WQ0010689_Residual Annual Report 2020_20210225

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0010689
Applicant/Permittee Baxter Healthcare Corporation
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * Corey Carpentier
Email Address*
[e-mail]
Project Information
........ ......... ............................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
828-756-6636
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0010689
Has Current Existing perm nurber
Applicant/Permittee Address* 65 Pitts Station Road
Facility Name * Baxter Healthcare Corporation DCAR
Please provide comments/notes on your current submittal below.
2020 Annual Report for Ash Residual Land Application
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Baxter Healthcare_ Annual Report.pdf 4.31MB
F Upload only 1 Rdocurrent (less than 250 `VB). Miltiple documents rust be combined into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Cot'e� Ca�Pewlet'
Submission Date 2/25/2021

Baxrer
2/ 19/2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2020 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
Enclosed is the 2020 Annual Ash Distribution Report using the forms provided by NCDEQ-
DWQ. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Ash Distribution Landowner Utilization Agreements
- Lab Sheets
There were no permit deviations during the 2020 Reporting Year.
If you have any questions or require additional information, please contact myself at 828-756-
6636.
Sincerely,
Corey Carpentier
Attachments: Annual Ash Report (3 copies)
Cc: Rickey Styles
Baxter Healthcare Corporation
PO Box 1390. Marion, NC 28752
T 828.756.4151

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 21 No Y --* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
WQ0010689
60
317.5
377.50
See DMSDF Supp, Form
317.5
Land Application
March
April
WQ0010689
55
390
445.00
See DMSDF Supp. Form
390
Land Application
May
June
WQ0010689
65
307.8
372.8
See DMSDF Supp. Form
307.8
Land Application
July
August
September
WQ0010689
50
329
379.00
See DMSDF Supp. Form
329
Land Application
October
November
December
Total from FORM DMSDF (sup)
230
1344.3
1574.3
1344.3
Totals:
Annual (d tons):
230
1344.3
1574.3
1344.3
Amendment(s used: None Bulking Agent(s) used: Dry Wood Chips
* if more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No 0, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/ 19/2021
Signature of Pe ittee Date Sign ure of Pr arer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2/ 19/2021
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0010689 FACILITY NAME:
PHONE:[phone] COUNTY:
FACILITY TYPE (please check one):
Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
McDowell OPERATOR: Baxter Healthcare
❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
0 Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment!
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
February
WQ0010689
60.00
317.50
377.50
Jim Pate, Paul Boone, Jim Brewer
317.50
Land Application
A it
P
WQ0010689
55.00
390.00
445.00
Jim
nBrewer, Roger Moore, Jeff
390.00
Land Application
June
WQ0010689
65.00
307.80
372.80
Max
ewe ollard, Jim Phillips, Jim
307.80
Land Application
September
WQ0010689
50.00
329.00
379.00
Jim Phillips, Roger Moore, Kenneth
Hughes, Roger Moore.
329.00
Land Application
Totals:
Annual (dry tons):
230
1344.3
1574.3
1344.3
Amendment(s) used:
1
Bulking A ent(s) used: Dry Wood Chips
n iQ `�rRmneacnF rc��.,.,i ��oronnat - Total Number of Form DMSDF (Supp) 1
* If more space is required, attach additional information sheets (FORM D%R

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689 Laboratory:
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analvsis Data
WQ0010689
NA
1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m )2
Sam le
NP8262020A
NP8262020B
SP5112020A
SP5112020B
NP03242020A
NP03242020B
Percent Moisture (%)
NA
59A
54.4
57.3
61.9
62.4
61.7
Aluminum
NA
11,800
11,200
9450
10800
7490
7250
Arsenic
75
ND
2.2
ND
ND
ND
ND
Cadmium
85
3.3
2.5
2.4
3.3
2.3
2.4
Copper
4,300
80
68.8
52.2
68.1
60..8
61.9
Lead
840
30.7
31.2
23.1
23.5
16.3
17.1
Mercury
57
ND
ND
ND
ND
ND
ND
Molybdenum
75
ND
ND
ND
2.5
ND
1.4
Nickel
420
21.2
18
15.5
17.5
13.5
12.9
Selenium
100
ND
ND
ND
ND
ND
ND
Zinc
7,500
270
226
207
235
173
172
Phosphorus
NA
3050
2390
3130
3140
3130
3140
Calcium
NA
119,000
97900
98800
118000
87300
93000
Magnesium
NA
15,800
13500
11200
13600
9980
10100
Potassium
NA 1
14,000
11100
17400
20700
12600
14600
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties four subm' in false information, including the possibility of fines and imprisonment for knowing violations."
Signattof Pr/parer
2/ 19/2021
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689
Facility Name: Baxter Healthcare Corporation North Cove
Steam Generation Plant Ash
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
WQ0010689
NA
Laboratory: 1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Com osite Date
NP8262020A
NP8262020B
SP5112020A
SP5112020B
NP03242020A
NP03242020B
Ammonia
ND
ND
ND
ND
ND
ND
Nitrate Nitrogen
ND
ND
ND
ND
ND
ND
Nitrite Nitrogen
ND
ND
ND
ND
ND
ND
PAN (by calc)
810
819
1620
2100
927
1060
SAR (by calc)
6
4.8
9.8
9.5
7.8
9.3
TKN
2700
2730
5400
7000
3090
3520
Sodium
8340
6100
12200
13000
9120
11200
pH
9.8
9
9
9
8.9
9.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2/ 19/2021
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to N: / (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall he taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g.. transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must he available during Iransponation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the fallowing shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot ofthe seasonal high water table or bedrock.
• Ash shall not he applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs Ibllowing a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill. misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash. 1_\ _
Signed (Ash Recipient): C� Date: 2-2 Q- c_0
Ash Recipient's Address: f f Ive-k %(�, C,
Intended Use of Ash:
Expected Qty/Yr: 0 _2�0 IV cres f nd: A 4 i2._
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization
Agreement (Valid thru Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to jZ r-, Pre4rvr
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheegecrpient).
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leakproof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage.- The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
• Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table,
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10*6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratorresults
are available upon request. y
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or oth of the ash.
Signed (Ash Recipient): Date: L
Ash Recipient's Addr 'r
Intended Use of As
Expected Qty/Yr:
Baxter Representative Signature: �✓J 1/

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided tom►. i/ y (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions •n this sheet.
Transport: Adequate provisions shall he taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
+ Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
Ash shall not be placed within one foot of the seasonal high water table or bedrock.
0 Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the inlixmation sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare. Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare. Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): /e, t�� Date: Ltd
Ash Recipient's Address: - 7t��' 6-a,.�,, XY ), rr, fZ_
Intended Use of Ash:✓ .•
Expected QlyNr: /OG )"T re f La C�d
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11130119) Baxter Co
L� � PY
L
Baxter Healthcare, Corp., is the generator of the ash provided to ll m /11 7 f4l t k 0
Application of the aforementioned ash is prohibited except in accordance witif the instructions on this sheegecipient),
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on We application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., Iimited to that needed
to meet the liming requirements of the crops being grown on the land).
' Ash shall not be stockpiled for more than 60 days prior to land application
' Application of bulk residuals shalt not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10'6 centimeters per second. If such a linerrcover is provided,
ash shall not be placed within 25 feet of any water supply well or spring,
• The ash shall not be applied to any site that is Hooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash: 5 I r ta, � !h Cw�
Expected Qty/Xr: �6
Baxter Representative Signature:
Page
Updated: i 1-07-14
Date:
nt
of�l srtd: . 21)0

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to 4�� 4 e g"o (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instro tions on this
rrawort: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e-g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ00f0689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied -
Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash: Z ,
Date: — e Z
Expected Qty/Yr: f .. Acresof Land: 4; D
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020
67

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19)y Baxter Copy
Baxter Healthcare Coash Pththekinkstgructions
Application of the�aforementionde shais pohibitd except in aprovided ctor c �on this sheet,ectprent).
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
trartspotter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
• to meet the liming requirements of the crops being grown on the land).
Asb aball not be stoc4fiW for more than 60 days prior to land application
• Applicetion of bulk residuals shall not occur within 100 feet of a public or private water supply
• A Copy of this Utilization ASreeatent shall be maintained at the land application site when bulk residuals are
b4% applied.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10'6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient):
Date;
Ash Recipient's Address: er4i>r Aow /�/ /✓C 2C7Sz
Intended Use of Ash: -
Expected Qty/Yr:
Baxter Representative Signature:
Acres of Land: _ �5
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to P G— �, ) e (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall he taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must he available during transportation or land application activities. Any spill oCcurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may he necessary under windy or rainy conditions or if erosion or runoff cannot he
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justiftted (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams.
perennial waterbodies, and wetlands,
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not he applied to any site under the following conditions:
(: Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0,5" rainfall
o fi the land application site does not have established vegetative cover crop
If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not he held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
hodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash
Signed (Ash Recipient): _ Date: l
Ash Recipient's Address: d �ILL y,
Intended Use of Ash:
Expected Qty/Yr: - Z%L—p ,v Acres of Land:
Baxter Representative Signature:
Page 2 of 3
Updated- January 2020

Baxter Healthcare, Corp.
2859 old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to l*f•4Kh> fRecipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall he adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be nccessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall he limited to those that can be agronomically justified (i.e... limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands,
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not he placed within one foot of the seasonal high water table or bedrock,
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow covered or other condition causing; runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be he'd liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore. Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): Date: f2ZL/
Ash Recipient's Address: A, S~ Q R "W,4 R Ne-BO W ,-f-
Intended Use of Ash: xr>/ 4 4� RPa/ne, (T-
Expected Qty/Yr: �� / v
Baxter Representative Si
of
Page 2 of 3
Updated: January 2020
/ VQ AV
�Ls-'/- /

