WQ0038580_Renewal Application_20210303 (2)

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0038580
Applicant/Permittee Town of Hillsborough
Applicant/Permittee Address PO Box429, Hillsborough, NC 27278
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Municipal
Facility Name Town of Hillsborough DCAR
County Orange
Fee Category Minor
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $0
Complete App Date 03/03/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Kendall
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3367511441
O Modification - Minor
G Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00038580
Fbs Current Existing permt number
Applicant/Permittee * Town of Hillsborough
Applicant/Permittee Address* PO Box429, Hillsborough, NC 27278
Facility Name * Town of Hillsborough DCAR
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spec'rfications, Calculations, Rc.)
Town of Hillsborough Permit Renewal - WQ0038580.pdf 9.3MB
Upload only 1 RCFdocurrent (less than 250 NS). NL@iple documents nest be corrbined into one RDFfile unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date
ff &Oaw
3/3/2021

March 2, 2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Renewal — WQ0038580
To Whom it May Concern:
EMA Resources is submitting the included permit renewal for the Town of Hillsborough,
WTP — DCAR Permit WQ0038580. The only changes are the Permiee and the plant
contact information.
If you have any questions concerning this modification, please contact Brent Collins —
Director of Technical Services
Respectfully,
Brent Collins
Director of Technical Services
brent.collins&emaresourcesinc.com
[phone]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

g
Inc.
Permit Modification
For
The Town of Hillsborough WTP -
WQ0038580
Distribution of Residual Solids
(503 Exempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
March 2, 2021
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

Current Permit

Water Resources
ENVIRONMENTAL QUALITY
PAT MCCRORY
6'o L'L'I nO?
DONALD R. VAN DER VAART
Secretary
S. JAY ZIMMERMAN
Director
August 19, 2016
KENNETH KEEL, PE — UTILITIES DIRECTOR
TOWN OF HILLSBOROUGH
POST OFFICE BOX 429
HILLSBOROUGH, NORTH CAROLINA 27278
Deat Mr. Keel:
Subject: Permit No. WQ0038580
City of Hillsborough Class A
Distribution Program
Distribution of Class A Water
Treatment Plant Residuals
Orange County
In accordance with your permit request received June 29, 2016, and subsequent additional
information received August 15, 2016, we are forwarding herewith Permit No. WQ0038580 dated August
19, 2016, to the Town of Hillsborough for the operation of the subject residuals management program.
This permit shall be effective from the date of issuance until July 31, 2021, and shall be subject to
the conditions and limitations as specified therein. Please pay particular attention to the monitoring
requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining
the required operational information shall result in future compliance problems.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and fled with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919) 807-
6336 or troy.dobykncdenr.gov.
Sincerely,
r
S. Jay Zimmerman, P.G., Directo
Division of Water Resources
cc: Orange County Health Department (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Roy Whitaker — EMA Resources (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919 807 6464

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Town of Hillsborough
Orange County
FOR THE
operation of a residuals management program for the Town of Hillsborough and consisting of the
distribution of Class A Water Treatment Plant residuals generated by the approved facility listed in
Attachment A with no discharge of wastes to surface waters, pursuant to the application received June 29,
2016, and subsequent additional information received by the Division of Water Resources, and in
conformity with other supporting data subsequently filed and approved by the Department of
Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated
under Title 40 Code of federal Regulations Part 257. This permit does not exempt the Permittee from
complying with the federal regulations.
This permit shall be effective from the date of issuance until July 31, 2021, and shall be subject to the
following specified conditions and limitations:
I. SCHEDULES
No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15ANCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109]
H. PERFORMANCE STANDARDS
The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Raleigh Regional Office supervisor, and take any immediate
corrective actions. [G.S. 143-215.1]
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2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L .0100]
3. Only residuals generated by the facilities listed in Attachment A are approved for distribution in
accordance with this permit. [G.S. 143-215.11
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T. 1105]
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [ 15A NCAC
02T .1106]
6. Setbacks for treatment and storage facilities shall be as follows:
Setback Description
Setback
feet
Habitable residence or place of public assembly under separate ownership or not to
be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams — intermittent and perennial, perennial waterbodies, and
wetlands
50
Wells with exception to monitoring wells
100
[15A NCAC 02T. 1108]
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7. Setbacks for Class A land applied bulk residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid
Cake 1
Private or public water supply
100
100
Surface waters (streams— intermittent and perennial,
100
25
perennial waterbodies, and wetlands
Surface water diversions (ephemeral streams,
25
0
waterwa s, ditches
Groundwater lowering ditches (where the bottom of
25
0
the ditch intersects the SHWT
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
1 Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, stinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[15A NCAC 02T .1108]
8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (hM://nutrients.soil.nesu.edu/,yields/indgxph�). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(bgp://www.ncagr.izov/SWC/tech/documents/9th Guidance_ Doc_100109.pd fl.
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftt)://ftp-fe.se.epov.usda.mov/NHO/practice-standards/standards/590.ndf}.
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[I5A NCAC 02T .I 109(b)(1)(k)]
WQ0038580 Version 1.0 Shell Version 160210 Page 3 of 11

The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium
adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may
seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high
SAR content; has agreed on proper residual application rates; and has agreed to operational
considerations to ensure that the high SAR content will not adversely impact the receiving sites.
Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a
mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained
from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services,
the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist.
[I5A NCAC 02T .0108(b)(1)]
OPERATION AND MAINTENANCE REQUIREMENTS
The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [15A NCAC 02T .1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and Iocation of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but
have an annual sampling frequency, may need to sample during winter months when pathogen
reduction is most likely to be negatively affected by cold temperatures).
[ 15A NCAC 02T .11001
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Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at [phone]. [15A NCAC 02T .0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110]
6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied Iiquid residuals, or if the slope is greater than
I S% for injected or incorporated bulk liquid residuals;
h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the
pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations
to the acceptable soil pH (6.0) will be noted in this permit;
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
WQ0038580 Version 1.0 Shell Version 160210 Page 5 of 11

