tl4 (5)
D21D6120 20:09 75.01-4
100
70.130 20
0210612D 20:09 17060-07-0
REPORT OF LABORATORY ANALYSIS
Date: 02I0712020 04:54 PM
This reporl shall not be repratlucetl,
except in lull,
without the writlen consent u( Pace Analytical Services.
LLC
Page 6 Dl 2e
PO Box 228 • Statesville, NC 28687 + 704/872/4697
Page 14 of 39

Pace Ajiaiytical Services, LLC
aceAna1Xical 9800 KinceyAve Stiita 100
W�"'PiSd�f.r•°em Hunlersville. NC 28078
° f7041875-9092
ANALYTICAL RESULTS
Project: FOREST CITY
Pace Project Nc.: 92462234
Sample: Samptes•200123.30.01 Lab V 92462234001 Collected: 01123120 12:15 Received' 01124120 08:54 Matrix: Solid
Results reported on s "dry weight" basis and are adjusted Far percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
82600 M3V TCLP Analytical Method: EPA82600
Surroga ties
Tcluena•d8 (S)
4-Bromonuorobenzere(S)
102 %
97 %
67-135
70'130
20 02/06l2020:09 203702
20 02106120 20:09 a60-00-4-4
Percent Moisture
Anniytical Method: ASTM D2974-87
Percent Moisture
87.3 %
0.10
7 01724/20 16:41
1010 Flashpolnt,Ctosad Cup
Analytical Method: EPA 1010A
Flashpoint
9045 pH Soil
>200 deg F
Analytical Melhod: EPA 90450
70.0
1 02103l20 13:20
pH at 25 Degrees C
9005 Paint Filter Liquid Test
5.4 Sid, Units
Analytical Method, EPA9095B
0.10
1 0112712D 75:28 H3
Free Liquids
733C S Reactive Cyanide
Pass 1.0 t 01131l201&27
Analytical Method: EPA 9014 Preparation Method: SW-848 7,3,3.2
Cyanide, ReecLye
ND mglk9
7.8
1 01129l20 15:57 01/29/20 1637
734S Reactive Sulfide
Analytical Method: SM 450052E-2011
preparation
Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
78.3
1 01/29/20 15:57 01/29120 16:00
REPORT OF LA130RATORY ANALYSIS
This report slial3 not he reproduced, exrepl in Full•
Date: 0210712020 04:50 PM without the wriryen consent of Pace Analytical Services. LLC
Page 7 of 26
PO Box 228 e Statesville, NC: 28687 e 704/872/4697
Page 15 of 39

CITY OF BELMONT
N C0021181

Waypoint.s
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number : 20-237-0007
Lab No: 73436
Sample ID: Belmont
Test
Moisture
Test
Project Belmont
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypoiritorlalocal.conl
REPORT OF ANAL PSIS
Results Units
96.0
Results Units
MOL
0.010
MQL
Report Date : 09/01/2020
Received : 08/24/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 811812020 13.15
DF Date I Time By Analytical
Analyzed Method
1 08/25/201411 FM SM-2540G
DF Date 1 Time By Analytical
Analyzed Method
Ammonia Nitrogen
3330
mg/Kg - dry
625
1
08/31/20 1SA5
JP3
SM-4500-NH3C
Nitrate4 Nitrite-N
355
mg/Kg - dry
123
1
08/26/20 14:45
7.13D
4500NO3F-2011
Organic. N
40800
mg/Kg - dry
6250
1
08/31/2.0 10:00
CALCULATION
PH
7.3
S.u.
1
08/26/2013:05
ADM
9045D
Total Solids
3.95
%
0.010
1
08/25/20 14:11
FMM
SM-2540G
Total Kjeldahi Nitrogen
44000
mg/Kg - dry
6250
1
08/31/20 10:00
JP3 iM-4500-NFl3CJKP
Phosphorus
22200
mg/Kg - dry
125
1.
08/28/20 04:24
DADS
6010D
Aluminum
47800
mg/Kg - dry
12.5
1
08/28/20 04:24
T3S
6010D
Arsenic
<12..5
mg/Kg - dry
12..5
1.
08/28/20 04:24
]ADS
6010D
Calcium
13100
mg/Kg - dry
1250
1
08/28/20 04:24
]ADS
6010D
Cadmium
<2,50
mg/Kg - dry
2.50
1
08/28/20 04:24
1AD5
6010D
Chromium
91.8
mg/Kg - dry
6.25
1
08/28/20 04:24
JADS
6010D
Copper
343
mg/Kg - dry
12.5
1
08/28/20 04:24
.LADS
6010D
Iron
26800
mg/Kg - dry
250
1
08/28/20 04:24
DADS
6010D
Lead
31.3
mg/Kg - dry
7.50
1
08/28/20 04:24
]ADS
6010D
Magnesium
3080
mg/Kg - dry
125
1
08/28/20 04:24
]ADS
6010D
Manganese
1130
mg/Kg - dry
12.5
1
08/28/20 04:24
T3S
6010D
Qualifiers/ OF
Definitions
Dilution Factor
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

Waypoint,(2) 7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
463s1
ANALYTICAL www.waypointanalytica1.corn
Southern Soil builders Project Belmont
Dennis Key
958 Hoots Road Information ; Report Date : 09/01/2,020
Roaring River , NC 28669
Report Number ; 20-237-0007
Lab No : 73436
Sample [D : Belmont
Test
REPORT OFANAL YSIS
Results Units MQL
Rer.Piveddj : 08/24/2020
Pauric Mc Groary Ph.D,, CPA
Agronomist
Matrix: Solids
Sampled: B/18/202013,15
DF Date / Time By Analytical
Analyzed Method
Mercury
Molybdenum
0.973
mg/Kg - dry
0.363
1
08/27/20 12:10
DD8
SW-7471B
Nickel
<6.25
mg/Kg - dry
6,25
1
08/28/20 04;24
]ADS
60100
Potassium
23.2
mg/Kg - dry
6.2 ,
1
08/28/20 04:24
3ADS
6010D
Selenium
2650
mg/Kg - dry
2.50
1
08/28/20 04:24
)ADS
60100
Sodium
<12.5
mg/Kg - dry
12.5
1
08/2.8/20 04;24
3ADS
6010D
zinc
6100
mg/Kg - dry
625
1
08/28/20 04;24
)ADS
6010D
Sulfur
1610
mg/Kg - dry
31,3
1
08/28/20 04:24
)ADS
6010D
10100
mg/Kg - dry
250
1
08/28/20 04:24
3ADS
6010D
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
MQL Method Quantitation limit
Page 4 of 6

PAN
Mineralization
Rate TICN NH3 NO3
0.3 44000 3330 355
PAN Surface
142211 mglkg 28.442 Ibsldry ton
0 Ibs total PAN
#DIVIO! ibs PAN/acre
PAN Injection
15886 mg/kg 31.772 lbsldry ton
0 Ibs total PAN
#DIVIO! lbs PAN/acre
Dry Tons/1000 gal
0.164715
1st year PAN
Ibs.lacre
Surface ibs_
Surface
_ 01
#DIV/01
1st year PAN
lbs_/acre
Injected lbs.
Injected
0
#DIVIO!
as clecimal Total dry Acres
NO2 % Solids tons/year Applied on
0 1 0.0395
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mglkg
mg/kg x .002 =Ibsldry ton
MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mglkg
mg/kg x .002 =lbsldry ton
1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal."
2000

SAR
Sodium Absorption Ratio
Na: Sodium (MgIL) Equivalent weight, 23
Ca: Calcium (MgIL) Equivalent weight: 20
Mg : Magnesium (MgIL) Equivalent weight 12
Milli Equivalent = MgIL 1 Equivalent weight
Na M IL Ca M IL AAninAnIr
240.95 1 517.45 1 121.66
10..(.MF.)a...(M�. Mg...M..)
Na
47609 25.8725 1 10.13833
SAR- Na Milli Equivalentl[0.5 X (Ca Milli Equivalent + Mg Milli equivalent))0.5 power
SAR = 2.468866 (From MgIL entered above)
SAR= 2.392046 (From ME entered below)
Na ME Ca (ME1 Mg (ME)
10.15 25.87 10.14
The amour
amount of E
Permitting

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 08/18/2020
Reported: 09/22/2020
For: Belmont
Comments:
Sample Number
200818-27-01
Parameter
30 Day Benchscale
Sample ID
BELMONT
Result
_
c1
Unit
%
Method
Analyzed
Analyst
EPA625-R-92ro
08/18/2020
WC
Respectfully submitted,
v -,,A, :YH?t ,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC; 28687 • 704/872/4697
Page 1 of 2

Analytical Results
U.S. Biosolids Inc T_
958 Hoots Road
Roaring River, NC 28669
Receive Date: 08/18/2020
Reported: 08/20/2020
For:
Comments: GEOMETRIC MEAN: 558 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200818-25-01
Fecal Coliforms
131
915
MPNIg
SM92210E-2006
08/19/2020
MI)
200818-25-01
Percent Solids
131
4.37
%
SM254CB-2011
08/19/2020
MD
200818-25-02
Fecal Coliforms
82
444
MPNIg
SM9221CF-2006
08/19/2020
MD
200818-25-02
Percent Solids
132
4.5
%
SM254OB-2011
08/19/2020
MD
200818-25-03
Fecal Coliforms
B3
<452
MPN/g
SM92210E-2005
08/19/2020
MD
200818-25-03
Percent Solids
B3
4.42
%
SM25406-2011
08/19/2020
MD
200818-25-04
Fecal Coliforms
B4
463
MPNIg
SM92210E-2006
08/19/2020
MD
200818-25-04
Percent Solids
B4
4.32
%
SM25406-2011
08/19/2020
MD
200818-25-05
Fecal Coliforms
65
<472
MPNIg
SMWMr-2006
08/19/2020
MD
200818-25-05
Percent Solids
B5
4.24
%
SM25402.2o11
08/19/2020
MD
200818-25-06
Fecal Coliforms
36
942
MPNIg
SM92210E-2006
08/19/2020
MD
200818-25-06
Percent Solids
B6
4.25
%
SM254OB-2011
08/19/2020
MD
200818-25-07
Fecal Coliforms
137
446
MPNIg
SM92210E-2006
08/19/2020
MD
200818-25-07
Percent Solids
B7
4,48
%
SM25403-2011
08/19/2020
MD
Respectfully submitted,
bVc
L
Dena Myers
NC Cert #440,
NCDW Cert 937755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Analytical Results`At
' '^
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 08/18/2020
Reported: 09/08/2020
For: BELMONT
Comments:
Sample Number
Parameter
Sample ID Result
Unit Method
Analyzed
Analyst
200818-26-01
Corrosivity
See Attached
SW-846
08/20/2020
PACE
200818-26-01
Ignitability
See Attached
1010M
08/20/2020
PACE
200818-26-01
Reactivity
See Attached
SW-846
08/20/2020
PACE
200818-26-01
TCLP
See Attached
as Noted
08/20/2020
PACE
Respectfully submitted,
r j,9 VA."jYY)- f� )
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Sox 228 - Statesville, NC 28687 • 704/872/4697
Page 1 of 30

