NC0006190_Regional Office Historical File Pre 2018

�. . -os a - v
CERTIFIED MAIL RECEIPT
(Domestic Mail Only;No Insurance Coverage Provided)
For delivery information visit our website at www.usps.com,
OFFICIAL. USE
0
Postage $
r
Certified Fee
Postmark
7 Return Receipt Fee
D (Endorsement Required) Here
Restricted Delivery Fee /� J
(Endorsement Required)
J To �s�C
3 DELTA APPAREL, INC -
sen
3 PO BOX 37
sire MAIDEN NC 28650
orFATTN: MR STEVE SLAUGHTER,PLANT MGR.
City swp/ma 5/27/l1

Certified Mail Provides:
• A mailing receipt
• A unique identifier for your mailpiece
• A record of delivery kept by the Postal Service for two years
Important Reminders:
■ Certified Mail may ONLY be combined with First-Class Mails or Priority Mail,
• Certified Mail is not available for any class of international mail.
• NO INSURANCE COVERAGE IS PROVIDED with Certified Mail. Fo
valuables,please consider Insured or Registered Mail.
• For an additional fee,a Return Receipt may be requested to provide proof o
delivery.To obtain Return Receipt service,please complete and attach a Returr
Receipt(PS Form 3811)to the article and add applicable postage to cover tht
fee.Endorse mailpiece"Return Receipt Requested".To receive a fee waiver foi
a duplicate return receipt,a USPS®postmark on your Certified Mail receipt i;
required.
• For an additional fee, delivery may be restricted to the addressee o
addressee's authorized agent.Advise the clerk or mark the mailpiece with thi
endorsement"Restricted Delivery".
■ If a postmark on the Certified Mail receipt is desired,please present the arti
cle at the post office for postmarking. If a postmark on the Certified Mai
receipt is not needed,detach and affix label with postage and mail.
IMPORTANT: Save this receipt and present it when making an inquiry.
PS Form 3800,August 2006(Reverse)PSN 7530-02-000-9047

-,ENDER: COMPLETE THIS SECTION COMPLETE THIS SECTION ON DELIVERY
• Complete items 1,2, and 3.Also complete A. Signature ,
item 4 if Restricted Delivery is desired. . , / , /—0 Agent
yy
• Print your name and address on the reverse "'� ;( � -"""t �� athtev-a. 0 AddressE
so that we can return the card to you. B. Received by(Prinfed Name) C. Date of Deliver
• Attach this card to the back of the mailpiece,
or on the front if space permits. 'TVA\-N 1\� 1-Ell/lQ' .5-31 . i I
1. Article Addressed to: D. Is delivery address differentrlif Yes
If YES,enter delivery add .
CN"-Tost[
,,,,
MAY3
,�11
1DELTA APPAREL,INCPO BOX 37 3. Service TypeUS?
MAIDEN NC 28650 0 Certified Mail 0 Express
ATTN:MR STEVE SLAUGHTER,PLANT MGR. 0 Registered 0 Return Receipt for Merchandis
swp/ma 5/27/11 0 Insured Mail 0 C.O.D.
4. Restricted Delivery?(Extra Fee) 0 Yes
7010 0290 0000 4565 0373
1 —_
DR Film,Rill Fahn lam 9(1R4 r)nmastin Rat um Rwrxint 10 oc_m_M_1 R.

UNITED STATES POSTAL.S8RV10E: -:.' :;i. • _.T� _ First-CIS IC1aiF: ..�
,:�<<_,--,ss:�. ,.,,, , ,..:..,.- , _ ,.., Postage&"Fees Paid
... LISPS „„,_
Permit No.G-10
• Sender: Please print your name, address, and ZIt+4 in this bex •
o '6
m o
to z
SURFACE WATER PROTECTION ��7 Z m
610 EAST CENTER AVE m 73 N Z m
SUITE 301 �� *� M"
MOORESVILLE NC 28115 C!o o A
7-2 c
r
0 ---4
-n -4
-n
C)
re
i,fiiiii,i=,t,ii,,,Iliiii,:ii,lii:i,i}isiifii,isi:iiiiiiiiiiii

Beverly Eaves Perdue
Governor
FILE fir,
[\icrn uaroma uepariment OT tnvircnimem arc �,,iaiurai t-,escurces
Division of Water Quality
Coleen H. Sullins
Director
May 27, 20 t 1
CERTIFILIP-MA,I'L, 7010 0290 0000 4565 0373
RETURN RECEIPT REQUESTED
Mr. Steve Slaughter, Plant -",Ianager
Z= --
Delta Apparel, Inc.
P. 0 B o x 3) 7
Maiden, North Carolina 28650
SUIBJE"C'I" Notice of Violation and Assessment of Civil
Penalty for Violations of KC. General Statute
14' 3-215, 1(a)(6) and NPDES Pertnit' No. NCO006 NO
Delta Apparel Maiden W"IX"TP
Catawba COUnty
Case No. LV-2011-0141
Dear Mr, Slaughter:
Dee Freernan
Secretary
This letter transmits a Notice of Violation and assessment of civil penalty in the amount of
$1,33506 (S1,250.00 civil penalty $85.06 enfoxcernent costs) against Delta Apparel,, Inc.
I -
This assessment is based upon, the following facts:. review has been conducted of the self -
monitoring data reported for Febraary 22011. This review has shown the subject facill'ity to be in
violation of the discharge limitations found in PDES Permit No,'NC0006190. The violations are
summarized in Attaclurient A to this letter,
Based upon the above facts, f conclude as as matter of law that Delta Apparel, Inc, violated the
terms, cc-riditions, or requirements of PDES Permit No. '-,'NCO006190 and North Carolina General
Statute (G.S,) 143-215. 1 (a)(6) in the manner and extent shown in Attaclunent A- A civil Penalty may
be assessed in accord ance v4-ith the maxtri-n-MIS established by G.S. 143-21 15,6A(a)(2).
Based upon the above findings offact and concluisions of law, and in accordance with authority
provided by the Secretary of the Departnient of Environment and Natural ReSOUNes and the Director
of the Division of Water Q�uality, 1, Robert B. Krehs, Surface Water Protection Regional St).pervisor
for the Mooresville Reel an, hereby inake the followi-ag, civil penalty assessinent agaimt 1)elta Apparel,
Inc.:
Mvve5ville Regicnal Office
Lccatcm 610 EastCen�er "V,,P, &Q001 Mocresville, "4,^ 28115
hcne (104)663-169F 04r 663-6040 Cusomer Seri, m 1-877-1323-5748
In le"net Nti):flpcT',a1 ncde7'r
A,n Fnta nn,-x)rt,,,.itv
One
NorthCarolina
I
Y � lafilhillil

RZ
25 s 0 For 1 of the one (1) violation of G.S. 143 _ 13,1(a)(61) and
N f1006190, lov discharging ° st into the
waters of the State in violation of tllc permit daily maximum
effluent limit for total phenols.
f'or 1 cif the one (1) violation of G.S. 143_215.1(a)(6) and
l'DS l'errnit No. NC0006190, by discharging waste into the
waters of the State in violation of the pernait monthly average
effluent limit for total phenols.
TOTAL CIVIL PENALTY
85-06 Enforcement casts,
1.335.06 TOTAL A.MOUNT MITE
Pursuant to G.S. 143M2115.6A(c), in determining the amount of the penalty l have taken into account the
Findings of Fact and Conclusions of Law and the f.ac=tors set forth at G.S. 143 ry 82.l(b), which are:
(1) The degree and extent of harm to the naatur al resources of the State; to the public health, or to
private property resulting from the violations
(2) The duration andgravity of tine violations;
(3) The effect on ground or surface water quantity or quality or on sir quality-
(4) The cost of rectifying the damage;
(5) The araaount ofmoney saved by noncompliance-,
(ti) Whether the violations were corrararatied w llfaally or it to ntionallv i
(7) The prior record of the violator in complying orfailing to comply with progranis over �&hich
the Environmental Nlanagernent Commission has regulatory authority; and
(8) 'The east to the State of the enforcement procedures,
Within thirty days of receipt of this notice, you must do one of the following:
. Submit payment of thepenalty:
Payment should be made directly to the order of the. Department of EuviTonn2eClt and Natura-al
Resources (ch) not include lvaive faarrr�,l, Payment of the penalty will not foreclose further
enforcement action for gray continuing or ne�,v vic lation(s)
Please, submit payment to the attention of:
Point Sotarce C:om li-act;,/Enfrcerneart Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27 9-161
CIS