1. Application exceeds agronomic rates.
[ 15A NCAC 02T. 1109]
9. A dated Utilization Agreement between the Permittee, his subcontractor distributing and applying the
residuals, and the entity agreeing to accept Class A bulk residuals shall be in place prior to distribution
of the bulk residuals. The agreement shall specify the subcontractors and the agreeing entity's
responsibilities. The Permittee, the subcontractor, and the entity accepting the Class A bulk residuals
shall sign the Utilization Agreement. The Utilization Agreement shall have a clause allowing the
recipient of the residuals to end the Utilization Agreement at any time by notifying the Permittee in
writing. If the recipient of the residuals sells the property, the Utilization Agreement shall automatically
terminate. If the permit is rescinded, the Utilization Agreement shall automatically terminate. The
duration of the Utilization Agreement shall be one to which the Permittee, the subcontractor, and the
recipient of the residuals agree. Any changes in the agreement that are necessitated by changes in the
permit shall be mailed to the subcontractor and the recipient of the residuals by certified mail with
return receipt. The Permittee shall keep these records on file for inspection by the Division for each
Utilization Agreement while that Utilization Agreement is in force. [15A NCAC 02T .0108(b)(1), 02T
.1104]
10. At a minimum, the Utilization Agreement shall stipulate the following:
a. By agreeing to accept the bulk Class A residuals, it is recognized that the application of these
residuals is allowed under the conditions. of this agreement including the prohibitions contained in
Condition II1.8. Land application of Class A residuals is considered the beneficial reuse of a waste
under 15A NCAC 02T .1100, and has been deemed permitted under 15A NCAC 02T .1103(4)
provided the conditions of this agreement are met. Any action resulting in damages to surface water
or groundwater, caused by failure to follow the conditions of this agreement, is subject to Division
enforcement action;
b. The person or entity accepting the bulk Class A residuals shall to the best of his knowledge meet
the following application requirements:
Class A Water Treatment Plant Residuals shall not be stockpiled for more than 60 days (after
the delivery of the last load) prior to land application unless the permittee notifies the Raleigh
Regional Office and receives approval to exceed the 60-day limit. At a minimum, the
information provided shall be the location, the date that the last load was delivered, the quantity
of residuals stockpiled, the percent solids of the residuals stockpiled, measures taken to prevent
stockpile runoff (e.g. placement, perimeter berms, etc.) and the anticipated date the residuals
will be spread.;
ii. Application of bulk residuals shall not occur within 100 feet of a public or private water supply
source;
iii. Application of bulk residuals shall not occur within 100 feet of any well, with the exception of
Division approved monitoring wells;
iv. Application of bulk residuals shall not occur within 25 feet of surface waters.
c. The generator of the Class A bulk residuals shall provide information on the proper use of the
residuals, including information on the nutrient quantities within the residuals and recommended
application rates. A copy of the label or information sheet attached to bags or other containers, as
specified in the labeling requirements under Condition III.12, is sufficient;
d. The applicator or party accepting bulk residuals from the Permittee shall supply all third parties
receiving bulk residuals with documentation specifying that application shall occur consistent with
the utilization agreement;
e. Instructions, including contact information for key personnel, shall be provided to the applicator or
party receiving bulk residuals in the event that any requirements specified in the utilization
agreement are not met.
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f. A copy of the Utilization Agreement shall be maintained at the land application sites when bulk
residuals are being applied.
[15A NCAC 02T .0108(b)(1), 02T .1104]
11. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to the
buyer. If an alternate storage site is used, approval must be obtained from the Division. [ 15A NCAC
02T .0108(b)(1)]
12. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[15A NCAC 02T. I 109(a)]
13. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the condition of the signed Utilization Agreement. The Permittee shall report to the Raleigh
Regional Office as per reporting conditions under Condition IV.8 any person or entity known to be
applying residuals contrary to the condition of the signed Utilization Agreement. [15A NCAC 02T
.1103(a)]
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IV. MONITORING AND REPORTING REQUIREMENTS
1. Any Division -required monitoring. (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide)
0.008)
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichlorocthylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1,0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[I5A NCAC 13A .0102(b), 02T .1101, 02T .l 1051
WQ0038580 Version 1.0 Shell Version 160210 Page 8 of 11.

3. An analysis shall be conducted on the Class A residuals at the frequency specified in Attachment A,
and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the
following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[I5A NCAC 02T. 11011]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan. The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (b)(2). Any exceptions from the requirements in this condition shall be specified in
Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)]
5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [ 15A NCAC 02B .0505]
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee. At a minimum, these records shall include the following:
a. Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals;
d. Volume of residuals distributed to each recipient;
e. Intended use of residuals;
f. If land application events performed by the Permittee - Nitrogen Application Rate based on RYES
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years),
[I5A NCAC 02T .0109(a)]
7. Three copies of an annual report shall be submitted on or before March V. The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting_Forms.
Instructions for reporting and annual report forms are available at
http://portal.nedenr.orgLweb/wq/aps/lau/rel2orting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[I5A NCAC 02T .1111(a)]
WQ0038580 Version 1.0 Shell Version 160210 Page 9 of 11

8. Noncompliance Notification
The Permittee shall report by telephone to the Raleigh Regional Office, telephone number (919) 791-
4200, as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following;
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)]
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [ 15A NCAC 02T .0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator
errors that could result in discharges to the environment, a threat to human health or a public nuisance.
The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of
inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee
shall maintain this inspection log for a period of five years from the date of inspection, and this log
shall be made available to the Division upon request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the distribution facilities permitted herein at any
reasonable time for the purpose of determining compliance with this permit; may inspect or copy any
records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
Vl. GENERAL CONDITIONS
1. failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.1]
WQ0038580 Version 1.0 Shell Version 160210 Page 10 of 11

4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [ 15A NCAC 02T .0105(c)(6)]
In the event the residuals program changes ownership or the Permittec changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b).
[15A NCAC 02T .0120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
A105(e)(3)]
Permit issued this the 19t' day of August 2016
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
?S. Jay Zimmerman, P.G., Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0038580
WQ0038580 Version 1.0 Shell Version 160210 Page 11 of 11

