WQ0031314_Residual Annual Report 2020_20210226

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?*
Annual Report Year*
Permit Number (IR)*
Applicant/Permittee
Email Notifications
........................................................................................................................................................................
Does this need review by the hydrogeologist?*
Regional Office
CO Reviewer
Admin Reviewer
* Annual Report
* Residual Annual Report
r Additional Information
r Other
2020
W00031314
Winston-Salem/Forsyth County Utilities Commission
O Yes t: No
Winston-Salem

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NM Staff
Name * William C Brewer
Email Address*
[e-mail]
electronic subntttal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ..........................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363977727
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0031314
Ras Current Existing permit number
Applicant/Permittee Address* 101 N. Main Street, Winston-Salem, NC 207101
Facility Name * Winston-Salem/Forsyth County Utilities Commission DCAR
Please provide comments/notes on your current submittal below.
Attached is the City of Winston-Salem's Annual Class A Residuals Report for the 2020
Calendar year. The permitted facility is the P.W. Swann Water Treatment Plant with the R.A
Thomas and R.W. Neilson Water Treatment Plants permitted as generating facilities on the
permit.
If you have any questions regarding this annual report please contact me at 336-397-7727.
Bill Brewer
Water Treatment Superintendent
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Etc.)
2020 City of Winston-Salem Permit WQ0031314 Residuals
19.87M6
Annual Report 021621.pdf
Upload only 1 RDFdocurrent (less than 250 NB). Miftiple docurrents mist be combined into one PDF file unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center

Raleigh, NC 27699-1617
Signature
Submission Date 2/26/2021

Winston-Salem / Forsyth County
I tffities
Water • Wastewater • Solid Waste
P.W. Swann Water Treatment Plant, 2800 River Ridge Road, Pfafftown, NC 27040
0: 336-727-8000, Ft 336-446-2574, cityofws.org/utilitles
9;1-
Date February/
ebruary x, 2021
TO: North Carolina Division of Environmental Quality
Aquifer Protection -Land Application Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Dear Sir or Madam,
Attached is our 2020 Residuals Land Application Annual Report and supporting documentation for the
City of Winston-Salem's Swann, Thomas and Neilson Water Treatment Plants for permit WQ0031314
Swann Water Treatment Plant
The Swann Water Treatment Plant operated in compliance with all parameters of its permit during the
2020 calendar year. The Swann WTP operates one equalization basin and two residuals lagoons that
produces a Class A Residual, which is 503 exempt. Residuals generated by filter washes flow through an
equalization basin, whereas solids removed from the plant's sedimentation basins flow by gravity directly
to the residuals lagoon in service. The lagoons are operated such that one lagoon accepts residuals while
the other Iagoon is cleaned or in reserve, During the 2020 calendar year, the Swann WTP contracted with
Synagro Central, LLC to land apply 207.05 dry tons of residuals to nearby farmland owned by various
fanners in Forsyth County. Listed below are documents associated with this land application event.
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form RSSF - Annual Rcsidual Sampling Summary Forth
• DEQ Fotn1 RSSF B -Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Pace Analytical (nutrient metal analysis data sheets)
• Lab data sheets front SummitEnvironmental Technologies, Inc. (TCLP, reactivity, ignitability,
and cyanide)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results
City Council: Mayor Allen Jolnes; Denise D. Adams, Mayor Pro Tempare, North Ward; Durban Hanes Backer Northeast Ward; Robert C. Ctark, Wost Ward;
John C. Larson, South Ward; Jeff Maclntash, Norilnyest Ward; Kevin Mundy, Southwest Ward; Annette Scippra, Fast Ward; James Taylor, Or., southeast Ward;
City Manager. Lee D. Garrity
County CommisSloners: David R. Plyler, Chaff; Pon Mattln, Vice chair; Fleming Ll-Amin; Ted Kaplan; Richard V. Unviile; Tanya Mmaniel; 61nHa 0, W hisenhunt;
Call311 or 336-727-8000 County Manager. Dudley Watts, Jr.
Winston-salem/rorsylh County Utility Commission: Randall5. Tuttlo, Chair; L. Wesley Curtis, Jr„ Wm Chair; Ifarard E. Day; Tam Griffin; Yvonne H. Woos;
cilylink rt eilyofws.org Wane Long; Hugh W.lerolean; Chrfs Parker, Donald R. Stewart; Charles Wilson; Allan Younger

Thomas Water 'Treatment Plant
The Thomas Water Treatment Plant operated ill compliance with all parameters of its permit during the
2020 calendar year. During the 2020 calendar year the Thomas WTP hauled 316.31 dry tons to the Manes
Mill Road Landfill located at 325 W. Hanes Mill Road, Winston-Salem, NC 27105.
Neilson Water Treatment Plant
The Neilson Plant operated in compliance with all parameters of its permit during the 2020 calendar year.
The Neilson Water Treatment Plant operates three residuals lagoons and produces a Class A Residual,
which is 503 exempt. Solids from the sedimentation basins flow directly to the residual lagoon in service.
The lagoons are in a rotation so one is in service, one is drying and one is empty and ready to be placed
into service. During the 2020 calendar year EMA Resources, Inc. removed and applied 338.8 dry tons of
residuals on land owned by Roger Spillman. Listed below are documents associated with this land
application event.
Section I
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form DMSDF (Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Fortin (Supplemental Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Fortin RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets fi•om Waypoint (nutrient metal analysis data sheets)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section S
• Field soil sampling results
If you have any questions or require additional information regarding our 2020 Annual Report, please call
Bill Brewer, Water Treatment Superintendent, at [phone].
Sincerely,
5&", 10-,
Courtney L. r' er
Perrnittec:
Courtney L. Driver
Director of Utilities
Utilities Administration
P.O. Box 2511
Winston-Salem, NC 27102
William C. Brewer
Preparer of Annual Report:
William C. Brewer -
Water Treatment Superintendent
Swann Water Treatment Plant
2800 River Ridge Road
Pfafftown, NC 27040

Winston-Salem/Forsyth County Utilities
WQ0031314
2020 Residuals Land Application Report
P.W. Swann Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• TCLP Data (summit Environmental Technologies, Inc.)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results
• Agricultural Lime Application Logs

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT -n:
WQ00031314 FACILITY NAME: Winston Salem - Swam WTP
PHONE: [phone] COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE (please check one): Hi Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes Q No ❑ —► If No skip parts A, B, C and certify form below
Part A*: Part B*:
Volume (dry tons) Recipient Information
Sources(s) (include NPDES 4 if
Month
Amendment/
applicable) Bulking AResidual In Product Out Name(s) Volume (dry tons) Intended use(s)
gent
January
February
March
April
May
June
July
August
September
October
November
Swann WTP 18.83 18.83
December
Swann WTP 188.22 188.22
Total from FORM DMSDF (sup) 0 0 0 0
Totals:
Annual (dry tons): 0 207.05 207.05 0
Amendment(s) used: I Bulki z: trent(s) used:
=, , C:aij— .4K�.4.., a���u AuuiuUuaL uuuiivauvi1 succu �Tkinivi uivi�Lr lsappJT Total Number of Form DMSDF (Supp)L
Part C: '
Facility was compliant during the past calendar year with all conditions of the land application permit p yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No --s If Na, Explain in Namtive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2_ All operation and maintenance requirements were compiled with or, in the case of deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
PC n es for sabmittuta a information, including the possibility of fines and imprisonment for knowing violations."
�•�•Zt�z1 � zl
Signature of Pe tte Date Signature o rep r** Date
(if different from Permittee)
'k*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T _1102 (26)
DE=NR FORM DMSDF (12/2006)

OPERATIONS SUMMARY - ALL OPERATIONS - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
WINSTON-SALEM, NC
WINSTON-SALEM, NC PW SWANN WTP LIQUID
MONTHNEAR
November 2020
December 2020
Report Date: 1/25/2021 3:50:02 PM
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
101,500.00 G 18.83 D 17.08
1,W4,300.00 G 188.22 D 170.71
TOTAL: 1115800-00 G 207.05 D 187.80

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WO Permit Number: WQ0031314 Laboratory:
Facility Name: WINSTON-SALEM, NC PACE ANALYTICAL
Residual Source WQ # or
NPDES#: NCO079821
WWTP Name: PW SWANN WTP
Residual Analysis Data
Product Type
Sample or Composite Date
WPL
09/09/20
WPL
09/09/20
WPL
09/09/20
WPL
09/09/20
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
3.27
4.02
3.61
4.45
Arsenic
75
7.3
4.8
6
3.5
Cadmium
85
<0.63
<0.52
<0.56
<0.47
Copper
4300
62
47
55
45
Chromium
NA
48
32
4D
28
Lead
840
24
15
21
14
Mercury
57
<0.57
<0.46
<1.1
<0.81
Molybdenum
75
<5
<4.1
<4.4
<3.7
Nickel
420
24
17
22
16
Selenium
100
4.7
4.4
4.1
<3
Zinc
7500
250
270
300
' 80
Total Phosphorus
NA
3700
2400
3100
2700
TKN
NA
24000
1200D
19000
20000
Ammonia -Nitrogen
NA
910
750
1400
1100
Nitrate and Nitrite
NA
22.6
19
24.3
19.7
For surface disposal facilities the ceiling concentration limits listed in this form are not appiicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
pas ' ility f fines and imprisonmen r knowing violations."
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (1212006)
Printed: 1/25/2021 3:51:35 PM For: 2055 04

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WO permit or were analyzed for over the past
calendar year. Use additional forms.as needed.
WQ Permit Number: WQ0031314 Laboratory:
Facility Name: WINSTON-SALEM, NC PACE ANALYTICAL
Residual Source
NPDES # or WQ#: NCO079821
WWTP Name: PW SWANN WTP
Residual Analysis Data
Product Type
Sample or Composite Date
Parameters (mg/kg dry weight)
Aluminium
Calcium
Magnesium
pH (s.u.)
Potassium
Sodium
PAN
SAR (Ratio)
WPL WPL WPL WPL
09109/20 09/09/20 09/09/20 09/09/20
160000
110000
140000
100000
1800
2200
2100
1400
1800
1500
1900
130D
6.50
6.60
6.70
6.70
1900
1500
2000
140D
<310
<260
<280
<230
<9714
<4894
<7764
<8130
0.2225
0,2091
0.2016
0.2234
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment r knowing violations."
ZI
ignature of Preparer " Date
_ ' 4
'Preparer is defined in 40 CFR Part 503.8(r) and 15 A NCAC 2T.1102(26)
Printed: 1/25/2021 4:03:53 PM For: 2055 04 DENR FORM RSSF-B (1212006)

Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form

FACILITY NAME; WINSTON-SALEM, NC
LANDOWNER: CITY OF WINSTON-SALEM
OPERATOR: CITY OF WINSTON-SALEM
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): ' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT #: WQ0031314 FIELD#: NC-FO-000X2-0-0002-
ANNUAL DRY TONS APPLIED: 4.68 SITE #. NC FO 00OX2
PREDOMINANT SOIL SERIES: FAIRVIEW
CROP 1 MAX. PAN: 183 CROP 2 NAME:
Page_ 1
ACRES UTILIZED: 3.0
ACRES PERMITTED: 4.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cord,
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Oate or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
izallon
TKN
Nitrogen
and Nitrite
(Ibslacre)
Application
Month
Solids
Dry Tons/AC
Source
Moist
Inches
Method'
Rate"
Rate"'
mg/kg
mglkg
mg/kg
Amount
UOM
Crap 1
Crap 2
Crop 1
Crop 2
12/10/2020
25.200.00
(G)
4.450
1.559
WSPWSWPL
SUR
0,5
0,40
20,000,00
1,100,00
19.70
25,344
FSH
Dee-20
25,200.00
(G)
' Total 26.344 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.011 0.001 1 0.140 1 0.087 0.044 0.003 0.012 0.050 0,009 0.561 8.417 Date I Lbs1Ac
tbslacre Applied 0.011 l 0.001 1 0,140 1 0.087 1 0.044 1 0.003 1 0.012 0.050 1 0.009
Permit Limit s acre 1st Crop 183
Federal C.P.L.R. (Ibslacre)""" 36,6 34.8 1 1,339.0 267.9 1 15.0 375.0 89.0 2,540.0
W SPW SW PL = W INSTON-SALEM, NC PW SWANN W TP LIQUID
"1 certify, undeflligni
alty oriaw, that this document %vas prepared under my direction or supervision in accordance with a system designed io assure that qualified personnel properly gathered and evaluated the infonttation submitted. I am
aware that ther mlties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required '"' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, [NJ - Injection, SURIN - lncorporation """" C.P.L.R, : Cumulative Pollutant Loading Rate
" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ." See Site pH & Lime Application Records Section of Report
Printed: 112912021 DENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: W INSTON-SALEM, NC WQ PERMIT #: W Q0031314 FIELD#,, NC-FO.ODOX2-0-0001- ACRES UTILIZED: 8.S
LANDOWNER: CITY OF WINSTON-SALEM ANNUAL DRY TONS APPLIEM 16.37 SITE #: NO FO OOOX2 ACRES PERMITTED: 8.5
OPERATOR: CITY OF W INSTON-SALEM PREDOMINANT SOIL SERIES: FAIRVIEW CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE WAY (FSH) CROP 1 MAX. PAN: 216 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): ` See list at bottom of report
Gallons (G)
i i
Site
]
i
Name �-
of Crap Type
I or Cubic Yards (Y)
+,
Cond.
Precip
Vofatl- Mineral- !
Ammonia
j Nitrate
PAN Applied
Receiving Residual
Date or or Wet Tons (W)
%
Residual
Dry, Wet,
[ Past 24 Hrs.
Appl[callon
Iizatfon Ization
TKN
Nitrogen
and Nitrite
(lbslacre)
Application
Month Amount UOM—'
[`
Solids i DryTanslAc Source
Moist
I
Inches
i
Method'
III
Rate- Rate"'
mg/kg
mglkg
i mglkg
Crop 1 Crop 2
Crop 1 Crop 2
�FSH
12/12/2020 88,20D.00 (G}
4.450 ?
1.926 WSPWSWPL I�_
�;
_��
SUR
0.5 0.40
—2p,00D.00
1,1DO.OD
i- 19.70
�31.308 'I
I- W
Dac-20 j 6a,200.00 (G)
Total
1.926
Total
31.308 0.000
P I
T Lime Applied
Annual lbslacre Applied
0.013
0.002 0.173
6.108
0X54
i 0.003
O.014 0.062
i 0,012 0.693
10.398
Date LbslAc
r;TJativelbslacreApplied
0.125
I- 0.013 0.596
0.108
0.109
0.007
0125�� 0.168
I 0A23�
2.903
Permit Limit s acre st Crop 216
Federal C.P.L.R. (lbslacre)'"" 36.6 3d.8 r 1,339 0 E 267 9 15A— 375.0 89.Oj 2,500.0 E— i
WSPWSWPL = W INSTON-SALEM, NO PW SWANN WTP LIQUID - -
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted, I am
aware that there are significant pe aICies for submitting false information, including the possibility of fines and imprisonment for knowing violations."
019,101%01�z !
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required "°' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
" Application Method: SUR - Surface, IN,i - Injection, SURIN - Incorporation '"" C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injectionllncorporation 1.0 •"" See Site pH & Lime Application Records Section of Report
Printed: 1/2912021 DENR FORM FSF {1=06)

FACILITY NAME: W INSTON-SALEM, NC
LANs] OWNER: BRANDON JONES
OPERATOR: BRANDON JONES
CROP 1 NAME: FESCUE HAY (FSH)
RE510UAL SOURCE(S):' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT m: WQ0031314 FIELD#A NC-F0-0DX10-0-0001-
ANNUAL DRY TONS APPLIED: 35.07 SITE m: NC FO 0OX10
PREDOMINANT SOIL SERIES: TOMLIN
CROP 1 MAX. PAN: 194 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 11.0
ACRES PERMITTED: 11.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cend.
Precip
Vclati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
lzation
TKN
Nitrogen
and Nitrite
(lbslacre)
Application
Month
Solids
DryTonslAc
Source
I Moist
Inches
Method'
Rate—
Rate"'
mg/kg
mglkg
mglkg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
12/10/2020
50,400.00
(G)
4.450
0.050
WSPWSWPL
SUR
0.5
0.40
20,000.00
1.100.00
19.70
13.824
FSH
12/11/2020
138.600.00
(G)
4.450
2.338
WSPWSWPL
SUR
0.5
0.40
1 20.000.00
1.100.00
19.70
38.016
FSH
Dec-20
185,000.00
(G)
ioim a.100 Total 51.840 0.000
AS CD CU CR PS FIG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.022 0.003 0.287 0.179 0.089 0.005 0,024 0.102 I 0.W9 1,146 17.217 I Date LbslAc
Cumulative Ibslacre Applied 0.022 0.003 0.287 0.179 0,089 0.005 0.024 0.102 0.019 1.148
Permit PAN Limit (lbslacre) 1st Crop 194
Federal C.N,L.R. (Itslacre)' " 36.6 1 34.8 1,339.0 267.9 I 15.0 375.0 89.0 1 2,500.0
WSPWSWPL = W€NSTON-SALEM, NC PW SWANN WTP LIQUID
"1 certify, under penaIt of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are si i if ant pens miffing false information, including the possibility of fins and imprisonment for knowing violations."
2-rZ
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required "-" Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate. Surface 0.5, Injectionllnco poration 1.0 """"" See Site pH & Lime Application Records Section of Report
Printed: 1/29/2021 OENR FORM FSF (12/2DO6)

FACILITY NAME: W INSTON-SALEM, NC
LANDOWNER: TONY APPERSON
OPERATOR: TONY APPERSON
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): 'See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT #: W00031314 FIELD#: NC-FO.006X9.0-0001-
ANNUAL DRY TONS APPLIED: 46.89 SITE #: NC FO 000X9
PREDOMINANT SOIL SERIES: TOMLIN
CROP 1 MAX PAN: 185 CROP 2 NAME;
Page: I
ACRES UTILIZED: 19,0
ACRES PERMITTED: 19.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond_
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
izatlon
TKN
Nitrogen
and Nitrite
(Ibslacre)
Application
Month
Solids
DryTonslAc
Source
Moist
Inches
Method'
Rate-
Rate-
mg/kg
mgtkg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
11/23/2020
28,000,00
(G)
4.450
0.273
WSPWSWPL
SUR
0.5
D.40
20.000.00
1,100.00
19.70
4.446
FSH
11/24/2020
42.000.00
(G)
4.450
0,410
WSPWSWPL
SUR
0.5
0,40
20.000.00
1.100.00
19.70
6.670
FSH
11/25/2020
31,500.00
(G)
4.450
0.308
WSPWSWPL
SUR
0.5
0.40
20.000.00
1,100.00
19.70
5.002
FSH
Nov 20
101,600.00
(G)
12/9/2020
69,300.00
(G)
4.450
0.677
WSPWSWPL
SUR
0.5
0.40
20,000.00
1,100.00
19,70
11.005
I FSH
12/10/2020
81,900.00
(G)
4A50
0,800
WSPWSWPL
SUR
0.5
0.40
20,000.00
1.100.00
19.70
13.006
i FSH
Dec-20
161,200.00
(G)
Total 2.468
Total 40.129 0.000
AS
CD
CU
CR
PS HG MO
NI
SE
ZN
P
Lime Applied
Annual Ibslacre Applied 0,017
0.002
0.222
0.138
0.069 0.004 D.018
0.079
0.015
0.888
13.327
Date
Lbs1Ac
Cumulative Ibslacre Applied 0.053
0.006
0.423
0.337
0.120 0.004
0.02E 0.172
0.035
2.686
Permit PAN Limit (Ibslacre) 1 st Crop
185
Federal C.P,L.R. (Ibslacre)"" 36.6 34.8 1.339.0
267.9 15.0 375.0 89.0 2,500.0
WSPWSWPL=WINSTON-SALEM, NC PW SWANN WTP LIQUID
"1 certify, under penalty 1711 W. that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gathered and evaluated the information submitted. I am
aware that there are sign it penalti ling false information, including the possibility
or nines and imprisonment for knowing violations."
-I -ak
SIGFATfJ RE OF LAND APPLIER
DATE
NR = Not Reported or Not Required
"' Mineralization Rates: Compost 0.1, Anaerobically digested-0.2, Aerobically digested-0,3, Raw Sludge-0.4
' Application Method: SUR - Surface, INJ - Injection, SURIN - lncorporation
- C.P.L.R.: Cumulative Pollutant Loading Rate
" Volatilization Rate: Surface 0.5, Injecticn/Incotpotation 1.0
"""" See Site pH & Lime Application Records Section of Report
Printed: 1/29/2021
DENR FORM FSF (1212006)