2. Submit is written request for remission, including at detailed justifitcation for inch request:
Plezo;e be aware rhat a request tbr remiss-410",-, is fininted, to consideration ot' 'lie Ifive ta.crors lilsted
below as the%,, rnav relate to the reasonableness o"' tl,�ie arriount of the penl-,Ilty azsses,-,,�d. Requesting
remission is not the proper procedure I'or coinasting whether the violation(s) occilirred or the accuracy
of any of the factual statements contained in the civil penalty assessment docunwnt. BecaLISC, i
remission request forecloses the option of an administrative licaring., such to request must be
accompanied by a waiver of' -your right to an adMiniStratiVe he and as StIpUlailion that no factual or
lea -al issues ar-, in dispute. Please pnOpare a detaded statement that establishes why yaia, believe the.
civil penalty shou.ld be remitted, and submit it to the Division of %Vater Qushty x, the addnes listed
belo-w. In detenninina whether a, remission rcqiu,a : will be approved, the factors shall be
considered.
(1) whether one ornnore (,-)f the civil penalty assessmeritfactors in GS� 1,4313-282,1(b) were
wrongIbIly applied to ttie detriment of the petitioner;
svhether tL violator promptly abated coiainuing environmental, damag I ge resultn- from
the violation-,
f,i whether the violation was inad-vement ol- a r-',stilt of an accident:
(4) r,vhether the violator had been ass�f-sse,! civil peiuiltiles for any ptevilous N-1olatioris- or
(5) whether payment Cat the civil Penalty will prevent, payment for tho retnamin g necess'atry
rerriedi,,.-il actions.
Please note that all infbrination presented tri support of your request for remission must be
submitted in The Director of the Division ofWater Qualitv �N III review our evidence and
inform you of his decision in the rnatter of your rl-mission request. The response will provide, details
regarding case, status, directions for payment. and provislon for fiarther appeal of the penalty to the
En,ronmental Management Conmnissiott s Conirnittee on Civil Pemilty Rennissions (Comrnittee)
Please be advised that the Committee cannot considcr information that Nvas n()t pa,,-t of the oripurial
ren-iission reque, t c(;insidlered by th, Director. Therelbre, it is very important that YOU prepare a
complete and thorough statement in support of your request for remissloo,
In order to r.equest remission, you must complete and sultnrit the enclosed "Waiver of Right to
an Administrative lil-arinL, and Stipulation of Facts," fc.)rm within, t1narty (30) day-s of'receipt of this
notice, The Division of it QUality also requests that you complete and stibrnit the enclosed
"Justification for Remission Request." Both f0MIS ShOUld be subrnitte�,J to the f'(,)11oNviT1g address:
Point Source C(�mi.')Iiince,,'Etifk.)rcCT11CIlt Unit
Division of Water (1).uality
1617 Nfail, Service Cent.-r
Raleieli, North Carolina 27699-1pia -7
OR
1 File as petition for an administrative hearing with the Office ol'Adininistrative Hearings:
If you wish to contest anv statenient in the attached asses,,,ment d0cllfllertl VC114 rnut file a
Petition for an achtfinistratiie hearin,,11T. Y-ou may obtain thc petition fOrnn fi,onl the Office of

Administrative Hearin&ls. You rnust the the peritionwith the Oft-icc of Administrative Hear'nes
- t .1)) days of receipt o I e no S considered tiled when it is received in 14
,,vi hi n thiny (", (,,I ;fit this notic � A peti * ri i
the ()f-5ce of Administrative 1--fearing s during nonnal office hours, The Office, of Admirdstrat]"Ve
Herrragsaccepts filings NIonday t1trough Friday betr--veen, the hours of 3:00 a.m- aInd 5-.00 p,m,.
except I for cifficial state holidays. The petition may be filed by facsimile (fax) or electronic mail by an
attached lite (vJth restrictions) -provide the signed original, one (1) copy and. a fifing Ice (if a filing
fee is required by N(,,GS § 15OB-23-2) is received in the Office cat Administrative Hearings within
seven (7) business days folloviingy the faxed or electronic transnussiom You should contact the
Office of Administrative Hearings with atl questions regarding, the filingg fee and/or the details of the
filing process, The mailing addresiand telephone and fax numbers for the Office of Adri-iinistrative
Hearings, are. tias follows:
office of Administrative Hearinas
6714 Mail Service Center
Raleigh, NC 27699-6714
Tel: (919) 4-7, 1 -3 )000
Fax: [phone] -], 10 0
One (I') co� tit." the petitioll mast aiso be served on DE'.,.\-R as follo�,-N-S-
py
Mary Penny Thonipson, (3cneral Counsct
DE, IN R
1601 Mail Seri ,icy Center
Raleigh, NC 2'699-1,601
Please indicate the case number (as found on page c,,rie ofthis iet',er) or, thle Petiti011.
dfs o, Z
Failure to e\crcise one of the options above %�snhjjj ti irty f`3 ays of receipt othinnceIS
lark), will tesult in this matter beii4l'l
evidenced by irn internal date,`time received stamp (not a post'n.
referred to the Attorney Gerieral's 0117 , gli a civil action.
-ice for collecti1on of the penalty- tllrc)u
Please be advised that iaclditional penalties may be assessed for violations that occur after the
the vj�jLaiLigq�,� ar -gj�q rq,,.jiL),j related �too
review period of this assessment, ff
col !�CiietlorL- ct�yltles, 'len MV, wish
o 1- --tI -- L— -
and' S —.11 —it!—
have any -i naltv
ej- al? r
to consid pjving fi-) a Spec]
contact t�j�, ff of
�)ect n staf, the
assessm P a-
i n Iffice_al J70�'-),h L)3--j&49!4,,
q0p o a].
ell
V
)ate) Robei B, Mebs, Regional Supervisor
Surface Watcr Protection
Mooresville Regional 0f[ICL-
Division of Water (,)uality

rT to `F 1F
cc:: Mooresville Regional Odic Compliance File. -vv./ attachment
Raleigh Compliance/Enforcement File Nvi attachments
Central Files w/ attacltl ents
rk/m

ATTACHNIENTA
C . ,V- 1-0141
Outfiall Date Parameter Re, )orted "ale Permit Limit
01 2112/1: 1 Total phenols 0,74 trig/L 8,0 lbq/ ay (Daily maximu'll)
001 /28/ 1. Total phenols 103 lbs/clay 4,0 lbs"'c-lay (nio ally average)
`flee ermittee report a monthly avera e concentration of T lbsday°. 1�(���e�er. the
February "'LZO11, ample analyzed for total phenolswas not properly , erverl for this
analysis as per Standard kethods and the validity of the. reported pherjol concentration is
questionable, Therefore, this result should not be used to calculate the montitl.y av crage.
The monthly average concentration using the `er ainin( three analyses is 10.3 lbs,play.

T Ta°, OF O'1 H CAROLINA fn EPA T"Y'II-''�,,T f3F EVTRC)`,""OENT
COUNTY OF CATAWBA AND °.TT °=5 t� *OU,
fly l`l lI f M.a'\ER OF h SSl SS;t,3ll L 3 WAIVER OFIZIGHTTO AN
OF CIVIL PENALTY AGAINST ADM iNISTR-ATIVE I JEARING AND
PERMIT NO. NCO006190
FILE NO. L V-2011-0' 41
llavi,mz been assessed civil penalties totaling $1335.06 for vif-latiarat(s) as Y ;yet firth in the
assessment document of the Division of Water Quality dated Nkla ' 27, 2011, the undersimed, es it a
to seek rennassion jai th ci-vil penalties, does hereby waive the ri.gLit to an udmaraa,�trata - hearing In the
above -stated matter and does stipulate that the facts are a4 .all et in the assessment document, the
undersiat- ed Ruther a nderstandis Haar, all evidence presented in support of remis-sion of this civil
penalty a :tst be submitted to the Director of the Division of Water Quality �vitl in 3`0 days of receipt o
remission s i t'n i �.� asthenoticenoticenoticeof�ass��saaa�:.�a�. No tag°�� in=lI l�aatyt �..t'at•e�aa�ost ���ll. 1lc.�����rl after 30
d a.I..s from the receipt of the notice of assessment.
This the alai' l l