ATTACHMENT A - Approved Residual Sources
Town of Hillsborough
Certification Date: August 19, 2016
Permit Number: WQ0038580 Version: 1.0
Owner
Facility Name
County
Permit
Biological
Maximum
D Tons
Monitoring
Frequency for
Monitoring
Frequency for
Monitoring
Frequency for
Approved
Number
Residuals
Per Year 1
Non -hazardous
Metals and
Pathogen &
Mineralization
Characteristics 2
Nutrients 3,5
Vector Attraction
Rate
Reductions 4, 3, 6
Town of Hillsborough
Town of Hillsborough WTP
Orange
PWS 0368015
No
750
Annually
See Table Below
See Table .Below
Total
750
L Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3_ Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen reductions as stipulated under permit Condition IVA.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Distributed
short tons per ear
Monitoring Frequency
Established in 40 CFR 503 and 15A NCAC 02T .11I1
<319
1/Year
=>319 - <1,650
1/ Quarter 4 times per ear.
=>1,650 - <16,500
1/60 Days 6 times per ear
=>16,500
1/month 12 times per ear
6. Class A Water Treatment Plant residuals are exempt from meeting the vector attraction reduction requirements in Condition IVA, provided they are not mixed with residuals that have been
generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Class A Water Treatment Plant
residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in 15A NCAC 02T .1102(6).
If no distribution events occur during a required sampling period (e.g. no distribution occurs during an entire year when annual monitoring is required), then no sampling
data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to
EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0038580 Version 1.0 Attachment A Page 1 of 1

DCAR Form

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
L APPLICANT INFORMATION:
1. Applicant's name: Town of Hillsborough, NC
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership E:1 Privately -Owned Public Utility
❑ Federal ❑ State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: K. Marie Strandwitz, PE Title: Utilities Director
Applicant's mailing address: PO Box 429
City: Hillsborough State: NC Zip: 27278-0429
Telephone number: [phone] Email Address: marie.strandwitzkWllsboroughnc.gov
2. Consultant's name: Brent Collins License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: EMA Resources Inc.)
Consultant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] Email Address: brent.collinsA_emaresourcesinc.com
3. Fee submitted: $0 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00038580
Date of most -recently issued permit: 08/19/16
Date of most -recently certified Attachment A (if different than the permit): 08/19/16
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Town of Hillsborough Water Treatment Plant
City: Hillsborough State: NC Zip: 27278-0429
Coordinates: Latitude: 36' 04' 03" Longitude: 79. 07' 28"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
County where facility is located: Orange
2. Facility contact (person familiar with residuals preparation):
Name: Nathan Cates Title: Interim WTP Superintendent
Mailing address: PO Box 429
City: Hillsborough State: NC Zip: 27278-
Telephone number: (!�19) 732-3621 E-mail address: Nathan.cateskhillsboroughnc.gov
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; p No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 365-730 days (Note: the Division requires minimum 30 days storage in units that are
separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); land applied at agronomic rates
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 750 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 750 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): The WTP residuals are wasted into one of two 1.5 MG lagoons. The solids settle
and the decant is pumped to the Town's sewer system. There are two additional drying lagoons that thickened residuals can be
pumped to drying via underdrains and solar evaporation. The combination of the four lagoons provide 1-2 years of storage.
6. Does the facility have a stormwater management plan? ® Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Decant is sent to the
Town's sewer s, s
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
EN
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes n No, Explain;
I, Marie Strandwitz — Utilities Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for
The Town of Hillsborough
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
st�
Signature:
Date: Mar 3, 2021
FORM: DCAR 06-16 Page 3 of 3

RSC Form

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Town of Hillsborough, NC
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
R
Town of Hillsborough, NC
Town of Hillsborough WTP
Orange
PWS: 0368015
750
750
'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Town of Hillsborough Water Treatment Plata
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: f=).
3. Facility contact person and title: Nathan Cates — Interim WTP Superintendent
Complete mailing address: PO Box 429
City: Hillsborough State: NC Zip: 27278-0429
Telephone number: [phone] E-mail address: nathan.cateskWIlsboroughnc.gov
4. Facility physical address: 711 Dimmock's Mill Rd
City: Hillsborough State: NC Zip: 27278-
Coordinates: Latitude: 36' 04' 03" Longitude: 79. 07' 28"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 3.0 MGD and facility average daily flow: 1_4 MGD
8. Average amount of residuals being generated at this facility 750 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: NA
Type and volume of residuals storage (i.e., outside of residuals treatment units): Two 1.5 MG earthen lagoons
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 8/15/19
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes W no. Flashpoint: >170 OF (> 140°F)
Passed reactivity test: W yes Ono. HCN: <0.25 mg/kg (<250) & H2S: <25 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
<0.1
Hexachlorobenzene
0.13
<0.1
Barium
100.0
<0.1
Hexachloro-1,3-Butadiene
0.5
<0.1
Benzene
0.5
<0.05
Hexachloroethane
3.0
<0.1
Cadmium
1.0
<0.1
Lead
5.0
<0.1
Carbon Tetrachloride
0.5
<0.05
Lindane
0.4
<0.005
Chlordane
0.03
<0.005
Mercury
0.2
<0.01
Chlorobenzene
100.0
<0.05
Methoxychlor
10.0
<0.005
Chloroform
6.0
<0.25
Methyl Ethyl Ketone
200.0
<0.5
Chromium
5.0
<0.1
Nitrobenzene
2.0
<0.1
m-Cresol
200.0
<0.1
Pentachlorophenol
100.0
<0.1
o-Cresol
200.0
<0.1
Pyridine
5.0
<0.1
p-Cresol
200.0
<0.1
Selenium
1.0
<0.1
Cresol
200.0
<0.1
Silver
5.0
<0.1
2,4-D
10.0
<0.002
Tetrachloroethylene
0.7
<0.05
1,4-Dichlorobenzene
7.5
<0.1
Toxaphene
0.5
<0.01
1,2-Dichloroethane
0.5
<0.05
Trichloroethylene
0.5
<0.05
1,1-Dichloroethylene
0.7
<0.05
214,5-Trichlorophenol
400.0
<0.1
2,4-Dinitrotoluene
0.13
<0.1
2,4,6-Trichlorophenol
2.0
<0.1
Endrin
0.02
<0.005
2,4,5-TP (Silvex)
1.0
<0.002
Heptachlor and its Hydroxide
0.008
<0.005
Vinyl Chloride
0.2
<0.05
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 08/15/19
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
15.8
Cadmium
85
39
<1.83
Copper
4,300
1,500
64.1
Lead
840
300
14.2
Mercury
57
17
<0.118
Molybdenum
75
n/a
<4.81
Nickel
420
420
16.5
Selenium
100
100
<18.1
Zinc
7,500
2,800
143
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.69 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 8/15/19
Parameter
Result
(mg/kg)
Aluminum
197000
Ammonia -Nitrogen
7630
Calcium
2090
Magnesium
1730
Nitrate -Nitrite Nitrogen
<185
pH (Standard Unit)
6.2
Phosphorus
1920
Potassium
930
Sodium
596
Total Kjeldahl Nitrogen
7330
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.38
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
3880
3810
Injection/Incorporation
7695
7625
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, 9 air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of