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 09, 2020
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: WOOD BOILER ASH 082620
Pace Project No.: 92492498
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on August 26, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92492498001 NP8262020A EPA 601OD
SH1
13
PASI-A
EPA 601OD
SH1
7
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
92492498002 NP8262020B EPA 601OD
SH1
13
PASI-A
EPA 601OD
SH1
7
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Sample: NP8262020A Lab ID: 92492498001 Collected: 08/26/20 08:30 Received: 08/26/20 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
11800 mg/kg
17.8
1
09/03/2015:31
09/04/2018:46
7429-90-5
Arsenic
ND mg/kg
1.8
1
09/03/2015:31
09/04/2018:46
7440-38-2
Cadmium
3.3 mg/kg
0.18
1
09/03/2015:31
09/04/2018:46
7440-43-9
Calcium
119000 mg/kg
178
10
09/03/2015:31
09/05/2015:57
7440-70-2
Copper
80.0 mg/kg
0.89
1
09/03/2015:31
09/04/2018:46
7440-50-8
Lead
30.7 mg/kg
0.89
1
09/03/2015:31
09/05/2016:00
7439-92-1
Magnesium
15800 mg/kg
17.8
1
09/03/2015:31
09/04/2018:46
7439-95-4
Molybdenum
ND mg/kg
0.89
1
09/03/2015:31
09/04/2018:46
7439-98-7
Nickel
21.2 mg/kg
0.89
1
09/03/2015:31
09/04/2018:46
7440-02-0
Potassium
14000 mg/kg
892
1
09/03/2015:31
09/04/2018:46
7440-09-7
Selenium
ND mg/kg
1.8
1
09/03/2015:31
09/05/2016:00
7782-49-2
Sodium
8340 mg/kg
892
1
09/03/2015:31
09/04/2018:46
7440-23-5
Zinc
270 mg/kg
1.8
1
09/03/2015:31
09/04/2018:46
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA601 OD Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 08/30/20
13:34
Initial
pH: 5.34; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
09/01/20 02:07
09/01/20 10:56
7440-38-2
Barium
2.1 mg/L
0.25
1
09/01/20 02:07
09/01/20 10:56
7440-39-3
Cadmium
ND mg/L
0.0050
1
09/01/20 02:07
09/01/20 10:56
7440-43-9
Chromium
ND mg/L
0.050
1
09/01/20 02:07
09/01/20 10:56
7440-47-3
Lead
ND mg/L
0.025
1
09/01/20 02:07
09/01/20 10:56
7439-92-1
Selenium
ND mg/L
0.10
1
09/01/20 02:07
09/01/20 10:56
7782-49-2
Silver
ND mg/L
0.025
1
09/01/20 02:07
09/01/20 10:56
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation
Method: EPA 7470A
Leachate Method/Date: EPA 1311; 08/30/20
13:34
Initial
pH: 5.34; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0.00020
1
09/01/2011:14
09/02/2015:47
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0048
1
08/28/2013:10
08/28/2016:13
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
59.4 %
0.10
1
08/27/20 14:51
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
8.8 Std. Units
0.10
1
08/31/20 15:14
REPORT OF LABORATORY ANALYSIS
BC
H3
This report shall not be reproduced, except in full,
Date: 09/09/2020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Sample: NP8262020A Lab ID: 92492498001 Collected: 08/26/20 08:30 Received: 08/26/20 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 09/09/2020 08:53 AM
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
810 mg/kg 0.12
1 09/08/2015:28 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 22.8
1 08/30/2013:07 08/31/2010:21 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
2700 mg/kg 117
1 09/04/20 06:47 09/05/20 01:34 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/kg 9.7
1 08/27/20 06:40 08/27/20 08:04
ND mg/kg 9.7
1 08/27/20 06:40 08/27/20 08:04 14797-55-8
ND mg/kg 9.7
1 08/27/20 06:40 08/27/20 08:04 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
3050 mg/kg 47.3
20 08/31/20 20:14 09/01/20 19:48 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Sample: NP8262020B Lab ID: 92492498002 Collected: 08/26/20 08:30 Received: 08/26/20 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
11200 mg/kg
14.2
1
09/03/2015:31
09/04/2018:49
7429-90-5
Arsenic
2.2 mg/kg
1.4
1
09/03/2015:31
09/04/2018:49
7440-38-2
Cadmium
2.5 mg/kg
0.14
1
09/03/2015:31
09/04/2018:49
7440-43-9
Calcium
97900 mg/kg
142
10
09/03/2015:31
09/05/2016:04
7440-70-2
Copper
68.8 mg/kg
0.71
1
09/03/2015:31
09/04/2018:49
7440-50-8
Lead
31.2 mg/kg
0.71
1
09/03/2015:31
09/05/2016:07
7439-92-1
Magnesium
13500 mg/kg
14.2
1
09/03/2015:31
09/04/2018:49
7439-95-4
Molybdenum
ND mg/kg
0.71
1
09/03/2015:31
09/04/2018:49
7439-98-7
Nickel
18.0 mg/kg
0.71
1
09/03/2015:31
09/04/2018:49
7440-02-0
Potassium
11100 mg/kg
712
1
09/03/2015:31
09/04/2018:49
7440-09-7
Selenium
ND mg/kg
1.4
1
09/03/2015:31
09/05/2016:07
7782-49-2
Sodium
6100 mg/kg
712
1
09/03/2015:31
09/04/2018:49
7440-23-5
Zinc
226 mg/kg
1.4
1
09/03/2015:31
09/04/2018:49
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA601 OD Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 08/30/20
13:34
Initial
pH: 5.17; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
09/01/20 02:07
09/01/20 10:59
7440-38-2
Barium
2.3 mg/L
0.25
1
09/01/20 02:07
09/01/20 10:59
7440-39-3
Cadmium
ND mg/L
0.0050
1
09/01/20 02:07
09/01/20 10:59
7440-43-9
Chromium
ND mg/L
0.050
1
09/01/20 02:07
09/01/20 10:59
7440-47-3
Lead
ND mg/L
0.025
1
09/01/20 02:07
09/01/20 10:59
7439-92-1
Selenium
ND mg/L
0.10
1
09/01/20 02:07
09/01/20 10:59
7782-49-2
Silver
ND mg/L
0.025
1
09/01/20 02:07
09/01/20 10:59
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation
Method: EPA 7470A
Leachate Method/Date: EPA 1311; 08/30/20
13:34
Initial
pH: 5.17; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0.00020
1
09/01/2011:14
09/02/2015:49
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0040
1
08/28/2013:10
08/28/2016:15
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
54.4 %
0.10
1
08/27/20 14:51
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.0 Std. Units
0.10
1
08/31/20 15:15
REPORT OF LABORATORY ANALYSIS
BC
H3
This report shall not be reproduced, except in full,
Date: 09/09/2020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
Sample: NP8262020B Lab ID: 92492498002 Collected: 08/26/20 08:30 Received: 08/26/20 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 09/09/2020 08:53 AM
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
819 mg/kg 0.12
1 09/08/2015:28 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 19.6
1 08/30/2013:07 08/31/2010:23 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
2730 mg/kg 95.3
1 09/04/20 06:47 09/05/20 01:35 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/kg 8.7
1 08/27/20 06:40 08/27/20 08:07
ND mg/kg 8.7
1 08/27/20 06:40 08/27/20 08:07 14797-55-8
ND mg/kg 8.7
1 08/27/20 06:40 08/27/20 08:07 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
2390 mg/kg 40.6
20 08/31/20 20:14 09/01/20 19:50 7723-14-0
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563609 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2987037 Matrix: Water
Associated Lab Samples: 92492498001, 92492498002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 09/02/2014:38
LABORATORY CONTROL SAMPLE: 2988250
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/L 0.0025 0.0024 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2988251 2988252
MS MSD
92492214001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0026 0.0028 103 108 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563070 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2985785 Matrix: Solid
Associated Lab Samples: 92492498001, 92492498002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 08/28/2014:27
LABORATORY CONTROL SAMPLE: 2985786
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.083 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2985787 2985788
MS MSD
92492279008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND 0.027 0.028 0.014 0.013 50 46 75-125 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 564356 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2991643
Associated Lab Samples: 92492498001, 92492498002
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
09/04/2017:19
Arsenic
mg/kg
ND
1.0
09/05/2014:30
Cadmium
mg/kg
ND
0.10
09/05/2014:30
Calcium
mg/kg
ND
10.0
09/04/2017:19
Copper
mg/kg
ND
0.50
09/04/2017:19
Lead
mg/kg
ND
0.50
09/04/2017:19
Magnesium
mg/kg
ND
10.0
09/04/2017:19
Molybdenum
mg/kg
ND
0.50
09/05/2014:30
Nickel
mg/kg
ND
0.50
09/05/2014:30
Potassium
mg/kg
ND
500
09/05/2014:30
Selenium
mg/kg
ND
1.0
09/05/2014:30
Sodium
mg/kg
ND
500
09/04/2017:19
Zinc
mg/kg
ND
1.0
09/04/2017:19
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2991644
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
465
93
80-120
Arsenic
mg/kg
50
48.5
97
80-120
Cadmium
mg/kg
50
47.7
95
80-120
Calcium
mg/kg
500
477
95
80-120
Copper
mg/kg
50
48.3
97
80-120
Lead
mg/kg
50
47.1
94
80-120
Magnesium
mg/kg
500
456
91
80-120
Molybdenum
mg/kg
50
49.0
98
80-120
Nickel
mg/kg
50
49.6
99
80-120
Potassium
mg/kg
500
ND
99
80-120
Selenium
mg/kg
50
44.5
89
80-120
Sodium
mg/kg
500
477J
95
80-120
Zinc
mg/kg
50
45.7
91
80-120
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2991645
2991646
MS
MSD
92493332001 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Cone.
Cone.
Result
Result
% Rec % Rec Limits RPD Qual
Aluminum mg/kg 815 565
573
2150
1120
236 53 75-125 63 M1,R1
Arsenic mg/kg ND 56.5
57.3
56.2
56.5
99 98 75-125 1
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2991645
2991646
MS
MSD
92493332001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
mg/kg
0.18
56.5
57.3
54.4
55.3
96
96
75-125
2
Calcium
mg/kg
6280
565
573
7350
2830
190
-602
75-125
89 M1,R1
Copper
mg/kg
4.0
56.5
57.3
62.1
57.1
103
93
75-125
8
Lead
mg/kg
1.6
56.5
57.3
54.8
52.9
94
89
75-125
3
Magnesium
mg/kg
535
565
573
1090
898
98
63
75-125
19 M1
Molybdenum
mg/kg
ND
56.5
57.3
56.7
53.9
100
94
75-125
5
Nickel
mg/kg
1.3
56.5
57.3
57.1
57.2
99
98
75-125
0
Potassium
mg/kg
1530
565
573
2090
1870
100
61
75-125
11 M1
Selenium
mg/kg
ND
56.5
57.3
54.8
55.4
96
96
75-125
1
Sodium
mg/kg
ND
565
573
589
550J
99
90
75-125
Zinc
mg/kg
17.2
56.5
57.3
68.0
66.6
90
86
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 11 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563608 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2987037
Matrix:
Water
Associated Lab Samples:
92492498001, 92492498002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
09/01/2010:13 BC
Barium
mg/L
ND
0.25
09/01/2010:13
Cadmium
mg/L
ND
0.0050
09/01/2010:13
Chromium
mg/L
ND
0.050
09/01/2010:13
Lead
mg/L
ND
0.025
09/01/2010:13
Selenium
mg/L
ND
0.10
09/01/2010:13
Silver
mg/L
ND
0.025
09/01/2010:13
LABORATORY CONTROL SAMPLE:
2988247
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
1-CS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.6
106
80-120
2.5
2.5
100
80-120
2.5
2.5
98
80-120
2.5
2.4
97
80-120
2.5
2.4
96
80-120
2.5
2.6
103
80-120
1.2
1.2
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2988248
2988249
MS
MSD
92490990001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
0.021J
2.5
2.5
2.6
2.6
102
104
75-125
3
Barium
mg/L
0.101
2.5
2.5
2.6
2.6
98
99
75-125
1
Cadmium
mg/L
ND
2.5
2.5
2.5
2.5
98
100
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.4
2.4
95
98
75-125
3
Lead
mg/L
ND
2.5
2.5
2.4
2.4
96
98
75-125
1
Selenium
mg/L
0.025J
2.5
2.5
2.6
2.6
101
103
75-125
2
Silver
mg/L
ND
1.2
1.2
1.2
1.2
97
98
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 562872 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92492498001, 92492498002
SAMPLE DUPLICATE: 2984989
92492615001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.9 19.7 15
SAMPLE DUPLICATE: 2984990
92492585003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.4 97.4 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563308 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
SAMPLE DUPLICATE: 2986845
92492276001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.5 8.4 0 H3
SAMPLE DUPLICATE: 2986846
92493052001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 12.1 12.1 0 E,H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563322 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2986871 Matrix: Solid
Associated Lab Samples: 92492498001, 92492498002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 10.0 08/31/20 09:58
LABORATORY CONTROL SAMPLE: 2986872
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 500 490 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2986873 2986874
MS MSD
92491829001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 440 1060 1020 965 990 50 54 90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2986875 2986876
MS MSD
70142573001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 592 472 500 840 849 53 51 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 564495 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2992347 Matrix: Solid
Associated Lab Samples: 92492498001, 92492498002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 09/05/20 01:19
LABORATORY CONTROL SAMPLE: 2992348
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 987 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2992349 2992350
MS MSD
92492238001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 1260 2070 1550 3180 2600 93 86 90-110 20 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 562675 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2984100
Associated Lab Samples: 92492498001, 92492498002
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 08/27/20 08:02
ND 4.0 08/27/20 08:02
ND 4.0 08/27/20 08:02
Qualifiers
LABORATORY CONTROL SAMPLE: 2984101
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.5 103 90-110
Nitrogen, Nitrite mg/kg 10 10.1 101 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.6 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2984102
2984103
MS
MSD
92492498001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
ND
36.4
36.9
38.7
37.2
106
101
90-110 4
Nitrogen, Nitrite
mg/kg
ND
24.4
24.6
25.8
24.9
106
101
90-110 4
Nitrogen, NO2 plus NO3
mg/kg
ND
60.8
61.6
64.5
62.0
106
101
90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
QC Batch: 563814 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492498001, 92492498002
METHOD BLANK: 2988985 Matrix: Solid
Associated Lab Samples: 92492498001, 92492498002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.98 09/01/2018:26
LABORATORY CONTROL SAMPLE: 2988986
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 42.4 42.4 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2988987 2988988
MS MSD
92492276001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 15500 3910 3510 20700 19100 131 101 90-110 8 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALIFIERS
Project: WOOD BOILERASH 082620
Pace Project No.: 92492498
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/09/2020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WOOD BOILERASH 082620
92492498
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92492498001
NP8262020A
EPA3050B
564356
EPA 601OD
564470
92492498002
NP8262020B
EPA3050B
564356
EPA 601OD
564470
92492498001
NP8262020A
EPA 3010A
563608
EPA 601OD
563624
92492498002
NP8262020B
EPA 3010A
563608
EPA 601OD
563624
92492498001
NP8262020A
EPA 7470A
563609
EPA 7470A
563741
92492498002
NP8262020B
EPA 7470A
563609
EPA 7470A
563741
92492498001
NP8262020A
EPA 7471B
563070
EPA 7471B
563136
92492498002
NP8262020B
EPA 7471B
563070
EPA 7471B
563136
92492498001
NP8262020A
ASTM D2974-87
562872
92492498002
NP8262020B
ASTM D2974-87
562872
92492498001
NP8262020A
EPA 9045D
563308
92492498002
NP8262020B
EPA 9045D
563308
92492498001
NP8262020A
SM 271 OB-2011
565053
92492498002
NP8262020B
SM 271 OB-2011
565053
92492498001
NP8262020A
EPA 350.1 Rev 2.0
1993
563322
EPA 350.1 Rev 2.0
1993
563325
Mod.
Mod.
92492498002
NP8262020B
EPA 350.1 Rev 2.0
1993
563322
EPA 350.1 Rev 2.0
1993
563325
Mod.
Mod.
92492498001
NP8262020A
EPA 351.2 Rev 2.0
1993
564495
EPA 351.2 Rev 2.0
1993
564761
92492498002
NP8262020B
EPA 351.2 Rev 2.0
1993
564495
EPA 351.2 Rev 2.0
1993
564761
92492498001
NP8262020A
EPA 353.2 Rev 2.0
1993
562675
EPA 353.2 Rev 2.0
1993
562680
92492498002
NP8262020B
EPA 353.2 Rev 2.0
1993
562675
EPA 353.2 Rev 2.0
1993
562680
92492498001
NP8262020A
EPA 365.1 Rev 2.0
1993
563814
EPA 365.1 Rev 2.0
1993
563843
92492498002
NP8262020B
EPA 365.1 Rev 2.0
1993
563814
EPA 365.1 Rev 2.0
1993
563843
Date: 09/09/2020 08:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