JLSTIFICATION FOR RE)4TSS1LLRE0BEST
DWQ Case Number- LV-2011-014 11
Assessed 'tarty: Deltas Apparel, Inc.
County: Catawba
Amount Assessed: S1,33506
Please use this form when requesting remission of this civil penalty- You rriust also complete the
de 7i `',� °.)'yit) i. `t at: t t" t: l t �( 2 1c�4ir'nn;str ativ � "�'-�`aP?Pr4, eta "t'1 t) 2 r ti F«
tai: _ _ _._._ _
i t request remission in this civil penalty, ' ou should attach any documents n°s the,, v+otr believe
support your request and are necessary for the Director r to consider in evahrar tt( vour request for
remission. Please be aware that to rr:tluest for rernission is limited to consideration of the five factors
listed below as ihev mwi relate to the reasonablenless of the amount of the civil penalty assessed.
Requesting remission is not the proper procedure for coraesting, wh flier the violation(s) occurred or
the accuracy of ariv of the factual statements ont-finned in ffie civil penaliv assessment document.
pursuant to N,� C:.G, . § l 4313- 82.1(c), rernission of a civil en lty may be granted only when one or
more of the following five factors a l�plies. Please the each factor that you believe applies to your
cast; and provide a detailed explanation, including carries of :rtrpportir���;ycic,ciinnerit . as to vvhy the
factor applies (attach additional pages as treaded),
a l- 1"fit
(a) c�att or more wit the cavil .t.tltal��" assessment factors in �. �r
vv"t'orlsfull'G tt 7 l?ed tG the etriir e t o tl''� Ott Et i3er (the ��xr. essin rz f zetor�° are lire in r�+�ii'. C'ivi.,
(b) the _ � it l�tc�r.. pert 11� �h tt �� �t�_rlt��agjn env irc�ritr:;r �� I �� �rar i�� rt staff tari< txa?rr� the
p Y k v. { �' z pT G J J "�
�ia?latier�-t ��, �:".. �:�:�'�#ed:rrttre stt�t�s tir�Xt 4'ot.l lt�t:r,�t: i`i� 't?i'"t`a'�r ?`trt t,,rC71Urt,�7iz i�,ae,�i�"��=efw1` r2it<ir'e or:rli"icntst'.);
_ (C) the vdoltationyvas inadvertent or 'a result o w n, accident (i.e,, ej jj�,z.n whzy the violation
ivas urrcrt=:tsrdable or nsomel hirr'x jrrrr could not prevent or prej)ar e
t13 e, rtor had not t been assessedm iv i. .iti y1:ka * nts tea violations;
(d) i tsrrt art the ivyil S t rr�t �"ill r vent �_Iy�ngrlt t'L�r 1 at rnttt# R r r etiiedial
actions (,e p explain, how piiynfii'w Cifthe civirp:nalt'i.? will it re.ieni you,from peffrrnziw2g the activities
arc c s sat'v to acr'7:e 1'e cL ?nj,1:'ia ce)'°
XPLANsF T ` : (use additional prges tar nec e sa. fir.

Violator: belt 4-,AppqrqL Inc,
Facility: Delta A VareL. _In c,_)4aicleta Ptant WWTP
Countv-.. Catavvba
Case Number: LV-2011-0141
Permit Number: NC0006190
1) The degree and extent of harm to the natural resources of the State, to the public health, or to
private property resulting from the violation;
No harm to the environment has been documented.
2) The duration and gravity of the violation;
The total phenois concentration of 30.7 lbs/day on February 2, 2011, exceeded the daily maximum
permit limit of 8,0 Ilss/day by 284.3%, This elevated concentration resulted in a monthly average
phenol concentration of 7,69 lbs/day as reported by the permittee. However, the phenol sample
collected on February 23, 2011, was accidentally destroyed by the analytical laboratory before
analysis. A phenol analysis was performed on an unpreserved portion of another sample collected
during the monitoring event. Because the sample was not properly preserved for total phenol
analysis as per Standard Methods the validity of the phenol concentration reported for this sample is
questionable and it should not be used to calculate the monthly average The monthly average
concentration using the other three samples is 10.3 lbs/day is exceeds the monthly average permit
limit of .0 lbs/day by 156,2W
3) The effect on ground or surface water quantity or quality, or on air quality;
The effect on the receiving stream is unknown. Phenol, when combined with chlorine, forms
chlorinated phenolic compounds with the potential to taint fish tissue and drinking water, thus
degrading taste and odor (organoleptic concerns),
4) The cost of rectifying the damage;
No damage has been documented.
5) The amount of money saved by noncompliance;
The amount of money saved by noncompliance Is uhknowrh�
6) Whether the violation was committed willfully or intentionally;
The Division of Water Quality has no evidence that the violations were committed willfully or
intentionally. The permittee
7) 'The prior record of the violator in complying or failing to comply with pre ants over which the
Environmental Management Commission has regulatory authority; and
There have been three previous CPAs for the Delta Apparel Maiden VVWTP during the life of the
permit with one CPA issued in the past twelve months.

Case Number t rt tion
V , 010-01 1 S1,335.87 L " for COD, ss aid in full, _..m.
J'he cast to the State of the enforcement procedures.
The cost to the Division of Water Quality lit i
SIL tf-c
Gate Robert B, Krebs, bs, Regional Supervisor
Surface Water Protection
Mooresville regional Office'
Division of Water Qualitv

MONITORING REPORT(MR) VIOLATIONS for: Report Date: 05111111 Pagei I of 9
ACTlON
PERMIT: NCO006190
FACILITY: Delta Apparel Inc - Delta Apparel I Maiden
COUNTY: Catawba
REGION: Mooresville
Limk Violation
MONtromNG OUTFALLI
REPORT ppt
\cOLATION UNIT OF
LOCAIL ION PARAMETER DATE FREQULNCY MEASURE LIMIT
CALCULATED
VALUE '16 OVER LHOi r
V!OLAT`10N TYPE VIOLATION ACTION
02-2011 001
EfflueM Phenoircs,"rotM Recoversib9e 02/02111 Weekly IbsIday 8
3074 284.25
Daily Maximum Exceeded None
02-2011 001
Effluent Phenot�cs, Total Recovera[de 02128111 Weekly IbS/day 4
7,68 9212
Monthly Average Excftded None
PERMIT: 1 O044253
FACILITY: North Carolina Lions Foundation In -Camp Dogwood
COUNTY: Catawba
REGION: avillb
WWTP
Limit Volatlon
MCNITOMNG OUTFALL/
REPORT PPI
VK)LVk110N UNT!'01'
LOCATION PARAMEIER DATE FREQUENCY MEASURE LINUT
rALGULATED
VeLtJF % OVER LIMIT
VIOLATION TYPE MC)i.ArION ACTEQnl
02-2011 001
Effluent solids, Total Suspended - 02128111 Weekly Mq/l 30
36,5 21,67
Monthly Average Exceeded one
Concentration

PLEASE PRINTCLEARLY OR TYPE
STATE OF NORTH CAROLINA
COUNTY OF CATAWBA
r- "! 1­­.FF-­,
IN ITIE" , OFFICE OF
ADMINISTRATNrF HEARINGS
Case No. LV-2011-0141
DELTA APPAREL, WC, ^Pit r
PETITIONER,
PETITION
V, FOR A
CONTESTED CASE ITEARING,
NORTH CAROLINA DEPARTMENTOF ENVIRONMENT ANN
NATURAL RESOURCES, Division of Water Quality, UUMJ'
RESPONDENT,
I hereby ask, for a contested cast hearing as provided for by North Carolina General Statute § I 5OB-23 because floc'k6s
Rcspondont assessed Petitioner a civil penalty for phenol cxcecdances disclosed in Petitioner's discharge monitoring report CTWTV'), At the
time of the DMR submittal, Petitioner informed Respondent that the plomol exceedances appeared to be related to laboratory error due, to a long
history of complianoevvith phenol limits and no known source relating to plant operations:
(4) Amount in controversy 5­1 —3550�_ (if applicable)
(If more space is needed, aulach additional pages,)
(5)13ecause of these facts, the State agency or board has° (check at least one from each column)
-_deprived me of properrry; —x, exceeded itsautheirty orjiurisdicticn;
—x _ordered me to pay a fine or civil penalty', or --x—,acted erroneously;
—x­—chherivise substantially prejudiced my rights; AND --- —failed to we proper procedure,
.--.x— acted arbitrarily Or C2111160USly, or
x — failed to act as requw o red b� Jar rule.
(7) Your phone number� ( 336 )721
(6) Date. -3535
(8) Print your frill address, OaoWest Fourth Street, Winston-Salem, NC 27101
(9) Print YOUr name: Lori P onarnt Esq,
(10) Your signature:
You must mail or deliver a COPY of this Petition to the State agency or board named on line (3) of this fiurm Yen should contact the agency or
board to determine the narne of the person W be served.
CERTIFICATE OF SERVICE
I certify that this Petition has been served on the State agency or bo&d named below by depositing a copy of it with the Unoed States Postal Service
with sufficient postage affixed OR by delivering it to the named agency or board:
Mary Penny Thompson, (dencral Counsio
North Carolina Dopartment of Enviicament and Natural Kesourccs
160! Mail Service Center
Raleigh, NC 27699-1601
(14) This the of Jurre, 2011,
(15)
Lori P—Hinnard
When you have completed this form, you MUST mail or deliver the ORIGINAL AND ONE COPY to the Office of Administrative Hearings, 67 �l
Mail Set -vice Center, Raleigh, NC 27699-6714:
11-06 (05110)
nn