Vicinity Map

. ,A
A7
�' • l
Property Boundary

Process Flow

u i.QQ.
Z� oil
F
pp5�I ' 8
033J 30
8 msl aQ
033J IlWdSONd ,. 033J 7LLSfKJ 150d
a=�
�uF
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YYo
El
0
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a 5C
W
ILI
C= UUS(OrJ 30N 033J ]0SM MW

Quantitative Justification

Quantitative Justification for Residuals Production Rate.
The Town of Hillsborough WTP currently thickens the residuals two 1.5MG lagoons. The WTP
has two additional dewatering lagoons for obtaining a cake product when weather conditions
allow.
Annual Gallons * lbs./Gallon * % Solids - lbs/ton = Annual Dry Tons
3,000,000 8.34 * 6% — 2,000 = 750

Analytical Information

Waypointo
ANALYTICAL
8/29/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-228-0032
Client Project Description: Hillsborough
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/16/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Hillsborough
Lab Report Number: 19-228-0032
Date: 8/27/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 2 of 6

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Hillsborough Report Date : 08/29/2019
755 Yadkinville Road Information : Received : 08/16/2019
Mocksville , NC 27028
Report Number : 19-228-0032 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 93637
Matrix: Solids
Sample ID : Hillsborough
Sampled:
8/15/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
97.3
%
0.010
1
08/16/19 16:20
ADM
SW-DRYWT
Ammonia Nitrogen
7630
mg/Kg -
dry
926
1
08/27/19 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<185
mg/Kg -
dry
185
185
1
08/27/19 12:36
ZBD
4500NO3F-2011
Organic N
<1910
mg/Kg -
dry
1910
1
ACA
CALCULATION
pH
6.2
S.U.
1
08/22/19 07:40
JSL
9045D
Total Solids
2.69
%
0.010
0.010
1
08/16/19 16:20
ADM
2540G-2011
Total Volatile Solids
32.5
%
0.010
0.010
1
08/16/19 16:20
ADM
2540G-2011
Total Kjeldahl Nitrogen
7330
mg/Kg -
dry
1910
1
08/26/19 15:30
CLP 4500NORGD-2011
Phosphorus
1920
mg/Kg -
dry
95.2
185
1
08/22/19 20:35
BKN
6010D
Aluminum
197000
mg/Kg -
dry
75.2
185
1
08/22/19 20:35
BKN
6010D
Arsenic
15.83
mg/Kg -
dry
15.5
18.5
1
08/22/19 20:35
BKN
6010D
Cadmium
<1.83
mg/Kg -
dry
1.83
3.70
1
08/22/19 20:35
BKN
6010D
Calcium
2090
mg/Kg -
dry
622
926
1
08/23/19 20:10
BKN
6010D
Chromium
33.1
mg/Kg -
dry
7.04
9.26
1
08/22/19 20:35
BKN
6010D
Copper
64.1
mg/Kg -
dry
5.37
9.26
1
08/22/19 20:35
BKN
6010D
Iron
61100
mg/Kg -
dry
157
185
1
08/22/19 20:35
BKN
6010D
Lead
14.2
mg/Kg -
dry
5.52
11.1
1
08/22/19 20:35
BKN
6010D
Magnesium
1730
mg/Kg -
dry
82.2
185
1
08/22/19 20:35
BKN
6010D
Manganese
5630
mg/Kg -
dry
6.78
18.5
1
08/22/19 20:35
BKN
6010D
Mercury
<0.118
mg/Kg -
dry
0.118
0.533
1
08/22/19 09:00
TJS
7471A
Molybdenum
<4.81
mg/Kg -
dry
4.81
9.26
1
08/22/19 20:35
BKN
6010D
Nickel
16.5
mg/Kg -
dry
6.11
9.26
1
08/22/19 20:35
BKN
6010D
Potassium
930
mg/Kg -
dry
110
185
1
08/22/19 20:35
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 19-228-0032
Lab No : 93637
Sample ID : Hillsborough
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Hillsborough
Information :
REPORT OFANALYSIS
Report Date : 08/29/2019
Received : 08/16/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 8/15/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<18.1
mg/Kg - dry
18.1
18.5
1
08/22/19 20:35
BKN
6010D
Sodium
5963
mg/Kg - dry
286
926
1
08/22/19 20:35
BKN
6010D
Zinc
143
mg/Kg - dry
40.0
46.3
1
08/27/19 15:21
BKN
6010D
Sulfur
6630
mg/Kg - dry
181
185
1
08/22/19 20:35
BKN
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
08/22/19 20:35
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-228-0032
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 08/16/2019 09:11:09
Page 5 of 6

ro
a
LQ
(D
Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources inc
Brent Collins I
Account #46245
755 Yadklnville Rd
Mocksville, NC 27028
Project description
Project/Site Location (City/State)
RUSH - Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limits)
Fed Ex UPS E]USPS
WW -Wastewater GW -Groundwater
Date Results Needed
Courier ❑ Client crop Off
OW - Drinking Water S - Soil /Solid a - Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone 11
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
[e-mail]
Z
N
A Cool < loc Na2S2a3 (Micro On IV)
O
�IZ
"E
-0
Cool
Waypo'
a`
t
r
0pHlic2
-
C H2504
'Y
Y
¢
Q
C
m
❑
D None Required
AfJALYTICAL
o
°
G
E
0
Cl)
LLI
E NaOH pii>la
2790 Whitten Read
Unless noted, all containers
�
cr
is
V1
M
Q
a1
�
�
F HNO3 pH<2
G HCLpHt2
MemphLs, TN 38133
o
Z
�
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1901) 213-2400
per Table II of 40 CFR Part
a
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x
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Z
L❑
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H x3vO4 p14,2
I Cool <= 6C NAZS203
136,
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z
m
r
pate
Time
Sample Identification
Required
Analysis/ Preservative
Comments/Notes
P
�X 5
C
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
M n, M g , Ma, H g, N i , Se, Na, P, S, K,Zn
IIIII� Ill IIII I IIII IIIII illll Ills IIIIII III I I�� IIIII IIII Ilu 624 � 9Z
09 0.45
HiilsboroucIh
For Laboratory Use Only
Sampled by (Name - Print)
L���bK w�; �G
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
C.
5eals
Seats
Lab
�
G/ N
Rel, quilshell b(SIGNATURE)
DTime
Received by: ]SIGNATURE]
pate Time
Blank/r
Relin i heci by, (SIGNATURE]
pate Time
Recei d by: (SIGNATURE)
Date Time
a�
Relinquished by:;SIGNATURE]
Date Time
Re a y: { ATURE]
Da Tl
_
D _7 : sss