ZaceAnaiytical
YMrpptNtiOn
1
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 10o
Huntersvdle. NC 28078
[phone]
Projed: 8elmont
Pace Project No.: 92491728
Sample; 200818.26,01
Results reported on a 'dry weight'
Lab ID: 92491728001 Collected: 08118/20 13:05 Received; 0812D120 11:47 Matrix: Solid
basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
OF Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 08125I20 09:28
Initial pH: 6.74; Final pH; 4.92
Pace National - Mt. Juliet
2,4,5-TP (SSlvex)
ND mglL 0.0020D
1 08/27/20 06,55 08127120 13:12 93-72.1
Surro
Surrogates
ND mg1L 0.00200
1 08/27120 06:55 08/27120 13:12 94-75-7
2,4-DCAA(S)
49.2 % 14.0-158
1 08f27120 06;55 08127/20 13:12 19719-28-9
$081 TCLP Pesticides RYE
Analytical Method: EPA 8061 B Preparation Method: EPA 3510C
Leachate Methodl0ate. EPA 1311; 08/26/20 12:00 tnibal pH; 4.99; Final pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
Chlordane (Technical)
ND uglL 0.50
ND
1 09102120 13:00 09103l20 12;23 58-89-9
Endrin
uglL 3,0
NO
1 091OD2013:00 091031201223 57-74-9
Heptachlor
u91L 0.50
NO
1 0910212013:00 0910312012:23 72-20-8
Heptachlor epoxide
ugJL 0.50
NO ugJL
1 09102/20 1100 09/03/20 12:23 76.44-8
Methoxyc
a 50
ND
1 09102/20 13:00 09/03/20 12:23 1024.57-3
Toxaphene
ugJL 1000
NDg1L
1 09/02/2013:00 0910312012:23 72-43.5
Surrogates
3.0
1 0910212013:00 0910312012:23 8001-35.2
Dewchlorobiphenyl (S)
Tetrachloro-m-xylene (5)
124 % 10.154
44
1 09IG2120 13:00 09103/20 12:23 2051-24-3
% 10.184
1 09/02/20 13:00 09103/20 Q2 23 877-09-8
8082 TCLP PCBs RVE
Analytical Method: EPA 8062A Preparation Method: EPA 3510C
Leachate MethodfData: EPA 1311; 08/26120 12:00
Initial pH: 4.99; Final pH: 5
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
NO ugJL 1000
1 09/02120 08:44 09/03/20 05;49 12674-11-2
PCB-1232 (Aroclor 1232)
NO uglL 1000
NO ugJL
1 09102I20 08:44 09/03/20 05:49 11104-28.2
PCB-1242 (Aroclor 1242)
1000
NO ugJL
1 09/02/20 08:44 D9103120 0549 11141-16-5
PCB-1248 (Aroclor 1248)
1000
ND ugJL
1 09/02/20 08:44 09/03120 05:49 53469-21.9
PCB-1254 {Aroclor 1254)
1000
ND ugJL
1 09/02/20 08:44 09/03/20 05:49 12672.29-6
PCB-1260 (Aroclor 1260)
1000
NO ug/L
1 09102l20 08:44 09/03/20 05A9 11097-69-1
Surrogates
1000
1 09/02120 08:44 09/03120 05:49 11096.82-5
Decachlorobiphenyl (S)
114 % 10.1 Bi
1 09/02120 08:44 09103/20 05:49 2051-24.3
6010 MET ICP, TCLP
Analytical Method: EPA 601 DID Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 08/26/20 13:00 Initial pH: 5.9; Final pH: 2
Pace Analytical Services - Asheville
Arsenic
Barium
ND mg1L 0.050
NO
1 081281200211 0B12912022:11 744018.2
Cadmium
mg1L 0.25
NO mg1L
1 08/28120 02:21 08/29/20 22:11 7440-39-3
Chromium
00050
ND mg1L
1 08/28/20 02:21 08/29/20 22:11 7440.43-9
Lead
0.050
NO mg1L 0.025
1 08/28/20 02:21 05/29120 22:11 7440-47-3
Selenium
NO mg/L
1 08128/20 02:21 08/29/20 22:11 7439.92-1
Silver
0,10
ND mglL 0.025
1 08/28120 02:21 08/29/20 22:11 7782-49-2
1 08/28/20 02:21 08129120 22,11 7440-22-4
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except In MI.
Date: p910412020 05 01 PM wilhoul the written consent of Pace Analytical Services, LLC.
Page 5 of 27
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 8 of 30

aceAinalytical e
trYns,MleYe6tLsen
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suile 100
Hunterswile, NC 28078
(700815-9092
Project: Belmont
Pace Project No.: 92491728
Sample: 200818.26.01 Lab ID: 92491729001 C011ected: 08118J20 13:05 Received: 0812012C 11:47 Matrix; Solid
Results reported on a 'drywalght' basis and are adjusted for percent niolsturs, sample slre and any dilutions.
Parameters Results Units Report Limit DF Prepared Araiyzed CAS No. 4ual
7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate MelhodlDate; EPA 1311; D8128120 13:00 Initial pH: 5.9; Final pH; 2
Pace Analytical Services - Asheville
Mercury NO mglL 0.00020 1 08/28/2010:00 08/2812012:46 7439-97-6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate Method/Date:
EPA 1311; 08128120 12:00 Initial
pH: 4.99; Final pH: 5
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
NO
uglL
50.0 1
09102/2011:02 0910312012:31 106.46.7
Hexachloro-1,3-butadiene
ND
ND
ug1L
uglL
50.0 1
0910212011:02 0910312012:31 121-14-2
Hexachlorobenzene
ND
50.0 1
09J0212011:02 0910312012:31 87-68.3
Hexachloroethane
NO
ug1L
50.0 1
09/02120 11;02 O9tO3120 12:31 110-74-1
2-Methylphenol(o-Cresol)
NO
ug1L
ug1L
50.0 1
09102J2011:02 09/0312012:31 67-72.1
3&4-Methylphenol(m&pCresol)
ND
ug1L
50.0 1
0910212011:62 0910312012:31 95-48-7
Nitrobenzene
NO
50.0 1
0910212011:02 0910312012:31 16831-10A
Penlachlorophenol
NO
ug1L
50.0 1
0910212011:02 0510312012:31 98.95-3
Pyridine
ug/L
100 1
0910212011:02 09/03/2012:31 87-86-5
2,4,5-Trichlorophenol
NO
ND
ug1L
50.0 1
0910212011:02 0910312012:31 110-86-1
2,4,6-Trichlorophenol
NO
uglL
%0 1
0910212011T02 09/03t2012:31 95-95A
Surrogates
uglL
50.0 1
09I0212011:02 09/0312012:31 88-06.2
Nitrobenzene-dS (S)
2-Fluorobiphenyl (8)
81
%
13-130 1
091OV20 11:02 09103/20 12:31 4165.60-0
Terphenyl-d14 (S)
56
112
%
13-130 1
09/02/20 WU2 09103/20 12:31 321-60.8
Phenoi-d6 (S)
68
%
25-130 1
09/02/20 11:02 09/03/20 12:31 1718-51-0
2-Fluorophenol (S)
76
%
%
10-130 1
09/02120 11:02 09/03/20 12:31 13127-88.3
2,4,6-Tribromophenol (S)
78
10.130 1
09102J20 11:02 09103120 12:31 367-12.4
%
10.137 1
09102/20 11:02 09/03/20 12:31 118.79-6
82600 MSV TCLP
Analytical Method: EPA8280D Leachate Method/Date:
EPA 1311: 08/28/20
Pace Analytical Services - Charlotte
10:57
Benzene
2.Butanone (MEK)
NO
NO
ug/4
100 20
08/30/20 20 56 71-43-2
Carbon letrachlor de
ND
ug1L
ug1L
200 20
100
08/30120 20:56 78-93-3
Chlerobenzene
NO
ug1L
20
100
08/30/20 20:56 56-23-5
Chloroform
NO
ug1L
20
08130/20 20:56 108-90-7
1,4-Dichlorobenzene
NO
uglL
100 20
100
08/30/20 20:56 67-66.3
1,2-Dichloroethane
ND
ug1L
20
08/30120 20:56 106-46-7
1,1-Dichloroethene
NO
ug1L
100 20
08/30/20 20:56 107-08-2
Tetrachloroethene
NO
ug1L
100 20
08/30120 20:56 75-35-4
Trichloroethene
NO
ugJL
100 20
08130120 20:56 127-18.4
Vinyl chloride
NO
ug1L
100 20
100
08/30120 20:56 79-01-6
Surrogates
20
4 Ofi130120 20:56 75-01
1,2-Dichloroethane-d4 (S)
Toluene-08 (S)
106
%
70.130 20
08130/20 20:56 17060-07-0
4-Bromonuofobenzene (S)
107
103
%
%
67-135 20
08130120 20:66 2037.26-5
70-130 20
08130/20 20:56 460-00.4
REPORT OF LABORATORY ANALYSIS
Date: 09104/2020 05:01 PM
This repdrl shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 27
PO Box 228 a Statesville, NC 28687 e 704/872/4697
Page 9 Of 30