MBL ka
One ffiest Fourth Strut
CARLYLEpr Winston-Salem, KC 2, 101
Lori P. Ifinnant
s �&x ( i) 721-.366
Direct Fax- [phone]
wwwwc-mconj
E-mail: 1iain3xt@.W�sr.cr�ara
Via Facsimile and U.S. Hail'(919-431-3100)
Office of Administrative Hearings
14 Mail Sen4ce Center
Raleigh, NC 2 - 714
e. Delta Apparel, Inc. v. North Carolina Department of Environment and Natural
Resources, Div iaan of Water Quality, Case No. , - 11-0141
Enclosed please find an original and two copies of the Petition for a Contested Case
Hearing in the captioned ease along with our check for $125 for the filing fee. Please file stamp
and return one of the copies to me in the enclosed postage -paid envelope,
1f y o have any questions, please call me,
grata � , eery truly,
h
v
Lon P. Hinnant
l?11.ajaa
cc" Mary fenny "1`hoinpst n, General Counsel
GE;( RGIA, i SOUTH CAROLINA / NONTH C:.A.v7.t7LINA d ViAGtNtA A':WASHINGTON D;G r' MARYLAND ,f DELAWhRE
WCSR 464594 V

TA`rE OF RTH CA LIMA IN TIIII OFFICE OF
ADMINISTRATIVE TI ATIVE HEARINGS
COUNTY OF CATAWBA I I EHR 08329
D LTA PPAREL, IN('
Petitioner
V, W14'HDRAWAL OF PET111ON
NORTH CAROLINA DEPARTMENT OF AECEIVED
ENVIRONMENT AND NATURAL DIVISION OF WATER QUALITY
RESOURCES, , DIVISION OF WATER QUALITY,
T (
Respondent. SWP SECTION
MOORESVILLE REGIONAL OFFICE
DE TA APPAREL, INC. ("Petitioner") and the Division of Water Quality of the North
Carolina Department of Environment and Natural Resources urces Rs ndent") in accordance with
the terms set out below, hereby enter into this Settlement Agreement (k"A reerrzent") in order 't
resolve certain un atters in controversy between thetas laaat-sraarat to N.C. Gen, Stat. §1013-31(b)a
WHEREAS, Respondent Blain s that petitioner violated N. Cw Gent. Stoat, t 1 -
21 ,1(a)( and certain tern -is of NI NES Permit No. NCO006190, and is liable for a Civil l Penalty
in the arzrount ofone thousand, two hundred Fifty dollars (l tl,tttl) and Enflar,enien Costs i.
eighty -five dollars and six. cents ( .06) totaling one thousand thice hundred thirty-five dollar
and six cents ($1,33 .tlfa), all as more specifically described in Matter No. LV 30l 1-01 1 dated
May 37, 2011, (hereinafter referred to as the "Total Claimed Amount"); and

N4q
WIERE S, Petitioner- filed the above -captioned petition challenging tile assessment f`
any penalty on the basis that there was laboratory orror in the phenol analysis of Petitioners
sample',
WHEREAS, Petitioner denies liability for tine `natal Claimed mQuirt; an
WHEREAS, Petitioner and Respondent through counsel have, atilt eed that a Settlement is
mutually beneficial-,
NOW THEREFORE, without any hearing, findings f of or conclusions of law its the
above -styled matter, and without admitting any liability, PETITIONER AND RESPONDENT
AGREE THA7„
1. In earner to avoid the cost and delay ref ftfrther litigation and without admitting any
liability, the Petitioner and Respondent have entered into this Agreement merit and have agreed that all
parties have been con-ectly designated and that there is no question as to raaisjoinder or
no njonider,
Without Audication of Respondent's claims and Petitioner's denial of
Respondent's claims, and without admitting to the underlying facts giving rise to issuance of the
cited penalty and any liability for the Total Claimed Amount, Petitioner agrees to pay to
Respondent and the Respondent agrees to accept as full satisfaction of` the Total Claimed
Amount, the SUM Of sip hundred twenty-five dollars and no/100 coats (Sd .tttt) PIUS S85.06 in
enforcement casts, totaling severe hundred tent dollars and six cents f$ 1tl.t1 >1 ("Settlement
Amount"),
3. The Petitioner will pay this Scttlenient Amount in one 1 payment within sixty
d j days of the date of Petitioner's authorized representative's signature on this Agreement.

The laaryaaterrt shall be made by check and made payable to the North Carolina Department of
Environment and Natural Rcsourc.cs and mailed to the following aaddress;
Amanda Foster
N:C~. Departnaerat Of JUStice
En irota.nicratal Division
P.Cy.Box c
Raleigh, NC 2760
The breach of any condition of Paragraphs phs and 3 by Petitioner will render..
Petitioner liable to Respondent t for the Total Claimed Amount.
Petitioner expressly agrees that by entering into this Agreement, Petitioner waives,
for purposes of collection of any stases due hereunder, any and all defenses to the Matters
Addressed, and that the issue in any action to collect said sums ,vill be limited to issues of
compliance ,vith this Agreement, Theparties agree* that this Agreement may not be used by any
third }'warty as the basis for ar claim of res jaadicata, collateral .estoppel or waiver with respect to
Petitioner's defenses and rights to maintain and prove that Petitioner is not liabliea, or responsible
for any of the Matters Addressed orr`the Total C:latirned Amount,
ty. Nothing in this Agreement shall restrict any right of Respondent to taiac any
enforcement action against Petitioner for any alleged violations first occurring on any date other
than those set forth in ; ltachmerrt A of the May 27, 2011 Notice of Violation and Assesst-neat of
Civil Penalty ("ContestedAction") which is data agency action prompting the initiation of this
contested case, however., Respondent cannot use in any ways any fact ofthis Contested Action in
any subsequent action or in the calculation of any future penalty:
7, Respondent and the Petitioner agree that, for purposes of any future bankruptcy
proceeding, this Agreement is not intended as, nor shall it be deemed to constitute, a novation o
any claaira-as asserted by Respondent against Petitioner. Petitioner- further agrees that all sums

payable to Respondent laaars raatat to this Agreement are nraraalisch;ar caablc in bankruptcy under l 1
U&C, § ? z Nothing in this Agreement releases any rraaaaalaschaarawtcaable claims that array, be
asserted by Respondent in any bankruptcy proceeding, and nothing in this Agreement shall be
deeraacai to waiver of the Respondent's right to rely on the nature of any claim or debt released in
this Agreement to show that tile claiitya or debt is raaaaa ii char eabl .
Fire parties agree (bat tic consideration tsar this settlement is the promises
contained herein and that this Agr crrient contains the whole agreement between thetas.
9, i"his Agreement, shall be binding capon the parties, their successors and assigns,
atPcrta cXcccation by the undersigned, who represent and warrant that they: are :authorized to attar
into this agreement on behalf ofthe parties hereto,
ltl. 'This Agreement ent may be executed in any taaamber Of caatraaterlaaarts, each ;r-rt`which
shall be citaa:.raaed an original, and all of which, together, shall constitute one and the same
instrument,
WITHDRAWAL OF PETITION
Entry of this Agreement serves as PctiticraaCr's Vcalaatataary Withdrawal with Prejudice : of
the Petition =car Contested Case Heating in this matter. The parties agree this matter is concluded
and that no further proceedings are needed or regUired to reso1ve the contested case.
NORTH CAROLINA DEPARTMENT
OF ENVIRONMENT AND NATURAL
RESOU RQES;,,D1V1S ION OF WATER
ALIT
Division of Water Quality
F
r
~a
Date:
DELTA APPAREL INC.
ate:

APPROVED S TO FORM B
ROY COOP
WOMBLE CR:LYLE SANDRIDGE
RICE
Dotlaff W. L ton
Load P. Hinnant_
Assistant Attorney General
Attorney at Law
.C, Departnicrit ofJustice
One WestFourth Street
Environmental DM S1011
Winston Salem, NC 27 10
P, 0, Box 629
Raleigh, NC 27602
ATTORNEYS FOR, R-ESPONDENT
lW"gate.
t �/, ��
Date-