FACILITY NAME: W INSTON-SALEM, NC
LANDOWNER: EDSEL WOOTON, JR
OPERATOR: EDSEL WOOTON, JR
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): ' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT#: W00031314 FIELD,: NC-YK-COX43.0-0001-
ANNUAL DRY TONS APPLIED: 85.51 SITE #: NC YK 0OX43
PREDOMINANT SOIL SERIES: CLIFFORD
CROP 1 MAX. PAN: 216 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 25.0
ACRES PERMITTED: 25.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX, PAN:
Gallons (G)
Site
Name of Crap Type
or Cubic Yards (Y)
Cone.
Precip
Volali-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
i
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrlte
(lbslacre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method'
Rate—
Rate"
mg/kg
mg/kg
mg/kg
Amount
UOM
Crap 1
Crop 2
Crop 1
I Crop 2 j
1219/2020
107.100.00
(G)
4.450
0.795
WSPWSWPL
SUR
0.5
0.40
20,000.00
1,100.00
19.70
12.926
FSH
12/10/2020
136.E00.00
(G)
4450
1.029
WSPWSWPL
SUR
0.5
0.40
20,000.00
1,100.00
19.70
16.727
FSH
12/11/2020
132,300.00
(G)
4.450
0.982
WSPWSWPL
SUR
0.5
0.40
20,000.00
1,10C.00
19.70
15.967
FSH
12/12/2020
88,200.00
(G)
4.450
0,655
WSPWSWPL
SUR
0.5
0.40
20,000,00
1.100.00
19.70
10.645
FSH
k
Dec-20
466,200.40
(G)
i
L oral s.4o i Total 56.265 0.000
AS CD CU CR PB HG MO NI SE ZN P I
IbslacreApplied 0.024 C.003 0.311 0.194 0.097 0.006 0.026 0.111 0.021 1.246 18,686 Date
dive lbslacre Applied 0.024 0.003 0.311 0,194 0.W7 0.006 0.026 0,111 0.021 1.246
3AN Urns[ (lbslacre) 1$1 Crop 216
Federal C.P.L.R. (lbslacre)"-' 36.6 34.8 1.339.0 267,9 I 15.0 375.0 1 89.0 1 2,500.0
WSPWSWPL= WINSTON-SALEM, NC PW SWANN WTP LIQUID
"I certify, under Wally of law, that this document was prepared under my direction or supervision in accordance with a system dcsia cd to assure that quali 51ed personne) properly gathered and evaluated the information submitted. I am
aware that there , gnifl ena lie Tics for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE t
NR = Not Reported or Not Required """ Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
" Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation ""'" C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 "'""' See Site pH & Lime Application Records Section of Report
Printed: 1/2912021 DENR FORM FSF (1212006)

FACILITY NAME: WINSTON-SALEM, NC
LAND OWNER: JIM STIMPSON
OPERATOR: JIM STIMPSON
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S),' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT M WO0031314 FIELD#: NC-FO-OOX11.0-0001-
ANNUAL DRY TONS APPLIED: 17.54 SITE #: NC FO 00X11
PREDOMINANT SOIL SERIES: OAK
CROP 1 MAX. PAN: 194 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 9.0
ACRES PERMITTED: 9.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
i
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volab-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
I Residual Dry, Wet,
Past24 Hrs.
Application
lization
izatien
TKN
Nitrogen
and Nitrite
(Ibslacre)
Application
Month
; Solids
❑ryTonslAc I Source Moist
1
Inches
Method'
Rate"
Rate—
mglkg
mglkg
mglkg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
12/11/2020
94.560.O0
(G) 4.450
1.948
WSPWSWPL
SUR
0.5
0.40
20,DO0.00
1.100.00
19.70
31.680
FSH
Dec-20
94,500,00
(G)
Total 1.948 Total 31.680 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.014 0.002 0.175 0,109 0,055 0.003 0.014 0.062 0.012 0.701 10.522 Date LbslAc
Cumulative Ibslacre Applied 0.014 0.002 0.175 0.109 0.055 0.003 0.014 0.062 0,012 0.701
Permit PAN Limit (Ibslacre) 1st Crop 194
Federal C.P.L.R. (Ibslacre)"-' 36.6 1 34.8 1 1,339.0 267.9 1 15.0 375.0 1 89.0 2,500.0
WSPWSWPL= WINSTON-SALEM, NC PW SWANN WTP LIQUID
"I certify. under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware Shat there a s' nifcar}l.poaahies For submitting false information, including the possibility of fines and imprisonment for knowing violations."
14! (/ - 2- 1~-17I -
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0.1. Anaerobically digested-0.2, Aerobically digested-0.3, Raw Siudge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation """ C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH 8; Lime Application Records Section of Report
Printed: 1/29/2021 DENR FORM FSF (1212006)

FACILITY NAME: W INSTON-SALEM. NC
LANDOWNER: CITY OF W INSTON-SALEM
OPERATOR: CITY OF W INSTON-SALEM
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S):' See list at bottom of report
Gallons (G)
or Cubic Yards (Y)
Date or
or Wet Tons (W)
%
Month
Amount
UOM
Solids DryTonsiAc
12l1212020
88,200.00
(G)
4,450T
,450 1.926
Dec-20
88,200.00
f
(G)
Total 1.926
lbslacre Applied
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT #: W00031314 FIELD#P: NC-FC-00OX2-0-0001-
ANNUAL DRY TONS APPLIED: 16.37 SITE 4: NC FO COOX2
PREDOMINANT SOIL SERIES: FAIRVIEW
CROP 1 MAX. PAN: 216 CROP 2 NAME:
Cumulative lbslacre Applied 0.125 1 0.013
— - '--- Site
Cond.
Precip Volati-
Residual Dry, Wet,
Past 24 Hrs. Application lization
Source Moist
Inches Method' Rate"
WSPWSWPL
W TSUR 0.5
CR PB I HG
.108 f 0.054 1 0.003
0.007
Page: 1
ACRES UTILIZED: 8.5
ACRES PERMITTED: 8.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Mineral- Ammonia
Nitrate
PAN Applied
ization TKN i Nitrogen
and Nitrite
(lbslacre)
Rate— mgtkg � mglkg
mglkg
Crap 1 Crop 2
0.40 2D,00D.DD 1,100.00
19.70
31.308
MO NI
014 0.062
2.903
Total 31.308 0,000
P I i
of Crop Type
ving Residual
Application
p 1 Crop 2
Date LbslAc
i
Permit PAN Limit (lbslacre) 1st Crop 216
Federal C.P.L.R. (ibsiacre)•••' 36.6 34.8 1,339,0 267.9 1 15.0 375.0 89.0 2,500.0 i
WSPWSW PL = W INSTON-SALEM, NC PW SWANN WTP LIQUID
" 1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. T am
aware that there are significant pegnities far submitting false information, including the possibility of tines and imprisonment for knowing vialatiott9."
rc-x 01 jr_20_�Z I
SIGNATURE OF LAND APPLiER DATE
NR = Not Reported or Not Required "` Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation "•` C.P. L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 "•" See Site pH & Lime Application Records Section of Report
Printed: 1129/2021 DENR FORM FSF (1212006)

Attach this form to the corresponding field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #.-
Operator:
Acres Used:
Winston-Salem, NC Total Dry Tons Applied (Annual): 4.68
WQ0031314 Cation Exchange Capacity (non 503 only):
City of Winston-Salem Owner: City of Winston-Salem Predominant Soil Series: Fairview
3 Acres Perinitted: 4 Site #: NC FO OOOX2 Field #:
FO 000X2 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
❑T/Ac./
o
App.
Event
1.56
Arsenic
0.011
0.000
0.000
0.000
0.000
O.00O
0.000
0.000
0.000
0.000
0.000
0.000
0.011
C-,tdnliunl
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.140
Chroin-iiiiii
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.087
Lead
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Merctuy
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
dentim
Nickel
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Selenium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Zinc
0.561
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.561
Total
Phos-
8.419
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.419
hor tt5
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of tines and
impri nment for knowing violations".
r
Signature of Land Applier Date

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC
WQ0031314
City of Winston-Salem Owner:
8.5 Acres Perfnitted:
Total Dry Tons Applied (Annual): 16.37
Cation Exchange Capacity (non 503 only):
City of Winston-Salem Predominant Soil Series:
8.5 Site #: NC FO 000X2
Fairview
Field #: FO 000X2 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C0111-
positc
Date
Total
P1105-
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
a
App.
Event
1.93
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.173
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.173
Clu•onuun
0.108
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Lend
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Mercury
0.003
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.014
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
denum
Nickel
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Selenium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Zinc
0.693
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.693
Total
Phos-
10.400
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.400
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
l am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprJAgninent for knowing violations".
Signature f Land Appli r Date

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Perinit #:
Operator:
Acres Used:
Winston-Salem, NC Total Dry Tons Applied (Annual):
WQ0031314 Cation Exchange Capacity, (non 503 only):
Brandon .Tones Owner: Brandon Jones Predominant Soil Series:
35.07
Tomlin
1 I Acres Permitted: I 1 Site #: NC FO OOX 10 Field #: FO OOX10 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
Phol-LISIMENNEENEENNE
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
DTIAc./
o
App
Event
3.19
Arsenic
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadnvunl
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.003
Copper
0.287
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.287
Chron-tium
0,179
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.179
Lead
0.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
denuns
Nieltel
0.102
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.102
Selenium
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
1.148
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.148
Total
Phos-
17.215
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
17.215
ilorlls
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I ain aware that there are significant penalties for submitting false information, including the possibility of fines and
impriso ntent for knowing violations".
Signature of Land Applier Date

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC Total Dry Tons Applied (Annual): 46.89
WQ0031314
Tony Apperson Owner:
19 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Tony Apperson Predominant Soil Series: Tomlin
19 Site #: NC FO 00OX9 Field #: FO OOOX9 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Phos-
T�MEEEEEENEEEE
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
2.47
Arsenic
0.017
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.222
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.222
Chromium
0.138
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.138
Lend
0.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Mercury
0.004
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 OMO
0.000
0.000
1 0.004
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.018
denuni
Nickel
0.079
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.079
Selenium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.888
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.888
Total
P1e08-
13.327
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
O.00O
0.000L.327
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including [lie possibility of fines and
impr�onnient for knowing violations".
vvv
Signature of Land Applier Date

Attach this form to the corresponding Field Loading Summary Corm to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC Total Dry Toes Applied (Annual): 86.51
WQ0031314 Cation Exchange Capacity, (non 503 only):
Edset Wooton, Jr. Owner: Edsel Wooton, Jr, Predominant Soil Series: Clifford
25
Acres Permitted: 25 Site #: NC YK OOX43 Field #: YK 0OX43 0001
Residual Analysis Data (Heavy Metals and Total Phospliorus use mg/kg, % Solids use Raw Percent #):
Total
Phos-
Phoro
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
DTIAc.I
o
App.
Event
3.46
14
Arsenic
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.024
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.311
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.311
Chroniiiiiii
0.194
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.194
Lead
0.097
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.097
Mercury
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
M°lye
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
dentin
Nickel
0.111
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.111
Selenium
0.021
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Zinc
1.246
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.246
Total
Phos-
18.689
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
18.689
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualifier) personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
Itnpriso ent for knowin violations".
Signature of and Applier Date

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC
Total Dry Tons Applied (Anneal): 17.54
WQ0031314 Cation Exchange Capacity (non 503 only):
Jim Stimpson Owner: Jim Stimpson Predominant Soil Series:
9 Acres Permitted: 9 Site #: NC FO 00X I I Field #:
Oak
FO OOX11 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
NVIRPWIW
C0111-
posite
Date
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
0
App.
Event
1.95
Arsenic
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadtnlunl
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.175
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.175
Clironiiui
0.109
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.109
Lead
0.055
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
1 0.000
0.000
0.000
0.055
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.003
Molyb-
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.014
denum
Nickel
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
SeleniLan
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.012
Zinc
0.701
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.701
Total
Phos-
10.519
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.519
torus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
impris nment for knowing violations".
-/ 5 z�
Signature o Land Applier Date

Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and
chain of custody's)
• TCLP Data (summit Environmental Technologies, Inc.)
• Copies of our SAR/PAN calculations

(--- ace Analytical 6
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Winston WTP
Lot Number:V110001
Date Completed:09/17/2020
i
09/18/2020 10:36 AM
Approved and released by:
Project Manager II: Lucas Odom
V7 q ACA4B
urrrx,uNVareea'nr1. eow
A C C R E 6 1 T E D
/
TESTING LA TORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 13

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5630
Case Narrative
Synagro
Lot Number: VI14001
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
The following sample was diluted due to the nature of the sample matrix: V110001-001, V110001-002,
V110001-003, V110001-004. Due to low percent solids, the samples were weighed at 3 times the normal
amount. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 13

Client:Synagro Laboratory ID:VI10001-001
Description: Winston WTP 1 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 3.27 09111/2020 0211
Date Received:0911012020
Inorganic non-metals
_
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 09/11/2020 0211 SRB
66315
1 350.1
(Ammonia - N ) 350.1
1 09/15/2020 1536 KMC
66593
1
(Nitrate - N ) 9056A
1 09/16/2020 1349 AMR
66889
1
(Nitrite - N ) 9056A
1 09/16/2020 1349 AMR
66890
1
(Phosphorus) 365.1
5 09/15/2020 1525 DMA
09/14/2020 1326 66566
1
(Soil pH meas) 9045D
1 091141202D 1243 AAB
66608
1 351.4
(TKN) 351.2
1 09/16/2020 1817 DMA
09/16/2020 1136 66562
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.27
%
1
Ammonia - N (gas diffusion)
350.1
910
31
16
mglkg
1
Nitrate - N (soluble)
9056A
19
15
3.1
mglkg
1
Nitrite - N (soluble)
9056A
3.6 J
6.1
3.1
mglkg
1
Phosphorus
7723-14-0 365.1
3700
770
150
mglkg
1
Soil pH measured in water @ 20.7 ° C
9045D
6.5
su
1
TKN
351.2
24000
770
770
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
747113
1 09/11/2020 1622 JAB2
09/11 /2020 1052 66330
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
2.4
0,57
mglkg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 30508
6010D
1 09/15/2020 0101 KSH2
O911112020 1437 66291
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
160000
200
75
mglkg
1
Arsenic
7440-38-2 6010D
7.3 J
7.5
2.5
mglkg
1
Cadmium
7440-43-9 6010D
ND
2.5
0.63
mg/kg
1
Calcium
7440-70-2 6010D
1800 J
2500
310
mglkg
1
Chromium
7440-47-3 6010D
48
5.0
1.3
mglkg
1
Copper
7440-50-8 6010D
62
5.0
2.3
mglkg
1
Iron
7439-89-6 6010D
45000
50
23
mglkg
1
Lead
7439-92-1 6010D
24
5.0
2.3
mglkg
1
Magnesium
7439-95-4 6010D
1800 J
2500
310
mglkg
1
Manganese
7439-96-5 6010D
1100
7.5
3.0
mglkg
1
Molybdenum
7439-98-7 6010D
ND
20
5.0
mglkg
1
Nickel
7440-02-0 6010D
24
20
5.3
mglkg
1
LOCI = Limit of Ouanlilation
D = Detected in the method blank
E = Quanlitation of compound exceeded the calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery Is out of criteria
P = The RPD between two GC columns exceeds
40 %
J = Estimated result <
LOQ and > DL
H - Out of holding lima
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 13

Client:Synagro Laboratory ID: VI10001-001
Description: Winston WTP 1 Matrix: Solid
Date Sampled:0910512020 1230 % Solids: 3.27 09/11/2020 0211
Date Received:09/1012020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 09/15/2020 0101 KSH2
O911112020 1437 66291
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
units
Run
Potassium
7440-09-7 6010D
1900 J
2500
310
mglkg
1
Selenium
7782-49-2 6010D
4.7 J
10
4.1
mglkg
1
Sodium
7440-23-5 6010D
NO
2500
310
mglkg
1
Zinc
7440-66.6 6010D
250
25
6.3
mglkg
1
LOQ = Limit of Quantitation B W Detected in the method blank E = Quanlitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Fstimated result � LOQ and ? DL
H - Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 13

Client:Synagro Laboratory ID:VI10001-002
Description: Winston WTP 2 Matrix: Solid
Date Sampled:09/0912020 1230 % Solids: 4.02 09/11/2020 0211
Date Received: 0911012020
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 254OG
1
09/11/2020 0211 SRB
66315
1 350.1
(Ammonia - N ) 350.1
1
09/15/2020 1538 KMC
66593
1
(Nitrate - N ) 9056A
1
09/16/2020 1523 AMR
66889
1
(Nitrite - N ) 9056A
1
09/16/2020 1123 AMR
66890
1
(Phosphorus) 365.1
2
09/15/2020 1525 DMA
09/14/2020 1326 66566
1
(Soil pH mews) 9045D
1
09/14/2020 1252 AAB
66608
1 351.4
(TKN) 351.2
1
09/16/2020 1817 DMA
09/16/2020 1136 66562
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.02
%
1
Ammonia - N (gas diffusion)
350.1
750
25
13
mglkg
1
Nitrate - N (soluble)
9056A
16
12
2.5
mglkg
1
Nitrite - N (soluble)
9056A
3.0 J
5.0
2.5
mglkg
1
Phosphorus
7723-14.0 365.1
2400
250
s0
mglkg
1
Soil pH measured in water @ 20.5 ° C
9045D
6.6
su
1
TKN
351.2
12000
620
620
mglkg
1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 09/11/20201625 JAB2 09111120201052 66330
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471 B
NO
1.9
0.46
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 09/15/2020 0107 KSH2
O9111/2020 1437 66291
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90.5 6010D
110000
170
62
mglkg
1
Arsenic
7440-38-2 6010D
4.8 J
6.2
2.1
mglkg
1
Cadmium
7440-43-9 6010D
NO
2.1
0.52
mglkg
1
Calcium
7440-70-2 6010D
2200
2100
260
mglkg
1
Chromium
7440-47-3 6010D
32
4.1
1.0
mglkg
1
Copper
7440-50-8 60100
47
4.1
1.9
mg/kg
1
Iron
7439-89-6 6010D
30000
41
19
mg/kg
1
Lead
7439-92-1 6010D
15
4.1
1.9
mglkg
1
Magnesium
7439-95-4 6010D
1500 J
2100
260
mg/kg
1
Manganese
7439-96.5 6010D
1100
6.2
2.4
mglkg
1
Molybdenum
7439-98-7 6010D
NO
17
4A
mglkg
1
Nickel
7440.02-0 6010D
17
17
4.3
mglkg
1
LOQ = Limit of Quantitatlon
B = Detected in the method blank
E = Quanlilation of compound exceeded the
calibration range
❑L = Detection Limit
ND - Not detected at or above the DL
N = Recovery is out of criteria
P = The RPO between two GC columns exceeds 4011.
J = Estimated result
LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analyt€cal Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] t1 www.pacelabs.com
Page 5 of 13

Client:Synagro Laboratory ID:V110001.002
Description: Winston WTP 2 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 4.02 09111/2020 0211
Date Received: 0911012020
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/15/2020 0107 KSH2 O911112020 1437 66291
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7
6010D
1500 J
2100
260
mglkg
1
Selenium
7782-49-2
6010D
4.4 J
8.3
3.4
mglkg
1
Sodium
7440-23-5
6010D
ND
2100
260
mglkg
1
Zinc
7440-66-6
6010D
270
21
5.2
mglkg
1
LOQ = Limit of Quantitatlon B = Detected in the method blank E = Quantilalion of compound exceeded the calibration range ❑L = Detection Limit
NO = Not detected at or above the DL N = Recovery Is out of criteria P - The RPD between two 00 columns exceeds 40 % J = Estimated result < LOQ and � DL
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 13