�IaceAnalXical r
e'W"ItalsssAws
ANALYTICAL RESULTS
Pace Analytical Services, LLC
91100KinceyAve. Suite too
Huntersville. NC 28018
[phone]
Project: Belmont
Pace Project No.: 92491728
Sample: 200318-26.01
Lab ID: 92491728001 Collected: 08l18120 13:05 Received: 08/20/20 11:47 Matrix: Solid
Results reported on a 'dry weight -basis and are adjusted for percent moisture, sample alze and any dlludons,
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No, Qust
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
96.6 % 0.10 1 08/20/20 18:34
1010 Flashpolnt,Closed Cup
Analytical Method: EPA 1010A
Pace Analytical Services - Asheville
Flashpoint
>200 deg F 70.0 1 09J02l20 13:26
9045 pH Soil
Anatytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6,7 Sid. Units 0.10 1 08l2412014727 H3
9095 Paint Filter Liquid Test
Analytical Method; EPA 9095B
Pace Analytical Services - Ashnvilllr
Free Liquids
Fall 1.0 1 0812512D 10:19
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-646 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
NO mglkg 29.2 1 08/24/20 17:48 08/25120 12:03
734S Reactive Sulilde
Analytical Method: SM 45ODS2F-2011 Preparation Method: SW446 7-3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
NO mglkg 292 1 08/24/2017:48 08)24120 18:D0
Sample: 200818.26.Ot
Lab ID: 92491728002 Collected: 08118/2013:05 Received: 08/20/20 11,47 Matrix: Water
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8082 GCS PCB RYE
Analytical Method: EPA 6062A Preparation Method: EPA 3510C i
Pace Analytical Services - Charlotte
PCB-1016 (Arodor 1016)
PCB-1221 (Aroalor 1221)
NO ug& 5.0 1 09/04/20 08:37 09)04120 14:51 12674.11-2
PCB-1232 (Aroclor 1232)
NO uglL 5.0 1 09/04/20 08:37 09104/20 14:51 11104-28.2
NO
PCB-1242 (Arodor 1242)
uglL 5.0 1 09113020 08:37 09/04120 14:51 11141-16.5
ND
PCB-1246 (Arodor 1248)
uglL 5.0 1 09104120 08:37 09/04/20 14:51 53489-21-9
ND
PCB-1254 {Arodor 12541
uglL 5.0 1 09/04/20 08:37 09J04120 14:51 12672-29-6
NO ug1L
PCB-1260 (Aroclor 1260)
5.0 1 09/04/20 08:37 09/04/20 14:51 11097-69-1
ND ug1L
Surrogates
5-0 1 09104/20 08:37 09104/20 14:51 11096-82-5
Decachlorobiphenyl (S)
125 % 10-161 1 09/04/20 08:37 09/04/20 14:51 2051-24-3
REPORT OF LABORATORY ANALYSIS
Dale: 0910412020 05:01 PM
This report shalt not be reproduced, except in full,
without the written Consent of Pace Analytical Services, LLC
Page 7 of 27
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 10 of 30

TOWN OF NORTH WILKESBORO
NC0020761

Waypoint(!D
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
46381 ANALYTICAL www.waypointanalytical.com
Southern Soil Builders
Dennis Key project North Wilkesboro
958 Hoots Road Information : Report Date : 06/11/2020
Roaring River , NC 28669 Received ; D6/03/2020
Report Number : 20-155-0005 R£PORTOFANACYSIS Pauric McGroary
Agronomist
Lab No : 72557
Sample ID ;North Wilkesboro Matrix: Solids
Sampled: 6/ 1/ 2020 12:30
Test Results Units MQL DF Date 1 Time 13y Analytical
Analyzed Method
Moisture
96.8
%
0.010
1
06/05/2016:47
FMM
SM-254OG
Test
Results
Units
MOL
DF
Date I Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
9560
mg/Kg - dry
781
1
06/10/20 14:00
JpJ
5M 4500 NF13C
Nitrate+Nitrite-N
263
mg/Kg -dry
150
1
06/09/20 15:41
ZBD
45DONO3F-2011
Organic N
48800
mg/Kg - dry
7810
1
06/10/20 10:00
CALCULATION
Too tal Solids
6.5
s,u.
1
06/09/20 05:20
JSL
9045D
Total Kjeidahl Nitrogen
3.22
%
0.010
1
06/05/2016:47
FIRM
SM-2540G
58400
mg/Kg - dry
7810
1
06/10/20 10:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
22900
mg/Kg - dry
156
1
06/09/20 22:24
KKM
6010D
Aluminum
56600
mg/Kg - dry
156
1
06/09/20 22;24
KKM
6010D
Arsenic
<15.6
mg/Kg - dry
15.6
1
06/09/20 22:24
KKM
6010D
Calcium
15900
mg/Kg - dry
1560
1
06/09/20 22:24
KKM
6010D
Cadmium
<3.13
mg/Kg - dry
3.13
1
06/09/20 22:24
KKM
6010D
Chromium
93.4
mg/Kg - dry
7.81
1
06/09/20 22:24
KKM
6010D
Copper
569
mg/Kg - dry
15.6
1
06/09/20 22:24
KKM
6010D
Iron
31900
mg/Kg - dry
313
1
06/09/20 22:24
KKM
6010D
Lead
55.6
mg/Kg - dry
9.38
1
06/09/2D 22:24
Kk;M
6010b
Magnesium
4060
mg/Kg - dry
156
1
06/09/20 22;24
KKM
6010D
Manganese
431
mg/Kg - dry
15,6
1
06/09/20 22:24
KKM
6010D
Qualifiers/ DF
Dilution Factor
Definitions
MQL
Method Quantitation Limit
L
Limit
Exceeded
Page 3 of 6

(2)
'O n
7621 W
80
-7 Road, Richmond,
YPOOWa
n
Main $t)4-743-9401 1Fax [phone]
27 -6446
ANALYTICAL
www.waypoiiitarialytical.com
46381
Southern Soil Builders
Dennis Key
Project
North Wilkesboro
Report Date : 06/11/2020
958 Hoots Road
Information :
Received : 06/03/2020
Roaring River , NC 28669
P� {� m` 69a,d'
Report Number : 20-155-0005
REPORTOFANAL VSIS
Pauric MCGroary
Agronomist
Lab No : 72557
Matrix: Solids
Sample ID : North Wilkesboro
Sampled: 6/1/2020 12:30
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
2.73
mg/Kg - dry
0.453
1 06/09/20 12:01 DDB SW-74718
Molybdenum
11.5
mg/Kg - dry
7.81
1 06/09/20 22:24 KKM 6010D
Nickel
33.8
mg/Kg - dry
7.81
1 06/09/20 22:24 Kh,M 60101)
Potassium
4500
mg/Kg - dry
313
1 06/09/20 22:24 KKM 6010D
Selenium
< 15.6
mg/Kg - dry
15.6
1 06/09/20 22:24 KKM 6010D
Sodium
1120
mg/Kg - dry
781
1 06/09/20 22:24 KKM 6010D
Zinc.
1660
mg/Kg - dry
39.1
1 06/09/20 22:24 KKM 6010D
Sulfur
10200
mg/Kg - dry
313
1 06/09/20 22:24 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
gage 4 of 6

PAN
Mineralization
Rate
:5ET84
NH3 NO3
0.3
: _
9560 263
PAN Surface
19695 mglko
39.39 Ibs/drS; tor,
0
Ibs total PAN
#DIVIO!
Ibs PANlacre
PAN Injection
24475 mglkg
48.95 Ibsldry ton
0 Ibs total PAN
#DIV/O! Ibs PAN/acre
Dry Tons/1000 gal.
0.134274
1st year PAN
Surface Ibs.
0
1st year PAN
Injected Ibs.
0
Ibs.lacre
Surface
#DIV/0f
Ibs.lacre
Injected
#DIV/0I
as aecimal Total dry Acres
!NO2 %Solids tons/year A lied on
0 0.0322
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2
mg/kg x .002
MR(TKN-NH3) + l (NH3)+NO3+NO2
mg/kg x .002
=mg/kg
=lbs/dry ton
=mg/kg
=Ibsldry ton
1000 X 8.34 X %solids_ X sp. pravi "=dry tons/1000gat."
2000

SAR
Sodium Absorption Ratio
Na: Sodium (Mg/L) Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L / Equivalent weight
Na M /L Ca M /L M MIL
36,06 1 511,98 130,73
N_a_(ME) CMM9E9
l Mg_LW
1,567826 21 10.89417
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.367035 (From Mg/L entered above)
=SAR= 0.367509 (From ME entered below)
Na (L) Ca (MEN Mg {MEN
1.57 1 25.6 10.9
The amour
amount of E
Permitting

aceAnallytical a
rwtr.y�ega6>t.eara
ANALYTICAL RESULTS
Project: USBIO N. WILKESBORO
Pace Project No.: 92470435
Pace Analytical Sarvlcae, LLC
9800 Kincey Ave. Suite too
huntersville. NC 28078
[phone]
Sample: 200319,22.01 Lab ID: 92470435001 Collected: 03119120 08:30 Received: 03120120 09:30 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted forpercent moisture, sampre size and any dilutions.
Parameters _ Results Units Report Limit OF Prepared Analyzed CAS No. Clual
Chiorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A
Leechate MethodlDate: 1311:03126i20 14:58 Initial pH: 6.32: Final pH: 4.98
Pace National - Mt. Juliet
2.4,5-TP (Sllvex) NO mgiL 0.00200 1 03/31/20 00:12 03/31120 08:09 93-72.1
2,4-D ND mg1L 0.00200 1 03131120 00:12 03/31120 08:09 94-75.7
Surrogates
2,4-DCAA (S)
73.8 %
14.0.168
1 03/31120 00:12 03131/20 08:09 19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081B Preparation
Method: EPA 351DO
Leachate Method/Date: EPA 1311; 03/26120
16:12
Initial pH: 5,78; Final pH: 5.2
Pace Analytical Services - Charlotte
gamma-BHC (Lindens)
ND ug1L
0.50
1 0313WO 17:06 0410112D 15:54 58-89-9
Chlordane (Technical)
NO ug/L
3.0
1 03130/20 1T,06 0410112D 15 54 57-74-9
Endrin
NO uglL
0.50
1 03/301201716 0410112015:54 72-20-8
Heptachlor
ND uglL
0.50
1 03130120 17:06 0410112015;54 76-44-8
Heptachlor epoxide
NO ug1L
0,50
1 03130120 17:06 04101120 15:54 1024-57-3
Methoxychlor
NO uglL
1000
1 03/3012017;06 04101/2015:54 72-43-5
Toxaphene
NO ug1L
3.0
1 03130l2017:06 04/01/2015:54 8001-35-2
Surrogates
Derachlorobiphenyl (5)
113 %
10.138
1 03130I20 17:06 04/01/20 15:54 2D51-24-3
Tetrachloro-m-xylene (S)
65 %
10-110
1 03130/20 IT06 04/01120 15:54 877-09-8
8082 GCS PCB
Analytical Method: EPA8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
NO uglkg
591
1 03/23120 13:27 03/26/20 02:04 12674-11-2
PCB-1221 (Aroclor 1221)
NO ug/kg
591
1 03/23/20 13:27 03/26/20 02:04 11104.28-2
PCB-1232 (Aroclor 1232)
NO uglkg
591
1 03/23/20 13:27 03/26/20 02:04 11141-16-5
PCB-1242 (Aroclor 1242)
NO uglkg
591
1 03123/20 1127 03/26120 02:04 53469-21.9
PCB-1248 (Aroclor 1248)
NO uglkg
591
1 03123120 13:27 03126120 02:04 12672.29-6
PCB-1254 (Aroctor 1254)
NO uglkg
591
1 03/23120 1327 03126/20 02,04 11097-69-1
PCB-1260 (Aroclor 1260)
NO uglkg
591
1 03/23120 13:27 03126/20 02:04 11096-82-5
Surrogates
Decachlorobiphenyl (S)
18 %
10-13D
1 03/23120 13:27 03/26120 02:04 2051-24.3
8082 TCLP PCBs RVE
Analytica) Method: EPA 8082A Preparation Method:
EPA 35100
Leachate Method/Date: EPA 1311; 03126)20 16:12
Initial PH: 5.78, Final pH: 5.2
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
ND uglL
1000
1 03/30/20 17:41 03131/20 23:41 12674-11-2
PCB-1221 (Aroclor 1221)
NO ug1L
1000
1 0313012017:41 0313V2023:41 11104.28-2
PCB-1232 (Aroclor 1232)
ND ug1L
100D
1 03/30/20 17:41 0T31120 23:41 11141.16-5
PCB-1242 (Aroclor 1242)
NO ug1L
1000
1 03/30/20 17:41 03131120 2341 53469-21-9
PCB-1248 (Aroclor 1248)
ND uglL
1000
1 03130120 1T41 03/31120 23:41 12672-29-6
PCB-1254 (Aroclor 1254)
NO ug1L
1000
1 03/30120 17:41 03/31/20 23:41 11097-69-1
PCB-1260 (Aroclor 1260)
Surrogates
NO ug1L
1000
1 03/30/20 17:41 03131/20 23:41 11096-82-5
Decachlorobiphanyl (5)
112 %
10-132
1 03)30120 17;41 03/31120 2141 2051-24.3
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except In rull.
Data: 04103r2020 05:07 PM
without the written consent of Pace AnaEylical Services, LLC.
Page 5 of 28
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 16 Df 39