Document Name:
DocumentRevised: a ruary 1,
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
I�PaCeAnalytical
F-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
Laboratory receiving sa ples:
Asheville Eden❑
Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Corfffition
W®# : 92492498
Sample Client Name:
pan Receipt
Project 4:
Courier: []Fed Ex
UPS ❑USPS -Client
❑ Commercial ❑Pace
❑Other:
92492498
Custody Seal Present? ❑Yes r❑No
Seals Intact? ❑Yes �No
J
Date/Initials Person Examining Contents:
2 •-' 0
Packing Material: ❑Bubble Wrap
❑Bubble Bags [one ❑ Other
Biological Tissue F zen?
[]Yes[]NoN/A
Thermometer:
❑ IR Gun ID: _
Type of lee: ❑Wet ❑Blue
�Non2
Cooler Temp (°C):Correction Factor: Add/Subtract (°C) /y
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): _
[]samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil { ❑ N/A, water sample)
Did samples on nate in a quarantine zone within
the United States: CA, NY, or SC (check maps)?
Did samples originate from a foreign source (internationally,
[—]NO
❑Yes VjNo
including Hawaii and Puerto Rico)? ❑Yes
Comments/Discrepancy:
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/Time/ID/Analysi
Headspace in VOA Vials (>5-5mm)
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE D15CREPANCY
[11Y.,
[]No
❑N/A
1.
Yes
[]No
❑N/A
2.
Yes
[IN.
❑N/A
3.
Oyes
QNo
❑NIA
4.
]Yes
❑No
❑N/A
5.
Yes
[]No
❑N/A
5.
[-]Yes
Igo
[-]N/A
Yes
[-]No
❑N/A
7.
❑Yes
❑No
13l/A
8.
Oes
❑No
❑N/A
9.
Dyes ❑No EP N/A 1 10.
❑Yes ❑No N/A I 11.
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Date:
Field Data Required? ❑Yes P14
Project Manager SRF Review:
Date:
Page 21 of 23

Document Name:
Document Revise February 7, 2019
"aceAnallc�1
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project * WO# : 92492498
PM: CD1 Due Date: 09/10/20
CLIENT: 92—Baxter
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pH Adjustment Log for Preserved Samples
Sample I❑
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 22 of 23

axter Biomass - Wood Boiler Ash - Ricky Styles
Ise test the sample(s) for the parameters as
d below.
i original results to: email: [e-mail]
i invoice and copy of results to: email: [e-mail]
cy Styles
irBiomass Purchase Order# 245667
Old Linville Rd.
m, NC 28752
756-6650
Sample #
Sample
Sample Date(s)
Grab or
Total Metals -
TCLP Metals
Ignitability,
pH
Total -Arsenic
Full
Moisture
BTU PER
Ammonia,
ph, TKN
Hg by
Total
Pan 1 SAR
Description
and time sample
Composite
by 6010, Al,
As, Ba, Cd,
Reactivity
Corrosivity
TCLP
Content
POUND
NitratelNitrile,
7471
Percent
Calculation
collected
As, Ba, Cd,
Cr, Pb, Hg,
Phosphorus
Solid
Ca, Cr, Cu, Fe,
Se, Ag
Pb, Mg, Mn,
Me, Ni, K, Se,
Ag, No, Zn,
total
NP8262020A
composite ash
8/2612020
composite
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
sample
8:30am
np82620206
composite ash
8126/2020
composite
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
sample
8:30am
Sample sent to: Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Custody
Project Manager. Tom Williams
9800 Kincey Avenue, Suite 10C
Huntersville, NC 28078
(704) 875 - 9092 ext. 233
�t
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co
N
O
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a_

(�Ia'ne Analytical
www.pacelabs.com
May 27, 2020
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: SOUTHPOND 051120
Pace Project No.: 92477121
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 11, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

(�Ia'cie Analytical
www.pacelabs.cem
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 20

(�Ia'cie Analytical
www.pacelabs.cem
SAMPLE ANALYTE COUNT
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92477121001 SP5112020A EPA6010D
RDT
13
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
DMN
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
92477121002 SP5112020B EPA 601 OD
IDS, RDT
13
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
DMN
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
KDF1
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