Client: Synagro Laboratory ID: Vt10001-003
Description: Winston WTP 3 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 3.61 09/11/2020 0211
Date Received: 0911012020
Inorganic
non-metals
_
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
09111 /2020 0211 SR$
66315
1 350.1
(Ammonia - N ) 350.1
2
09/15/2020 1550 KMC
66593
1
(Nitrate - N ) 9056A
1
09/16/2020 1542 AMR
66889
1
(Nitrite - N ) 9056A
1
09/16/2020 1542 AMR
66890
1
(Phosphorus) 365.1
5
09/15/2020 1528 DMA
09/14/2020 1326 66566
1
(Soil pH meas) 9045D
1
09/14/2020 1253 AAB
66608
1 351.4
(TKN) 351.2
1
09/16/2020 1825 DMA
09/16/2020 1136 66562
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.61
%
1
Ammonia - N (gas diffusion)
350.1
1400
55
29
mglkg
1
Nitrate - N (soluble)
9056A
21
14
2.8
mglkg
1
Nitrite - N (soluble)
9056A
3.3 J
5.5
2.8
mglkg
1
Phosphorus
7723-14-0 365.1
3100
690
140
mglkg
1
Solt pH measured in water @ 20.6 ° C
9045❑
6.7
su
1
TKN
351.2
19000
690
690
mglkg
1
Run Prep Method
Analytical Method
dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 09/11/2020 1627 JAB2
09/11 /2020 1052 66330
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
NO
4.6
1.1
mglkg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 09/15/2020 0112 KSH2
09/11/2020 1437 66291
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90.5 6010D
140000
180
67
mglkg
1
Arsenic
7440-38-2 6010D
6.0 J
6.7
2.2
mglkg
1
Cadmium
7440-43-9 6010D
ND
2.2
0.56
mglkg
1
Calcium
7440-70-2 6010D
2100 J
2200
280
mglkg
1
Chromium
7440-47-3 6010D
40
4.4
1.1
mglkg
1
Copper
7440-50-8 6010D
65
4.4
2.0
mg/kg
1
Iron
7439.89-6 6010D
37000
44
20
mg/kg
1
Lead
7439.92-1 6010D
21
4.4
2.0
mg/kg
1
Magnesium
7439.95.4 6010D
1900 J
2200
280
mg/kg
1
Manganese
7439-96-5 6010D
1300
6.7
2.6
mglkg
1
Molybdenum
7439-98-7 6010D
NO
18
4.4
mglkg
1
Nickel
7440.02.0 6010D
22
18
4.7
mglkg
1
LOQ = Limit of Quantitalion
B = Detected in the method blank
E = Quantitalion of compound exceeded the
calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GG columns exceeds 40%
J = Estimated result <
LOQ and n DL
H = Out of holding time
W - Reported an wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 13

Client:Synagro Laboratory ID: VI10001-003
Description: Winston WTP 3 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 3.61 09/11/2020 0211
Date Received: 09/1012020
!CP-AES
Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 30508 6010D 1 09/15120200112 KSH2 09111/20201437 66291
CAS
Analytical
Parameter
Number
Method
Result Q
LOO
DL
Units
Run
Potassium
7440-09-7
6010D
2000 J
2200
280
mglkg
1
Selenium
7782-49-2
6010D
4.1 J
8.9
3.6
mglkg
1
Sodium
7440-23-5
6010D
ND
2200
280
mglkg
1
Zinc
7440.66.6
6010D
300
22
5.6
mglkg
1
LOQ - Limit of Quantitatlon B = Detected in the method blank E = Quanlilation of compound exceeded the calibration range ❑L = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 k J = Estimated resutt < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 13

Client:Synagro Laboratory ID: V110001-004
Description: Winston WTP 4 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 4.45 09/11/2020 0211
Date Received: 0911012020
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
09/11/2020 0211 SRB
66315
1 350.1
(Ammonia - N ) 350.1
2
09/15/2020 1552 KMC
66593
1
(Nitrate - N ) 9056A
1
09/16/2020 1601 AMR
66889
1
(Nitrite - N ) 9056A
1
09/16/2020 1601 AMR
66890
1
(Phosphorus) 365.1
5
09/15/2020 1528 DMA
09/14/2020 1326 66566
1
(Sail pH mess) 9045D
1
09/14/2020 1255 AAB
66608
1 351.4
(TKN) 351,2
1
09/16/2020 1825 DMA
09/16/2020 1136 66562
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4,45
%
1
Ammonia - N (gas diffusion)
350.1
1100
45
23
mg/kg
1
Nitrate - N (soluble)
9056A
17
11
2.2
mg/kg
1
Nitrite - N (soluble)
9056A
2.7 J
4.5
2.2
mglkg
1
Phosphorus
7723.14-0 365.1
2700
560
110
mglkg
1
Solt pH measured in water @ 20.8 ° C
9045D
6.7
su
1
TKN
351.2
20000
560
560
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Hatch
1 7471B
7471B
1 09/11/20201634 JAB2
09/11/20201052 66330
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471E
NO
3.4
0.81
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 09/15/20200129 KSH2
09/11/20201437 66291
CAS Analytical
Parameter
Number Method
Result Q
LOQ
OIL
Units
Run
Aluminum
7429-90-5 6010D
100000
150
56
mglkg
1
Arsenic
7440-38-2 6010D
3.5 J
5.6
1.9
mglkg
1
Cadmium
7440-43-9 6010D
NO
1.9
0,47
mg/kg
1
Calcium
7440-70.2 6010D
1400 J
1900
230
mg/kg
1
Chromium
7440-47-3 6010D
28
3.7
0.93
mglkg
1
Copper
7440-50-8 60100
45
3.7
1.7
mglkg
1
Iron
7439-89-6 601013
26000
37
17
mglkg
1
Lead
7439-92-1 601013
14
3.7
1.7
mglkg
1
Magnesium
7439-95-4 6010D
1300 J
1900
230
mglkg
1
Manganese
7439-96-5 6010D
1000
5.6
2.2
mglkg
1
Molybdenum
7439-98-7 6010D
NO
15
17
mg/kg
1
Nickel
7440-02-0 6010D
16
15
3.9
mglkg
1
LOG = Limit of Quantitalion
B = Detected in the method blank
E = Quantitatlon of compound exceeded the calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery Is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOG and > DL
It = Out of holding time
W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacclabs.com
Page 9 of 13

Client:Synagro Laboratory ID:VI10001-004
Description: Winston WTP 4 Matrix: Solid
Date Sampled:0910912020 1230 % Solids: 4.45 09/11/2020 0211
Date Received:09110 /2020
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/15/2020 0429 KSH2 O9/11/2020 1437 66291
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DI.
Units
Run
Potassium
7440-09-7
60100
1400 J
1900
230
mglkg
1
Selenium
7782-49-2
6010D
NO
7A
3.0
mg/kg
1
Sodium
7440-23-5
601OD
NO
1900
230
mg/kg
1
Zinc
7440-66-6
6010D
180
19
4.6
mg/kg
1
LOQ = Limit of Quantization B = Detected In the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD behveen two GC columns exceeds 40% J = Estimated result � LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 13

PACE ANALYTICAL SERVICESL-L.-LC..
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.gacelabs.com
Page 12 of 13

PACE ANALYTICAL SEG'=,)VKQEG, LLC
Sbta:) r--vm� 4 n31SmAws lk-
I%--w** Ywnkis L'U40ISC- 14
Sample Receipt Checklist (SRQ
Np I of I
V11-1— MO. Kr7-711111
Clitenn; SY-NAGRO CaOlcrIns ec:etl:ry,+F.fudc:tsll +69+'Ilii2(PO Leto; V1I0041
--
Mears of rWipl: [7 S.F.Sl C_lieatt V] UPS [ Fct11 s Oth:r -
Q Yes
❑ :401
i. %Vefe w kid s;ttli pmracnt on the cooler? - -
YQ1
n Nal 0 NA
12.1fctrst2dy 3ca13 ►were preawt, %Vffn fi% Intact cilJ unbrokn'
_
�H gilt it): NA _ Chlorine Str;p It) NA 'I-osted by: _
Orie,,,inal I: rgrcrrlu rFporF rwips .' Ueri%ed (Com'tted) tcntpersturr upon rxczip' 11AM[d Soup -Cup ID: 20-14111
1.7 11.? `c NA 1NA T NA i NA IC CIA r N.A oG
Method: ❑Te,:t?eratuty Bhmk OAgaiust Bottle; IR Gun In; 5 IR Gun Carm-.flon [+actor: 0 _ T
_Method of coolant- 0 Wet lee d Ice P:r ks ❑ i) Ix ❑ None
❑ Yes
❑ No
O NA
T If tanFet - wa of any cooler :xcccdecl 6.OPC, %vas F; ajc;.t Manager 1`oti r1w?
t'M 06-AS Kotilte:tl IIy; phone I emai! ; face-to-fscc (circle one).
0 Yes! 0 No
d NA
C In the ctwimq:raial coariar : N.n king Slip a3acltcd to thry I'nm' - -
Ycf
❑ ha
5. Wem proper eux-ody prucr;ttlre.s (rti:ccla:sltied'recer��.i f fullu+vcd't -
6. Were sarnp;t IDs li-,red on dte COC?
7. Wei sampla"limW on ail satnpk: conzalners?
® Yes
two
0 Yes
❑ 7NO
0 Ye3
0 No
ONO
& Was collecl-on datr. R time lit.rd un the COC?
❑ Yrs
9, t'4M cullect:nn em`•= & time fisted an all sample contarnurs?
0 Ym
© t1r),
IC. Did all inWtrlretion (li7, date, time) Qoree wit[, the COC?
0 i't
❑ NU
111.
Wcrc tens to to wfrlm ed listed oa the COC?
0 Ya
71'M
11. VA all swnp[cs a. -tire in the proper cnn:j:rcr3 far each to , and+o. in gcod calltlhinn
Carklitoken, lids_ w, cu,}1 _ _
wag adejimatc sample volumt: uvxilah;c 7
ti'C3
❑ r4c
113.
Yes
❑ No
14. Ul= 01 tramplea received within V, tfic holdin- time„ 4S hours, whidltYvr comes first?
No
15- Were rnv sumpla cur[ainem1ltiasln�letce�s(Cre[t cltic).tr.tp[as Hot lisrc�r[ on COC"?
U-yy
0 No
21 NAA
16.for VGA and RSK-175 mpanles, were bj: blcs present(% -or 6ttrrn ir. diarncl^r)
to any of the VITA vitls7
❑ Yes;
N-a
VJ NA
17. Were all DROhj;idnkOnuWcnt sarn lei rcocivcd at a ptl of <??
1$. Wcrw all Cyanide samples roman vt:d to a pti ? :2 and sulfide sarn ]eS mucived a -,a p] I ? 99
Wefe �dI .applhu • hIF1,!'f KNicya�rdr,'�rtcno l 5 (� 0.5m /L) sanples freo nFr st ua[
❑ Ye-31
❑ N01
NA
❑ Vey
❑ No
ONE
❑ 0 NOl ®NA129. t4E-e riFent remarkitr=umts (ix, requ�t�l dilutions,145?VISD (h�ignations, ett:.,,)
correctly transcaii W from do C'OCOCrote the ccmtmca*, section in I,iMS'>
© YesYe; mi 21- Was the quoit mjmKr listed oqt iha uwitairier lzbel? If fis- ote R TEA
;ample Prese-rimbon (Must be comp'ete d fur arty sample's) incorr"tly pr so-vtd or v ith IicaclsFxtce. )
4;mroe(s) NA -- ,.vvrc racb-cd iucnr wAy prgseried uad iNurc ar jusred accordingly
n sample recti4ing,,Yitsf NA _rtL of ciml; om: 1-12SO4; HNOi, I-10, Na011 wing SR ;9 NA
Ime of pte.s`erratitm NA � If Oorc grin one lf, rvalrwa fs naeded, abase note N the cummcnts. below-
nple(s) NA wam rece:Vud wit'r bubblts ?6 mm in diameler,
np.e3is? NA _ %Yem rcce:'vec %%silt TRC > {15 vineO(If# 19 is ran) ulrtl v crw
.meted accordingly in sample tcaivmg tr;th sofrim. ;biosttl ele (Nla3Sr()3) with Shealy ID: NA
bucWt lu;.eis appti:d by_ 1SH Date: H!l0rX20
C'rxmrr:rr�
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of t3

SUMMIEF
E19MOMdEMTAL TEeHNALOC,IG5, WC
Analytical Lahoralorles
December 18, 2020
Alex Fax
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Winston WTP
Dear Alex Fox:
Summit Environmental Technologies, hte.
3310 Witt St.
Cnyahoga Falls, Ohio 44223
TEL: [phone] Fi11: [phone]
Website: help.11immseliek.c4gan
Order No.: 20120299
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/4/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St,
Cuyahoga Falls, Ohio 44223
Arkansas Sa-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1790279, Nevada OH009232020-I, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 34

SUMMIT SumrriitEnvironmental Tech»ologies,If,c' Case Narrative
3310 Wire St.
ENVI"OHMENTAL TECiW01 G11;S, MC Cnyaltoga Falls, Ohio 44223 WO#: 20120299
Arm(ytical Laboralol *4 TEL: [phone] FAX: [phone]
]i'ebsite: httn://w,mv.settek.conn Date: 12/18/2020
CLIENT: Synag-o
Project: Winston WTP
WorkOrder Narrative:
20120299: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Forth, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report, Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Notes:
40PPM SVOC-MSTR_S(8270): 8270 CCV exhibits high recovery for Pyridine. Associated samples are
N.D. for this analyte.
LCS-46757 SVOC-BNA TCLP(8270): Possible high bias for Pyridine due to high recovery in CCV.
Original
Page 2 of 34

111 SrrnanitEnWronmeutalTechrrologies,L; Qualifiers and Acronyms
SUMM3310 Whi ti
ENVIrt4HtdEI4TAL TECt NOLCVGIFS. INC Cuyahoga Fails, Ohio 442� WO#: 20120299
analytical Laboratories TEL: [phone] FAY.- (330) 253-44t
ltrebsile: hun.-Avinv.sellek eo Date: 12/18/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
d The repotted value is greater than the Method Detection Limit but less than the Repotting Limit,
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
ur Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
RIQDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high {+),
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-l+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-l+ The 1CV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional infonnation
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
Wr
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 34

�' � Sununu Errvirrotnuerrlal Technologies, Inc. yy or'korder
SU3310 Wirr Sf.
r=NV1Pl0N1,1CNYAL r[CnNOLOGIF$, INC, Cuyahoga Falls, Ohio 44223 Sample Summary
Analy0cai Laborafories TEL: [phone] FiIX.• [phone] WO#: 20120299
Website: hLW.//unrwsettelc.corn 18Dec-20
CLIENT: Synagro
Project: Winston WTP
Lab ,SampleID Client Sample ID Tag No Date Collected Date Received ihlatrix
20120299-001 Winston WTP 12/2/2020 1 1:15:00 AM 12/44/2020 10:55:00 AM Sludge
Page 4 of 34

Srmaalt Stmlrrrrurreretal Tec,rrealagier, Inc.ffj DATES REPORT
u �I�
3310 Mhr Sr.
1 T
ENVIAMAIENTAL
1rCHNOLgcIES.
INC. Crrralroga balls, Ohio 44223
Analytical
Labera(afle5
TEL. [phone] FAX: [phone] WOti: 20120299
Wahsite: h0a:/hvivxsse7rek.cnirr 18-Dec 20
Client:
Synagro
Project:
Winston WTP
Sample ID
Client Sample ID
Cnlleetion Date Matrix Test Name Lcaclmtc Dntc Prep Date Analysis Date
20120299-001 A
Winston NVfP
1212/2020 1 L 15:00 AM Sludge Fgnitability oFSDlids (S%V-846: 10-10) 12JI012020 530i 16 PM
pH (SW9045D) 12/712020 12:13:39 PM
Reactive Cyanide (901417.3.3 2)-Solid 12113/2020 12:46r00 PM
Reactive Sulfide (9034)17.3.4.2 12113/2020 12:46:00 PM
TCLP Herbicides by EPA 8321➢ 12116/2020 6A7:00 PM
TCLP Mercury Analysis (SW13111747121912020 10c26t06 AM 12/10/2020 9:40:00 AM 12110/2020 3:05:00 PM
TCLP Metals Analysis (SWI31 V60107219/2020 10:26:06 AM IV912020 10:45:00 AM 1219/2020 U3:41 PM
TCLP Pesticides Analysis (SW1311180219/2020 10:26:06 AM 12/9/2020 12:25:00 PM 12/12/2020 1:03:00 AM
TCLP Pesticides Analysis (SW 13l 118(1219)2020 10`.26:05 AM 12/912020 12:25:00 PM 12/12)2020 1:03:00 AM
TCLP Semi-Volatiles Analysis 12/91202010:26:06AM 1219/2020 12:25:00 PM 12/9/2020 10:30:00 PM
(SW l31 118270)
TCLP Volatiles Analysis 12/9/2070 6:08:00 PM
Original
Page 5 of 34

IT Summil Fnvironnienial Technologies, Inc. Analytical Report
SUMM3310 Mn St.
ENVIItONPAENTAL fEl: MOLomFS, we Cuyahoga Falls, 01no 44223 (base report)
Analytical Laborsrorias TEL: [phone] F,9X.• [phone] WOO: 20120299
Websile: h1tp:11unvw.se11ek.eo7n Date Reported: I2/18/2020
CLIENT:
Synagro
Matrix:
SLUDGE
Lab TD:
20120299-OOIA
Project:
Winston WTP
Client Sample.ID Winston WTP
Tag Number:
Collection Date: 12/2/2020 11: I5:00 AM
Analyses Result RL Qual Units DE Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00200
mg1L
1
12110/2020 3:05:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
NID
0.500
mglL
1
1219/2020 6:23:41 PM
TCLP Barium(Ba)
ND
5.00
mg/1-
1
12/9/2020 6:23:41 PM
TCLP Cadmium(Cd)
ND
0.100
mglL
1
12/9/2020 6:23:41 PM
TCLP Chromium(Cr)
ND
0.200
mg1L
1
12/9/2020 6:23:41 PM
TCLP Lead(Pb)
ND
0,500
mg1L
1
1219/2020 6:23:41 PM
TCLP Selenium(Se)
ND
0,0500
mgiL
1
1219/2020 6:23:41 PM
TCLP Silver(Ag)
N❑
0,500
mg1L
1
1219/2020 6:23:41 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.200
mglL
2
12/9/2020 10:30:00 PM
2,4,5-Trichlorophenal
ND
0.500
mglL
2
12/9/2020 10:30:00 PM
2,4,6-Trichlorophenol
ND
0.500
mglL
2
12/9/2020 10:30:00 PM
2,4-Dinitrotoluene
ND
0.100
mglL
2
12/9/2020 10:30:00 PM
Cresols, Total
ND
10.0
mglL
2
12/9/2020 10:30.00 PM
Hexachloro-1,3-butadiene
ND
0.0400
mglL
2
12/9/2020 10:30:00 PM
Hexachlorobenzene
ND
0.100
mglL
2
12/9/2020 10:30:00 PM
Hexachloroethane
ND
0.200
mglL
2
12/9/2020 10:30:00 PM
Nitrobenzene
ND
0.200
mg1L
2
12/9/2020 10:30:00 PM
Penlachlorophenol
ND
0,500
mglL
2
12/9/2020 10:30:00 PM
Pyridine
N❑
0,500
QC+ mg1L
2
12/9/2020 10:30:00 PM
Surr: 2-Fluorophenol
41.2
10 - 157
%Rec
2
12/9/2020 10:30:00 PM
Surr: Phenol-d6
46.8
10 - 169
%Rec
2
12/9/2020 10:30A0 PM
Surr: Nitrobenzene-d5
46.2
32.1 - 130
%Rec
2
12/9/2020 10:30:00 PM
Surr. 2,4,6-Tribromophenol
58.6
45.4 - 166
%Rec
2
12/9/2020 10:30:00 PM
Surr. 2-Fluorobiphenyl
57.6
35.7 - 130
%Rec
2
12/9/2020 10:30:00 PM
Surr: p-Terphenyl-d14
116
74.7 - 145
%Rec
2
12/9/2020 10:30:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
11 Iiolding times for preparation or analysis exceeded
M Manual Integration
used to detera inc area responsc
MC Value is below Minimum Compound Limit,
N Tentatively identified
compounds
ND Not Detected
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal
< MDL
Page 6 of 34

summill
Summit Fmvironmenial Technologies, Lee.
3310 fYM St.
Analytical Report
ENVln0NMCNTAL n-MM I00KES, INC
Cttvahoga Falls, Orin 44223
(base report)
AnHlyfloaf Laboratonot
7EL: [phone] FAX. [phone]
WON: 20120299
Websile: htfP.'1Avww.settek.ro) y
Date Reported: 12/18/2020
CLIENT: Synag-o
Tag Number:
Matrix: SLUDGE
Collection Date:
12/2/2020 11:15:00 AM
Lab ID: 20120299-OOIA
Project: Winston WTP
Client Sample ID Winston WTP
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
0.0250
mg/L
1 12/12/2020 1:03:00 AM
Toxaphene
ND
0.0500
mg/L
1 12/12/2020 1:03:00 AM
Endrin
ND
0.00250
mg/L
1 12/12/2020 1:03:00 AM
gamma-BHC
ND
0.00250
mg/L
1 12/12/2020 1:03:00 AM
Heptachlor
NO
0.00250
mg/L
1 12/12/2020 1:03:00 AM
Heptachlor epoxide
ND
0.00250
mg1L
1 12/12/2020 1:03:00 AM
Methoxychlor
ND
0.00250
mg1L
1 12/12/2020 1:03:00 AM
Surr: TCMX
73.1
10 - 119
%Rec
1 12/12/2020 1:03:00 AM
Surr: DCB
71.3
10 - 119
%Rec
1 12/12/2020 1:03:00 AM
TCLP HERBICIDES BY EPA 8321 B
SW8321A
Analyst: TM
2,4-D
N❑
0.500
mg/L
50 12/16/2020 6:47:00 PM
2,4,5-TP
ND
0.500
mg/L
50 12116l2020 6:47:00 PM
Surr: 2,4-Dichlorophenylacetic aci
83.2
70 - 130
%Rec
50 12/16/2020 6:47:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50 12/9/2020 6:08:00 PM
1,2-Dichloroethane
ND
0.250
mg1L
50 12/9/2020 6:08:00 PM
MEK
ND
5.00
mg1L
50 12/9/2020 6:08:00 PM
Benzene
ND
0.250
mg1L
50 12/9/2020 6:08:00 PM
Carbon tetrachloride
ND
0.250
mg1L
50 12/9/2020 6:08:00 PM
Chlorobenzene
ND
2.50
mg1L
50 12/9/2020 6:08:00 PM
Chloroform
ND
0.250
mg1L
50 1219/2020 6:08:00 PM
Tetrachloroethene
ND
0.250
mg1L
50 1219/2020 6:08:00 PM
Trichloroethene
ND
0.250
mg1L
50 1219/2020 6:08:00 PM
Vinyl chloride
ND
0.100
mg1L
50 12/9/2020 6:08:00 PM
Surr. 4-Bromofluorobenzene
90.5
70 - 130
%Rec
50 12/9/2020 6:08:00 PM
Surr: Dibromofluoromethane
98.8
70 - 130
%Rec
50 12/9/2020 6:08:00 PM
Surr. Toluene-d8
98.9
70 - 130
%Rec
50 12/9/2020 6:08:00 PM
Qualifiers: E Analyte detected in the associated
Method Blank
E Value above quantitation range
If Holding times for preparation or analysis exceeded
M Manual Integra(ion used to determine area response
MC Value is below Minimum Compound
Limit.
N Tentatively identified compounds
L4D Not Detected
P Second column confirmation
exceeds
PL Permit Limit
R RPD outside accep(ed recovery limits Original
RL Reporting Detection Limit
LI Samples with CaICVal < MDL
Page 7 of 34