acMnalytical a
■wrpapNSYs.can
ANALYTICAL RESULTS
Project; USBIO N. WILKESBORO
Pace Project No.: 92470435
Pace Analytical Services, LLC
9600 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sampla: 20D319.22.01 Lab iD: 92470435001 Collected: 03119/20 08:30 Received: 03120/20 09:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted !or percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, clual
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate MethodlDale: EPA 1311; 04/01120
16:10 Initial pH: 7,42: Final pH: 4.5
Pace Analytical Services - Asheville
Arsenic
NO
nI
0.050
1
04102/2011:11 04/0212017:58 7440-38-2
Barium
NO
mg1L
0.25
1
04YO212011:11 04102l2017:58 7440-39-3
Cadmium
NO
mglL
0,0050
1
04/02/2011:11 0410212017:58 7440.43.9
Chromium
NO
mglL
0.050
1
04/0212011:11 0410212017:58 7440-47-3
Lead
NO
mg1L
0.025
1
0410212011:11 0410212017:58 7439-92.1
Selenium
NO
mg1L
0.10
1
04/0212011:11 0410212017:58 7782-49-2
Silver
NO
mg1L
0.025
1
04/0212011:11 041021201758 7440-22-4
7470 Mercury, TCLP
Analytical Method:
EPA 7470A Preparation
Method:
EPA 7470A
Leachate MelhodlDete:
EPA 1311; 04/01120 16:10 Initial pH: 7.42; Final pH: 4.5
Pace Analytical
Services - Asheville
Mercury
NO
mg1L
0.00020
1
04102r2011:35 0410212016:04 1439-97.6
8270E TCLP RVE
Analytical Method:
EPA 8270E Preparation
Method:
EPA 3510C
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
NO
ug1L
50.0
1
03/30120 20:50 03131/20 13:46 106-46-7
2,4-Dinitrotoluene
NO
uglL
50.0
1
0313012020:51) 03131/2013:46 121-14-2
Hexachloro-1,3-butadiene
NO
uglL
50.0
1
03/30120 20:50 03131120 13:46 87-68.3
Hexachlorobanzene
NO
ug1L
50.0
1
03130/2020:50 03131120 13:46 118-74-1
Hexachloroathane
NO
ug1L
50.0
1
03130120 20:50 03131120 13 46 67-72-1
2-Methylphenol(o-Cresol)
NO
ugll-
50.0
1
03/30/20 20:50 03/31120 13:46 95-48-7
3&4-Methyiphenol(m&p Cresol)
NO
uglL
50.0
1
03/30/20 20'50 03/31120 13:45 15831-10-4
Nitrobenzene
NO
ug1L
50.0
1
03130/20 20:50 03/31120 13:46 98.95-3
Pentachlorophenol
NO
ug1L
100
1
03/30/20 20:50 03/31/20 13:46 87-86-5
Pyridine
NO
ug1L
50.0
1
03/30/20 20:50 03/31/20 13:46 110-86-1
2,4,5-Trich1orophenol
NO
uglL
50.0
1
03/30120 20:50 03/31/20 13:46 95-95-4
2,4,6-Trichlorophenol
NO
uglL
50.0
1
03/30120 20:50 01131120 13:46 88-06-2
Surrogates
Nitrobenzene-d5 (S)
89
%
12.102
1
03/30/20 20:50 03131/20 13:46 4165-60.0
2-Fluorobiphenyl (S)
90
%
13.107
1
03130120 20:50 03131120 1146 321-60.8
Terphenyl-04 (S)
108
%
21.132
1
03130120 20:50 03/31120 13:46 1718-51-0
Phenol-d6 (S)
49
%
10.110
1
03/30/20 20:50 03/31120 13:46 13127.88.3
2-Fluarophenol (S)
61
%
10-110
1
03/30/20 20:50 03/31/20 13:46 367-12-4
2,4,6-Tribromophenol (S)
99
%
27-108
1
03130/20 20:50 03/31/20 13:46 118.79.6
8260D MSV TCLP
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Benzene
NO
uglL
100
20
0313112004:46 71-43-2
2-Bulanone (MEK)
3640
uglL
200
20
03131120 04A6 78-93-3
Carbon tetrachloride
NO
ug1L
100
20
03/31120 04:46 56-23-5
Chlorobenzene
NO
uglL
100
20
03/31120 04:46 108-90-7
Chloroform
ND
ug1L
100
20
03/31/20 04:46 67-66-3
1,4-Dichlorobenzene
NO
ug1L
100
20
03131/20 04:46 106-46-7
REPORT OF LABORATORY ANALYSIS
This report shall not ba reproduced. except In Full,
Date: 04/0312020 05:07 PM without the written consent of Pace Analytical Services, LLC,
Page 6 of 28
PO Box 228 a Statesville, NC 28687 9 704/872/4697
Page 17 of 39

aceAnalytical e
r.'pilcNallixe ll
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KmcayAve. Suite 100
Hunlersville, NC 28018
[phone]
Project: USBIO N. WILKESBORO
Pace Project No.: 92470435
Sample: 200319,22,01
Lab ID: 92470435001 Collected:
G3119/20 08:30
Received: 03/20/20 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sampie size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
8260D MSV TCLP
Analytical Method: EPAS2600
Pace Analytical Services - Charlotte
1,2-Dichloroelhane
NO uglL
100
20
03131/20 04A6 107.06-2
1,1-Dichloraelhene
N❑ ug1L
100
20
03/31/20 04:46 75-35-4
Tatrachlaroethene
ND ugiL
100
20
03/31120 04:46 127-18-4
Trichlorcethene
ND ug1L
100
20
0313112004:46 79-01-6
Vinyl chloride
ND ug1L
100
20
03131/20 04:46 75.01-4
Surrogates
1,2-Dichloroelhane-dill (S)
106 %
70-130
20
03/31120 04:46 17060-07-0
Tolueri (S)
104 %
67-135
20
03131120 0446 2037-26-5
4-Bromofluorobenzene (S)
103 %
70-130
20
03131/20 04A6 450-00-4
Percent Moisture
Analytical Method; ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
94.5 %
0.10
1
03/23120 1525
1010 Flashpcint,Clased Cup
Analytical Method: EPA 1010A
Pace Analytical Services - Asheville
Flashpolnl
s200 deg F
70.0
1
03131/20 11:46
9045 pH Soil
Analytical Method: EPA90450
Pace Analytical Services - Asheville
pH at 25 Degrees C
619 Slid. Units
0.10
1
03/30/20 14:34 H3
9095 Paint Filter Liquid Test
Analytical Method: EPA9095B
Pace Analytice! Services - Asheville
Free Liquids
Fall
1.0
1
03/27120 16:40
733C S Reactive Cyanide
Analylicat Method: EPA 9D14 Preparation
Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
N0 mg/kg
17.9
1
03/23120 15:02 03/23/20 15:44
7348 Reactive Sulfide
Analytical Method: SM 4500S2F-2011
Preparation
Method: SW-846 7.3.4.2
Pace Analytical Services- Greensburg
Sulfide, Reactive
NO ni
179
1
03/23/20 15:02 03I23120 15:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In Full,
Date: 0410312020 05:07 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 28
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 18 of 39

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 06/01/2020
Reported: 07/15/2020
For: N Wilkesboro
Comments:
Sample Number Parameter Sample ID Result
200601-16-01 30 Day Benchscale N. Wilkes 12
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Unit Method Analyzed Analyst
EGA625-R-9210 06/01/2020 WC
PO Sox 228 • Statesville, NC 28687 • 704/872/4697
Page 9 of 3

