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HomeMy WebLinkAboutWQ0005135_Residual Annual Report 2020_20210225Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* W00005135 Applicant/Permittee von Drehle Corporation Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Fayetteville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Robert T. Branch Email Address* bbranch@branchrs.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363129007 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WO0005135 Ras Current Existing permt number Applicant/Permittee Address* von Drehle Corporation - 126 First Street Cordova, NC Facility Name * von Drehle Corporation RLAP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) class_B_vd_2020-Final.pdf 7.69MB upload only 1 FDF docurrent (less than 250 IvB). Multiple documents rust be corrbined into one RJF file unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/25/2021 2020 ANNUAL REPORT VON DREHLE CORPORATION CLASS B CORDOVA, NORTH CAROLINA PERMIT #WQ0005135 Prepared For: Von Drehle Corporation 126 First Street Cordova, North Carolina 28330 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill, SC 29732 February 2021 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732 PHONE (336) 312-9007 February 25, 2021 North Carolina Department of Environmental Quality Division of Water Resource — Non -discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2020 LAND APPLICATION ANNUAL REPORT Von Drehle Corporation Cordova, North Carolina Permit No. WQ0005135 Branch Residuals & Soils Project No. 2014-110 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Von Drehle Corporation. This data includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Reduction Forms, 8) Fecal and Salmonella Results, 9) Soils Lab Data, 10) 2020 Application Summary Table, and 11) 2020 Application Condition Summaries. Total production for 2020 was 60,907 wet tons for this facility. Disposal/applications were as follows: • 26,568.51 wet tons (9,958.53 dry tons) applied as Class A under separate permit, and • 34,338.49 wet tons applied to the farms in North Carolina. A total of 34,338.49 wet tons (12,143.05 dry tons) of residual by-product paper were land applied to the farms at US1 and Hamlet (430 acres). Both Hamlet and US-1 sites received 55 lbs/acre nitrogen topdressing in March 2020. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sin y, Robert Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Attachment cc: Von Drehle Corporation TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Forms VIII Fecal and Salmonella Documentation and Results IX Soil Analysis Reports X 2020 Application Summary Table XI 2020 Application Condition Summaries CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0005135 County: Richmond Year: 2020 Facility Name (as shown on permit): von Drehle Corporation Land Application Operator: Bio-Nomic Services, Inc Phone: (704) 529-0000 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes [J No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals ApOication Summa . Total number of application fields in the ermit: 18 Total number of fields utilized for land application durin the year: 18 Total amount of dry tons applied during the year for all application sites: 12,143.05 Total number of acres utilizes for land application during the year: 430.00 Part B - Annual Comoiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. � Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. Justin Dawkins, Cordova Plant Manager ` Al f I- Permittee Name and Title (type or print) Signature f�Permittedd Date , 2-1 c'�C'�-�-i cam— 2l w-e I Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006) I a, No a R Oki i 111131 mm, 05 19 in 10 w I I X119-al ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0005135 Facility Name: von Drehle Corporation Residual Source WQ # or City of Rockingham IUP #0015 NPDES #: WWTP Name: Cordova Facility Residual Analvsis Data Laboratory: 1) 2) 3) 4) 5) Microbac Labs Parameter (mg/kg) Ceiling Conc. Limit Sam le or Com osite Date 12/16/2019 2/172020 4/162020 6/8/2020 8/10/2020 10/12/2020 Percent Solids (%) NA 36.50 35.50 30.20 36.30 37.00 42.30 Arsenic 75 <1.91 <2.06 1 <2.45 <2.08 <1.92 <1.89 Cadmium 85 <0.191 <0.206 <0.245 1 <0.245* <0.192 1 0.20 Copper 4,300 24.60 19.30 16.90 14.30 67.20 32.00 Chromium NA NA NA NA NA NA NA Lead 840 <1.91 <2.06 <2.45 <2.08 <1.92 <1.89 Mercury 57 <0.261 <0.653 <0.825 <0.679 <0.662 <0.658 Molybdenum 75 -e5.74 <6.19 <7.34 1 <6.23 <5.77 <5.67 Nickel 420 <3.82 <4.12 <4.89 <4.15 <3.85 3.78 Selenium 100 <1.91 <2.06 <2.45 <2.08 40.40 <1.89 ' Zinc 7,500 74.80 1 168.00 94.80 87.90 104.00 74.30 Total Phosphorus NA 0.74 0.86 42.00 109.00 4.30 3.50 TKN NA 482.00 579.00 86.00 91.20 3.64 1940.00 Ammonia -Nitrogen NA <2.74 <2.55 <64 <2.65 <44.1 <4.50 Nitrate and Nitrite NA <2.96 <14.48 1 1 <3.73 1 <1.82 <14.23 <1.865 Cadmium was not analyzed in the 611 BCD sample by lab as marked on the chain of custody. The cadmium value from the 4/16/20 sample was used for calculation purposes. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informal, includigg the possibility of fines and imprisonment for knowing violations." Signature of *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) 2r �-3f Z Date DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 23 Acres Permitted: 23 Site #: 3 Field #: n/a WcB 652.68 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-5 MB Sample or Com- 8/10/20 posite Date % Solids 37.00 Arsenic 1.92 Cadmium 0.19 Chromium 0.00 Copper 67.20 Lead 1.92 Mercury 0.66 Molyb- denum 5.77 Nickel 3.85 Selenium 40.40 Zinc 104.00 Total Phos- 4 horus (Calculated in lbs/acre): Annual Heavy Metal Field Loadings �o 9 0 28.38 m s Arsenic 0.11 0.11 Cadmium 0.01 0.01 Chromium 0.00 0.00 Copper 3.81 3.81 Lead 0.11 0.11 Mercury 0.04 0.04 Molyb- 0.33 0.33 denum Nickel 0.22 0.22 Selenium 2.29 2.29 Zinc 5.90 5.90 Total Phos- 0.24 0.24 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including tl possWll of tines and imprisonment for knowing violations" 2 Z-S z Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 253.82 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB Acres Used: 9.1 Acres Permitted: 9.1 Site #: 3 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-5 MB 1 1 i Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ;e V � En 0 27.89 m_ 0• n 7 � Arsenic 0.11 0.11 Cadmium 0.01 0.01 �hromium 0.00 0.00 Copper 3.75 3.75 Lead 0.11 0.11 Mercury 0.04 0.04 Molyb- 0.32 0.32 denum Nickel 0.21 0.21 Selenium 2.25 2.25 Zinc 5.80 5.80 Total Phos- 0.24 0.24 Morus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the polity of fines and imprisonment for knowing violations" (�7 - 2�� Zz Z3 Z( Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 13.2 Acres Permitted: 13.2 Site #: 3 Field #: 380.73 n/a WrR Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft vd 2020-5 MR 4 • • : 1 1 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): -o an � n a 0 28.84 a �a y s Arsenic 0.11 0.11 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 3.88 3.88 Lead 0.11 0.11 Mercury 0.04 0.04 Molyb- 0.33 0.33 denum Nickel 0.22 0.22 Selenium 2.33 2.33 Zinc 6.00 6.00 Total Phos- 0.25 0.25 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including t Possibility of fines and imprisonment for knowing violations" c= Z Z32 r Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 317.28 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB Acres Used: 11.1 Acres Permitted: 11.1 Site #: 3 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): WIT, M11 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): 4 8 a� 0 28.58 m n• � y R y .. o• � Arsenic 0.11 0.11 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 3.84 3.84 Lead 0.11 0.11 Mercury 0.04 0.04 Molyb- 0.33 0.33 denum Nickel 0.22 0.22 Selenium 2.31 2.31 Zinc 5.95 5.95 Total 1 Phos- 0.25 0.25 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including th ossibility of fines and imprisonment for knowing violations" 2�__ z 0 Z� Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 18.9 Acres Permitted: 18.9 Site #: 3 Field #: 550.39 n/a WcB 3A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-5 M8 2020.E-MB Sample or Com- posite Date 8/10/20 10 12 20 % Solids 37.00 42.30 Arsenic 1.92 1.89 Cadmium 0.19 0.20 Chromium 0.00 0.00 Copper 67.20 32.00 Lead 1.92 1.89 Mercury 0.66 0.66 Molyb- denum 5.77 5.67 Nickel 3.85 3.78 Selenium 40.40 1.89 Zinc 104.00 74.30 Total Phos- horus 4 4 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 1 O ap a 0 26.38 2.74 n H y w a Arsenic 0.10 0.01 0.11 Cadmium 0.01 0.00 0.01 Chromium 0.00 0.00 0.00 Copper 3.55 0.18 3.72 Lead 0.10 0.01 0.11 Mercury 0.03 0.00 0.04 Molyb- 0.30 0.03 0.34 denum Nickel 0.20 0.02 0.22 Selenium 2.13 0.01 2.14 Zinc 5.49 0.41 5.89 Total Phos- 0.23 0.02 0.25 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the po lity of fines and imprisonment for knowing violations" Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 1,078.74 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB Acres Used: 37.2 Acres Permitted: 37.2 Site #: 3 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): -a mmn-s MR 3H ® Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 29.00 m y Arsenic 0.11 0.11 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 3.90 3.90 Lead 0.11 0.11 Mercury 0.04 0.04 Molyb- 0.33 0.33 denum Nickel 0.22 0.22 Selenium 2.34 2.34 Zinc 6.03 6.03 Total Phos- 1 0.25 0.25 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin possibility of fines and imprisonment for knowing violations" Z3 l Signature of Land Applier Author Daryl D. Merritt Date t DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 24.6 Acres Permitted: 24.6 Site #: 3 Field #: 663.26 n/a WCA 6A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-6-MB Annual Heavy Metal Field Loadings (Calculated in ibs/acre): aw H 0 26.96 Arsenic 0.10 0.10 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 1.73 1.73 Lead 0.10 0.10 Mercury 0.04 0.04 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ibility of fines and imprisonment for knowing violations" 777 ,--2,- ?ZZZ-3 2- Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.5 Acres Permitted: 37.5 Site #: 3 Field #: 1,075.01 n/a WcR 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-5 MR 302fL6-MR Sample or Com- posite Date 8/10/20 10/12r20 % Solids 37.00 42.30 Arsenic 1.92 1.89 Cadmium 0.19 0.20 Chromium 0.00 0.00 Copper 67.20 32.00 Lead 1.92 1.89 Mercury 0.66 0.66 Molyb- denum 5.77 5.67 Nickel 3.85 3.78 Selenium 40.40 1.89 Zinc 104.00 74.30 Total Phos- horus 4 4 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): a� y e 15.95 12.71 s Arsenic 0.06 0.05 0.11 Cadmium 0.01 0.01 0.01 Chromium 0.00 0.00 0.00 Copper 2.14 0.81 2.96 Lead 0.06 0.05 0.11 Mercury 0.02 0.02 0.04 Molyb- 0.18 0.14 0.33 denum Nickel 0.12 0.10 0.22 Seleniuml 1.29 0.05 1.34 Zinc 3.32 1.89 5.21 Total 1 Phos- 0.14 0.09 0.23 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin h ssibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 470.62 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbB Acres Used: 19.1 Acres Permitted: 19.1 Site #: 4 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): A 2020-3 MB 2020-4 MB Sample or Com- posite Date 4/16/20 6820 % Solids 30.20 36.30 Arsenic 2.45 2.08 Cadmium 0.25 0.25 Chromium 0.00 0.00 Copper 16.90 14.30 Lead 2.45 2.08 Mercury 0.83 0.68 Molyb- denum 7.34 6.23 Nickel 4.89 4.15 Selenium 2.45 2.08 Zinc 94.80 87.90 Total Phos- horus 42 109 Annual Heavy Metal Field Loadings (Calculated in ibs/acre): �o may' y 0 23.24 1.40 o• Arsenic 0.11 0.01 0.12 Cadmium 0.01 0.00 0.01 Chromium 0.00 0.00 0.00 Copper 0.79 0.04 0.83 Lead 0.11 0.01 0.12 Mercury 0.04 0.00 0.04 Molyb- 0.34 0.02 0.36 denum Nickel 0.23 0.01 0.24 Selenium 0.11 0.01 0.12 Zinc 4.41 0.25 4.65 Total 1 Phos- 1.95 0.30 2.26 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ossibility of fines and imprisonment for knowing violations" -023 Z Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 1,106.47 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbB Acres Used: 37.1 Acres Pernutted: 37.1 Site #: 4 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-3 MR 2020.4 MR Sample or Com- posite Date 4/16/20 618/20 % Solids 30.20 36.30 Arsenic 2.45 2.08 Cadmium 0.25 0.25 Chromium 0.00 0.00 Copper 16.90 14.30 Lead 2.45 2.08 Mercury 0.83 0.68 Molyb- denum 7.34 6.23 Nickel 4.89 4.15 Selenium 2.45 2.08 Zinc 94.80 87.90 Total Phos- horus 42 109 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): a� y n S 0 12.56 17.26 d a a Arsenic 1 0.06 0.07 1 1 1 1 0.13 Cadmium 0.01 0.01 0.01 Chromium 0.00 0.00 0.00 Copper 0.42 0.49 0.92 Lead 0.06 0.07 0.13 Mercury 1 0.02 0.02 0.04 Molyb- 0.18 0.22 0.40 denum Nickel 0.12 0.14 0.27 Selenium 0.06 0.07 0.13 Zinc 2.38 3.03 5.42 Total Phos- 1 1.06 3.76 4.82 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ossibility of fines and imprisonment for knowing violations" Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 759.67 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 22.4 Acres Permitted: 22.4 Site #: 4 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-2 M8 2020-3 MR Sample or Com- posite Date 2/17/20 4/16 20 % Solids 35.50 30.20 Arsenic 2.06 2.45 Cadmium 0.21 0.25 Chromium 0.00 0.00 Copper 19.30 16.90 Lead 2.06 2.45 Mercury 0.65 0.83 Molyb- denum 6.19 7.34 Nickel 4.12 4.89 Selenium 2.06 2.45 Zinc 168.00 94.80 Total Phos- horus 1 42 Annual Heavy Metal Field Loadings (Calculated in "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ossibIlity of fines and imprisonment for knowing violations" ZJ Zt Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 1,276.78 Permit #: W00005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 50.8 Acres Permitted: 50.8 Site #: 4 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-3 MR 2020.4 MR Sample or Com- posite Date 4/16/20 6/8/20 % Solids 30.20 36.30 Arsenic 2.45 2.08 Cadmium 0.25 0.25 Chromium 0.00 0.00 Copper 16.90 14.30 Lead 2.45 2.08 Mercury 0.83 0.68 Molyb- denum 7.34 6.23 Nickel 4.89 4.15 Selenium 2.45 2.08 Zinc 94.80 87.90 Total Phos- horns 42 109 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): �o ma= � 0 24.79 0.34 o• Arsenic 0.12 0.00 0.12 Cadmium 0.01 0.00 0.01 Chromium 0.00 0.00 0.00 Copper 0.84 0.01 0.85 Lead 0.12 0.00 0.12 Mercury 0.04 0.00 0.04 Molyb- 0.36 0.00 0.37 denum Nickel 0.24 0.00 0.25 Selenium 0.12 0.00 0.12 Zinc 4.70 0.06 4.76 Total Phos- 2.08 1 0.07 2.16 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the pos ' ility of fines and imprisonment for knowing violations" Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 272.47 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 11.1 Acres Permitted: 11.1 Site #: 4 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020.3 MA Annual Heavy Metal Field Loadings (Calculated in lbs/acre): o a= � n 0 24.55 m a fly � y O n 7 � Arsenic 0.12 0.12 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 0.83 0.83 Lead 0.12 0.12 Mercury 0.04 1 1 0.04 Molyb- 0.36 0.36 denum Nickel 0.24 0.24 Selenium 0.12 0.12 Zinc 4.65 4.65 Total 1 Phos- 2.06 2.06 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin a ility of. Ines and imprisonment for knowing violations" ZZ KJ7 or z Z� Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 489.14 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 19.2 Acres Permitted: 19.2 Site #: 4 Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft vd 2020-4 Me Annual Heavy Metal Field Loadings (Calculated in lbs/acre): S a 25.48 o Arsenic 0.11 0.11 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 0.73 0.73 Lead 0.11 0.11 Mercury 0.03 0.03 Molyb- 0.32 0.32 denum Nickel 0.21 0.21 Selenium 0.11 0.11 Zinc 4.48 4.48 Total Phos- 5.55 5.55 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" �- / z� Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 28.9 Acres Permitted: 28.9 Site #: 4 Field #: 844.88 n/a ThA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd ?mn-4 MR is Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 29.23 o• Arsenic 0.12 0.12 Cadmium 0.01 0.01 Chromiurr 0.00 0.00 Copper 0.84 0.84 Lead 0.12 0.12 Mercury 0.04 0.04 Molyb- 0.36 0.36 denum Nickel 0.24 0.24 Selenium 0.12 0.12 Zinc 5.14 5.14 Total Phos- 6.37 6.37 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ssibility of fines and imprisonment for knowing violations" Z� 2 � Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 28.6 Acres Permitted: 28.6 Site #: 4 Field #: 844.88 n/a TbA 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-4 MR Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �o a� y 0 29.54 ra na g• Arsenic 0.12 0.12 Cadmium 0.01 0.01 Zhromiurr 0.00 0.00 Copper 0.84 0.84 Lead 0.12 0.12 Mercury 0.04 1 1 1 0.04 Molyb- 0.37 0.37 denum Nickel 0.25 0.25 Selenium 0.12 0.12 Zinc 5.19 5:19 Total Phos- 6.44 6.44 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu g the ossibility of fines and imprisonment for knowing violations" tgnature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 18.9 Acres Permitted: 18.9 Site #: 4 Field #: 537.04 n/a TbA AA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2020-4 MB 2020-5 MB Sample or Com- posite Date 6/8/20 8/10/20 % Solids 36.30 37.00 Arsenic 2.08 1.92 Cadmium 0.25 0.19 Chromium 0.00 0.00 Copper 14.30 67.20 Lead 2.08 1.92 Mercury 0.68 0.66 Molyb- denum 6.23 5.77 Nickel 4.15 3.85 Selenium 2.08 40.40 Zinc 87.90 104.00 Total Phos- horus 109 4 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): v 18.82 9.59 o' Arsenic 0.08 0.04 0.12 Cadmium 0.01 0.00 0.01 Chromium 0.00 0.00 0.00 Copper 0.54 1.29 1.83 Lead 0.08 0.04 1 0.12 Mercury 0.03 0.01 0.04 Molyb- 0.23 0.11 0.35 denum Nickel 0.16 0.07 0.23 Selenium 0.08 0.78 0.85 Zinc 3.31 2.00 5.30 Total Phos- 4.10 0.08 4.19 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu the possibility of fines and imprisonment for knowing violations" �- 2 Z Z Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 569.18 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 19.3 Acres Permitted: 19.3 Site #: 4 Field #: 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ,,,i )mns nen Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �o a� S 0 29.49 d Arsenic 0.12 0.12 Cadmium 0.01 0.01 ::hromiurr 0.00 0.00 Copper 0.84 0.84 Lead 0.12 0.12 Mercury 0.04 1 1 1 0.04 Molyb- 0.37 0.37 denum Nickel 0.24 0.24 Selenium 0.12 0.12 Zinc 5.18 5.18 Total 1 Phos- 6.43 6.43 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the wssibility of fines and imprisonment for knowing violations" 2 Z1 Signature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 23.00 Owner: von Drehle Corporation Annual Dry Tons Applied: 652.68 Site #: I Acres Permitted: 23.00 Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop I Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A O o F; a r, _ o Specify Totals Per Acre , o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, Wct, Moist) Precip. Past 24 Hrs. Inches d 2 _ s ,;' G m a o• c m ^. �; N . 2 " d � " * s :3 TKN m • k • z a = 3 'o a eo o 03 -gfkg Nitrate and Nitrite m W k PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals In Gal. Crop 1 Crop 2 Crop 1 Crop 2 Sep-20 1,764.041 76.70 37.00 28.38 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 2.39 X TOTALS: 77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.81 0.11 0.04 0.33 0.22 2.29 5.90 0.24 2.39 0.00 Date Ibs/ac Current Cumulative Ibs/acre .......................... 0.53 2.23 NA 17.31 0.44 0.06 NA 2.82 2.74 44.25 0.42 2.22 NA 13.50 0.33 0.02 NA 2.60 0.45 38.34 36 34 NA 1,338 267 15 NA 374 89 2,498 . . . . . . ................................. 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation VV �i **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Signature of Land Applier Date Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R�A,,�� 1R Ft'1R11A FCF /19l9MR1 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 9.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 253.82 Site #: 2 Acres Permitted: 9.10 Operator: von Drehle Corporation Predominat Soil Series Wcg Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop I Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A O 0 w oReport Specify Totals Per Acre , o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) $110 Cond. (Dry, Wet) Moist Precip. Past 24 Hrs. Inches n o M n. n d ' = c m * N o > 5 a g ` w a c > TKN m W k L Z Y = 9 o'oo c ? mWkg Nitrate and Nitrite m PAN Applied pP (]bs/acre) Must Select Crop 1 or Crop 2 Wei Cu.Yd. Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Sep-20 686.00 75.38 37.00 27.89 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 2.35 X TOTALS: 75 As Cd Cr Cu Pb HR Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.75 0.11 0.04 0.32 0.21 2.25 5.80 0.24 2.35 0.00 Date lbs/ac Current Cumulative lbs/acre 35.62 0.38 0.07 NA 15.06 0.36 0.05 NA 1.83 S0.46 0.27 0.06 NA 11.31 0.26 0.02 NA 1.62 29.82 36 34 1 NA 1 1,338 267 15 NA 374 89 2,498 80.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 03, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RAkip rnphe r lzr r, wonnai ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized: 13.20 Owner: von Drehle Corporation Annual Dry Tons Applied: 380.73 Site #: 4 Acres Permitted: 13.20 Operator: von Drehle Corporation Predominat Soil Series Wcg Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop I Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A C7 o m a ro s o Specify Totals Per Acre , /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste etc.) Site Cond. (Dry, Wet. Moist) Precip. Past 24 Hrs. inches 4 b " _ o m : c = w > 3 � " m : m > TKN m k Z Y 'o a 0 o R. m k • Nitrate and Nitrite m . PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wei Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Oct-20 1,029.00 77.95 37.00 28.84 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 2.43 X TOTALS: 78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.88 0.11 0.04 0.33 0.22 2.33 6.00 0.25 2.43 0.00 Date lbs/ac Current Cumulative lbs/acre 0.53 0.97 NA 12.66 0.52 0.07 NA 1.48 2.86 40.53 0.42 0.96 NA 8.79 0.41 0.03 NA 1.26 0.53 34.53 36 34 NA 1,338 267 1 15 1 NA 1 374 1 89 1 2,498 1 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation J **Volitilization Rate: Surface- 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 03, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RIiftp Fn1alu Fqt= /iq/7t1t1F1 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 11.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 317.28 Site #: 5 Acres Permitted: 11.10 Operator: von Drehle Corporation Predominat Soil Series Wcg Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A 3 C7 o Specify Totals Per Acre , o Solids As Decimal Volume Applied per Acre DT: Ac Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc.) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. Inches o $ n = �. o „ 0--_ c _. ; w . N • w > m ,, > TKN m • Z Y 9 ti'oo c c, w m • • Nitrate and Nitrite PAN Applied pp (Ibs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop I Crop 2 Oct-20 857.50 77.25 37.00 28.58 von Drehle Paper INC 1.00 1 0.40 3.64 44.10 _MWkg 1 14.23 2.41 X TOTALS: 77 As Cd Cr Cu Pb H2 Mo Ni Se Zn P I PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.84 0.11 0.04 0.33 0.22 2.31 5.95 0.25 1 2.41 1 0.00 Date lbs/ac Current Cumulative Ibs/acre 0.67 1.06 NA 14.62 0.53 0.06 NA 1.72 3.28 43.46 0.56 1.04 NA 10.78 0.42 0.02 NA 1.50 0.97 37.51 36 34 NA 1,338 267 15 NA 374 89 2,498 ' , ' * . . . . I FIE Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Z Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Signature of Land Applier Date Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RAI,,p Fn„A,, r ce i,,>nnnni ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 18.90 Owner: von Drehle Corporation Annual Dry Tons Applied: 550.39 Site #: 3A Acres Permitted: 18.90 Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A 3 C7 _ � o Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, mac) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. Inches o 3 v T m a a. c A = n w • 5 a " w t w TKN mgtkg Z a .: 3 o c �^ w• mgtkg Nitrate and Nitrite mgfkgCrop PAN Applied (Ibs/acre) Must Select Crop 1 or Crop 2 Wei Tons _ Cu.Yd. Report Totals in Gal. 1 Crop 2 Crop 1 Crop 2 Sep-20 1,347.50 71.30 37.00 26.38 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 2.22 X Nov-20 122.50 6.48 42.30 2.74 von Drehle Paper INC 1.00 0.40 1940.00 4.50 1.87 4.28 X TOTALS: 78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P ITAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.72 0.11 0.04 0.34 0.22 2.14 5.89 0.25 1 6.50 0.00 Date Ibs/ac Current Cumulative Ibs/acre .......................... 0.59 0.07 NA 11.62 0.48 0.06 NA 1.20 2.65 27.04 0.47 0.06 NA 7.90 0.37 0.02 NA 0.97 0.51 21.14 36 34 NA 1 1,338 267 15 NA 374 89 2,498 1 80.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Z.� Z **Volitilization Rate: Surface - 0.5, Nection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading P VR FnRM FRF /19/2nnnt ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 37.20 Owner: von Drehle Corporation Annual Dry Tons Applied: 1,078.74 Site #: 313 Acres Permitted: 37.20 Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o o S i Sv cify Totals Per Acre o Solids As Decimal Volume Applied per Acre DT.iAc Residual Sources (NPDES #, WQ#, Fert., Animal Waste etc.) Site Cond. (Dry Wet,Hrs. Moist ) Precip Past 24 Index o 3 0 s A o w ' c X w c 'm_ TKN m k � z 3 as c $ .. m Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop I or Crop 2 Cu.Yd. Report Totals In Gal. Crop 1 Crop 2 Crop I Crop 2 Sep-20 2,915.50 78.37 37.00 29.00 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 2.44 X TOTALS: 78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 3.90 0.11 0.04 0.33 0.22 2.34 6.03 0.25 2.44 0.00 Date I lbs/ac Current Cumulative lbs/acre .......................... 