SUMM111
Sunindl Environmental Technologies, Inc.
3310 Wn St.
AnalyticM Report
EKAIIItOWAENTAL T[C1ffdG]LCIC;tFS, (NC
Cuyahoga Falls, Ohio 44223
(base report)
Analytical taborafones
TEL: [phone] FAX.- [phone]
WO#: 20120299
lPehsite; lute://w�nwseltek.com
Date Reported: 12/18/2020
Synagro
Tag Number:
CLIENT:
Mah•ix:
SLUDGE
Collection Date:
12/2/2020 11:15:00 AM
Lab ID:
20120299-OOIA
Project:
Winston WTP
Client Sample ID Winston WTP
Analyses
Result RL Qual Units
DF Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND
0.490 mg/Kg 1
12113/2020 12:46:00 PM
ICNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: CXS
Ignitability nonflammable
mmisec 1
12110/2020 5:30:16 PM
RCI
SW9045D
Analyst: VVK
PH (SW9045D)
pN 7.2
sm,@20,OC 1
1217/2020 12:13:39 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)12.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
12113/2020 12:46:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Linut
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 8 of 34

Summit Environraeutal Technologies, lne.
Accreditation Program
SUMMIT
3310 1Vin St.
Anal teS Report
P
ENVIRt7NWINTAL TECHNOLnfli53, MC,
Cuyahoga Falls, Ohio 44223
Aralyflcal Laboraloroes
TEL: [phone] FAX: [phone]
WO#: 20120299
JYebsite: httt�://svtivn.sellek.con�
18-Dee20
Client:
Synagro
State: NW
Project:
Winston WTP
Program Name: NC WW_SCM
Sample ID 'Matrix
Test Name
Analyte
Status
20120299-OOIA Sludge
ignilability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
N
Sludge
Reactive Sulfide (9034)17.3.4.2
Sulfide, Reactive
N
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW131116010)
Lead
A
Sludge
TCLP Metals Analysis (SW131 1/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW131118081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BliC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311l8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
IA-Diclilorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
2,4,5-Triclilorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW 1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethanc
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original #1
Page 9 of 34

summimir SuninfilEnviroprnaeutalTechnologies, Inc. AccreditationProgram
33101Yin St. Ana teS Report
ENVIRONMENTAL TECHMOLOGIC-5, INC Cuyahoga Frills, Ohio 44223 Y p
AnMyrlcal Laboratorleg TEL: [phone] FAX.- [phone] Woft: 20120299
lYebsile: hitnalivivmsettekeoin I8-Dec-2.0
Client: Synagro
Project: Winston WTP
State: NW
Program Name: NC WW SCM
Sample 1D mfltrix
Test Name
Analyte
Status
20120299-001A Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetiachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethcnc
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
- Key -- Key - — —
NC WW SCM A Accredited NC M1W SCM N Not Accredited
Original #1
Page 10 of 34

S uMM'EF sr, nn€rF.,n.,,br,taen1a17echt33101s, k'c. QC SUMMARY REPORT
33I0 Q ilr St.
ENVIIIONIAENTAL TMINOLOGI€5, INC CuyahognFnBr, 01iio44223
Anelyfleel LabclralcirleE ITL: [phone] rAr. (33o) 253-4489 NV04: 20120299
IVebsfle: h1rn:/hvnIvseuek-rnne 18-Dec-20
Client: Synagro
Project: Winston WTP 13atchlD: 46751
Sample ID: MB46751
SampType: NIBLK
TestCade: TCLP-VOC•M Units: mglL
Prep Date:
RunNo: 121165
Client ID: PBS
Batch ID: 46751
TestNo: SW8260 SW1311M
Analysis Date: 121912020
SegNo: 3110032
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLlmil RPD Ref Val
%RPD RPDL€mit Qual
1,1-Dichloraethene
ND
0.250
1,2-Dlchlorcethane
ND
0.250
MEK
NO
5.00
Benzene
ND
0.250
Carbon tetrachloride
ND
0.250
Chlorohonzene
ND
2.50
Chloroform
ND
0.250
Telrachloreethene
N❑
0.250
Trichlaroethene
ND
0.260
Vinyl chloride
ND
0.100
Surr:4-Bromolluorobenzene
2250
Surr: Dibromofluoromethane
2510
Surr: Toluene-d8
2460
250o 89.8 70 130
2500 100 70 130
2500 98.5 70 130
Sample ID: LCS-46751
SampType: LCS
TeslCode: TCLP-VOC•M Units: mglL
Prep Date:
RunNo: 121165
Client ID: LCSS
Balch ID: 46751
TestNo: SW8260 SW13i1M
Analysis Date: 121912020
SegNo: 3110033
Analyte
Result
PQL SPK value SPK Re! Val
%REC Lowl-imit HighLlmil RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene 0.906 0.250
1,2-Dichlamelhaae 0.927 0.250
MEK ND 5.00
Benzene 0.925 0.250
Quallf€ersp 13 Analyte detected in the associated Method Blank
J Analyte detected below quantilation IimiLa
ND Not Detected
R RPD outside accepted recovery limits
1.00 0
90.7
64.7
136
1.00 0
92.7
70
130
5.00 0
79.4
55.1
149
1.00 0
92.5
70
130
E Value above quantitation moge
11 14oldingtimesforprepamtionoranal5
M Manual integration used to determine area
response
MC Vahre its below Minimum Compound
Original
P Second column confirmation exceed,
PL Permit Limit
RE, Reporting Deteclion Limit
S $pike Recovery onlside accepted reco
Page 11 of 34

Summiot
331010 Ts"^+arirErrrirar+a+enrnl7echut'ire S1. s.lrrc. QC SUMMARY REPORT
ENvinowaENTAL1iCIINOt0t;WS,1NC CaynhogaFalls,01uoaa223
WON: 24120299
Armlytical taborararles TEL. [phone] Filth [phone]
I1'eAsire: 1,trn:/hv�mrsenek emn 18-Dec-20
Client: Synagro
Project: Winston WTP HatchID: 46751
;ample ID: LCS-46761
SampType: LCS
TestCade: TCLP-VOC•M Units: mg1L
Prep Date:
RunNo: 121165
3lienl ID: I.CSS
Batch ID: 46751
TeslNo: SW8260 SWI311M
Analysis Date: 121912026
SegNo: 3110033
Walyte
Result
PQL SPK value SPK Ref Vat
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.951
0.250
1.00
0
95.1
70
130
Chlarobenzene
ND
2.50
1.00
0
90.4
70
130
Chloroform
0.885
0.250
1.00
0
88.4
70
130
Telrachloroethene
0.877
0.250
1.00
0
87.7
70
134
Trichloroethene
0.918
0.250
1.00
0
91.8
62.8
160
Vinyl chloride
0.856
0.100
1.00
0
85,6
67.1
130
Surr:4-Bromofluorobenzene
2540
2500
102
70
130
Surr: Dibromo8uoromethane
2450
2500
98.0
70
130
Surr: Toluene-d8
2480
2500
ODA
70
130
;ample ID: 20120398-OOIAMS
SampType: MS
TestCode: TCLP•VOC•M Units: mg1L
Prep Date:
RunNo: 121165
aienl to: BetchQC
Batch ID: 46751
Tes1No: SW8260 SW1311M
Analysis Dale: 121912020
SegNo: 3110043
Inalyle
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua!
1,1-Dichloroeth
1,2-Dichloroelh
MEK
Benzene
Carbon tetfachl
Chlarobenzene
Chloroform
Telrachloroeth
Qualifiers;
one
ene
1.04
0.250
ane
1.01
0.250
ND
5.00
1.11
0.260
oride
1.07
0,250
ND
2.50
0.998
0.250
0.999
0.250
B Analyte detected in the associated Method Blank
J Analytc detected below quantRation limits
ND Not Detected
R RPA outside accepted recovery limits
1.00
0
104
13.6
1.00
0
101
55.7
5.00
0
91.8
65.3
1.00
0.0635
104
49.2
1.00
0
107
26.7
1.00
0
102
33.7
1.00
0
99.6
48.5
1.00
a
99.9
19.2
E Value above guantitation range
kl Manual Tntegration used to determine arcs response
P Second column confirmation exceeds
RL Reporting Detection Limit
202
138
118
145
156
159
145
191
H Holding times for preparation or anal3
MC Value it below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 12 of 34

=rrm
S UMM 1 Sruumit E7mirotimeirfrr! Tech-ff, hie. QC SUMMARY REPORT
331030 I!'ivt St,
ENVIOONMENTALYCHWO1.0alE5,114, CrrynhagnFalis.0lriv44223
ArWyll"I Lahoralories TF.L: [phone] FAX, [phone] W6il: 20120299
Wehsiee; iirrn;1Asgotm ,verrek.caru 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46751
iample ID: 20120398-001 AM S
SampType: MS
TestCode: TCLP-VOC-M Units: mg1L
Prep Date:
RunNo: 121165
311ent ID: 13atchOC
Batch ID: 46751
TesiNo: SW8260 SW1311M
Analysis Dale: 121912020
SegNo: 3110043
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimil RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
L04 0.250
1.00
0 104
38.4
16-1
Vinyl chloride
0.980 0.100
1.00
0 98.0
27.3
161
Surr:4-Bromofluorobenzene
2550
2500
102
70
130
Surr: Dibromofluoromethane
2520
2500
101
70
130
Surr: Toluene-dil
2540
2500
101
70
130
'ample ID: 20120398.001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg1L
Prep Date:
RunNo: 121165
;lient ID: 13atchQC
Batch ID: 46751
TestNo: SW8260 SW1311M
Analysis Date: 121912020
SegNc,: 3110051
lnalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLimil RPD Ref Val
%RPD RPDLlmit Qual
1,1-Diclhloroethene
1.06
0.250
1,2-Dichloroethane
1.00
0.250
MEK
ND
5.00
Benzene
1.10
0.250
Carbon tetrachloride
1.07
0.250
Chlorobenzene
ND
2.50
Chloroform
1.00
0.250
Tetrachloroethene
0.982
0.250
Trichloroethene
1.04
0.250
Vinyl chloride
1.09
0.100
Sum 4-Bromofluoroben7ene
2570
Surr: Dibromofluaromethane
2490
Qualifiers: B Analyte detected in the associated
Method Blank
3 Anelyledetected below quantitationlimits
ND Not Detected
R RPD outside accepted recovery limits
1.00
0
106
13.E
1.00
0
100
55.7
5.00
0
93.8
65.-
1.00
0.0635
104
49.2
1.00
0
107
26.7
1.00
0
102
33.7
1.00
0
100
48.E
1.0a
0
98.2
19.2
1.00
0
IN
38A
1.00
0
109
27.3
2500
103
70
2500
99.5
70
E Value above quantitatiou range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Repwiing Datcclian Lintil
202
1.04
1.48 25
138
1.01
0.941 25
130
0
0 25
145
1.11
0.634 25
156
1.07
0.280 25
159
0
0 25
1145
0.996
0.601 25
191
0.999
1.77 25
167
1.04
0.337 25
161
0.980
11,0 25
130
0 25
130
0 25
H Holding times for preparation or aoal3
MC Value is below Minimum Compound
PL Pennit Limit
S Spike Recovery outside accepted reco
Original
Page 13 of 34

ummi� 3310 Srmlmlth'rnlrolrnrerttar7echres QC SUMMARY REPORT
33J0 ll'irr Sr
EN19t1ONIdENTAL TECHNOLOGIES, INC CiDwIr ga Falls, Ohio 44223 fflAnalyflcal Laborstorlee TFL: [phone] PAP: [phone] 1VOH: 20120299
Websire: huu:/Avnwsettekcum 18-Der20
Client: Synagro
Project: Winston WTP
BatehID: 46751
"sample ID: 2012039B-001AMS❑
SampType: MSD
TestCode: TCLP-VOC-M Units: mglL
Prep pate:
RunNa: 121165
SHent ID: BatchQC
Batch ID: 46751
TestNo: SW8260 SWW1M
Analysis Date: 121912020
SegNo: 3110051
4nalyte
Result
PQL SPK value SPK Ref Val
%RPC LowUmit HighLirnit RPD Ref Val
%RPO RPDLImit Oval
Surr: Toluene-dil
2490
Qualifiers: B Annlyte detected in the associated Method Blank
J Analylc detected belmv quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
2500 99.6 70 130
F Value above quaraitatinnrange
M Manual Integration used to determine area response
P Second column confinvation exceeds
IIL Reporting Detection Limit
a
H Holding times for preparation or anal]
MC Value is below Minimum Compound
PL Permit Limil
S Spike Recovery outside accepted reca
25
Original
Page 14 of 34

SUMMIT Srrrurnil Environmental Technologies, Lrc•.
3310Win A
ENVMONMENTAL r�CHNOLDgIES, INC Ctrynhoga Falls, Ohta 44223
A ralytleal Laboratories TEI - [phone] FA,V,- [phone]
We>Lsife: hr1p:/Avua»senek.con+
Client; Synagro
Project: Winston WTP
QC SUMMARY REPORT
WON: 20/20299
l8-Dec-20
BateltlD: 46757
;ample ID: M13 46757
SampType: M13LK
TeslCode: SVOC•BNA T Units: mg1L
Prep Dale: 121912020
RunNo: 121173
lient ID: PBS
Batch ID; 46757
Tes1No: SW8270 SW3510C
Analysis Data: 121912020
SegNo: 3110322
,nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimil RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenal
ND
0.250
2,4,6-Tdchlorophenol
ND
0.250
2,4-Dinitrotoluens
N❑
0.0500
o-Cresol
N❑
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachtorophenot
ND
0.250
Pyridine
N❑
0.250
Surr: 2-Fluarophenal
0.736
Sum PhenoW6
0.864
Suer: Nilrobenzane-d5
0.814
Sum: 2,4,6-Tribromophenol
0.866
Surr: 2-Pluarabiphenyl
0.909
Surr: p-Terphenyi-d14
1.18
1.000
73.6
10
130
1.000
86.4
10
130
1.000
81.4
19
130
1.000
86.6
10
130
1.000
90.9
22
130
1.000
118
34
130
Qualiticrs: B Malyte detected in theassociated Mcthod Blank
E
Value above quamitalion range
H
Holding times forprepanuion or anal)
J Analyte detected below qua6titatio»limits
M
Manual Integration usedtodetetmine arearesponse
MC
Value is below Minimum Compound
ND Not Detected
P
Second column confrnnaiion exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery omside accepted reco
QC+
Original
Page 15 of 34

�� '� Stuvr+rrit F.m•iinnmenfu7 Technologies, htc.
3310 11'i1St. QC SUMMARY REPORT
7
m'ln0NrdeN7nLieCnNOtomr.g,tt;C C'tryahagaFolls,Ohio 44223
Annlpflcaf Laboralarles TEL: (33t1) 253-8211 FiLI': [phone] WON: 20/20299
Websitec hrto:Ilinviv.sellek..com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46757
;ample ID: LCSA6757
SampType: LCS
TestCode: SVOC-BNA_T Units: mg1L
Prep Date: 121912020
RunNo: 121173
:Iient ID: LCSS
Batch ID: 46757
TestNo: SW8270 SW3519C
Analysis Date: 1219120213
SegNo: 3110323
lnalyte
Result
PQL SPK value SPK Rof Val
%RFC LowLlmil HighUmil RPD Rof Val
%RPD RPDLlmil Qual
1,4-Dlchlorobenzene
0.515
0.100
0-8000
0
64.4
36.4
130
2,4,5-Trichlorophenol
0.750
0.250
0.8W0
0
93.8
31.7
132
2,4,6-Trichlorophenol
0.708
0.250
0.80o0
0
88.5
31.1
133
2,4-Dinitrotoluene
0.768
0.0500
0.8000
0
96.0
43.3
130
o-Cresol
0.6112
0.250
0.8000
0
76.5
32.9
130
Cresols, Total
N❑
5.00
1.600
0
77.8
31.7
130
Hexachloro-1,3-butadiene
0.531
0.0200
0,8000
0
66.4
31.4
130
Hexachlorobenzene
0.787
0.0500
0.8000
0
98.4
43.1
130
Hexachloroathane
0.471
0,100
0,8000
0
58.9
36.5
130
Nitrobenzene
0.560
0.100
0.8000
0
70.0
39.5
130
Pentachlorophenol
0.745
0.250
0.8000
0
93.2
34
130
Pyridine
0.466
0.260
0.8000
0
58.2
10
130
Sum 2-Fluoraphenal
0.690
1.000
69.0
17.1
130
Surr: Phenol-d6
0.878
1.000
87.8
10
130
Surr: Nitrobenzene-d5
0.758
1.000
75,8
32.6
130
Surr:2,4,6-Trihromophenol
1.02
1.000
102
4.43
130
Sun:2-Flucrobiphenyl
0.884
1.000
89.4
41.8
130
Surr: p-Terphenyl-dl4
1.17
1.000
117
36.4
130
QuaGfrens: H Analyle detected in the associated Medtad Blank
1 Malylc delectcd below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantization range
M Manual htte�'ation used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holdingtimestbrprepatationoranal7
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reca
mQC+
Original
Page 16 of 34

summlyOwurrif Eimironn+enrul Technologies, lneffl331091hr Sr. QC SUMMARY REPORT
ENVIOONAIENTAL TECHNOLnnirS, INC Qryahoga Falls, Ohio 44223
Analyrlcal Laborawlec TCL: [phone] FAX.- [phone] WOM 20120299
Websiler htinr/Awn, sertck.cwm 18 Deo-20
Client: Synagro
Project: Winston WTP BatchID: 46757
3arple ID: 20120387-001AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mglL
Prep Dale: 121912020
RunNo: 121173
'Ilenl le; BatchQC
Batch ID: 46757
TestNo: SW6270 SW35i0C
Analysis Date: 121912020
SegNo: 3110324
lnalyle
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HlghLimit RPD Ref Val
%RPD RPLIUmit Oval
1,4-Dlchlorobenzene
0.580
0.200
0.8000
0
72.6
33.8
126
2,4,5-Trichloraphenal
0.775
0.500
MUD
0
96.9
283
144
2,4,6-Trichloraphenal
0.716
0,500
0.8000
0
89.4
12.8
153
2,4-Dinitrotoluene
0,703
0.100
0.8000
0
87.9
20.4
155
0-Cresol
0.679
0.500
0.8000
0
84.9
10
148
Cresols, Total
ND
10.0
1.600
0
84.6
10
148
Hexachloro-1,3-butadfene
0.577
0.0400
0.8000
0
72.2
29
130
Hexachlorahenzene
0.765
0.100
0.8000
0
957
33.7
134
Hexachloroethane
0.529
0.200
0.8000
0
66.2
32.8
132
Nilrobenzene
0.700
0.200
0.8000
0
87.5
20
158
Pentachlorophonol
0.685
0.500
0.8000
0
85.7
10
176
Pyridine
ND
0.500
0.8000
0
61.7
10
130
Surr: 2-Fluorophenol
0.721
1.000
72.1
3.39
130
Surr: Phenol-d6
0.881
1.000
88.1
5
130
Surr: Nitfabenzene-d5
0.783
1.000
78.3
14.5
154
Sort: 2,4,6-Trihromophenol
0.946
1.000
94.6
19.5
130
Surr.2-Pluorobiphenyl
0.942
1.000
94.2
34.4
130
Sure: p-Terphenyl-d14
1.07
1.000
107
8.86
156
Qualifiers: B Analyte detected
in the associated Method Blank
E Value above quantitation range
H Holding times for preparation oranill
3 Malyle detected
below quantization limits
M Manual Integration used to determiae
area response
MC Value is below Minimum Compound
ND Not Detected
1' Second eolumn confirmation exceeds
PL permit Limit
R RPD outside accepted recovery limits
R1. Reporting Detection
Limit
S Spike Recovery outside accepted mco
mQC+
Original
Page 17 of 34