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
08/22/2019
Reported:
08/23/2019
For:
Hillsborough
Comments:
Geometric Mean <70 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190822-16-01
Fecal Coliforms
1
<67
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-01
Percent Solids
1
3.00
%
SM2540B-2011
08/22/2019
WC
190822-16-02
Fecal Coliforms
2
<62
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-02
Percent Solids
2
3.22
%
SM2540B-2011
08/22/2019
WC
190822-16-03
Fecal Coliforms
3
<69
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-03
Percent Solids
3
2.88
%
SM2540B-2011
08/22/2019
WC
190822-16-04
Fecal Coliforms
4
<75
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-04
Percent Solids
4
2.67
%
SM2540B-2011
08/22/2019
WC
190822-16-05
Fecal Coliforms
5
<69
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-05
Percent Solids
5
2.88
%
SM2540B-2011
08/22/2019
WC
190822-16-06
Fecal Coliforms
6
<80
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-06
Percent Solids
6
2.50
%
SM2540B-2011
08/22/2019
WC
190822-16-07
Fecal Coliforms
7
<71
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-07
Percent Solids
7
2.80
%
SM2540B-2011
08/22/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190822-16-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client: 5J�
plts."'IfG
�tf't� .4ek
STATFSVILLE ANALYTICAL
Address:
?s5 Yd /�
122 Court Street • P.O. Box 228
C� Y%JJk.-
Statesville,NC 28687
[phone]
��//
Mac,Vlvd1Y— /tfc— 2702Jr
Contact Person:
t
Phone # FAX#
Clain of
Custody Record
PO # Requisitioned by: Crime Date)
Customer
Lab -ID #y)
Time Sampled
Date Sampled
a
E
Matrix
Parameters requested for analysis
Sample ID#
(Grab Only)
[Grab Orl
wa9e w ww
z
s
Q
,-
(o00L
7
O7
Relinquished by:
Time 9.00 90, pm Date r/ 22119
Sampled by: /3�[
Received by:
Time Q 6�, pm Date / � l�
Transported by:
Relinquished by:
Time am, pm Date _/�/
Holding times met:
Received by:
Time am, pm Date
_t_J_
Compliance work: 1/
Composite Sampling #1:
Time begin am, pm Date /
/
Non-compliance work:
Time end am, pm Date J_/
lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date
r-
00
1.0
00
tV
U
Z
N
tL
(a
Ln
00
tV
tV
x
0
m
0
a-

aceAnalytical
National Center for Testing & Innovation
ANALYTICAL REPORT
August 26, 2019
EMA Resources
Sample Delivery Group: L1129947
Samples Received: 08/16/2019
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
HILLSBOROUGH L1129947-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
9
10
11
12
13
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1129947 03/26/19 16:41
PAGE:
2 of 22

HILLSBOROUGH L1129947-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
Landon Whitaker 08/15/19 08:30 08/16/19 09:00
Cp
Batch
Dilution Preparation
date/time
W G1331785
1 08/20/1914:2 0
WG1332728
1 08/21/1917:18
WG1333521
1 08/22/19 22:55
WG1332229
1 08/21/1919:18
W G1333140
1 08/23/1913:19
W G1332 965
1 08/23/1913:45
WG1333707
1 08/23/19 08:34
WG1333743
1 08/23/19 09:04
W G1332 983
1 08/22/1918:45
WG1333658
1 08/23/19 08:27
WG1334090
1 08/26/19 07:09
WG1334093
1 08/25/19 08:23
Analysis
date/time
08/20/1914:20
08/21/1917:18
08/23/1912:57
08/21/1919:18
08/23/1914:48
08/23/1913:45
08/23/1912:15
08/23/191100
08/22/1918:45
08/24/1916:00
08/26/1915:07
08/26/19 03:56
Analyst
CGD
CGD
JER
MJA
JIC
MJA
ABL
CCE
BMB
MT-1
LEL
AO
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 4 of 22

HILLSBOROUGH
Collected date/time: 08/15/19 08:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1129947
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
8/21/2019 5:18:37 PM
WG1332728
TCLP ZHE Extraction -
8/20/2019 2:20:50 PM
WG1331785
Fluid 1
8/21/2019 5:18:37 PM
WG1332728
Initial pH 7.43
8/21/2019 5:18:37 PM
WG1332728
Final pH 4.81
8/21/2019 5:18:37 PM
WG1332728
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 0.250 1 08/23/201912:57 WG1333521
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/21/201919:18 WG1332229
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.86 T8 1 08/23/201914:48 WG1333140
Sample Narrative:
L1129947-01 WG1333140: 6.86 at 23.9C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 08/23/201913:45 WG1332965
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 08/23/201912:15 WG1333707
Dilution Analysis
Batch
date / time
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
SDG:
DATE/TIME: PAGE:
L1129947
03/26/19 16:41 5 of 22