(�Ia'cie Analytical
www.pacelabs.cem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Sample: SP5112020A
Lab ID: 92477121001 Collected:
05/11/20 09:00
Received: 05/11/20 14:26 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
9450 mg/kg
186
10
05/19/20 08:43
05/24/20 11:22
7429-90-5
Arsenic
ND mg/kg
18.6
10
05/19/20 08:43
05/24/20 11:22
7440-38-2
Cadmium
2.4 mg/kg
1.9
10
05/19/20 08:43
05/24/20 11:22
7440-43-9
Calcium
98800 mg/kg
186
10
05/19/20 08:43
05/24/20 11:22
7440-70-2
Copper
52.2 mg/kg
9.3
10
05/19/20 08:43
05/24/20 11:22
7440-50-8
Lead
23.1 mg/kg
9.3
10
05/19/20 08:43
05/24/20 11:22
7439-92-1
Magnesium
11200 mg/kg
186
10
05/19/20 08:43
05/24/20 11:22
7439-95-4
Molybdenum
ND mg/kg
9.3
10
05/19/20 08:43
05/24/20 11:22
7439-98-7
Nickel
15.5 mg/kg
9.3
10
05/19/20 08:43
05/24/20 11:22
7440-02-0
Potassium
17400 mg/kg
9300
10
05/19/20 08:43
05/24/20 11:22
7440-09-7
Selenium
ND mg/kg
18.6
10
05/19/20 08:43
05/24/20 11:22
7782-49-2
Sodium
12200 mg/kg
9300
10
05/19/20 08:43
05/24/20 11:22
7440-23-5
Zinc
207 mg/kg
18.6
10
05/19/20 08:43
05/24/20 11:22
7440-66-6 B
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0055
1
05/12/2016:10
05/13/2012:37
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
57.3 %
0.10
1
05/12/20 15:29
Percent Solids
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Total Solids
42.7 %
0.10
1
05/12/20 17:02
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.0 Std. Units
0.10
1
05/18/20 13:56
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
Plant Available Nitrogen
1620 mg/kg
0.12
1
05/27/20 16:12
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg
21.7
1
05/26/20 11:48
05/26/20 14:09
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
5400 mg/kg
272
5
05/13/20 13:40
05/14/20 06:24
7727-37-9
Date: 05/27/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

(�Ia'cie Analytical
www.pacelabs.cem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Sample: SP5112020A
Lab ID: 92477121001 Collected: 05/11/20 09:00 Received: 05/11/20 14:26 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.2 1 05/12/20 11:22 05/12/20 16:24 M1
Nitrogen, Nitrate
ND mg/kg 9.2 1 05/12/20 11:22 05/12/20 16:24 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.2 1 05/12/20 11:22 05/12/20 16:24 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
3130 mg/kg 46.9 20 05/18/20 18:48 05/18/20 21:42 7723-14-0 M6, R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

(�Ia'cie Analytical
www.pacelabs.cem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Sample: SP5112020B
Lab ID: 92477121002 Collected: 05/11/20 09:00 Received: 05/11/20 14:26 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
10800 mg/kg 24.7 1 05/19/20 08:43
05/22/20 18:38
7429-90-5
Arsenic
ND mg/kg 2.5 1 05/19/20 08:43
05/22/20 18:38
7440-38-2
Cadmium
3.3 mg/kg 0.25 1 05/19/20 08:43
05/22/20 18:38
7440-43-9
Calcium
118000 mg/kg 247 10 05/19/20 08:43
05/24/20 11:25
7440-70-2
Copper
68.1 mg/kg 1.2 1 05/19/20 08:43
05/22/20 18:38
7440-50-8
Lead
23.5 mg/kg 1.2 1 05/19/20 08:43
05/22/20 18:38
7439-92-1
Magnesium
13600 mg/kg 24.7 1 05/19/20 08:43
05/22/20 18:38
7439-95-4
Molybdenum
2.5 mg/kg 1.2 1 05/19/20 08:43
05/22/20 18:38
7439-98-7
Nickel
17.5 mg/kg 1.2 1 05/19/20 08:43
05/22/20 18:38
7440-02-0
Potassium
20700 mg/kg 1240 1 05/19/20 08:43
05/22/20 18:38
7440-09-7
Selenium
ND mg/kg 2.5 1 05/19/20 08:43
05/22/20 18:38
7782-49-2
Sodium
13000 mg/kg 1240 1 05/19/20 08:43
05/24/20 11:29
7440-23-5
Zinc
235 mg/kg 2.5 1 05/19/20 08:43
05/22/20 18:38
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg 0.0054 1 05/12/2016:10
05/13/2012:39
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
61.9 % 0.10 1
05/12/20 15:29
Percent Solids
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Total Solids
38.1 % 0.10 1
05/12/20 17:02
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.0 Std. Units 0.10 1
05/18/20 13:57
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
Plant Available Nitrogen
2100 mg/kg 0.12 1
05/27/20 16:12
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 18.2 1 05/26/20 11:48
05/26/20 14:13
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
7000 mg/kg 452 5 05/13/20 13:40
05/14/20 06:25
7727-37-9
M1,R1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP5112020B Lab ID: 92477121002 Collected: 05/11/20 09:00 Received: 05/11/20 14:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 10.2 1 05/12/20 11:22 05/12/20 16:28
Nitrogen, Nitrate
ND mg/kg 10.2 1 05/12/20 11:22 05/12/20 16:28 14797-55-8
Nitrogen, Nitrite
ND mg/kg 10.2 1 05/12/20 11:22 05/12/20 16:28 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
3140 mg/kg 48.6 20 05/18/20 18:48 05/18/20 21:44 7723-14-0
Date: 05/27/2020 05:02 PM
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 541054 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2883526 Matrix: Solid
Associated Lab Samples: 92477121001, 92477121002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 05/13/2011:30
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2883527
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.087 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883528 2883529
MS MSD
92476815001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0049 0.033 0.033 0.036 0.035 96 94 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 542257
QC Batch Method: EPA 3050B
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2889245
Associated Lab Samples: 92477121001, 92477121002
Parameter Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
2889246
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA6010D
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank
Result
Spike
Cone.
500
50
50
500
50
50
500
50
50
500
50
500
50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.7
Reporting
Limit Analyzed
Qualifiers
10.0
05/22/2018:24
1.0
05/22/2018:24
0.10
05/22/2018:24
10.0
05/22/2018:24
0.50
05/22/2018:24
0.50
05/22/2018:24
10.0
05/22/2018:24
0.50
05/22/2018:24
0.50
05/22/2018:24
500
05/22/2018:24
1.0
05/22/2018:24
500
05/24/2011:07
1.0
05/22/2018:24
LCS
Result
474
46.7
46.7
465
49.3
47.0
465
49.3
47.6
503
43.6
513
43.4
LCS
% Rec
95
93
93
93
99
94
93
99
95
101
87
103
87
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Pace Analytical Services, LLC
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Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2889249
2889250
MS
MSD
92477833003 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Cone.
Cone.
Result
Result % Rec
% Rec Limits RPD Qual
Aluminum mg/kg 18900 495
503
38300
31700 3930
2550 75-125 19 E,M1
Arsenic mg/kg 1.7 49.5
50.3
43.0
42.0 84
80 75-125 3
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2889249
MS
92477833003 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
2889250
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Cadmium
mg/kg
0.094J
49.5
50.3
45.5
44.6
92
88
75-125
2
Calcium
mg/kg
21800
495
503
3730
3360
-3650
-3660
75-125
11 M1
Copper
mg/kg
47.4
49.5
50.3
117
107
140
118
75-125
9 M1
Lead
mg/kg
15.3
49.5
50.3
47.6
48.5
65
66
75-125
2 M 1
Magnesium
mg/kg
3540
495
503
3920
4120
75
115
75-125
5
Molybdenum
mg/kg
ND
49.5
50.3
36.0
36.1
72
72
75-125
0 M1
Nickel
mg/kg
12.2
49.5
50.3
64.0
59.4
105
94
75-125
7
Potassium
mg/kg
783
495
503
1050
962
54
36
75-125
9 M1
Selenium
mg/kg
2.2
49.5
50.3
40.9
39.7
78
74
75-125
3 M1
Sodium
mg/kg
ND
495
503
594
571
91
85
75-125
4
Zinc
mg/kg
45.4
49.5
50.3
103
85.3
116
79
75-125
19
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2889251
MS
92477835005 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
2889252
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
31100
487
570
22500
37100
-1760
1050
75-125
49 E,M1,R1
Arsenic
mg/kg
2.8
48.7
57
44.7
49.8
86
83
75-125
11
Cadmium
mg/kg
ND
48.7
57
47.2
53.5
97
94
75-125
13
Calcium
mg/kg
2640
487
570
1950
3290
-142
114
75-125
51 M1,R1
Copper
mg/kg
49.0
48.7
57
82.4
114
69
114
75-125
32 M1,R1
Lead
mg/kg
12.3
48.7
57
53.1
63.4
84
90
75-125
18
Magnesium
mg/kg
3350
487
570
2640
3950
-146
105
75-125
40 M1,R1
Molybdenum
mg/kg
0.35J
48.7
57
41.3
44.1
84
77
75-125
6
Nickel
mg/kg
10.3
48.7
57
52.6
66.0
87
98
75-125
23 R1
Potassium
mg/kg
1720
487
570
1500
2070
-45
61
75-125
32 M1,R1
Selenium
mg/kg
ND
48.7
57
43.1
46.7
88
81
75-125
8
Sodium
mg/kg
ND
487
570
563
664
94
98
75-125
17
Zinc
mg/kg
55.8
48.7
57
73.8
106
37
89
75-125
36 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 541058 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92477121001, 92477121002
SAMPLE DUPLICATE: 2883539
92476799001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 18.3 19.0 4
SAMPLE DUPLICATE: 2883708
92477246002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.5 18.7 9
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 541991 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92477121001, 92477121002
SAMPLE DUPLICATE: 2888138
92477516001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.4 6.3 2 D6,H3
SAMPLE DUPLICATE: 2888139
92477874004 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.5 5.9 10 D6,H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 543369 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2894109 Matrix: Solid
Associated Lab Samples: 92477121001, 92477121002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 9.3 05/26/20 14:06
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2894110
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 481 487 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2894111
2894112
MS
MSD
92477121001
Spike
Spike
MS MSD MS MSD % Rec
Parameter Units Result
Conc.
Conc.
Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND
1070
1110
1060 1100 98 99 90-110 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 541199
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2884202
Associated Lab Samples: 92477121001, 92477121002
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2884203
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 34.5 05/14/20 05:49
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
1000 963 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2884204 2884205
MS MSD
92476348001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 34700 2930 2380 39700 36000 171 55 90-110 10 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2884629 2884630
MS MSD
92477121002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 7000 1870 1810 8100 6650 59 -19 90-110 20 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 541024 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2883338
Associated Lab Samples: 92477121001, 92477121002
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 05/12/2016:22
ND 4.0 05/12/2016:22
ND 4.0 05/12/2016:22
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2883339
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9
15.3 103 90-110
Nitrogen, Nitrite
mg/kg
9.9
9.8 99 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.8
25.1 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2883340
2883341
MS
MSD
92477121001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
ND
34.2
34.9
27.5
30.1
80
86
90-110 9
Nitrogen, Nitrite
mg/kg
ND
22.7
23.2
21.1
22.7
91
96
90-110 7
Nitrogen, NO2 plus NO3
mg/kg
ND
57.2
58.1
48.6
52.9
83
89
90-110 8 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Project: SOUTHPOND 051120
Pace Project No.: 92477121
QC Batch: 542148 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92477121001, 92477121002
METHOD BLANK: 2888840 Matrix: Solid
Associated Lab Samples: 92477121001, 92477121002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.75 05/18/20 21:41
Pace Analytical Services, LLC
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LABORATORY CONTROL SAMPLE: 2888841
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 43.9 44.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888842 2888843
MS MSD
92477121001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 3130 99.3 111 1870 2810 -1280 -293 90-110 40 M6, R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALIFIERS
Project: SOUTHPOND 051120
Pace Project No.: 92477121
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
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RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SOUTHPOND 051120
92477121
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92477121001
SP5112020A
EPA 3050B
542257
EPA 601 OD
542394
92477121002
SP5112020B
EPA 3050B
542257
EPA 601 OD
542394
92477121001
SP5112020A
EPA 7471B
541054
EPA 7471B
541152
92477121002
SP5112020B
EPA 7471B
541054
EPA 7471B
541152
92477121001
SP5112020A
ASTM D2974-87
541058
92477121002
SP5112020B
ASTM D2974-87
541058
92477121001
SP5112020A
ASTM D2974-87
541347
92477121002
SP5112020B
ASTM D2974-87
541347
92477121001
SP5112020A
EPA 9045D
541991
92477121002
SP5112020B
EPA 9045D
541991
92477121001
SP5112020A
SM 271 OB-2011
543747
92477121002
SP5112020B
SM 271 OB-2011
543747
92477121001
SP5112020A
EPA 350.1 Rev 2.0
1993
543369
EPA 350.1 Rev 2.0
1993
543418
Mod.
Mod.
92477121002
SP5112020B
EPA 350.1 Rev 2.0
1993
543369
EPA 350.1 Rev 2.0
1993
543418
Mod.
Mod.
92477121001
SP5112020A
EPA 351.2 Rev 2.0
1993
541199
EPA 351.2 Rev 2.0
1993
541486
92477121002
SP5112020B
EPA 351.2 Rev 2.0
1993
541199
EPA 351.2 Rev 2.0
1993
541486
92477121001
SP5112020A
EPA 353.2 Rev 2.0
1993
541024
EPA 353.2 Rev 2.0
1993
541032
92477121002
SP5112020B
EPA 353.2 Rev 2.0
1993
541024
EPA 353.2 Rev 2.0
1993
541032
92477121001
SP5112020A
EPA 365.1 Rev 2.0
1993
542148
EPA 365.1 Rev 2.0
1993
542216
92477121002
SP5112020B
EPA 365.1 Rev 2.0
1993
542148
EPA 365.1 Rev 2.0
1993
542216
Date: 05/27/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 20