From: Francies, Gary
Sent: Monday, July 11, 2011 1Z54 PM
To: Allocco, Marcia
Cc: Krebs, Rob" Sledge, Bob,- Wiggins, Kent
Subject: Data Review Delta Apparel Phenol
Marcia
As you requested, on July 8, 2011, 1 conducted a paper trail data review for the 2/2/ 11 effluent grab phenol sample
from Delta Apparel analyzed by Pace Analytical - Asheville (lab ID-. 9286943002). The sample was analyzed per EPA
Method 420.4, semi automated colorimetric procedure, on a Konelab analyzer on 2/8/2011. The review included
looking at sample check in procedures in addition to the specific data set that included the sample in question.
Observations made include:
Nothing was documented that indicated a mix up or problem with the sample at sample check in at the laboratory —
reviewed Chain of Custody and Sample Condition Upon Receipt forms.
Phenol samples are collected in a unique sample bottle, an amber 250 ml bottle, that is not used for any other samples.
This greatly reduces the chances that bottles were inadvertently mixed up.
While the value obtained was unusually high, for both this particular facility and phenol samples in general, there was
nothing within the sample run that indicated a problem with the value obtained. The fact that the sample was a grab
sample indicates that a slug of something containing the unusually high concentration of phenols may have been
collected.
•
There were two matrix spike and duplicate analyses quality control failures with this run (both have ± 10 % acceptance
criteria) . None involved the sample in question. Matrix spike and duplicate quality control analyses are dependent upon
the particular matrix of the sample used for the spike and duplicate and therefore are not something that invalidates or
leads to questions about another sample in a particular analytical run. In this instance the spikes and duplicates had low
recovery, not adding any support to a false high value for any samples. The quality control measures that are more
reflective of the entire analytical run, the blank and the Continuing Calibration Verification standard (CCV), met
acceptance criteria, In fact they were very good, The value of the blank and CCV four samples prior to the sample in
question were -0.002 and 0.250 mg/1 (true value 0.250 mg/l, 100% recovery) respectively. The value of the blank and
CC V immediately after the sample in question were -0.003 and 0.247 mg/L (99% recovery).
In conclusion, there was nothing found in the data review to invalidate the value obtained for the sample In question,
Gary

qqq
Have you signed up to receive automatic email notices of changes to polices, regulations and
resources pertaining to astewater/ rOLind titer Laboratory Certification that could have an
impact can your day to day operations If not, send a blank email to the following address t
poet on the list
QENR,gKQ.La0�Cet n__-�or lists. .. �ncTai.l. net
`mail correspondence to and fr rrr this address is subject to the ?forth Carolina Public Records Law and may be
disclosed to gird parties unless the content is exempt by statute or other regulation.
Cary Francies - Gar .Franc es ntdenr, o
North Carolina Dept. of En ironrnent and Natural Resources-
shehille Regional Office
Division of Water Quality - Laboratory Certification
209 U1 . 70 Highway
6 annanoa, LAC 28778
Tel:-26-4677
Fax; 28-2 -704

From:
Laton, Don [[e-mail]]
Sent:
Monday, July 11, 2011 1122 AM
To:
Aliocco, Marcia,- Hinnant, Loh
Cc:
Krebs, Rob-, Sledge, Bob, Francies, Gary
Subject:
RE: Delta Apparel
Everyone -
I can be reached by telephone at 919-716-6963
dolaton@ncdoi,.gov is my e-mail.
Lori:
I have very limited time to discuss this matter until Fri, of this week, I'm aware of the mediator selection deadline on the 14th.
So, let's take a little time today or tomorrow to discuss the case..
I'm generally familiar with the facts of the matter through conversations with staff in the Central Office
My apologies for any inconvenience I may have caused by not contacting you earlier. A Notice of Appearance was mailed last•
week.
Don
-----Original Message -----
From: Allocco, Marcia [mailto-marcia.allocco@ncdenr,gov]
Sent: Monday, July 11, 201110:59 AM
To: Hinnant, Lori
Cc: Krebs, Rob; Sledge, BobLaton, Don; Francies, Gary
Subject: RE Delta Apparel
Hi Lori,
I received an email that stated Don Laton at the Attorney General's Office is the assigned attorney for the case.
Unfortunately, I do not have his phone number although I have copied him on this email. Gary Francies with our Lab
Certification Group is doing a more thorough data review at Pace Analytical and he will share his findings with Mr. Laton,
Regards,
Marcia
----- Original Message -----
From., Hirmant, Lori ([e-mail]
Sent., Monday, July 11, 20119:02 AM
To: Allocco, Marcia
Subject: Delta Apparel
Have you heard from the attorney that has been assigned the Contested Case matter? I have not,
Lori P, Ffinnant
Womble Carlyle Sandridge & Rice, PLLC
One West Fourth Street
Winston Salem, NC 27101
Phone [phone]
Fax [phone]

IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements Imposed by the IRS, we inform you that any U.S. tax
R
advice contained in this communication (or in any attachment) is not intended or written to bcannot used, and ca not:USR
be used, for
the purpose of (I) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to
another party any transaction or matter addressed In this communication for in any attachment).
CONFIDENTIALITY NOTICE- This electronic mail transmission has been sent by a lawyer, It may contain information that is
confidential, privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you
are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it, or any
attachments. if you have received this message in error, please delete this message and any attachments from your system
without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the part
of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication, Thank you
for your cooperation.
2

g
y1II
mNot"
qC��Client
_
,, .
II II
000"
iftmmon
MaMCL&=
�COLLECTEa_..
SAWLE
SL
OLM
OT
Pace pr
� E
IIIIIII I��I � I
II���� llu IIII
III III II III Illlllll�l
I
�
SAMPLOR4e
k

Fvt Ul=&M-1110111 0 X
FaceAnalytical Client Name�fbL Project #_OP 9 614,3
Where Received- Huntersville M Asheville Eden
r-7-
Courier: EJ Fed Ex 0, UPS_USPS El Ckem nt [I Cornerciai Pace Other
J
OP
pl`�
"'
Custody Seal on Cooler/Box Present., Dyes no Seals intact: yes no A
'v
Packing Material: D Bubble Wrap [�Bubble Bags 0 None 00ther
Thermometer Used: Ili Gun - T904 Type of Ice: & Blue None Samples on ice, coolwrrg process has begun
Temp Correction Factor: Add t Subtract -4
Date and in' I Peiso�exa ining
,orrected Cooler Temp.: C Biological Tissue is Frozen: Ye' o/
contents,
emp ShOUld be above Freezing to 6'C; Comments: 79M
'hair; of Custody Present'. �Yps 0No 13WA ,
.hain of Custody Fdled Out.- _!rF_ "
`I.iNo El NiA 2,
'hat' of Custody Rehnqritshed; yes E]No OKA 3,
,ampler NarnL& &Wature on COCL Yes D No EDNA 4,
0 'a
;amples Arrived within Hold Time,- q ]No EINIAd.
Analysis
b
�hort Hold Time Analysis (<72hr)- ryas lin. C] NiA 6,
nush Turn Around Time t equested dyes lnsd [3rtA 7
ufficient Volume: Yes Dud EINIA 8,
:orrect Containers Used: Yes ON LINIA 9,
-Pace Containers Used, 14yes ON ONJA
u LJ "J
ontsiners Intact: Yes C]No 0 NIA 10,
iltered volume received fcErDissoE�ved tests DYes n-No NIA 11, rh,__ n_ I r_�
amp8e Labeie� match CDC, fll)(es Dud DNIA 12
-includes datedirne/ID/Analysis Matrix" �J k
I containers needing preservation have been checked,
,Ylyes ONo EINJA 13,
I containers needing preservation are round to be in
nrchance vvith EPA recommendation, /`Yes DNo EJNIA
,epVons, VOA, cafform, TOC, O&G, VVII-DRO (water) ID Yea Duo
7 lnfliW when eomp@eled
imples checked for dechlorination: /Yes 0 No EINIA 14.
�adspace in VOA Vas 0Y,_1 1111, INIA 15,
ip Blank Present', fires Ono INIA, 16,
ifs Blank Custody Seals F'resent DYes Ono �JNIA
ace Trip Blank Lot# (if purchased):
lent Notification/ Resolution. Reid Data Required? Y N
Person Contacted: Date(Time-
'orr ments/ Resolution:

Pace Anaryticat Services, Inc. Pace Analytical Services, Inc. Pace Analybcal Services, Inc.
205 East Meadow Road -- Sub A 2225 Riverwde Dr 9800 Kincey Ave Suite 100
Eden, NC 27288 Ashes,We NC 28804 riuntersviRe, NC 2 B078
[phone] [phone] [phone]
February 16, 2011
Mr. Wayne Kelly
Delta Apparel
1.0, Box 37
100 West Pine Street
Maiden, NC 28650
RE, Project: FEBRUARY 11 WEEK 1 DAY 2
Pace Project No,-, 9286943
Dear Mr, Kelly:
Enclosed are the analytical results for sample(s) received by the laboratory on February 02, 2011,
The results relate only to the samples included in this report, Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me,
Sincerely,
Erin Waters
erin,waters@pacelabs-cord
Project Manager
Enclosures
cc Mr Jackie Marvell, Delta Apparel
REPORT OF LABORATORY ANALYSIS
"his report shall nW, be reproduced. except in kfll,
without the written consent M Pace Analytical Services, r nc
Page 1 of 14

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, In
aceAnacal 206 East oleanow Road - Su rto A 2225 Riverside Dr, 9800KmceyAve Suiteloo
Eden, NC 27288 Asheville. NC 28804 Hunterqville, NC,28078
[phone] [phone] [phone]
CERTIFICATIONS
Prolect: PEBRUARY 11 WEEK 1 DAY 2
Pace, Project No., 9286943
Asheville Certification I
2225 Riverside Dr., Asheville, NC 28804 North Carobna Wastewater Certification #: 40
Connecticut Certification #PH-0106 Pennsylvania Certification #: 68-03578
Ronda;NELAP Certification # E87648 South Carolina Biciassay Certification #:99030002
Massachusetts Certification #: M-NC030 South Carolina CertifiGation #. 99030001
New Jersey C ertificabon # NC 01 I Virginia Certification #. 00072
North Carolina gloassay Cerinficatmn # 9 West Virginia Certification #. 3,56
North Carolina Drinking Water Certification #37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Caroilria Drinking Water Certification #: 37738 Virginia Drinking Water CerbficatQn # 00424
REPORT OF LABORATORY ANALYSIS
This report iihaH not be reproduoed, except in ful!
without the wntten consent of Pace AnaCliticalt Services, inc,
-MIX"

PPIFF,
Pace Analytical Services,, Inc,
Pace Analytical Services, Inc,
Pace Analytical Services, Inc.
ceAnalyfical
205 East Meadow Road - Sude A
2226 Rtvemde Dr,
9800 Kinoey Ave Suite 100
mwpacelab&o" Eden, NC 272a8
AsheviVe NC 28804
Huntersvilfe, NC 28078
[phone]
[phone]
[phone]
SAMPLE ANAL
E COUNT
Project
FEBRUARY 11 WEEK 1 DAY 2
Pace Project No,
9286943
Analytes,
Lab ID
Sample to
Method
Analysts
Reported
Laboratory
S286943001
EFFLUENT COMP
SM 2540D
KPP
1
PASI-E
EPA 200,7
JMVV
2
PASI-A
SM 5210B
SHB
1
PASN-A
EPA 501
SAJ
I
PAS@ -A
9286943002
EFFLUENT GRAB
EPA 1201
RAB
1
PASI-A
SM 4500-S2D
RAB
I
PAST -A
EPA 420A
SAJ
I
RASI-A
9286943003
AERATION BASIN I GRAB
SM 25401)
KPP
I
PASI-E
EPA 160 4
JKS
I
PAST -A
9286943004
AERATION BASIN 2 GRAB
SM 2540D
KPP
I
PASI-E
EPA 160A
JKS
1
PAST -A
REPORT OF LABORATORY ANALYSIS Page 3 of 14
TNs report shall not be repmduced, except in full,
wahout the wdoen consent of Pam Analyticad Selvices, Inc

/*,,�2 0
aceAnalytical
PaceAnetyticai Services, Inc,
205 East Meadow Road - Suite r\
Eden, Nt27288
[phone]
Pace Analytical Smiees, rocs
2225 ilivemde Car,
Asheville, NG 28804
(828)254-71 6
ANALYTICAL RESULT
Pace Analytical Services, tnc
MR
980O KinceyAve Suite lifts
Hunteravifle NC 28078
(t r14)875-9Ci97
Prate t: FEBRUAR'Y' 11 VVEEK 1 DAY 2
Pace Project No,: 9286943
Sample: EFFLUENT COMP
LabID: 92869 3001 Collected.
02102/11 07U0
Received, 02/0 111 11,32 Matrix Water
Parameters
Results Units Report Limit
DF
Prepared
,Analyzed
C.A$ No
Quid
2540D Total Suspended Solids
Analytical Method. SM 2540D
Total Suspended Steads
11.3 mgr'L
8.3
1
02104/11 09:24
200,7 MET 1QP
Analytical hlelhird' EPA 200,7 Preparation Method: EPA 2007
Chromium
ND a lL
5,0
1
02106111 13 00
02108(11 22 34
7440-47_3
Copper
18 9 uglL
5.0
1
02106111 13,00
02,108/11 2 34
7440-50-8
5210E BCD, 5 day
,Analytical Method: SM 5210E
12Qta, 5 day,
D mgr`t_
ZO
1
02J03il l 11:08
02108/11 13.15
t14
350.1 Ammonia
Analytical Method. EPA 3%1
Nitrogen, Ammonia :
0,10 rng/L
9.10
1
02/11111 12:58
7664-41-7
Sample; EFFLUENT CRAB
Lab ILt: 9286943002 Collected
02,102,11 0630
Received 02102/11 11.32 Matrix., Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No,
Qual
120.1 Specific Conductance
Analytical Method: EPA 120.1
Speofic Conductance
11600 urnhoslcrtl
10,0
f
92103111 22A0
N2
4500S2C1 Sulfide Water
Analytical Method: SM 4500-S2L1
Sulfide
Alto mg1L
010
1
02a/08/11 23:00
18496 25-8
4204 Phenolics, Total
Analytical Method FP.A 42014
Phenol
3.6 mg/L
0.10
10
02108/11 1426
108-95-2
Sample. AERATION BASIN 1 GRAB
Lab ID: 9286943003 Collected:
02r`02,111 06.20
Received. 02/02111 11,32 Matnx Water
Parameters
Results Units Report Limit
OF
Preoaret
Analyzed
CAS No.
Qu l
2540D Total Suspended Solids
Analytical Method° SM 2540D
Total Suspended Solids
5240 rngll_
250
1
02,104i11 09.25
160.4 TVSS
AAalytEcal Method ERA 160.4
Volable Suspended Salida
4560 rng1L
109 0
1
02108/11 13:29
Sample: AERATION BASIN 2 GRAB
Lab tD. 9286943004 Collected
02102111 86 25
Received: 0219 t 11 11 32 Matrix: Water.
Parameters
Pesults Units Report Lirrr1
DF
Prepared
,Analyzed
CAS No,
Qual
2540D Total Suspended Solids
.Analytical Method SM 2540
Total Suspended Solids
5980 mg1L
250
`I
02t04111 09 26
Hate 02116120111 04:17 Poll REPORT OF LABORATORY ANALYSIS Page 4 a1 14
This repiwit shall not be reproducedexcept ir:full;
without the wart{en ro asent at Pace Analytical Services, Inc,_,

j It PaceAnalytical Services, Inc Pace Analytical Services, Inc: Pace Analytical Services, Inc:
" f is 205 East Meadow Road - SutteA, 2225 R4erssde Dr 9800 Kincey Ave, Suite IG
w4wpaivelftaxv
Eden NC 27288 Aghevs4e, NG 295it4 Hu€reter wite NC 26076
[phone] (82 )254-r176 (704)876_999
ANALYTICAL RESULTS
Project FEBRUARY 11 WEEK 1 DAY 2
Paco Project Nci : 9286943
Sample: AERATION BASIN 2 GRAB Lab I : 52864404 Coltected, 02102/11 tip 25 Received02102111 11:32 Matn x Water
Parameters Results Units Report Limit DF Prepared Analyzed SAS No, Qual
1160,4 TVSS _ Analytical Method EFTA 160A
Volattle Suspended Solids 5050 rnglL 100 1 02108111 13 3tt
Date. 211 ,i2011 0417 PM REPORT OF LABORATORY ANALYSIS Page a of 1
This eport Vital not be repinduiaed, except in fun,
without the w6ttert consent of Race AnaiyticW Services Pnc,:

Pace Analytical Services, Inc, Pace Analytical Services, Inc.
aceAnalytcalo 205 Easl Meadow Road - Suite A 2225 Rwersde Dr.
wwwPecakI&SCOnt Eden. NC 272BB Asheville. NO, 28804
;336)6234921
(62B)254-7176
Pace Analytical Servi
9800 Kincey Ave, Suite 100
Hunten;Wle, NC 28076
[phone]
Project, FEBRUARY I I WEEK 1 DAY 2
PaCe Project No, 9286943
QC Batch: EDEN16617
Analysis Method:
SM 2540D
QC Batch Method SM 2540D
Analysis Destai ctron
2540D 7otal Suspended Solids
Associated Lab Sarnplies- 9286943001 9286943003,9286943004
METHOD BLANK: 559873
Matrix,- Water
Associated Lab Samples: 9286943001 9286943003,9286943004
Blank Reporting
Parameter Units
Result Limit
Analyzed QuaHfiers
Total Suspended Solids mg/L
ND
2.5 02/04111 09 15
LABORATORY CONTROL SAMPLE. 569874
Spike LC S
LCS % Rec
Parameter Units
Cons, Resuit
% Rec Limits Qualrfiers
Tolai Suspended Solids mg/L
250 248
99 80-120
SAMPLE DUPLICATE 559,R75
9286867003 Dup
Parameter Units
Result Result
RPD Quaiifiers,
-Tolal Suspended Solids mg1L
129
144 11 R2
SAMPLE DUPLICATE. 559876
9286943004 Dup
Parameter Units
Result Result
RPD Quafifiers
Total Suspended Solids mg/1"
5980 5600 7
Dada02116/2011 04:17 PM REPORT OF LABORATORY ANALYSIS
TNs report shall not be reproduced except in fuTi,
voIhow the written consent of Pace: Analytcal SeNices, Mc
MIX,.

k
Pace Analytical Services, Inc. Pace Analytical Services, Inc_
Pace Analytical Services, Inc.
Ceiit
205 East Meadow Road - Suite A 2225 RiversOe Llr
980O Kinirey Ave Suite rs9
Eden, No 27288 Asheveile, NC 2SP04
riunrersvflie, etc 28978
(336)621,-8921 (828)284-71 79
(704)8 i9-9tt92
QUALITY CONTROL DATA
Project FEBRUARY 11 WEEK t DAY 2
Pace Project No ' 9286943"
QC* Batch MPRP17835
Analysis fathead` EPA 200,7
QC Batch Method: EPA 200 7
Analysis Llesempt on, 200 7 MET
Associated Lab Samples9286943001
METHOD BLANK 5595
Matrix Water
Associated Lab Samples 9286943001
Blank; Reportln '
Parameter
Units
Result Limit: Analyzed QUalitters
Uhrorruum
uglL
ND 5,0 02108/1120.31
Copper
ug/L
Nth 50 02108/11 20,31
LABORATORY CONTROL SAMPLE.
559555
Spike LCS LCFS % Red
Parameter
Units
Ctonc; Result % Rec LimitsQUali3ers
.........
Uhr°orrtium
ug/L
500 502 100 85-115
Copper
ug/L
500 488 98 85-115
MATRIX SPdKE SAMPLE.
559556
9286861005 Spike MS 1v1S
% Rec
Parameter
Units;
Result Cons, Result, % Rec
Urnits Qualifiers
Cfhr15rT8duEt"4.
ug/L
Ct.041 rm1L 500 545 101
70-130
Copper
ug/L
0.024 mg1L 500 560 107
70-13
MATRiX SPIKE SAMPLE
559558
9287001001 Spike MS MS
% Rec
Parameter
Units
Result Cron; RCsuit Re
Urnits Qualifiers
Uhronuum
ug/L
16.2 503 504 98
70-130
Copper
ug/L
ND 500 520 104
70-130
SAMPLE DUPLICATE' 559557
"92 942004 C1up
Parameter
Units
Result Result RED Qualifiers
Chromium
ug/L
ND 66J
Chipper
ug/L
ND 63J
SAMPLE DUPLICATE. 559,559
9287001002 Dup
Parameter
Units
Result Result RPU Qualifiers
Chromium
a 1L.
239 246 3
copper
ug/L
255, 258 1
Cate 02/1612011 04 17 Plat
REPORT OF LABORATORY ANALYSIS
Page 7 of 14
Thm report shall not be reproduCed, except m fall,
without the written consent of Pace Analytical Services, 6rtc

Pace Analytical Services, Inc, Pace Analytical Services, Ind. Pace Analytical S-7 'a. qw
205 East Nlead�w 25 Road - Suite A 22Riverside Dr. 9800 Kinrey Ave, Suite 1 uO
aceAnallyfical"' Eden, NC 272,98 Ashevihe, NC 2880A Hunlersvdie, NC 28078
Wwalpaceiabs com
[phone] [phone] [phone]
WAMIXL#�� .�
Project FEBRUARY 11 WEEK I DAY 2
Pace Project No.: 9286943
QC BatchET/1 5264
Analysis Method EPA 120 1
QC Batch Who& EPA 120,1
Analysis Descri 120.1 Specific Conductance
Associated Lab Samples: 9286943002
MET140D BLANK: 559813
Matrix
Water
Associated Lab Samples 9286943002
Blank
Repa,rting
Parameter
Units
Result
Limit
Analyzed Quafifiers
Specific Conductance
urnhas/cm
ND
10,0
02103111 22 40 N2
LABORATORY CONT ROL SAMPLE:
559814
Spike
LCS
LOS % Rec
Parameter
Units
Conic
ReSU11
% Rec Lvmts Qualifiers
Specific Conductance
urnhos/cm
1410
1440
102 90-110 N2
SAMPLE DUPLiCATE, 559815
9286755001
Dup
Parameter
Units
Result
Result
RPD QuWifiers
Specific Conductance
umhos1crn
476
475
0 N2
SAMPLE DUPLICATE 559816
928,6755002
Dup
Parameter
UnIls
Result
Resuft
RPD Quafifiers
Specific Conductance
umhosicrn
1330
1310
1 N2
Date: 02116/2011 04:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall nol be reproduced exrxpt in fall
without the written consent cif Pace Analytical SeNices, Inc
Page 8 of 14

a°
Pace Analytical Services, Inc face Anallyficai Services, Inc.
Paco Analytical Services, Inc.
205 Last Meadow Road - SuiteA 2225 Riverside Or
ace
9800 Kkncey Ave. Suite 100
WWwPffcWhb&C0M
Eden, NC 2728Achevffle, NC 285
Huntersville NC 28078
[phone] t82 ; s4.7 -7
(704)87 -9092
QUALITY CONTROL DATA
Pncatet t: FEB RUARY 11 WEEK 1 DAY
Pace Project No 9286943
C Batch. FT/18300
Anaiy ss Method EPA 160 A
QC Batch Method EPA 18t1 4
Analysis Description: 160,A Total Volatile Suspended Solids
Assoc4ted Lab Samples 9286943003 9286943004
METHOD BLANK: 561094
Matrix: Water
Associated Lab Samples 9286943003, 928694300
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Volatile Suspended Solids M911-
ND 1.0 E2/08t11 13,29
SAMPLE DUPLICATE; 561095
9286943003 Uud
Pararnet r Units
Result Result RPD Qualifiers
Volatile Suspended Solids rng/L
4880 4499 A
Lute 02/1612011 04:17 PM REPORT OF LABORATORY ANALYSIS
Thm report sdaai9 not be aeprodixed, except m fur,
without the written dransent of Pace Analytical Services, inr,
Page deaf 1

+ t Face Analy icat Services, Inc, Pace Analytical Services, Inc..
7 t r T 24 Past Meadow Road - Suite A 2225 Riverside Dn
Eden, NC 27288 AshevOle NC 28804
[phone](928),254-72 7
AAJALITY CONTROL
Pace A alyticat Services, Inc.
9800±t,rceyAve suiteIDD
Huntcrswtle, NC 28978
(7 ,1)875-9092
Project: FFSRUARY 11 WEEK 1 DAY 2'
Pace Project No.: 92 943
QC Batch, WET/15309
Analysis Method,
Sly 4500-S211
CC Batch Method: SM14500—S2La
Analysis Ltesnriptiom
4 0OS2D Sulfide Water,
Assodated Lab Sarnp8 s. 9286942002
METHOD BLANK561466
Matrix: Water
Associated Lab Samples, 9286943002
Blank: RepC1r`t➢fR€
Parameter
Units
Result Limit
Analyzed
Quallfiers
_-
su fide
mg/L
IND 0:10 02108111 23
00
LABORATORY CONTROL ?L SAMPLE
561467'
Spike LCS
LC S
% Rec
Parameter
Units
Ctins,;. Result
% Red
Limits d uaIifiers
Su fide
mElifl,
.5 05,2
104
90-110
MATRIX IX SPXE SAMPLE
56146B
928682 002 Spike
MS
MS % Reb
Parameter
Units
Result Cone,
Result
% Reu Limits Qualifiers
Sulfide
rt /L
ND 5
053
106 75-125
SAMPLE GUPUCATF 561469
..�_a
,...,., gym.......
286285019 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Sulfide
mtgfL
107 107
fl
Late. 02/1612011 04:17 PM REPORT OF LABORATORY ANALYSIS
T"hrs report shall not be reproduced, except in full.
w•fthout the xrntten consent of Pace AnaEyl oil Seroces, Inc
Pape 10 of 14