Analytical Results 1
U.S. Biosoilds Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
03/1912020
Reported:
03/20/2020
For:
N. Wilkesboro
Comments:
GM 5545 MPNIg
Sample Number
Parameter Sample ID
Result
Unit
Method
Analyzed
Analyst
200319-20-01
Fecal Coliforms 1
4772
MPNIg
SM92210E-2006
03/19/2020
WC
200319-20-01
Percent Solids 1
4.82
%
SM254OB-2011
03/19/2020
WC
200319-20-02
Fecal Coliforms 2
5000
MPNIg
SM92210E-2006
03/19/2020
WC
200319-20-02
Percent Solids 2
4.60
%
SM264OB-2011
03/19/2020
WC
200319-20-03
Fecal Coliforms 3
6553
MPN/g
SM92210E-2006
03/19/2020
WC
200319-20-03
Percent Solids 3
3.51
%
SM2540B-2011
03/19/2020
WC
200319-20-04
Fecal Coliforms 4
4283
MPNIg
SM92210E-2006
03/19/2020
WC
200319-20-04
Percent Solids 4
5.37
%
SM25408.2011
03/19/2020
WC
200319-20-05
Fecal Coliforms 5
4863
MPN/g
SM92210E•2006
03/19/2020
WC
200319-20-05
Percent Solids 5
4.73
%
SM2549B-2011
03/19/2020
WC
200319-20-06
Fecal Coliforms 6
7849
MPNIg
SM92210E-2006
03/19/2020
WC
200319-20-06
Percent Solids 6
2.93
%
SM25403-2011
03/19/2020
WC
200319-20-07
Fecal Coliforms; 7
7143
MPNIg
SM92210E-2006
03/19/2020
WC
200319-20-07
Percent Solids 7
3.22
%
SM254OB-2011
03/19/2020
WC
Respectfully submitted,
"Op jj�7 f I
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

TOWN OF RUTHERFORDTON
N C0025909

i
Waypo' nt • 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 u Fax [phone]
46381 ANALYTICAL www.waypointanalytical.rom
Southern Soil Builders
Dennis Key Project Rutherfordton Report Date : 05/11/2020
958 Hoots Road Information : Received : 05/04/2020
Roaring River , NC 28669
Report Number : 20-125-0007 REPORT OF ANALYSIS Pauric McGroary
Agronomist
Lab No : 71218 Matrix: Solids
Sample ID : Rutherfordton Sampled: 4/30/2020 12:30
Test Results Units MOO DF Date / Time By Analytical
Analyzed Method
Moisture
98.5
%
0.010
1
05/05/2016:46
ICA
SM-2S40G
Test
Results
Units
MOIL
OF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
17100
mg/Kg - dry
6670
1
05/11/20 14:00
JPJ
SM-4500-NH3C
Nitratei-Nitrite-N
408
mg/Kg - dry
326
1
05/11/20 13:32
7BD
4500NO3F-2011
Organic N
74000
mg/Kg - dry
16700
1
05/08/20 11:00
CALCUI-ATION
PH
6.6
S.u.
1
05/11/20 05:23
JSL
9045D
Total Solids
1.45
%
0.010
1
05/05/20 16:46
.I CA
SM-2540G
Total Kjeldahl Nitrogen
91300
mg/Kg - dry
16700
1
05/08/20 11:00
JPJ
;M-4500-NH3C rKP
Phosphorus
14800
mq/Kg - dry
333
1
05/06/20 15:23
TJS
6010D
Aluminum
18500
mg/Kg - dry
333
1,
05/06/21) 15:23
TJS
60101)
Arsenic
<33.3
mg/Kg - dry
33.3
1
05/06/20 15:23
TJS
6010D
Calcium
9670
mg/Kg - dry
3330
1
05/06/20 15:23
TJS
6010D
Cadmium
<6.67
mg/Kg - dry
6.67
1
05/06/20 15:23
TJS
60101D
Chromium
35,2
mg/Kg - dry
16.7
1
05/06/20 15:23
TJS
60101)
Copper
588
mg/Kg - dry
33.3
1
05/06/20 15:23
'rJS
6010D
Iron
20100
mg/Kg - dry
667
1
05/06/20 15:23
'rJ5
60100
Lead
26.9
mg/Kg - dry
20.0
1
05/06/20 15:23
TJS
60101)
Magnesium
2910
mg/Kg - dry
333
1
05/06/20 15:23
TJS
6010D
Manganese
352
mg/Kg - dry
33.3
1
05/06/20 15:23
TJS
6010D
Qualifiers/ DF
Definitions
Dilution Factor
I_
Limit Exceeded
MQI
Method Quanbtation Limit
Page 3 of 6

Waypoint,(5
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number :20-125-0007
Lab No : 71218
Sample Ib : Rutherfordton
Test
7621 Whitepine Road, Richrnond, VA 23237
Main 804-743-9401 " Fax [phone]
www.waypointanalytical.conl
Project Rutherfordton
Information :
REPORT OFANAC PSIS
Results Units MQL
Report Date : 05/11/2020
Received : 05/04/2020
Pauric McGroary
Agronomist
Matrix: Siolids
Sampled: 4/30/2020 12:30
DF Date 1 Time By Analytical
Analyzed Method
Mercury
<0.933
mg/Kg - dry
0.933
1
05/06/20 13:53
DDH
SW-7471E3
Molybdenum
<16J
mg/Kg -dry
16.7
Nickel
1
05/06/20 15:23
TJS
6010D
18.6
mg/Kg -dry
16.7
1
05/05/20 15:23
TJS
6010D
Potassium
4350
mg/Kg -dry
667
1
05/06/20 15:23
T'JS
6010D
Selenium
<33.3
mg/Kg - dry
33.3
1
05/06/20 15:23
TJS
6010D
<1670
mg/Kg - dry
1670
1
05/06/20 15:23
-fJ5
60100
ZncSodium
1050
mg/Kg - dry
83.3
1
05/06/20 15:23
-TJS
6010D
Sulfur
Sulfur
9600
mg/Kg - dry
667
i
05/06/20 15:23
T]S
6010D
Qualifiers/ DF Dilution Factor — --
Definitions L Limit Exceeded
MQL Method Quantitation Limit
Page 4 of 6

PAN
Mineralization
Rate TKN NHNO3
0.3 91300 1100
8
PAN Surface
31218 mglkg
62.436 lbs/dry ton
0 Ibs total PAN
#DIVIO! jibs PAN/acre
PAN Injection
39768 mglkg
79.536 lbs/dry ton
0 Ibs total PAN
#DIVIO! jibs PAN/acre
Dry Tons11000 gal.
0.060465
1st year PAN
lbs./acre
Surface lbs.
Surface
01
#DIVIO!
1st year PAN
lbs./acre
Injected lbs.
Injected
0
#DJV/0!
rasl decimal Total dry Acres
NO2 % Solids tonslyear Applied on
0 0.0145
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mglkg
mg/kg x .002 =Ibsldry ton
MR(TKN-NH3) + l (NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibsldry ton
1000 X 8.34 X %solids X sp. gravity
2000
"=dry tons/1000gal."

SAR
Sodium Absorption Ratio
Na : Sodium (MgIL) Equivalent weight: 23
Ca : Calcium (MgIL) Equivalent weight: 20
Mg : Magnesium (MgIL) Equivalent weight: 12
Milli Equivalent = MgIL / Equivalent weight
Na M /L Ca M IL M MIL
24.21 1 140.21 1 42.19
Na„(M),
Ca.,_(ME)
MgME),
1.052609
7.0105
3.515833
SAR= Na Milli EquivalenU[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.458821 ](From Mg/L entered above)
CSAR= 0;457604 (From ME entered below)
Na (MEJ Ca �(MMq f ME1.05 73.52
The amour
amount of a
Permitting

U.S. eiosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
Reported:
For:
Comments:
Analytical Results
04/30/2020
06/02/2020
Rutherfordton
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200430-29-01 30 Day Benchscale Rutherfordton 11 % EPA625-R-9210 04/30/2020 WC
200430-29-01 TCLP Rutherfordton See Attached as Noted
05/01/2020 PACE
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 31

30 Day Bench Worksheet Sample ID #' -'930- 29
WEEK 1
Sam les Total Solids Volatile Solids-` VnlaEilc Fraction
2 _
Avera e:
WEEK 2
Sam les l otal Solids Volatile Solids % Volatile Fraction
1
2?
3 5
Avera c.
WEEK 4
Sam les Total Solids Volatile Solids %Volatile Fraction
2 -
WEEK 5
Sam les Total Solids Volatile Solids % Volatile F action
1 � -
2 10.
r
Ar•Cra c: �pµ2' -- 1
WEEK 5
Sara les Total Soliatile Solids "/o Volatile Fraction
3
Averts e:
a
0-'1Hb 0-A5Q
x I W.
0 311�-(0.I19 by 6. Llq�'-)q )
an Kleec.k Reduction; Initial % Vol. Frac. - Final °/a Vol. Frac. X Ioo = o/,,
Initial % Vol. Frac, -- ( Initial % Vol. Frac. X Final % Vol. Frac.)
FINAL RESULT � _"/0 0.1
U. 21�3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 31 of 31