SUMMIT
UMIMI Summit Ermirwu+reufnl Techrtolugies, h+c QC SUMMARY REPORT
33I0 N+Nr Sf.
ENVIAONh1ENTAL TECIINOWGIES, INC GryafmgaFa!!s, 01+ia44223 WM: 20120299
AnnlyHraf Laboratories TEL: [phone] Fff..- [phone]
IYeLsite, htm:1A;gv ,seftek.cnnr 18-Dec-20
Client: Synagr0
Project: Winston WTP BatchID: 46757
ample to: 20120397.001APASD
SampType: MSD
TestCade: SVOC-13NA T Units: mg1L
Pfep Date: 121912020
RunNo: 121173
'lienl ID: BatchQC
Batch ID: 46757
TestNo: SW8270 SW3510C
Analysis Date: 121912020
SegNo: 3110325
nalyto
Resuft
PQL SPK value SPK Ref Val
%REC LowLimlt Highl-imit RPD fief Val
%RPD RPDLimit Clual
1,4-Dichlorahenzene
0A08
0.200
0.8000
0
76.0
33.8
126
0.5804
4.64
30
2,4,5 Tdchlarophenol
0,708
0.500
0.8000
0
09.8
28.7
144
0.7748
3.00
30
2,4,6-Tdcblorophenol
0.781
0.500
0.8000
0
97.6
12.8
153
0.7156
8.71
30
2,4-Dinitratoluene
0.738
0.100
0.8000
0
92.3
20.4
155
0.7032
4.88
30 m
o-Cresol
0.697
0.500
0.8000
0
87.1
10
148
0,6702
2.56
30
Cresols, Total
N❑
10.0
1.600
0
88.6
10
148
0
0
30
Hoxachloro-1,3-butadiene
0-655
0.0400
0.8000
0
81.9
29
130
0.5772
12.7
30
Hexachlorobenzene
0.871
0.100
0.8000
0
109
33.7
134
0.7652
12.9
30
Hexachloroelhane
0.556
0.200
0.8000
0
69.6
32.8
132
0.5292
5.01
30
Nitrobenzene
0.790
0.200
0.8000
0
98.8
20
158
0.7000
12.1
30
Pentachlarophenol
0.750
0.500
0.8000
0
93.8
10
176
0.6852
9.03
30
Pyridine
0.555
0.500
0.8000
0
69.4
10
130
0.4936
11.7
30 mQC+
Surr:2-Ftuorophenol
0.706
1.000
79.6
3,39
130
0
Surr: Phenol-d6
0.984
1.000
98.4
10
130
0
Surr: Nitrobenzene-d5
0.896
1,000
89.6
14.5
154
0
Surr: 2,4,6-Tdbromophenol
0.963
1.000
96.3
19.5
130
0
Sun:2-Flunrobiphenyl
1.09
1.000
109
34.4
130
0
Surr. p-Terphenyl-d14
1.24
1.000
124
8.86
156
0
Qualifiers; B Analyte detected in the associated Method Blank E Value above qumrtilation range H Holding times for preparation or anal)
0 Analyte detected below quantitatiou limits M Manual Integration used to detctmine area response MC Value is below Minimum Compound
ND Not Detected P Second column con5mPermit
ration exceeds PL Peit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery ovlside accepted reco
Page 18 of 34

COrdpoui uM i jir strrtl°';r E,n ir.oanremal 3310 Teclaer,tl'in sr. Lin QC SUMMARY REPORT
33fo
nj ENVMONtl ENTAL TECHN01.0niES, INC Gryalioga F.&, 01,io44223 WO#: 20120299
Analytical taboratariee TF..L: [phone] FAX.- (330) 253-448V
O'eAsite: lrtrn://tr�rnr.reuek rnnr 18-Dec20
Client: Synagro
Project: Winston WTP BatchlM 46758
Sample ID: 20120299-001ams
SampType: MS
TestCode: TCLP-SVOC- Units: mg1L
Prep Date: 121912020
RunNo: 121304
Client ID: Winston WTP
Balch ID: 46758
TestNo: SW8081 SW3510C
Analysis Date: 12f1212020
SegNo: 3115479
Analyte
Result
PQL SPK value SPK Ref Val
%R£C Lowl-imit Highl-imil RPD Ref Val
%RPD RPDLimit Qua]
Endriu
0.00970
0.000500
0.0100
0
97.0
10
224 An
gamma-BHC
0.00984
0.000500
0.0100
0
98.4
10
192
Heptachlor
0.0114
01000500
0.0100
0
114
10
107
Heptachlar epoxide
0.0106
0.000500
0.0100
0
1106
10
208
Methoxychlor
0.0124
0.000500
0.0100
0
124
10
251
Surr: TCMX
17.5
20.00
87.6
10
157
Surr: DOB
17.1
20.00
85.7
10
194
Sample ID: 20120299-001amsd
SampType: MSD
TeslCode: TCLP-SVOC- Units: mg1L
Prep Date: 121912020
RunNo: 121304
Client 1D: Winston WTP
Balch ID; 46758
TestNo: SW8061 SW3510C
Analysis Dale: 1211212020
SegNo: 3115480
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimil RPD Ref Val
% RPD RPDLimit Qua[
Endrin
0.00872
0.000500
0.0100 0
87.2
10
224
0.00970 10.6
30 m
gamma-BHC
0.00823
0.000500
0.0100 0
82.3
10
192
0.00984 17.8
30
Heptachlor
0.00957
0.000500
0.0100 0
95.7
10
197
0.0114 17.7
30
Heptachlorepoxide
0.00900
0.000500
0.0100 0
90.0
10
208
0.0106 16.2
30
Melhoxychlor
0.0104
0.000500
0.0100 0
104
10
251
0.0124 17.0
30
Surr: TCMX
14.7
20,00
73.5
10
157
0
Surr: DOB
15.0
20.00
75.0
10
194
0
Qualifiers:
B
Aaalyte detected in the associated Method Blank
E Value shove quanlitation range
14
Holding times for preparation or analy
J
Analyte detccicd below quantitation limits
M Manual Integration used to determine
area
response
MC
Value is belmy Minimum Compound
Original
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepled recovery limits
RL Reporting Detection Limit
8
Spike Recovery outside accepted reca
Page 19 of 34

S U '11 summitlilmirolrtaenhrl 7edmoli St.
3310 I0 Min St.
ENvinONkmENTALTECIINOLO(;IFS,niC Ci0•nliagrrl•'oIts. Ohio-14223
Analyffeaf Laboralar19E TF.L� [phone] FLY.• [phone]
IYe8she: litre://u ivw.setrek.cam
Client: Synagro
Project: Winston WTP
QC SUMMARY REPORT
WON: 20I20299
18-Dec-20
BatchU): 46758
Sample ID: LCSA6758
SampType: LCS
TestCode: TCLPSVOC- Units: mg1L
Prep Date: 121912020
RunNo: 121304
Client ID: LCSS
Batch tD: 4675a
TestNo: SW8081 SW3510C
Analysis Date: 1211212020
SegNo: 3115482
Analyte
Result
PQL SPK value SPK Ref Val
%REC LawLimit HighLimil RPD Ref Val
%RPD RPDLlmit Oual
Endrin
0.0107
0.000500
0.0100
0
107
10
130 m
gamma-BHC
0,00914
0.000500
0.0100
0
91.4
10
130
Heptachlor
0.0105
0.000500
0.0100
0
105
10
130
Heptachlor epoxide
0.00994
0.000500
0.0100
0
99.4
10
130
Melhoxychlor
0.0111
0.000500
0.0100
0
111
10
178
Surr: TCMX
16.8
20.00
83.9
10
130
Surr: DCB
20.6
20.00
103
10
130
Sample ID: MB-46758
SampType: MBLK
TestCode: TCLPSVOC- Units: mg1L
Prep Dale: 121912020
RunNo: 121304
Client ID: PBS
Batch ID: 46758
TestNo: SW8081 SW3510C
Analysis Dale: 1211212020
SegNo: 3115483
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
N❑
0.00500
Endrin
ND
0.000500
gamma-BHC
N❑
0.000500
Heptachlor
ND
0.000500
Heplachlorepoxide
ND
0.000500
Melhoxychlor
ND
0.000500
Suer: TCMX
15.3
Surr. DOB
19.6
Quoliners; B
Analyte detected in the associated Method Blank
I
Analyle detected below quantitation limits
ND
Not Detected
R
RPD Outside accepted recovery limits
20.00 767 10 119
20.00 98.1 10 119
E. Value above quantitation range H Holdingtintes for preparation oranaq
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted rccu
Original
Page 20 of 34

.Sruumir Eimironnrerrinl Teclp3310 H lot. QC SUMMARY REPORT
33I0 HIM Sr. SUMMARY 1 REPORT
ffISUMMIT
, Clr}nkpga Falls, Ohio 44223 lV0#: 20120299
Annfyflcaf Laboreforlas TEL: [phone] FAX. [phone]
IS ehsite. hifp:Mrmv.sellek.mnl 18 Dec-20
Client: Synagre
Project: Winston WTP BatclilD: 46776
Sample ID: MB-46776
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1211012020
RunNo: 121216
Client ID; PBS
Batch ID: 46776
TestNo: SW7470A SW7470A
Analysis Data: 1211012020
SegNo; 3111910
Analyte
Result
PQL SPK value SPX Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample 1D: LCS46776
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/1012020
RunNo: 121216
Client ID: LCSS
Batch ID: 46776
TestNo: SW7470A SW7470A
Analysis Date: 12/1012020
SegNo: 311f911
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00400 0.00200 0.00400 0 100 80 120
Sample ID: 20120268.00IAMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Data: 1211131200 2
RunNo: 121216
Client ID: BatehQC
Batch ID: 46776
TestNo: SW7470A SW7470A
Analysis Date: 1211012020
SegNo: 3111915
Anatyle
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00421 0.00200 0,00400 0,000108 103 75 125
Sample ID: 20120288-ODIAMSD
SampType: MS13
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1211012020
RunNo: 121216
Client ID: BatchQC
Batch ID: 46776
TestNo: SW7470A SW7470A
Analysis Dale: 1211012020
SegNo: 3111916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowltmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
� Mercury
0.00442 0.00200 0.00400 0.000108 108 75 125 0.00421 - 4.87 20
Qualifiers: B Analyte detected in the associated Method Blank F Value above quantitalionrange H Holding times forprepnmtion or anal}
1 Analyte detected below quantitation limits M Manual 0 legration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPDoulsideacecpledrzcovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 34

E=Mcrmsumm'll Snmmrt Frrvirnus+er+la!'I'ecAnooWec- QC SUMMARY' REPORT
3310 Wit,
in St.
Er ENWrtO) MENTAL T[6ttrtDWGIES, INC. CirynlrngaFalls, Olde44223
Analytlral Labareiortes TTL: [phone] FLY: (330) 253-44$9 WOO 20120299
Websire: Ann:/Avm,uellek.com 79-Aec--20
Client: Synagro
Project: Winston WTP 1latchlD: 46776
Sample ID: 20120286.001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Dale: 1211012020
RunNo: 121216
Client lD: Batch QC
Batch ID: 46776
TestNo; SW7470A SW7470A
Analysis Date: 1211012020
SegNo: 3111916
Analyte
Result
PQL SPK value SPK Ref Val
% REC Lo%vUrnit HlghLlmlt RPD Rat Val
% RPD RPDLlmit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Valueabovequantitatiommnge H Holding times for pmpamtion or anal}
J Analyte detected below quamitation limits M Manual integration used to determine area response MC Value is below Minimum Compound
1\.D h'et Detected P Second column eon0rmatian exceeds PL Permit Limit
Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 34

��' � Sumndf Ermironmeuurl Technologies.Nrc.
Mn 3310 Win Sr
ENVIRONMENTAL TECHNrII noI>:S, INC Crq,ahogaralls, 01do 44223
Analytical LahoratorleF TF_L: [phone] FAX., [phone]
IVeb.Oe. hrloaAvm,,sertek.eon+
Client: Synagro
Project: Winston WTP
QC SUMMARY REPORT
WM 20120299
18-Dvo-20
BatchtD: R121019
;ample ID: CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.020.20
Prep Date:
Runhlo: 121019
;lien; ID: LCSS
Batch ID: R121019
TestNo: SW9045D
Analysis Date: 121712020
SegW7 3105339
Ina]yte
Result
PQL SPK value SPK Re( Val %REC
LowLimil HighL;mit RPD Ref Val
% RPD RPDLimit Qua]
pH
7.0 7.0 0 101 90 110
Qllsllners: B Ann]yte detected in the associated h4ellzod Btank L Value above quanlitation Lange H Holding Times for preparation oranal�
J Aualyte detected below quantization limits M Manual Integration used to determine area response MC Value is below Miuimum Compound
Original
ND Not Detcc[rd P Second column confirmation exceeds PL Pezmit Limit
R RPD outside accepted recovery limits ILL Reporting Dclection Limit S Spike Recovery outside accepted reco
Page 23 of 34

umm' Summit F,iniroeareulal Teclumlagier, Me. ir 33I0 H'in Sr. QC SUMMARY REPORT
ENVIhONIArWrAL VEMINOI Orlr3, RIC Crrynhnga Falls, Ohio 44223
ANalytIcal LaboraroHes 7EL: [phone] FLY.' (330) 253-4-189 1V0#: 2012,0299
If ebsite: I+ttn:/hwiarsettekcam 7S-Dee-20
Client: Synagin
Project: Winston WTP BatchID: R12I019
Sample ID: LCS-R121019
SampTypa: LCS
TestOnde: pH_0[I(9045D Units: s.u.@20AC
Prep Date:
RunNo: 121019
Client ID: LCSW
Batch ID: R121019
TestNo: SW9045D
Analysis Date: 12A12020
SegNe: 3104675
Analyte.
Result
PQL SPK value SPK Ref Val %REC
LowLimil HighLimit RPD Ref Val
%RPD RPDLimil Qual
pH 7.0 7.0 0 101 90 110
Sample ID: 20120229.001ADUP
SampType: DUP
TestCode: pH_oil(9045D Units: s.u.@20.1C
Prep Date:
RunNo: 121019
Client ID: BatahQC
Batch ID: R121019
TestNo: SW9045D
Analysis Date: 121712020
SegNo: M04677
Analyte
Result
PQL SPK value SPK Ref Val % REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimi1 Qua[
pH 6,7 0 0
6.7 0.1 10
Qualifiers: H Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analy
I Analyte detected below quantitation limits M Mmmal bitegauon used to detemtine arcarespome MC Valve is belowhfiiiimuni Compound
ND Not Detected P Second column confirmation exceeds FL Permit Limit Original
m
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 34

srra,,r En,l ono a ,ur Technologies, Il.suMMI� 33101Flinst. QC SUMMARY REPORT
ENVInflNMENTAC IFGHNIMISIES, ntC 11s, Ohio 44223
ArralytlCal Laboraloges TF.L: 030) 2j3-8211 FAX. [phone] IV04: 20120299
IVehsife: hrin:/hwnmser7e.F.conr IS-Dec-20
Client: Synagro
Project: Winston WTP BatchLD: R121273
Sample ID: LCS-R121273
Sarnp7ype: LCS
TeslCode: Ignitabiiity_S Units: mmisec
Prep Date:
RunNo: 121273
ClienL ID: LCSS
Balch ID: R121273
TestNo: SWIM
Analysis pate: 1211012020
SegNo: 3113,380
Analyse
Result
PQL SPK value SPK Ref Vai
%REC Lowl-imil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 7.94 7.240 ❑ 110 70 130
Sample ID: 20120299-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mmisec
Prep Date:
RunNo: 121273
Cllent ID: Winston WTP
Batch ID: R121273
TestNo: SW7030
Analysis Date: 12110/2020
SegNo: 3113982
Analyte
Result
PQL SPXvalue SPK Ref Val %REC
LowUmit HighLimil RPD Ref Val
%RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 20120496.001ADUP
SampType: DUP
TeslCode: Ignitahllity_S Units: mmisec
Prep Data:
RunNo: 121273
Client ID: BatchQC
Batch ID: R121273
TestNo: SW1030
Analysis Date: 1211012020
SegNo: 31 i3984
Analyte
ReSull
PQL SPK value SPK Ref Val %REC
Lowl.imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 2.2 0 0 20
Sample ID: 20120496-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mmisec
Prep Dale:
RunNo: 121273
Client ID: Batch QC
Batch ID: R121273
TestNo: SW1030
Analysis Data: 1211012020
SegNo: 3114016
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLlmit HighLimil RPD Ref Val
%RPD RPDLimit Qual
Ignitablllty
nonflammable
Qualiflers: B Analyte detected in the associated Method Blank
! Analyte detected below quantitationlimits
ND NotDctected
R RPD outside accepted recovery limits
0 0 20
E Value above quantitation range A Holding tines for preparation or analy
M Manual letesration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 25 of 34

EnSUMMIT
Srrnrmir Eurirmmrenru7 T elnalogies, In.
33I0 I ['in Si.
ENVInoi4meNTALTECtiNtlt-OniF5,R1C 0,)whoga Falls, Ohio 44223
Analyrlral Caharaforles TEL: [phone] FAX. [phone]
Wehvrte: hgR:lArug,seriek.cnm
QC SUMMARY REPORT
WOI;: 20120299
1s-Dee-2o
Client: Synagro
Project: Winston WTP BatCItID: R121273
Sample Ill: 20120496.002ADUP
SampType: DUP
TestCode: Ignifabilit _S Units: mmisec
Prep Date:
RunNo: 121273
-lient ID: BetchQC
Batch ID: R121273
TestNo: SW1030
Analysis Date: 12110/2020
SegNo: 3114016
4nelyte
Result
PQL SPX value SPK Ref Val
%REC Lowl-Imit High Limit RPD Ref Val
%RPD RPDLImit Qual
Qualifies-s: B Analyte detected in the associated Method Blank E Value above gtramitation range H Holding times for preparation or anay
3 Analyte detected below quantitalion liruits M Manual Integration used to detcrn» ne area response MC Value is bciow Minimum Compound
ND Not Delecred P Second columnconfirmation exceeds PL Pemrit Limit Original
R RPD uutside accepted recovery limits RL ReportinglMection Limit S Spike Recovery outside accepted reco
Page 26 of 34