HILLSBOROUGH SAMPLE RESULTS
Collected date/time: 08/15/19 08:30 L1129947
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
08/22/201918:45
WG1332983
1,1-Dichloroethene
ND
0.0500 0.70 1
08/22/201918:45
WG1332983
2-Butanone (MEK)
ND
0.500 200 1
08/22/201918:45
WG1332983
Tetrachloroethene
ND
0.0500 0.70 1
08/22/201918:45
WG1332983
Trichloroethene
ND
0.0500 0.50 1
08/22/201918:45
WG1332983
Vinyl chloride
ND
0.0500 0.20 1
08/22/201918:45
WG1332983
(S) Toluene-dH
103
80.0-120
081221201918.45
WG1332983
(S) 4-Bromofluorobenzene
96.2
77.0-126
081221201918.45
WG1332983
(S) 1,2-Dichloroethane-d4
103
70.0-130
0812212019 18.45
WG1332983
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S)2,4-DichlorophenylAcetic Acid 81.8
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 08/24/201916:00
WG1333658
0.00200
10
1 08/24/201916:00
WG1333658
14.0-158
081241201916.00
WG1333658
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 08/26/201915:07
WG1334090
Endrin
ND
0.00500
0.02
1 08/26/201915:07
WG1334090
Heptachlor
ND
0.00500
0.0080
1 08/26/201915:07
WG1334090
Lindane
ND
0.00500
0.40
1 08/26/201915:07
WG1334090
Methoxychlor
ND
0.00500
10
1 08/26/201915:07
WG1334090
Toxaphene
ND
0.0100
0.50
1 08/26/201915:07
WG1334090
(S) Decochlorobiphenyl
71.9
10.0-128
081261201915.07
WG1334090
(S) Tetrochloro-m-xylene
67.3
10.0-127
081261201915.07
WG1334090
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 08/26/2019 03:56
WG1334093
2,4-Dinitrotoluene
ND
0.100
0.13
1 08/26/2019 03:56
WG1334093
Hexachlorobenzene
ND
0.100
0.13
1 08/26/2019 03:56
WG1334093
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 08/26/2019 03:56
WG1334093
Hexachloroethane
ND
0.100
3
1 08/26/2019 03:56
WG1334093
Nitrobenzene
ND
0.100
2
1 08/26/2019 03:56
WG1334093
Pyridine
ND
0.100
5
1 08/26/2019 03:56
WG1334093
3&4-Methyl Phenol
ND
0.100
400
1 08/26/2019 03:56
WG1334093
2-Methylphenol
ND
0.100
200
1 08/26/2019 03:56
WG1334093
Pentachlorophenol
ND
0.100
100
1 08/26/2019 03:56
WG1334093
2,4,5-Trichlorophenol
ND
0.100
400
1 08/26/2019 03:56
WG1334093
2,4,6-Trichlorophenol
ND
0.100
2
1 08/26/2019 03:56
WG1334093
(S) 2-Fluorophenol
19.6
10.0-120
0812612019 03.56
WG1334093
(S) Phenol-d5
13.9
10.0-120
0812612019 03.56
WG1334093
(S) Nitrobenzene-d5
34.4
10.0-127
0812612019 03.56
WG1334093
(S) 2-Fluorobiphenyl
39.7
10.0-130
0812612019 03.56
WG1334093
(S) 2,4, 6-Tribromophenol
55.0
10.0-155
0812612019 03.56
WG1334093
(S) p-Terphenyl-d14
68.6
10.0-128
0812612019 03.56
WG1334093
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 6 of 22

WG1333521 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1129947-01
Method Blank (MB)
(MB) R3443599-1 03/23/1912:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1129818-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1129313-08 03/23/1912:32 • (DUP) R3443599-3 03/23/1912:33
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide U 0.000 1 0.000 20
L1129818-33 Original Sample (OS) • Duplicate (DUP)
(OS) L1129313-33 03/23/1912:42 • (DUP) R3443599-6 03/23/1912:43
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Reactive Cyanide 0.0849 0.0891 1 4.86 J 20
Laboratory Control Sample (LCS)
(LCS) R3443599-2 08/23/19 12:28
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.67 107
Rec. Limits LCS Qualifier
50.0-150
L1129818-32 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1129313-32 03/23/19 12:36 • (MS) R3443599-4 03/23/19 12:40 • (MSD) R3443599-5 03/23/19 12:41
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 U 0.871 0.650 52.1 38.9 1 75.0-125 J6 J3 J6 29.1 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 7 of 22

WG1333521 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1129947-01
L1129818-41 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129313-41 03/23/19 12:51 • (MS) R3443599-7 03/23/19 12:52 • (MSD) R3443599-8 03/23/19 12:54
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.72 0.206 1.38 1.26 68.6 61.2 1 75.0-125 J6 J6 9.66
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 3 of 22

WG1332229
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3442971-1 03/21/191913
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1129198-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1129947-01
(OS) L1129193-02 03/21/1919:13 • (DUP) R3442971-3 03/21/1919:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide 29.5 29.5 1 0.176 20
Laboratory Control Sample (LCS)
(LCS) R3442971-2 08/21/19 19:18
Spike Amount LCS Result
Analyte mg/kg mg/kg
Reactive Sulfide 100 112
LCS Rec. Rec. Limits LCS Qualifier
112 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 9 of 22

WG1333140 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1129947-01
Laboratory Control Sample (LCS)
(LCS) R3443680-1 03/23/19 1443
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS: 9.94 at 23.1C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 10 of 22

WG1332965
Wet Chemistry by Method D93/1010A
L1129887-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1129337-01 03/23/1913:45 • (DUP) R3443639-2 03/23/1913:45
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
L1130263-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1129947-01
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1130263-01 03/23/1913:45 • (DUP) R3443639-3 03/23/1913:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3443639-1 08/23/19 13:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 83.8 102 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 11 of 22

WG1333707 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1129947-01
Method Blank (MB)
(MB) R3443590-1 03/23/191151
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control
Sample Duplicate (LCSD)
(LCS) R3443590-2 03/23/1911:53 • (LCSD) R3443590-3 03/23/191155
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0318 0.0323
106 108 80.0-120 1.59 20
L1129911-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1129911-01 03/23/19 1157 • (MS) R3443590-4 03/23/19 12:03 • (MSD) R3443590-5 03/23/19 12:05
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0317
0.0311 106 104 1 75.0-125 1.84 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 12 of 22

WG1333743
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1129947-01
(MB) R3443547-1 03/23/1910:52
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic 0.0355
J 0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead U
0.0330
0.100
Selenium U
0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3443547-2 08/23/1910:55 • (LCSD) R3443547-3 08/23/1910:57
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.73
9.87
97.3
98.7
80.0-120
Barium
10.0
9.99
10.1
99.9
101
80.0-120
Cadmium
10.0
9.81
9.92
98.1
99.2
80.0-120
Chromium
10.0
9.65
9.84
96.5
98.4
80.0-120
Lead
10.0
9.90
10.0
99.0
100
80.0-120
Selenium
10.0
9.78
9.94
97.8
99.4
80.0-120
Silver
2.00
1.81
1.83
90.4
91.6
80.0-120
L1129947-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
LCS Qualifier LCSD Qualifier RPD
RPD Limits
1.46
20
1.30
20
1.12
20
1.96
20
1.09
20
1.64
20
1.32
20
(OS) L1129947-01 03/23/19 1100 • (MS) R3443547-5 03/23/19 1106 • (MSD) R3443547-6 03/23/19 1109
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.89
9.84
98.3
97.8
1 75.0-125
Barium
10.0
ND
10.2
10.2
102
101
1 75.0-125
Cadmium
10.0
ND
9.94
9.94
99.4
99.4
1 75.0-125
Chromium
10.0
ND
9.87
9.81
98.7
98.1
1 75.0-125
Lead
10.0
ND
10.1
9.97
101
99.7
1 75.0-125
Selenium
10.0
ND
9.89
9.88
98.9
98.8
1 75.0-125
Silver
2.00
ND
1.83
1.83
91.7
91.7
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.495
0.263
0.0219
0.526
0.981
0.0332
0.0317
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT:
EMA Resources
SDG:
L1129947
DATE/TIME:
03/26/19 16:41
PAGE:
13 of 22