aceAnalytical M CHAIN -OF -CUSTODY Analytical Request Document
1!
.
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
Company: Baxter Biomass Billing Information:
Address: 28S9 Old Linville Rd, Marion, NC 28752
ReportTo: Ricky Styles Email To: [e-mail]
Copy To: Site Collection Info/Address:
Customer Proje Name/Number. State: County/City: Time Zone Collected:
So 0 V4 s- 1' 670 NC / [ ]PT [ ]MT [ ]CT [X]ET
Phone: [phone] Site/Facility ID #: Compliance Monitoring?
Email: [ ] Yes I ] No
Collected By (print): Purchase Order # : DW PWS ID #:
S IeS Quote #: DW Location Code:
C011 ed y sign ture): Turnaround Date Required: Immediately Packed on Ice:
L'&Wess44 [ ] Yes [ ] No
Sample Disposal: Rush: Field Filtered fit applicable):
[ ] Dispose as appropriate [ ] Return [ ] Same Day [ ] Next Day [ ] Yes ( ] No
[ ] Archive: [ ] 2 Day [ 13 Day [ ] 4 Day [ 15 Day
'I ] Hold: (Expedite Charges Apply) Analysis:
" Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (8), Vapor (V), Other (OT)
Comp / Collected (or Res # of
Composite End
Customer Sample ID Matrix • Grab Composite Start) Cl Ctns
Date Time Date Time
� �'fl 2oZD
Customer Remarks / Special Conditions / Possible Hazards: (Type of Ice Used: �Wgt Blue Dry None
(Packing Material Used:
Radchem sample(s) screened (<500 cpm): Y N 7
(Signature)
uished by/Company: (Signature) Date/Time:
(Sign
Relinquished by/Company: (Signature) Date/Time: lReceived by/Company: (Signature)
LAOUSE 0 WO# = 92477121
92477121
Container Preservative Type "" I Lab Project Manager:
aber or
—Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (S) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Analyses
Lab Profile/Une:
Lab Sample Receipt Checklist:
-Z3
Custody Seals Present/Intact Y NA
In
Custody Signatures Present Y I NA
J
`
Collector Signature Present N NA
O
Bottles Intact N NA
15
ClCorrect
Battles N NA
V
to
Sufficient Volume N NA
Ui
Samples Received on Ice Y yY NA
Q N
VOA - Headspace Acceptable Y N >in
fU
aj
USDA Regulated Soils Y V NA
QC/�
'=
=
O
Sample* in Ho Lding Time �N NA
4
Residual Chlorine Present Y N N,<
r0
Z
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C1 Strips:
Sample Acceptable Y N XA
Imo+,_
rn
co
pH
pH Strips:
C
U
Sulfide Present Y N biK
N
O O
Z
tti
~
QS
Lead Acetate Strips:
-�
X
CDLAB
USE ONLY:
�I
0
�'
Z
Lab Sample++II# / Comments:
SHORT HOLDS PRESENT (<72 hours) : Y' N N/A
Lab Tracking #:
Samples received via:
FEDER UPS affent Courier Pace Courier
Date/Tim-7/1e: f�
�F1/rG 0 7 Z(
MTJL LAB USE ONLY
Table #:
Date/Time:
Acctnum:
Template:
Prelogin:
PM:
Date/Time:
PB:
LAB Sample Temperature Info:
Temp Blank Received: Y 1K NA
Therm ID#: 7-0 L
Cooler 1 Temp Upen Receipt: _ 6+
Cooler 1 Therm Corr. Eactorp;;:—OC
Cooler 1 Corrected Temp:
Comments:
Trip Blank Received: Y-N NA
HCL McOH TSP Other
Nan Conformance(s): Page:
YES / f4d of: _

Document Name:
Document Revised: February 7, 2018
ceAnapICBl
Sample Condition Upon Receipt(SOUR)
Page 1 of 2
Document No.:
Issuing Authority!
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coiiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
W4#:92477121
PM: CRl Due Date: 05/26/20
CLIENT: 82-Baxter
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Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Caroina compliance samples, a copy of this form will be sentto the Borth Carolina DEHNR Certification utnce ti,e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 20 of 20