0.62 0.07 NA 11.94 0.49 0.06 NA 1.22 2.87 28.74 0.51 0.06 NA 8.04 0.38 0.02 NA 0.99 0.52 22.71 . 36 34 NA 1,338 267 15 NA 374 89 2,498 1 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1-7 **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RAf4jQ rnRna I:cF t1w9nnai ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehie Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized: 24.60 Owner: von Drehle Corporation Annual Dry Tons Applied: 663.26 Site #: 6A Acres Permitted: 24.60 Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A 0 o w fD Specify Totals Per Acre o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry' Wet, Precip Past 24 Hrs. Inches n K n 2 _. Zr F. c ;0 = m :� G o' a o w R i o o TKN m z a B '0 a n �. m Nitrate and Nitrite m W k PAN Applied pp (Ibs/acre) Must Select Crop 1 or Crop 2 7-7 ffinGal. Crop 1 Crop 2 Crop 1 Crop 2 Nov-20 1,568.00 63.74 42.30 26.96 von Drehie Paper INC 1.00 0.40 1940.00 4.50 1.87 42.09 X TOTALS: 64 As Cd Cr Cu Pb He Mo Ni Se Zn P PAN I PAN 2 Lime ADvlied Annuallbs/acre 0.10 0.01 0.00 1.73 0.10 0.04 0.31 0.20 0.10 4.01 0.19 42.09 0.00 Date lbs/ac Current Cumulative lbs/acre .......................... 0.40 0.97 NA 9.25 0.46 0.08 NA 1.47 0.42 34.79 :: 0.30 0.95 NA 7.53 0.36 0.04 NA 1.27 0.32 30.79 36 34 NA 1,338 267 15 NA 374 89 2,498 F 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Zz Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rip Fnpne 1=cF ri,;nnnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized: 37.50 Owner: von Drehle Corporation Annual Dry Tons Applied: 1,075.01 Site #• 6B Acres Permitted: 37.50 Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o o Specify Totals Per Acre e, ,o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc.) Site Cond. (� Wet, Moist) Preci p' Past 24 Hrs. Inches a 3 9 a _. °a w - c : N m ° > 70 ev = ; w > TKN mWkg z a = a w a ? w' mg&& Nitrate and Nitrite mWkL PAN Applied PP (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Oct-20 1.617.00 43.12 37.00 1 15.95 von Drehle Paper INC 1.00 0.40 3.64 44.10 14.23 1.34 X Nov-20 1,127.00 30.05 42.30 12.71 von Drehle Paper INC 1.00 0.40 1940.00 4.50 1.87 19.85 X TOTALS: 73 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 2.96 0.11 0.04 0.33 0.22 1.34 5.21 0.23 21.19 1 0.00 Date lbs/ac Current Cumulative lbs/acre 0.41 0.96 NA 10.14 0.45 0.06 NA 1.45 1.65 35.78 0.30 0.94 NA 7.18 0.35 0.02 NA 1.23 0.32 30.57 36 34 NA 1,338 267 15 NA 374 89 2,498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop -I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation �l**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading 14KR FORM F.RF t12/2nnF1 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 19.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 470.62 Site #: I Acres Permitted: 19.10 Operator: von Drehle Corporation Predominat Soil Series Tbg Cation Exchange Capacity (non 503): NA Crop I Name: Wheat Crop I Max PAN: 108.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A K O _ c �- 0 :. Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. Inches 3 s = °n °: � c ' c X _: � = _ 0 o M R " : m o =3 TKN mWkg Z Y .� a a a ? p' mWku Nitrate and Nitrite mgtkg PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons _ Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jun-20 1,470.00 1 76.96 30.20 1 23.24 von Drehlc Paper INC 1.00 0.40 86.00 64.00 3.73 3.56 X Jul-20 73.50 3.85 36.30 1.40 von Drehle Paper INC 1.00 0.40 91.20 2.65 1.82 0.11 X TOTALS: 81 As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.12 0.01 0.00 0.83 0.12 0.04 0.36 0.24 0.12 4.65 2.26 3.67 0.00 Date lbs/ac Current Cumulative lbs/acre 0.76 0.23 NA 5.42 0.45 0.12 NA 1.44 L16 25.95 0.64 0.22 NA 4.59 0.33 0.08 NA 1.20 1.04 21.30 36 34 NA 1 1,338 267 IS 1 NA 374 89 1 2,498 1 108.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** 1 Permit PAN Limit Ist/2nd Crop "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2 O-3 Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R1qWR FnRM FRF ri919nrwn ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #• 4 Acres Utilized: 37.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 1,106.47 Site #• 2 Acres Permitted: 37.10 Operator: von Drehle Corporation Predominat Soil Series T66 Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 108.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A _ C7 50 <: Specify Totals Per Acre /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, yet Moist) Precip Past 24 Hrs. Inches o 3 9 T n. a w a _• o X E � w . N . o ay " R TKN m • z Y ... 3 o c f9 o m m • Nitrate and Nitrite m • k • PAN Applied PP (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Re n p° Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jun-20 1,543.50 41.60 30.20 12.56 von Drehle Paper INC 1.00 0.40 86.00 64.00 3.73 1.92 X Jul-20 1,764.00 47.55 36.30 17.26 von Drehle Paper INC 1.00 0.40 91.20 2.65 1.82 1.38 X TOTALS: 89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.13 0.01 0.00 0.92 0.13 0.04 0.40 0.27 0.13 5.42 4.82 3.30 0.00 Date I Ibs/ac Current Cumulative Ibs/acre 0.63 0.18 NA 5.80 0.51 0.12 NA 1.20 1.16 26.22 0.49 0.17 NA 4.88 0.38 0.08 NA 0.94 1.03 20.80 36 34 NA 1,338 267 1 15 1 NA 1 374 1 89 1 2,498 108.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 03, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R!,ip CAPRA cac m,)P;nna% ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 22.40 Owner: von Drehlc Corporation Annual Dry Tons Applied: 759.67 Site M 3 Acres Permitted: 22.40 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop I Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A t7 O m fD 50 Specify Totals Per Acre u Solids As Decimal Volume Applied per Acre DTiAc Residual Sources (NPDES #, WQ#, Fert.,Animal Waste, etc.) Site Cond. (Dry Wet, Moist 1 Precip Past 24 Hrs. Inches o 3 a S C w 0. •o• = c ;a _: � + N w :e a R is * •_ 0' TKN -Wkg Z a - 3 w'o c f9 w m k 1 Nitrate and Nitrite m• k g PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Apr-20 1,269.27 56.66 35.50 20.12 von Drehle Paper INC 1.00 0.40 579.00 2.55 1 14.48 9.96 X May-20 1,023.44 45.69 30.20 13.80 von Drehle Paper INC 1.00 0.40 86.00 64.00 3.73 2.11 X TOTALS: 102 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.15 0.02 0.00 1.24 0.15 0.05 0.45 0.30 0.15 9.37 1.19 12.07 0.00 Date lbs/ac Current Cumulative Ibs/acre .......................... 0.40 0.08 NA 5.80 0.41 0.09 NA 1.07 0.54 23.35 0.25 0.07 NA 4.56 0.26 0.04 NA 0.77 1 0.39 13.98 36 34 NA 1,338 267 IS NA 374 1 89 1 2,498 FIT 1.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2 Z **Volitilization Rate: Surface - 0.5, InjectionAncorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 03, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RAftJR MRM FRF 117/9(11161 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 50.80 Owner: von Drehle Corporation Annual Dry Tons Applied: 1,276.78 Site #: 4 Acres Permitted: 50.80 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop I Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o s Specify Totals Per Acre • Solids As Decimal Volume Applied per Acre DT'Ac Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc 1 Site Cond. (Dry Wet, Moist) Precip Past 24 Hrs. Inches e V R- �. ° m a o. c _: N o > � w > TKN m Z a -: 9 OQ c fD o • m• k Nitrate and Nitrite m- k, PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Cro 1 p Cio 2 p Cio 1 p Cro 2 p May-20 4,170.06 82.09 30.20 24.79 von Drehle Paper INC 1.00 0.40 86.00 64.00 3.73 3.79 X Jul-20 48.00 1 0.94 36.30 0.34 von Drehle Paper INC 1.00 0.40 91.20 2.65 1.82 0.03 X TOTALS: 83 As Cd Cr Cu Pb He Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 0.85 0.12 0.04 0.37 0.25 0.12 4.76 2.16 3.82 0.00 Date lbs/ac Current Cumulative lbs/acre 0.58 0.16 NA 6.92 0.52 0.12 NA 1.52 0.59 27.87 0.46 0.15 NA 6.08 0.40 0.07 NA 1.27 0.46 23.11 36 34 NA 1,338 267 15 NA 374 89 2,498 111.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Z-2e"Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Annerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading P4^p Fnpm FCF /19/2nnai ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 11.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 272.47 Site #: 5 Acres Permitted: 11.10 Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o fD E- o Specify Totals Per Acre o o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc.) Site Cond. (Dry' wct� Moist) Precip. Past 24 Hrs. Inches > -o �? _ o w a= c m = m + N * w 0 5 � " d w s w Es, 7 TKN m W k g Z Y o 3 a, c a I m• k Nitrate and Nitrite m W k g PAN Applied pp (lbs/acre) Must Select Crop I or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop I Crop 2 Crop I Crop 2 May-20 902.22 81.28 30.20 24.55 von Drehle Paper INC 1.00 0.40 86.00 64.00 3.73 3.76 X TOTALS: 81 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual lbs/acre 0.12 0.01 0.00 0.83 0.12 0.04 0.36 0.24 0.12 4.65 2.06 3.76 0.00 Date lbs/ac Current Cumulative lbs/acre 0.52 0.99 NA 7.33 0.42 0.09 NA 1.74 0.75 27.34 0.40 0.98 NA 6.50 0.30 0.05 NA 1.50 0.63 22.68 36 34 NA 1,338 267 15 NA 374 89 2,498 1 111.001 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R Wp FnRae FCF riwnnnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 19.20 Owner: von Drehle Corporation Annual Dry Tons Applied: 489.14 Site #: 7 Acres Permitted: 19.20 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop I Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A t7 fD S eci Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste etc.) Site Cond. (Dry' Wet Moist) precip. Past 24 Hrs. Inches K v s _. ° p "• o• ° w m ° � " a : TKN mgikg Z > a a a > 2. w mWkg Nitrate and Nitrite mWkL PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons _ Cu.Yd. Report �o Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jul-20 1,347.50 70.18 36.30 25.48 von Drehle Paper INC 1 1.00 0.40 1 91.20 2.65 1.82 2.03 X TOTALS: 70 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.11 0.01 0.00 0.73 0.11 0.03 0.32 0.21 0.11 4.48 5.55 2.03 0.00 Date lbs/ac Current Cumulative Ibs/acre .......................... 0.53 1.02 NA 7.27 0.32 0.08 NA 1.49 1.04 24.33 0.43 I.01 NA 6.54 0.21 0.04 NA 1.28 0.94 19.85 36 34 NA 1,338 267 15 NA 374 89 2,498 I 111.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 6< Z ,/ 2 Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ` Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RJ R Fntzha FCF 11 g/gnom ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 28.90 Owner: von Drehle Corporation Annual Dry Tons Applied: 844.88 Site #: 8 Acres Permitted: 28.90 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop I Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o 5r Specify Totals Per Acre , c Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, Wet, Moist) Precip Past 24 Hrs. Inches v v z = 0 m aR. ' c 7' _: M m N o > R ' 0' > TKN mg/kg Z a 3 o'oo c " -Wkg Nitrate and Nitrite mgfkg PAN Applied (Ibs/acre) Must Select Crop I or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Aug-20 2,327.50 80.54 36.30 29.23 von Drehle Paper INC 1.00 0.40 91.20 2.65 1.82 2.33 X TOTALS: 81 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 0.84 0.12 0.04 0.36 0.24 0.12 5.14 6.37 2.33 0.00 Date lbs/ac Current Cumulative Ibs/acre .......................... 0.57 1.04 NA 7.42 0.34 0.09 NA 1.88 1.04 27.10 0.45 1.02 NA 6.58 0.21 0.05 NA 1.64 0.92 21.96 36 34 NA 1,338 267 15 NA 374 89 2,498 111.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation z Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading P4ftp FnRM FCF r12/gnnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 28.60 Owner: von Drehle Corporation Annual Dry Tons Applied: 844.88 Site #: 9 Acres Permitted: 28.60 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A o $ specify Totals Per Acre o Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. Inches 3 .a a C n a o 0 w N . w o• � x+ 5 o. � TKN mg/kg z a 9 a c n o R. m k Nitrate and Nitrite m k PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals to Gal. Crop 1 p Crop 2 p Crop 1 p Crop 2 p Jul-20 2,327.50 1 81.38 36.30 29.54 von Drehle Paper INC 1.00 0.40 91.20 2.65 1 1.82 2.36 X TOTALS: 81 As Cd Cr Cu Pb HR Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 0.84 0.12 0.04 0.37 0.25 0.12 5.19 6.44 2.36 0.00 Date lbs/ac Current Cumulative lbs/acre .......................... 0.66 1.06 NA 6.65 0.30 0.09 NA 1.65 1.07 26.66 0.54 I.04 NA 5.81 0.18 0.05 NA 1.41 0.95 21.47 36 34 NA 1,338 267 1 15 NA 374 89 2,498 Il t 1.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2 **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 11 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading � R01 R Ff1RM FCFl19Mnr1R1 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 18.90 Owner: von Drehle Corporation Annual Dry Tons Applied: 537.04 Site #: 6A Acres Permitted: 18.90 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop 1 Name: Wlieat Crop 1 Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A c R f° Soccify Totals Per Acre eo Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc. Site Cond. (Dry' Wet, Most) Preci p Past 24 Hrs. tones a a -. R a o• c m • ^ o x' �° w ,*, K > TKN m Z Y 3 oo c o w in. e Nitrate and Nitrite m . k PAN Applied (Ibs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Aug-20 980.00 51.85 36.30 18.82 von Drehle Paper INC 1.00 0.40 91.20 2.65 1.82 1.50 X Sep-20 490.00 25.93 37.00 9.59 von Drehlc Paper INC 1.00 0.40 3.64 44.10 14.23 0.81 X TOTALS: 78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 1.83 0.12 0.04 0.35 0.23 0.85 5.30 4.19 2.31 0.00 Date lbs/ac Current Cumulative lbs/acre 0.82 1.11 NA 7.46 0.41 0.08 NA 1.66 1.91 26.34 0.71 I.10 NA 5.64 0.29 0.05 NA 1.43 1.06 21.03 36Tl:34 NA 1 1,338 267 1 15 NA 1 374 89 2,498 I l l l.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date 'Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 03, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading RAtS,R FnRee Fcr= r, wmnm ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 19.30 Owner: von Drehle Corporation Annual Dry Tons Applied: 569.18 Site #: 6B Acres Permitted: 19.30 Operator: von Drehle Corporation Predominat Soil Series ThA Cation Exchange Capacity (non 503): NA Crop 1 Name: Wheat Crop l Max PAN: 111.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A $ O O Er Totals Per Acre , /o Solids As Decimal Volume Applied per Acre DTiAc Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry Wet Moist) Prccip. Past 24 Hrs. 1.1. K M a �. G m o a 2. w N a g m TKN m� k Z Y ' a a c `° ' m W k g Nitrate and Nitrite m• PAN A lied pp (lbs/acre) Must Select Crop I or Crop 2 Wei Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Aug-20 1,568.00 81.24 36.30 29.49 von Drehle Paper INC 1.00 1 0.40 91.20 2.65 1 1.82 2.35 X TOTALS: 81 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual lbs/acre 0.12 0.01 0.00 0.84 0.12 0.04 0.37 0.24 0.12 5.18 6.43 2.35 0.00 Date Ibs/aC Current Cumulative lbs/acre .......................... 0.87 1.11 NA 6.54 0.42 0.09 NA 1.73 1.19 27.95 0.75 1.10 NA 5.70 0.29 0.05 NA 1.49 1.06 22.77 36 34 NA 1,338 267 15 NA 374 89 2,498 111.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit I st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 2Z� "V *Application Method: S - Surface, IN - Injection, INC - Incorporation *Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading P4R Enna rcF mq/gnnm RESIDUAL ANALYSIS LAB SHEETS 6)MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Wednesday, December 25, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 10 VMICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 12/16/2019 Cordova, NC 28330 Reported: 12/25/2019 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, K91-0301-01 Solid Grab 12/16/19 10:35 12/16/19 12:49 Grab Page 2 of 10 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K91-0301-01 Collection Date: 12/16/2019 10:35 Calculation Plant Available Nitrogen EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N SM 2540 G-2011 % Solids SM 4500 NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Calculation Sodium Adsorption Ratio, SAR EPA 9045 D pH at 25 °C SM 4500 P F-2011 Phosphorus, Total (as P) General Parameters ASTM D2216-10 Percent Solids Total Metals - AA EPA 7471A Mercury Total Metals - ICP EPA 601 OD Aluminum Result RL Units Dilution Note Prepared Analyzed Analyst 146 mg/kg 1 12/24/19 1412 12/24/19 1412 BNS 1.59 0.0685 mg/kg dry 1 12/17/19 1508 12/24/19 1210 VAA 0.37 1.37 mg/kg dry 1 12/17/19 1508 12/24/19 1210 VAA 36.5 1.00 % 1 12/17/19 1011 CLB <2.74 2.74 mg/kg dry 1 y 12/21/19 1251 MT 482 1.37 mg/kg dry 1 12/17/19 0854 TBM Result RL Units Dilution Note Prepared Analyzed Analyst 0.430 NA 1 12/24/19 1412 12/24/19 1412 BNS 7.9 1 0 S U 1 H 12/19/19 1321 CLB 0.74 0.069 mg/kg dry 1 12/24/19 1120 VAA Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 38.1 1.00 % (by wt.) 1 y 12/18/19 1131 12/19/19 0635 .1ST Result RL Units Dilution Note Prepared Analyzed Analyst <0.261 0.261 mg/kg dry 1 J 12/19/19 0718 12/19/19 1422 TMM Result RL Units Dilution Note Prepared Analyzed Analyst 819 38.2 mg/kg dry 1 y 12/19/19 0959 12/20/19 1242 JYH Microbac Laboratories. Inc 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 10 0�iMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K91-0301-01 Collection Date: 12/16/2019 10:3 Total Metals - ICP Result RL Units Dilution Note Prepared Analyzed Analyst Arsenic <1.91 1.91 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Cadmium <0.191 0.191 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Calcium 239000 9560 mg/kg dry 100 D3, Y 12/19/19 0959 12/20/19 1322 JYH Copper 24.6 1.91 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Lead <1.91 1.91 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Magnesium 2040 47.8 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Molybdenum <5.74 5.74 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Nickel <3.82 3.82 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Potassium <95.6 95.6 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Selenium <1.91 1.91 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Sodium 1090 47.8 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Zinc 74.8 1.91 mg/kg dry 1 Y 12/19/19 0959 12/20/19 1242 JYH Microbac Laboratories Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 10 )MICROBACr Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Result RL Batch KL91627 - Wet Chem Solid - SM 2540 G-2011 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Blank (KL91627-BLK1) Prepared &Analyzed: 12/17/2019 % Solids <1.00 1.00 % Duplicate (KL91627-DUP1) Source: K91-0216-05 Prepared & Analyzed: 12/17/2019 % Solids 93.6 1.00 % 93.6 0.02 10 Batch KL91933 - Wet Chem Solid - SM 4500 NH3 C-2011 Blank (KL91933-BLK1) Prepared &Analyzed: 12/21/2019 Ammonia as N <1.00 1.00 mg/kg wet Blank (KL91933-BLK2) Prepared & Analyzed: 12/21/2019 Ammonia as N <1.00 1.00 mg/kg wet Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch 1391-1105 - Wet-Solids-S - ASTM D2216-10 Blank (139L1105-BLK7) Prepared: 12/18/2019 Analyzed: 12/19/2019 Percent Solids 100 1.00 % (by wt.) LCS (1391-1105-13SI) Prepared: 12/18/2019 Analyzed: 12/19/2019 Percent Solids 79.6 % (by 80.0 99.5 90-110 wt.) Duplicate (1391-1105-DUP1) Source: M91-1102-01 Prepared: 12/18/2019 Analyzed: 12/19/2019 Percent Solids 1.31 1.00 % (by 1.38 5.18 10 wt.) Total Metals -AA Result MDL RL Batch B91-1172 - 7471 - EPA 7471A Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Blank (B9L1172-BLK1) Prepared & Analyzed: 12/19/2019 Mercury <0.00417 0.00417 0.104 mg/kg wet LCS (1391-1172-13S1) Prepared &Analyzed: 12/19/2019 Mercury 0.289 0.00417 0.104 mg/kg 0.267 108 80-120 wet LCS Dup (B9L1172-BSD1) Prepared &Analyzed: 12/19/2019 Mercury 0.267 0.00417 0.104 mg/kg 0.267 100 80-120 7.70 20 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 5 of 10 Total Metals - AA Batch 1391-1172 - 7471 - EPA 7471A MIICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Spike Source %REC RPD Result MDL RL Units Level Result %REC Limits RPD Limit Notes Post Spike (691-1172-PS1) Source: M91-1184-01 Prepared & Analyzed: 12/19/2019 Mercury 0.781 ug/L 1.00 -0.107 78.1 80-120 M5 Post Spike (1391-1172-PS2) Source: K91-0301-01 Prepared & Analyzed: 12/19/2019 Mercury 1.89 ug/L 1.00 0.725 117 80-120 Spike Source %REC RPD Total Metals - ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch 1391-1188 - 3051A 6010 - EPA 6010D Blank (1391-1188-BLK1) Prepared: 12/19/2019 Analyzed: 12/20/2019 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (891-1188-13SI) Prepared: 12/19/2019 Analyzed: 12/20/2019 Aluminum 243 20.0 mg/kg 250 97.3 80-120 wet Arsenic 9.27 1.00 mg/kg 10.0 92.7 80-120 wet Cadmium 1.22 0.100 mg/kg 1.25 97.2 80-120 wet Calcium 248 50.0 mg/kg 250 99.1 80-120 wet Copper 12.4 1.00 mg/kg 12.5 98.9 80-120 wet Lead 12.3 1.00 mg/kg 12.5 98.2 80-120 wet Magnesium 246 25.0 mg/kg 250 98.4 80-120 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 10 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Spike Source %REC RPD Total Metals - ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch 1391_1188 - 3051A 6010 -EPA 6010D LCS (B9L1188-BS1) Prepared: 12/19/2019 Analyzed_: 12/20/2019 Molybdenum 26.0 3.00 mg/kg 25.0 104 80-120 wet Nickel 12.5 2.00 mg/kg 12.5 99.9 80-120 wet Potassium 1240 50.0 mg/kg 1250 99.1 80-120 wet Selenium 9.28 1.00 mg/kg 10.0 92.8 80-120 wet Sodium 1250 25.0 mg/kg 1250 100 80-120 wet Zinc 24.1 1.00 mg/kg 25.0 96.2 80-120 wet LCS Dup (B9L1188-BSD1) Prepared: 12/19/2019 Analyzed: 12/20/2019 Aluminum 239 20.0 mg/kg 250 95.6 80-120 1.75 wet Arsenic 9.19 1.00 mg/kg 10.0 91.9 80-120 0.813 wet Cadmium 1.20 0.100 mg/kg 1.25 95.7 80-120 1.58 wet Calcium 241 50.0 mg/kg 250 96.4 80-120 2.83 wet Copper 12.2 1.00 mg/kg 12.5 97.8 80-120 1.11 wet Lead 12.3 1.00 mg/kg 12.5 98.5 80-120 0.301 wet Magnesium 241 25.0 mg/kg 250 96.5 80-120 1.97 wet Molybdenum 25.8 3.00 mg/kg 25.0 103 80-120 0.694 wet Nickel 12.4 2.00 mg/kg 12.5 99.2 80-120 0.755 wet Potassium 1200 50.0 mg/kg 1250 96.3 80-120 2.87 wet Selenium 9.54 1.00 mg/kg 10.0 95.4 80-120 2.74 wet Sodium 1220 25.0 mg/kg 1250 97.5 80-120 2.88 wet Zinc 24.0 1.00 mg/kg 25.0 95.8 80-120 0.444 wet Post Spike (891-1188-PSI) Source: M91-1184-01 Prepared: 12/19/2019 Analyzed: 12/20/2019 Aluminum 41.4 mg/L 5.00 37.1 85.8 80-120 Arsenic 0.325 mg/L 0.200 0.137 94.0 80-120 Cadmium 0.0261 mg/L 0.0250 0.00253 94.4 80-120 Calcium 398 mg/L 5.00 388 186 80-120 Copper 0.443 mg/L 0.250 0.211 92.9 80-120 Lead 0.370 mg/L 0.250 0.142 91.2 80-120 Magnesium 29.8 mg/L 5.00 25.6 83.1 80-120 Molybdenum 0.514 mg/L 0.500 0.0160 99.6 80-120 Nickel 0.476 mg/L 0.250 0.245 92.6 80-120 Microbac Laboratories, Inc. 20 20 20 20 20 20 20 20 20 20 20 20 20 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 7 of 10 iMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Spike Source %REC RPD Total Metals - ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch 691-1188 - 3051A 6010 - EPA 6010D Post Spike (1391-1188-13SI) Source: M9L1184-01 Prepared: 12/19/2019Analyzed: 12/20/2019 Potassium 26.3 mg/L 25.0 2.52 94.9 80-120 Selenium 0.140 mg/L 0.200 -0.0536 70.0 80-120 Sodium 24.3 mg/L 25.0 0.491 95.2 80-120 Zinc 0.963 mg/L 0.500 0.512 90.1 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 10 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9L0301 Definitions %: Percent % (by wt.): Percent by Weight D3: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time J: The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample. M5: Post digestion spike is outside of acceptance limits. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 18.2°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to t applicable accreditation standard unless otherwise noted. l The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 12/25/2019 23:37 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 10 `K9L0301' _ Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-8774 CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME S ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 POq PROJECT I LOCATION: Cordova - 60-day series /OF a o r T L E S TYPE OF ANALYSIS PRESERVATION CODE E m lD E C E Q 3 E a) W V a Q CL oa () E U > 'N (D m 2 � > '2 iin a0 - YKa Z U' c 1N) E '— 05 Q N O Z o Z � Z a o a i— z N n W In �o h o CODE: A = None B = HNO3 (pH<2)+ <4°C C = H2SO4 (pH«) + u1°c D = NaOH + <4°C E = ZN Acetate + <4°C F= HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: Lt i. l 4 I I +�'1 ! t r' 4 DATE I METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME coMP GRAB PH D.o. TEMP •c CHLORINE Residual from paper plant f �� ) b: X 2 A A AI A I A I A A A A t 1 A A A A A A A A A in Resin tl Data Tlma _ RecaWad by: (Signature) r Date Time in fished by: Date Time Received by: (Signature) Date Time 3 4 Relinquished by: Date ime Received by: ISggnatura) Data Tima 5 6 Comments or Special Hazards REV4 c ' Page 10 of 10 ( DMICRORAC R Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Friday, February 28, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 10 V MI ICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOBO221 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 02/17/2020 Cordova, NC 28330 Reported: 02/28/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOB0221-01 Solid Grab 02/17/20 11:05 02/17/20 11:33 Grab Page 2 of 10 {_WMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0221-01 Collection Date: 02/17/2020 11:05 Inorganics Total Calculation Sodium Adsorption Ratio, SAR EPA 9045 D pH at 25 °C SM 4500 P F-2011 Phosphorus, Total (as P) General Parameters Calculation Plant Available Nitrogen EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N SM 2540 G-2011 % Solids SM 4500 NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen General Parameters ASTM D2216-10 Percent Solids Metals Total by AA EPA 7471 A Mercury Metals Total by ICP EPA 6010D Aluminum Result 0.560 7.6 RL Units Dilution Note Prepared Analyzed Analyst NA 1 02/27/20 1334 02/27/20 1334 BNS 1.0 S.U. 1 02/25/20 1531 VAA 0.86 0.064 mg/kg dry 1 02/27/20 1120 VAA Result RL Units Dilution Note Prepared Analyzed Analyst 176 mg/kg 1 02/27/20 1334 02/28/20 1401 BNS 1.78 0.637 mg/kg dry 1 02/18/20 1757 02/20/20 1030 VAA <12.7 12.7 mg/kg dry 1 02/18/20 1757 02/20/20 1030 VAA 39.2 1.00 % 1 02/17/20 1415 TBM <2.55 2.55 mg/kg dry 1 Y 02/18/20 1014 VAA 579 0.500 mg/kg 1 02/26/20 1125 JAW Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 35.5 1.00 % (by wt.) 1 Y 02/19/20 0729 02/20/20 0545 CB Result RL Units Dilution Note Prepared Analyzed Analyst <0.653 0.653 mg/kg dry 1 02/24/20 0701 02/25/20 1357 TMM Result RL Units Dilution Note Prepared Analyzed Analyst 1120 41.2 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 10 VMICROBAC'!i Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0221-01 Collection Date: 02/17/2020 11:05 Metals Total by ICP Result RL Units Dilution Note Prepared Analyzed Analyst Arsenic <2.06 2.06 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Cadmium <0.206 0.206 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Calcium 186000 10300 mg/kg dry 100 D3, Y 02/21/20 0906 02/21/20 1603 JYH Copper 19.3 2.06 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Lead <2.06 2.06 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Magnesium 1650 51.6 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Molybdenum <6.19 6.19 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Nickel <4.12 4.12 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Potassium <103 103 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Selenium <2.06 2.06 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Sodium 1240 51.6 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Zinc 168 2.06 mg/kg dry 1 Y 02/21/20 0906 02/21/20 1516 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 10 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source General Parameters Result RL Units Level Result %REC Batch KBO1432 - Wet Chem Solid - SM 2540 G-2011 %REC Limits RPD RPD Limit Notes Blank (KBO1432-BLK1) Prepared & Analyzed: 02/17/2020 % Solids <1.00 1.00 % Duplicate (KBO1432-DUP7) Source: KOB0204-09 Prepared & Analyzed: 02/17/2020 % Solids 94.1 1.00 % 94.0 0.1 10 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOB0892 - Wet-Solids-S - ASTM D2216-10 Blank (130130892-131-K1) Prepared: 02/19/2020 Analyzed: 02/20/2020 Percent Solids 100 1.00 % (by wt.) LCS (130130892-13W) Prepared: 02/19/2020 Analyzed: 02/20/2020 Percent Solids 78.9 % (by 80.0 98.7 90-110 wt.) Duplicate (BOB0892-DUP1) Source: MOB1005-21 Prepared: 02/19/2020 Analyzed: 02/20/2020 Percent Solids 99.2 1.00 % (by 99.2 0.0159 10 wt.) Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOB1140 - 7471 -EPA 7471A Blank (BOB 1140-BLK1) Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOB1140-BS1) Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury <0.250 0.250 mg/kg 0.267 86.8 80-120 wet Matrix Spike (BOB1140-MS1) Source: MOB1171-02 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 0.316 0.275 mg/kg 0.293 ND 108 75-125 dry Matrix Spike Dup (BOB1140-MSD1) Source: MOB1171-02 Prepared' 02/24/2020 Analyzed: 02/25/2020 Mercury <0.276 0.276 mg/kg 0.294 ND 93.7 75-125 13.7 20 dry Post Spike (BOB1140-PS1) Source: MOB1105-01 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 1.01 ug/L 1.00-0.0701 101 80-120 Post Spike (BOB1140-PS2) Source: MOB1171-02 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 1.07 ug/L 1.00 0.0555 101 80-120 Post Spike (BOB1140-PS3) Source: MOB1173-01 Prepared: 02/24/2020 Analyzed: 02/25/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 10 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOB1140 - 7471 - EPA 7471A Post Spike (BOB1140-PS3) Source: MOB1173-01 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 1.79 ug/L 1.00 0.593 119 80-120 Post Spike (BOB1140-PS4) Source: KOB0221-01 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 1.16 ug/L 1.00 0.0489 111 80-120 Post Spike (BOB1140-PS5) Source: MOB1606-01 Prepared: 02/24/2020 Analyzed: 02/25/2020 Mercury 1.07 ug/L 1.00-0.0423 107 80-120 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOB1078 - 3051A 6010 -EPA 601 OD Blank (BOB1078-BLK1) Prepared &Analyzed: 02/21/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOB1078-BS1) Prepared &Analyzed: 02/21/2020 Aluminum 228 20.0 mg/kg 250 91.3 80-120 wet Arsenic 8.92 1.00 mg/kg 10.0 89.2 80-120 wet Cadmium 1.14 0.100 mg/kg 1.25 91.5 80-120 wet Calcium 232 50.0 mg/kg 250 92.8 80-120 wet Copper 11.6 1.00 mg/kg 12.5 92.9 80-120 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 10 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Metals Total by ICP Result Batch BOB1078 - 3051A 6010 - EPA 6010D RL Spike Units Level Source Result %REC %REC Limits RPD RPD Limit Notes LCS (13081078-13SI) Prepared &Analyzed: 02/21/2020 Lead 11.7 1.00 mg/kg 12.5 93.4 80-120 wet Magnesium 233 25.0 mg/kg 250 93.1 80-120 wet Molybdenum 24.7 3.00 mg/kg 25.0 99.0 80-120 wet Nickel 11.9 2.00 mg/kg 12.5 94.9 80-120 wet Potassium 1140 50.0 mg/kg 1250 91.5 80-120 wet Selenium 8.90 1.00 mg/kg 10.0 89.0 80-120 wet Sodium 1150 25.0 mg/kg 1250 92.0 80-120 wet Zinc 22.9 1.00 mg/kg 25.0 91.5 80-120 wet Matrix Spike (BOB1078-MS1) Source: MOB1171-02 Prepared &Analyzed: 02/21/2020 Aluminum 5800 16.3 mg/kg 203 2850 NR 75-125 dry Arsenic 13.0 0.813 mg/kg 8.13 5.84 87.6 75-125 dry Cadmium 1.56 0.0813 mg/kg 1.02 0.803 74.7 75-125 dry Calcium 27100 40.7 mg/kg 203 29600 NR 75-125 dry Copper 21.8 0.813 mg/kg 10.2 12.0 96.3 75-125 dry Lead 20.2 0.813 mg/kg 10.2 9.86 101 75-125 dry Magnesium 3320 20.3 mg/kg 203 2450 430 75-125 dry Molybdenum 20.6 2.44 mg/kg 20.3 2.65 88.4 75-125 dry Nickel 20.3 1.63 mg/kg 10.2 11.2 89.4 75-125 dry Potassium 2480 40.7 mg/kg 1020 991 147 75-125 dry Sodium 1030 20.3 mg/kg 1020 144 87.5 75-125 dry Matrix Spike Dup (BOB1078-MSD1) Source: MOB1171-02 Prepared &Analyzed: 02/21/2020 Aluminum 5660 16.9 mg/kg 211 2850 NR 75-125 2.40 20 dry Arsenic 13.9 0.845 mg/kg 8.45 5.84 95.8 75-125 7.21 20 dry Cadmium 1.59 0.0845 mg/kg 1.06 0.803 74.9 75-125 2.01 20 dry Calcium 34500 42.3 mg/kg 211 29600 NR 75-125 24.2 20 dry Copper 23.2 0.845 mg/kg 10.6 12.0 106 75-125 6.23 20 dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 10 .i M ICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOB1078 - 3051 A6010 - EPA 601OD Matrix Spike Dup (8081078-MSD1) Source: MOB1171-02 Prepared &Analyzed: 02/21/2020 Lead 19.5 0.845 mg/kg 10.6 9.86 90.9 75-125 3.48 20 dry Magnesium 3490 21.1 mg/kg 211 2450 493 75-125 4.91 20 dry Molybdenum 22.4 2.54 mg/kg 21.1 2.65 93.7 75-125 8.47 20 dry Nickel 24.8 1.69 mg/kg 10.6 11.2 129 75-125 20.2 20 dry Potassium 2760 42.3 mg/kg 1060 991 168 75-125 10.7 20 dry Selenium 5.21 0.845 mg/kg 8.45 ND 61.6 75-125 1.46 20 dry Sodium 1100 21.1 mg/kg 1060 144 91.0 75-125 6.69 20 dry Zinc 69.3 0.845 mg/kg 21.1 42.2 128 75-125 1.75 20 dry Post Spike (6081078-PS1) Source: MOB1272-01 Prepared & Analyzed: 02/21/2020 Aluminum 337 mg/L 5.00 328 179 80-120 Arsenic 0.445 mg/L 0.200 0.260 92.4 80-120 Cadmium 0.0201 mg/L 0.0250 -0.00253 80.4 80-120 Calcium 11.6 mg/L 5.00 6.79 96.8 80-120 Copper 0.249 mg/L 0.250 0.0246 89.9 80-120 Lead 0.254 mg/L 0.250 0.0280 90.5 80-120 Magnesium 11.5 mg/L 5.00 6.60 98.1 80-120 Molybdenum 0.503 mg/L 0.500 0.0134 98.0 80-120 Nickel 0.267 mg/L 0.250 0.0374 91.7 80-120 Potassium 24.5 mg/L 25.0 1.40 92.6 80-120 Selenium 0.212 mg/L 0.200 0.0279 92.0 80-120 Sodium 151 mg/L 25.0 123 113 80-120 Zinc 0.766 mg/L 0.500 0.305 92.1 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 10 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0221 Definitions %: Percent % (by wt.): Percent by Weight 1133: Dilution was performed due to high target analyte concentration. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 13.4°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certifications) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 02/28/2020 22:44 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 10 'KOB0221• { ate'. Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-87 CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME B ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 PO# PROJECTILOCATION: Cordova - 60-dayseries #OF a a T T L E S TYPE OF ANALYSIS PRESERVATION CODE = E W tr E C E = Q = C y U c � Q 0- o v E 2 U > (D m g _r j 'y y a - s U Z _ O N E 0 w CO Z o Z co Z Z a o a I— F c. Ol a V) o ~ o CODE: A = None B = HNO3 (pH<2) + <4`C C = H2SO4 (pH<2) + <4°C D= NaOH + <4°C E= ZN Acetate + <4°C F= HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 gpMP, co M �vv uh DATE / METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB PHI D.O. TEMP •C CHLORINE 0-1 Residual from paper plant '/ L/ 1 T O (I � D S X 2 A A A A A A A A A Z- 1 A A A A A A A A A ReD ad Date Time RecoW d try: ('nature) Oal Tim. 1 ZIj9'L� ?�U7 2 n I�� R utshad by. Date Time Raeehed by: (signature) Data Ttme 011 3 4 ReRnquishad by: Data Time Ra.eWed by: (Signature) Oat. Time 5 6 Comments or Special Hazards: REVIEWED Page 10 of 16 VMICROBAC R Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Friday, May 8, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 13 Revised Report: Amended for reanalysis of test. Von Drehle Corporation Mr. Chris Fowler 126 First Street Cordova, NC 28330 Sample Summary Report V M ICROBAC-" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Project Name: Residuals Sample - 60 day Project / PO Number: N/A Received: 04/16/2020 Reported: 05/08/2020 Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOD0234-01 Solid Grab 04/16/20 12:12 04/16/20 12:50 Grab Page 2 of 13 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KODO234 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOD0234-01 Collection Date: 04/16/2020 12:12 Inorganics Total Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Sodium Adsorption Ratio, SAR 0.700 NA 1 04/28/20 2127 04/28/20 2128 BNS EPA 9045D pH at 25 °C 8.4 1.0 S.U. 1 H 04/16/20 1547 TBM SM 4500-P F-2011 Phosphorus, Total (as P) 42 0.83 mg/kg dry 1 04/17/20 1336 JAW General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Plant Available Nitrogen 27.9 mg/kg 1 04/28/20 2127 04/28/20 2128 BNS EPA 300.0, Rv. 2.1 (1993) Nitrate as N 2.08 0.0827 mg/kg dry 1 04/16/20 2316 JAW Nitrite as N <1.65 1.65 mg/kg dry 1 04/16/20 2316 JAW SM 2540 G-2011 % Solids 30.2 1.00 % 1 04/20/20 1335 MT SM 4500-NH3 C-2011 Ammonia as N <64.0 64.0 mg/kg dry 1 Y 04/22/20 1524 JAW SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 86.0 0.500 mg/kg 1 04/17/20 0843 TBM General Parameters ASTM D2216-10 Percent Solids Metals Total by AA EPA 7471A Mercury Metals Total by ICP EPA 6010E Aluminum Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 29.7 1.00 % (by wt.) 1 Y 04/30/20 1036 05/01/20 0545 ERP Result RL Units Dilution Note Prepared Analyzed Analyst <0.825 0.825 mg/kg dry 1 04/30/20 0626 05/01/20 1006 TMM Result RL Units Dilution Note Prepared Analyzed Analyst 981 48.9 mg/kg dry 1 04/30/20 0936 04/30/20 1346 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 13 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOD0234-01 Collection Date: 04/16/2020 12:12 Metals Total by ICP Result RL Units Dilution Note Prepared Arsenic <2.45 2.45 mg/kg dry 1 04/30/20 0936 Cadmium <0.245 0.245 mg/kg dry 1 04/30/20 0936 Calcium 168000 12200 mg/kg dry 100 D3 04/30/20 0936 Copper 16.9 2.45 mg/kg dry 1 04/30/20 0936 Lead <2.45 2.45 mg/kg dry 1 04/30/20 0936 Magnesium 1970 61.2 mg/kg dry 1 04/30/20 0936 Molybdenum <7.34 7.34 mg/kg dry 1 04/30/20 0936 Nickel <4.89 4.89 mg/kg dry 1 04/30/20 0936 Potassium <122 122 mg/kg dry 1 04/30/20 0936 Selenium <2.45 2.45 mg/kg dry 1 04/30/20 0936 Sodium 1480 61.2 mg/kg dry 1 04/30/20 0936 Zinc 94.8 2.45 mg/kg dry 1 04/30/20 0936 Analyzed Analyst 04/30/20 1346 JYH 04/30/20 1346 JYH 05/08/20 1436 KHL 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH 04/30/20 1346 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 13 VMICROBAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KODO234 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch KD01535 - Wet Chem Solid - EPA 9045D Duplicate (KDO1535-DUP1) pH at 25 °C 8.4 Source: KOD0234-01 Prepared & Analyzed: 04/16/2020 1.0 S.U. 8.4 0 10 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch KD01704 - Wet Chem Solid - SM 4500-Norg C-2011 Blank (KDO1704-BLK1) Prepared &Analyzed: 04/17/2020 Total Kjeldahl Nitrogen <0.500 0.500 mg/kg LCS (KDO1704-BSI) Prepared &Analyzed: 04/17/2020 Total Kjeldahl Nitrogen 28.6 0.500 mg/kg 30.0 95 90-110 Batch KD02322 - Wet Chem Solid - SM 2540 G-2011 Blank (KD02322-BLK1) Prepared &Analyzed: 04/20/2020 % Solids <1.00 1.00 % Duplicate (KD02322-DUP1) Source: KOD0234-01 Prepared &Analyzed: 04/20/2020 % Solids 30.6 1.00 % 30.2 2 10 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1666 - Wet-Solids-S -ASTM D2216-10 Blank (BOD1666-BLKI) Prepared: 04/30/2020 Analyzed: 05/01/2020 Percent Solids 100 1.00 % (by wt.) LCS (BOD1666-BSI) Prepared: 04/30/2020 Analyzed: 05/01/2020 Percent Solids 74.4 % (by 80.0 93.0 90-110 wt.) Duplicate (BOD1666-DUP1) Source: MOD1866-01 Prepared: 04/30/2020 Analyzed: 05/01/2020 Percent Solids 98.4 1.00 % (by 98.4 0.0388 10 wt.) Metals Total by AA Result RL Batch BOD1647 - 7471 -EPA 7471A Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Blank (BOD1647-BLK1) Prepared: 04/30/2020 Analyzed: 05/01/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOD1647-BS1) Prepared: 04/30/2020 Analyzed: 05/01/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 13 iMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1647 - 7471 - EPA 7471A LCS (BOD1647-BSI) Mercury LCS Dup (BOD1647-BSD1) Mercury Post Spike (BOD1647-PS1) Mercury Post Spike (BOD1647-PS2) Mercury Post Spike (BOD1647-PS3) Mercury Prepared: 04/30/2020 Analyzed: 05/01/2020 0.307 0.250 mg/kg 0.267 115 80-120 wet Prepared: 04/30/2020 Analyzed: 05/01/2020 0.285 0.250 mg/kg 0.267 107 80-120 7.32 wet Source: KOD0234-01 Prepared: 04/30/2020 Analyzed: 05/01/2020 1.62 ug/L 1.00 0.398 123 80-120 Source: MOD1889-01 Prepared: 04/30/2020 Analyzed: 05/01/2020 3.58 ug/L 1.00 3.03 54.5 80-120 Source: MOD1889-02 Prepared: 04/30/2020 Analyzed: 05/01/2020 3.51 ug/L 1.00 1.90 161 80-120 20 M5 M5 M5 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1659 - 3051A 6010 - EPA 6010E Blank (BOD1659-BLK1) Prepared &Analyzed: 04/30/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOD1659-BS1) Prepared &Analyzed: 04/30/2020 Aluminum 245 20.0 mg/kg 250 98.1 80-120 wet Arsenic 9.33 1.00 mg/kg 10.0 93.3 80-120 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 13 MICROBAC,`` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1659 - 3051A 6010 - EPA 6010B LCS (BOD1659-BS1) Prepared &Analyzed: 04/30/2020 Cadmium 1.21 0.100 mg/kg 1.25 96.7 80-120 wet Calcium 248 50.0 mg/kg 250 99.3 80-120 wet Copper 12.5 1.00 mg/kg 12.5 99.9 80-120 wet Lead 12.7 1.00 mg/kg 12.5 101 80-120 wet Magnesium 254 25.0 mg/kg 250 102 80-120 wet Molybdenum 26.2 3.00 mg/kg 25.0 105 80-120 wet Nickel 12.6 2.00 mg/kg 12.5 101 80-120 wet Potassium 1220 50.0 mg/kg 1250 97.2 80-120 wet Selenium 9.28 1.00 mg/kg 10.0 92.8 80-120 wet Sodium 1230 25.0 mg/kg 1250 98.1 80-120 wet Zinc 24.5 1.00 mg/kq 25.0 98.2 80-120 wet Duplicate (BOD1659-DUP1) Source: MOD1866-01 Prepared & Analyzed: 04/30/2020 Aluminum 5040 15.0 mg/kg 5610 10.8 20 dry Arsenic 3.61 0.748 mg/kg 3.64 0.849 20 dry Cadmium 0.250 0.0748 mg/kg 0.265 5.73 20 dry Calcium 10800 37.4 mg/kg 10500 2.15 20 dry Copper 12.8 0.748 mg/kg 13.0 1.10 20 dry Lead 6.73 0.748 mg/kg 6.76 0.405 20 dry Magnesium 3780 18.7 mg/kg 3980 5.08 20 dry Molybdenum <2.24 2.24 mg/kg ND 20 dry Nickel 8.78 1.50 mg/kg 9.11 3.67 20 dry Potassium 1090 37.4 mg/kg 1140 4.52 20 dry Selenium <0.748 0.748 mg/kg ND 20 dry Sodium 160 18.7 mg/kg 184 13.6 20 dry Zinc 38.9 0.748 mg/kg 40.2 3.27 20 dry Duplicate (BOD1659-DUP2) Source: MOD1866-01 Prepared & Analyzed: 04/30/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 13 VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1659 - 3051A 6010 - EPA 6010B Duplicate (BOD1659-DUP2) Source: MOD1866-01 Prepared & Analyzed: 04/30/2020 Aluminum 4730 15.2 mg/kg 5610 17.1 20 dry Arsenic 3.59 0.760 mg/kg 3.64 1.20 20 dry Cadmium 0.244 0.0760 mg/kg 0.265 8.21 20 dry Calcium 10600 38.0 mg/kg 10500 0.789 20 dry Copper 29.0 0.760 mg/kg 13.0 76.5 20 dry Lead 9.48 0.760 mg/kg 6.76 33.5 20 dry Magnesium 3580 19.0 mg/kg 3980 10.6 20 dry Molybdenum <2.28 2.28 mg/kg ND 20 dry Nickel 8.44 1.52 mg/kg 9.11 7.71 20 dry Potassium 1040 38.0 mg/kg 1140 9.08 20 dry Selenium <0.760 0.760 mg/kg ND 20 dry Sodium 146 19.0 mg/kg 184 22.8 20 dry Zinc 44.4 0.760 mg/kg 40.2 9.92 20 dry Matrix Spike (BOD1659-MS1) Source: MOD1866-08 Prepared & Analyzed: 04/30/2020 Aluminum 7120 14.1 mg/kg 176 5620 849 75-125 dry Arsenic 10.3 0.705 mg/kg 7.05 3.83 91.1 75-125 dry Cadmium 1.11 0.0705 mg/kg 0.881 0.247 98.2 75-125 dry Calcium 11600 35.2 mg/kg 176 11000 347 75-125 dry Copper 18.7 0.705 mg/kg 8.81 11.1 86.9 75-125 dry Lead 13.1 0.705 mg/kg 8.81 5.15 90.2 75-125 dry Magnesium 4690 17.6 mg/kg 176 4170 299 75-125 dry Molybdenum 16.8 2.11 mg/kg 17.6 ND 95.2 75-125 dry Nickel 17.5 1.41 mg/kg 8.81 9.19 94.3 75-125 dry Potassium 2030 35.2 mg/kg 881 1090 107 75-125 dry Selenium 6.50 0.705 mg/kg 7.05 ND 92.2 75-125 dry Sodium 1090 17.6 mg/kg 881 204 100 75-125 dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 13 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Metals Total by ICP Result Batch BOD1659 - 3051A 6010 - EPA 6010E Matrix Spike (BOD1659-MS1) _ Zinc 58.8 Matrix Spike Dup (80131659-MSD1) Aluminum 5490 Arsenic 10.4 Cadmium 1.13 Calcium 11100 Copper 19.3 Lead 13.3 Magnesium 4130 Molybdenum 18.2 Nickel 17.2 Potassium 1870 Selenium 6.77 Sodium 1050 Zinc 54.6 Post Spike (BOD1659-PSI) Aluminum 150 Arsenic 0.278 Cadmium 0.0295 Calcium 281 Copper 0.502 Lead 0.352 Magnesium 111 Molybdenum 0.488 Nickel 0.456 Potassium 50.2 Selenium 0.186 Sodium 28.1 Zinc 1.44 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Source: MOD1866-08 Prepared & Analyzed: 04/30/2020 0.705 mg/kg 17.6 39.4 110 75-125 dry Source: MOD1866-08 Prepared & Analyzed: 04/30/2020 15.0 mg/kg 188 5620 NR 75-125 25.9 20 dry 0.751 mg/kg 7.51 3.83 87.8 75-125 1.68 20 dry 0.0751 mg/kg 0.939 0.247 94.5 75-125 2.00 20 dry 37.6 mg/kg 188 11000 62.3 75-125 4.34 20 dry 0.751 mg/kg 9.39 11.1 88.2 75-125 3.26 20 dry 0.751 mg/kg 9.39 5.15 87.2 75-125 1.79 20 dry 18.8 mg/kg 188 4170 NR 75-125 12.7 20 dry 2.25 mg/kg 18.8 ND 96.8 75-125 7.98 20 dry 1.50 mg/kg 9.39 9.19 85.4 75-125 1.66 20 dry 37.6 mg/kg 939 1090 83.0 75-125 8.24 20 dry 0.751 mg/kg 7.51 ND 90.1 75-125 4.12 20 dry 18.8 mg/kg 939 204 89.8 75-125 3.94 20 dry 0.751 mg/kg 18.8 39.4 80.9 75-125 7.34 20 dry Source: MOD1866-08 Prepared & Analyzed: 04/30/2020 mg/L 5.00 141 173 80-120 mg/L 0.200 0.0963 91.1 80-120 mg/L 0.0250 0.00622 93.1 80-120 mg/L 5.00 277 82.3 80-120 mg/L 0.250 0.278 89.6 80-120 mg/L 0.250 0.129 89.2 80-120 mg/L 5.00 105 123 80-120 mg/L 0.500 0.00712 96.1 80-120 mg/L 0.250 0.231 89.9 80-120 mg/L 25.0 27.4 91.2 80-120 mg/L 0.200 0.00438 90.8 80-120 mg/L 25.0 5.14 91.7 80-120 mg/L 0.500 0.991 90.2 80-120 Spike Source %REC RPD Metals SPLP by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1197 - EPA 245.1 & EPA 7470A - EPA 7470A Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 13 )MICROBAC'- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Spike Source %REC RPD Metals SPLP by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1197 - EPA 245.1 & EPA 7470A - EPA 7470A Blank (60D1197-BLK1) Prepared & Analyzed: 04/22/2020 Mercury <0.000200 0.000200 mg/L LCS (BOD1197-BS1) Prepared &Analyzed: 04/22/2020 Mercury 0.00404 0.000200 mg/L 0.00400 101 80-120 Matrix Spike (BOD1197-MSI) Source: MOD1414-01 Prepared &Analyzed: 04/22/2020 Mercury 0.00459 0.000222 mg/L 0.00444 ND 103 75-125 Matrix Spike Dup (BOD1197-MSD1) Source: MOD1414-01 Prepared &Analyzed: 04/22/2020 Mercury 0.00427 0.000222 mg/L 0.00444 ND 96.1 75-125 7.07 20 Post Spike (BOD1197-PSI) Source: MOD1414-01 Prepared & Analyzed: 04/22/2020 Mercury 0.835 ug/L 1.00-0.0139 83.5 85-115 M5 Post Spike (BOD1197-PS2) Source: MOD1414-01 Prepared & Analyzed: 04/22/2020 Mercury 1.06 ug/L 1.00-0.0139 106 85-115 Spike Source %REC RPD Metals SPLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1271 - 3015A 6010 - EPA 6010B Blank (BOD1271-BLK1) Prepared: 04/23/2020 Analyzed: 04/24/2020 Aluminum <0.200 0.200 mg/L Arsenic <0.0200 0.0200 mg/L Cadmium <0.00200 0.00200 mg/L Calcium <0.500 0.500 mg/L Copper <0.0100 0.0100 mg/L Lead <0.0200 0.0200 mg/L Magnesium <0.500 0.500 mg/L Molybdenum <0.0100 0.0100 mg/L Nickel <0.0200 0.0200 mg/L Potassium <2.00 2.00 mg/L Selenium <0.0350 0.0350 mg/L Sodium <0.500 0.500 mg/L Zinc <0.0200 0.0200 mg/L LCS (BOD1271-BS1) Prepared: 04/23/2020 Analyzed: 04/24/2020 Aluminum 6.42 0.200 mg/L 6.25 103 80-120 Arsenic 0.239 0.0200 mg/L 0.250 95.5 80-120 Cadmium 0.0314 0.00200 mg/L 0.0313 100 80-120 Calcium 6.40 0.500 mg/L 6.25 102 80-120 Copper 0.320 0.0100 mg/L 0.313 102 80-120 Lead 0.321 0.0200 mg/L 0.313 103 80-120 Magnesium 6.41 0.500 mg/L 6.25 103 80-120 Molybdenum 0.635 0.0100 mg/L 0.625 102 80-120 Nickel 0.323 0.0200 mg/L 0.313 103 80-120 Potassium 32.2 2.00 mg/L 31.3 103 80-120 Selenium 0.243 0.0350 mg/L 0.250 97.2 80-120 Sodium 32.1 0.500 mg/L 31.3 103 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 15 of 13 VMICROBAC- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Spike Source %REC RPD Metals SPLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOD1271 - 3015A 6010 - EPA 6010B LCS (BOD1271-BS1) Prepared: 04/23/2020 Analyzed: 04/24/2020 Zinc 0.630 0.0200 mg/L 0.625 101 80-120 Matrix Spike (BOD1271-MS1) Source: MOD1347-01 Prepared: 04/23/2020 Analyzed: 04/24/2020 Aluminum 81.0 1.60 mg/L 50.0 31.2 99.5 75-125 Arsenic 1.97 0.160 mg/L 2.00 ND 98.4 75-125 Cadmium 0.254 0.0160 mg/L 0.250 ND 102 75-125 Calcium 197 4.00 mg/L 50.0 148 98.2 75-125 Copper 2.59 0.0800 mg/L 2.50 0.0736 100 75-125 Lead 2.51 0.160 mg/L 2.50 ND 100 75-125 Magnesium 52.3 4.00 mg/L 50.0 2.59 99.5 75-125 Molybdenum 5.10 0.0800 mg/L 5.00 ND 102 75-125 Nickel 2.52 0.160 mg/L 2.50 ND 101 75-125 Potassium 261 16.0 mg/L 250 ND 105 75-125 Selenium 2.18 0.280 mg/L 2.00 0.220 98.0 75-125 Sodium 1800 4.00 mg/L 250 1570 93.8 75-125 Zinc 5.20 0.160 mg/L 5.00 0.138 101 75-125 Matrix Spike Dup (BOD1271-MSD1) Source: MOD1347-01 Prepared: 04/23/2020 Analyzed: 04/24/2020 Aluminum 80.6 1.60 mg/L 50.0 31.2 98.8 75-125 0.423 20 Arsenic 1.98 0.160 mg/L 2.00 ND 99.0 75-125 0.552 20 Cadmium 0.256 0.0160 mg/L 0.250 ND 102 75-125 0.863 20 Calcium 194 4.00 mg/L 50.0 148 92.5 75-125 1.46 20 Copper 2.59 0.0800 mg/L 2.50 0.0736 101 75-125 0.143 20 Lead 2.51 0.160 mg/L 2.50 ND 101 75-125 0.287 20 Magnesium 52.7 4.00 mg/L 50.0 2.59 100 75-125 0.612 20 Molybdenum 5.12 0.0800 mg/L 5.00 ND 102 75-125 0.423 20 Nickel 2.54 0.160 mg/L 2.50 ND 102 75-125 0.897 20 Potassium 266 16.0 mg/L 250 ND 106 75-125 1.54 20 Selenium 2.24 0.280 mg/L 2.00 0.220 101 75-125 2.58 20 Sodium 1780 4.00 mg/L 250 1570 84.5 75-125 1.30 20 Zinc 5.20 0.160 mg/L 5.00 0.138 101 75-125 0.0712 20 Post Spike (BOD1271-PSI) Source: MOD1345-02 Prepared: 04/23/2020 Analyzed: 04/24/2020 Aluminum 5.10 mg/L 5.00 0.0488 101 80-120 Arsenic 0.190 mg/L 0.200 -0.00167 95.2 80-120 Cadmium 0.0250 mg/L 0.0250 -0.000126 100 80-120 Calcium 5.38 mg/L 5.00 0.357 100 80-120 Copper 0.253 mg/L 0.250 0.00305 99.9 80-120 Lead 0.251 mg/L 0.250 0.00140 99.7 80-120 Magnesium 5.00 mg/L 5.00 0.0627 98.7 80-120 Molybdenum 0.503 mg/L 0.500 -0.00222 101 80-120 Nickel 0.259 mg/L 0.250 0.00851 100 80-120 Potassium 25.7 mg/L 25.0 0.0944 103 80-120 Selenium 0.194 mg/L 0.200 -0.00350 97.0 80-120 Sodium 158 mg/L 25.0 133 102 80-120 Zinc 0.602 mg/L 0.500 0.105 99.4 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 11 of 13 V M ICROBAC'- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOD0234 Definitions %: Percent % (by wt.): Percent by Weight 133: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time 111115: Post digestion spike is outside of acceptance limits. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram mg/L: Milligrams per Liter NA: Not Applicable Q7: CCV recovery is above acceptance limits. However there is no impact on the reported value. RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 7.1 °C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certifications) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and subject to Microbac s standard terms and conditions which can be located and Administration reviewed at <https://www.microbac.com/standard-terms-cond/tlons>. Reported: 05/08/2020 15:36 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com IPage 12 of 13 Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / E i C CHAIN OF CUSTODY RECORD {KOD0234" I11Il11111j111H1 PAGE 1 OF 1 CLIENT NAME 6 ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 POM FROIFT I LOCATION: ova - 60-da series #OF a O T T L E s TYPE OF ANALYSIS PRESERVATION CODE E : E U E C •E E = y y U) .L Q m CL o U E ii t0 E > °) C m 2 J E > (aZ (D 0 (L - x Z Ut _ O C N E o ¢ - C) 0 z = Z Z ¢ a o a F z Y H cL � o o CODE: A =None B = HNO3 (pH<2) +<4°C C= H2SO4 (pH<2) + <4'C D= NaOH + <4°C E= ZN Acetate + <4°C F=HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910 410-9131 (L,I(k,v DATEIMETHOO OF SHIPMENT: Micro6ac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB PX D.D. TEMP °c REs' CXLORINE Residual from paper plant l6 Z b IS Z X 1 2 A A A A A A A I A A 1 A A A A A A A A A Rellnquis Data Time 2 Time 3( ReEnquisned by: Data Time Recatnd by. (Slpneture) Date Time 3 4 Relinquished by. Data Time Raeeived by. (Sgnatum) Data Time 5 t3 Comments or Special Hazards: M lck" Page 13 of 13 rlL*0 M I C R 0 B A C Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Wednesday, June 17, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 9 V M IGROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOFO109 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 06/08/2020 Cordova, NC 28330 Reported: 06/17/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOF0109-01 Solid Grab 06/08/20 13:00 06/08/20 15:48 Grab Page 2 of 9 VMICROBAC'' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOFO1O9 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOF0109-01 Collection Date: 06/08/2020 13:00 Inorganics Total Calculation Sodium Adsorption Ratio, SAR EPA 9045D pH at 25 °C SM 4500-P F-2011 Phosphorus, Total (as P) Plant Available Nitrogen EPA 300.0, Rv. 2.1 (1993) Nitrate as N Nitrite as N SM 2540 G-2011 % Solids SM 4500-NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen General Parameters ASTM D2216-10 Percent Solids Metals Total by AA EPA 7471 A Mercury Metals Total by ICP EPA 6010D Aluminum Result 0.540 8.6 <0.66 Result 28.3 RL Units Dilution Note Prepared Analyzed Analyst NA 1 06/17/20 1021 06/17/20 1021 BNS 1.0 S.U. 1 H O6/11/20 1410 TBM 0.66 mg/kg dry 1 06/11/20 1233 JDW RL Units Dilution Note Prepared Analyzed Analyst mg/kg 1 06/17/20 1021 06/17/20 1021 BNS 0.500 0.0658 mg/kg dry 1 06/09/20 1656 06/10/20 0905 JDW <1.32 1.32 mg/kg dry 1 06/09/20 1656 06/10/20 0905 JDW 37.7 1.00 % 1 06/09/20 1743 MT <2.65 2.65 mg/kg dry 1 Y 06/10/20 1410 JDW 91.2 0.500 mg/kg 1 06/11/20 0932 TBM Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 36.3 1.00 % (by wt.) 1 Y 06/15/20 1213 06/16/20 0530 JST Result RL Units Dilution Note Prepared Analyzed Analyst <0.679 0.679 mg/kg dry 1 06/16/20 0558 06/16/20 1008 TMM Result RL Units Dilution Note Prepared Analyzed Analyst 913 41.5 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 0f 9 6)MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOF0109-01 Collection Date: 06/08/2020 13:00 Metals Total by ICP Result RL Units Dilution Note Prepared Analyzed Analyst Arsenic <2.08 2.08 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Calcium 200000 10400 mg/kg dry 100 D3 06/16/20 0546 06/16/20 1400 JYH Copper 14.3 2.08 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Lead <2.08 2.08 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Magnesium 1980 51.9 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Molybdenum <6.23 6.23 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Nickel <4.15 4.15 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Phosphorus 109 104 mg/kg dry 1 Y 06/16/20 0546 06/16/20 1323 JYH Potassium <104 104 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Selenium <2.08 2.08 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Sodium 1240 51.9 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Zinc 87.9 2.08 mg/kg dry 1 06/16/20 0546 06/16/20 1323 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 9 '* MICRr)BAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch KF01231 - Wet Chem Solid - SM 2540 G-2011 Blank (KFO1231-BLK1) Prepared &Analyzed: 06/09/2020 % Solids <1.00 1.00 % Duplicate (KFO1231-DUP1) Source: KOF0109-01 Prepared & Analyzed: 06/09/2020 % Solids 37.3 1.00 % 37.7 1 10 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOF0832 - Wet-Solids-S -ASTM D2216-10 Blank (BOF0832-BLK1) Prepared: 06/15/2020 Analyzed: 06/16/2020 Percent Solids 100 1.00 % (by wt.) LCS (BOF0832-BS1) Prepared: 06/15/2020 Analyzed: 06/16/2020 Percent Solids 77.6 % (by 80.0 97.0 90-110 wt.) Duplicate (BOF0832-DUP1) Source: MOF1143-01 Prepared: 06/15/2020Analyzed: 06/16/2020 Percent Solids 58.8 1.00 % (by 67.3 13.4 10 R2 wt.) Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOF0887 - 7471 - EPA 7471A Blank (BOF0887-BLK1) Prepared &Analyzed: 06/16/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOF0887-BSI) Prepared &Analyzed: 06/16/2020 Mercury 0.294 0.250 mg/kg 0.267 110 80-120 wet LCS Dup (BOF0887-BSD1) Prepared &Analyzed: 06/16/2020 Mercury 0.298 0.250 mg/kg 0.267 112 80-120 1.35 20 wet Post Spike (BOF0887-PSI) Source: KOF0109-01 Prepared &Analyzed: 06/16/2020 Mercury 125 ug/L 1.00 0.0896 116 80-120 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOF0882 - 3051A 6010 - EPA 6010D Blank (BOF0882-BLK1) Prepared &Analyzed: 06/16/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 0f 9 .�MICRnRA(- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOF0882 - 3051A 6010 - EPA 6010D Blank (BOF0882-BLK1) Prepared &Analyzed: 06/16/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Phosphorus <50.0 50.0 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOF0882-BSI) Prepared &Analyzed: 06/16/2020 Aluminum 236 20.0 mg/kg 250 94.4 80-120 wet Arsenic 9.24 1.00 mg/kg 10.0 92.4 80-120 wet Calcium 246 50.0 mg/kg 250 98.3 80-120 wet Copper 12.4 1.00 mg/kg 12.5 99.1 80-120 wet Lead 12.5 1.00 mg/kg 12.5 99.7 80-120 wet Magnesium 250 25.0 mg/kg 250 100 80-120 wet Molybdenum 25.9 3.00 mg/kg 25.0 104 80-120 wet Nickel 12.5 2.00 mg/kg 12.5 99.8 80-120 wet Phosphorus 237 50.0 mg/kg 250 94.7 80-120 wet Potassium 1240 50.0 mg/kg 1250 98.8 80-120 wet Selenium 9.39 1.00 mg/kg 10.0 93.9 80-120 wet Sodium 1250 25.0 mg/kg 1250 99.8 80-120 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 9 rCAMICROBAC- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOF0882 - 3051A 6010 - EPA 6010D LCS (BOF0882-BSI) Prepared & Analyzed: 06/16/2020 Zinc 24.3 1.00 mg/kg 25.0 97.3 80-120 wet LCS Dup (BOF0882-BSD1) Prepared &Analyzed: 06/16/2020 Aluminum 239 20.0 mg/kg 250 95.5 80-120 1.12 20 wet Arsenic 9.37 1.00 mg/kg 10.0 93.7 80-120 1.35 20 wet Calcium 252 50.0 mg/kg 250 101 80-120 2.57 20 wet Copper 12.6 1.00 mg/kg 12.5 101 80-120 1.66 20 wet Lead 12.7 1.00 mg/kg 12.5 101 80-120 1.75 20 wet Magnesium 254 25.0 mg/kg 250 102 80-120 1.61 20 wet Molybdenum 26.4 3.00 mg/kg 25.0 106 80-120 1.87 20 wet Nickel 12.7 2.00 mg/kg 12.5 102 80-120 1.81 20 wet Phosphorus 240 50.0 mg/kg 250 96.1 80-120 1.48 20 wet Potassium 1260 50.0 mg/kg 1250 101 80-120 1.70 20 wet Selenium 9.51 1.00 mg/kg 10.0 95.1 80-120 1.27 20 wet Sodium 1270 25.0 mg/kg 1250 102 80-120 2.02 20 wet Zinc 24.7 1.00 mg/kg 25.0 98.7 80-120 1.51 20 wet Post Spike (BOF0882-PS1) Source: KOF0109-01 Prepared & Analyzed: 06/16/2020 Aluminum 12.9 mg/L 5.00 7.92 98.7 80-120 Arsenic 0.204 mg/L 0.200 0.00306 101 80-120 Copper 0.367 mg/L 0.250 0.124 97.0 80-120 Lead 0.244 mg/L 0.250 0.00553 95.4 80-120 Magnesium 21.4 mg/L 5.00 17.2 85.5 80-120 Molybdenum 0.561 mg/L 0.500 0.0467 103 80-120 Nickel 0.243 mg/L 0.250 0.00681 94.5 80-120 Phosphorus 5.98 mg/L 5.00 0.944 101 80-120 Potassium 25.7 mg/L 25.0 0.389 101 80-120 Selenium 0.204 mg/L 0.200 0.00104 102 80-120 Sodium 35.7 mg/L 25.0 10.7 100 80-120 Zinc 1.24 mg/L 0.500 0.762 95.5 80-120 Post Spike (BOF0882-PS2) Source: KOF0109-01 Prepared & Analyzed: 06/16/2020 Calcium 25.5 mg/L 5.00 16.8 173 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 9 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOF0109 Definitions %: Percent % (by wt.): Percent by Weight D3: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable R2: Duplicate RPD is outside of acceptance limits. Visual examination confirms sample is non -homogeneous. RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 5.2°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (CDC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certifications) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and Reported: 06/17/2020 18:00 reviewed at <httos://www.microbac.com/standard-terms-conditions>. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com 'Drvl 1 Page 8 ci Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-87 *KOF0109` 111111111 CHAIN OF CUSTODY RECORD PAGE "I OF I_ CLIENT NAME S ADDRESS: Corp. 126 First Street Cordova, NC 28330 Pot 7ROjCTV[LOCA'nON:SOF a - 60-dayseries B 0 T T L B S TYPE OF ANALYSIS PRESERVATION CODEVonDrehle E E V E C •E Q = N N rA U d Q O 0 E 2 U = ID c] m J = cn a S Z _ O C IN E fn X ¢ Z + o Z Z Z a 0 L a I— Z Y I— CL 'O O to l0 o \ CODE: A = None B = HNO3 (pH<2) + <4°C C-H2SO4(pH<2)+<4'C D= NaOH + <4'C E= ZN Acetate + <4°C F=HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910 410-9131 SAMPLER: /, / )A��(,,y L� r; h f' GATE/ METHOD OF SHIPMENT: Microbac LAB ID 9 SAMPLE TYPE DATE TIME COMP GRAB PH 0.0. TEMP'C IRE CNLORINE ` \ Residual from paper plant 6 g z0 3' 0 () X 2 A A A A A A A A A 5. 6 ZU j3r�� 1 A A A A I A A A I A A R.Iinq 0 Time Reci ed signet4lre) Date Timm $ Z i) 15; u ITIM6 2 (/UJ�C[ i Relinquished by: Date Reee'ned by: (Signahw.) Date Tim. 3 4 Relinquished by. Data Time Received brc (Signature) Dele Tlm. 5 g Comments or Special Hazards: REVIEWED Page 9 of 9 *M1rP0BAC F Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS TDD- KOH0099 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Friday, August 28, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 11 ((�)MICROBACA Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 08/10/2020 Cordova, NC 28330 Reported: 08/28/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOH0099-01 Solid Grab 08/10/20 12:29 08/10/20 13:59 Grab Page 2 of 11 VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOH0099-01 Collection Date: 08/10/2020 12:29 Inorganics Total Calculation Sodium Adsorption Ratio, SAR EPA 9045D pH at 25 °C SM 4500-P F-2011 Phosphorus, Total (as P) General Parameters EPA 300.0, Rv. 2.1 (1993) Nitrate as N Nitrite as N SM 2540 G-2011 % Solids SM 4500-NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen General Parameters ASTM D2216-10 Percent Solids Metals Total by AA EPA 7471A Mercury Metals Total by ICP EPA 6010D Aluminum Arsenic Cadmium Calcium Result 0.360 8.6 4.3 Result 1.13 <13.1 38.8 RL Units Dilution Note Prepared Analyzed Analyst NA 1 08/27/20 1408 08/27/20 1408 BNS 1.0 S.U. 1 H 08/26/20 1120 TBM 0.60 mg/kg dry 1 08/17/20 1529 JDW RL Units Dilution Note Prepared Analyzed Analyst 0.657 mg/kg dry 1 08/18/20 1303 JDW 13.1 mg/kg dry 1 08/18/20 1303 JDW 1.00 % 1 08/12/20 1414 MT <44.1 44.1 mg/kg dry 1 Y 08/19/20 1657 JDW 3.64 0.500 mg/kg 1 08/18/20 1100 TBM Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 37.0 1.00 % (by Wt.) 1 Y 08/13/20 0951 08/14/20 0735 ERP Result RL Units Dilution Note Prepared Analyzed Analyst <0.662 0.662 mg/kg dry 1 08/13/20 0638 08/13/20 1412 TMM Result RL Units Dilution Note Prepared Analyzed Analyst 1010 38.5 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH <1.92 1.92 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH <0.192 0.192 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH 190000 9620 mg/kg dry 100 D3 08/13/20 0755 08/14/20 1425 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 3 of11 VMICROBAC', Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOH0099-01 Collection Date: 08/10/2020 12:29 Metals Total by ICP Result RL Units Dilution Note Prepared Analyzed Analyst Copper 67.2 1.92 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Lead <1.92 1.92 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Magnesium 1910 48.1 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Molybdenum <5.77 5.77 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Nickel <3.85 3.85 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Potassium <96.2 96.2 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Selenium 40.4 1.92 mg/kg dry 1 B2 08/13/20 0755 08/14/20 1408 JYH Sodium 822 48.1 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Zinc 104 1.92 mg/kg dry 1 08/13/20 0755 08/14/20 1408 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 11 (WMICROBAC`� Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville General Parameters Result RL Batch KHO1409 - Wet Chem Solid - SM 2540 G-2011 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Blank (KHO1409-BLK1) Prepared & Analyzed: 08/12/2020 % Solids <1.00 1.00 % Duplicate (KHO1409-DUP1) Source: KOH0099-01 Prepared &Analyzed: 08/12/2020 % Solids 38.2 1.00 % 38.8 2 10 Batch KHO1822 - Wet Chem Solid - SM 4500-Norg C-2011 Blank (KHO1822-BLK1) Prepared &Analyzed: 08/18/2020 Total Kjeldahl Nitrogen <0.500 0.500 mg/kg LCS (KHO1822-BS1) Prepared &Analyzed: 08/18/2020 Total Kjeldahl Nitrogen 28.6 0.500 mg/kg 30.0 95 90-110 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0605 - Wet-Solids-S -ASTM D2216-10 Blank (BOH0605-BLK1) Percent Solids LCS (BOH0605-BS1) Percent Solids Duplicate (BOH0605-DUP1) Percent Solids Metals Total by AA Batch BOH0580 - 7471 - EPA 7471A 99.9 79.0 8.93 Result Prepared: 08/13/2020 Analyzed: 08/14/2020 1.00 % (by wt. ) _ Prepared: 08/13/2020 Analyzed: 08/14/2020 % (by 80.0 98.8 90-110 wt.) Source: MOH0646-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 1.00 % (by 8.96 wt. ) V.Zau IV Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Blank (BOH0580-BLK1) Prepared &Analyzed: 08/13/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOH0580-BSI) Prepared &Analyzed: 08/13/2020 Mercury 0.297 0.250 mg/kg 0.267 111 80-120 wet Matrix Spike (BOH0580-MS1) Source: MOH0514-03 Prepared &Analyzed: 08/13/2020 Mercury 0.808 0.480 mg/kg 0.512 0.528 54.7 75-125 dry Matrix Spike Dup (BOH0580-MSD1) Source: MOH0514-03 Prepared & Analyzed: 08/13/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com M2 Page 5 of 11 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0580 - 7471 - EPA 7471A Matrix Spike Dup (BOH0580-MSDI) Source: MOH0514-03 Prepared & Analyzed: 08/13/2020 Mercury 0.864 0.458 mg/kg 0.488 0.528 68.9 75-125 6.76 20 M2 dry Post Spike (BOH0580-PSI) _ Source: MOH0508-01 Prepared & Analyzed: 08/13/2020 Mercury 1.21 ug/L 1.00 0.185 102 80-120 Post Spike (BOH0580-PS2) Source: MOH0514-03 Prepared & Analyzed: 08/13/2020 Mercury 5.07 ug/L 1.00 3.93 115 80-120 Post Spike (BOH0580-PS3) Source: MOHO558-01 Prepared &Analyzed: 08/13/2020 Mercury 3.74 ug/L 1.00 2.65 109 80-120 Post Spike (BOH0580-PS4) Source: MOH0560-01 Prepared & Analyzed: 08/13/2020 Mercury 3.36 ug/L 1.00 2.70 65.6 80-120 Post Spike (BOH0580-PS5) Source: MOH0616-01 Prepared & Analyzed: 08/13/2020 Mercury 1.03 ug/L 1.00 0.0889 93.8 80-120 Post Spike (BOH0580-PS6) Source: MOH0643-01 Prepared & Analyzed: 08/13/2020 Mercury 1.27 ug/L 1.00 0.113 116 80-120 Post Spike (BOH0580-PS7) _ Source: MOH0646-01 Prepared & Analyzed: 08/13/2020 Mercury 1.53 ug/L 1.00 0.456 108 80-120 Post Spike (BOH0580-PS8) Source: MOH0667-01 Prepared & Analyzed: 08/13/2020 Mercury 1.87 ug/L 1.00 0.610 126 80-120 Post Spike (BOH0580-PS9) Source: KOH0099-01 Prepared & Analyzed: 08/13/2020 Mercury 1.29 ug/L 1.00 0.104 118 80-120 Post Spike (BOH0580-PSA) Source: MOH0560-02 Prepared & Analyzed: 08/13/2020 Mercury 3.39 ug/L 1.00 2.16 123 80-120 Post Spike (BOH0580-PSB) Source: MOH0560-03 Prepared & Analyzed: 08/13/2020 Mercury 3.71 ug/L 1.00 2.53 118 80-120 Post Spike (BOH0580-PSC) Source: MOH0560-04 Prepared & Analyzed: 08/13/2020 Mercury 3.28 ug/L 1.00 2.35 93.0 80-120 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0583 - 3051A 6010 - EPA 6010D Blank (BOH0583-BLK1) Prepared: 08/13/2020 Analyzed: 08/14/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Microbac Laboratories, Inc. 2592 Hope Mills Rd i Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 11 6)MICROBACK Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0583 - 3051 A6010 - EPA 601 OD Blank (BOH0583-BLK1) Prepared: 08/13/2020 Analyzed: 08/14/2020 Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOH0583-BSI) Prepared: 08/13/2020 Analyzed: 08/14/2020 Aluminum 241 20.0 mg/kg 250 96.2 80-120 wet Arsenic 9.39 1.00 mg/kg 10.0 93.9 80-120 wet Cadmium 1.23 0.100 mg/kg 1.25 98.4 80-120 wet Calcium 251 50.0 mg/kg 250 101 80-120 wet Copper 12.5 1.00 mg/kg 12.5 100 80-120 wet Lead 12.6 1.00 mg/kg 12.5 101 80-120 wet Magnesium 247 25.0 mg/kg 250 98.7 80-120 wet Molybdenum 26.8 3.00 mg/kg 25.0 107 80-120 wet Nickel 12.7 2.00 mg/kg 12.5 102 80-120 wet Potassium 1260 50.0 mg/kg 1250 101 80-120 wet Selenium 9.23 1.00 mg/kg 10.0 92.3 80-120 wet Sodium 1270 25.0 mg/kg 1250 101 80-120 wet Zinc 24.7 1.00 mg/kg 25.0 98.7 80-120 wet Matrix Spike (BOH0583-MSI) Source: MOH0616-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 Aluminum 19800 18.4 mg/kg 230 21300 NR 75-125 dry Arsenic 31.3 0.920 mg/kg 9.20 22.9 91.3 75-125 dry Cadmium 12.9 0.0920 mg/kg 1.15 11.7 107 75-125 dry Calcium 41800 46.0 mg/kg 230 41000 347 75-125 dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 11 �MICR0 A Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0583 - 3051 A6010 - EPA 601 OD Matrix Spike (BOH0583-MS1) Source: MOH0616-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 Copper 737 0.920 mg/kg 11.5 756 NR 75-125 dry Lead 74.4 0.920 mg/kg 11.5 66.6 67.7 75-125 dry Magnesium 7380 23.0 mg/kg 230 7410 NR 75-125 dry Molybdenum 52.6 2.76 mg/kg 23.0 30.4 96.2 75-125 dry Nickel 142 1.84 mg/kg 11.5 145 NR 75-125 dry Potassium 5320 46.0 mg/kg 1150 4850 40.9 75-125 dry Selenium 63.8 0.920 mg/kg 9.20 61.8 20.8 75-125 dry Sodium 2500 23.0 mg/kg 1150 1530 84.8 75-125 dry Zinc 1000 0.920 mg/kg 23.0 1120 NR 75-125 dry Matrix Spike Dup (BOH0583-MSD1) Source: MOH0616-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 Aluminum 20000 21.0 mg/kg 262 21300 NR 75-125 1.12 20 dry Arsenic 32.0 1.05 mg/kg 10.5 22.9 86.9 75-125 2.24 20 dry Cadmium 12.8 0.105 mg/kg 1.31 11.7 90.1 75-125 0.382 20 dry Calcium 41600 52.4 mg/kg 262 41000 200 75-125 0.657 20 dry Copper 791 1.05 mg/kg 13.1 756 266 75-125 7.06 20 dry Lead 75.3 1.05 mg/kg 13.1 66.6 66.6 75-125 1.27 20 dry Magnesium 7350 26.2 mg/kg 262 7410 NR 75-125 0.449 20 dry Molybdenum 54.9 3.15 mg/kg 26.2 30.4 93.2 75-125 4.32 20 dry Nickel 158 2.10 mg/kg 13.1 145 94.6 75-125 10.6 20 dry Potassium 5540 52.4 mg/kg 1310 4850 53.3 75-125 4.21 20 dry Selenium 67.2 1.05 mg/kg 10.5 61.8 50.8 75-125 5.21 20 dry Sodium 2640 26.2 mg/kg 1310 1530 84.7 75-125 5.24 20 dry Zinc 1030 1.05 mg/kg 26.2 1120 NR 75-125 2.49 20 dry Post Spike (BOH0583-PS1) Source: MOH0643-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 Aluminum 8.24 mg/L 5.00 3.45 95.8 80-120 Arsenic 0.193 mg/L 0.200 0.00456 94.0 80-120 Cadmium 0.0291 mg/L 0.0250 0.00502 96.2 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 11 ,VMICROBA( Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOH0583 - 3051A 6010 - EPA 6010D Post Spike (BOH0583-PS1) Source: MOH0643-01 Prepared: 08/13/2020 Analyzed: 08/14/2020 Calcium 30.6 mg/L 5.00 27.6 60.1 80-120 Copper 0.361 mg/L 0.250 0.115 98.3 80-120 Lead 0.258 mg/L 0.250 0.00962 99.2 80-120 Magnesium 5.65 mg/L 5.00 1.12 90.7 80-120 Molybdenum 0.535 mg/L 0.500 0.00567 106 80-120 Nickel 0.575 mg/L 0.250 0.324 100 80-120 Potassium 25.8 mg/L 25.0 2.25 94.2 80-120 Selenium 0.236 mg/L 0.200 0.0437 95.9 80-120 Sodium 28.2 mg/L 25.0 4.78 93.6 80-120 Zinc 0.670 mg/L 0.500 0.184 97.3 80-120 Definitions %: Percent % (by wt.): Percent by Weight 132: Target analyte is detected in the method blank at or above the reporting limit. The sample concentration is 10 times that found in the blank. 133: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time M2: Matrix spike recovery is outside of acceptance limits, biased low. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 11.3°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 11 VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOH0099 Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to e applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Mlcrobac's standard terms and conditions which can be located and reviewed at <httos://www.microbac.com/standard-terms-conditions>. Reported: 08I28I2020 11:44 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 10 of 11 `KOH0099' Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-87 CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME B ADDRESS:. VonDrehle Corp. 126 First Street Cordova, NC 28330 POP PROJECT I LOCATION: Cordova - 60-day series #OF a O T T L E s TYPE OF ANALYSIS PRESERVATION CODE E .E U E m E 2 Q E �_ V a Q �, o V E s m !) E .c m J E •N a Y 2 Z 0 _ O N j < ¢ - Z o Z Z Z as ' d I— Z H a to g ~ o CODE: A = None B = HNO3 < + <4°C (pH 2) C = H2SO4 (pH<2) +<4'C D = NaOH + <4'C E= ZN Acetate + <4°C F= HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER n I ' f Lj i3�' DATE I METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP ORA13 PH O.O. TI:MP'C CHLORINE Residual from paper plant l!D/2 0 (7,: Z 9 X 1 2 NA A I A I A I A I A A A A 3 1 A A A A A A A A A Relinq a D I Time Rece Bat �rtN 1 �f�o 20 1J.J � 2 �f Rell ulshed by. Date Time ReeeWed by. (519naMM) Date Time 3 4 Relinquished by: oats Time Received by: (Signature) Data Time 5 6 Comments or Special Hazards: REVIEWED Page 1of1 VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJ0203 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Monday, November 23, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 12 0MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 10/12/2020 Cordova, NC 28330 Reported: 11/23/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Tyne Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOJ0203-01 Solid Grab 10/12/20 12:23 10/12/20 15:57 Grab Page 2 of 12 6)MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOJO203-01 Collection Date: 10/12/2020 12:23 Inorganics Total Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Sodium Adsorption Ratio, SAR 0.330 NA 1 11/09/20 1943 BNS EPA 9045D pH at 25 °C 8.2 1.0 S.U. 1 H 11/03/20 1151 11/02/20 1527 TBM SM 4500-NH3 G-2011 Ammonia as N <4.50 4.50 mg/kg 1 y 11/02/20 1701 JO SM 4500-P F-2011 Phosphorus, Total (as P) 3.5 0.59 mg/kg dry 1 10/22/20 0024 10/22/20 0044 JAW General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Plant Available Nitrogen 582 mg/kg 1 11/06/20 1324 11/06/20 1324 BNS EPA 300.0, Rv. 2.1 (1993) Nitrate as N 0.685 0.0591 mg/kg dry 1 11/03/20 1246 11/03/20 1251 JDW Nitrite as N <1.18 1.18 mg/kg dry 1 11/03/20 1246 11/03/20 1251 JDW SM 2540 G-2011 % Solids 42.3 1.00 % 1 10/14/20 0954 TBM Analyses Subcontracted to: ECI General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst EPA 351.2, Rv. 2 (1993) Total Kjeldahl Nitrogen 1940 0.5 mg/kg 1 10/12/20 1223 11/05/20 0000 RP Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst ASTM D2216-10 Percent Solids 36.2 1.00 % (by wt.) 1 Y 10/16/20 0719 10/19/20 0710 JMH Metals Total by AA Result RL Units Dilution Note Prepared Analyzed Analyst EPA 7471A Mercury <0.658 0.658 mg/kg dry 1 10/19/20 0724 10/20/20 1212 TMM Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOJO203-01 Collection Date: 10/12/2020 12:23 Metals Total by ICP Result RL Units Dilution Note EPA 6010E Aluminum 1360 37.8 mg/kg dry 1 Arsenic <1.89 1.89 mg/kg dry 1 Cadmium 0.199 0.189 mg/kg dry 1 Calcium 219000 9450 mg/kg dry 100 D3 Copper 32.0 1.89 mg/kg dry 1 Lead <1.89 1.89 mg/kg dry 1 Magnesium 2220 47.2 mg/kg dry 1 Molybdenum <5.67 5.67 mg/kg dry 1 Nickel <3.78 3.78 mg/kg dry 1 Phosphorus 142 94.5 mg/kg dry 1 y Potassium <94.5 94.5 mg/kg dry 1 Selenium <1.89 1.89 mg/kg dry 1 Sodium 805 47.2 mg/kg dry 1 Zinc 74.3 1.89 mg/kg dry 1 Prepared Analyzed Analyst 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1203 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL 11/05/20 0540 11/09/20 1032 KHL Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 12 iMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Batch Log Summary EPA 351.2, Rv. 2 (1993) [none] BATCH-BLK1 (Solid) BATCH-BS1 (Solid) BATCH-BS1 (Solid) BATCH-MS1 (Solid) BATCH-MS1 (Solid) KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant Grab BATCH-BLK1 (Solid) Method Batch Laboratory ID Client I Source ID ASTM D2216-10 BOJO893 BOJ0893-DUP1 KOJO203-01 B0J0893-BS1 BOJO893-BLK1 KOJO203-01 Residual fmm Paper Plant, Grab Method Batch Laboratory ID Client I Source ID EPA 7471A BOJ1022 BOJ1022-BLK1 130J1022-13S1 BOJ1022-BSD1 BOJ1022-MRL1 BOJ1022-PS1 MOJ0921-01 BOJ1022-PS2 MOJ0922-01 BOJ1022-PS4 MOJ0995-02 130J1022-PS5 MOJ1117-02 KOJO203-01 Residual from Paper Plant, Grab BOJ1022-PS6 KOJO203-01 BOJ1022-PS7 MOJ1192-01 BOJ1022-PS8 MOJ1282-04 BOJ1022-PSA MOJ1364-01 BOJ1022-PS9 MOJ1307-01 BOJ1022-PSB MOJ1117-01 BOJ1022-SRL1 MOJ1307-01 Method Batch Laboratory ID Client I Source ID EPA 601 OB BOK0235 BOK0235-MRL1 BOK0235-BLK1 BOK0235-BS1 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab BOK0235-PS1 KOJO203-01 Microbac Laboratories, Inc, 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 EPA 6010E BOK0235 BOK0235-SRL1 KOJO203-01 BOK0235-MS1 MOK0141-20 BOK0235-MSD1 MOK0141-20 KOJO203-01 RE 1 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID SM 2540 G-2011 KJO1306 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab KJO1306-DUP1 KOJO203-01 KJO1306-BLK1 KJO1306-BLK1 KJO1306-DUP1 KOJO203-01 Method Batch Laboratory ID Client / Source ID EPA 300.0, Rv. 2.1 (1993) KJO1410 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID SM 4500-P F-2011 KJ02103 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID EPA 9045D KKO0309 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client I Source ID SM 4500-NH3 G-2011 KKO0310 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID Calculation KKO0528 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID Calculation KKO0906 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch KJ01306 - Wet Chem Solid - SM 2540 G-2011 Blank (KJO1306-BLKI) Prepared &Analyzed: 10/14/2020 % Solids <1.00 1.00 % Duplicate (KJO1306-DUP1) Source: KOJO203-01 Prepared & Analyzed: 10/14/2020 % Solids 41.9 1.00 % 42.3 1 10 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 12 V M ICROBAC.. Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOJO893 - Wet-Solids-S - ASTM D2216-10 Blank (BOJO893-BLK1) Percent Solids LCS (B0J0893-BS1) Percent Solids Duplicate (BOJO893-DUP1) Percent Solids Metals Total by AA Batch BOJ1022 - 7471 - EPA 7471A 100 80.2 36.2 Result Prepared: 10/16/2020 Analyzed: 10/19/2020 1.00 % (by wt.) Prepared: 10/16/2020 Analyzed: 10/19/2020 % (by 80.0 100 90-110 wt.) Source: KOJO203-01 Prepared: 10/16/2020 Analyzed: 10/19/2020 1.00 % (by 36.2 wt.) 0.145 20 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Blank (BOJI022-BLK1) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOJ 1 022-BS1) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.315 0.250 mg/kg 0.267 118 80-120 wet LCS Dup (BOJ1022-BSDI) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.314 0.250 mg/kg 0.267 118 80-120 0.318 wet Post Spike (BOJ 1 022-PSI) Source: MOJ0921-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 2.98 ug/L 1.00 1.77 121 80-120 Post Spike (BOJ 1 022-PS2) Source: MOJ0922-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.50 ug/L 1.00 0.318 119 80-120 Post Spike (BOJ1022-PS4) Source: MOJ0995-02 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 4.68 ug/L 1.00 3.33 136 80-120 Post Spike (BOJ1022-PS5) Source: MOJ1117-02 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.52 ug/L 1.00 0.252 127 80-120 Post Spike (BOJ1022-PS6) Source: KOJO203-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.05 ug/L 1.00-0.0221 105 80-120 Post Spike (BOJ1022-PS7) Source: MOJ1192-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.752 ug/L 1.00 -0.133 75.2 80-120 Post Spike (BOJ1022-PS8) Source: MOJ1282-04 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 3.06 ug/L 1.00 1.66 140 80-120 Post Spike (BOJI022-PS9) Source: MOJ1307-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Microbac Laboratories, Inc. 20 M5 M5 M5 M5 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 7 of 12 V MI ICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOJ1022 - 7471 -EPA 7471A Post Spike (BOJ I 022-PS9) Source: MOJ1307-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Mercury 6.93 ug/L 1.00 3.92 301 80-120 M5 Post Spike (BOJ1022-PSA) Source: MOJ1364-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.19 ug/L 1.00 0.338 85.5 80-120 Post Spike (80J1022-PS13) Source: MOJ1117-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Mercury 5.04 ug/L 1.00 4.10 93.9 80-120 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOK0235 - 3051A 6010 - EPA 601 OB Blank (BOK0235-BLK1) Prepared: 11 /05/2020 Analyzed: 11 /09/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper <1.00 1.00 mg/kg wet Lead <1.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Phosphorus <50.0 50.0 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium <1.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOK0235-BSI) Prepared: 11 /05/2020 Analyzed: 11 /09/2020 Aluminum 238 20.0 mg/kg 250 95.2 80-120 wet Arsenic 9.05 1.00 mg/kg 10.0 90.5 80-120 wet Calcium 255 50.0 mg/kg 250 102 80-120 wet Copper 12.3 1.00 mg/kg 12.5 98.3 80-120 wet Microbac Laboratories, Inc. 2592 Hope Mills Rd 1 Fayetteville, NC 28306 1910.864.1920 p 1 www.microbac.com Page 8 of 12 O M ICROBAC'5 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Metals Total by ICP Result Batch BOK0235 - 3051A 6010 - EPA 6010B RL Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes LCS (BOK0235-BS1) Prepared: 11 /05/2020 Analyzed: 11 /09/2020 Lead 12.4 1.00 mg/kg 12.5 98.9 80-120 wet Magnesium 260 25.0 mg/kg 250 104 80-120 wet Molybdenum 26.1 3.00 mg/kg 25.0 105 80-120 wet Nickel 12.4 2.00 mg/kg 12.5 99.2 80-120 wet Phosphorus 234 50.0 mg/kg 250 93.7 80-120 wet Potassium 1270 50.0 mg/kg 1250 101 80-120 wet Selenium 9.27 1.00 mg/kg 10.0 92.7 80-120 wet Sodium 1270 25.0 mg/kg 1250 101 80-120 wet Zinc 24.2 1.00 mg/kg 25.0 96.9 80-120 wet Matrix Spike (BOK0235-MS7) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 11600 18.6 mg/kg 233 11100 196 75-125 dry Arsenic 11.3 0.932 mg/kg 9.32 3.58 83.3 75-125 dry Calcium 1870 46.6 mg/kg 233 1100 330 75-125 dry Copper 20.5 0.932 mg/kg 11.6 10.3 88.2 75-125 dry Lead 21.8 0.932 mg/kg 11.6 13.3 72.4 75-125 dry Magnesium 696 23.3 mg/kg 233 405 125 75-125 dry Molybdenum 23.7 2.79 mg/kg 23.3 ND 102 75-125 dry Nickel 14.8 1.86 mg/kg 11.6 1.63 114 75-125 dry Phosphorus 462 46.6 mg/kg 233 249 91.6 75-125 dry Potassium 1500 46.6 mg/kg 1160 330 101 75-125 dry Selenium 10.7 0.932 mg/kg 9.32 5.30 58.4 75-125 dry Sodium 1140 23.3 mg/kg 1160 ND 97.9 75-125 dry Zinc 43.4 0.932 mg/kg 23.3 13.3 129 75-125 dry Matrix Spike Dup (BOK0235-MSD1) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 12200 19.8 mg/kg 247 11100 437 75-125 5.23 20 dry Arsenic 11.3 0.989 mg/kg 9.89 3.58 78.2 75-125 0.233 20 dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 12 V M ICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOK0235 - 3051A 6010 - EPA 601 OB Matrix Spike Dup (BOK0235-MSD1) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Cadmium 1.26 0.0989 mg/kg 1.24 102 75-125 200 20 dry Calcium 1480 49.4 mg/kg 247 1100 153 75-125 23.3 20 dry Copper 18.6 0.989 mg/kg 12.4 10.3 67.7 75-125 9.70 20 dry Lead 21.3 0.989 mg/kg 12.4 13.3 64.2 75-125 2.34 20 dry Magnesium 767 24.7 mg/kg 247 405 147 75-125 9.69 20 dry Molybdenum 24.6 2.97 mg/kg 24.7 ND 99.4 75-125 3.46 20 dry Nickel 14.5 1.98 mg/kg 12.4 1.63 104 75-125 2.13 20 dry Phosphorus 435 49.4 mg/kg 247 249 75.5 75-125 5.93 20 dry Potassium 1600 49.4 mg/kg 1240 330 102 75-125 6.00 20 dry Selenium 10.6 0.989 mg/kg 9.89 5.30 53.3 75-125 1.62 20 dry Sodium 1190 24.7 mg/kg 1240 ND 96.4 75-125 4.45 20 dry Zinc 39.6 0.989 mg/kg 24.7 13.3 106 75-125 9.24 20 dry Post Spike (BOK0235-PS1) Source: KOJO203-01 Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 17.9 mg/L 5.00 12.9 99.6 80-120 Arsenic 0.199 mg/L 0.200 0.00154 99.0 80-120 Cadmium 0.0262 mg/L 0.0250 0.00190 97.0 80-120 Copper 0.545 mg/L 0.250 0.305 96.1 80-120 Lead 0.245 mg/L 0.250 0.00846 94.5 80-120 Magnesium 26.0 mg/L 5.00 21.2 96.3 80-120 Molybdenum 0.560 mg/L 0.500 0.0454 103 80-120 Nickel 0.242 mg/L 0.250 0.0109 92.5 80-120 Phosphorus 6.32 mg/L 5.00 1.35 99.3 80-120 Potassium 26.4 mg/L 25.0 0.529 104 80-120 Selenium 0.198 mg/L 0.200 0.000117 99.1 80-120 Sodium 33.1 mg/L 25.0 7.67 102 80-120 Zinc 1.18 mg/L 0.500 0.707 93.7 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 10 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Definitions %: Percent % (by wt.): Percent by Weight D3: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time M5: Post digestion spike is outside of acceptance limits. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 7.3°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and Reported: 11 /23/2020 08:20 reviewed at <httas://www.microbac.com/standard-terms-conditions>. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 11 of 12 "KPP OJccPP0203' Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-8774 fE CHAIN OF CUSTODY RECORD PAGE— OFF_ CLIENT NAME B ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 Po PROJECT I LOCATION: Cordova - 60-da series #OF a O T T L E S TYPE OF ANALYSIS PRESERVATION CODE E 3 E U E E Q E = d W N Q `D o U U U E > rh C Co J E > y a c� Y Z Ur = p N E pO� 03 < ¢ LN Z Zo Z Z a a o IL Z IP- CL a v) o o CODE: A = None B = HNO3 (pH< 2 ) + -WC C=H2SO4(pH<2)+<4'C D= NaOH + c4°C E= ZN Acetate + c4'C F= HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910 410-9131 SAMPLER: / 1 t DATE I METHOD OF SHIPMENT: Microbac LAB ID ar SAMPLE TYPE DATE TIME COMP DRAG PH D.O. TEMP °C CHLORINE Residual from paper plant / I ZO X 2 A A A I A I A A A A A 1 1 A A A A A A A A A Relinquis Date Time It= e • (signature) Date Time Relinquished by Data Time Received by. (Signature) Data Tune 3 4 Relinquished by: Date me Received by. (slgnatun) Date Time 5 6 Comm is or Spedal Hazards: �5 `5T REVIIEEQ\WED Page 12 o 112 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Project Description Residuals Sample -Annual For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Friday, March 6, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 14 0MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Von Drehle Corporation Project Name: Residuals Sample - Annual Mr. Chris Fowler Project / PO Number: 2030767 126 First Street Received: 02/25/2020 Cordova, NC 28330 Reported: 03/06/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from paper plant KOB0372-01 Solid Grab 02/25/20 12:09 02/25/20 14:57 Page 2 of 14 VMICROBA(-' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Analytical Testing Parameters Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K080372-01 Collection Date: 02/25/2020 12:09 Inorganics Total EPA 9045D pH SW-846 7.3.3.2 Reactive Cyanide SW-846 7.3.4.1 Reactive Sulfide General Parameters ASTM D2216-10 Percent Solids EPA 1030 Ignitability of Solids Metals TCLP by AA EPA 7470A Mercury Metals TCLP by ICP EPA 6010B Arsenic Barium Cadmium Chromium Lead Selenium Silver Volatile Organic Compounds TCLP by GCMS EPA 8260E Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note Prepared Analyzed Analyst 8.4 S.U. 1 H4 03/05/20 1526 03/05/20 1630 EPT <10.0 10.0 mg/kg 1 y 03/06/20 1110 03/06/20 1146 JRH <100 100 mg/kg 1 y 03/06/20 1006 03/06/20 1048 EPT Result RL Units Dilution Note Prepared Analyzed Analyst 38.0 1.00 % (by wt.) 1 y 03/03/20 1327 03/04/20 0609 C9 <2 2 2.2 mm/sec 1 y 03/04/20 0000 CSH Result RL Units Dilution Note Prepared Analyzed Analyst <0.00200 0.00200 mg/L 1 03/02/20 0656 03/03/20 1013 TMM Result RL Units Dilution Note Prepared Analyzed Analyst <0.200 0.200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL 0.246 0.100 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL <0.0200 0.0200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL <0.0500 0.0500 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL <0.200 0.200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL <0.350 0.350 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL <0.100 0.100 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Result RL Units Dilution Note Prepared Analyzed Analyst Benzene <50.0 50.0 ug/L 10 2-Butanone <100 100 ug/L 10 Carbon tetrachloride <50.0 50.0 ug/L 10 Chlorobenzene <50.0 50.0 ug/L 10 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com 03/04/20 1723 ZTL 03/04/20 1723 ZTL 03/04/20 1723 ZTL 03/04/20 1723 ZTL Page 3 of 14 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0372-01 Collection Date: 02/25/2020 12:09 Volatile Organic Compounds TCLP by GCMS Chloroform 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogate: 4-B romofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1,2-Dichloroethane-d4 Surrogate: Toluene -dB Herbicides TCLP by GC/ECD EPA 9151 A 2,4,5-TP (Silvex) [2C] 2,4-D [2C] Surrogate: 2,4-Dichloropenylacetic acid [2C] Pesticides TCLP by GC/ECD EPA 8081 A alpha -Chlordane Enddn gamma Chlordane gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogate: 2,4, 5,6-Tetrach loro-m-xylene Surrogate: Decachlorobiphenyl (BZ-209) Semivolatile Organic Compounds TCLP by GCMS EPA 8270C Result RL Units Dilution Note Prepared Analyzed Analyst <50.0 50.0 ug/L 10 03/04/20 1723 ZTL <50.0 50.0 ug/L 10 y 03/04/20 1723 ZTL <50.0 50.0 ug/L 10 y 03/04/20 1723 ZTL <50.0 50.0 ug/L 10 03/04/20 1723 ZTL <50.0 50.0 ug/L 10 03/04/20 1723 ZTL <100 100 ug/L 10 03/04/20 1723 ZTL 104 Limit: 86-115 % Rec 10 03/04/20 1723 ZTL 95.9 Limit: 86-118 % Rec 10 03/04/20 1723 ZTL 93.5 Limit: 80-120 % Rec 10 03/04/20 1723 ZTL 104 Limit: 88-110 % Rec 10 03/04/20 1723 ZTL Result RL Units Dilution Note Prepared Analyzed Analyst <2.00 2.00 ug/L 1 03/02/20 1600 03/03/20 2006 ECL <20.0 20.0 ug/L 1 03/02/20 1600 03/03/20 2006 ECL 53.7 Limit: 20-144 % Rec 1 03/02/20 1600 03/03/20 2006 ECL Result RL Units Dilution Note Prepared Analyzed Analyst <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL <10.0 10.0 ug/L 1 03/02/20 0910 03/04/20 2152 ECL 74.0 Limit: 20-130 % Rec 1 03/02/20 0910 03/04/20 2152 ECL 49.9 Limit: 25-140 % Rec 1 03/02/20 0910 03/04/20 2152 ECL Result RL Units Dilution Note Prepared Analyzed Analyst Pyridine <250 250 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB 1,4-Dichlorobenzene <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB 2-Methylphenol <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB 3-,4-Methylphenol <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB Hexachloroethane <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB Nitrobenzene <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB Microbac Laboratories, Inc. 2592 Hope Mills Rd 1 Fayetteville, NC 28306 1910.864.1920 p 1 www.microbac.com Page 4 of 14 (�)MICROBAC'ql Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0372-01 Collection Date: 02/25/2020 12:09 Semivolatile Organic Compounds TCLP by GCMS Hexachlorobutadiene 2,4,6-Trchlorophenol 2,4, 5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Surrogate: 2-Fluorophenol Surrogate: Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-Fluorobiphenyl Surrogate: 2,4,6-Tribromophenol Surrogate: p-Terphenyl-d14 Result RL Units <50.0 50.0 ug/L <50.0 50.0 ug/L <50.0 50.0 ug/L <50.0 50.0 ug/L <50.0 50.0 ug/L <250 250 ug/L 59.0 Limit: 19-119 % Rec 36.0 Limit: 10-120 % Rec 89.7 Limit: 35-114 % Rec 94.9 Limit: 43-116 % Rec 149 Limit: 22-142 % Rec 84.3 Limit: 10-130 % Rec Dilution Note Prepared Analyzed Analyst 1 y 03/02/20 1350 03/03/20 1716 SCB 1 y 03/02/20 1350 03/03/20 1716 SCB 1 y 03/02/20 1350 03/03/20 1716 SCB 1 y 03/02/20 1350 03/03/20 1716 SCB 1 y 03/02/20 1350 03/03/20 1716 SCB 1 y 03/02/20 1350 03/03/20 1716 SCB 1 03/02/20 1350 03/03/20 1716 SCB 1 03/02/20 1350 03/03/20 1716 SCB 1 03/02/20 1350 03/03/20 1716 SCB 1 03/02/20 1350 03/03/20 1716 SCB 1 S1 03/02/20 1350 03/03/20 1716 SCB 1 03/02/20 1350 03/03/20 1716 SCB Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 14 MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Inorganics Total Result RL Batch B00O292 - Wet Chem -Default Prep - EPA 9045D Spike Source Units Level Result %REC %REC RPD Limits RPD Limit Notes LCS (B00O292-BSI) Prepared & Analyzed: 03/05/2020 pH 6.0 S.U. 6.03 99.6 0-200 LCS (B00O292-BS2) Prepared & Analyzed: 03/05/2020 pH 9.0 S.U. 9.01 100 0-200 Duplicate (B00O292-DUP1) Source: KOB0372-01 Prepared &Analyzed: 03/05/2020 pH 8.6 S.U. 8.4 1.89 5 Batch B000321 - Wet Chem -Default Prep - SW-846 7.3.4.1 Blank (B000321-BLK1) Prepared &Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg LCS (B000321-BS1) Prepared &Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg 474 50-150 LCS (B000321-BS2) Prepared & Analyzed: 03/06/2020 Reactive Sulfide 1250 100 mg/kg 1580 79.1 50-150 Duplicate (B000321-DUP1) Source: MOB2142-01 Prepared & Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg ND 50 Batch B000326 - Reactive Cyanide/Sulfide - SW-846 7.3.3.2 LCS (B000326-BS1) Prepared &Analyzed: 03/06/2020 Reactive Cyanide <500 500 mg/kg 0.5-100 Duplicate (B000326-DUP1) Source: MOB2142-01 Prepared &Analyzed: 03/06/2020 Reactive Cyanide <10.0 10.0 mg/kg ND 50 General Parameters Result RL Batch B000130 - Wet-Solids-S -ASTM D2216-10 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Blank (B000130-BLK1) Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 100 1.00 % (by wt.) LCS (B000130-BS1) Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 77.6 % (by 80.0 97.0 90-110 wt.) Duplicate (B000130-DUP1) Source: KOB0372-01 Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 38.2 1.00 % (by 38.0 0.499 10 wt.) Batch B000168 - Ignitability Prep - EPA 1030 LCS (B000168-BS1) Prepared &Analyzed: 03/04/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 0 14 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000168 - Ignitability Prep - EPA 1030 LCS (B000168-BS1) Ignitability of Solids 2.5 Metals TCLP by AA Result Batch B000010 - EPA 245.1 & EPA 7470A - EPA 7470A Prepared & Analyzed: 03/04/2020 2.2 mm/sec 2.4 102 88-111 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Blank (B000010-BLK1) Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury <0.000200 0.000200 mg/L LCS (B000010-13SI) Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.00388 0.000200 mg/L 0.00400 96.9 80-120 Matrix Spike (B000010-MS1) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.0378 0.00200 mg/L 0.0400 ND 94.4 75-125 Matrix Spike Dup (B000010-MSD1) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.0373 0.00200 mg/L 0.0400 ND 93.2 75-125 1.31 20 Post Spike (B000010-PSI) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.965 ug/L 1.00 0.00927 95.6 85-115 Spike Source %REC RPD Metals TCLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000013 - 3015A 6010 - EPA 6010B Blank (B000013-BLK1) Prepared & Analyzed: 03/02/2020 Arsenic <0.0250 0.0250 mg/L Barium <0.0125 0.0125 mg/L Cadmium <0.00250 0.00250 mg/L Chromium <0.00625 0.00625 mg/L Lead <0.0250 0.0250 mg/L Selenium <0.0438 0.0438 mg/L Silver <0.0125 0.0125 mg/L LCS (B000013-BS1) Prepared &Analyzed: 03/02/2020 Arsenic 0.242 0.0250 mg/L 0.250 97.0 80-120 Barium 0.627 0.0125 mg/L 0.625 100 80-120 Cadmium 0.0311 0.00250 mg/L 0.0313 99.6 80-120 Chromium 0.314 0.00625 mg/L 0.313 101 80-120 Lead 0.321 0.0250 mg/L 0.313 103 80-120 Selenium 0.236 0.0438 mg/L 0.250 94.5 80-120 Silver 0.247 0.0125 mg/L 0.250 98.9 80-120 Matrix Spike (B000013-MS1) Source: MOB1971-02 Prepared & Analyzed: 03/02/2020 Arsenic 0.243 0.0250 mg/L 0.250 ND 97.3 75-125 Barium 0.666 0.0125 mg/L 0.625 0.0255 103 75-125 Cadmium 0.0313 0.00250 mg/L 0.0313 ND 100 75-125 Chromium 0.319 0.00625 mg/L 0.313 ND 102 75-125 Lead 0.323 0.0250 mg/L 0.313 ND 103 75-125 Selenium 0.239 0.0438 mg/L 0.250 ND 95.6 75-125 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 14 VMICROBAC!` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOBO372 Spike Source %REC RPD Metals TCLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000013 - 3015A 6010 - EPA 6010B Matrix Spike (B000013-MS1) Source: MOB1971-02 Prepared &Analyzed: 03/02/2020 Silver 0.252 0.0125 mg/L 0.250 ND 101 75-125 Matrix Spike Dup (B000013-MSD1) Source: MOB1971-02 Prepared & Analyzed: 03/02/2020 Arsenic 0.248 0.0250 mg/L 0.250 ND 99.1 75-125 1.75 20 Barium 0.662 0.0125 mg/L 0.625 0.0255 102 75-125 0.617 20 Cadmium 0.0311 0.00250 mg/L 0.0313 ND 99.6 75-125 0.681 20 Chromium 0.318 0.00625 mg/L 0.313 ND 102 75-125 0.133 20 Lead 0.321 0.0250 mg/L 0.313 ND 103 75-125 0.590 20 Selenium 0.245 0.0438 mg/L 0.250 ND 97.9 75-125 2.40 20 Silver 0.249 0.0125 mg/L 0.250 ND 99.6 75-125 1.13 20 Post Spike (B000013-PSI) Source: MOB1971-01 Prepared & Analyzed: 03/02/2020 Arsenic 0.193 mg/L 0.200 0.000963 95.9 75-125 Barium 0.512 mg/L 0.500 0.0143 99.5 75-125 Cadmium 0.0247 mg/L 0.0250 0.000036( 98.7 75-125 Chromium 0.249 mg/L 0.250 0.000450 99.4 75-125 Lead 0.252 mg/L 0.250 0.00155 100 75-125 Selenium 0.189 mg/L 0.200 -0.000378 94.5 75-125 Silver 0.196 mg/L 0.200 -0.000288 98.2 75-125 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B000167 - 5030 8260 - EPA 8260B Blank (B000167-BLK1) Prepared & Analyzed: 03/04/2020 Benzene <5.00 5.00 ug/L 2-Butanone <10.0 10.0 ug/L Carbon tetrachloride <5.00 5.00 ug/L Chlorobenzene <5.00 5.00 ug/L Chloroform <5.00 5.00 ug/L 1,2-Dichloroethane <5.00 5.00 ug/L 1,1-Dichloroethene <5.00 5.00 ug/L Tetrachloroethene <5.00 5.00 ug/L Trichloroethene <5.00 5.00 ug/L Vinyl chloride <10.0 10.0 ug/L Surrogate:4-8romofluorobenzene 24.4 ug/L 25.0 97.6 86-115 Surrogate: Dibromoiluoromethane 23.7 ug/L 25.0 94.7 86-118 Surrogate:1,2-Dichloroethane-d4 23.4 ug/L 25.0 93.6 80-120 Surrogate: Toluene -dB 24.5 ug/L 25.0 98.1 88-110 LCS (B000167-BSI) Prepared &Analyzed: 03/04/2020 Benzene 20.6 5.00 ug/L 20.0 103 80-121 2-Butanone 20.5 10.0 ug/L 20.0 103 10-170 Carbon tetrachloride 18.5 5.00 ug/L 20.0 92.5 65-140 Chlorobenzene 20.6 5.00 ug/L 20.0 103 80-120 Chloroform 18.8 5.00 ug/L 20.0 94.1 80-125 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 14 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B000167 - 5030 8260 - EPA 8260E LCS (B000167-BS1) 1,2-Dichloroethane 18.4 1,1-Dichloroethene 20.1 Tetrachloroethene 19.0 Trichloroethene 19.1 Vinyl chloride 16.8 Surrogate: 4-Bromofluorobenzene Surrogate: Dibromolluoromethane Surrogate: 1, 2-Dichloroethane-d4 Surrogate: Toluene-0 LCS Dup (B000167-BSD1) Benzene 2-Butanone Carbon tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride 20.6 20.9 18.2 20.8 18.7 18.2 19.7 19.2 19.1 16.7 23.0 23.8 23.0 24.2 Prepared & Analyzed: 03/04/2020 5.00 ug/L 20.0 92.0 80-129 5.00 ug/L 20.0 100 80-132 5.00 ug/L 20.0 94.8 80-124 5.00 ug/L 20.0 95.6 80-122 10.0 ug/L 20.0 84.2 50-170 ug/L 25.0 92.1 86-115 ug/L 25.0 95.2 86-118 ug/L 25.0 91.8 80-120 ug/L 25.0 97.0 88-110 Prepared & Analyzed: 03/04/2020 5.00 ug/L 20.0 103 80-121 0.215 10.0 ug/L 20.0 104 10-170 1.58 5.00 ug/L 20.0 91.0 65-140 1.61 5.00 ug/L 20.0 104 80-120 1.11 5.00 ug/L 20.0 93.7 80-125 0.441 5.00 ug/L 20.0 91.2 80-129 0.825 5.00 ug/L 20.0 98.3 80-132 2.13 5.00 ug/L 20.0 96.0 80-124 1.23 5.00 ug/L 20.0 95.4 80-122 0.236 10.0 ug/L 20.0 83.6 50-170 0.711 Surrogate: 4-Bromofluorobenzene 23.9 ug/L Surrogate: Dibromofluoromethane 24.5 ug/L Surrogate: 1,2-Dichloroethane-d4 23.9 ug/L Surrogate: Toluene -dB 24.7 ug/L Herbicides TCLP by GC/ECU Result RL Units Batch B000069 - 8151 WATER - EPA 8151A Blank (B000069-BLK1) 2,4,5-TP (Silvex) [2C] 2,4-D [2C] Surrogate: 2,4-Dichloropenylacetic acid [2C] LCS (B000069-BSI) 2,4,5-TP (Silvex) [2C] 2,4-D [2C] <0.200 0.200 <2.00 2.00 4.90 0.427 0.200 4.34 2.00 Surrogate: 2,4-Dichloropenylacetic acid [2C] 5.03 LCS Dup (B000069-BSD1) 2,4,5-TP (Silvex) [2C] 0.354 2,4-D [2C] 3.74 Surrogate.. 