SUMMIT Srnnnillnin,,,nenr„1T•cl„310FEinSt. QC SUMMARY REPORT
3310 fl irr St.
ENvino raeNTAL MMINE31LO ES, WC Crgvrhoga Calls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone] WON: 20I20299
13'c8rire: 111r1+://urotvsurcl.can, 18-Dec-20
Client: Synagro
Project: Winston WTP BateldD: R121312
Sample ID: Blank
SampType: MBLK
TeslCode: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 121312
Client ID: P13W
Batch ID: R121312
TestNo: SW9014
Analysis Date: 1211312020
SegNo: 3114988
Analyle
Result
PQL SPK value SPK Ref Val
%REC LowLimit HfghLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive No 0.485
Sample ID: LCS
SampType: LCS
TestCode: Cyanlde,Rea Units: mglL
Prep Date:
RunNo: 121312
Client ID: LCSW
Batch ID: R121312
TestNo: SW9014
Analysis Date: 12/1312020
SegNo: 3114989
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit High Limit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.51 GA90 10.00 0 95A 85 115
Sample ID: Ri.Check
SampType: RLC
TeslCode: Cyanide,Rea Units: mg)L
Prep Date:
RunNo: 121312
Client ID: Batch=
Batch ID: R121312
TestNo: SW9014
Analysis Date: 1211312020
SegNo: 3114991
Analyie
Result
PQL SPK value SPK Ref Val
%REC LowLimil High Limit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 0.543 0,481 0.5000 0 109 65 135
Sample ID: 20120711-007AMS
SampType: MS
TeslCode: Cyanide,Rea Units: mgll.
Prep Date:
RunNo: 121312
ClientJr); BatchOC
Batch ID: R121312
TestNo: SW9014
Analysis Date: 12/1312020
SegNo: 3115003
Aualyle
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.45 OA90
10.00 0 94.5 75
125
Qualifiers: B
Analyle detected in the associated Method Blank
E Value above quantitation range
H
Holding times forpreparadon oranall
1
Analyle detected below quantitation limits
M Manual Integration used to detemtirto area response
MC
Value is below Mutimunt Compound
ND
Not Detected
P Second column confimtatiat exceeds
PL
Permit Limit
k
RPD outside accepted "ovcry limits
RL Repoating Detection Limit
S
Spike Recovery outside accepted reeo
Original
Page 27 of 34

S V I Summit 6,n.i,.nnarenrrrl Teda331O er, Inil'in Si. c. QC SUMMARY REPORT
3310
6NVOILINkt ENTAL TECHNULD¢IES, INC Ctry�nlln eFa!!s, Ohio 44223 WO#: 20120299
Ansfy1tcal Laboratories TEL: [phone] FAX.- [phone]
Wehsite: hJrp:1Auitw.senek.enn+ 18Dee-20
Client: Synagro
Project, Winston WTP RatcbID: R121312
Sample ID: 20120711.007AMS
SampType: MS
TesiCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 121312
Client ID: Ba1chQC
Batch ID: R121312
TestNo: SWO014
Analysis Date: 1211312020
SegNo: 3115003
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit 1-119hUmit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20120711-007AMSD SampType: MSD
TesiCode: Cyanlde,Rea Units: mglL
Prep Date:
RunNo: 121312
Client 113: BatchQC Batch ID: R121312
TestNo: SW9014
Analysis Date: 1211312020
SegNo: 3115004
Analyte Result
PQL SPK value SPK Ref Val
%REC LowUrnil Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.46 OA81 10.00 0 94.6 75 125 9.446 0,121 16
Quantiers: B Analyte detected in the associated Mc[hod Blank E Value ahove quantitation range H Holding times for preparation a anall
J Analyte detceted helow quantitation limits M Manual lutegration used io detemtine area response MC Value is belnw Murimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Ortgitlal
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 34

frSUMMIT
3310 Sunrmi(Em•irwrmen(ul TeclnJs,hle. QC SUMMARY "PORT
3310 A iu Si. lY1SUMMARY
ENVInoNhtEHTAL'rEcHHoLo0:E5,INC OriahogaFalls. Ohio 44223
Analy:lcal Laboratolles TF.b: [phone] FAX. [phone]VQfi: 20/20299
Wehsile: 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: R121313
Sample ID: MB-R121313
SampType: MBLK
TeslCode: Sulfide,React Units: mglL
Prep Date:
RunNo: 121313
Client ID: PBW
Batch ID: R121313
TestNo: SW9034
Analysis Date: 12/1312020
SegNo: 3115019
Analyte
Result
PQL SPK value SPK Ref VW
%REC LowLimtt HighLimi€ RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R121313
SampType: LCS
TestCade: Sulfide,React Units: mglL
Prep Data:
RunNo: 121313
Client ID: LCSW
Batch ID: R121313
TestNo: SW9034
Analysis Date: 12M312020
SegNo: 3115020
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3130 25.0 3090 0 101 85 115
Sample ID: 20120711-007AMS
SampType: MS
TestCade: Sulflde,React Units: mglL
Prep Date:
RunNo: 121313
Client ID: Batch=
Batch ID: M21313
Tes1Ne: SW9034
Analysis bate: 1211312020
SegNo: 3115031
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLIm€t Qual
Sulfide, Reactive 2870 25.0 3090 0 92.9 75 125 IN
Sample ID: 20120711.0117AMSD
SampType: MSD
TestCade: Sulfide,React Units: mglL
Prep Date:
RunNo: 121313
Client [Di BatchQC
Batch ID: R121313
TestNo: SW9034
Analysis Date: 12M312020
SegNo: 3115032
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2730. 25.0
3099 0 88.3 75
125
2870 5.00 SO W
Qualifiers: B Analyte detected in the associated Aledrod Blank
6 Value above quandlation range
H
Haldingtitnesforprepamtionoranat7
] Analytedeteetedbelowquanti[ationlimiis
M Manual integration used to determine area response
MC
Value is below Minimtun Canpound
ND Not Detected
P Second colwnn confirmation e>;ceuls
PL
Original
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Linrit
S
Spike Recovety outside accepted reco
Page 29 of 34

summ'ttir Srrnanil F.In irmuaerrral Teckn310THn Sr. Inc. QC SUMMARY REPORT
ErENVatOM1.WNTnL TecttrloLoaiFa, IRC Ct lroga Fa33101lls, 01no 44223
AnafyffCal Laboraforles 7CL: (330) 2534211 FAX, [phone] Woff: 20120299
FYcbsire: l�da://uwtvseuek.emre l S-Dec-.ZO
Client: Synagrn
Project: Winston WTP RatchlD: R121313
Sample ID: 20120711-007AMSD
SampTyps: MSD
TestCode: Sulfide,React Units: mglL
Prep Dale:
RunNo: 121313
Client ID: BatchQC
Batch ID: R121313
TestNo: SW9034
Analysis Date: 1211312020
SegNo: 3115032
Analyte
Result
PQL SPK value SPX Ref Val
% REC LowLimit HighUrnit RPD Ref Val
% RPD RPDLlmiI Qual
Quallfiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second caltrmn confirmation exceeds
RL keportiug Detection Limit
H Holding tintes for preparation or anaty
MC Value is below Minimum Compound
PL Pennit Limit
S Spike Recovery outside accepted reco
Original
Page 30 of 34

M' s""'°''1 Erl i,vnnle,aal Technninglrs, lire. QC SUMMARY REPORT
3310 ff rn S1.
ENVIRONrdENTAL TECHNOLOOIFS, INC Cuyahoga Falls, 01da44223 ffjAnalyffcal Laboratoiles 1EL: [phone] FAX.' [phone] 1V0#: 2012D244
IVebsile: h8o://wn-wsellek.cmn 18-Dec-20
Client: Synagro
Project: Winston WTP BatellID: R121521
Sample ID: MR
SampType: MBLK
TestCode: SVOC-Herb_ Units: mgfL
Prep Dale:
RunNo: 121521
Client ID: PBW
Batch ID: R121521
TestNo: SW8321A
Analysis Date: 12/1612020
SegNo: 3123461
Analyze
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit 1-119hUmit RPD Ref Val
%RPD RPDLimit Qual
2,4-D NO OA250
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.847 11.000 84.7 70 130
Sample ID: LCS
SampType: LCS
TeslCode: SVOC-Herb_ Units: mg1L
Prep Date:
RunNo: 121521
Client ID: LCSW
Batch ID: R121521
TestNo: SW8321A
Analysis Date: 1211612020
SegNo: 3123462
Analyte
Result
PQL SPK value SPK Ref Val
%RHC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.339 0.0250 0.3000 0 113 70 13o
2,4,5-TP 0.293 0.0100 0.3000 0 97.8 10 130
Surr: 2,4-Dichlerophenylacetic acid 2.85 3.000 94.9 70 130
Sample ID: LCS
SampType; LCSD
TestCode: SVOC-Herb_ Units: mgtL
Prep Date:
RunNo: 121521
Client ID: LC5802
Batch ID: R121521
TestNo: SW8321A
Analysis Dale: 1211612020
SegNo: 3123463
Analyze
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimil Qual
2,4-D 0.324 0.0250 0.3000 0 108 70 130 0.3389 4.46 30
2,4,5-TP 0.280 0.0100 0.3000 0 93.3 70 130 0.2934 4.71 30
Surr: 2,4411chlerophenylacetic acid 2.71 1.000 271 70 130 0 30 S
Qualifiers: B Analyte detected in the associated Method BlanL E Value above quantitation range H Holding limes ror preparation or anal]
1 Analyte detected below quantization limits M Manual Integration used to determine area response )AC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL PemritLuuh Original
R RPD outside accepted recovery limits RL Reporting Delectioa Limit S Spike Recovery outside accepted reco
Page 31 of 34

SUMMIT
Snnnnit Ent4winueulal Technalogies, Lie. QC SUMMARY REPORT
3310 TI O Sl,
ENVIAONIAEWAL TLCHHOLOGIfS, nIC Cigahoga Falls, Ohio 44223
Artalysicei Lahoratorlev TFL: [phone] F ff..- [phone] 1VO#: 20/20299
IVeheile: 1r11v:/r5rvmsellek.mnv 18-Dec-20
Client: Synagro
Project: Winston w,rP Batchm: R121521
Sample ID: 20120773.001AMS
SampType: MS
TestCode: SVOC-Herb_ Units: mg1L
Prep Data:
RunNo: 121521
Client ID: Betch=
Batch ID; R121521
TestNo: SW8321A
Analysis Date: 1211612020
SegNo: 3123465
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLlmit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
15.9
1.25 15.00 0.5200
102
70
130
H
2,4,5-TP
13.0
0.500 15.00 0
87.0
70
130
H
Sutr. 2,4-Dichlorophonylacetic acid
126
150.0
41.6
70
130
SH
Sample ID: 20120773.00IAMS
SampTypo: MSD
TestCode: SVOC-Herb_ Units: mg1L
Prep Date:
RunNo: 121521
Client ID: BatchQC
Batch ID: R121521
TestNo: SW8321A
Analysis Date: 12H61202D
SegNa: 3123466
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-intit HighLlmit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
2,4,5-TP
Surr: 2,4-Dichlarophenylacelic acid
16.0 1.25 15.00 0.5200 103
13.1 0.500 15.00 0 87.6
127 50.00 126
Qualifiers: B Aualyte detected in the associated Method Blank
S Analyte detected below quantitation limits
ND Nat Detected
R RPD outside accepted recovery limits
70 130 15.88 0.784 30 H
70 130 13.05 0.726 30 H
70 130 0 30 H
E Value above quantitatian range H Holding tunes for preparation or anal]
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Repodiug Detection Limit S Spike Recovery outside accepted reco
Original
Page 32 of 34

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Page 1 of 1

SUMMITm5uorrt Enriroru�ierrtu! Technologies, Inc.
3310 Wiu St.
ENVI"ONMENTAL TEGIINOLDGIFR, INC. 0(yabogvralis, 01210 44223 Sample Lag -In Check List
Analvlrcal l aboralorles TEL: [phone] FAX., [phone]
Websile: hupalwrvm.settel.com
Client Name: SYN-NC-27028 Work Order Number: 20120299
RcptNo: 1
Logged by: Jacqueline Rasiie 121412020 10:55:00 AM
Completed By: Jacqueline Rasile 12/6/2020 3:47:22 PM
Reviewed By: Jennifer Woolf 12/7/2020 2:04:11 PM
Chain of Custody
1. Is Chain of Custody complete?
Yes
❑
No 'Vi Not Present 1
2, How was the sample delivered?
FedEx
L. og In
3. Coolers are present?
Yes
FVI
No
NA
4, Shipping container/cooler in good condition?
Yes
W]
No .
Custody seals intact on shipping containerlcooler?
Yes
❑
No Not Present Vi
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
✓❑
No U
NA
6, Were all samples received at a temperature of >0° C to 6.0°C
Yes
0
No Ll
NA
7. Sample(s) in proper container(s)?
Yes
No
$, Sufficient sample volume for indicated test(s)?
yes
❑.
No II
g. Are samples (except VOA and ONG) properly preserved?
Yes
No I
10. Was preservative added to bottles?
Yes
❑
No J,
NA
11, Is the headspace in the VOA vials less than 114 inch or 6 mm?
Yes
❑ No L_i No VOA Vials No,
12. Were any sample containers received broken?
Yes
No WI
13. Does paperwork match bottle labels?
Yes
U No ❑
(Note discrepancies on chain of custody)
14, Are matrices correctly identified on Chain of Custody?
Yes
No ❑
15. Is it clear what analyses were requested?
Yes
No ❑
16. Were all holding times able to be met?
Yes
❑ No ❑
(If no, notify customer for authorization.)
Special Handling (if annlicable}
17. Was client notified of all discrepancies with this order?
Yes
❑ No ❑ NA ❑
Person Notified: [ Alex Fox Date:
12/7/2020
By Whom: jJennifer Woolf Via:
Ls/] elMail ❑ Phone ❑ Fax ❑ In Person
Regarding: lsamDle date listed as 9122/20. time as 10/15/20
Client Instructions: It was sampled on 1212/20 and time collected be 11:15 shipped at 1:00
18. Additional remarks:
sample date incorrect
Cooler Information
LCooier No Temp °C
I Condition
Seal Intact
I Seal No I
Seal Date
Signed By
Page 34 of 34

qc, 1"51L 12 0 2. q q3 mg
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Section 4
• Maps of the residuals disposal sites

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MAP LEGEND
Area of Interest (AOI)
E] Area of Interest (AO I)
Soils
Soil Map Unit Polygons
0 Soil Map Unit Lines
13
Soil Map Unit Points
Special
Point Features
LO)
Blowout
®
Borrow Pit
Clay Spot
Closed Depression
Gravel Pit
Gravelly Spot
0
Landfill
IL
Lava Flow
Marsh or swamp
a
Mine or Quarry
0
Miscellaneous Water
0
Perennial Water
V
Rock Outcrop
+
Saline Spot
'.�
Sandy Spot
Severely Eroded Spot
Sinkhole
p
Slide or Slip
Sodic Spot
Soil Map —Forsyth County, North Carolina
Spoil Area
Stony Spot
Very Stony Spot
Wet Spot
Other
Speclal Line Features
Water Features
_ Streams and Canals
Transportation
r r Rails
ram/ Interstate Highways
US Routes
Major Roads
Local Roads
Background
® Aerial Photography
MAP INFORMATION
The soil surveys that comprise your AOI were mapped at
1:15,800.
Warning: Soil Map may not be valid at this scale.
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
line placement. The maps do not show the small areas of
contrasting soils that could have been shown at a more detailed
scale.
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System: Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of distance or area are required.
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Forsyth County, North Carolina
Survey Area Data: Version 20, Jun 3, 2020
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: May 18, 2019—May
21, 2019
The orthophoto or other base map on which the soil lines were
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
USDA Natural Resources Web Soil Survey 2/3/2021
Conservation Service National Cooperative Soil Survey Page 2 of 3

Soil Map —Forsyth County, North Carolina
Map Unit Legend
FaC
Fairview f ne sandy loam, 6 to 0.8
7.9%
10 percent slopes
FaD Fairview fine sandy loam, 10 to
0.0
0.1%
15 percent slopes
FaF
Fairview fine sandy loam, 15 to
1.21 12.0 %
45 percent slopes
NaB
Nathake sandy loam, 2 to 6
1.4
13.7%
percent slopes
NaC
Nathalie sandy loam, 6 to 10
2.8
28.3%
percent slopes
TmB
Tomlin loam, 2 to 6 percent
1.4
13.9%
slopes
Tbtals for Area of Interest
10.0
100.0%
usDA Natural Resources Web Soil Survey 2/3/2021
Conservation Service National Cooperative Soil Survey Page 3 of 3

36" 926"N
36° 9' S N
Soil Map —Forsyth County, North Carolina it
m �
550580 550BEO 593740 550M 55M
3
Map Scale: 1:3,250 if printed on A porbrait (9.5' x 11") sheet
Meters N
0 45 90 180 270
A
Feet
0 454 300 6t10 9�0
Map projection: Web Mercator Comercooniirobaas: WGSM Edge tics: UTM Zone 17N WGS8 4
USb1 Natural Resources Web Soil Survey
Conservation Service National Cooperative Soil Survey
36' 9 26" N
v
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f?
o_
0
55mm 5510ao
3
213/2021
Page 1 of 3

Sail Map —Forsyth County, North Carolina
MAP LEGEND
MAP INFORMATION
Area of interest iAog
Spoil Area
The soii surveys that comprise your AOI were mapped at
11
�..,... 1!
Area ofinterest (AOI)
Stony Spat
f:15,800.
_.,__................_.,.m._...,......,......_._.,_..._.._.__._.�._.__—_.-_.......m._.......r,_
soilst
verySlonyspot
Warning: Soil Map may not be valid at this scale.
Soil Map Unit Polygons
Wet spot
Enlargement of maps beyond the scale of mapping can cause
Soil Map Unit Lines
misunderstanding of the detail or mapping and accuracy or soii
p
Other
line placement. The maps do not show the small areas of
®
Soil Map Lint Points
Special Line Features
Contrasting soils that could have been shown at a more detailed
Special
Point Features
scale.
Blowoul
Water Features
_ .,.
Streams and Canals
Please rely on the bar scale on each map sheet for map
Barrow Pit
measurements,
Transportation
Clay Spot
#_H
Rails
Source of Map: Natural Resources Conservation Service
Closed Depression
Web Soil Survey URL:
Interstate Highways
Coordinate System: Web Mercator (EPSG:3857)
r
Gravel Pit
US Routes
Maps from the Web Soil Survey are based an the Web Mercator
e
Gravelly Spot
Major Roads
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Landfill
Local Roads
Albers equal-area conic projection, should be used if more
Lava Flow
accurate calculations of distance or area are required.
Background
Marsh or swamp
Aerial Photography
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Mine orQuarry
Soil Survey Area: Forsyth County, North Carolina
Miscellaneous Water
Survey Area Data: Vamlon 20, Jun 3, 2020
Perennial Water
Soil map units are labeled (as space allows) for map scales
Rock Outcrop
1:50,000 or larger.
Saline Spot
Date(s) aerial images were photographed: May 18, 2019--May
21, 2019
Sandy Spot
The orthophoto or other base map on which the soil lines were
Severely Eroded Spot
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
gJ
Sinkhole
shifting of map unit boundaries may be evident.
y,
Slide or Slip
Sodic Spot
usDA Natural Resources Web Soil Survey 21312021
WO Canservalion Service National Cooperative Soil Survey Page 2 of 3

Soil Map —Forsyth County, North Carolina
Map Unit Legend
Map Unit Symbol
Map Unit Name
Acres in AOI
Percent of AOI
CmC2
Clifford clay loam, 6 to 10
0.3
1.7%
percent slopes, moderately
eroded
FaF
1.0
5.3%
Fairview fine sandy loam, 15 to
45 percent slopes
TmB
Tomlin loam, 2 to 6 percent
9.8
51.1 %
slopes
TmC
Tomlin loam, 6 to 10 percent
4.8
25.4%
slopes
Tomlin loam, 10 to 15 percent
2.9
TmD
15.3%
slopes
1.1 %
WmB
Wickham fine sandy loam,
0.2
mesic, 2 to 6 percent slopes
Totals for Area of Interest
19.1
100.0%
u Natural Resources Web Soil Survey 213/2021
r Conservation Service National Cooperative Soil Survey Page 3 of 3