(�Ia'ne Analytical
www.pacelabs.com
April 09, 2020
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 25, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
Revised Report: Report revised to add missing element Mg
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92470925001 NP 03242020 A EPA 601 OD
RDT
13
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
DMN
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
92470925002 NP 03242020 B EPA 601OD
RDT
13
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
DMN
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Sample: NP 03242020 A
Lab ID: 92470925001 Collected:
03/24/20 15:00
Received: 03/25/20 11:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
7490 mg/kg
24.2
1
03/29/20 09:37
03/29/20 20:37
7429-90-5
Arsenic
ND mg/kg
2.4
1
03/29/20 09:37
03/29/20 20:37
7440-38-2
Cadmium
2.3 mg/kg
0.24
1
03/29/20 09:37
03/29/20 20:37
7440-43-9
Calcium
87300 mg/kg
121
5
03/29/20 09:37
03/30/20 12:46
7440-70-2
Copper
60.8 mg/kg
1.2
1
03/29/20 09:37
03/29/20 20:37
7440-50-8
Lead
16.3 mg/kg
1.2
1
03/29/20 09:37
03/29/20 20:37
7439-92-1
Magnesium
9980 mg/kg
24.2
1
03/29/20 09:37
03/29/20 20:37
7439-95-4
Molybdenum
ND mg/kg
1.2
1
03/29/20 09:37
03/29/20 20:37
7439-98-7 BC
Nickel
13.5 mg/kg
1.2
1
03/29/20 09:37
03/29/20 20:37
7440-02-0
Potassium
12600 mg/kg
1210
1
03/29/20 09:37
03/29/20 20:37
7440-09-7
Selenium
ND mg/kg
2.4
1
03/29/20 09:37
03/29/20 20:37
7782-49-2
Sodium
9120 mg/kg
1210
1
03/29/20 09:37
03/29/20 20:37
7440-23-5
Zinc
173 mg/kg
2.4
1
03/29/20 09:37
03/29/20 20:37
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0055
1
03/30/2013:08
03/30/2016:51
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
62.4 %
0.10
1
03/26/20 18:20
Percent Solids
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Total Solids
37.6 %
0.10
1
03/26/20 18:27
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
8.9 Std. Units
0.10
1
03/30/20 14:58
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
Plant Available Nitrogen
927 mg/kg
0.12
1
04/06/20 10:27
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg
25.6
1
04/02/20 13:44
04/04/20 15:05
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
3090 mg/kg
98.6
1
04/02/20 15:45
04/03/20 07:54
7727-37-9
Date: 04/09/2020 10:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Sample: NP 03242020 A
Lab ID: 92470925001 Collected: 03/24/20 15:00 Received: 03/25/20 11:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.2 1 03/25/20 21:58 03/26/20 00:55
Nitrogen, Nitrate
ND mg/kg 9.2 1 03/25/20 21:58 03/26/20 00:55 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.2 1 03/25/20 21:58 03/26/20 00:55 14797-65-0 R1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
3130 mg/kg 51.2 20 03/25/20 19:03 03/26/20 21:28 7723-14-0
Date: 04/09/2020 10:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Sample: NP 03242020 B
Lab ID: 92470925002 Collected:
03/24/20 15:00
Received: 03/25/20 11:54 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
7250 mg/kg
15.5
1
03/29/20 09:37
03/29/20 20:40
7429-90-5
Arsenic
ND mg/kg
1.6
1
03/29/20 09:37
03/29/20 20:40
7440-38-2
Cadmium
2.4 mg/kg
0.16
1
03/29/20 09:37
03/29/20 20:40
7440-43-9
Calcium
93000 mg/kg
155
10
03/29/20 09:37
03/30/20 15:11
7440-70-2
Copper
61.9 mg/kg
0.78
1
03/29/20 09:37
03/29/20 20:40
7440-50-8
Lead
17.1 mg/kg
0.78
1
03/29/20 09:37
03/29/20 20:40
7439-92-1
Magnesium
10100 mg/kg
15.5
1
03/29/20 09:37
03/29/20 20:40
7439-95-4
Molybdenum
1.4 mg/kg
0.78
1
03/29/20 09:37
03/29/20 20:40
7439-98-7 BC
Nickel
12.9 mg/kg
0.78
1
03/29/20 09:37
03/29/20 20:40
7440-02-0
Potassium
14600 mg/kg
777
1
03/29/20 09:37
03/29/20 20:40
7440-09-7
Selenium
ND mg/kg
1.6
1
03/29/20 09:37
03/29/20 20:40
7782-49-2
Sodium
11200 mg/kg
777
1
03/29/20 09:37
03/29/20 20:40
7440-23-5
Zinc
172 mg/kg
1.6
1
03/29/20 09:37
03/29/20 20:40
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method:
EPA 7471 B
Pace Analytical Services - Asheville
Mercury
ND mg/kg
0.0047
1
03/30/2013:08
03/30/2016:53
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
61.7 %
0.10
1
03/26/20 18:21
Percent Solids
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Total Solids
38.3 %
0.10
1
03/26/20 18:27
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.2 Std. Units
0.10
1
03/30/20 15:00
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Pace Analytical Services - Asheville
Plant Available Nitrogen
1060 mg/kg
0.12
1
04/06/20 10:27
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg
24.2
1
04/02/20 13:44
04/04/20 15:09
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
3520 mg/kg
113
1
04/02/20 15:45
04/03/20 07:55
7727-37-9
Date: 04/09/2020 10:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
Sample: NP 03242020 B Lab ID: 92470925002 Collected: 03/24/20 15:00 Received: 03/25/20 11:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 10.1 1 03/25/20 21:58 03/26/20 01:01
Nitrogen, Nitrate ND mg/kg 10.1 1 03/25/20 21:58 03/26/20 01:01 14797-55-8
Nitrogen, Nitrite ND mg/kg 10.1 1 03/25/20 21:58 03/26/20 01:01 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus 3140 mg/kg 52.2 20 03/25/20 19:03 03/26/20 21:29 7723-14-0
Date: 04/09/2020 10:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 533211 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2846196 Matrix: Solid
Associated Lab Samples: 92470925001, 92470925002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 03/30/2015:40
LABORATORY CONTROL SAMPLE: 2846197
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.082 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2846198 2846199
MS MSD
92470840005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0039 0.033 0.033 0.040 0.048 110 134 75-125 18 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 533129 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2845972
Associated Lab Samples: 92470925001, 92470925002
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
03/29/20 20:01
Arsenic
mg/kg
ND
1.0
03/29/20 20:01
Cadmium
mg/kg
ND
0.10
03/29/20 20:01
Calcium
mg/kg
ND
10.0
03/29/20 20:01
Copper
mg/kg
ND
0.50
03/29/20 20:01
Lead
mg/kg
ND
0.50
03/29/20 20:01
Magnesium
mg/kg
ND
10.0
03/29/20 20:01
Molybdenum
mg/kg
ND
0.50
03/29/2016:59 BC
Nickel
mg/kg
ND
0.50
03/29/20 20:01
Potassium
mg/kg
ND
500
03/29/20 20:01
Selenium
mg/kg
ND
1.0
03/29/20 20:01
Sodium
mg/kg
ND
500
03/29/20 20:01
Zinc
mg/kg
ND
1.0
03/29/20 20:01
LABORATORY CONTROL SAMPLE:
Parameter
2845973
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
477
95
80-120
Arsenic
mg/kg
50
46.7
93
80-120
Cadmium
mg/kg
50
47.7
95
80-120
Calcium
mg/kg
500
473
95
80-120
Copper
mg/kg
50
50.2
100
80-120
Lead
mg/kg
50
48.6
97
80-120
Magnesium
mg/kg
500
452
90
80-120
Molybdenum
mg/kg
50
46.0
92
80-120
Nickel
mg/kg
50
49.3
99
80-120
Potassium
mg/kg
500
ND
95
80-120
Selenium
mg/kg
50
45.0
90
80-120
Sodium
mg/kg
500
480J
96
80-120
Zinc
mg/kg
50
47.1
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2845974
2845975
MS
MSD
92470181001 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Cone.
Cone.
Result
Result % Rec
% Rec Limits RPD Qual
Aluminum mg/kg 16600 437
437
23300
22700 1550
1420 75-125 3 M1
Arsenic mg/kg 7.7 43.7
43.7
43.5
43.0 82
81 75-125 1
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/09/2020 10:49 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

aceAnalytical
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2845974
2845975
MS
MSD
92470181001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
mg/kg
0.22
43.7
43.7
38.0
37.8
87
86
75-125
1
Calcium
mg/kg
560
437
437
1020
935
105
86
75-125
9
Copper
mg/kg
14.3
43.7
43.7
56.1
55.3
96
94
75-125
1
Lead
mg/kg
33.8
43.7
43.7
71.9
69.3
87
81
75-125
4
Magnesium
mg/kg
794
437
437
1240
1250
103
104
75-125
0
Molybdenum
mg/kg
0.45
43.7
43.7
33.2
33.2
75
75
75-125
0
Nickel
mg/kg
8.7
43.7
43.7
47.5
47.3
89
89
75-125
0
Potassium
mg/kg
746
437
437
1170
1180
97
99
75-125
1
Selenium
mg/kg
ND
43.7
43.7
34.1
32.8
78
75
75-125
4
Sodium
mg/kg
ND
437
437
395J
393J
88
87
75-125
Zinc
mg/kg
44.1
43.7
43.7
88.4
86.1
101
96
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 532768 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92470925001, 92470925002
SAMPLE DUPLICATE: 2843694
92470802002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 22.8 21.1 8
SAMPLE DUPLICATE: 2843695
92471037002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 95.1 95.1 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 533115 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
SAMPLE DUPLICATE: 2845927
92470434001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.7 6.7 0 H3
SAMPLE DUPLICATE: 2845928
92470925001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.9 9.0 1 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 533973 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2849823 Matrix: Solid
Associated Lab Samples: 92470925001, 92470925002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.9 04/04/20 15:02
LABORATORY CONTROL SAMPLE: 2849824
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 490 519 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2849825 2849826
MS MSD
92470925001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 1300 1280 1340 1290 102 100 90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 533910 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2849719 Matrix: Solid
Associated Lab Samples: 92470925001, 92470925002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 04/03/20 07:44
LABORATORY CONTROL SAMPLE: 2849720
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 1060 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2849721 2849722
MS MSD
92470496002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 19200 1110 980 25000 21100 527 195 90-110 17 M6, R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 532553 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2842951
Associated Lab Samples:
92470925001, 92470925002
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 3.9 03/26/20 00:49
ND 3.9 03/26/20 00:49
ND 3.9 03/26/20 00:49
Qualifiers
LABORATORY CONTROL SAMPLE:
2842952
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9
14.9 100 90-110
Nitrogen, Nitrite
mg/kg
10
10.0 101 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.9
24.9 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2842953
2842954
MS
MSD
92470925001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
39.9
37.3
40.0
36.3
100
97
90-110
10
Nitrogen, Nitrite
mg/kg
ND
26.6
24.8
27.9
24.9
104
100
90-110
11 R1
Nitrogen, NO2 plus NO3
mg/kg
ND
66.5
62
67.9
61.2
100
97
90-110
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/09/2020 10:49 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
QC Batch: 532485 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92470925001, 92470925002
METHOD BLANK: 2842480 Matrix: Solid
Associated Lab Samples: 92470925001, 92470925002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.91 03/26/20 21:25
LABORATORY CONTROL SAMPLE: 2842481
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 39.1 40.3 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2842482 2842483
MS MSD
92470730001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 161 87.6 87.6 252 268 104 122 90-110 6 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: NORTH POND 3-24-2020
Pace Project No.: 92470925
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NORTH POND 3-24-2020
92470925
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92470925001
NP 03242020 A
EPA 3050B
533129
EPA 601 OD
533154
92470925002
NP 03242020 B
EPA 3050B
533129
EPA 601 OD
533154
92470925001
NP 03242020 A
EPA 7471 B
533211
EPA 7471 B
533262
92470925002
NP 03242020 B
EPA 7471 B
533211
EPA 7471 B
533262
92470925001
NP 03242020 A
ASTM D2974-87
532768
92470925002
NP 03242020 B
ASTM D2974-87
532768
92470925001
NP 03242020 A
ASTM D2974-87
532993
92470925002
NP 03242020 B
ASTM D2974-87
532993
92470925001
NP 03242020 A
EPA 9045D
533115
92470925002
NP 03242020 B
EPA 9045D
533115
92470925001
NP 03242020 A
SM 271 OB-2011
534531
92470925002
NP 03242020 B
SM 271 OB-2011
534531
92470925001
NP 03242020 A
EPA 350.1 Rev 2.0
1993
533973
EPA 350.1 Rev 2.0
1993
534088
Mod.
Mod.
92470925002
NP 03242020 B
EPA 350.1 Rev 2.0
1993
533973
EPA 350.1 Rev 2.0
1993
534088
Mod.
Mod.
92470925001
NP 03242020 A
EPA 351.2 Rev 2.0
1993
533910
EPA 351.2 Rev 2.0
1993
534207
92470925002
NP 03242020 B
EPA 351.2 Rev 2.0
1993
533910
EPA 351.2 Rev 2.0
1993
534207
92470925001
NP 03242020 A
EPA 353.2 Rev 2.0
1993
532553
EPA 353.2 Rev 2.0
1993
532563
92470925002
NP 03242020 B
EPA 353.2 Rev 2.0
1993
532553
EPA 353.2 Rev 2.0
1993
532563
92470925001
NP 03242020 A
EPA 365.1 Rev 2.0
1993
532485
EPA 365.1 Rev 2.0
1993
532802
92470925002
NP 03242020 B
EPA 365.1 Rev 2.0
1993
532485
EPA 365.1 Rev 2.0
1993
532802
Date: 04/09/2020 10:49 PM
REPORT OF LABORATORY ANALYSIS
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Page 18 of 19

CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical y
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
LAB USE ONLY- Affix Workorder/Login Labe[ Here or List Pace Workorder Number or
W0# : 92470925 6
l ll l I I II rn
Al
Container P 9247092S
Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (a) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (6) ammonium sulfate,
(C) ammonium hydroxide, (D) T5P, (Ul Unpreserved, (0) Other
Company: Baxter Biomass
Billing Information:
Address: 2859 Old Linville Rd, Marion, NC 28752
Report To: Ricky Styles
Email To: [e-mail]
Copy TO:
Site Collection Info/Address:
Analyses
Lab Profile/Line:
Customer Project Name/Number:
¢,L ?evd 3- 7-9-0.42C 1
State: County/City: Time Zone Collected:
NC / [ ]PT [ ]MT [ ]CT [X]ET
=
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7+
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tB
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N
U
Z
a
Lab Sample Receipt Checklist:
Custody Seals Present/Intact Y NA
Signatures Present Y NA
Collector Signature Present N NA
Bottles Intact N NA
Correct Bottles N NA
sufficient volume N NA
Samples Received on ice Y 9DiJA
VOA - Headspace Acceptable �Yt N
USDA Regulated Soils VV N NA
Samplea in Holding Time � N NA
Residual Chlorine Present r N<T�
Cl Strips:
Sample pH Acceptable Y N
pH Strips:
Sulfide Present Y N A
Lead Acetate Strips:
LAB USE ONLY:
Lab Sample 9 / Comments:
q
12I
Phone:[phone]
Email:
Site/Facility ID #:
Compliance Monitoring?
[ ]Yes [ ]No
Collected By (print[:
Purchase Order #: •33 37
Quote N:
DW PWS ID #:
DW Location Code:
Collected y lsig atu ):
Turnaround Date Required:
.� 3 -- ZDZ 0
Immediately Packed on Ice:
[ ] Yes [ ] No
Sample Disposal.
[ ] Dispose as appropriate [ ] Return
[ ] Archive:
[ 1 Hold:
Rush:
[ ] Same Day [ ] Next Day
[ ] 2 Day [ ] 3 Day [ 14 Day [ ] 5 Day
(Expedite Charges Apply)
Field Filtered {if applicable):
[ ] Yes [ ] No
Analysis:
Matrix Codes (Insert in Matrix box below): Drinking Water [DW), Ground Water (GW), Wastewater (WW),
Product {P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample 10
Matrix "
Comp /
Grab
Collected (or
Composite Start[
Composite End
Res
CI
# of
Ctns
Date
Time
Date
Time
NPc:3., i2020
3Z ar
3P .1
y
-oc�!
rVP ��Zy z��c i3
P
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--b�
Customer Remarks / Special Conditions / Possible Hazards:
Type of Ice Used: Wet Blue Dry N
SHORT HOLDS PRESENT (<72 hours) : Y N N/A
LAB Sample Temperature Info:
Temp Blank Received: Y � NA
Therm IDH : f 0"'43 v
Cooler 1 Temp Upon Receipt: Ioc
Cooler 1 Therm Corr. Factor:-- oC
Cooler 1 Corrected Temp: 2f. oC
Comments-
Packing Material Used: ✓
tab Tracking #:
Radchem sample(s) screened (<500 cpm): Y N NA`
Samples received via:
FEDEX UPS lie Courier Pace Courier
Re'nquishe by A y: (S gnature
Date/Time: 1l j 3 f
J� 25/�
Received by/Company: (Signature)
l✓i� �� ��
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 18, 2020
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on February 28, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Revised Report: Report revised to add Magnesium result
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
TNI
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Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Pace Analytical Services Montana
150 N. 9th Street, Billings, MT 59101
A2LA Certification: # 3590.01
EPA Region 8 Certification #: 8TMS-L
Idaho Certification #: MT00012
Minnesota Dept of Health Certification #: 030-999-442
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
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CERTIFICATIONS
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REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
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SAMPLE ANALYTE COUNT
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92467333001 SP2272020A EPA6010D
SH1
13
PASI-A
EPA 7471 B
SOO
1
PASI-A
EPA 6010B
EJS
4
PASI-MT
ASTM D2974-87
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
KDF1
1
PASI-A
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Sample: SP2272020A
Lab ID: 92467333001 Collected:
02/27/20 11:45
Received: 02/28/20 14:09 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Aluminum
12000 mg/kg
22.6
1
03/09/20 09:25
03/12/20 20:55
7429-90-5
Arsenic
2.6 mg/kg
2.3
1
03/09/20 09:25
03/12/20 20:55
7440-38-2
Cadmium
2.0 mg/kg
0.23
1
03/09/20 09:25
03/12/20 20:55
7440-43-9
Calcium
81300 mg/kg
113
5
03/09/20 09:25
03/13/20 13:18
7440-70-2
Copper
53.7 mg/kg
1.1
1
03/09/20 09:25
03/12/20 20:55
7440-50-8
Lead
18.0 mg/kg
1.1
1
03/09/20 09:25
03/12/20 20:55
7439-92-1
Magnesium
11000 mg/kg
22.6
1
03/09/20 09:25
03/12/20 20:55
7439-95-4
Molybdenum
1.4 mg/kg
1.1
1
03/09/20 09:25
03/12/20 20:55
7439-98-7
Nickel
14.7 mg/kg
1.1
1
03/09/20 09:25
03/12/20 20:55
7440-02-0
Potassium
17400 mg/kg
1130
1
03/09/20 09:25
03/13/20 13:56
7440-09-7
Selenium
ND mg/kg
2.3
1
03/09/20 09:25
03/12/20 20:55
7782-49-2
Sodium
13600 mg/kg
1130
1
03/09/20 09:25
03/13/20 13:56
7440-23-5
Zinc
167 mg/kg
2.3
1
03/09/20 09:25
03/12/20 20:55
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method:
EPA 7471 B
Mercury
ND mg/kg
0.0045
1
03/10/2013:49
03/11/2018:35
7439-97-6
SAR 6010B / ASA 10.3.2.1
Analytical Method: EPA 6010B
Calcium saturated paste
ND meq/L
1.0
20
03/10/20 12:51
7440-70-2
AL, N2
Magnesium saturated paste
10.0 meq/L
1.6
20
03/10/20 12:51
7439-95-4
AL, N2
Sodium Adsorption Ratio
46.5
0.20
20
03/10/20 12:51
AL, N2
Sodium saturated paste
106 meq/L
0.86
20
03/10/20 12:51
7440-23-5
AL, N2
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
59.1 %
0.10
1
03/02/20 15:12
Percent Solids
Analytical Method: ASTM D2974-87
Total Solids
40.9 %
0.10
1
03/02/20 15:21
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
8.6 Std. Units
0.10
1
03/02/20 15:53
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Plant Available Nitrogen
1400 mg/kg
0.12
1
03/12/20 12:11
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
ND mg/kg
19.7
1
03/09/20 09:36
03/11/20 13:19
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
4650 mg/kg
382
5
03/09/20 09:15
03/10/20 04:34
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mg/kg
9.6
1
02/28/20 22:14
02/29/20 01:53
Nitrogen, Nitrate
ND mg/kg
9.6
1
02/28/20 22:14
02/29/20 01:53
14797-55-8
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP2272020A Lab ID: 92467333001 Collected: 02/27/20 11:45 Received: 02/28/20 14:09 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrite ND mg/kg 9.6 1 02/28/20 22:14 02/29/20 01:53 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus 1730 mg/kg 21.1 10 03/04/2010:18 03/04/2014:03 7723-14-0
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 529229
Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92467333001
METHOD BLANK: 2826551
Matrix: Solid
Associated Lab Samples: 92467333001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060
03/11/2017:45
LABORATORY CONTROL SAMPLE: 2826552
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.083 0.088
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2826553 2826554
MS MSD
92467158001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND
0.047 0.047 0.049
0.056 104 118 75-125 13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 529214 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92467333001
METHOD BLANK: 2826492
Associated Lab Samples: 92467333001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
03/12/20 20:37
Arsenic
mg/kg
ND
1.0
03/12/20 20:37
Cadmium
mg/kg
ND
0.10
03/12/20 20:37
Calcium
mg/kg
ND
10.0
03/12/20 20:37
Copper
mg/kg
ND
0.50
03/12/20 20:37
Lead
mg/kg
ND
0.50
03/12/20 20:37
Magnesium
mg/kg
ND
10.0
03/12/20 20:37
Molybdenum
mg/kg
ND
0.50
03/12/20 20:37
Nickel
mg/kg
ND
0.50
03/12/20 20:37
Potassium
mg/kg
ND
500
03/13/2013:30
Selenium
mg/kg
ND
1.0
03/12/20 20:37
Sodium
mg/kg
ND
500
03/13/2013:30
Zinc
mg/kg
ND
1.0
03/12/20 20:37
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2826493
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
506
101
80-120
Arsenic
mg/kg
50
45.6
91
80-120
Cadmium
mg/kg
50
48.2
96
80-120
Calcium
mg/kg
500
502
100
80-120
Copper
mg/kg
50
51.2
102
80-120
Lead
mg/kg
50
49.5
99
80-120
Magnesium
mg/kg
500
480
96
80-120
Molybdenum
mg/kg
50
47.4
95
80-120
Nickel
mg/kg
50
50.2
100
80-120
Potassium
mg/kg
500
ND
97
80-120
Selenium
mg/kg
50
44.0
88
80-120
Sodium
mg/kg
500
489J
98
80-120
Zinc
mg/kg
50
47.3
95
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2826494
2826495
MS
MSD
92467277001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Aluminum mg/kg
12100
7930
7930
22900
22400
137
131
75-125 2 M1
Arsenic mg/kg
ND
793
793
762
720
95
89
75-125 6
Cadmium mg/kg
1.7
793
793
783
742
99
93
75-125 5
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2826494
2826495
MS
MSD
92467277001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
110000
7930
7930
122000
122000
162
160
75-125
0 M1
Copper
mg/kg
185
793
793
1040
993
109
102
75-125
5
Lead
mg/kg
10.4
793
793
809
768
101
96
75-125
5
Magnesium
mg/kg
4270
7930
7930
12500
12100
104
99
75-125
3
Molybdenum
mg/kg
ND
793
793
781
739
98
93
75-125
6
Nickel
mg/kg
9.5
793
793
817
770
102
96
75-125
6
Potassium
mg/kg
ND
7930
7930
13100
12900
107
104
75-125
2
Selenium
mg/kg
ND
793
793
720
695
91
88
75-125
3
Sodium
mg/kg
ND
7930
7930
9990
9510
107
101
75-125
5
Zinc
mg/kg
643
793
793
1440
1400
100
95
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 664221
Analysis Method:
EPA6010B
QC Batch Method: EPA 6010B
Analysis Description:
Sodium Adsorption Ratio, SAR
Associated Lab Samples: 92467333001
METHOD BLANK: 3562891
Matrix:
Solid
Associated Lab Samples: 92467333001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Calcium saturated paste
meq/L
ND
0.50
03/10/20 12:25 AL,N2
Magnesium saturated paste
meq/L
ND
0.82
03/10/20 12:25 AL,N2
Sodium saturated paste
meq/L
ND
0.43
03/10/20 12:25 AL,N2
LABORATORY CONTROL SAMPLE: 3562892
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Calcium saturated paste
meq/L
20.6
20.2
98 77-123 AL, N2
Magnesium saturated paste
meq/L
15.6
15.8
101 62-138 AL,N2
Sodium Adsorption Ratio
4
3.7
93 87-114 AL,N2
Sodium saturated paste
meq/L
17.2
15.7
92 75-125 AL, N2
SAMPLE DUPLICATE: 3562894
10510201003
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Calcium saturated paste
meq/L
3.2
3.4
5 AL,N2
Magnesium saturated paste
meq/L
10
11.0
10 AL,N2
Sodium Adsorption Ratio
3.8
3.9
4 AL,N2
Sodium saturated paste
meq/L
9.7
10.6
9 AL,N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 528016 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92467333001
SAMPLE DUPLICATE: 2820772
92467337001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 15.3 15.2 0
SAMPLE DUPLICATE: 2820773
92467448010 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.1 17.5 9
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 527855 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92467333001
SAMPLE DUPLICATE: 2820091
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2820092
Parameter
pH at 25 Degrees C
92465991005 Dup
Units Result Result RPD Qualifiers
Std. Units 5.0 5.0 0 H3
92465944002 Dup
Units Result Result RPD Qualifiers
Std. Units 3.9 3.9 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 529206
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92467333001
METHOD BLANK: 2826474
Matrix: Solid
Associated Lab Samples: 92467333001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 9.6
03/11/20 13:11
LABORATORY CONTROL SAMPLE: 2826475
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg
472
482
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2826476
2826477
MS
MSD
92467300004
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/kg 627
1180
1320 1790
2000 99 104
90-110 11 R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2826478
2826479
MS
MSD
92467333001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Ammonia mg/kg ND
1200
1170 1200
1130 100 96
90-110 6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 529107
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Associated Lab Samples: 92467333001
METHOD BLANK: 2826242
Matrix: Solid
Associated Lab Samples: 92467333001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0
03/10/20 04:02
LABORATORY CONTROL SAMPLE: 2826243
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000 1020
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2826244 2826245
MS MSD
2629595001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 33900
833 866 20100
36200 -1660 270 90-110 57 M6, R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2020 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