/�,AceAnaVica(
wiral.pitel3bS-00m
ANALYTICAL RESULTS
Pace All,
lylit:ai 3frylGea, LLC
9800 Kincey Ave. Suite 100
Huntersville, 1i0 26078
[phone]
Project. US Siosolids-Ruth
Pace Project No.: 92475930
Lab ID: 92475930i}Di C ollected: 04130I2012:45
Received: Matrix: Solid
Sample: Rutherfordton
"dry weight" basis
f0510 ution2009-07
and are adjusted for percent moisture, sample size and any dilutions.
Results reported on a
Report Limit OF
Prepared Analyzed No. Oual
Parameters
Results Units
_CAS
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA 8151A Preparation Method: 8151A
1311; 05107/20 11:35 Initial pH
6.65. Final pH: 5
1.eachate Method/Date:
Pace National - Mt. Juliet
ND mglL 0.00200 1
05110120 23:33 05/12120 04:03 93-72-1
2,4,5-TP (Silvex)
0.00200 1
05110120 23:33 05112)20 04:03 94-75-7
2 4 D
NO mg1L
Surrogates
% 14.0.158 1
45110120 23:33 05112/20 04:03 19719-28.9
2A-DCAA {S}
626
Analytical Method: EPA 8081B Preparation Melhod: EPA3510C
8001 TCLP Pesticides RVE
Leachete MelhodlDate: EPA 1311, 051C4120 16-28
Pace Analytical Services - Charlotte
ND ugh. 0.50 1
C5105120 17:24 05/07120 17:55 58-89-9
gamma-BHC (Lindane)
3 0 1
05105/20 17:24 05107120 17:55 57-74-9
Chlordane (Technical)
ND ug1L
0.50 1
05/0512017:24 05107120 17:55 72-20.8
Endrin
ND ug1L
NO uglL 0.50 1
05/06120 17,24 05107120 17:55 'I6.44-8
Heptachlor
ND ug11- 0.50 1
05105120 17:24 05/07120 17:55 1024.57.3
Heptachlor epoxide
ND ug7L 1000 1
05105120 17:24 05/0712017:55 12-43.5
Methoxychtor
NO uglL 3.0 1
05105120 17,24 05107i20 1755 9001-35-2
Toxaphene
Surrogates
77 °G 10.138 1
05105120 17:24 05/07120 1 T55 2051-24-3
Decachlorobiphenyl (S)
77 % 10.110 1
05105/20 17:24 05f07120 17:55 877.09-8
Telrachloro-m-xylene (S)
8082 TCLP PC8s RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachale MelhodlDate: EPA 1311; 05/04120 16:2B
Pace Analytical Services • Charlotte
PCB-1016 (Aroc6r 1016)
NO ug7L 1000 1
05105f20 17:24 05107120 21:35 12674-11.2
PCB-1221 (Aroclor 1221)
NO ug7L 1000 1
05105120 17:24 0510712021 35 11104-28-2
PCB•1232 (Aroclor 1232)
NO u9fl- 1000 1
05105/20 1724 05107/20 21:35 11141-16-5
PCB-1242 {Aroclor 1242)
NO uglL 1000 1
05/05120 17:24 05107120 21:35 53469-21-4}
PCB-1248 (Aroclor 1248)
NO ugll- 1000 1
05/05120 t 7 24 05J07120 21:35 12672-29-6
PCB-1254 (Aroclor 1254)
ND uglL 1000 1
05105f20 17:24 05/07120 21:35 11097.69-1
PCB-1260 (Aroclor 1260)
NO ug7L 1000 1
05105/20 17:24 05107120 2135 11096-82-5
Surrogates
Decachlorobiphenyl (S)
77 % 10-132 1
05/05120 17:24 05107120 21:35 2051-24-3
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD Preparation Method:
EPA 301CA
t_eachate MelhodlDate: EPA 1311, 05112/20 14:20 Initial pH: 6.76: Finai pH: 5
Pace Analytical Services - Asheville
Arsenic
NO mg1L 0.050 1
0503120 23:09 0504120 15.44 7440-3B-2
Barium
NO mg11- 0.25 1
C5113120 23:09 0504120 15:44 7440-39-3
Cadmium
NO mg1L 0.0050 1
05113120 23:09 05/14/20 15A4 7440.43.9
Chromium
NO n1911- 0.050 1
C5113/20 23:09 05/14/20 15 44 7440-47-3
Lead
NO mg7L 0.025 1
05113/20 23.09 05114120 15:44 7439-92-1
Selenium
NO mglL 0.10 1
05/13/20 23:09 05114120 15:44 7782-49-2
Silver
NO mglL 0.025 1
05113/20 23:09 05114/20 15:44 7440-22-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full.
Date: 0511512020 04:42 PM
without the written consent of pace Analytical Services,
LLC. Page 5 of 26
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 9 of 31

aceAna,(Xical
www,plcl)ibs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suile 100
Huniersvhe, NC 28078
(704 )675-9092
Project: US Biosolids-Ruth
Pace Project No.: 92475930
Sample: Rutherfordton
Lab ID: 92475930ooi Collected: 04/30120 12:45 Received: 0510V20 09:07 Matrix: Solt
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
_ Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP
Anafytica! Method: EPA 7470A Preparation Method: EPA 7470A `
Leachate Method/Dale: EPA 1311; 05/12/20 14:20 Initial
pH: 6.76: Final pH: 5
Pace Analytical Services -Asheville
Mercury
NO mglL 0,00020 1
05115/20 0935 05/15/20 15:38 7439.97.6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate MethodlDate: EPA 1311; 05104/20 16:28
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
ND uglL 50.0 1
05/05/20 14A1 05/08120 21:01 106-46-7
Hexachlorc-1,3-butadiene
NO uglL 50,0 1
ND
05/05120 14:41 05108/20 21:01 121-14-2
Hexachlorobenzene
uglL 50,0 1
ND
05105/2014:41 0510812021:C1 87-68-3
Hexachforoethane
UgIL 50.0 1
NO
05/05/20 14 41 05/08120 21:01 118-74.1
2-Methyiphenol(n-Cresol)
uglL 50.0 1
NO
05/05/20 14.41 05108/20 21',01 67.72-1
3&4-Methylphenol(m&p Cresol)
uglL 50.0 1
424
G5105120 14:41 05108/20 21:01 95-46.7
Nitrobenzene
uglL 50.0 1
NO
05/05120 14:41 0510B120 21:01 15831.10-4
158313
Pentachlorophenol
ug1L 50.0 1
NO
05/05120 14:41 05/0812D 21:01
Pyridine
uglL 100 1
NO
05105/20 14 41 05l08124 21:01 87-95-5
2,4,5•Trich)orophenol
ug1L 50,0 1
NO ug1L
0510SI20 14:41 05/08/20 21:01 110-86.1
2,4.6-Trichlorophenol
50.0 1
NO uglL
05/05/20 14:41 05108/20 21:01 95-954
Surrogates
50.0 1
05/05120 14:41 O5/C8120 21:01 88-06-2
Ntrobenzene-d5(S)
2-Fluarobiphenyl (S)
39 % 12-102 1
05/05120 14:41 05106/20 21:01 4165-60-0
Terphenyi-d14 (S)
35 % 13-1 D7 1
71
05/05120 14:41 05lOB120 21:01 321-60.8
Phenol-d6 (S)
% 21.132 1
24
05/05/20 14 41 05108120 21:01 1718.51-0
2-Fiuorophenol (S)
% 10.110 1
30 %
05/05/20 14A1 05/08120 21:01 13127-88-3
2,4,6•Tribromophenol (S)
10-110 1
54 %
05/05120 14,41 05108l20 21:01 367-12-4
27-108 1
05/05120 14:41 05/08/20 2101 118.79-6
8260D MSV TCLP
Analytical Method: EPA 62600 Leachate MelhodlDate:
EPA 1311: 05)13120 10:51
Pace Analytical Services • Charlotte
Benzene
2-Butanone {MEK)
ND uglL 100 20
DSli3f20 12:27 71-43.2
Carbon tetrachloride
ND uglL 200 20
NO
05/13120 12 27 78.93-3 vl
Chlcrobenzene
uglL 100 20
NO
05113/2012:27 56-23-5
Chloroform
uglL 100 20
NO
0511312012:27 108-90-7
1,4-Dichlorobenzene
uglk 100 20
NO
051312012:27 67-66-3
1,2-bichioroelhane
uglL tOD 20
ND
05/1312012',27 106-0.6-7
1,1-Dichloroathene
uglL 100 20
NO
05113720 12:27 107-06-2
Telrachloroethane
uglL 100 20
ND
0511312012:27 75-35.4
Trichloroethene
ug1L 100 20
NO ug1L
05/13120 12:21 127-18.4
Vinyl chloride
100 20
NO uglL 100
05/13120 12,27 79-01-6
Surrogates
20
0511312012:27 75-01-4
1.2-Dlchloroethane-d4(S)
101 % 70-130 20
Toluene•d8(Sj
106 0
70
4511312012;27 17060-07-0
4-Bromolluorobenzene (S)
67-135 20
101 %
05113120 12 27 2037-26-5
70-130 20
05113l2012:27 460-00-4
REPORT OF LABORATORY ANALYSIS
Dale: 05/15/2024 04:42 PM
This report shall not be reproduced, except in full,
without the written consen(of Pace Atalylical Services,
I -LC.
Pegg 6 of 26
PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 10 of 31

s ?CeAnalyica(
www.Datr�leds,torn
ANALYTICAL RESULTS
Pace Analytleal 5ervices, LLC
0800 KinceyAve. Suite JOG
tluntersvilie, NC 28078
[phone]
Project: US Biosolids-Ruth
Pace Project No.: 92475930
Sample: Rutherfordton
Results reported on a "dry weight"
Lab ID: 92475930001 Gollecled: 04/30/20 12:45 Received: 05101l20 09:07 Matrix: Solid
basis and
are adjusted for percent moisture, sample
size and any drlutfons-
Parameters
Y Results Units Report Limit OF
Prepared Analyzed CAS No.
Percent Moisture
Analytical Method: ASTM D2974.87^
Pace Analytical Services - Charlotte
Percent Moisture
99.0 % 010 1
05101120 16', 46
1010 Flashpolnt,Closed Cup
Analytical Method: EPA 1010
Pace Analytical Services - New Orleans
Flashpoint
a212 deg F 75,0 1
05114120 11:45
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.6 Std- Units 0.10 1
9095 Paint Filter Liquid Test
Analytical Method: EPA 9095B
05112/20 13:37
Pace Analytical Services-AshevNe
Free Liquids
Fail
1.0 1
05112120 10:19
733C S Reactive Cyanide
Analytical Method: EPA9014 Preparation Moihod: SW-846 7.112
Pace Analytical Services - Greensburg
Cyanide, Reactive
ND mglky 95.1 1
05/06120 17,27 05/06/20 18:56
734S Reactive Sulfide
Anaiylical Method: SM 450052F-2011 Preparation Method SW-846 7.3 4,2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mglkg 951 1
05/06/20 1727 05106120 17:30
Sampre: Ruthertordton- PCB
Lah ID: 92475930002 Collected: pgl30/20 12:45
Received: 05101/20 09:07 Matri), Water
Parameters
_Results Units Report Limit OF
Prepared Analyzed CAS No.
8082 GCS PCB RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
PC8-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
ND uglL 0.50 1
05106120 21,03 05/03120 1228 12674.11-2
PCB-1232 [Aroclor 1232)
NO uglL 0.50 1
ND uglL
05/06120 21 t21 05/08120 12:28 11104-28-2
PCB-1242 (Aroclor 1242)
0,50 1
NO uy1L
05106/20 21:03 D5106120 12:28 11141.16-5
PCB-1248 [Aroclor 1248)
0.50 1
NO
O51oG120 21:03 05I08120 12:28 53469-21-9
PCB• 1248 (Aroclor 1248)
uglL 0.50 1
NO ug1L
05/06/20 21 03 05/08120 12:28 12672-29-6
PCB-1260 (Aroclor 1260)
0.50 1
NO
05/06/20 21:03 05/08120 12:28 11097.69-1
Surrogates
uglL 0.50 1
05106/20 21:03 05/08/20 12,25 11096-825
Decachlorobiphenyl (S)
67 %
10-130 1
05/06120 21:03 05/08120 12:28 2051-24-3
Dale: 05/15/2020 04:42 PM
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced. ezcePt in lull,
without the written consent of Pare Analytica[ seroioes, LLC.
Qua[
H3
Ctu a i
Page 7 of 26
PO Box 228 • Statesville, NC 2868.7 e 704/872/4697
Page 11 of 31