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MAP LEGEND
Area of Interest (A01)
E] Area of Interest (AOI)
Soils
0 Soil Map Unit Polygons
Soil Map Unit Lines
®
Soil Map Unit Points
Special
Point Features
U
Blowout
Borrow Pit
Clay Spot
Closed Depression
Gravel Pit
Gravelly Spot
p
Landfill
A.
Lava Flow
w
Marsh or Swamp
JZ
Mine or Quarry
Miscellaneous Water
0
Perennial Water
IV
Rock Outcrop
+
Saline Spot
Sandy Spot
�C_
Severely Eroded Spot
Sinkhole
Siide or Slip
Sodic Spot
Soil Map —Forsyth County, North Carolina
MAP INFORMATION
1�
Spoil Area
The soil surveys that comprise your AOl were mapped at
9:15,800.
Stony Spot
Very Stony Spot
Warning: Soil Map may not be valid at this scale.
wet Spot
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
Other
line placement. The maps do not show the small areas of
rr
Special Line Features
contrasting soils that could have been shown at a more detailed
scale.
Water Features
-_ Streams and Canals
Transportation
Rails
,s Interstate Highways
US Routes
Major Roads
Local Roads
Background
0 Aerial Photography
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System: Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of distance or area are required.
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Forsyth County, North Carolina
Survey Area Data: Version 20, Jun 3, 2020
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: May 18, 2019—May
21, 2019
The orthophoto or other base map on which the soil lines were
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
USDA Natural Resources Web Soil Survey 2l312021
Conservation Service National Cooperative Soil Survey Page 2 of 3

Soii Map —Forsyth County, North Carolina
Map Unit Legend
Map Unit Symbol
Map Unit Name
Acres in AOI
Percent of AOI
PpD2
Poplar Forest clay loam, 10 to
D.6
5.9%
15 percent slopes,
moderately eroded
TmB
Tomlin loam, 2 to 6 percent 4.6
34.8%
slopes
TmD
Tomlin loam, 10 to 15 percent 2A
15.3 %
slopes
T092 I Tomlin clay loam, 2 to 6
2.1
16.31%
percent slopes, moderately
eroded
7b02 Tomlin clay loam, 6 to 10
1.41 10.5 %
percent slopes, moderately
eroded
ToD2
Tomlin clay loam, 10 to 15
.2.3
17.2^/
percent slopes, moderately
eroded
Totals for Area of Interest
13.2
100.D
USDA Natural Resources Web Soil Survey 2/312021
2rwConservation Service National Cooperative Soil Survey Page 3 of 3

36° S' 4° N
36° 7 39" N
YK — Xu 3
Soil Map —Yadkin County, North Carolina
547030 547120 547210 5473M 547390
3
Map Scale: 1:3,710 If printed on A pabalt a 5 x 11" sheet
Meters
$ N 0 50 100 200 30]
A ze1
Map projection: Web Mercator Caner o>a�inates: WGS84 Edge tics: LrrM Zane 17N WGS84
USDA Natural Resources Web Soil Survey
Conservation Service National Cooperative Soil Survey
36" OWN
N
I
o_
36° T39"N
547480 547570
3
2J312021
Page 1 of 3

MAP LEGEND
Area of Interest (A01)
❑
Area of Interest JA01)
Soils
L_J
Sall Map Unit Polygons
Soil Map Unit Lines
®
Soil Map Unit Paints
Special
Point Features
(6
Blowout
®
BDR-w Plt
Clay Spot
O
Closed Depression
Gravel Pit
Gravelty Spot
Landfill
Lava Flow
46
Marsh or swamp
Mine or Quarry
Miscellaneous Water
0
Perennial Water
V
Rock outcrop
+
Saline Spot
!
Sandy Spot
Severely Eroded Spot
0
Sinkhole
Jip
Slide or Slip
jy
Sodic Spot
Soil Map --Yadkin County, North Carolina
Spoil Area
Stony Spiel
Very Stony Spot
Wet Spot
Other
Spacial Line Features
Water Features
.. Streams and Canals
Transportation
r-i--r Ralls
Interstate Highways
_ - US Routes
Major Roads
Local Roads
Background
IQ Aarial Photography
MAP INFORMATION
The soil surveys that comprise your A01 were mapped at
1:15,800.
Warning: Soil Map may not be valid at this scale.
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
line placement. The maps do not show the small areas of
contrasting soils that could have been shown at a more detailed
scale.
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System: Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of &stance or area are required,
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Yadkin County, North Carolina
Survey Area Data: Version 23, Jun 3, 2020
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: May 18, 2019—May
21, 2019
The orthopholo or other base map on which the soil lines were
compiled and digitized probably differs from the background
Imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
UsD.\ Natural Resources Web Soil Survey 21312021
a Conservation Service National Cooperative Soil Survey Page 2 of 3

Soil Map —Yadkin County, North Carolina
Map Unit Legend
Map Unit Symbol
Map Unit Name
Acres in AOI
Percent of AOI
Cab
Clifford fine sandy loam, 2 to 6
1.4
4.5%
percent slopes
Clifford sandy clay loam, 2 to 6
83.2%
CcB2
25.3
percent slopes, moderately
eroded
CcC2
Clifford sandy clay loam, 6 to
2.2
7.3%
10 percent slopes,
moderately eroded
FaD
Fairview fine sandy loam, 10 to
0.4
1.4%
15 percent slopes
1.3%
FaE
Fairview fine sandy loam, 15 to
0.4
25 percent slopes
FeE3
Fairview clay loam, 15 to 25
0.3
0.9%
percent slopes, severely
eroded
GuE
Gullied land -Fairview complex,
0.4
1.4%
10 to 25 percent slopes
30.4
Totals for Area of Interest
100.0%
USD,� Natural Resources Web Soil Survey 2/3/2021
Conservation Service National Cooperative Soil Survey Page 3 of 3

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MAP LEGEND
Area of Interest (AOI)
E] Area of Interest (AOI)
Soils
Q Soil Map Unit Polygons
�e Soil Map Unit Lines
®
Soil Map Unit Points
Special
Point Features
tod
Blowout
0
Borrow Pit
Clay Spot
Closed Depression
Gravel Pit
Gravelly Spot
Landfill
L
Lava Flow
Marsh or swamp
Mine or Quarry
Miscellaneous Water
Peronniai Water
,V
Rock Outcrop
+
Saline Spot
Sandy Spot
.�
Severely Eroded Spot
Sinkhole
p
Slide or Slip
Sodic Spot
Soil Map —Forsyth County, North Carolina
MAP INFORMATION
Spoil Area
The soil surveys that comprise your AOI were mapped at
1:15,1300.
Stony Spot
LiZ
Very Stony Spot
Warning: Soil Map may not be valid at this scale.
y
Wet Spot
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
h,
Other
line placement. The maps do not show the small areas of
Special Line Features
contrasting soils that could have been shown at a more detailed
scale.
Water Features
Streams and Canals
Transportation
+44 Rails
Interstate Highways
- US Routes
Major Roads
Local Roads
Background
® Aerial Photography
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System. Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of distance or area are required.
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Forsyth County, North Carolina
Survey Area Data: Version 20, Jun 3, 2020
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: May 18, 2019—May
21. 2019
The orthophoto or other base map on which the soil lines were
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
USDA Natural Resources Web Soil Survey. 2/3/2021
Conservation Service National Cooperative Soil Survey Page 2 of 3

Sniff Map —Forsyth County, North Carolina
Map Unit Legend
Map Unit Symbol
Map Unit Name
Acres in AO1
Percent of AO1
CoA
Codorus loam, 0 to 2 percent
0.7
8.9%
slopes, frequently flooded
.ikB
Jackland fine sandy loam, 2 to
V
0.8%
6 percent slopes
Ok8
Oak Level loam, dark surface,
4.6
59.7%
2 to 6 percent slopes
RaC
Rasalc fine sandy loam, 6 to
1.6
20,7%
10 percent slopes
SmD Siloam sandy loam, 10 to 15
0.8
10.0%
percent slopes
Totals for Area of Interest
7.6
100.0%,
Natural Resources Web Soil Survey 213/2021
Conservation Service National Cooperative Soil Survey Page 3 of 3

Section 5
• Field soil sampling results
• Agricultural Lime Application Logs

Agricultural Lime Application Log
Year: 2020
Project: Winston
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
from soil analysis)
Applied(CCE Eq.)
FO-X9-I
6.0
O.OTIAc.
YK-X43-1
5.8
0.5TIAc.
FO-XI0-1
6.1
0.0 TIAC
FO-X11-1
5.9
0.5TIAc.
FO-X2-1
6.8
O.OTIAc.
FO-X2-2
6.8
O.OTIAc.
*Lime will be applied when conditions improve.

Page 1 of 1
Report No: 21-004-0511
Account No: 12259
Advisor: 5ynagro/Columbus NC
Mary Brewer
284 Boger Rd
Mocksville NC 27028
Waypointo
ANALYTICAL
Client: Winston WTF
2020
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: FO-X2
Date Received: 01/04/2021
Date of Report: 01/06/2021
Lab No Field ID Sample 1D
Soil Class HM% li pH
Ac
P-1
K-1
S-1
Mn-1
Mn-A11 Mn-Al2
Zn-1
Zn-Al Cu-1
CEC BS% Ca% li ESP Na
109899 1
MIN
6.8
0.2
42
60
48
188
11 a
0
180
180 230
8.5 98 73 20 1.4 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (t/acre)
0.0
N
150
P2O5
40
K2O
30
S
20
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
09900 2
MIN
6.8
0.2
33
56
50
281
173
0
155
155 180
8.2 97 70 23 1.0 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lblacre
Lime (t/acre)
0.0
N
150
P2O5
60
K2O
30
S
20
Mn
0
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meg110Ccm3; Np3 N in mg/dm3; WN in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.govlagronomil
Report No. FY21-SL011134
Client: Tony Apperson
Advisor: Synagro
Predictive
3640 River Ridge Rd
5ynagro
�4,��f'll
PFAFFTOWN, NC 27040
284 Boger Rd.
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County :Forsyth
Links to Helpful Information
Client ID: 408618
Advisor ID: 503079
Sampled: 10/27/2020 Received: 10128/2020 Completed: 11/12/2020
Farm: FO-X9
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P205
K20 Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 120
80 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in glcm3; GEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class: Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI
Cu-1 Na ESP SS -I NO3-N
0.22 1.06
6.9 84 1.1 6.0 9 31
50 32
150 1058 652 153 153
57 0.1 1
North. Carolina
;'."N
Al
Ie+haccr• in.nS F ur.il C�.>'rn:u+�i�,n
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve 7rox1er, Commissioner ofAciriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi
Report No. FY21-SL011134
Tony Apperson
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
Iblacre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K2O
potash
for the crop being grown, not on soil test results. K-1 and P-I values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.govlagronomilpubs.htm.
NOa-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncacrr.pov/aaronomi/obpart4.htmt Sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P2O5
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routine)
Zn-1
zinc index
available)j indicate levels of plant nutrients or other fertility measurement. Visit www.nca r. ov/a ronomilu rst.htm

Page 1 of 1
Report No: 21-004-0513
Account No: 12259
Advisor: SynagrolColumbus NC
Mary Brewer
284 Boger Rd
Mocksville NC 27028
Waypoint.(D
ANALYTICAL
Client: Brandon Jones
2020
Lab No Field 1D Sample ID Soil Class HM% W/V pH Ac
09903 1 MIN 2.3 6.1 1.1
Crop Recommendations: Rec Uom Lime (t/acre) N
1- Fescue Hay Iblacre 0.5 150
Comment:
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: FO-X10
Date Received: 01/04/2021
Date of Report: 01/05/2021
P-1
K-1
S-1
Mn-1
Mn-All Mn-Al2
Zn-I Zn-Al Cu-1 GEC BS% Ca% Mg% ESP Na
7
37
104
225
150 0
238 238 70 8.0 87 58 25 0.7 0.1
P205
K20
S
Mn
Zn Cu
B Mg Last Crop
128
64
20
0
0 0
0 0
Test result units = CEC and Na in mec{1100cm3; NO3 N in mgldm3; WN in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 21-004-0514
Account No: 12259
Advisor: Synagro/Columbus NC
Mary Brewer
284 Boger Rd
Mocksville NC 27028
D
Waypoint(
ANALYTICAL
Client: Jim Stimpson
2020
Lab No Field !D Sample 1D Soil Class HM% W/V pH Ac
09904 1 MIN 1.5 5.9 1.2
Crop Recommendations: Rec Uom Lime (Vacre} N
1- Fescue Hay Ib/acre 0.5 150
Comment:
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm:FO-X11
Date Received: 01/04/2021
Date of Report: 01/05/2021
P-1
K 1
S-1
Mn-1
Mn-All Mn-Al2
Zn4 Zn-Al Cu-1 CEC SS% Ca% Mg% ESP Na
7
17
121
444
285 0
230 230 55 7.2 83 52 29 0.7 0
P205
K2
S
Mn
Zn Cu
8 Mg Last Crop
128
107
20
0
0 0
0 0
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in glcm3
North Carolina Division of Water quality Certification 9257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Rage 1 of 1
Report No: 21-004-0515
Account No: 12259
Advisor: SynagrolColumbus NC
Mary Brewer
284 Boger Rd
Mocksville NC 27028
e
Waypoint
ANALYTICAL
Client: Eddie Wooten
2020
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm:4K-X43
Date Received: 01/0412021
Date of Report: 01/06/2021
.ab No Field 1D Sample ID
Soil Class HM% WIV pH
Ac
P-1
K-1
S-1
Mn-1
Mn-All Mn-Al2 Zn-1 Zn-Al Cu-1 CEC BS% Ca% Mgt ESP Na
)9905 1
MIN 1.2 5.8
0.8
9
27
77
119
91 0 130 130 30 4.4 81 46 31 1.2 0.1
:rop Recommendations:
Rec Uom Lime (bacre)
N
P2 05
K20
S
Mn
Zn Cu B Mg Last Crop
i- Fescue Hay
lb/acre 0.5
150
122
84
20
0
0 0 0 0
Comment:
Test result units = CEO and Na in meg1100cm3; NO3 N in mgldm3; WN in g1cm3
North Carolina Division of Water Quality Certification 9257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Winston-Salem/Forsyth County Utilities
WQ0031314
2020 Residuals Land Application Report
R.W. Neilson Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form DMSDF(Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form DMSDF(Supp) -Class A Annual Distribution and
Marketing/Surface Disposal Certification and Summary Form (Supplemental
Information)
• DEQ Form RSSF -Annual Residual Sampling Summary Form
• DEQ Form RSSF B -Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT 9: WQ0031314 FACILITY NAME: Winston Salem - Neilson Water Treatment Plant
PHONE: COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes Rl No ❑ —► If No skiu harts A. B. C and certifv form below
Part Ax
Part B*:
Volume (dry tons)
Sources(s) (include NPDES # i€
Recipient Information
Name(s)
Volume (dry tons)
Intended use(s)
Mouth Amendment/
applicable) Residual In Product Out
Bulking Agent
January
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF (sup)
0
338.8
338.8
Totals: Annual (dry tons):
0
338.8
338.8
33S-9
Amendment(s) used:
Bulking Aaent(s) used:
m u more space is required, attach additional information sheets (FORIM DMSDF (supp)); Total Number of Form DMSDF (Supp)L 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
I _ All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2_ All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submi a information, including the possibility of fines and imprisonment for knowing violations."
;2- ;2.2 - 20z 1 0,- Z a -an a ►
Signature of Penn tte Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (1212006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0031314 FACILITY NAME:
Forsyth
PHONE:
COUNTY:
FACILITY TYPE (please check one):
Winston Salem - Neilson Water Treatment Plant
OPERATOR: City of Winston Salem
❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
❑ Distribution and Marketing (complete Parts A, and 13)
Part A*:
Part B*:
Mouth
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient information
Amendment)
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
May
Neilson WTP-NCO086011
338.8
338.8
Roger Spillman
338.8
soil amendment
Totals:
Annual (dry tons):
0
338.8
338.8 338.8
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information. sheets (FORM DMSDF (supp)):
Total Number of Form DMSDF (Supp)l 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0031314
Facility Name: Winston SalemlForsyth County Utilities Commission
Residual Source WQ # or
NPDES #:
NCO086011
WWTP Name: Neilson Water Treatment Plant
Residual Analysis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
m /k a
Sample or Composite Date
4/22/20
#1
4/22/20
#2
4/22/20
#3
4/22/20
94
Spring
Average
Percent Solids (%)
NA
28.4
29.3
28.7
32.7
30
Arsenic
75
6.22
7.54
7.52
7.67
7
Cadmium
85
0.327
0.334
0.321
0.3
0
Copper
4,300
47.7
48.4
51.4
49
49
Chromium
NA
59.4
59.2
61.5
60.5
60
Lead
840
27.8
33.3
35
33.2
32
Mercury
57
0.0901
0.102
0.0842
0.0929
0
Molybdenum
75
1.6
0.889
0.946
0.996
1
Nickel
420
24.5
24.6
26
24.6
25
Selenium
100
1.13
1.11
1.15
1.08
1
Zinc
7,500
115
120
128
122
121
Total Phosphorus
NA
1760
2060
2190
1880
1973
TKN
NA
2720
2530
3140
2630
2755
Ammonia -Nitrogen
NA
392
478
442
490
451
Nitrate and Nitrite
NA
16.6
1 16.6
28.5
18
20
'For surface disposal facilities the cciling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
. a
Signature of
-a-aoa I
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0031314 Laboratory:
Facility Name: Winston Salem/Forsyth County Utilities Commission
Residual Source NCO086011
NPDES # or WQ#:
WWTP Name: Neilson Water Treatment Plant
Residual Analysis Data
1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
4/22/20
# 1
4/22/20
42
4/22/20
43
4/22/20
#4
Spring
Average
Aluminum
108000
116000
118000
112000
113500
Calcium
820
716
763
787
771.5
Magnesium
2220
2540
2840
2440
2510
PH
5.8
5.6
5.5
5.5
5.6
Potassium
2160
2280
2460
2170
2267.5
Sodium
45.9
70.9
70.9
77.4
66.275
PAN
1144
1076
1329
1119
1167
SAR
0.1
0.15
0.14
0.17
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4a- ada�
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

Section 2
• DEQ Form MFLSF -Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston Salem - Neilson WTP Total Dvy Tons Applied (Annual): 338.80
WQ0031314 Cation Exchange Capacity (non 503 only): 0
Roger Spillman Owner: Roger Spillman Predominant Soil Series: MrB2
27 Acres Permitted: 27 Site #: DV8 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
1 !
Com-
posite
Date
ro
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
DT/Ac./
0
App•
Event
12.55
Arsenic
0.18I
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.181
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.232
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.232
Chromium
1.511
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.511
Lead
0.811
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.811
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
denum
Nickel
0.625
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.625
Selenium
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Zinc
3.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.044
Total
Phos-
49.502
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
49.502
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
'e. e G" 1/29/2021
Signature of Land AppIier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Winston Salem -Neilson WTP
Land Owner:
Operator:
Roger Spillman
WQ Permit #: WQ0031314 Field #: 9 Acres Utilized:
Annual Dry Tons Applied: 338.80 Site #: DV8 Acres Permitted:
Roger Spillman Predominant Soil Series: MrB2
Crop l Name: Teff-Hay
Crop 1 Max. PAN: 198 Crop 2 Name
Cation Exchange Capacity (non 503):
Rye Grass Crop 2 Max. PAN:
27
27
50
o
�- o
ca
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES 9, WQ#,
Fert., Animal
aste, etc)
Soil
Cond.
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
a
� ?
_
- n'
c
C
„. 3
o
w
c, �-
N'
jF �:
°
-
_�
* N •
iF a.
3'
TKN
mglkg
z
a 9
'0 3
_
.. �.
mglkg
Nitrate
and
Nitrite
mglkg
PAN Applied
pp
Lbs/acre
{ )
Name of Crop Type
ReceivingResidua]
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/13/20
405
1 29.8
3.765
Neilson WTP
Dry
<.5"
S
0.5 1
0.4
2755 1
450.5
19.9
9.796
NA
Teff
5/14/20
630
29.8
5.856
Neilson WTP
Dry
<.5"
S
0.5
0.4
2755
450.5
19.9
13.667
NA
Teff
5/15/201
315
29.8
2.928
Neilson WTP
Dry
<.5"
S
0.5
0.4
2755
450.5
19.9
6.834
NA
Teff
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
13501
0
As
Cd
Cu
Cr
Pb
H.g
Mo
Ni
Se
Zn
P
29.287
0.000
Lime Applied
Annuallbs/acre
0.181
0.008
1.232
1.511
0.811
0.003
0.028
0.625
0.028
3.044
49.502
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.181
0.008
1.232
1.511
0.811
0.003
0.028
0.625
0,028
3.044
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit Istl2nd Crop
1 198 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/29/2021 **Volatilization Rate: Surface - 0.5, Injectionfincorporation - 1.0
Signature of Land Applier Date I` Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and
chain of custody's)
r Copies of our SAR/PAN calculations

Waypointo
ANALYTICAL
5f6f2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-114-0113
Client Project Description: Winston - Salem
Neilson WTP
Clemmons, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/23/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method, Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 15