(�Ia'cie Analytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 527782
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92467333001
METHOD BLANK: 2819807
Matrix: Solid
Associated Lab Samples: 92467333001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 4.0
02/29/20 01:50
Nitrogen, Nitrite
mg/kg
ND 4.0
02/29/20 01:50
Nitrogen, NO2 plus NO3
mg/kg
ND 4.0
02/29/20 01:50
LABORATORY CONTROL SAMPLE: 2819808
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
15 15.1
101 90-110
Nitrogen, Nitrite
mg/kg
10 10.4
104 90-110
Nitrogen, NO2 plus NO3
mg/kg
25 25.5
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2819809 2819810
MS MSD
92467333001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/kg
ND
35.7 36.1 38.2
37.8 107 105
90-110 1
Nitrogen, Nitrite mg/kg
ND
23.7 24.2 26.1
26.3 109 109
90-110 1
Nitrogen, NO2 plus NO3 mg/kg
ND
59.6 60.3 64.3
64.0 105 104
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2020 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 19

(�Ia'cie Analytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
QC Batch: 528191
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92467333001
METHOD BLANK: 2821467
Matrix: Solid
Associated Lab Samples: 92467333001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Phosphorus mg/kg
ND 1.0
03/04/2013:25
LABORATORY CONTROL SAMPLE: 2821468
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits
Qualifiers
Phosphorus mg/kg
50
50.2
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2821469
2821470
MS
MSD
92466575001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits RPD Qual
Phosphorus mg/kg 75.5
87.3
94 223
231 169
165
90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2821471
2821472
MS
MSD
92466656001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits RPD Qual
Phosphorus mg/kg 10.5
45.6
49.1 50.4
53.2 88
87
90-110 5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2020 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 19

(�Ia'cie Analytical
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QUALIFIERS
Project: Baxter Biomass 2/27
Pace Project No.: 92467333
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-MT Pace Analytical Services - Montana
ANALYTE QUALIFIERS
AL The lab does not hold A2LA accreditation for this parameter.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/18/2020 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 19

(�Ia'cie Analytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Baxter Biomass 2/27
92467333
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92467333001
SP2272020A
EPA 3050B
529214
EPA 6010D
529325
92467333001
SP2272020A
EPA 7471B
529229
EPA 7471B
529569
92467333001
SP2272020A
EPA 6010B
664221
92467333001
SP2272020A
ASTM D2974-87
528016
92467333001
SP2272020A
ASTM D2974-87
527967
92467333001
SP2272020A
EPA 9045D
527855
92467333001
SP2272020A
SM 2710B-2011
530116
92467333001
SP2272020A
EPA 350.1 Rev 2.0
1993
529206
EPA 350.1 Rev 2.0
1993
529259
Mod.
Mod.
92467333001
SP2272020A
EPA 351.2 Rev 2.0
1993
529107
EPA 351.2 Rev 2.0
1993
529413
92467333001
SP2272020A
EPA 353.2 Rev 2.0
1993
527782
EPA 353.2 Rev 2.0
1993
527783
92467333001
SP2272020A
EPA 365.1 Rev 2.0
1993
528191
EPA 365.1 Rev 2.0
1993
528426
Date: 03/18/2020 04:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 19

I __. aceAnalyticaly CHAIN -OF -CUSTODY Analytical Request Document
Chain -of -Custody is a LEGAL DOCUMENT -Complete all releventfields
Company: Baxter Biomass Billing Information:
Address: 2859 Old Linville Rd, Marion, NC 28752
ReportTo: Ricky Styles Email To: [e-mail]
Copy To: Site Collection Info/Address:
Customer Project Name/Number: State: County/City: Time Zone Collected:
NC / [ ]PT [ )MT [ ]'
Phone: 828-7S6-6650 Site/Facility ID 9: Compliance Monitoring?
Email: [ ] Yes [ ] No
Collected By (print): Purchase Order # : DW PWS ID #:
I,, t s dry Quote #: DW Location Code:
Collected By {signature): Turnaround Date Required: Immediately Packed on Ice:
[ I Yes [ ]NO
Sample Disposal: Rush: Field Filtered (if applicable):
[ I Dispose as appropriate [ ] Return [ ] Same Day [ ) Next Day [ ] Yes [ ] No
[ ] Archive: [ ] 2 Day [ ] 3 Day [ ] 4 Day [ ) 5 Day
[ ] Hold: (Expedite Charges Apply) Analysis:
' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP], Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
ET
Comp / Collected (or Composite End Res # of
Customer Sample ID Matrix " Grab Composite Start) C1 Ctns
Date Time Date Time
P.1-)- TV2D R SL Cc-ap �-27-0 ,►:jc.Q 1-27'zc ,r:z✓5+�
Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: Wet Blue Dry 2n
Packing Material Used: I
WO## : 92467333 rrderNumber or
1111111111111111111111
92467333 NLY
Container Preservative Type *" [ Lao rrultLi. manager:
•" Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (lJ) Unpreserved, (0) Other
Analyses
Lab Profile/Line:
Lab Sample Receipt Checklist:
Custody Seals Present/intact Y [�
J
Custody Signatures Present Y t
@
`
Collector Signature Present N
°
Bottles Intact N
t7
OL
Correct Bottles N
J
rn
Sufficient Volume
uj C
=
Samples Received on Ice Y �N
Q N
11
VOA — Headspace Acceptable
(D
Q U)
USDA Regulated Soils
N
p
�.
Samples in Holding Time Y
Residual Chlorine Present Y N
Z
Z
-
C1 Strips:
CED y
2
p
U
Sample PH Acceptable Y N
7. _
CI)
pff Strips:
.0 Z
C
t,
Sulfide Present Y
iU
Of
Lead Acetate Strips:
ti
V
Q
C
I, -a
fn
LAB USE ONLY:
d
0
L
Z
Lab Sample # / Comments:
°CL21
Q
CL
X
M
�� i673
SHORT HOLDS PRESENT (<72 hours) : Y ('N1 N/A
Lab Tracking Tracking #:
Samples received via:
Radchem sample(s) screened (<500 rpm): Y N A FEDEX UPS Client Courier Pace Courier
Datefrime: JR7ed by/ ompa y: (Signature) Date/Time:MTJL LAB USE ONLY
Table #:
Date/Time: ! Received by/Company: (Signature) Date/Time: Acctnum:
Prelogin:
Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM:
PB:
LAB Sample Temperature Info:
Temp Blank Received: Y1
Therm ID#: 13 �i
Cooler 1 Temp Upon Receipt:
Cooler 1 Therm Corr. Factor
Cooler 1 Corrected Temp:
Comments:
Trip Blank Received: Y l�t V
HCL McOH TSP Other
Non Conform s): Page:
YES , O of: _
NA
oc

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
�fAceAnaf;,trcal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 I%vaterj DOC, CLHg
**Bottom half of box is to list number of bottle
Project Wp# : 92467333
PM: CD1 Due Date: 03/13/20
CLIENT: 92-13axter
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ply Adjustment Log for Preserved Samples _
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot #
adjusted added
_.___._ .� hi .+k rarcu— nFHNn [Prtification Office (Le.
Note: Whenever there is a discrepancy affecting North Carolina compliance hdillp—, d e,upy � „ .i• . �_i_ �• ••• _-
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 19 of 19