2,4-Dichloropenylacetic acid 12C] 4.19 0.200 25.0 95.6 86-115 25.0 98.2 86-118 25.0 95.4 80-120 25.0 99.0 88-110 Spike Source %REC Level Result %REC Limits 20 20 20 20 20 20 20 20 20 20 RPD RPD Limit Notes Prepared: 03/02/2020 Analyzed: 03/03/2020 ug/L ug/L ug/L 5.00 98.1 20-144 Prepared: 03/02/2020 Analyzed: 03/03/2020 ug/L 0.500 85.4 25-120 ug/L 5.00 86.8 20-110 ug/L 5.00 101 20-144 Prepared: 03/02/2020 Analyzed: 03/03/2020 ug/L 0.500 70.7 25-120 18.9 ug/L 5.00 74.8 20-110 14.8 ug/L 5.00 83.9 20-144 T 30 30 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 14 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC Pesticides TCLP by GC/ECD Result RL Units Level Result %REC Limits RPD Batch B000027 - 351OC 8081 - EPA 8081A RPD Limit Notes Blank (B000027-BLK1) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane <0.0500 0.0500 ug/L Endrin <0.0500 0.0500 ug/L gamma Chlordane <0.0500 0.0500 ug/L gamma-BHC (Lindane) <0.0500 0.0500 ug/L Heptachlor <0.0500 0.0500 ug/L Heptachlor epoxide <0.0500 0.0500 ug/L Methoxychlor <0.0500 0.0500 ug/L Toxaphene <1.00 1.00 ug/L Surrogate:2,4,5,6-Tetrachloro-m-xylene 0.141 ug/L 0.200 70.4 20-130 Surrogate. Decachlorobiphenyl (BZ-209) 0.155 ug/L 0.200 77.4 25-140 LCS (B000027-BSI) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 0.536 0.0500 ug/L 0.500 107 40-120 Endrin 0.544 0.0500 ug/L 0.500 109 40-138 gamma Chlordane 0.543 0.0500 ug/L 0.500 109 40-136 gamma-BHC (Lindane) 0.559 0.0500 ug/L 0.500 112 30-134 Heptachlor 0.519 0.0500 ug/L 0.500 104 40-130 Heptachlor epoxide 0.473 0.0500 ug/L 0.500 94.7 40-120 Methoxychlor 0.558 0.0500 ug/L 0.500 112 40-150 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 0.153 ug/L 0.200 76.6 20-130 Surrogate Decachlorobiphenyl (BZ-209) 0.154 ug/L 0.200 76.9 25-140 LCS (B000027-BS2) Prepared: 03/02/2020 Analyzed: 03/04/2020 Toxaphene 1.71 1.00 ug/L 2.00 85.3 41-126 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 0.147 ug/L 0.200 73.7 20-130 Surrogate: Decachlorobiphenyl (BZ-209) 0.147 ug/L 0.200 73.7 25-140 LCS Dup (B000027-BSD1) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 0.566 0.0500 ug/L 0.500 113 40-120 5.44 30 Endrin 0.563 0.0500 ug/L 0.500 113 40-138 3.40 30 gamma Chlordane 0.558 0.0500 ug/L 0.500 112 40-136 2.80 30 gamma-BHC (Lindane) 0.589 0.0500 ug/L 0.500 118 30-134 5.18 30 Heptachlor 0.543 0.0500 ug/L 0.500 109 40-130 4.63 30 Heptachlor epoxide 0.492 0.0500 ug/L 0.500 98.3 40-120 3.81 30 Methoxychlor 0.578 0.0500 ug/L 0.500 116 40-150 3.49 30 Surrogate: 2,4,5,6-Tetrach1oro-m-xy1ene 0.164 ug/L 0.200 82.1 20-130 Surrogate: Decachlorobiphenyl (BZ-209) 0.158 ug/L 0.200 79.1 25-140 Matrix Spike (B000027-MSI) Source: MOB1987-01 Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 5.30 0.500 ug/L 5.00 ND 106 40-120 Endrin 5.54 0.500 ug/L 5.00 ND 111 40-138 gamma Chlordane 5.38 0.500 ug/L 5.00 ND 108 40-136 gamma-BHC (Lindane) 5.65 0.500 ug/L 5.00 ND 113 30-134 Heptachlor 4.70 0.500 ug/L 5.00 ND 93.9 40-130 Heptachlor epoxide 4.74 0.500 ug/L 5.00 ND 94.7 40-120 Methoxychlor 5.44 0.500 ug/L 5.00 ND 109 40-150 Surrogate: 2,4,5,6-Tetrach1oro-m-xy1ene 1.39 ug/L 2.00 69.3 20-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 10 of 14 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD Pesticides TCLP by GC/ECU Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000027 - 3510C 8081 - EPA 8081A Matrix Spike (B000027-MS1) Surrogate: Decachlorobiphenyl (BZ-209) Semivolatile Organic Result Compounds TCLP by GCMS Batch B000055 - 3510C 8270 - EPA 8270C Blank (B000055-BLK1) Pyridine 1,4-Dichlorobenzene 2-Methylphenol 3-,4-Methylphenol Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4, 6-Trichlorophenol 2,4, 5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Surrogate: 2-FI uorophenol Surrogate: Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-FI uorobiphenyl Surrogate: 2, 4, 6-Tribromophenol Surrogate: p-Terphenyl-04 Blank (B000055-BLK2) Pyridine 1,4-Dichlorobenzene 2-Methylphenol 3-,4-Methylphenol Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4, 5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Surrogate: 2-FI uoroph enol Surrogate: Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-Fl uorobiph enyl Surrogate: 2, 4, 6-Tribromophenol Surrogate: p-Terphenyl-04 Source: MOB1987-01 Prepared: 03/02/2020 Analyzed: 03/04/2020 0.849 ug/L 2.00 42.5 25-140 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Prepared: 03/02/2020 Analyzed: 03/03/2020 <25.0 25.0 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <25.0 25.0 ug/L 58.4 ug/L 100 58.4 19-119 36.8 ug/L 100 36.8 10-120 41.1 ug/L 50.0 82.3 35-114 44.1 ug/L 50.0 88.2 43-116 124 ug/L 100 124 22-142 53.5 ug/L 50.0 107 10-130 Prepared: 03/02/2020 Analyzed: 03/04/2020 <25.0 25.0 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <25.0 25.0 ug/L 58.4 ug/L 100 58.4 19-119 35.8 ug/L 100 35.8 10-120 41.5 ug/L 50.0 82.9 35-114 43.9 ug/L 50.0 87.9 43-116 128 ug/L 100 128 22-142 52.2 ug/L 50.0 104 10-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 11 of 14 6)MICROBAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD Semivolatile Organic Result RL Units Level Result %REC Limits RPD Limit Notes Compounds TCLP by GCMS Batch B000055 - 3510C 8270 - EPA 8270C LCS (B000055-BS1) Prepared: 03/02/2020 Analyzed: 03/03/2020 Pyridine <25.0 25.0 ug/L 50.0 48.8 10-100 1,4-Dichlorobenzene 38.9 5.00 ug/L 50.0 77.7 29-112 2-Methylphenol 43.3 5.00 ug/L 50.0 86.5 30-120 3-,4-Methylphenol 40.4 5.00 ug/L 50.0 80.9 20-130 Hexachloroethane 38.1 5.00 ug/L 50.0 76.2 21-115 Nitrobenzene 46.1 5.00 ug/L 50.0 92.2 40-120 Hexachlorobutadiene 47.8 5.00 ug/L 50.0 95.5 22-124 2,4,6-Trichlorophenol 55.3 5.00 ug/L 50.0 111 50-135 2,4,5-Trichlorophenol 55.6 5.00 ug/L 50.0 111 53-123 2,4-Dinitrotoluene 58.4 5.00 ug/L 50.0 117 57-128 Hexachlorobenzene 57.9 5.00 ug/L 50.0 116 53-125 Pentachlorophenol 60.5 25.0 ug/L 50.0 121 35-138 Surrogate:2-Fluorophenol 57.5 ug/L 100 57.5 19-119 Surrogate: Phenol-d5 38.4 ug/L 100 38.4 10-120 Surrogate: Nitrobenzene-d5 41.8 ug/L 50.0 83.6 35-114 Surrogate:2-Fluorobiphenyl 44.1 ug/L 50.0 88.1 43-116 Surrogate:2,4,6-Tribromophenol 129 ug/L 100 129 22-142 Surrogate: p-Terphenyl-04 53.7 ug/L 50.0 107 10-130 LCS Dup (B000055-BSD1) Prepared: 03/02/2020Analyzed: 03/03/2020 Pyridine <25.0 25.0 ug/L 50.0 48.6 10-100 0.528 30 1,4-Dichlorobenzene 38.8 5.00 ug/L 50.0 77.6 29-112 0.125 30 2-Methylphenol 43.2 5.00 ug/L 50.0 86.5 30-120 0.0516 30 3-,4-Methylphenol 39.7 5.00 ug/L 50.0 79.5 20-130 1.70 30 Hexachloroethane 38.9 5.00 ug/L 50.0 77.9 21-115 2.16 30 Nitrobenzene 47.7 5.00 ug/L 50.0 95.5 40-120 3.54 30 Hexachlorobutadiene 47.6 5.00 ug/L 50.0 95.3 22-124 0.267 30 2,4,6-Trichlorophenol 56.6 5.00 ug/L 50.0 113 50-135 2.42 30 2,4,5-Trichlorophenol 55.1 5.00 ug/L 50.0 110 53-123 0.943 30 2,4-Dinitrotoluene 59.1 5.00 ug/L 50.0 118 57-128 1.24 30 Hexachlorobenzene 60.1 5.00 ug/L 50.0 120 53-125 3.71 30 Pentachlorophenol 62.8 25.0 ug/L 50.0 126 35-138 3.62 30 Surrogate:2-Fluorophenol 58.3 ug/L 100 58.3 19-119 Surrogate: Phenol-d5 38.9 ug/L 100 38.9 10-120 Surrogate: Nitrobenzene-d5 42.1 ug/L 50.0 84.2 35-114 Surrogate:2-Fluorobiphenyl 44.8 ug/L 50.0 89.6 43-116 Surrogate:2,4,6-Tribromophenol 132 ug/L 100 132 22-142 Surrogate: p-Terphenyl-04 54.2 ug/L 50.0 108 10-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 12 of 14 VMICROBAC'`� Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Definitions % (by wt.): Percent by Weight H4: The test was performed outside of the EPA recommended holding time of 15 minutes. mg/kg: Milligrams per Kilogram mg/L: Milligrams per Liter mm/sec: Millimeter per Second 03: LCS recovery is below acceptance limits. The reported value is estimated. 04: ICV recovery is above acceptance limits. The reported value is estimated. R1: Duplicate RPD is outside of acceptance limits. RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units S1: Surrogate recovery is above acceptance limits. ug/L: Micrograms per Liter ug/mL: Micrograms per Milliliter Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 8.3°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and subject to Microbac's standard terms and conditions which can be located and Administration reviewed at <httas://www.mlcrobac.com/standard-terms-conditions>. Reported: 03/06/2020 19:15 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 13 of 14 *KOB0372* Mlcrobac-Fayetteville (PMICROBAC' 2592 Hope Mills Rd. CHAIN OF CUSTODY RECOR 1 111j 1I[]I see�[ 111ttt I�[ Fayetteville, NC 2309 Number Wulf ItII III pJI11�9� InstrucUms on beck Lab Report Address Invoice Address Turnaround Time TO BE COMPLETEDSYMICfi Client Name: V0.401 M It Client Name: [] Routine (5 to 7 business days) Temp. Upon Receipt rC)3. 3 Tharm ID Address: Address: [] RUSH* (notify lab) Holding Time Clty, State, Zlp: ddva City, State, ZIP: (needed by) Samples Recelvod on le No NIA .. Contact: rw�G Contact ReportType Custody Seels Intact? as o WA Telephone No.: Telephone No.: Results Only [ ] Level I [ ] Level 2 [] Lave17 [ ] Level [ Send Re�ortvia: —[1Mag _ [ ] Fax [x),e-mail _. send Inv_oice_via: 1_1 M_'.N.! _j. l F??I-.I] e; mad .• Project _ cation: PO_ No.: Com_pllancaMon!todng? []Yes• (.],Noj_JAgenWProgram, _ Sampled 6y,(PRINT�_ h a/'%'�L J�'f _ _ Sampler Slgnatug _ Sampler Phone Ng_ _ _ .— _. __ _ _ _•.._--.____ — ..- ' Mabix Types: So5/Sogd (S), Sludge, 09, Wlpe, Drinking Water (OW), undwater(GW), Surface Water (SW), Waste Water (WM, 09er (specify) "Preselvagve T r. 1) HN07, H2SO4, (3 HCI, 4 Nal H, ( Zinc Acetate, (9) Methanol, Sodium Biaulfale, (6 Sodium Th!osNfate, (9) Hexane, (U) Unpresarved Lab ID I Client Sample ID . I Collected I CVetted me I Containers I Matrix) C or p I P type etive � / / / / / / / / / / / / / I Addldonal Nafes ate, 0b -Possible Hazardldentificatio []Hazardous []Non -Hazardous []Radloactiva Sam []Dlsposeasapproprlate• []Return []Archive REVIEWED Rdin a lure " J ],.S-o •Reei By(signalure) 512oMmL r P RallrrfuTsihod By (signature) DateMme Received By (signature) DetaTitms Relinquished By (signature) Date/Time 'Received By (signature) Datemme I Paae 14 of 14 1 PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 3/l/2020 To 4/30/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) Rl > »> > > ........ A1t.D (No Prior Test) ❑ Process to Further Reduce Patlio ens O If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thenno 1Mlic❑ .•........ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ............. . Class B: JAIt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying Ll Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ ..................... . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er of Excee Frequency of Analysis Sample Type Analytical Tech- Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.8 Grams 0 imonthl Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) O 1 Alt. 3 (30-day bench) LJ JAlt, 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ JAlt 7 (Drying - Stable) LJ JAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El I No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the `—' vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) z�& - —O� /� / Sig re of Preparer* Date Signa of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WWTP Name: Cordova Facility Monitoring Period: From 5/1/2020 To WQ Permit Number: NPDES Number: 6/30/2020 WQ0005135 NA Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El ........... A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[]Thernio lulic❑ ........... ..................... Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ ........... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ jAerobic Digestion ❑ ........... .............. . Anaerobic Digestion ❑ .............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o Excee- Frequency of Analysis Sample Type Anaica Tech- Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) < 0.7 NA < 0.7 Grams 0 imonthl) Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-daybench) ❑ jAlt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) Ll I Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." U "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer N e and Title (type or print) Land Applier N and Title (if applicable)(type or print) Signature of Preparer* Date Signa of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 7/l/2020 To 8/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ 71 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) �l Alt.D (No Prior Test) L Process to Further Reduce Pathogens J If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat D in ❑ Heat Treatment❑ Thenno lulic❑ ..................... Beta Ray ❑ Ganuna Ray ❑ Pasteurization 11 Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ; If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ _.. _..... _ ...................... If applicable to alternative performed (Class A or Class B) complete the followinj monitoring data: Parameter Allowable Level in Sludge Pathogen Density Numner or Excee- Frequency of Aal sis Sample Type Analytical Tech - Minimum Geo. Mean aximu Unitsfienrec Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.7 GPa/s 0 imonthl Grab 16g2 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ 1 Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ jAlt 7 (Drying - Stable) Ll Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El jNo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 9/l/2020 To 10/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) 1J Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El ...... .. AIt.D (No Prior Test) J Process to Further Reduce Pathogens ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying Ll Heat Treatment[] Thenno lulic❑ Beta Ray ❑ Gamma Ray Ll Pasteurization ❑ Class B: jAlt. (1) Fecal Density L] I Alt. (2) Process to Significantly Reduce Pathogens J ....... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying LJ I Composting . ] jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NumDer of Excee- r1pnrpc Frequency of Analysis Sample Type Anal ica Tech - Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram oftotal solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per grams total solid (dry weight) <0.3 NA 0.7 GPams 0 imonthl Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) Lj I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) Ll JAIt. 8 (Drying - Unstable) L] Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier N e and Title (if applicable)(type or print) '� Z Z� al Signature of Preparer* Date Signature o Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 11/1/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A71 Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) AIt.D (No Prior Test) ❑ Process to Farther Reduce Patho ens v If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermo liilic❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density 01 Alt. (2) Process to Significantly Reduce Pathogens ❑ If a plicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ I Air Dryuig L] Composting ❑ Aerobic Digestion Ll Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample Typeninup na ►ca Tech- MinimumGeo. Mean MaximumUnits Fecal Colifotm 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.7 MPN/ 0 imonthl Grab 11682 Vector Attraction Reduction (I k NCAC 02T .1107) -Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAlt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) U JAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed Cl CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the y vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applie ame and Title (if applicable)(type or print) o ZJ 2 1 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) FECAL COLIFORM AND SALMONELLA DOCUMENTATION Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jan - Feb 2020 Biological Consulting Services ............ . ................. a It Z .................. Ile ............................... * atue ii ar. ............ ............ ............... .......... ......... .... ................ ....... ............ 'T: I ... ... ..... ... tgi' :. j.r. Y. ..... ...... 2002077 2/6/20 < 0.07 < 0-6 2002078 2/6/20 < 0.07 < 0.6 2002079 2/6/20 < 0.07 < 0.6 2002080 2/6/20 < 0.07 < 0.7 2002081 2/6/20 0.07 0.8 2002082 2/6/20 < 0.07 < 0.6 2002083 2/6/20 < 0.07 < 0.7 ....... Exceedances ... . .... ............... All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. nc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. February 14, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis IMethod Salmonella JEPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, 1."'.-� �•,/�Vil.i.h.. � 1����.L �.. Yam... Bonnie Mull, MPH Laboratory Operations Manager - Page 1 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-1 Sample Date/Time: February 05, 2020 13:42 BCS Sample ID: 2002077 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 45.8 Amount Analyzed: 29.98 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-2 Sample Date/Time: February 05, 2020 13:45 BCS Sample ID: 2002078 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 42.8 Amount Analyzed: 30.10 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950. EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11�G-A3EiA' � � M Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-3 Sample Date/Time: February 05, 2020 13:48 BCS Sample ID: 2002079 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 44.7 Amount Analyzed: 30.10 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-4 Sample Date/Time: February 05, 2020 13:52 BCS Sample ID: 2002080 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 39.9 Amount Analyzed: 29.99 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mI- sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ,IlaC=Milk A JM p7 . ;: ., Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-5 Sample Date/Time: February 05, 2020 13:55 BCS Sample ID: 2002081 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 38.5 Amount Analyzed: 30.10 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 13, 2020 13:46 Analyst: Jessica Weglarz, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-6 Sample Date/Time: February 05, 2020 13:59 BCS Sample ID: 2002082 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 40.3 Amount Analyzed: 30.00 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:201 7 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTENRITTEN CONSENT OF BCS LABORATORIES 0."�% flac-WA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-7 Sample Date/Time: February 05, 2020 14:03 BCS Sample ID: 2002083 Sample Description: Biosolid Date Received: February 06, 2020 9:56 Amount Submitted:100 mL bottle % Solids: 39.5 Amount Analyzed: 30.09 g Receipt Temperature: 3.1 deg C Preserved: Yes Analysis Start: February 06, 2020 10:15 Analysis Stop Date: February 11, 2020 13:13 Analyst: Jessica Weglarz, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 6&03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6of8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES l AAW I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: February 14, 2020 Page 7 of 8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11c1 __ . DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8of8 Final Report BCS ID 2002077, 2002078, 2002079, 2002080, 2002081, 2002082, 2002083 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:201 7 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES i(ac-nRA 10W =� CHAIN OF CUSTODY RECORD www.microbioservices.com FL DOH Laboratory #E82924. EPA# FL01147 BCS Laboratories 4609 NW 6th street, Building A Gainesville, FL 32609 Tel. (352) 377-9272, Fax. (352) of-5630 Client Name and Address: �) G1 t �- �£ 'S I / 7 S �," •� (r j�,J'I �� f � Compliance Monitoring? E] Yes No City/State/Zip: �oCV_. J;: /?l7 c' Project ID: Nlc t j_��b Project Manager: I)., L '6 .ail. Facility/Site: Telephone Number: Fax No.: Report To: L Sampler Name: (Print) l,ip, F� ;?,._ -f' Email: j (� �;1,1, I-(� ti,��. �i'e; •�� Sampler Signature: E;1t.t f .(✓ Invoice To: 54-•t Matrix u U mLu a t c V` `o c w arc a a uN�i E o. arFaxd W Wa . • E EU. E NC N D Z 0 Cw 01 —° rn r u¢Oi c° U c m cc o Sample ID Description E v E a- ' ° s io ¢u>i c uL UJ to = m a r a z •>`.=. O o z ). r)Z Branch Residuals and Soils VD 2002077 021061202D 9:56 Branch Residuals and Soils VD•2 2Do2078 Oy0612020 9:56 Branch Residuals and Soils 2002080 D210612020 9:66 Branch Residuals and Soils VD-5 2002081 0210612020 9:66 I I r o a 0 K N a �'�% 7 I•`•/7 } �' 1.11 Y V i) U T I —0 -.5- ): fj j 1 T ( 1 Branch Residuals and Soils Branch Residuals and Soils VD-3 2002079 VD-6 2002082 m 02/09/2020 9:66 0210612020 9:56 Special Instructions: Laboratory Comments: Method of Shipment: '/ UPS) Postal DHL FEDEX Other: Temp. @ recp't: Ic� -C IR• LQ Conectedtar-Iq Custody Seal: Intact Broken t Nl�YY% 71,76itl byy/� Date l�. Time Received by: Date Time %? %- __ '/ 1--' Presence of visable ice C�(f N Presence of ice picks 1`Y N Re inquished by: Date Time Received by BCS Laboratories- Date Time 5 ) 20 J � Hold Time a•-_...•,w.•,ar.crn.....•...•a,�,.,.....•-..., r..-r;a:a.acxw-,,. ,�: _:t•..� Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Mar Apr 2020 Biological Consulting Services L"Ab::Y.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:..:..on ........................................................................................................................................................................................ ..................................................... .... ............................. ........ ....... . i�* u":al on : ................................................ ........................................................ .... .... ............ ............................*.............. .. . ... . 2004007 4/2/20 < U.U-/ < U.N 2004008 4/2/20 < 0.07 < 0.7 2004009 4/2/20 < 0.07 < 0.7 2004010 4/2/20 < 0.07 < 0.7 2004011 4/2/20 < 0.07 < 0.7 2004012 4/2/20 < 0.07 < 0.6 2004013 4/2/20 < 0.07 < 0.7 Exceedances ........... ... . ...... ... All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. inc, BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. April 07, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: N/A Analysis IMethod Salmonella 1EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD1 BCS Sample ID: 2004007 Date Received: April 02, 2020 9:58 Sample Date/Time: April 01, 2020 13:42 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 34.4 Amount Analyzed: 30.06 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD2 Sample Date/Time: April 01, 2020 13:45 BCS Sample ID: 2004008 Sample Description: Biosolid Date Received: April 02, 2020 9:58 Amount Submitted:100 mL bottle % Solids: 35.9 Amount Analyzed: 30.00 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �� K 1i C MRA ¢ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD3 BCS Sample ID: 2004009 Date Received: April 02, 2020 9:58 Sample Date/Time: April 01, 2020 13:48 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 38.6 Amount Analyzed: 30.04 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD4 Sample Date/Time: April 01, 2020 13:51 BCS Sample ID: 2004010 Sample Description: Biosolid Date Received: April 02, 2020 9:58 Amount Submitted:100 mL bottle % Solids: 37.6 Amount Analyzed: 29.97 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilaC-MRA � .«hr , Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD5 BCS Sample ID: 2004011 Date Received: April 02, 2020 9:58 Amount Analyzed: Analysis Start: Analyst 29.97 g April 02, 2020 11:34 Wei -yea Hsu, M.S. Sample Date/Time: April 01, 2020 13:54 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 37.2 Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Stop Date: April 07, 2020 9:35 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD6 Sample Date/Time: April 01, 2020 13:58 BCS Sample ID: 2004012 Sample Description: Biosolid Date Received: April 02, 2020 9:58 Amount Submitted:100 mL bottle % Solids: 41.1 Amount Analyzed: 29.92 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD7 Sample Date/Time: April 01, 2020 14:01 BCS Sample ID: 2004013 Sample Description: Biosolid Date Received: April 02, 2020 9:58 Amount Submitted:100 mL bottle % Solids: 38.5 Amount Analyzed: 30.00 g Receipt Temperature: 5.9 deg C Preserved: Yes Analysis Start: April 02, 2020 11:34 Analysis Stop Date: April 07, 2020 9:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES llac-� �$ Client: Branch Residuals and Soils Project: N/A Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES latTmRA I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: April 07, 2020 Page 7 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 1 7025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES IOM P� 11c�C-MESA A� sNOW DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2004007, 2004008, 2004009, 2004010, 2004011, 2004012, 2004013 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 1 7025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 7 i17c-A MRf¢` CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A �r �L FL DOH Laboratory #E82924, EPA# FL01147 Gainesville, FL 32609 7 , J 1 Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: J- l r-1'1: I �'e "`' ' �` ' S ' h� 1�" �� �''{ '� (a Z41 Compliance Monitoring? E]Yes No City/State/Zip: i,'� .: t' 5L' 7 ' j y' i Project ID: Project Manager: h'„ {; is K:_a.,- Facility/Site: Telephone Number: Fax No.: Report To: �" Li �a1 Sampler Name: (Print) Email: I, " a• r.l` Sampler Signature: t"--fJ Invoice To: Rem Branch Residuals and Soils VD1 2004007 0410212020 9:58 by: C O r, � _d � t5�� t3p U7 a) m`a C ro d f0 0 -4 is E r _ 101. '° i= a ❑ P z t7 U tL X Q.Fw Z u C7 (' k -N Branch Residuals and Sails Branch Residuals and Sails V02 vo3 _ 2004008 2004009 04102/2020 9:58 0410212020 9:58 - Method of Shipment UPS Postal DHL FEDEX Date Time Received by: -- Date Date Time lReceived by BCS Laboratories Date q "2 U s EL N H •> N Q. Q 2 E E E ma v vm .t3oz C °� C w In .np m 0 3 ots °u L c" p N c C aI .. Q I- L o •- m m r4 E e' E m .8 a) 3 L to p 5 a ... d n Branch Residuals and Soils VD4 2004010 04102/2020 9:58 ' 1 1 Branch Residuals and Soils V05 2004011 041021202D 9:58 N IA O 'p N N Laboratory Comments:: " l �j -4 1-3 -C Temp. @ recp't: ` -' • 1e IR-' p Custody Seat: Intact Corrected for IR Broken Presence of visable ice Y 1e Presence of ice packs N (JJ Hold Time Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 May Jun 2020 Biological Consulting Services ................................ .... .. ....................... Ile-.$a. moo ... 4: .......... ........... ....... ... ....................... .. .....er:n ::.: ........................ :: ::4:' e: r 2006154 6/12/20 < 0.07 < 0.7 2006155 6/12/20 < 0.07 < 0.7 2006156 6/12/20 < 0.07 < 0.7 2006157 6/12/20 < 0.07 < 0.7 2006158 6/12/20 < 0.07 < 0.7 2006159 6/12/20 < 0.07 < 0.7 2006160 6/12/20 < 0.07 < 0.7 ....... .......... ........ ................... .... ................... .... ................... Exceedances ................ ......... ........................................ ................................... All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. inc BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, /NC. June 17, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:201 7 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD1 BCS Sample ID: 2006154 Date Received: June 12, 2020 9:59 Amount Analyzed: 30.10 g Analysis Start: June 12, 2020 10:40 Sample Date/Time: June 11, 2020 13:52 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 39.7 Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD2 BCS Sample ID: 2006155 Date Received: June 12, 2020 9:59 Amount Analyzed: 30.04 g Analysis Start: June 12, 2020 10:40 Analyst: Wei -yea Hsu, M.S. Sample Date/Time: June 11, 2020 13:54 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 39.7 Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Stop Date: June 17, 2020 10:35 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .lac a"AB! Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD3 BCS Sample ID: 2006156 Date Received: June 12, 2020 9:59 Amount Analyzed: 30.10 g Analysis Start: June 12, 2020 10:40 Sample Date/Time: June 11, 2020 13:56 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 39.7 Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD4 BCS Sample ID: 2006157 Date Received: June 12, 2020 9:59 Amount Analyzed: 29.97 g Analysis Start: June 12, 2020 10:40 Sample Date/Time: June 11, 2020 13:58 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 38.8 Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 113C'4SBA' A" Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD5 Sample Date/Time: June 11, 2020 14:00 BCS Sample ID: 2006158 Sample Description: Biosolid Date Received: June 12, 2020 9:59 Amount Submitted:100 mL bottle % Solids: 39.7 Amount Analyzed: 29.99 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: June 12, 2020 10:40 Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD6 Sample Date/Time: June 11, 2020 14:02 BCS Sample ID: 2006159 Sample Description: Biosolid Date Received: June 12, 2020 9:59 Amount Submitted:100 mL bottle % Solids: 39.9 Amount Analyzed: 30.09 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: June 12, 2020 10:40 Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES iladq If�A` p1< Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD7 Sample Date/Time: June 11, 2020 14:05 BCS Sample ID: 2006160 Sample Description: Biosolid Date Received: June 12, 2020 9:59 Amount Submitted:100 mL bottle % Solids: 39.2 Amount Analyzed: 30.10 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: June 12, 2020 10:40 Analysis Stop Date: June 17, 2020 10:35 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11ae�RA $� Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Intact Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES a S� ac; AP&B`� I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: June 17, 2020 Page 7 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Jlacawx, 41" DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numericvalue given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2006154, 2006155, 2006156, 2006157, 2006158, 2006159, 2006160 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES aeJailAJIM CHAIN OF CUSTODY RECORD BC$ Laboratories www.microbioservices.com 4609 NW 6th Street, Building A W,07�:l r-c • FL DOFI Laboratory #E82924, EPA# FL01147 Gainesville, FL 32609 Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: i'-' rW 'r Cs 1. �''> ��' Compliance Monitoring? CYes❑ No City/State/Zip: due! fl; (1 :'c Project ID: Project Manager: ii41 Facility/Site: Telephone Number: 33L 31Fax No.: Report To: Sampler Name: (Print) Iii i Email: .