Analytical Results
11:�_
U.S. Blosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
04/30/2020
Reported:
05/01/2020
For:
Rutherfordton
Comments:
GM <1361 MPN/g
Sample Number
200430-28-01
200430-28-01
200430-28-02
200430-28-02
200430-28-03
200430-28-03
200430-28-04
200430-28-04
200430-28-05
200430-28-05
200430-28-06
200430-28-06
200430-28-07
200430-28-07
Parameter Sample ID
Fecal Coliforms 1
Percent Solids 1
Fecal Coliforms 2
Percent Solids 2
Fecal Coliforms 3
Percent Solids 3
Fecal Coliforms 4
Percent Solids 4
Fecal Coliforms 5
Percent Solids 5
Fecal Coliforms 6
Percent Solids 6
Fecal Coliforms 7
Percent Solids 7
Result
<1333
1.50
<1408
1.42
<1316
1.52
<1439
1.39
<1527
1.31
<1274
1.57
<1250
1.60
Unit
MPN/g
%
MPNIg
%
MPN/ 9
%
MPNI 9
%
MPNI 9
%
MPNI 9
%
MPNI 9
°
�0
Method
SM92210E-2006
SM25406-2011
SM92210E-2006
SM25408-2011
SMP2210E-2006
SM25408-2011
SMR2210E-200s
SM25408-2011
SM92210E-200s
SM25409-2011
SM92210E-loos
SM25406-2011
SM92210E-loos
SM25409-2011
Analyzed
04/30/2020
04/30/2020
04/30/2020
04/30/2020
04/30/2020
04130l2020
04130/2020
04/3012020
04130/2020
04130/2020
04130/2020
0413()12020
04130/2020
04/30/2020
Analyst
WC
WC
WC
WC
WC
WC
WC
WC
WC
WC
WC
WC
WC
WC
Respectfully submitted,
1
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 . 704/872/4697
Page 1 of 4

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO13548
Client: Dennis Key
Advisor: Zach Key
%�'r„.,_..•.
Predictive
958 Hoots Rd
Southern Soil Builders
0
Roaring River, NC 28669
958 Hoots Rd
Mehlich-3 Extraction
Soil Report
Roaring River, NC 28669
i
Sampled County: WilkesLinks
to Helpful Information
Client ID: 466849
Advisor ID: 231531
Sampled: 11/09/2020 Received: 11/13/2020 Completed: 12/08/2020 Farm:
Sample ID: DK01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20 Mg S Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 1.5 120-200 0
100 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in g1cnl3; CEC and Na in meg1100 cm3; NO3-N in mgldtttl):
Soil Class: Mineral
I
HM%a WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.92 0.94 7.6 65 2.7 5.2 460 22 52 11
93 95 74 763 763
1404 0.2 3
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.goviagronomil
Report No. FY21-SLO13548
Dennis Key
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
I
I is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronurrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NOs-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.nca r. ov/a ronomi/ob arl4.htm lnd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-I
zinc index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone]
f
Website: www.ncagr.govlagronomil
Report No. FY21-SLO13546
/
Client:
Warren/Lee Walker
Advisor:
Zach Key
�"�
Predictive
4493 Clingman Rd
Southern Soil Builders
,,,��
Ronda, NC 28670
958 Hoots Rd
K
Soil Report Mehlich-3
Extraction
Roaring River, NC 28669
Sampled County: Wilkes
-�'
Links to Helpful Information
Client ID: 444516
Advisor
ID: 231531
Sampled:
Received: 11/13/2020 Completed: 12/08/2020
Farm:
Sample ID: LW1
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tons/acre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-FescuelOGrasslTim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W1V in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dn13]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.41 1.01
15.1 95 0.8 6.8 434 87
85 6
52
209
130
434
434
270
0.2 1
Sample ID: LW2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- FescuelOGrasslTim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in glcrn3; CEC and Na in meg1100 cm3; NO3-N in mg/drrt3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 1,04
17.0 95 0.9 6.7 550 144
82 8
75
189
120
771
771
311
0.2 1
Sample ID: LW3
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
70
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 1.00
18.0 97 0.6 6.9 559 34
88 7
53
156
96
943
943
462
0.2 1
North Carol in
rl
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Aariculture

i NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomcl
Report No. FY21-SL013546
Warren/Lee Walker
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
B
boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for Field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soli class I
an excellent source, 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2 i
1
Mn-1
manganese index
in a ex
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
min anese nsoil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronuthents_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/a.qronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb11000 sq ft, If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.aov/agronomi/obpart4.htm sf;nd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-1, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SI 013549
NA
Client: William (Bill Jr)/Kathleen Porter
Advisor:
Zach Key {
Builders Soil B S
Predictive
1{
3573 Greenhorn Rd.
Southern ouers
i
�I= ��
Roaring River, NC 28669
958 Hoots Rd
River, NC 28669
_
s. Soil Repof Mehlich-3 Extraction
Sampled County :Wilkes
Roaring
-- Links to Helpful Information
Client ID: 151551
Advisor
ID: 231531
Sampled: 11/09/2020 Received: 11/1312020 Completed: 12/07/2020 Farm:
Sample ID: BP01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20 Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrasslTim, M 0.0 120-200 0
0 0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - WIV in g/cmr3; CEC and Na in meg1100 cm3; NO3-N in mgldd]:
Soil Class: Mineral
HM% WN CEC BS% Ac PH P-1 K-1 Ca% Mg%
S-1 Mn-1 Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0,92 1.05 13.3 87 1.7 6.1 300 252 54 24
65 144 102 460
460
226
0.2 2
Sample ID: BP02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20 Mg S Mn
Zn
Cu
B
Information E
Lime History:
1- FescuelOGrasslTim, M 0.7 120-200 0
0 0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - WIV in glcrr�; CEC and Na in meg1100 cm3; NO3-N in mglda]:
Soil Class: Mineral
HM% WN CEC Bs% Ac pH P-1 K-1 Ca% Mg%
S-I Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.81 0.94 11.1 81 2.2 5.7 312 113 58 18
63 173 121 787
787
1775
0.1 1
Sample ID: BP03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
`K20 Mg S Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.3 120-200 0
70 0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in glcm}; CEC and Na in meg1100 cm3; NO3-N in mgldrr�]:
Soil Class: Mineral
i
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 0.96 13.4 86 1.9 5.9 389 34 71 13
82 159 112 658
658
1078
0.2 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Aariculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.govlagronomil
Report No. FY21-SL013549
William (Bill Jr)/Kathleen Porter
Page 2 of 3
Sample ID: BP04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5 K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 1.0
120-200 0 60
0
0
0 0
0 0
Note: 12
2- 0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm):
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-1 Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 1.04 12.7 81 2.4 5.6 311 41
67 13 68 112
84
576 576
701 0.2 2

NCDABCS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomil
Report No. FY21-SLO13549
William (Bill Jr)/Kathleen Porter
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
Mn-All
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-1
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
min anese nsail class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Microautrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/aqronomi/pubs.htm.
NOa-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawnslgardens, are listed in units of lb11000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncaqr.govIaL7ronomilobpart4.htm and information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-I
zinc index
remaining 16 (P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm

NCDABCS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomc
Report No. FY21-SL019723
k
Client: Charlie Killian
Advisor:
Zach Key
Predictive
fTAr
114 Kimmswick Rd
Charlotte, NC 2$214
Southern Soil Builders
958 Hoots Rd
"C� Mehlich-3 Extraction
Soil i l Report
Roaring River, NC 28669
g
r
Sampled County: Gaston
Links to Helpful Information
Client ID: 272310
Advisor
ID: 231531
Sampled: 11/25/2020 Received: 11/30/2020 completed: 01/27/2021
Farm:
Sample ID: MH21
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O Mg S
Mn
Zn
Cu
8
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.4
120-200 0
100 0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - WN in glcrrf ; CEC and Na in meg1100 cm3; NO3-N in mg/drri3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.56 0.99 8.2 83 1.4 5.8 71 19
62 19
43
258 172
290
290
347
0.1 1
Sample ID: MH24
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- FescuelOGrass/Tim, M 1.0
120-200 0
100 0 0
0
0
0
0
Note: 12
i
2 - 0.0
Test Results [units - W!V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.92 1.00 7.3 71 2.1 5.5 258 20
57 13
63
220 149
646
646
576
0.2 3
Sample ID: MH25
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-FescuelOGrasslTim, M 1.0
120-200 0
110 0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class.
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-Ali Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.97 0.89 6.5 69 2.0 5.4 213 17
56 11
80
244 163
613
613
648
0.2 3
North Carolina
��=[rtea:� artag! fs•�?ti�,ira;:�s�;+ats�-r,
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO19723
Charlie Killian
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
a
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to $ inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at onf
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be �> 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations givers. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
Mn-All
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ibll000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/oboart4.himt f ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertifizerl
P205
phosphate
S-1
sulfur index
Test Results
j SS -I
soluble salt index
j WN
weight per volume
zn-AI
zinc availabilityindex
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
I Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-Ali, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.govlegronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO20226
Client:
Evelyn Davis
Advisor:
Zach Key
Predictive
318 McKinney Mill Rd
Southern Soil Builders
'r +
Ellenboro, NC 28040
958 Hoots Rd
Meh)ICiI-3
Soli Report
Extraction
Roaring River, NC 28669
Sampled County : Rutherford
Links to Helpful Information
Client ID: 514904
Advisor
ID: 231531
Sampled: 11/23/2020 Received: 11/30/2020 Completed: 01/29/2021
Farm:
Sample ID: RD1A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information E
Lime History:
1-FescuelOGrass/Tlm, M 0.6
120-200 0
70
0 0
0
0
0
0
Note: 12
2 - 0.0
i
Test Results (units - W/V in glcrrf3; CEC and Na in meg1100 cm3; NO3-N in mg1drrt3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-1
Na ESP SS-1 NO3-N
0.32 1.20 3.8 63 1 A 5.5 80 33
44 15
32
177
123
177
177
92
0.1 3
Sample ID: RD1B
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - FescuelOGrass/Tim, M 0.8
120-200 50
100
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results junits - W!V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldrrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-I
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 1.02 6.1 70 1.8 5.5 38 19
51 18
42
207
141
149
149
122
0.1 2
Sample ID: RD2
Recommendations: Lime
Nutrients (lblacre)
More
f
Crop (tonslacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrasslTim, M 0.7
120-200 10
100
0 0
0
0
0
0
Note: 12 i
2 - 0.0
Test Results [units - WN in g/cm73; CEC and Na in meg1100 cm3; NO3-N in mg/clnr]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0,41 0.97 7.8 76 1.8 5.6 57 22
57 18
47
93
73
129
129
165
0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxter. Commissioner of Acriculture

i NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO20226
Evelyn Davis
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib11000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-i levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to Note: Secondary Nutrients and Micronutrients In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncag r.gov/agronomilpubs. htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncaor.govlacironomi/oboart4.htmt #sf,nd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WiV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS-1, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.pov/apronomi/uyrst.htm