WG1332983
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS)
by Method
8260D
L1129947-01
Method Blank (MB)
C p
(MB) R3443293-2 03/22/191134
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
TC
I
Benzene U
0.0167
0.0500
Carbon tetrachloride U
0.0167
0.0500
FS
Chlorobenzene U
0.0167
0.0500
Chloroform U
0.0833
0.250
1,2-Dichloroethane U
0.0167
0.0500
[Cn]
1,1-Dichloroethene U
0.0167
0.0500
2-Butanone (MEK) U
0.167
0.500
5Sr
Tetrachloroethene U
0.0167
0.0500
Trichloroethene U
0.0167
0.0500
Vinyl chloride U
0.0167
0.0500
(S) Toluene-dH 102
80.0-120
(S) 4-Bromofluorobenzene 100
77.0-126
GI
(S) 1,2-Dichloroethane-d4 102
70.0-130
[Al
Laboratory Control Sample (LCS)
(LCS) R3443293-1 03/22/19 09:55
FSC
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
Benzene 0.0250
0.0234
93.6
70.0-123
Carbon tetrachloride 0.0250
0.0230
91.8
68.0-126
Chlorobenzene 0.0250
0.0229
91.5
80.0-121
Chloroform 0.0250
0.0239
95.7
73.0-120
1,2-Dichloroethane 0.0250
0.0239
95.7
70.0-128
1,1-Dichloroethene 0.0250
0.0232
92.8
71.0-124
2-Butanone (MEK) 0.125
0.127
101
44.0-160
Tetrachloroethene 0.0250
0.0227
90.7
72.0-132
Trichloroethene 0.0250
0.0244
97.5
78.0-124
Vinyl chloride 0.0250
0.0221
88.4
67.0-131
(S) Toluene-dH
101
80.0-120
(S) 4-Bromofluorobenzene
98.7
77.0-126
(S) 1,2-Dichloroethane-d4
102
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1129947
03/26/19 16:41 14 of 22

WG1332983 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1129947-01
L1129911-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129911-03 03/22/19 13 25 • (MS) R3443293-3 03/22/19 20:44 • (MSD) R3443293-4 03/22/19 2104
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
1.25
ND
0.697
0.820
55.1
65.0
Carbon tetrachloride
1.25
ND
0.467
0.620
37.4
49.6
Chlorobenzene
1.25
ND
0.882
0.957
70.5
76.5
Chloroform
1.25
ND
0.790
0.876
63.2
70.1
1,2-Dichloroethane
1.25
ND
1.01
1.08
81.2
86.2
1,1-Dichloroethene
1.25
ND
0.369
0.503
29.5
40.3
2-Butanone (MEK)
6.25
ND
6.59
6.41
105
103
Tetrachloroethene
1.25
ND
0.574
0.723
45.9
57.8
Trichloroethene
1.25
ND
0.647
0.771
51.8
61.7
Vinyl chloride
1.25
ND
0.262
0.353
21.0
28.3
(S) Toluene-dH
104
103
(S) 4-Bromofluorobenzene
99.6
102
(S) 1,2-Dichloroethane-d4
97.5
105
ACCOUNT:
EMA Resources
PROJECT:
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
16.3
27
1 23.0-159
J3 28.2
28
1 33.0-152
8.14
27
1 29.0-154
10.3
28
1 29.0-151
6.00
27
1 11.0-160
J3 30.7
29
1 10.0-160
2.74
32
1 10.0-160
22.9
27
1 10.0-160
17.5
25
1 10.0-160
J3 29.7
27
80.0-120
77.0-126
70.0-130
SDG:
DATE/TIME:
PAGE:
L1129947
03/26/19 16:41
15 of 22

WG1333658
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1129947-01
(MB) R3444010-1 03/24/1910:02
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 62.8
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3444010-2 03/24/191017
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4-D 0.0500
0.0364
72.8
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0358
71.6
50.0-125
(S) Z4-Dichlorophenyl Acetic
670
14. 0-158
Acid
L1129693-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129693-04 03/24/19 11:46 • (MS) R3444010-3 03/24/19 12:01 • (MSD) R3444010-4 03/24/19 12:15
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0390
0.0398
78.0
79.6
2,4,5-TP (Silvex)
0.0500
ND
0.0395
0.0407
79.0
81.4
(S) Z4-Dichlorophenyl Acetic
71.2
73.0
Acid
ACCOUNT:
EMA Resources
PROJECT:
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 50.0-120 2.03 20
1 50.0-125 2.99 20
14.0-158
SDG: DATE/TIME: PAGE:
L1129947 03/26/19 16:41 16 of 22

WG1334090
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1129947-01
(MB) R3444319-2 03/26/191303
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
89.3
10.0-128
(S) Tetrochloro-m-xylene
71.7
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3444319-1 08/26/1912:50
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.0102
102
55.0-129
Endrin
0.0100
0.00944
94.4
57.0-134
Heptachlor
0.0100
0.00895
89.5
27.0-132
Methoxychlor
0.0100
0.00957
95.7
54.0-155
(S) Decachlorobiphenyl
84.7
10.0-128
(S) Tetrochloro-m-xylene
76.6
10.0-127
L1129737-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129737-01 03/26/19 13:15 • (MS) R3444319-3 03/26/19 13:27 • (MSD) R3444319-4 03/26/19 13:40
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.0107
0.00888
107
88.8
1 14.0-141
Endrin
0.0100
ND
0.0103
0.00849
103
84.9
1 10.0-160
Heptachlor
0.0100
ND
0.00852
0.00703
85.2
70.3
1 16.0-136
Methoxychlor
0.0100
ND
0.0103
0.00841
103
84.1
1 10.0-160
(S) Decachlorobiphenyl
89.2
73.4
10.0-128
(S) Tetrochloro-m-xylene
86.3
65.7
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
18.6 40
19.3 39
19.2 40
20.2 34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 17 of 22