`•_, r �,��,l,f bKa ;�,� ;.may` Sampler Signature: ti"i-' Invoice To: Branch Residuals and Soils Matrix I Analysis VO4 2006157 2 v S 2 U 06112I2020 9:59 p � � �- e. a = N (if S Branch Residuals and Sails u m u p , j -0 y` U X X p o a CL V05 d d '° a h m E o: v q m 2006156 n T a y N u `w +D L° a 1= > N E m U o C g a 06112I2020 9:59 m E u `� 0 6 -'� r H ii _a`! 3 i rn ,3 va c _ o= 0 _ 0 'o -' o f n _ Q in m in E o n o ii. v " m E o w 5 g U o u c E p E U _ U c rn c rn o �° )ample ID I Description i- d z 1p a E v �, v L o u, '° c o Co L i I°- u ou a=� :6 I-- c°> w m n" _° 0 u m as <° i w z r o in c `✓(.� ( /, i!/p I • i 2 I - Branch Residuals and Soils Vol tt 7 l Y r 2006154 0611212020 9:59 Branch Residuals and Soils VD2 O6M212020 9:59 Branch Residuals and Sods t•y Y •D 4 ' %• S �� I i' j �•' t y / Y % V03 2006156 Branch Residuals and Sods Branch Residuals and Soils VD6 VD7 06/1212020 9:59 2006159 2006160 0611212020 9:59 06/12/2020 9:69 _ ipeciai Instructions: Laboratory Comments-- Method of ShipmentUPS "Postal FEDEX Other Temp. @ recp't:•C R. , J� Corrected for IR Custody Seal: Broken N/A tell qu!she l)y �r Date Time Received by Date Time y,i Presence of vfeable Ice Presence of Ice pac N telinquished by: Date Time RIYLVE/b(►y/11BI/CS rie alte Time rLabor�i i_ 9 �C� H�Id Time �.�,,.� Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jul - Aug 2020 Biological Consulting Services ............................. Anal jr. V I . r. ...a. UO ........ a ..... Y on �Nig .... moo ... 0:** .......... .................................... .................. ..... ........... ................... .................. .... .... ........ . ........ . ................................. ... ................. ................................... M-P .N:::: ef� igrams: 2007337 7/23/20 < 0.07 < 0.7 2007338 7/23/20 < 0.07 < 0.6 2007339 7/23/20 < 0.07 < 0.6 2007340 7/23/20 < 0.07 < 0.7 2007341 7/23/20 < 0,07 < 0.7 2007342 7/23/20 < 0.07 < 0.6 2007343 7/23/20 < 0.07 < 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. Inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, /NC. July 29, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova NC Analysis IMethod Salmonella 1EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, wWITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilac-h'IRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-1 Sample Date/Time: July 22, 2020 13:45 BCS Sample ID: 2007337 Sample Description: Biosolid Date Received: July 23, 2020 9:55 Amount Submitted:100 mL bottle % Solids: 35.2 Amount Analyzed: 29.95 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: July 23, 2020 10:50 Analysis Stop Date: July 28, 2020 9:33 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-2 Sample Date/Time: July 22, 2020 13:47 BCS Sample ID: 2007338 Sample Description: Biosolid Date Received: July 23, 2020 9:55 Amount Submitted:100 mL bottle % Solids: 40.2 Amount Analyzed: 30.10 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: July 23, 2020 10:50 Analysis Stop Date: July 29, 2020 9:16 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 113C4ARAAlf i �% �". �71. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-3 BCS Sample ID: 2007339 Date Received: July 23, 2020 9:55 Amount Analyzed: 30.09 g Analysis Start: July 23, 2020 10:50 Sample Date/Time: July 22, 2020 13:49 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 41.7 Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Stop Date: July 29, 2020 9:16 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-4 BCS Sample ID: 2007340 Date Received: July 23, 2020 9:55 Amount Analyzed: 29.94 g Analysis Start: July 23, 2020 10:50 Sample Date/Time: July 22, 2020 13:51 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 39.3 Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Stop Date: July 29, 2020 9:16 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES i13C9hRA .......... Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-5 BCS Sample ID: 2007341 Date Received: July 23, 2020 9:55 Amount Analyzed: 29.98 g Analysis Start: July 23, 2020 10:50 Analyst: Wei -yea Hsu, M.S. Sample Date/Time: July 22, 2020 13:52 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 38.3 Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Stop Date: July 29, 2020 9:16 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-6 BCS Sample ID: 2007342 Date Received: July 23, 2020 9:55 Amount Analyzed: 30.10 g Analysis Start: July 23, 2020 10:50 Sample Date/Time: July 22, 2020 13:53 Sample Description: Biosolid Amount Submitted:100 mL bottle % Solids: 42.3 Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Stop Date: July 29, 2020 9:16 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AAB �`�'�� Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD-7 Sample Date/Time: July 22, 2020 13:55 BCS Sample ID: 2007343 Sample Description: Biosolid Date Received: July 23, 2020 9:55 Amount Submitted:100 mL bottle % Solids: 41.6 Amount Analyzed: 30.10 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: July 23, 2020 10:50 Analysis Stop Date: July 29, 2020 9:16 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AA=T!t! Client: Branch Residuals and Soils Project: Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, A7-DHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES :lac")/iufRps � �•�� I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: July 29, 2020 Page 7 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES la fNR TNI DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2007337, 2007338, 2007339, 2007340, 2007341, 2007342, 2007343 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, /WIITHHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ii�G-=.fihftA CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A FL DOH Laboratory #E82924, EPA# FLO1147 Gainesville, FL 32609 >A � <` 0,(1 Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: 1/ y,_ , leez , ^ S r ' sw' • ='� �r 1 Compliance Monitoring? CYes❑ No City/State/Zip: i CcC--V W(I -i c r 1 7 3 Z Project ID: E cJ i `I -I I D Project Manager: i 9 -�i�� �. �- �� Facility/Site: CcEcly+n,Nc Telephone Number: 3s'G- fit ' `? cc, Fax No.: Report To: _ PeA,—k- SamplerName:(Print) P,0j, Email: (J%12ry z"I r DC czk2sc— Sampler Signature: Invoice To: SFr Branch Residuals and Sails Matrix Analysis VD-6 2007342 N 2 •u m •9 ;� r; 07123/2020 9:55 c v u T, _ N U Branch Residuals and Soils VD-7 2007343 0712312020 9:55 am le ID ! Description a rn m n E F C L " :o d z 19 �' o y w m i T '� a O U o u E FT U a `0 m� m N D ran N " n u c 2` y v o y 1p t to w m m 3 o t. U _ 0a) D N d ;Z' w `w o a w to m m 3 V A 10 c:i °5 E v 0 o a r� € 0 u- > E x° - `.� c, a f0 o E w ._ U F° _ ui :r_ W `w, a m U a O t E U U m c '2 °� X X w O m c X X w O u o �' w �XXC W D M Or- m a> yl C rr o ~ m¢ Q. 3 z L o m a < m L ai \i- - ( %lit I_q- i - it > 2 Branch Residuals and Soils l VD-1 2007337 0712312020 9:55 �,r 7 -Llj I . 5 1 '}5' 11, Branch Residuals and Soils VD-2 2007338 I:53 07123/20209:55 HL Branch Residuals and Soils VD-3 Branch Residuals and Soils Branch Residuals and Suits 2007339 VD-4 VD-5 07/2312020 9:55 2007340 2007341 pecial Instructions: 0712312020 9:55 ' 07,2312020 9:55 Laboratory Comments: G 1 Method of Shipment. UPS) Postal FEDEX Other: Temp. 0 recp't: C E02 Dat 7/� 2 jZ Time 2, Received by. Date Time IR- [ /. Custody Seal: Intact -/ Broken Correcled tor,IR J Presence of visable ice elinquished by: Date Time Received by.}CS Laboratories: ale Presence of ice pac -� N 1�t/-•.L'�` 1.1 (j i�Time �, IHold Time m;,.-,,...�.«.:.•.,. Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Sept Oct 2020 Midwest Laboratories ........................................................................................ L#a...x#nalyze,..: :.:.:.:.:.:.:.....:.:.........:.:.....................:.....:.........:.:.:.:...:.:.:...:......:.....:...:.....:.. ....................................................................................... to �.� . e - n ...:.:::.:al e� :l uo � l ,.eo..da�r3... u..a.....nel.a.:. `e'i °' r . 1564389-01 9/17/20 <0.3 1564389-02 9/17/20 <0.3 1564389-03 9/17/20 <0.3 1564389-04 9/17/20 0.7 1564389-05 9/17/20 0.7 1564389-06 9/17/20 <0.3 1564389-07 9/17/20 <0.3 o All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. / 1 Midwest / Laboratories' 24 September 2020 Robert Branch Branch Residuals & Soils - 56895 1735 Heckle Blvd. Rock Hill, SC 29732 RE: Von Drehle Cordova Midwest Laboratories 13611 B Street Omaha, NE 68144 P 402-334-7770 F 402-334-9121 www.midwestlabs.com Work Order: 1564389 Enclosed are the results of analyses for samples received by the laboratory on 2020-09-16 11:20. If you have any questions concerning this report, please feel free to contact me. Sincerely, Heather Ramig Project Manager heather@midwestlabs.com The result(s) issued an this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 1 of 14 Midwest ` 13611 B Street 13611 B Street Laboratories' Omaha, P 402-33434-77707770 F 402-334-9121 www.midwestiabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received VD-1 1564389-01 Solid 2020-09-1514:02 2020-09-1611:20 VD-2 1564389-02 Solid 2020-09-1514:24 2020-09-1611:20 VD-3 1564389-03 Solid 2020-09-1514:18 2020-09-1611:20 VD-4 1564389-04 Solid 2020-09-1514:15 2020-09-1611:20 VD-5 1564389-05 Solid 2020-09-1514:09 2020-09-1611:20 VD-6 1564389-06 Solid 2020-09-15 14:11 2020-09-16 11:20 VD-7 1564389-07 Solid 2020-09-1514:27 2020-09-1611:20 Containers used for the following analyses: 1564389-01 A: EPA 1682, SM 2540 G 1564389-02 A: EPA 1682, SM 2540 G 1564389-03 A: EPA 1682, SM 2540 G 1564389-04 A: EPA 1682, SM 2540 G 1564389-05 A: EPA 1682, SM 2540 G 1564389-06 A: EPA 1682, SM 2540 G 1564389-07 A: EPA 1682. SM 2540 G Analysis Results Reviewed by: SM 2540 G reviewed by jdb5. EPA 1682 reviewed by jzh4. The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable lest parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 2 of 14 Midwest Midwest Laboratories 13611 B Street ♦ Laboratories' Omaha, NE P 402-334-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-1 Laboratory ID: 1564389-01 Sampled DateTme: 2020-09-15 14:02 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 40.99 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella < 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 3 0f 4 ' Midwest 13611 B Street 13611 B Street ` Laboratories' Omaha, NE 68144 P 402-334-77704-7770 F 402-334-9121 www.midwestiabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-2 Laboratory ID: 1564389-02 Sampled Datemme: 2020-09-15 14:24 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 39.92 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella < 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 4 of 4 Midwest Midwest Laboratories 1611 3611 B Street . Laboratories' Omaha, NE P 402-334-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-3 Laboratory ID: 1564389-03 Sampled Date/Time: 2020-09-15 14:18 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 42.98 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella < 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued an this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 5 Of= Midwest 13611 B Street 13611 B Street + r Laboratories' Omaha, NE 8144 P 402-334-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-4 Laboratory ID: 1564389-04 Sampled DateTme: 2020-09-15 14:15 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 40.16 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella 0.7 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 6 o= Midwest Midwest Laboratories 13611 B Street ♦ Laboratories' Omaha, NE P 402-334-777 4 4-7770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-5 Laboratory ID: 1564389-05 Sampled Date/Time: 2020-09-1514:09 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 39.28 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella 0.7 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 7 o= Midwest Midwest Laboratories 13611 B Street ♦ Laboratories' Omaha, NE P 402-334-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-6 Laboratory ID: 1564389-06 Sampled Date/Time: 2020-09-15 14:11 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 39.80 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella < 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16116:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 8 o= Midwest 13611 B Street 13611 B Street . Laboratories' Omaha, NE P 402-334-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Sample ID: VD-7 Laboratory ID: 1564389-07 Sampled DateMme: 2020-09-15 14:27 Dry Weight Reporting As Received (Container) / Analyte Result Limit Units Result Method Prepared Analyzed Analyst Notes Environmental Chemistry Percent Solids 0.01 % 41.18 % SM 2540 G 2020-09-16 2020-09-17 ssm5 (A) Microbiology Salmonella < 0.3 MPN/4g < MPN/4g EPA 1682 2020-09-16/16:44 2020-09-21/15:00 kas2 (A)/ HT dry The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 9 Of 14 Midwest Midwest Laboratories 13611 B Street . Laboratories' Omaha, NE 68144 P 402-334-77704-7770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Environmental Chemistry - Quality Control Reporting Spike Source %REC RPD IAnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B006424 Blank (B006424-BLK1) Percent Solids LCS (B006424-BSI) Percent Solids Duplicate (B006424-DUP1) Percent Solids Duplicate (B006424-DUP2) Percent Solids 100.0 0.01 % 96.58 0.01 % Source: 1564389-03 42.97 0.01 % Source: 1564265-02 1.460 0.01 % Prepared: 2020-09-16 Analyzed: 2020-09-17 Prepared:2020-09-16 Analyzed:2020-09-17 97.1 99.5 80-120 Prepared: 2020-09-16 Analyzed: 2020-09-17 42.98 0.0233 20 Prepared:2020-09-16 Analyzed:2020-09-17 1.470 0.683 20 The result(s) issued an this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 10 o= Midwest 13611 B Street 13611 B Street Laboratories' Omaha, P 402-33434-77707770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Certified Analyses included in this Report Method Analyte Certifications EPA 1682 in Solid Salmonella FL,WA SM 2540 G in Solid Percent Solids FL, IA,WA Code Description Number Expires FL Florida Department of Health E87918 06/30/2021 IA Iowa Department of Natural Resources 064 05/01/2021 KS Kansas Department of Health and Environment E-10402 04/30/2020 NE State of Nebraska Dept of Health & Human Services NE-04-05 06/30/2021 OK Oklahoma Department of Environmental Quality 2019-094 08/31/2021 TX Texas Commission on Environmental Quality T104704416-20-14 07/31/2021 UT State of Utah Department of Health NE000012020-10 07/31/2021 WA State of Washington Department of Ecology C912 06/07/2020 The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 11 of 4 ` Midwest Midwest Laboratories 13611 B Street ♦ Laboratories' Omaha, NE 68144 402-334-7770 P 402-334-7770 F 402-334-9121 www.midwestlabs.com Branch Residuals & Soils - 56895 Project: Von Drehle Cordova 1735 Heckle Blvd. Reported: Rock Hill, SC 29732 Project Manager: Robert Branch 2020-09-24 17:38 Notes and Definitions HT Hold time exceeded, not suitable for regulatory purposes. < Less than reporting limit NR Not Reported dry Sample results reported on a dry weight basis RPD Relative Percent Difference EPA 524.2, EPA 624, EPA 8260, OA-I, TCLP VOC, GRO, and all microbiological analyses are conducted in the facility located at 13606 B Street, Omaha, NE 68144. All other analyses are conducted in the main facility located at 13611 B Street, Omaha, NE 68144. The result(s) issued on this report only reflect the analysis of the sample(s) submitted. For applicable test parameters, Midwest Laboratories is in Work Order: 1564389 compliance with NELAC requirements. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Page 12 Of 4 /�\ midwes Midwest Laboratories, Inc 136116 Street, Omaha, NE 66144 •j: R aboratOrICS- 402-334- 770 Account Number/ Company Name: 1# Purchase Order: -.- a I V 71%'ame:BA41a6,JI ss:!}35� �iK1P fv 103'Z7 Ciry, State: gxx. EQI/ SC ZIP: zi L Fhone:313wa-2ev1 FAX: Ibn Email:1ZAv pe—ve�K�•CA W W154tlbq CHAIN OF CUSTODY RECORD Chain of Custody Record: Yes I.(� No Samples for Regulatory Use: Yesj No �! o• a Oier.t Name: VcsFName: Sample ID: Address: _ Sample Date: T( (j- EC ZR. Sample rime: Phone: PROJECT INFORMATION BOTTLE ORDER INFO TESTS REQUESTED o - ID yIl���-o_ri `iii�i �C%Q.�owt COMMAi.ct r COMPANY: (Spnatvn),��� 1. D s�s✓v ,n z oC .. Z 4 1 1 �• I I Lab Number/ Order tt Use) SAMPLER: (SgiaN11 r ' ( a m 0 (Internal SAMPLE ID/ LOCATION DATE TIME U z a f c c 2 I n- v ' Z`� ! ► j I v 5 I Z I 2- v I -&I l' f l `F MEW T564389 QQ coc �� _ f I i Sticker #:1 I i I 1 Rant l �1 �a7 3.� -1 I R.wiv.d by:(Sgnamn) 4�yV,,t 1120 Cooler ^ arrived m(act: Yes !rl No L I or, Arrival: ut haau by. (Slpnitua� -- Egrd7ln. R.c/ga bS: 1 V Temperature ----_I In Field: Yes � No u aanipuanad ay.(agn:Dan; D:wrma i Raabaa bS: (sgnamn) Preserved Chain orcoucq, wdl baw a agnatM Upon ranlpttaa a UI;Wu Ogmtu b:J��lir �'.f 1'���1 %C�RMvc•Ip.�weyMk DIYs:batia,nu,ginal acxompnuessMpm.nC mDY tJ lnaOlnatarFWtl.FINa S p-J 1��4es Cad. SO-5aa, WA-WaSer. SL-S6dge. Or-0tRer C41, 33( 31Z 4co� IQv.6 -a -In dta ab. or q»dac Wtnsai nto tM mRra .Midw.at LM—Wrin w411an13r" your WMPKI) Using -.deed cart maeuda(,A—ava.bbl.). RC FORM C!v.]-Fff. ae397DA i1, Midwest f Laboratories® Lab Number: Thermometer Used: ❑ Therm Fisher 1R I to Sample Temperature (°C): Z- \ Sample Acceptance Checld Document Number: RC CUKLIST Revision No `o Effective Date: 1/31/2 r q Page 1 c 1*9 rn coc Sticker #: 2 0 Cooler Intact: Yes ❑ No Received on Ice: bbYes ❑ No Hand Delivered: ❑ Yes NNo [Date & Initials of person accenting samples: 1t4 Comments Chain of Custody resent? Yes I ❑ I No 0 N/A Sample 1D(s): C1Yes ❑ No ❑ N/A Sample Location(s): �b Yes ❑ No ❑ N/A Client contact tD Yes ❑ No 0 N/A Analysis Requested: ( Yes ❑ No ❑ N/A Date & Time of collection: Yes I0 No ❑ N/A Sampler name on COC? ja Yes ❑ No ❑ N/A Chain of custody relinquished with signature? Yes ❑ No 10 1 N/A Chain of custody complete? N Yes ❑ No ❑ N/A Sample labels match COC? CY Yes ❑ No ❑ N/A Written in indelible ink? �p Yes ❑ No 10 1 N/A Labels indicate proper preservation? Lk Yes ❑ No ❑ N/A Samples arrived within hold time? -& Yes D No ❑ N/A Samples arrived within correct temperature? Fl Yes ❑ No ❑ N/A Sufficient volume? Yes ❑ No ❑ N/A Appropriate containers used? Yes ❑ No ❑ N/A Filtered volume received for dissolved tests? ❑ Yes ❑ No 0 N/A Headspace in VOA vials? 0 Yes ❑ No Cr I N/A Trip Blank present? 10 Yes I * No 10 1 N/A Client Notification/Resolution: Date/Time Contacted: Person Contacted: Comments/Resolution: Contacted By: Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Nov Dec 2020 Biological Consulting Services .................................................. ..... ......... ......................... . ...... ....... . . .. . ............ . S a mon ................. Mon a**' e -.41"' . .. ...... ....... ........................... ......................... .............................................. ......................... ........................ ..... .... ...................... ....................... ...................... . ........... .......... per. m .............. P 2011362 11/24/20 < 0.07 < 0.7 2011363 11/24/20 < 0.07 < 0.7 2011364 11/24/20 < 0.07 < 0.6 2011365 11/24/20 < 0.07 < 0.-6 2011366 11/24/20 < 0.07 < 0.6 2011367 11/24/20 < 0.07 < 0.6 r 2011368 11/24/20 < 0.07 < 0.6 ................... ........ ... .................. ........ ... . ................... ................ Exceedances ................ ................ All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. inc BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, /NC. December 01, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES lac=iulRa` Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-1 Sample Date/Time: November 23, 2020 13:48 BCS Sample ID: 2011362 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 36.1 Amount Analyzed: 30.02 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-2 Sample Date/Time: November 23, 2020 13:50 BCS Sample ID: 2011363 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 40.0 Amount Analyzed: 29.96 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:201 7 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 118C-JNIRA` AI,AB �'�' Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-3 Sample Date/Time: November 23, 2020 13:52 BCS Sample ID: 2011364 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.0 Amount Analyzed: 30.00 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-4 Sample Date/Time: November 23, 2020 13:54 BCS Sample ID: 2011365 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 46.5 Amount Analyzed: 29.96 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Coo i#8C?iillFiA. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-5 Sample Date/Time: November 23, 2020 13:56 BCS Sample ID: 2011366 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 42.5 Amount Analyzed: 29.92 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-6 Sample Date/Time: November 23, 2020 13:58 BCS Sample ID: 2011367 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.2 Amount Analyzed: 30.08 g Analysis Start: November 24, 2020 11:45 Analyst: Robert Pimentel Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Stop Date: December 01, 2020 9:15 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025".2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A�M ' Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-7 Sample Date/Time: November 23, 2020 14:00 BCS Sample ID: 2011368 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.0 Amount Analyzed: 30.00 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 113C-d1IRA Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES i{ac-ate AAB�' I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. I y Date: December 01, 2020 Page 7 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence orabsence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ttaqgyp." CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A FL DOH Laboratory #E82924, EPA# FL01147 Gainesville, FL 32609 �,� 2 } J 1 i IV a 5 t �.- �t� - ; n Tel. (352) 377-9272, Fax. (352) 37 7-5630 Yes No C F Client Name and Address: l� L� 7 i �. 2`I I Compliance Monitoring? City/State/Zip: 2v' k. }�+ 11 5 C c' y j ? Project ID: Z ujq _ jj D Project Manager: ;?,I, (%^A c ( Facility/Site: vi ; 4 Telephone Number:.33(, ^i2•gLt'} Fax No.: Report To: Sampler Name: (Print) -',A-A Email: �,1,J-1Y4vvLq�,,At�A-� Sampler Signature: Invoice To: -"yd - - Branch Residuals and Soils Matrix Analysis VD-6 2D11367 111241202010:14 a ii �i " u -P \ _ a N d Residuals and Soils 2011366 Sample ID / Description °1 m n° n L N z 7 U = iL 4` d ° n A m E E N m u o111241202010:14 u ; n �.. o 0 C ' r v U °v U. � ca r nT u7 m cE ° a N O tE0 c m J f0OBranch g 2 X u` c LLJa> LU 0m E $ y o .3 w .c z L 0 d mV0 rQ3:E 'nD 0: / ` I Branch Residuals and Soils -P Z 13• St VD-1 v (� 2011362 13. sa I i {✓ 11/2412020 10:14 v7. L/ 13 3 � l Branch Residuals and Soils VD•2 2011363 11/24/2020 10:14 \1 I� uJ Branch Residuals D- and Soils Branch Residuals and Soils Branch Residuals and Soils 2011364 VD-1 VD-5 1112412D20 10:14 2011365 2011366 Special Instructions: 111241202010:14 111241202010:14 -aboratoryComments: 'Postal I i /� Method of Shipment: UP FEDEX Other: Temp. @ recp't: . `7 -C Repql5istied b : Date Time Received by:—' Date Time IR- I i Corrected for . I /7 Custody Seal: Intact Presence Ice Broken Y N/A--) N of visable �f% Relinquished by: Date Time Received by BCS Laboratories: Date Time Presence of Ice packs N �5��_•.Lr.r'..�- + � 'i (Hold Time ..Y.,,-.wF.rr / ux.m_.rv.