NCDABCS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomit
Report No. FY21-SLO17652
' ' k
Client:
Larry Bailey
Advisor:
Zach Key
" Predictive
2174 Salem Church Rd
Southern Soil Builders
�t�
Bostic, NC 28018
958 Hoots Rd
` `' Soi I Report Mehlich-3
"
Extraction
Roaring River, NC 28669
Sampled County : Rutherford
Links to Helpful Information
Client ID: 492927
Advisor
ID: 231531
Sampled: 11/23/2020 Received: 11/25/2020 Completed: 01/14/2021
Farm:
Sample ID: LB1
Recommendations. Lime
Nutrients (lb/acre)
More
Crop (tonstacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.3
120-200 10
30
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units -WN in glcrr?; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-Ali Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.66 0.95 7.0 82 1.2 5.8 58 59
59 20
38
123
91
209
209
191
i
0.1 1 I i
Sample ID: LB2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonstacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- FescuelOGrass/Tim, M 0.0
120-200 0
10
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W1V in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldrn3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-Ali Mn-AI2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.66 0.94 10.6 86 1.4 5.9 105 77
60 23
37
100
77
322
322
213
0.1 1
Sample ID: LB3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonstacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage 0.6
180-220 0
80
0 0
0
0
0
0
Note: 3
2 - 0.0
Test Results [units - WN in 91cm3; CEC and Na in meg1100 cm3; NO3-N in mgldmP]:
Soil Class:
Mineral
HM% W1V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-Ali Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS -I NO3-N
0.60 1.01 6.3 77 1.4 5.6 154 60
57 15
38
146
105
293
293
281
0.1 2
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner ofAcfriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.govlagronomi/
Report No.
FY21-SL017652
Larry Batley
Page 2 of 3
Sample ID: LB4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.4
120-200 0
0
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results (units - WN in
g1cm3; CEC and Na in meg1100 cm3; NO3-N
in mg/dm31:
Soil Class:
Mineral
HM% WN CEC BS% Ac PH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-Al
Cu-I Na ESP
SS-1 NO3-N
0,71 1.01 7.9
81 1.5 5.8 139 106
51 23
34
124
91
247
247
170 0.1
1
Sample ID: LB5
Recommendations: Lime
Nutrients (lblacre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, silage 0.0
180-220 0
40
0
0
0
0
0 0
Note: 3
2- 0.0
Test Results [units - WN in
glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac PH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.56 1.07 9.6
92 0.8 6.5 196 84
67 20
42
166
109
467
467
470 0.2
2
Sample ID: LB6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tire, M 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - WN in
g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3];
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.60 1.08 6.7
86 1.0 6.1 91 41
60 23
51
87
68
207
207
230 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO17652
Larry Bailey
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
I Cu-I
copper index
ESP
I
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
I MI
mineral class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
ii Mn-AI2
Mn-I
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
manganese index
notations appear on the soil report, refer to Note: SecondarV Nutrients and Micronutrients In general, homeowners do not
M-0
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/oboart4.htmtl# ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
'test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-Al
zinc availability index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncac7r.qov/a_q nomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone] Websits: www.ncagr.gov/agronomi/ Report No. FY21-SLO19721 i'
Client:
Norman McDaniel
Advisor:
Zach Key
Predictive
167 McKinney Mill Rd.
Southern Soil Builders
Ellenboro, NC 28040
958 Hoots Rd
it Extraction
Soil Report
Roaring River, NC 28669
Sampled
Sampled County : Rutherford
Links to Heipful Information
Client ID: 139529
Advisor ID: 231531
sampled: 11/23/2020 Received: 11/30/2020 completed: 01/27/2021 Farm:
Sample ID: NM01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20
Mg S
Mn
Zn
Cu
B
Information
E! Lime History.
1 - FescuelOGrasslTim, M 0.0 120-200 0
40
0 0
pH$
0
0
0
Note: 12 Note:
2-
Test Results [units - W1V in glcwP; CEC and Na in megi100 cm3; NO3-N in mg1drn3]:
Soil Class.
Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.36 1.16 7,5 97 0.2 7.1 88 49 69 25
30
198
119
173
173
173
0.1 1
Sample ID: NM02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.5 120-200 10
40
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meg/100 cm3; NO3-N in mg1dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.41 1.04 5.3 75 1.3 5.6 61 54 49 21
32
88
70
114
114
85
0.1 2
Sample ID: NM03
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre) N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage 0.0 180-220 10
90
0 20
pH$
0
0
0
Note: 3 Note:
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 1.12 8.0 97 0.2 7.1 78 55 68 26
23
207
125
183
183
179
0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Aariculture

wI-nn9r-c n,--.._.-.-,.o_ no.a_:__ n.-___. 'A...,, -,
i
I
Norman McDaniel
Page 2 of 3
i
Sample ID: NMA
Recommendations:
Lime
Nutrients (lb/acre)
More
E
Crop
(tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.0
0 0
50
0 20 PH$
0
0 0
Note: 3 Note:
2-
Test Results [units - WN in glcrm3; CEC and Na in meg1100 cm3; NO3-N
in mgldm3]:
Soil Class: Mineral
I
HM% WN CEC
BS% Ac PH
P-1 K-1
Ca% Mg%
S-1 Mn-i
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-I Na ESP
SS-1 NO3-N
0.27 1.03 7.5
94 0.5 6.8
70 42
65 26
22 129
76 282
282
189 0.1
1
Sample ID: NMB
Recommendations:
Lime
Nutrients (Iblacre}
More
Crop
(tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History.
1-Soybean
0.0
0 0
70
0 20 PHA
0
0 0
Note: 3 Note:
2 -
0.0
Test Results [units - WN in glcrr?; CEC and Na in meg1100 cm3; NO3-N
in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I Zn-AI
Cu-I
Na
ESP SS-1 NO3-N
0.18 1.24 3.7 87 0.5 6.5 118 36
57 25
15
141
87
139 139
86
0.0
Sample ID: NMC
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn Zn
Cu
B
Information
Lime History:
1- Soybean 0.0
0 0
30
0
20
0 0
0
0
Note: 3
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N
in mgldm3]:
Soil Class:
Mineral
i
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-Ali
Mn-Al2
Zn-i Zn-AI
Cu-I
Na
ESP SS-1 NO3-N
0.41 1.07 7.8 91 0.7 6.5 177 59
72 15
24
266
162
385 385
416
0.1
1

NCDABCS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLC19721
Norman McDaniel
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
Bs%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib11000 sq ft) at on�t
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate]
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
copper index
ESP
ESP
exchangeable sodium percent II
€! Fertilizer
HM%
percent humic matter
f Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
4 lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
I K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
i Mg%
%CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
i Mn-Al2
Mn-availability index for crop 2
1 Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.govlagronomilpubs.htm.
NO3 N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home fawns/gardens, are listed in units of Ib11000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncavr.aov/aaronomi/obroart4.htmtlt ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-I
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.Qov/aQronomi/uvrst.htm

I NCDABCS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO21310
k
Client:
Frank / Sherry Lawson
Advisor.
Zach Key
s f Predictive
232 Ellenbom Henrietta Rd I PO
Box
Southern Soil Builders
1061
958 Hoots Rd
Mec-x
Soil Repoft h hli
Extraction
ti t 3 E
Ellenboro, NC 28040
Roaring River, NC 28669
g
.$
�Links to Helpful Information
Sampled Count Rutherford
P Y -
Client ID: 59779
Advisor 10: 231531
Sampled: 11/25/2020 Received: 12/04/2020 Completed: 02/12/2021
Farm:
Sample ID: FLA1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History.
1-Prairiegrass 0.0
120-200 0
80
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.46 0.94 10.0 95 0.5 6.9 70 23
84 9
37
204
119
181
181
165
0.1 i
Sample ID: FLA2
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tons/acre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - FescuelOGrass/Tim, M 0.0
120-200 0
60
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldnt3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 0.93 18.4 99 0.2 7.3 206 39
89 9
53
732
437
765
765
399
0.1 1
Sample ID: FLB1
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P205
K20
Mg S
Mn
Zn
cu
B
Information
Lime History:
1- FescuelOGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; GEC and Na in meg/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-Alt Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.96 20.4 99 0.2 7.2 278 140
86 10
58
1338
801
927
927
389
0.1 0
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&GS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL021310
Frank / Sherry Lawson
Page 2 of 3
Sample ID: FLB2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0
0
pH$
0
0 0
Note: 12 Mote:
2- 0.0
Test Results [units - W1V in
g1cm3; CEC and Na in meq/100 cm3; NO3-N
in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.71 1.06 8.6
92 0.7 6.6 90 82
63 25
35
184
118
130
130
248 0.1 1
Sample ID: FLB3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - FescuelOGrass/Tim, M 0.0
120-200 0
80
0
0
pH$
0
0 0
Note: 12 Note:
f
2- 0.0
Test Results [units - WN in
g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.41 0.92 19.1
97 0.6 7.0 306 28
88 9
55
192
117
340
340
439 0.2 1
Sample ID: FLB4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
i Lime History:
I _Fescue/OGras5/Tlm, M 0.0
120-200 0
10
0
0
pH$
0
0 0
Note: 12 Note:
2- 0.0
Test Results [units - WIV in
glcnii; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS%, Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.46 0.96 12.5
93 0.8 6.6 157 71
79 12
54
597
366
303
303
295 0.2 2
Sample ID: FLC1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-FescuelOGrass/Tim, M 0.0
120-200 20
0
0
0
0
0
0 0
Note: 12
2- 0.0
Test Results [units - W1V in
glcm3; CEC and Na in meq/100 cm3; NO3-N in mgldrn
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.51 0.96 7.6
85 1.1 6.0 51 128
60 17
37
1244
763
322
322
162 01 1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO21310
Frank / Sherry Lawson
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to Note: Secondary Nufn, nts_and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.govlaqronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncapr.gov/agronomi/obpart4.htn*fsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cud, S-I, SS-1, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaqr.clovlagronomiluvrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P2O5
phosphate
S-1
sulfur index
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index