Paco Analytltal Services, Inca Pact Analytical Services, Inc.
Pace Analytical Services„ Inc,
205 East Meadow Road - Suite A 2225 R versfide uf:
980O KinoeyAve 844elOC
Eden, 27288 Abe4`tFEe, NC 2834
lua €ersva9le, PS C 2k30; t4
(3 6)623-8921 (82 )254-7 N 16
[phone]
QUALITY CONTROL DATA
Prolect. FEBRtiARY 11 WEEK 1
DAY 2
Pace Protect No- 9286943
QC Batch LET 15250
Analysis Method SIR 5210B
QC Batch Method SM 5210L1
Analysis Description; 521OB BOO, 5 day
Associated Lab aarrlplas 92 694300
METHOD BLANK: 559317
Matrix: Water
Associated Lab Samples 9286943001
Flank Reporting
Parameter
Un t Result Limit Analyzed < Qualifiers
FQ , 5 day rrlg/L
ND 2.0 02/08111 1115
LABORATORY CONTROL SAMPLE 559313
Spike LQS LE % Res
Parameter
knits Gone Result % Rec Umits Qualifier -
BOD, 5 day mgrL
198 155 78 84--11513
SAMPLE DUPLICATE, 55 319
9287026001 Dup
Parameter
Emits Result Result RPD Qualrfiers
FQC1, 5 day mg/L_
27.0 33.0 20 I34
Date0211 /2011 04 17 Pit
REPORT OF"LABORATORY ANRALLY I
Page 11 of 14
This mport shall not be reprsdwoe4, exnept in fait,
wdr lout the written consent of Pace Analytical Services Nnc.,

aceAnal
ytical
wroerparmelabs com
Pace Analytical Services, Inc,
2e5 Past Meadow Road - Suite
Eden, NC 27288
t3991823-8921
tM i
Face Analytical Services, Inc,
2225 Riverside D
AsheusfVe, NC 28804
[phone]
Pace AnalyticalSeraicea,9no..
9899 hi(mcey-A., Suttee loo
Huntersvdie, NC 28078
[phone]'
Project: FEBRUARY 11 WEEK 1 DAY
Pace Project plo.9286943
QC Batch: VVETAJ9097
Analysis Method EPA 350.1
QC flitch Method EPA 350 1
Analyses D scrilabon 350.1 ,Arritnorara
Associated Lab SampMes 9286943001
METHOD BLANK 562545
MatWater
Associated Fat; Sametes, 9286943001
Blank Reporting
Parameter
Units
Result l rrn'st Analyzed
Qualifier
Nitrogen, Ammonia
rtm ]L
ND 0,10 02/11111 1215
E..? BORATORY CONTROL, SAMPLE.
562546
Spike I LQS
% Rec
Parameter
!Inns
Gant; Result % Res
Limits Qualifier's
Nitrogen,
g
g/L
5 5.1 103
90110
MATRIX SPIKE SAMPLE
662547
9287108001 Spike MS
NIS
% Res
Parameter
Units
Result Cons Result
% Reo
Limits Qualifiers'
Nitrogen, Ammonia
rrlgtL
269 5 31.8
98
90-110
MATRIX SPIKE SAMPLE:
562549
9287357001 Spike Ms
MS
% Rec
Parameter
r.�..�._...__.�
Units
Result E"onc: Result
%Ret
limits Qualifiers
Nitrogen, Ammonia
----L
mg/
-ND -� 5 6.._u...�
,w 17_...
90-110 131 .a.�.ss.
SAMPLE DUPLICATE, 562548
286867 01 Cup
Parameter
Units
Result Result RPD
Qualifiers
Nitrogen AM rromar
rrrglL
ND ND
SAft9PLEDUPLICATE: 562550
286925002 Dog
Parameter
Units
Result Result RED
Qualifiers
Nitrogen Ark monta
fitrgiL.
017 0.17 t
Caw 02116a2011 tit 17 PM
REPORT OF LABORATORY LYSI
Pace 12 of 14
This ,report shall riot to reproduced except in full,
without the written consent of Pace Analytical Services, Inc

Race Analytical Services, the.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-692
Pace Analytical Services, Inc,
2225 Riversce ter:
Asheville, NC 2R804
[phone]
QUALITY CONTROL DATA
Face Aniaytica$ Services, Inc:.
9800 Kdncey Ave. Suite 100
Hunter ville, NC 28078
[phone]
Project FEBRUA,RY 11 WEEK 1 DAY 2
Paces Project No: 9286943
CC Batch: WETA19062
Analysis Method. EPA420A
CC Batch Method EPA 420A
Analysis Description: 420.4 Phenolri
Associated Lab Samples 9286 4300
METHOD BLANK 560428
Matrix: Water
Associated Laic Samples: 9286943002
Blank Reporting
Parameter
Units
Result - Limit
Analyzed
Qualifiers
Phenol _
rng1L
Nth 0,010
02/08/111159
LABORATORY CONTROL SAMPLE,
560429
Spike LOS-
LCS
% Rec
Parameter
Units
Conc: Result
% Red
Limits Qualifiers
Phenol
mg/L
25 0.26
99
90-110
MATRIX SPIKE SAMPLE:
560430
9286694001 Spine
MS
MS
% Rec
Parameter
Units
Result Cann:
Result
% Rae
Limits qualifiers
Phenol _
mg1L
NC .25
0095
� 35
90-110 M1
MATRIX SPIKE: SAMPLE
560431
9286694002; Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Phenol
img/L
ND 25
0 090
34
90-11a h11
SAMPLE DUPLICATE 560432
9287004002 Du
Parameter
Units
ResultResult
RPD
Qualifiers
Phenol
mglL
0.11 0.073
41 D6
SAMPLE DUPLICATE: 560433
9286569002 Du
Parameter Units Result Result RPD Qualifiers
Phenol mgfL 0.034 0 076 77 D6
Date 0211612011 04,17 Pit REPORT OF LABORATORY ANALYST
'Tires report shall not be reproduced, except in fuki,
without the written consent of Pace Anakytical Services. Inc.,

qPace Analytical Services, Inc. Pace Analytical Services, Inc, Pace Analytical Services, Inc.. y Ave Suit
e
1
ace,AnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kinsey Ave, Suite 1 0a
sv
7 [lie NC 280
corri Eden, NC 27288 Asheville, NC 28804, Huntersv[fle, NC 28078
[phone] [phone] [phone]
QUALIFIERS
Project, FEBRUARY 11 WEEK I DAY 2
Pace Project No., 9286943
DEFINITIONS
RE - Dilution Factor, if reported, represents the factor applied to the reported data due to changes In sample preparation, dilution of
the sample aliquot, or moisture content,
ND - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and betow the adjusted reporting limit.
MDL -Adjusted Method Detection Limit
S - Surrogate
1,2-Diphony1hydrazme (8270 listed analyte) decomposes to Azottenzene,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values,
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable,
SG - Silica Get - CleanUp
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodipherylarnine decomposes and cannot be separated from Diphertylamine using Method 8270, The result reported for
each au alyte is a combined concentration
Pace Analytical is NELAP accredited Contact your Pace. PM for the current list of accredited analytes
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-E Pace Analytical Servioes, - Eden
ANAL QUALIFIERS
134 The gfucose/glutarnic acid standard exceeded the range of 198 plus or minus 30,5 mgfL
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control Ilmits
M1 Matrix spike recovery exceeded QC limits Batch accepted based on laboratory control sample (LCS) recovery
N2 The We does not hold NELAC accreditation for this parameter
R2 RPD value was outside control limits due to matrix interference,
Date: 02/16i(2011 0417 Phil
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except infrifl,
without the written consent of Pam Analytical Services, Inc.
lat
Page 14 of 14