WG1334093 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1129947-01
Method Blank (MB)
(MB) R3444119-1 03/25/19 23:43
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
44.1
10.0-127
(S) 2-Fluorobiphenyl
48.9
10.0-130
(S) p-Terphenyl-d14
65.0
10.0-128
(S) Phenol-d5
10.3
10.0-120
(S) 2-Fluorophenol
18.5
10.0-120
(S) 2,4, 6-Tribromophenol
49.2
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3444119-2 08/26/19 00:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.195
39.0
18.0-120
2,4-Dinitrotoluene 0.500
0.386
77.2
49.0-124
Hexachlorobenzene 0.500
0.344
68.8
44.0-120
Hexachloro-1,3-butadiene 0.500
0.189
37.8
19.0-120
Hexachloroethane 0.500
0.167
33.4
15.0-120
Nitrobenzene 0.500
0.234
46.8
27.0-120
Pyridine 0.500
0.155
31.0
10.0-120
2-Methylphenol 0.500
0.180
36.0
28.0-120
3&4-Methyl Phenol 0.500
0.192
38.4
31.0-120
Pentachlorophenol 0.500
0.370
74.0
23.0-120
2,4,5-Trichlorophenol 0.500
0.354
70.8
44.0-120
2,4,6-Trichlorophenol 0.500
0.328
65.6
42.0-120
(S) Nitrobenzene-d5
37.4
10.0-127
(S) 2-Fluorobiphenyl
55.5
10.0-130
(S) p-Terphenyl-d14
69.5
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1129947 08/26/19 16:41 18 of 22

WG1334093 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1129947-01
Laboratory Control Sample (LCS)
(LCS) R3444119-2 08/26/19 00:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 12.4 10.0-120
(S) 2-Fluorophenol 19.6 10.0-120
(S) 2,4, 6-Tribromophenol 70.0 10. 0-155
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 08/26/19 16:41 19 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
F
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
Rc
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
Case Narrative (Cn)
Quality Control
Summary (Qc)
Sample Chain of
Custody (Sc)
Sample Results (Sr)
Sample Summary (Ss)
Qualifier
J
J3
J6
T8
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Description
The identification ofthe analyte is acceptable, the reported value is an estimate.
The associated batch QC was outside the established quality control range for precision.
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1129947 03/26/19 16:41 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1129947 03/26/19 16:41 21 of 22

Billing Information:
Analysis
/
Container
/ Preservative
Chain of Custody Page _ a,
EMA Resources
Mr. Brent Collins IPreS
755 Yadkinville Road Chk
Analytical
755 Yadkinville Road
Mocksville, NC 27028
f
Mocksville, NC 27028
12065 Lebanon Rd
Report to:
Email To: brent.collins@emaresourcesinccom
Mr. Brent Collins
nohe 515 75s s se }TC`�
Phone: SM767-5859
Fax: [phone]
Project
City/State
Description:
Collected
Lff
Client Project#
Lab Project#
Phone: 33b-751-1441
B050I,
Fax: 336-7S1-1442
a
Acctnum, WARES
Collected by (print):
Site/Facility ID N
PO N
o
u,
Z
U
Template-T114i3
Collected by (signature):
Rush? (Lab MUST Be Notified] Quote p
rL
G
Prelogin: P689629
Same Day Five Day
Next Day S Day (Rad Only) Date Results Needed
TSR: 702 -Cassandra Foster
Immediately
_
_Two Day _ 10 Day (Rad Only) No.
U
_
w
PB: I
Packed on Ice N Y
Three Day of
I-q
M
Shipped Via: FedEX Ground
mple ID
Sarni
Comp/Grab
Matrix'
Depth
P
Date
Time
ntrs
U
U
Re­ks Sacs ple C(lab oily)
Ss
s '
&l��f rg
�,,,,
2
X
X
—`
pH Temp
r Matrix:Remarks:
SS -Soil AIR - Air F- Filter
Sample Receia:
CDC Seal Present/Intact: _NP _Y N
—N
CCC Signed/Accurate: .Jf
GW - Groundwater 8- Bioassay
Bottles arrive intact. :/7T ti
WW - Wastewater
Flow Other
Correct bottles used: L"T
DW - Drinking ate
ff
Sam ies returned via:
Sufficient volwne sent: !1X _t;
OT-other 5(VQl�i
_LIPS _Fed Ex _Courier Tracking
—
If A❑nli=able
V0A Zero Keadspace: Y N
FreseerAvFalticln+CorrreAcft/Clhleckedr:f —Y —N
9
Date.
Time:
Received by: (Signature)
Trip Blank Received: Ye / No
i
ellS
3..3b�
eoH
MD SLREEN: CU.5 �iirV 11r
�J BIR
If preservation required by Login: Date/Time
Re uish by : (Signatur
Date:
Time:
Received by: (Signature)
Temp: 41UPC Bottles Received:
Relinquished by : (Signature)
Date:
Time:
ReceivIld for lab y: (Signat flDate:
Time:
Hold:
CondItia

Town of Hillsborough Permit Renewal -
WQ0038580
Final Audit Report
Created:
2021-03-03
By:
Brent Collins ([e-mail])
Status:
Signed
Transaction ID:
CBJCHBCAABAAZQvL eldcPtOVsK2IQor4eG6xYwFDdmz
2021-03-03
"Town of Hillsborough Permit Renewal - WQ0038580" History
Document created by Brent Collins ([e-mail])
2021-03-03 - 12:26:20 PM GMT- IP address: 24.88.129.34
P+ Document emailed to Marie Strandwitz ([e-mail]) for signature
2021-03-03 - 12:27:22 PM GMT
Email viewed by Marie Strandwitz ([e-mail])
2021-03-03 - 12:28:53 PM GMT- IP address: 24.211.150.18
Document e-signed by Marie Strandwitz ([e-mail])
Signature Date: 2021-03-03 - 12:30:06 PM GMT - Time Source: server- IP address: 24.211.150.18
Agreement completed.
2021-03-03 - 12:30:06 PM GMT
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