Waypointo
ANALYTICAL
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZO816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
2/18/2023
Georgia
State Program
04015
6130/2020
Illinois
State Program - NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program - NELAP
04015
6130/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program - NELAP
68-03195
5/31/2020
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2111/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program - NELAP
T104704180
9/30/2020
Virginia
State Program
00106
6/30/2020
Virginia
State Program - NELAP
460181
9114/2020
Washington
State Program
C1018
7131/2020
Page 1 of 1 00001/20414-0113
Page 2 of 15

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 ° Fax 901.213,2440
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-114-0113
Client Project Description: Winston - Salem
Neilson WTP
Clemmons, NC
Lab No Client Sample ID Matrix Date Collected Date Received
89496
Neilson WTP
#1
Solids
04/22/2020 08:15
04/23/202-0
89497
Neilson WTP
#2
Solids
04/22/2020 08:30
04/23/2020
89498
Neilson WTP
#3
Solids
04/22/2020 08:45
04/23/2020
89499
Neilson WTP
#4
Solids
04/22/2020 09:00
04/23/2020
Page 3 of 15

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Winston - Salem
Lab Report Number: 20-114-0113
Late: 5/5/2020
2790 Whitten Road, Memphis, TN 38133
Main 901,223,2400 ° Fax [phone]
www.waypointanalytica1.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 91934
Analyte: Aluminum
QC Batch No: L489415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Calcium
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Cadmium
QC Batch No: L489193
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Chromium
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Copper
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Iron
QC Batch No: L489415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L489415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L489415
Page 4 of 15

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L489193
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Selenium
QC Batch No: L489193
This analyte was analyzed at a dilution due to IEC interferencelmatrix interference.
Analyte: Zinc
QC Batch No: L489193
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 89496 (Neilson WTP #1)
Analyte: Aluminum
QC Batch No: L489071/L488688
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L489071/L488688
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L489071/L488688
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 15

s
Waypoint 2i90 Whitten Road, Memphis, TN 3$133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
FMA Resources Inc
Mr. Brent Collins Project Winston - Salem Report Date : 05/06/2020
755 Yadkinvilie Rd Information : Neilson WTP Received : 04/23/2020
Mocksville , NC 27028 Clemmons, NC
Danyale Love
Report Number : 20-114-0113 REPORT OFANALYSIS Project Manager
Lab No : 89496
Matrix: Solids
Sample ID : Neilson WTP #1
Sampled:
4/22/2020
8:15
Test
Results
Units
MDL
MQL
DF
Date lTime
By
Analytical
Analyzed
Method
Moisture
71.7
070
1
04/27/2015:31
JDT
SW-DRYWT
Ammonia Nitrogen
392
mg/Kg - dry
88.3
1
05/04/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<16.6
mg/Kg - dry
16,6
16.6
1
04/30/20 14:42
ZBD
4500NO3F-2011
Organic N
2332
mg/Kg - dry
299.3
1
05/04/20 14:00
DH
CALCULATION -
pH
5.8
S.U.
1
05/04/20 05:30
JSL
9045D
Total Solids
28.4
%
0.010
0.010
1
04/24/20 10:14
CJR
2544G-2011
Total Volatile Solids
21.7
%
0.010
0.010
1
04/24/20 10:14
CJR
254OG-2011
Total Kjeldahl Nitrogen
2720
mg/Kg - dry
299
1
05/05/20 15:55
CLP 4500NORGD-2011
Phosphorus
1760
mg/Kg - dry
9.75
17.7
1
04/27/20 18:47
BKN
6010D
Aluminum
108000
mg/Kg - dry
81.6
88.3
5
04/28/20 12:48
TJS
6010D
Arsenic
6.22
mg/Kg - dry
0.848
1.77
1
04/27/20 18:47
BKN
6010D
Cadmium
0.327J
mg/Kg - dry
0.0706
0.353
1
04/27/20 18:47
BKN
6010D
Calcium
820
mg/Kg - dry
137
177
1
04/27/20 18:47
BKN
6010D
Chromium
59.4
mg/Kg - dry
0.833
0,883
1
04/27/20 18:47
BKN
6010D
Copper
47.7
mg/Kg - dry
1.10
1.77
1
04/27/20 18:47
BKN
6010D
Iran
51600
mg/Kg - dry
151
177
5
04/28/20 12:48
TJS
6010D
Lead
27.8
mg/Kg - dry
0,636
1.06
1
04/27/20 18:47
BKN
6010D
Magnesium
2220
mg/Kg - dry
9.12
17.7
1
04/27/20 18:47
BKN
6010D
Manganese
343
mg/Kg - dry
1.15
1.77
1
04/27/20 18:47
BKN
6010D
Mercury
0.0901
mg/Kg - dry
0.0123
0.0558
1
04/27/20 15:09
DDB
7471A
Molybdenum
1.60
mg/Kg - dry
0,477
0.883
1
04/27/20 18:47
BKN
6010D
Nickel
24.5
mg/Kg - dry
0.424
0.883
1
04/27/20 18:47
BKN
6010D
Potassium
2160
mg/Kg - dry
109
177
5
04/28/20 12:48
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 6 of 15

Waypontoi
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number:20-114-0113
Lab No : 89496
Sample ID: Neilson WTP #1
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Winston - Salem
Information : Neilson WTP
Clemmons, NC
REPORT OFANAL YSIS
Report Date : 05/06/2020
Received
�nQ�: 04/23/2020
Q;�l�+c1Ki't� Q/- -`
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/22/2020 8:15
Test
Results
Units
MDL
MQL
DF
Date I Time
Analyzed
By
Analytical
Method
Selenium
<1.13
mg/Kg - dry
1.13
1.77
1
04/27/20 18:47
BKN
6010D
Sodium
<45.9
mg/Kg - dry
45,9
88.3
1
04/27/20 18:47
BKN
6010D
Zinc
115
mg/Kg - dry
2.86
4.42
1
04/27/20 18:47
BKN
6010D
Sulfur
2100
mg/Kg - dry
18.3
35.3
1
04/27/20 18:47
BKN
6010D
Sodium Absorption Ratio
0.10
Ratio
1
04/27/20 18:47
CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 7 of 15

0 Waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Winston - Salem Report Date : 05/06/2020
755 Yadkinville Rd Information : Neilson WTP Received : 04/23/2020
Mocksville , NC 27028 Clemmons, NC
00,
REPORTOFANALYSIS Danyale Love
Report Number : 20-114-D113 Project Manager
Lab No: 89497
Matrix: Solids
Sample ID : Neilson WTP #2
Sampled:
4/22/2020
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
71.1
%
1
04/27/2015:31
JDT
SW-DRYWT
Ammonia !Nitrogen
478
mg/Kg - dry
96.5
1
05/04/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<16.6
mg/Kg - dry
16.6
16.6
1
04/30/20 14:42
ZBD
450ONO3F-2011
Organic N
2048
mg/Kg - dry
306.9
1
05/04/20 14:00
DH
CALCULATION —
pH
5.6
s.u.
1
05/04/20 05:30
JSL
9045D
Total Solids
29.3
%
0.010
0.010
1
04/24/20 10:14
CJR
2540G-2011
Total Volatile Solids
22.4
%
0.010
0.010
1
04/24/20 10:14
CJR
2540G-ZO11
Total Kjeldahl Nitrogen
2530
mg/Kg - dry
307
1
05/05/20 15:56
CLP 4500NORGD-2011
Phosphorus
2060
mg/Kg - dry
9.55
17.3
1
04/28f20 20:43
KKM
60101)
Aluminum
116000
mg/Kg - dry
160
173
10
04/29/20 12:53
TJS
6010D
Arsenic
7.54
mg/Kg - dry
0.830
1.73
1
04/28/20 20:43
KKM
6010D
Cadmium
0.3343
mg/Kg - dry
0.0692
0.346
1
04/28/20 20:43
KKM
6010D
Calcium
716
mg/Kg - dry
134
173
1
04/28/20 20:43
KKM
6010D
Chromium
59.2
mg/Kg - dry
0.816
0.865
1
04/28/20 20:43
KKM
6010D
Copper
48.4
mg/Kg - dry
1.07
1.73
1
04/28/20 20:43
KKM
6010D
Iron
55000
mg/Kg - dry
295
346
10
04/29/20 12:53
TJS
6010D
Lead
33.3
mg/Kg - dry
0.622
1.04
1
04/28/20 20:43
KKM
6010D
Magnesium
2540
mg/Kg - dry
8.93
17.3
1
04/28/20 20:43
KKM
6010D
Manganese
433
mg/Kg - dry
1.12
1.73
1
04/28/20 20:43
TJS
6010D
Mercury
0.102
mg/Kg - dry
0.0116
0.0522
1
04/27/20 15:11
DDB
7471A
Molybdenum
0.889
mg/Kg - dry
0.461
0.865
1
04/28/20 20:43
KKM
60101)
Nickel
24.6
mg/Kg - dry
0.415
0.865
1
04/28/20 20:43
KKM
6010D
Potassium
2280
mg/Kg - dry
21.4
34.6
1
04/28/20 20:43
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation
Limit
Page 8 of 15

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-114-0113
Lab No : 89497
Sample ID: Neilson WTP #2
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Winston - Salem
Information : Neilson WTP
Clemmons, NC
REPORT OPANAL YSIS
Report Date ; 05/06/2020
Received ; 04/23/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/22/2020 8:30
Test
Results
Units
MDL
MQL
DF Date / Time
Analyzed
By
Analytical
Method
Selenium
<1.11
mg/Kg - dry
1.11
1.73
1 04/28/20 20:43
TJS
6010D
Sodium
70.93
mg/Kg - dry
45.0
86.5
1 04/28/20 20:43
KKM
6010D
Zinc
120
mg/Kg - dry
2.80
4.33
1 04/28/20 20:43
KKM
6010D
Sulfur
1940
mg/Kg - dry
17.9
34.6
1 04/28/20 20:43
KKM
60100
Sodium Absorption Ratio
0.15 J
Ratio
1 04/28/20 20:43
CALCULA-HON
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 9 of 15

0 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901,213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Winston - Salem Report Date : 05/06/2020
755 Yadkinville Rd Information : Neilson WTP Received ; 04/23/2020
Mocksv411e , NC 2702$ Clemmans, NC Q0,6&
REPORT Danyale Love
Report Number : 20-114-0113 Project Manager
Lab No ; 89498 Matrix: Solids
Sample ID : Neilson WTP #3 Sampled: 4/22/2020 8:45
Test Results Units MDt_ MOL DF Date / Time By Analytical
Analyzed Method
Moisture
72.2
%
1
04/27/2015:31
JDT
SW-DRYWT
Ammonia Nitrogen
442
mg/Kg -
dry
89.9
1
05/04/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
28.5
mg/Kg -
dry
17.2
17.2
1
04/30/20 14:43
ZBD
4500NO3F-2011
Organic N
2701
mg/Kg -
dry
236.0
1
05/04/20 14:00
DH
CALCULATION
pH
5.5
S.U.
1
05/04/20 05:30
JSL
9045D
Total Solids
28.7
%
0.010
0.010
1
04/24/20 10:14
CJR
2540G-2011
Total Volatile Solids
21.1
%
0.010
0.010
1
04/24/20 10:14
CJR
2540G-2011
Total Kjeldahl Nitrogen
3140
mg/Kg -
dry
236
1
05/05/20 15:57
CLP 4500NORGD-2011
Phosphorus
2190
mg/Kg -
dry
9.93
18.0
1
04/28/20 20:48
KKM
6010D
Aluminum
118000
mg/Kg -
dry
166
180
10
04/29/20 12:58
TJS
6010D
Arsenic
7.52
mg/Kg -
dry
0.863
1.80
1
04/28/20 20:48
KKM
6010D
Cadmium
0.3213
mg/Kg -
dry
0,0719
0.360
1
04/28/20 20:48
KKM
6010D
Calcium
763
mg/Kg -
dry
139
180
1
04/28/20 20:48
KKM
6010D
Chromium
61.5
mg/Kg -
dry
0,848
0.899
1
04/28/20 20:4B
KKM
6010D
Copper
51.4
mg/Kg -
dry
1.12
1.80
1
04/28/20 20:48
KKM
6010D
Iron
56800
mg/Kg -
dry
306
360
10
04/29/20 12:58
TJS
6010D
Lead
35.0
mg/Kg -
dry
0.647
1.08
1
04/28/20 20:49
KKM
6010D
Magnesium
2840
mg/Kg -
dry
9.28
18.0
1
04/28/20 20:48
KKM
6010D
Manganese
558
mg/Kg -
dry
1.17
1.80
1
04/28/20 20:48
TJS
6010D
Mercury
0.0842
mg/Kg -
dry
0.0107
0.0486
1
04/27/20 15:12
DDB
7471A
Molybdenum
0.946
mg/Kg -
dry
0.485
0.899
1
04/28/20 20:48
KKM
6010D
Nickel
26.0
mg/Kg -
dry
0.431
0.899
1
04/28/20 20:48
KKM
6010D
Potassium
2460
mg/Kg -
dry
22.2
36.0
1
04/28/20 20:48
TJS
6010D
Qualifiers/ DF
Dilution Factor
3
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 10 of 15

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical. corn
46245
EMA Resources Inc
Mr. Brent Collins
Project Winston - Salem
Report Date : 05/06/2020
755 Yadkinville Rd
Information : Neilson WTP
Received : 04/23/2020
Mocksville , NC 27028
Clemmons, NC
Danyale Love
Report Number: 20-114-0113
REFORTOFANALYSIS
Project Manager
Lab No : 89498
Matrix: Solids
Sample ID : Neilson UVTP #3
Sampled: 4/22/2020 8:45
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<1.15
mg/Kg -
dry
1.15
1.80
1
04/28/20 20:48
T]S
6010D
Sodium
70.91
mg/Kg -
dry
46.8
89.9
1
04/28/20 20:48
KKM
6010D
Zinc
128
mg/Kg -
dry
2.91
4.50
1
04/28/20 20:48
KKM
6010D
Sulfur
2130
mg/Kg -
dry
18.6
36.0
1
04/28/20 20:48
KKM
6010D
Sodium Absorption Ratio
0.14 ]
Ratio
1
04/28/20 20:48
CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 11 of 15

0
Waypoint, Z790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Winston - Salem Report Date : 05/06/2020
755 Yadkinville Rd Information : Neilson WTP Received : 04/23/2020
Mocksville , NC 27028 Clemmons, NC
❑anyale Love
Report Number: 20-114-0113 REPORT OPANALYSIS Project Manager
Lab No : 89499 Matrix: Solids
Sample ID : Neilson WTP #4 Sampled: 4/22/2020 9:00
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
70.4
%
1
04/27/2016:50
JDT
SW-DRYWT
Ammonia Nitrogen
490
mg/Kg - dry
84.5
1
05/04/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
18.0
mg/Kg - dry
16.3
16.3
1
04/30/20 14:44
ZED
4500NO3F-2011
Organic N
2142
mg/Kg - dry
337.8
1
05/04/20 14:00
DH
CALCULATION -
pH
5.5
S.U.
1
05/04/20 05:30
JSL
9045D
Total Solids
32.7
%
0.010
0.010
1
04/24/20 10:14
CJR
254OG-2011
Total Volatile Solids
17.8
%
0.010
0.010
1
04/24/20 10:14
CJR
254OG-2011
Total Kjeldahl Nitrogen
2630
mg/Kg - dry
338
1
05/05/20 15:58
CLP
4500NORGD-2011
Phosphorus
1880
mg/Kg - dry
9.32
16.9
1
04/28/20 21:04
KKM
6010D
Aluminum
112000
mg/Kg - dry
156
169
10
04/29/20 13:03
TJS
6010D
Arsenic
7.67
mg/Kg - dry
0.811
1.69
1
04/28/20 21:04
KKM
60101)
Cadmium
0.3003
mg/Kg - dry
0.0675
0.338
1
04/28/20 21:04
KKM
6010D
Calcium
787
mg/Kg - dry
131
169
1
04/28/20 21:04
KKM
6010D
Chromium
60.5
mg/Kg - dry
0.797
0.844
1
04/28/20 21:04
KKM
6010D
Copper
49.0
mg/Kg - dry
1.05
1.69
1
04/28/20 21:04
KKM
6010D
Iron
54700
mg/Kg - dry
288
338
10
04/29/20 13:03
TJS
6010D
Lead
33.2
mg/Kg - dry
0.608
1.01
1
04/28/20 21:04
KKM
60101)
Magnesium
2440
mg/Kg - dry
8.72
16.9
1
04/28/20 21:04
KKM
6010D
Manganese
402
mg/Kg - dry
1.10
1.69
1
04/28/20 21:04
TJS
6010D
Mercury
0.0929
mg/Kg - dry
0.00996
0.0453
1
04/27/20 11:43
DDB
7471A
Molybdenum
0.996
mg/Kg - dry
0.456
0.844
1
04/28/20 21:04
KKM
6010D
Nickel
24.6
mg/Kg - dry
0.405
0.844
1
04/28/20 21:04
KKM
6010D
Potassium
2170
mg/Kg - dry
20.9
33.8
1
04/28/20 21:04
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation
Limit
Page 12 of 15

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadldnville Rd
Mocksville , NC 27028
Report Number : 20-114-0113
Lab No : 89499
Sample ID : Neilson WTP #4
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 1 fax [phone]
www.waypointanalyticaLcom
Project Winston - Salem
Information : Neilson WTP
Ciemmons, NC
REPORT OFANAL YSIS
Report Date : 05/06/2020
Received, �}0,4/23/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/22/2020 9:00
Test
Results
Units
MDL
MQL
DF
Date 1 Time
Analyzed
sy
Analytical
Method
Selenium
<1.08
mg/Kg - dry
1.08
1.69
1
04/28/20 21:04
T]S
6010D
Sodium
77.43
mg/Kg - dry
43.9
84.5
1
04/28/20 21:04
KKM
6010D
Zinc
122
mg/Kg - dry
2.74
4.22
1
04/28/20 21:04
KKM
6010D
Sulfur
2010
mg/Kg - dry
17.5
33.8
1
04/28/20 21:04
KKM
6010D
Sodium Absorption Ratio
0.173
Ratio
1
04/28/20 21:04
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 13 of 15

•
Waypoi nt(2) Z790 Whitten Road,3.240 Memphis, TN .2W
Main 901.213.24D0 °Fax 901.213.244d
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-114-0113
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F_ 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
9 Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
40 Yos
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
10 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
9 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) j Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes I& No
Signature: Kristina A. McAdams Date & Time: 4/23/2020 14:20:30
Page 14 of 15

Client Name/Address
Client Project Manager/€onuct
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755"Yadkinvllle Rd
Mocksville, NC 27028
ProjectOescription
Prnject/siteLocation (city/State)
RUSH —Additional charges apply
MethodofShi meat
Matrix Key
1 t 3�
J f -q C .�-4 p"L
%C�� 5 O r. / ��
fy i�Y
Special Detection Umii(s)
Date Results Needed
[D Fed tic UPS ElU5P5
Courier Client Drop Off
WW —Wastewater G4td Groundwater
DW � Drinking Water S — Soil /Solid
EI.J 1�J
0 -- Olt
0Lry��?r�sij5
P- Product M -Misc
/L
Other
Project Number
Project Manager Phone-#
Project Manager Email
Purchase Order Number
Site/t acinty ID #
336-399-36 6
[e-mail]
(di
A Coat c =C Na7.5�03 (Micro Only)
g m
at.
O
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cool K= BC
C H2504 pW2
ANALYTICAL
a
E
�
mifr
co
n None Required
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2790 'Whitten Road
c
a
Memphis. TM 38133
Unless noted, all ContalnErsca
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> �`)
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[phone]
per Table tl of 40 CFR Part
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136.
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Date
Time
Sample Identification
REguired
Analysis / Preservative
Comments/Notes
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✓
✓
Metals:Ai,AS,C8,Cd,Cr,Cu,Fe,Pb
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EMA Resouvices Inc
Winston - salem
020
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Client Remarks/Comments
Sludge Samples -
Report.Dry Weight
Ice
custody
LabCorirments
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Date Time
-
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Date Time Rer elved by- ISIGNATURE)
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Section 4
• Maps of the residuals disposal sites

'�O
Es

Section 5
a Field soil sampling results

Page 1 of 1
Report No: 21-055-0587
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypo'10 t
ANALYTICAL
Client: Roger Spillman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: DVO8
Date Received: 02/24/2021
Date of Report: 02/25/2021
Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
103170 09 09 MIN 7.0 0.0 27 23 15 1225 0 0 498 498 110 21.3 100 60 39 0.3 0.1 I
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.