-rsar.u.. SOIL ANALYSIS REPORTS Page 1 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 s Waypoint ANALYTICAL "Every acre... Every year. "m SOIL ANALYSIS REPORT Date Received: 11/03/2020 Date Of Analysis: 11/04/2020 Date Of Report: 11/18/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Analytical Method(s): Mehlich 3 SMP Buffer pH Olsen P Ammonium Acetate Loss On Ignition Water pH NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A BI ppm Rate M3 ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 3-1 03561 3.0 L 104 2 VL 5 L NC = 4 22.1 VL NC = 11 47.2 VL 2490 VH 10.8 VL 8.5 6.93 0.0 12.9 I MIN 3-2 03563 2.2 L 88 2 VL 4 L NC = 3 10.3 VL NC = 5 1 26.2 VL 12510 VH 1 5.28 VL 1 8.5 1 6.93 1 0.0 1 12.8 MIN 3-3A 03564 2.8 L 100 4 L 3 VL NC=2 9.31 VL NC=5 30.1 VL 12450 VH 6.69 VL 8.5 6.93 0.0 12.6 MIN 3-3B 03565 3.0 L 104 2 VL 3 VL NC=2 13.8 VL NC=7 31.4 VL 12540 VH 14.6 VL 8.5 6.93 0.0 13.1 MIN 3-4 03566 3.3 MH 110 2 VL 7 L NC=6 18.1 VL NC=9 35.6 VL 12560 VH 23.7 VL 8.5 6.93 0.0 13.2 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NO3 N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 3-1 0.4 3.0 96.5 0.4 0.0 8 L NC=17 8.7 H NC=217.5 6 VL NC=38 28 L 1.9 M NC=95.0 0.6 H 0.36 3-2 0.2 1.7 98.0 0.2 0.0 7 L NC=15 8.1 H NC=202.5 5 VL NC=31 18 VL 1.0 M NC=50.0 0.5 M 0.18 3-3A 0.2 2.0 97.2 0.2 0.0 9 L NC 9.5 VH NC=237.5 5 VL NC=31 17 VL 1.0 M NC=50.0 0.6 H 0.23 3-3B 0.3 2.0 96.9 0.5 0.0 13 M NC=27 10.2 VH NC=255.0 5 VL NC=31 16 VL 0.9 M NC=45.0 0.7 H 0.48 3-4 0.4 2.2 97.0 0.8 0.0 14 M NC=29 10.0 VH NC=250.0 6 VL NC=38 21 VL 0.8 L NC=40.0 0.9 H 0.78 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Tennessee, Inc. Oscar Ruiz Page 2 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 11 /03/2020 Date Of Report: 11/18/2020 r Waypoint ANALYTICAL "Every acre... Every year. ",m SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P2% K20 Mg S Zn Mn Fe Cu B Field ID bu/acre Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 31 Wheat 50 0.0 88 106 112 18 17 0 6 0 0 3-2 Wheat 50 0.0 88 106 121 25 18 0 6 0.8 0.5 3-3A Wheat 50 0.0 88 93 122 25 16 0 6 0.8 0 3-3B Wheat 50 0.0 88 106 119 25 13 0 6 0.9 0 3-4 Wheat 50 0.0 88 106 115 24 13 0 6 1.0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the ✓� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 3 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypoint(D ANALYTICAL "Every acre... Every year. SOIL ANALYSIS REPORT Date Received: 11 /03/2020 Date Of Analysis: 11 /04/2020 Date Of Report: 11,18/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Analytical Method(s): Mehlich 3 SMP Buffer pH Olsen P Ammonium Acetate Loss On Ignition Water pH NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A BI ppm Rate M3 ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 3-5 03567 2.5 L 94 2 VL 5 L NC=4 8.72 VL NC=4 22.3 VL 2510 VH 11.3 VL 8.5 6.93 0.0 12.8 MIN 3-6A 03568 2.4 L 92 2 VL 4 L NC=3 8.28 VL NC=4 21.4 VL 12620 VH 5.74 VL 8.4 6.93 0.0 13.3 MIN 3-6B 03569 2.1 L 86 3 VL 9 L NC=7 13.6 VL NC=7 25.4 VL 12910 VH 6.9 VL 8.4 6.93 0.0 14.8 MIN 3-6B1 03570 1.4 VL 72 3 VL 17 M NC = 14 5.43 VL NC = 3 11.7 VL 11730 VH 4.51 VL 8.3 6.93 0.0 8.8 MIN 4-1 03571 3.2 M 108 7 L 27 M NC = 22 32.3 VL NC = 17 39.3 VL 12570 VH 13.5 VL 8.3 6.93 0.0 13.3 MIN Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NON ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 3-5 0.2 1.5 98.0 0.4 0.0 14 M NC=29 9.2 VH NC=230.0 4 VL NC=25 16 VL 0.8 L NC=40.0 0.6 H 0.38 3-6A 0.2 1.3 98.5 0.2 0.0 9 L NC = 19 7.7 H NC = 192.5 3 VL NC = 19 20 VL 0.7 L NC = 35.0 0.5 M 0.19 3-6B 0.2 1.4 98.3 0.2 0.0 6 L NC=12 8.2 H NC=205.0 3 VL NC9 19 VL 0.6 L NC=30.0 0.5 M 0.20 3-6B1 0.2 1.1 98.3 0.2 0.0 4 VL NC=8 3.0 M NC=75.0 3 VL NC 35 L 0.5 L NC=25.0 0.1 VL 0.22 4-1 0.6 2.5 96.6 0.4 0.0 14 M NC=29 9.7 VH NC=242.5 10 VL NC=63 60 M 1.2 M NC=60.0 0.8 H 0.44 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium) H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Salts ms/cm x 640 = ppm. Analysis prepared by: Waypdnl Analytical Tennessee, Inc. Oscar Ruiz Page 4 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 11/03/2020 Date Of Report: 11 /18/2020 0 Waypo,,Int ANALYTICAL "Every acre... Every year. ",m SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID bu/acre Tons/A lb/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 3-5 Wheat 50 0.0 88 106 122 25 13 0 6 1.0 0 3-6A Wheat 50 0.0 88 106 122 25 16 0 6 1.1 0.5 3-68 Wheat 50 0.0 88 99 119 25 19 0 6 1.2 0.5 3-6B 1 Wheat 50 0.0 88 99 113 25 20 0 6 1.3 1.0 41 Wheat 50 0.0 88 75 103 22 13 0 5 0.6 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Jn work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 5 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypoint(D ANALYTICAL "Every acre... Every year.", SOIL ANALYSIS REPORT Date Received: 11/03/2020 Date Of Analysis: 11/04/2020 Date Of Report: 11/18/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Analytical Method(s): Mehlich 3 SMP Buffer pH Olsen P Ammonium Acetate Loss On Ignition Water pH NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A BI ppm Rate M3 ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 4-2 03572 4.1 M 126 10 M 11 L NC = 9 13.7 VL NC = 7 36 VL 2500 VH 7.24 VL 8.5 6.93 0.0 12.9 IMIN 4-3 03574 5.6 H 156 8 M 15 M NC = 12 10.1 VL NC = 5 28.4 VL 2510 VH 5.42 VL 8.5 6.93 0.0 12.8 MIN 4-4 03575 2.7 L 98 4 L 12 L NC = 10 14.7 VL NC = 8 28.9 VL 12600 VH 5.46 VL 8.4 6.93 0.0 13.3 MIN 4-5 03576 5.3 H 150 5 L 6 L NC=5 17.6 VL NC=9 38.5 VL 12540 VH 5.68 VL 8.4 6.93 0.0 13.1 MIN 4-6A 03577 3.2 MH 108 7 L 13 L NC = 11 21.7 VL NC = 11 40.2 VL 12560 VH 6.35 VL 8.4 6.93 0.0 13.2 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Exchangeable sodium Percentage % K % Mg % Ca % Na % H % NO, N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 4-2 0.3 2.3 96.9 0.2 0.0 11 M NC=23 12.4 VH NC=310.0 7 VL NC=44 21 VL 1.5 M NC=75.0 0.7 H 0.24 4-3 0.2 1.8 98.0 0.2 0.0 1 1 12 M NC=25 13.4 VH NC=335.0 6 VL NC=38 17 VL 1.6 M NC=80.0 0.5 M 0.18 4-4 0.3 1.8 97.7 0.2 0.0 10 L NC=21 10.4 VH NC=260.0 6 VL NC=38 19 VL 1.3 M NC=65.0 0.6 H 0.18 4-5 0.3 2.4 96.9 0.2 0.0 16 M NC=33 14.4 VH NC=360.0 7 VL NC=44 13 VL 1.0 M NC=50.0 0.6 H 0.19 4-6A 0.4 2.5 97.0 0.2 0.0 13 M NC=27 11.3 VH NC=282.5 7 VL NC=44 16 VL 0.9 M NC=45.0 0.6 H 0.21 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Tennessee, Inc. Oscar Ruiz Page 6 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 11 /03/2020 Date Of Report: 11/18/2020 o Waypoint ANALYTICAL "Every acre... Every year. ",M SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P2% K20 Mg S Zn Mn Fe Cu B Field ID bu/acre Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 4 2 Wheat 50 0.0 88 60 119 24 14 0 6 0 0 4-3 Wheat 50 0.0 88 70 121 25 14 0 6 0 0.5 4-4 Wheat 50 0.0 88 93 118 25 15 0 6 0.5 0 4-5 Wheat 50 0.0 88 87 115 23 12 0 6 0.8 0 4-6A Wheat 50 0.0 88 75 112 22 13 0 6 0.9 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the ✓� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 7 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypointl ANALYTICAL "Every acre... Every year. SOIL ANALYSIS REPORT Date Received: 11/03/2020 Date Of Analvsis: 11/04/2020 Date Of Report: 11/18/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 o Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehire Analytical Method(s): Mehlich 3 SMP Buffer pH Olsen P Ammonium Acetate Loss On Ignition Water pH NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A BI ppm Rate M3 ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 4-6B 03578 5.1 H 146 8 M 18 M NC = 15 23.3 VL NC = 12 46.7 VL 2660 VH 8.36 VL 8.5 6.93 0.0 13.8 MIN 4-7 03579 3.6 M 116 5 L 12 L NC = 10 13.8 VL NC = 7 36.6 VL 12640 VH 1 6.63 VL 1 8.5 1 6.93 1 0.0 1 13.6 MIN 4-8 03580 4.1 M 126 4 L 9 L NC = 7 27.5 VL NC = 14 46.2 VL 12720 VH 8.7 VL 8.4 6.93 0.0 14.1 MIN 4-9 03581 4.2 M 128 5 L 9 L NC=7 20.7 VL NC=11 46.3 VL 12970 VH 7.11 VL 8.4 6.93 0.0 15.3 MIN 4-10 03582 1.3 VL 70 3 VL 32 H NC = 27 18.6 VL NC = 10 22 L 490 VH 8.25 VL 6.7 6.92 0.1 2.8 MIN Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NO3 N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 4-613 0.4 2.8 96.4 0.3 0.0 14 M NC=29 13.4 VH NC=335.0 6 VL NC=38 21 VL 2.0 M NC=100.0 0.7 H 0.26 4-7 0.3 2.2 97.1 0.2 0.0 17 M NC=35 13.4 VH NC=335.0 6 VL NC=38 17 VL 1.8 M NC=90.0 0.6 H 0.21 4-8 0.5 2.7 96.5 0.3 0.0 15 M NC=31 13.7 VH NC=342.5 7 VL NC=44 16 VL 1.5 M NC=75.0 0.7 H 0.27 4-9 0.3 2.5 97.1 0.2 0.0 12 M NC=25 11.9 VH NC=297.5 6 VL NC=38 16 VL 1.5 M NC=75.0 0.6 H 0.20 4-10 1.7 6.5 87.5 1.3 3.6 5 L NC=10 1.2 L NC=30.0 10 VL NC=63 109 H 0.6 L NC=30.0 0.1 VL 1.28 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Tennessee, Inc. Salts ms/cm x 640 = ppm. Oscar Ruiz Page 8 of 8 Report Number: 20-308-9039 Account Number:22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 11/03/2020 Date Of Report: 11/18/2020 s Y Wa oint ANALYTICAL "Every acre... Every year. ". SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehlre Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P2% 1K20 Mg S Zn Mn Fe Cu B Field ID bu/acre Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A r6B Wheat 50 0.0 88 70 111 18 13 1 0 1 6 1 1 0 1 0 4-7 Wheat 50 0.0 88 87 119 24 11 0 6 0 0 4-8 Wheat 50 0.0 88 93 107 19 12 0 6 0 0 4-9 Wheat 50 0.0 88 87 113 25 14 0 6 0 0 4-10 Wheat 50 0.0 88 99 88 24 20 2.0 5 1.2 1.0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the ✓n work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz 2020 APPLICATION SUMMARY TABLE VON DREHLE CORPORATION LAND APPLICATION PROGRAM PERMIT NO. WQ0005135 2020 APPLICATION SUMMARY Tract $E . ...................... Fieid:::::::::2lcres::::::Dade:Spreacl:::::::Wet:Tiins.:.: ................................. ......................... ;. /o. Solids::::::::ACjre:::. Dry:Tons:/ ...... :::::::::::: ::.Dry. Tons Crop PAN 3 1 23 Sep-20 1,764.00 37.00 28.38 652.68 Wheat 2.39 2 9.1 Sep-20 686.00 37 27.89 253.82 Wheat 2.35 4 13.2 Oct-20 1,029.00 37 28.84 380.73 Wheat 2.43 5 11.1 Oct-20 857.50 37 28.58 317.28 Wheat 2.41 3A 18.9 Sep-20 1,347.50 37 26.38 498.58 Wheat 6.50 Nov-20 122.50 42.30 2.74 51.82 Wheat 3B 37.2 Sep-20 2,915.50 37.00 29.00 1,078.74 Wheat 2.44 6A 24.6 Nov-20 1,568.00 42.30 26.96 663.26 Wheat 42.09 6B 37.5 Oct-20 1,617.00 37.00 15.95 598.29 Wheat 21.19 Nov-20 1,127.00 42.30 12.71 476.72 Wheat 4 1 19.1 Jun-20 1,470.00 30.20 23.24 443.94 Wheat 3.67 Jul-20 73.50 36.30 1.40 26.68 Wheat 2 37.1 Jun-20 1,543.50 30.20 12.56 466.14 Wheat 3.30 Jul-20 1,764.00 36.30 17.26 640.33 Wheat 3 22.4 Apr-20 1,269.27 35.50 20.12 450.59 Wheat 12.07 May-20 1,023.44 30.20 13.80 309.08 Wheat 4 50.8 May-20 4,170.06 30.2 24.79 1,259.36 Wheat 3.82 Jul-20 48.00 36.30 0.34 17.42 Wheat 5 11.1 May-20 902.22 30.20 24.55 272.47 Wheat 3.76 7 19.2 Jul-20 1,347.50 36.30 25.48 489.14 Wheat 2.03 8 28.9 Aug-20 2,327.50 36.3 29.23 844.88 Wheat 2.33 9 28.6 Jul-20 2327.5 36.3 29.54 844.88 Wheat 2.36 6A 18.9 Aug-20 980.00 36.3 18.82 355.74 Wheat 2.31 Sep-20 1 490.00 1 37.00 9.59 181.30 Wheat 6B 1 19.3 1 Aug-20 1 1,568.00 1 36.30 29.49 1 569.18 Wheat 2.35 Total Acreage 430.00 von Drehle Wet Tons Dry Tons Permit I Limit 34,338.49 12,143.05 112,500 Branch Residuals Soils, LLC Confidential 2/22/2021 Page 1 2020 APPLICATION CONDITION SUMMARIES LAND APPLICATION LAB ANALYSES FOR VON DREHLE WERE REORDERED TO AID IN THE SORTING OF DATA. THE FOLLOWING DATA NAMES WERE SUBSTITUTED AS FOLLOWS: Lab name on Field Summaries Lab name on re' art.talculatiuns vd 2020-1 MB vd 2020-1 MB vd 2020-3 MB vd 2020-2 MB vd 2020-5 MB vd 2020-3 MB vd 2020-7 MB vd 2020-4 MB vd 2020- 9 MB vd 2020-5 MB vd 2020-11 MB I vd 2020-6-MB von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Mar - Apr 2020 von Drehle Paper Farmer: Bio-Nomics Services Acres: 22.4 Site/Tract: 4 Application Method: Incorporated Field: 3 Percent Solids: 35.5 Residual Report No.: vd 2020-3 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 4/27/20 3 312.18 Warm,Clear Dry 0.00 4/28/20 3 265.85 Warm,Clear Dry 0.00 4/29/20 3 266.42 Warm,Clear Dry 0.00 4/30/20 3 424.82 Warm, Cloud3 Dry 0.00 Total WOT-ous 1409 2Z von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 May - Jun 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 19.1 Site/Tract: 4 Application Method: Incorporated Field: 1 Percent Solids: 30.2 Residual Report No.: vd 2020-5 MB Crop: Wheat ............................ ........... ................... Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 6/9/20 1 98.00 Wan-n,Cloudy Moist Trace 6/10/20 1 98.00 Hot,Clear Moist 0.00 6/11/20 1 73.50 Hot,Cloudy Dry 0.04 6/12/20 1 49.00 Wann,Cloudy Dry 0.05 6/15/20 1 147.00 Wann,Cloudy Dry 0.34 6/16/20 1 147.00 Cool,Cloudy Moist 0.13 6/17/20 1 147.00 Cool,Cloudy Dry Trace 6/18/20 1 147.00 Warm,Clear Moist 0.00 6/19/20 1 171.50 Wann,Cloudy Dry Trace 6/22/20 1 171.50 Hot,Cloudy Dry Trace 6/23/20 1 73.50 Hot,Cloudy Moist 0.20 6/29/20 1 49.00 Hot,Cloudy Dry 0.23 6/30/20 1 98.00 Hot,Clear Moist 0.00 Total yVet Tons 1,470;00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 May - Jun 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 37.1 Site/Tract: 4 Application Method: Incorporated Field: 2 Percent Solids: 30.2 Residual Report No.: vd 2020-5 MB Crop: Wheat Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 6/9/20 2 98.00 Wann,Cloudy Moist Trace 6/10/20 2 73.50 Hot,Clear Moist 0.00 6/11/20 2 73.50 Hot,Cloudy Dry 0.04 6/12/20 2 49.00 Warm,Cloudy Dry 0.05 6/15/20 2 122.50 Warm,Cloud Dry 0.34 6/16/20 2 73.50 Cool,Cloudy Moist 0.13 6/17/20 2 73.50 Cool,Cloudy Dry Trace 6/18/20 2 73.50 Warm,Clear Moist 0.00 6/19/20 2 98.00 Warm,Cloudy Dry Trace 6/22/20 2 122.50 Hot,Cloudy Dry Trace 6/23/20 2 49.00 Hot,Cloudy Moist 0.20 6/24/20 2 171.50 Warrn,Cloudy Moist 0.05 6/26/20 2 196.00 Warm,Cloud Dry 0.40 6/29/20 2 98.00 Hot,Cloudy Dry 0.23 6/30/20 2 171.50 Hot,Clear Moist 0.00 Total Wet Tons �,543.50 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 May - Jun 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 22.4 Site/Tract: 4 Application Method: Incorporated Field: 3 Percent Solids: 30.2 Residual Report No.: vd 2020-5 MB Crop: Wheat ......................... ................... ............... . ................... ............... .. ....... ........................ . . ........ . Date Field No. fi Subeld Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 5/1/20 3 173.89 Warm,Cloudy Moist 0.31 5/4/20 3 292.71 Wann,Clear Dry 0.00 5/5/20 3 242.97 Warm,Cloudy Moist 0.48 5/6/20 3 241.57 Warm,Cloudy Moist 0.41 5/7/20 3 72.30 Wann,Cloudy Moist 0.03 Total Wet Tons von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 May - Jun 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 50.8 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 30.2 Residual Report No.: vd 2020-5 MB Crop: Wheat . .... .... ...... ...... ... ............... Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 5/12/20 4 24.50 Warm,Clear Dry 0.00 5/13/20 4 218.73 Wann,Clear Dry 0.00 5/15/20 4 173.11 Warm,Clear Dry 0.00 5/18/20 4 286.99 Warm,Clear Dry 0.00 5/19/20 4 238.47 Wann,Cloudy Moist 0.36 5/21/20 4 123.43 Cool,Cloudy Moist 0.35 5/25/20 4 292.66 Hot,Clear Dry 0.00 5/26/20 4 121.50 Warm,Clear Dry 0.00 5/27/20 4 267.30 Warm,Clear Dry 0.00 5/29/20 4 194.40 Warm,Cloudy Moist 0.07 6/1/20 4 291.15 Warm,Clear Dry 0.00 6/2/20 4 292.67 Warm,Clear Dry 0.00 6/3/20 4 244.81 Warm,Clear Dry 0.00 6/4/20 4 218.11 Hot,Clear Dry 0.00 6/5/20 4 218.76 Hot,Clear Dry 0.00 6/8/20 4 315.47 Hot,Cloudy Dry 0.12 6/9/20 4 72.00 Warm,Cloudy Moist Trace 6/23/20 4 192.00 Hot,Cloudy Moist 0.20 6/26/20 4 240.00 Warm,Cloudy Dry 0.40 6/29/20 4 144.00 Hot,Cloudy Dry 0.23 Wet Tons 44-79-96: von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 May - Jun 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 11.1 Site/Tract: 4 Application Method: Incorporated Field: 5 Percent Solids: 30.2 Residual Report No.: vd 2020-5 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 5/7/20 5 100.51 Warm,Cloudy Moist 0.03 5/8/20 5 197.01 Warm,Clear Dry 0.00 5/11/20 5 317.22 Warm,Clear Dry 0.00 5/12/20 5 220.28 Warm,Clear Dry 0.00 5/26/20 5 67.20 Warm,Clear Dry 0.00 Total Wet Tons 902.22 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 19.1 Site/Tract: 4 Application Method: Incorporated Field: 1 Percent Solids: 36.3 Residual Report No.: vd 2020-"- MB Crop: Wheat Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/13/20 1 73.50 Hot,Clear Dry 0.00 Total Wet Tons 73.50 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 37.1 Site/Tract: 4 Application Method: Incorporated Field: 2 Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat ------------------ Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/1/20 2 171.50 Hot,Cloudy Dry 0.00 7/2/20 2 245.00 Hot,Cloudy Moist 0.03 7/3/20 2 196.00 Hot,Clear Dry 0.00 7/6/20 2 294.00 Hot,Clear Dry 0.00 7/7/20 2 294.00 Hot,Clear Dry 0.00 7/10/20 2 563.50 Hot,Clear Dry 0.00 Total Wet Tons 1,764.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 50.8 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat . . - .... - Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/13 `20 4 48.00 Hot,Clear Dry 0.00 Total Wet Tons 48.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 18.9 Site/Tract: 4 Application Method: Incorporated Field: 6A Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/26/20 6A 367.50 Warm,Clear Dry 0.00 8/27/20 6A 147.00 Hot,Clear Dry 0.00 8/28/20 6A 196.00 Hot,Clear Dry 0.00 8/31 /20 6A 269.50 Hot,Clear Dry 0.00 Total Wet Tons 980.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 19.3 Site/Tract: 4 Application Method: Incorporated Field: 6B Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/13/20 6B 220.50 Hot,Clear Dry 0.00 8/22/20 6B 612.50 Warm,Cloud Dry 0.20 8/24/20 6B 343.00 Warm,Clear Dry 0.00 8/25/20 6B 318.50 Wann,Cloudy Dry 0.10 8/26/20 6B 73.50 Warm,Clear Dry 0.00 Total Wet Tons 1,568.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 19.2 Site/Tract: 4 Application Method: Incorporated Field: 7 Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/13/20 7 171.50 Hot,Clear Dry 0.00 7/14/20 7 294.00 Hot,Clear Dry 0.00 7/15/20 7 245.00 Hot,Cloudy Dry 0.05 7/16/20 7 220.50 Hot,Clear Dry 0.00 7/17/20 7 171.50 Hot,Clear Dry 0.00 7/20/20 7 245.00 Hot,Clear Dry 0.00 Total Wet Tons 1,347.5Q von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 28.9 Site/Tract: 4 Application Method: Incorporated Field: 8 Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat ..................... . Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/3/20 8 441.00 Hot,Clear Dry 0.00 8/5/20 8 269.50 Hot,Clear Moist 0.00 8/6/20 8 269.50 Hot,Clear Dry 0.00 8/7/20 8 269.50 Warm,Cloudy Dry 0.08 8/10/20 8 294.00 Hot,Cloudy Dry T 8/12/20 8 269.50 Hot,Clear Moist 0.00 8/14/20 8 147.00 Hot,Cloudy Dry 0.01 8/17/20 8 269.50 Warm,Clear Dry 0.00 8/22/20 8 98.00 Wann,Cloudy Dry 0.20 :::::Tofa1::VVet: T"ot�s 3217;50:: von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 July - August 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 28.6 Site/Tract: 4 Application Method: Incorporated Field: 9 Percent Solids: 36.3 Residual Report No.: vd 2020-7 MB Crop: Wheat ------------- Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/21/20 9 269.50 Hot,Cloudy Dry 0.12 7/22/20 9 294.00 Hot,Clear Dry 0.00 7/23/20 9 294.00 Hot,Clear Dry 0.00 7/24/20 9 196.00 Hot,Cloudy Dry 0.28 7/27/20 9 269.50 Hot,Clear Dry 0.00 7/28/20 9 269.50 Hot,Clear Dry 0.00 7/29/20 9 196.00 Hot,Clear Dry 0.00 7/30/20 9 269.50 Hot,Cloudy Dry 0.20 7/31/20 9 269.50 Hot,Cloudy Dry 0.01 Total Wet Tons ,327;50 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 18.9 Site/Tract: 4 Application Method: Incorporated Field: 6A Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat -------------- ------------------ ------------------------ Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/1/20 6A 196.00 Hot,Cloudy Dry 0.00 9/2/20 6A 294.00 Hot,Clear Moist 0.00 Total Wet Tons 490:00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 23 Site/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/7/20 1 269.50 Hot,Clear Dry 0.00 9/8/20 1 269.50 Warm,Clear Dry 0.00 9/9/20 1 147.00 Warm,Clear Dry 0.00 9/10/20 1 196.00 Warm,Cloudy Dry 0.02 9/11/20 1 171.50 Warm,Clear Dry 0.00 9/14/20 1 269.50 Warm,Clear Dry 0.00 9/15/20 1 367.50 Hot,Cloudy Dry 0.05 9/16/20 1 73.50 Warm,Clear Dry 0.00 Total Wet Tons 1,764.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 9.1 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/3/20 2 269.50 Hot,Clear Dry 0.00 9/4/20 2 269.50 Hot,Clear Dry 0.00 9/7/20 2 147.00 Hot,Clear Dry 0.00 Total Wet Tuns 686.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nornics Acres: 13.2 Site/Tract: 3 Application Method: Incorporated Field: 4 Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat .................................................................................................. Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 10/13/20 4 490.00 Warm,Cloudy Moist 0.10 10/14/20 4 343.00 Warm,Clear Dry 0.00 10/15/20 4 49.00 Warm,Clear Dry 0.00 10/22/20 4 147.00 Warm,Clear Dry 0.00 ::::'vital MO: -9:00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 11.1 Site/Tract: 3 Application Method: Incorporated Field: 5 Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 10/15/20 5 98.00 Warm,Clear Dry 0.00 10/17/20 5 196.00 Warm,Clear Moist 0.00 10/19/20 5 245.00 Warm,Clear Dry 0.00 10/20/20 5 98.00 Warm,Clear Dry 0.00 10/21/20 5 196.00 Warm,Clear Dry 0.00 10/23/20 5 24.50 Warm,Clear Dry 0.00 'dotal Wet Tons $57,50 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 18.9 Site/Tract: 3 Application Method: Incorporated Field: 3A Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat ............ .. ..................... ------------------- Date Field No. fi Subeld Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/16/20 3A 220.50 Wann,Clear Dry 0.00 9/19/20 3A 245.00 Wann,Clear Moist 0.00 9/21/20 3A 294.00 Wann,Clear Dry 0.00 9/22/20 3A 294.00 Wann,Clear Dry 0.00 9/23/20 3A 294.00 Warin,Clear Dry 0.00 T tal .0 Wet Tons 1,347-50 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 37.2 Site/Tract: 3 Application Method: Incorporated Field: 3B Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat .......... .................... ....... ........ .............. ..... ........ .............. Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/27/20 3B 196.00 Warm,Clear Moist 0.00 9/28/20 3B 343.00 Warm,Cloudy Dry 0.01 9/29/20 3B 343.00 Warm,Cloudy Dry 0.08 10/1/20 3B 465.50 Warm,Clear Moist 0.00 10/2/20 3B 147.00 Warm,Clear Dry 0.00 10/5/20 3B 245.00 Cool,Clear Dry 0.00 10/6/20 3B 245.00 Warm,Clear Dry 0.00 10/7/20 3B 343.00 Warm,Clear Dry 0.00 10/8/20 3B 343.00 Warm,Clear Dry 0.00 10/9/20 3B 196.00 Warm,Clear Dry 0.00 10/13/20 3B 49.00 Warm,Cloudy Moist 0.10 Total WO -Tons 2,9�S.SQ von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Sept - Oct 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 37.5 Site/Tract: 3 Application Method: Incorporated Field: 6B Percent Solids: 37 Residual Report No.: vd 2020-9 MB Crop: Wheat Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 10/21/20 6B 245.00 Warm,Clear Dry 0.00 10/22/20 6B 147.00 Warm,Clear Dry 0.00 10/23/20 6B 24.50 Warm,Clear Dry 0.00 10/26/20 6B 318.50 Warm,Cloud Dry T 10/27/20 6B 245.00 Warm,Clear Moist 0.00 10/28/20 6B 196.00 Warm,Clear Dry 0.00 10/29/20 6B 245.00 Warm,Clear Dry 0.00 10/30/20 6B 196.00 Warm,Clear Dry 0.00 Total Wet Tons 1,617.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Nov -Dec 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 18.9 Site/Tract: 3 Application Method: Incorporated Field: 3A Percent Solids: 42.3 Residual Report No.: vd 2020-11 MB Crop: Wheat Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 11/5/20 3A 122.50 Warm,Clear Dry 0.00 Total Wet Tons 12240 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Nov -Dee 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 24.6 Site/Tract: 3 Application Method: Incorporated Field: 6A Percent Solids: 42.3 Residual Report No.: vd 2020-11 MB Crop: Wheat .............. Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 11/9/20 6A 367.50 Warm,Clear Dry 0.00 11/10/20 6A 318.50 Warm,Cloud Dry T 11/15/20 6A 294.00 Warm,Clear Dry 0.00 11/16/20 6A 294.00 Warm,Cloudy Dry 0.02 11/17/20 6A 294.00 Cool,Clear Dry 0.00 :.:TQtatWet .Ons ..........:.. ,....:...:. 568.00 von Drehle Corporation Cordova, North Carolina Bio-Nomic Services WQ0005135 Nov -Dec 2020 von Drehle Paper Farmer: Bio-Nomics Acres: 37.5 Site/Tract: 3 Application Method: Incorporated Field: 6B Percent Solids: 42.3 Residual Report No.: vd 2020-11 MB Crop: Wheat ..................................................................................................................... .................................................................................................................... ..................................................................................................................... ..................................................................................................................... ..................................................................................................................... ..................................................................................................................... .................................................................................................................... ..................................................................................................................... ................................................................................................................... ..................................................................................................................... ................................................................................................................... ..................................................................................................................... Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 11/2/20 6B 269.50 Cool,Cloudy Moist 0.10 11/3/20 6B 294.00 Cool,Clear Dry 0.00 11/4/20 6B 245.00 Cool,Clear Dry 0.00 11/5/20 6B 98.00 Warm,Clear Dry 0.00 11/6/20 6B 220.50 Warm,Clear Dry 0.00 'i Qta.:::.:.:.:.:.::.:.:.:.::::::::::::1 � '7:04: