WQ0011244_Residual Annual Report 2020_20210224

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0011244
Applicant/Permittee City of Oxford
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide inforration on the person to be contacted by N B Staff
Name * Lysa Finnerty
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
14105376150
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0011244
Fbs Current Existing perrrit number
Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220
Facility Name * City of Oxford RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report for City of Oxford NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form} Engineering Fans, Specifications, Calculations, Bc.)
Oxford NC 2020 Annual Report FINAL.pdf 9.87MB
upload only 1 F3Fdocurrent (less than 250 fvB). Miltiple documents rust be confined into one F7Ffile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/24/2021

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 24, 2021
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report for Permit No. WQ0011244
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Oxford, NC.
If you have any questions or need additional information, please do not hesitate to contact Amy
Ratliff at [phone] or Ryan Copeland at [phone].
Sincerely,
W�1 01_ I t
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Amy Ratliff, City of Oxford
Ryan Copeland, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF OXFORD, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0011244
2020 ANNUAL REPORT

City of Oxford, NC
Residuals Land Application Program
2020 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

> ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00011244 County Granville Year 2020
Facility Name (as shown on permit) City of Oxford W WTP NPDES No. NCO025054
Land Application Operator SMagro Phone# Q36) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 26
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 159.38
Total number of acres utilized for land application during the year: 50.8
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." n ,
Amy Ratliff. City Engineer 9t ` (C / &, A 7'' / q /Z/
Permi a, a Title (type or print) Signature o e Date
-Z' i
ature of Preparer* Date Si a f and tier Date
(if different from Permittee) (if different om Permittee an Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
OXFORD,NC
OXFORD, NC AEROB. DIGESTED LIQUID
MONTH/YEAR
May 2020
November 2020
TOTAL
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
911,400.00 G 117.82 D 106.86
294,000.00 G 41.56 D 37.70
1,205,400.00 G 159.38 D 144.56
Report Date: 2/5/2021 2:47:36 PM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00011244 Laboratory:
Facility Name: OXFORD, NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source WQ # or Inc.
NPDES#: NCO025054
WWTP Name: OXFORD
Residual Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Sample or Composite Date 01115/20 04/02/20 07/30/20 10/14/20
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids
NA
2.50
3.10
3.86
3.39
Arsenic
75
<20
<16.1
3.2
3.8
Cadmium
85
<4
<3.23
0.6
1A
Copper
4300
341
8.61
290
450
Chromium
NA
34.7
<8.06
26
42
Lead
840
18.4
<9.68
18
30
Mercury
57
<0.604
<0.506
1.1
<0.56
Molybdenum
75
<10
<8.06
5.1
8.5
Nickel
420
<10
<8.06
8.7
12
Selenium
100
<20
<16.1
3.5
7.5
Zinc
7500
1120
40.3
1100
1800
Total Phosphorus
NA
18200
1130
19000
18000
TKN
NA
68000
49400
44000
37000
Ammonia -Nitrogen
NA
9440
13700
13000
11000
Nitrate and Nitrite
NA
276
<154
34.6
62
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
and im isonment for knowing violations."
Z�Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1 102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/5/20212:47:09 PM For: 2049 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WO Permit Number:
WQ001 1244 Laboratory:
Facility Name:
OXFORD, NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source
Inc.
NPDES # or WQ#:
NCO025054
WWTP Name:
OXFORD
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Sample or Composite Date
01/15/20
04/02/20
07/30/20
10/14120
Parameters (mg/kg dry weight)
Aluminium
39500
1610
29000
46000
Calcium
17000
1270
8900
16000
Magnesium
3440
739
2400
4200
PH (S.U.)
7.00
6.90
7.10
7.50
Potassium
3890
1750
2100
2900
Sodium
2500
1880
1300
2100
PAN
22516
17744
15835
13362
SAR (Ratio)
0.7209
1.8198
0.6184
0.7011
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Z55� ignature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1 102(26)
Printed: 2/5/20212:60:35 PM For: 2049 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
1 /27/2020
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-017-0013
Project Description: Oxford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/17/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�a f• c•—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-017-0013
Client Project Description: Oxford
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
70208
Oxford
Solids
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
01/15/2020
08:55
01/17/2020
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

i
Waypoint.:
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Mary Brewer
Project
Oxford
Report Date : 01/27/2020
284 Boger Road
Information :
Received : 01/17/2020
Mocksville , NC 27028
Pam« mL 60wr
Pauric McGroary
Report Number : 20-017-0013
REPORT OFANALYSIS
Agronomist
Lab No : 70208
Matrix:
Solids
Sample ID : Oxford
Sampled:
1/15/2020 8:55
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
97.5
%
0.010
1
01/21/2016:44
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
9440
mg/Kg -
dry
4000
1
01/24/20 13:30
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
276
mg/Kg -
dry
193
1
01/24/20 13:43
ZBD 4500NO3F-2011
Organic N
58400
mg/Kg -
dry
10000
1
01/24/20 10:00
CALCULATION
pH
7.0
S.U.
1
01/23/20 05:46
JSL 9045D
Total Solids
2.50
%
0.010
1
01/21/20 16:44
ADM SM-2540G
Total Kjeldahl Nitrogen
68000
mg/Kg -
dry
10000
1
01/24/20 10:00
JPJ ;M-4500-NH3C-TKl`
Phosphorus
18200
mg/Kg -
dry
200
1
01/23/20 00:43
JTR 6010D
Aluminum
39500
mg/Kg -
dry
200
1
01/23/20 00:43
JTR 6010D
Arsenic
<20.0
mg/Kg -
dry
20.0
1
01/23/20 00:43
JTR 6010D
Calcium
17000
mg/Kg -
dry
1000
1
01/23/20 00:43
JTR 6010D
Cadmium
<4.00
mg/Kg -
dry
4.00
1
01/23/20 00:43
JTR 6010D
Chromium
34.7
mg/Kg -
dry
10.0
1
01/23/20 00:43
JTR 6010D
Copper
341
mg/Kg -
dry
10.0
1
01/23/20 00:43
JTR 6010D
Iron
13000
mg/Kg -
dry
200
1
01/23/20 00:43
KKM 6010D
Lead
18.4
mg/Kg -
dry
12.0
1
01/23/20 00:43
JTR 6010D
Magnesium
3440
mg/Kg -
dry
200
1
01/23/20 00:43
JTR 6010D
Manganese
440
mg/Kg -
dry
20.0
1
01/23/20 00:43
JTR 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 5

i
Waypoint.:
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Mary Brewer
Project
Oxford
Report Date : 01/27/2020
284 Boger Road
Information :
Received : 01/17/2020
Mocksville , NC 27028
Pam« mL 60wr
Pauric McGroary
Report Number : 20-017-0013
REPORT OFANALYSIS
Agronomist
Lab No : 70208
Matrix: Solids
Sample ID : Oxford
Sampled: 1/15/2020 8:55
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
<0.604
mg/Kg
- dry
0.604
1 01/22/20 14:24 TJS SW-7471B
Molybdenum
<10.0
mg/Kg
- dry
10.0
1 01/23/20 00:43 JTR 6010D
Nickel
<10.0
mg/Kg
- dry
10.0
1 01/23/20 00:43 JTR 6010D
Potassium
3890
mg/Kg
- dry
200
1 01/23/20 00:43 JTR 6010D
Selenium
<20.0
mg/Kg
- dry
20.0
1 01/23/20 00:43 JTR 6010D
Sodium
2500
mg/Kg
- dry
1000
1 01/23/20 00:43 JTR 6010D
Zinc
1120
mg/Kg
- dry
50.0
1 01/23/20 00:43 JTR 6010D
Sulfur
8240
mg/Kg
- dry
200
1 01/23/20 00:43 JTR 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 5

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 2-4237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 20-017-0013
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 01/17/2020 13:01:33
Page 5 of 5

Waypointo
ANALYTICAL
4/15/2020
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-097-0003
Project Description: Oxford N&M
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/6/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-097-0003
Client Project Description: Oxford N&M
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
70954
Oxford
N&M
Solids
04/02/2020
07:40
04/06/2020
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Mary Brewer
Project
Oxford
N&M
Report Date : 04/15/2020
284 Boger Road
Information :
Received : 04/06/2020
Mocksville , NC 27028
P��G mL 60wr
Pauric McGroary
Report Number : 20-097-0003
REPORT OFANALYSIS
Agronomist
Lab No : 70954
Matrix:
Solids
Sample ID : Oxford N&M
Sampled:
4/2/2020 7:40
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
96.9
%
0.010
1
04/07/2016:15
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
13700
mg/Kg -
dry
3230
1
04/15/20 14:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<154
mg/Kg -
dry
154
1
04/13/20 14:02
ZBD 4500NO3F-2011
Organic N
35800
mg/Kg -
dry
8060
1
04/13/20 14:00
CALCULATION
pH
6.9
S.U.
1
04/13/20 05:39
JSL 9045D
Total Solids
3.10
%
0.010
1
04/07/20 16:15
ADM SM-2540G
Total Kjeldahl Nitrogen
49400
mg/Kg -
dry
8060
1
04/13/20 14:00
JPJ ;M-4500-NH3C-TKl`
Phosphorus
1130
mg/Kg -
dry
161
1
04/08/20 20:56
TJS 6010D
Aluminum
1610
mg/Kg -
dry
161
1
04/08/20 20:56
TJS 6010D
Arsenic
<16.1
mg/Kg -
dry
16.1
1
04/08/20 20:56
TJS 6010D
Calcium
1270
mg/Kg -
dry
806
1
04/08/20 20:56
TJS 6010D
Cadmium
<3.23
mg/Kg -
dry
3.23
1
04/08/20 20:56
TJS 6010D
Chromium
<8.06
mg/Kg -
dry
8.06
1
04/08/20 20:56
TJS 6010D
Copper
8.61
mg/Kg -
dry
8.06
1
04/08/20 20:56
TJS 6010D
Iron
1110
mg/Kg -
dry
161
1
04/08/20 20:56
TJS 6010D
Lead
<9.68
mg/Kg -
dry
9.68
1
04/08/20 20:56
TJS 6010D
Magnesium
739
mg/Kg -
dry
161
1
04/08/20 20:56
TJS 6010D
Manganese
35.8
mg/Kg -
dry
16.1
1
04/08/20 20:56
TJS 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

�'
WayP
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Mary Brewer
Project
Oxford
N&M
Report Date : 04/15/2020
284 Boger Road
Information :
Received : 04/06/2020
Mocksville , NC 27028
P��G mL 60wr
Pauric McGroary
Report Number : 20-097-0003
REPORT OFANALYSIS
Agronomist
Lab No : 70954
Matrix: Solids
Sample ID : Oxford N&M
Sampled: 4/2/2020 7:40
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
<0.506
mg/Kg
- dry
0.506
1 04/08/20 11:48 DDB SW-7471B
Molybdenum
<8.06
mg/Kg
- dry
8.06
1 04/08/20 20:56 TJS 6010D
Nickel
<8.06
mg/Kg
- dry
8.06
1 04/08/20 20:56 TJS 6010D
Potassium
1750
mg/Kg
- dry
161
1 04/08/20 20:56 TJS 6010D
Selenium
<16.1
mg/Kg
- dry
16.1
1 04/08/20 20:56 TJS 6010D
Sodium
1880
mg/Kg
- dry
806
1 04/08/20 20:56 TJS 6010D
Zinc
<40.3
mg/Kg
- dry
40.3
1 04/08/20 20:56 TJS 6010D
Sulfur
260
mg/Kg
- dry
161
1 04/08/20 20:56 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 20-097-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 04/06/2020 10:34:11
Page 5 of 6

SAMPLING LOG #
PROJECT MANAGER: _ g4AN _ `'O tUANQ
14-41 1 A&
7821
Rich
I ll��lf f llf IF JlrIlf� NIlll llfll�f Nl�f l lllf l lllf l llf 11 ill 1111 46478 W OF CLl�'ri`ODY
Dxfnrd Noe, 10 3�:33 ORD & ANALYSIS
RECORD
l attest that tyre propw iier« sampdng procedures
were used during the collectlon of these samples.
Phone:
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OP SAMPLING METHOD METHOD
LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
Relinquished by Sampler. Date Time Recleved by: REMARKS:
Relinquished by: D Time ad by: - -
Relinquishes! by: 1 a Time Reoleved by.
SPECIAL. INSTRUCTIONS:
16
For monitoring purposes. PO#: -
SAMPLE
ANALYSIS REQUEST
I.D.
SL1
SL2
NH4-N
NDa-N
Organic
Cd
Co
NI
Pb
As
Hg
Se
pH
CaCO3
!gtjlv.
Volatile
Solids
Mo
CI
NO2-N
vY�4))
100V
1009
P00
Po
10
1000
11009
110off
140
1�0
1000
too
P00
IO
SLi: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL.2: Basic Test SLt plus Suftr, Calcium, Magnesium, Sadfum, Iron, Aluminum, Manganese, Copper and Zinc
w
0
v
a

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Oxford WWTP
Lot Number:VG31064
Date Completed:08/10/2020
08/11/2020 6:42 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VG31064
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure. The LOQ has
been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VG31064-001
Description: OXFORD WWTP Matrix: Solid
Date Sampled:07/30/2020 0822 % Solids: 3.86 08/01/2020 2011
Date Received:07/31/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 08/01/2020 2011 SRB
62017
1 350.1
(Ammonia - N ) 350.1
25 08/06/2020 1641 DMA
62563
1
(Nitrate - N ) 9056A
1 08/05/2020 1439 AMR
62554
1
(Nitrite - N ) 9056A
1 08/05/2020 1439 AMR
62552
1
(Phosphorus) 365.1
25 08/05/2020 0843 DMA
08/04/2020 1258
62258
1
(Soil pH meas) 9045D
1 08/07/2020 2324 SRB
62831
1 351.4
(TKN) 351.2
1 08/05/2020 1718 DMA
08/05/2020 1005
62372
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.86
%
1
Ammonia - N (gas diffusion)
350.1
13000
650
340
mg/kg
1
Nitrate - N (soluble)
9056A
31
13
2.6
mg/kg
1
Nitrite - N (soluble)
9056A
3.6 J
5.2
2.6
mg/kg
1
Phosphorus
7723-14-0 365.1
19000
3200
650
mg/kg
1
Soil pH measured in water @
21.7 ° C
9045D
7.1
su
1
TKN
351.2
44000
650
650
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 08/05/2020 0855 JAB2
08/01/2020 1641
62042
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
1.1 J
2.0
0.48
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 08/05/2020 1630 KSH2
08/04/2020 1422
62041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
29000
170
64
mg/kg
1
Arsenic
7440-38-2 6010D
3.2 J
6.4
2.1
mg/kg
1
Cadmium
7440-43-9 6010D
0.60 J
2.1
0.54
mg/kg
1
Calcium
7440-70-2 6010D
8900
2100
270
mg/kg
1
Chromium
7440-47-3 6010D
26
4.3
1.1
mg/kg
1
Copper
7440-50-8 6010D
290
4.3
1.9
mg/kg
1
Iron
7439-89-6 6010D
10000
43
19
mg/kg
1
Lead
7439-92-1 6010D
18
4.3
1.9
mg/kg
1
Magnesium
7439-95-4 6010D
2400
2100
270
mg/kg
1
Manganese
7439-96-5 6010D
370
6.4
2.5
mg/kg
1
Molybdenum
7439-98-7 6010D
5.1 J
17
4.3
mg/kg
1
Nickel
7440-02-0 6010D
8.7 J
17
4.5
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VG31064-001
Description: OXFORD WWTP Matrix: Solid
Date Sampled:07/30/2020 0822 % Solids: 3.86 08/01/2020 2011
Date Received:07/31/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 08/05/2020 1630 KSH2
08/04/2020 1422
62041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
2100
2100
270
mg/kg
1
Selenium
7782-49-2 6010D
3.5 J
8.5
3.5
mg/kg
1
Sodium
7440-23-5 6010D
1300 J
2100
270
mg/kg
1
Zinc
7440-66-6 6010D
1100
21
5.3
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7
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PACE ANALYTICAL SERVICES, LLC
Sl:&aly GrvlronWnr#1 .'^rveerx, Im.
L]ocundn[ Nu-,Fa:NiGrCILEC 14
Sample Receipt Checkl6t
Client: I " Coolerinsprr-Aral idate 1
_
IV,QM5 7Fr roil r: VO SPS1 ❑ C1=east UI'S ❑ FedFx O-
❑ YQN u 1. wtru Custod SG41!s ent On the oaol,z?
Yes No NA 2. Ifcust_Qdv setals UrEre irdact ail
PI-1 SCrip ID Cldorille Strap Ili, -
Crri ,pal t enture u n vipt } 1D i d (C zeutadj tem rani upon £oc
-�1 }°C � C {' °C 'C
Method: C]'rcmVeretut+e H A�dins# finttles Ift un ID:
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3, lIf t4N]3Ma-l�r�e nFr,ny rUDIM exceeded UrC, W
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0 No
J5r
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cs
T iD
6- were Minple Us listed an the COC?
y
❑ No
7- Wem sample IN listed on;lI saitiplc container
No
8, Was anllettim date & time liffwd on 11 L; C0C'?
El -No
9, Was collection dace &time listed on all ea'mple
IvYes
e€
0 NiF
10. Did all conlairier label iuformation I11% date, t:
l es
l 1 NI)
I], Wue tests to be pafrnmcd listed on the COC'+
Dry "s
O NP
12. Did all samples arrivr in the proper cont:uners
(unhmkrn, lids m. els,)?
u�
0 Jti p
13- W &q ate uale sarapk %,olusue available?
Yes
❑ 'o
14, Were all samples received ""thin Y3 xhe l,nldin
Yes
Na
15. WerVc Pny .5wn Ieh cDniaiuers lniss' sycas (
[j Y"s
❑ h1a,
1'1
16- For VOA and 1;'3IC-175 kamrAes. w= babble
in au of the VOA. AA140
CT Y'es
Na
NA
I i, Were all 1 winetals{nutrlent sarn lee receive
�s Y"cs
No
+ A
19. Wom sill evunide .3amples received at a } l
❑ Yas
]�fn
r
19' were all app s Jc N Hp TIQdl�p p ]eno
(SRC)
Pap 1 of:
frectiec Is
d uiAwokan?
Tested by: _ T
rirt a6SOIld Snats..Cup 1D:
IR 6LID COMC iiV11 FAr:tor:
0 — M 7 -
^C
15 Ptoject Managcr Natlfwd?
n (circle on k
d to this furnf?
xeivcxk} C�llvvrGd?
contaimm?
me) agree with the CM'7
fog wh test and/or it goad condition
tiTm, or 48 hours„ wMdiewr names first?
irck one) samples Not liswd on UCK3 `?
prc:uwa t �*"Pea-siz$" ('I."ar Gram in diamclot)
i-at apHof<2?
', and soltlde samplaN reuaivcd at n PH> 9?
62M-6-mM,) samples tree of resid;ral
❑ Yes '�`20. Wv% client ren]wkainr quests ur (i,c. rcqsiW di u .OnS, '%4'NM dcsi flPDS: ells--_)
❑ " cnrri�cily transcribed hwn the COC inky the COi a t eut section in L1MS'�
[] Y09 0 21. Was the av6G number listed on the container hcY? If fi otc� fl
;ample Pres(- mttion (Mint lie coinpteted fcT any sampk(s) int:011tetly P Menred or will] hm-15paer-)
�arnple(s) _WeM rCCaiYEit inKA tly pMSW%red and were AdjUmd accordinQly
" sample retefyfttig with mL of circle one., H2804, 11114103, Hi J, *d 1H using It * _
Gene of pmwvadw _ If more illats one preservative is MC9W, le a note in the. eaDunuits laelow,
aitlple(s) _wort{ received with bubbles mm to diflmeGcr,
unng;es s) we're recaiwd will 'CRCs AS MWL (If s`19 is no) and Were
jDsle;l accordingly in s�mplo receiviug �sith wdilari Ihic�sulf to (Na�S�D]] i& Shmaly lf],
Slk harcnde labels applied by: i Date, j 1 O
Con]mcr.N:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Oxford
Lot Number:VJ16006
Date Completed:10/23/2020
NIM�� Mr�
10/28/2020 3:24 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VJ16006
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample -001 was weighed out at 3 times the normal amount. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VJ16006-001
Description: OXFORO N&M Matrix: Solid
Date Sampled:10/14/2020 1005 % Solids: 3.39 10/17/2020 0144
Date Received:10/16/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 10/17/2020 0144 LSH
70234
1 350.1
(Ammonia - N ) 350.1
10 10/19/2020 1724 DRD
70365
1
(Nitrate - N ) 9056A
1 10/21/2020 1932 AMR
70656
1
(Nitrite - N ) 9056A
1 10/21/2020 1932 AMR
70657
1
(Phosphorus) 365.1
25 10/20/2020 1740 DMA
10/20/2020 1300
70385
1
(Soil pH meas) 9045D
1 10/20/2020 2239 AAB
70569
2 351.4
(TKN) 351.2
1 10/21/2020 1737 DMA
10/21/2020 1201
70594
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.39
%
1
Ammonia - N (gas diffusion)
350.1
11000
300
150
mg/kg
1
Nitrate - N (soluble)
9056A
44
15
3.0
mg/kg
1
Nitrite - N (soluble)
9056A
18
5.9
3.0
mg/kg
1
Phosphorus
7723-14-0 365.1
18000
3700
740
mg/kg
1
Soil pH measured in water @
19.3 ° C
9045D
7.5
su
1
TKN
351.2
37000
740
740
mg/kg
2
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/20/2020 1342 JAB2
10/20/2020 0910
70438
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
2.3
0.56
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/22/2020 0131 KSH2
10/17/2020 1518
70258
2 3050B
601OD
1 10/22/2020 1406 KSH2
10/17/2020 1518
70258
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
46000
200
73
mg/kg
1
Arsenic
7440-38-2 6010D
3.8 J
7.3
2.4
mg/kg
1
Cadmium
7440-43-9 6010D
1.1 J
2.4
0.62
mg/kg
1
Calcium
7440-70-2 6010D
16000
2400
310
mg/kg
1
Chromium
7440-47-3 6010D
42
4.9
1.2
mg/kg
1
Copper
7440-50-8 6010D
450
4.9
2.2
mg/kg
1
Iron
7439-89-6 6010D
18000
49
22
mg/kg
1
Lead
7439-92-1 6010D
30
4.9
2.2
mg/kg
1
Magnesium
7439-95-4 6010D
4200
2400
310
mg/kg
1
Manganese
7439-96-5 6010D
670
7.3
2.9
mg/kg
1
Molybdenum
7439-98-7 6010D
8.5 J
20
4.9
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VJ16006-001
Description: OXFORO N&M Matrix: Solid
Date Sampled:10/14/2020 1005 % Solids: 3.39 10/17/2020 0144
Date Received:10/16/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 10/22/2020 0131 KSH2
10/17/2020 1518 70258
2 3050B
6010D 1 10/22/2020 1406 KSH2
10/17/2020 1518 70258
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
12 J 20
5.1
mg/kg
2
Potassium
7440-09-7 6010D
2900 2400
310
mg/kg
1
Selenium
7782-49-2 6010D
7.5 J 9.8
4.0
mg/kg
1
Sodium
7440-23-5 6010D
2100 J 2400
310
mg/kg
1
Zinc
7440-66-6 6010D
1800 24
6.1
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
SI►-+aLy Qrxi.- mmotal Scrotces, ]cc.
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$ample Receipt Checklixt ( .Eta'}
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McPnRofrerript: 0 5 S1 ddlicrit m UPE M fedLx {)Cher',
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Ycsl LJ Nol A NA 2- If CUMIAly 50j& were pro%M, 1vtre 014y intact a_nd rinhml on?
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9. Way collection date & :iFri r listed on ail sample conrainein?
10. Did nJlcunla[nerJabol infOMW1011 (ID- &de, tune)agree xvidl tl
1 I, Wcmbus to be per firmed listed on Uke C OC F
12- Did nil scam pJes arrive in the proper coirtai rrors for rack test a ydl
(unbroken, [ids an, etc,)': —
11 Was OA4' fuu[e Sam Je vnlumr. ova3abl-0
14. Were ail samples reuuivec w hi.n Vz be holding Umc or 46 hour
15, Were any samples -ontaillers missin ewce-srt (ciTrle ore,' sanip[i
16, FOc VOA and RSK-J 75 sarapier,, were.. bubbles preSanL ' pci si
rR Any of the VOA vials?
I?. %Vca-c riII ) WVmetaJ&inl3triant samples recr:iKd Ft a [I of t
IS. Were ail cynnidc samples received at a uH > 12 arrd sulfide sam
0 ves 0 NIO ®NA 20- Werc client remarkV uasts (i.e. requested dilutions- ASS,+MSD
correctly tmnscribe-d front the COC intro die ❑rpr, rr mit sect ion i,i. UK
❑ 'e_VFN-al 121, W8.4 `.ham q.ElDte number I_slud on die container label? If 24
minpic Preservaiina (Must be ctunpidPEI for- any sample(s) incaljwly preserved arw9th IJC
;mrLp-efs) NAwere receivM incorl�ectly prcr&T%cd at
ILalup10 "CLTivillLr vOhh N"A __rnl_ofeirle Oric. H'a1 U4, 11NO3, HC4NinLOA ILSingSR9. WA
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djusted accordingly in =mpk rviceivin.q with sodium tlliosulfatk (Na292N with S11ea1y [D: N
K Loroode labtlsapplie!dby 13MG Dom- H 16MO2D
C'oTirnents;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: OXFORD, NC WQ PERMIT #: W00011244 FIELD#: NC-GR-00060-0-0002- ACRES UTILIZED: 31.9
LANDOWNER: ROBERT CERW IN ANNUAL DRY TONS APPLIED: 117.82 SITE #: NC GR 00060 ACRES PERMITTED: 31.9
OPERATOR: JAKE ISLEY PREDOMINANT SOIL SERIES: LIGNUM CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 190 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
SiteName
of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
i
Date or
or Wet Tons (W)
%
i
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
I
Solids DryTons/Ac
Source
Moist
Inches
Method*
'' Rate**
Rate*'*
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
5/11/2 220
13Q200.00 (G)
3.100
0.528
OXAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
49,400.00
137700.00
154.00
18.724
FSH
5/12/2020
111,600.00 (G)
3.100
0.452
OXAEDL
DRY
110-<1/2"
SUR
0.5
0.30
49,400.00
13,700.00
154.00
16.049
FSH
5/13/2020
111,600.00 (G)
3.100
0.452
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
49,400.00
13,700.00
154.00
16.049
FSH
5/14/2020
117,800,00 (G)
3.100
0.477
OXAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
49,400.00
13,700.00
154.00
16.941
FSH
5/15/2020
124,000.00 (G)
3.100
0.502
OXAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
49,400.00
13,700.00
154.00
17.832
FSH
5116/2020
124,000.00 (G)
3.100
0.502
OXAEDL
DRY
"0-<1!2"
SUR
0.5
0.30
49,400.00
13,700.00
154.00
17.832
FSH
5/1712020
86,800.00 (G)
3.100
0.352
OXAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
49,400.00
S 13,700.00
# 154.00
12A83
FSH 3 '
5/18/2020
105,400.00 (G)
3.100
0.427
OXAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
49,400.00
13,700.00
q 154.00
15.158
FSH
1-
May-20
911,400.00 (G)
1
1
l
i
Total
3.692
Total
131.068 0,000
AS
CD
CuPB��O.
MO
NI
SE
ZN
�8347
Lime Applied
FA.1-allbslacreApplied
0,119
0.024
F:0.0��0,06O0.0724
�0.060
0.060
0.119
0.298��
Date Lbs/Ac
(Ibs/acre) 1st
Federal C.P
22.771
1,339.0 I t 267
0.064
375.0
109.771
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required **' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation ***' C.P.L.R.: Cumulative Pollutant Loading Rate
°* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0**** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: OXFORD, NC WQ PERMIT #: WO0011244 FIELD#: NC-GR-00060-0-0005- ACRES UTILIZED: 11.7
LANDOWNER: ROBERT CERW IN ANNUAL DRY TONS APPLIED: 30.53 SITE M NC GR 00060 ACRES PERMITTED: 11.7
OPERATOR: JAKE ISLEY PREDOMINANT SOIL SERIES: ENON CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 194 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Site Name of Crop Type
or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application l
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
11/9/2020 138,000.00 (G) 3.390 1.667 OXAEDL
11/10/2020 78,000.00 (G) 3.390 0.942 OXAEDL
I
Nov-20 216,000.00 (G)
¢
DRY
DRY
"0-11/2"
110-<1/2"
SUR
SUR
0.5
0.5
0.30
0.30
37,000.00
37,000.00
11,000.00
11,000A0
62.00
62.00
44.558
25.185
FSH
FSH
Total 2.609
Total
69.743 0.000
CD
CR
PB�SE
ZN
P
Lime Applied
EEAS
lAnnuai Ibstacre Applied 20 OA06
E2!34�90.219
0.157
0.003
0.044
�Nl
9
9.395
93.952
Date
Lbs/Ac
Cumulative Ibs/acre Applied 0.311 0.089
22.855
3,100
1.599
0.057
0.475
1,078
0.489
101.020
Permit PAN Limit (Ibs/acre) 1st Crop
r-orlaral C.P_I R. /lhs/arrel**** 36.6 34.8
1,339.0
267.9
15.0
375.0
89.0
2,500.0
194
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
�,J -2 j
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobicaliy digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation °*** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injectiontincorporation 1.0 ****` See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: OXFORD, NC WO PERMIT #: WQ0011244 FIELD#: NC-GR-00060-0-0006- ACRES UTILIZED: 7.2
LAND OWNER: ROBERT CERW IN ANNUAL DRY TONS APPLIED: 11.03 SITE #: NC GR 00060 ACRES PERMITTED: 7.2
OPERATOR: JAKE ISLEY PREDOMINANT SOIL SERIES: ENON CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 194 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond. Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
% Residual Dry, Wet, Past 24 Hrs. Application
lization
ization TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids Dry Tons/Ac Source Moist Inches Method'
Rate**
Rate*** mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
11/10/2020
78,000.00
(G)
3.390 1.531 OXAEDL DRY "0-<1/2" SUR
0.5
0.30 37,000.00
11,000,00
62.00
40.926
FSH
Nov-20
78,000.00
(G)
Total 1.531 a vaao
AS
CD�CU�C�R�Mo��NI�SEAnnual
ibslacre Applied
0.012
0.003�PB�HG
5.513
55.132
Date
Lbs/Ac
19.474
Limit
0.045
85.981
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 15.0 31b.0 I ua.v z,ouu.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

SECTION 4

MM1 T Summit Environmental Technologies, Inc.
SU3310 Win St.
F.NVIRONMENTALTECHNOLAG1ES,INQ Cuyahoga Falls, Ohio44223
ArrBlytical Labaroxories TEL: [phone] FAX.- [phone]
Website: httn:Ilwww.settek.com
July 24, 2018
Clay Fisackerly
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Oxford TCLP 2018
Dear Clay Fisackerly:
Order No.: 18061305
Summit Environmental Technologies, Inc. received 1 sample(s) on 6/22/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 27

��' � Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
F"OR0NMENTkL7ECHNOLOGIES,INC- Cuyahoga Falls, Ohio44223 wo#: 18061305
Arrafytrcal Lshor43Jv 'jes TEL: [phone] FAX.- [phone]
Wehsite: httn://www.settek.com Date: 7/24/2018
CLIENT: Synagro
Project: Oxford TCLP 2018
WorkOrder Narrative:
18061305: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
18061305-OOIA 391811: Prep Comments for MtlPrep_TCLP(3010A), Sample 18061305-OOIA:
Sample had a yellow tint, had limited volume, and was filtered after digestion.
18061305-OOIA 391857: Prep Comments for SVPrep_BNATot_TCLP(3510), Sample 18061305-
001A: Sample is a soapy solution, Limited volume
18061305-OOIA 391855: Prep Comments for SVPrep_CPest_TCLP(3510), Sample 18061305-OOIA:
Sample is a soapy solution, Original pH of sample is acidic; sample was neutralized prior to extraction,
Limited volume
Original
Page 2 of 27

SUMMIT Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win S
FNVIRONMENTALTfGHNOLOGIE$,mr, Cuyahoga Falls, Ohio442� WO#: 18061305
ArrAytical Lohprarorles TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co, Date: 7/24/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 27

FHYIRONMENTAL TECHNOLOGIES, 1RC
ArriOytrcel Labomivries
CLIENT: Synagro
Project: Oxford TCLP 2018
Lab SampleID Client Sample ID
18061305-001 Oxford TCLP 2018
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Tag No Date Collected
6/21/2018 12:30:00 PM
Workorder
Sample Summary
WO#: 18061305
24 Jul-l8
Date Received Matrix
6/22/2018 10:20:00 AM Sludge
Page 4 of 27

min' Summit Environmental Technologies, Inc. DATES REPORT
su3310 Win St.
r=HVIRONMENTAL TECHHOLAOar=S, INC_ Cuyahoga Falls, Ohio 44223
Analyllosl 1 abcNs� IieS TEL: [phone] FAX.- [phone] WO#: 18061305
Wehsite: http://www.settek.com 24 Jul-18
Client: Synagro
Project: Oxford TCLP 2018
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
18061305-OOIA Oxford TCLP 2018 6/21/2018 12:30:00 PM Sludge Ignitability of Solids (SW-846: 1030)
7/23/2018 2:00:00 PM
pH (SW9045D)
7/9/2018 5:18:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
6/25/2018 2:29:00 PM
Reactive Sulfide (9034)/7.3.4.2
6/25/2018 2:29:00 PM
TCLP Herbicides Analysis (SW1311/87/1/2018 6:00:00 PM
7/3/2018 12:30:00 PM
7/11/2018 7:20:00 PM
TCLP Mercury Analysis (SW1311/74") 7/1/2018 6:00:00 PM
7/3/2018 10:55:00 AM
7/3/2018 3:43:00 PM
TCLP Metals Analysis (SW1311/6010 7/1/2018 6:00:00 PM
7/2/2018 3:20:00 PM
7/5/2018 8:34:41 PM
TCLP Pesticides Analysis (SW1311/8(7/l/2018 6:00:00 PM
7/2/2018 1:00:00 PM
7/11/2018 2:30:00 PM
TCLP Semi-Volatiles Analysis 7/1/2018 6:00:00 PM
7/2/2018 11:15:00 AM
7/9/2018 12:18:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
7/1/2018 6:00:00 PM
7/4/2018 2:16:00 AM
Original
Page 5 of 27

MMIT Summit Environmental Technologies, Inc.
SU3310 Win St.
FNVIRONMENTAL7ECHNOLOMES,If%iC Cuyahoga Falls, Ohio44223
ArrAytical LshpY43xprjes TEL: [phone] FAX. [phone]
Website: httn:11'h settek.com
Analytical Report
(base report)
WO#: 18061305
Date Reported: 7/24/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 6/21/2018 12:30:00 PM
Lab ID: 18061305-OOIA
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
SW7470A SW7470A Analyst: EAM
ND 0.0100 mg/L 1 7/3/2018 3:43:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
2.50
mg/L
1
7/5/2018 8:34:41 PM
TCLP Barium(Ba)
ND
25.0
mg/L
1
7/5/2018 8:34:41 PM
TCLP Cadmium(Cd)
ND
0.500
mg/L
1
7/5/2018 8:34:41 PM
TCLP Chromium(Cr)
ND
1.00
mg/L
1
7/5/2018 8:34:41 PM
TCLP Lead(Pb)
ND
2.50
mg/L
1
7/5/2018 8:34:41 PM
TCLP Selenium(Se)
ND
0.250
mg/L
1
7/5/2018 8:34:41 PM
TCLP Silver(Ag)
ND
2.50
mg/L
1
7/5/2018 8:34:41 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.160
mg/L
2
7/9/2018 12:18:00 PM
2,4,5-Trichlorophenol
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
2,4,6-Trichlorophenol
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
2,4-Dinitrotoluene
ND
0.0800
mg/L
2
7/9/2018 12:18:00 PM
o-Cresol
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
m/p-Cresol(s)
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
Cresols, Total
ND
8.00
mg/L
2
7/9/2018 12:18:00 PM
Hexachloro-1,3-butadiene
ND
0.0320
mg/L
2
7/9/2018 12:18:00 PM
Hexachlorobenzene
ND
0.0800
mg/L
2
7/9/2018 12:18:00 PM
Hexachloroethane
ND
0.160
mg/L
2
7/9/2018 12:18:00 PM
Nitrobenzene
ND
0.160
mg/L
2
7/9/2018 12:18:00 PM
Pentachlorophenol
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
Pyridine
ND
0.400
mg/L
2
7/9/2018 12:18:00 PM
Surr: 2-Fluorophenol
25.2
10 - 109
%Rec
2
7/9/2018 12:18:00 PM
Surr: Phenol-d6
27.0
10 - 109
%Rec
2
7/9/2018 12:18:00 PM
Surr: Nitrobenzene-d5
31.6
19 - 120
%Rec
2
7/9/2018 12:18:00 PM
Surr: 2,4,6-Tribromophenol
33.4
10 - 120
%Rec
2
7/9/2018 12:18:00 PM
Surr: 2-Fluorobiphenyl
41.8
22 - 117
%Rec
2
7/9/2018 12:18:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
O RSD is greater than
RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 6 of 27

MMIT Summit Environmental Technologies, Inc.
SU3310 Win St.
FNVIRONMENTAL7ECHNOLOMES,If%iC Cuyahoga Falls, Ohio44223
ArrAytical LshpY43xprjes TEL: [phone] FAX. [phone]
Website: httn:11'h settek.com
Analytical Report
(base report)
WO#: 18061305
Date Reported: 7/24/2018
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 6/21/2018 12:30:00 PM
Lab ID:
18061305-OOIA
Project:
Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 89.7
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
35.1
Surr: DCB
56.0
SW8270D SW351OC Analyst: BJH
34 - 116 %Rec 2 7/9/2018 12:18:00 PM
SW8081 SW351OC Analyst: JBN
0.0200
mg/L
1
7/11/2018 2:30:00 PM
0.0400
mg/L
1
7/11/2018 2:30:00 PM
0.00200
mg/L
1
7/11/2018 2:30:00 PM
0.00200
mg/L
1
7/11/2018 2:30:00 PM
0.00200
mg/L
1
7/11/2018 2:30:00 PM
0.00200
mg/L
1
7/11/2018 2:30:00 PM
0.00200
mg/L
1
7/11/2018 2:30:00 PM
10 - 119
%Rec
1
7/11/2018 2:30:00 PM
10 - 119
%Rec
1
7/11/2018 2:30:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D ND 1.00 d
2,4,5-TP ND 0.500 d
Surr: DCAA 83.7 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
SW8151A SW8151A Analyst: JBN
mg/L 1 7/11/2018 7:20:00 PM
mg/L 1 7/11/2018 7:20:00 PM
%Rec 1 7/11/2018 7:20:00 PM
SW8260B SW1311 M Analyst: CTB
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
2.50
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.500
mg/L
100
7/4/2018 2:16:00 AM
0.200
mg/L
100
7/4/2018 2:16:00 AM
Qualifies: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 27

MM' Summit Environmental Technologies, Inc.
SU3310 Win St.
Analytical Report
FNVIRQNMENTAL7ECHNOLOGIES,If%iC
Cuyahoga Falls, Ohio44223
(base report)
Arr.Aytical LshpY43xprjes TEL: [phone] FAX. [phone]
WO#: 18061305
Website: http://www.settek.com
Date Reported: 7/24/2018
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
6/21/2018 12:30:00 PM
Lab ID: 18061305-OOIA
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
Surr: 4-Bromofluorobenzene 107
70 - 130 %Rec
100 7/4/2018 2:16:00 AM
Surr: Dibromofluoromethane 106
70 - 130 %Rec
100 7/4/2018 2:16:00 AM
Surr: Toluene-d8 105
70 - 130 %Rec
100 7/4/2018 2:16:00 AM
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg
1 6/25/2018 2:29:00 PM
RCISOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1 7/23/2018 2:00:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 6.8
s.u.@21.7C
1 7/9/2018 5:18:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1 6/25/2018 2:29:00 PM
Qualifies: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 27

Summit Environmental Technologies, Inc.
Accreditation
Program
MM I T
EISU3310 Win St.
Anal tes Report
y p
FNVIRONMENTkLTECHNOLOGIIES,Mr,
Cuyahoga Falls, Ohio44223
Arrafytrcal Lahprelprly*
TEL: [phone] FAX.- [phone]
WO#:
18061305
Wehsite: http://www.settek.com
24 Jul-l8
Client: Synagro
State: NW
Project: Oxford TCLP 2018
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
18061305-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Original # 1
Page 9 of 27

Summit Environmental Technologies, Inc.
Accreditation
Program
MM I T
EISU3310 Win St.
Anal tes Report
y p
FNVIRONMENTkLTECHNOLOGIIES,Mr,
Cuyahoga Falls, Ohio44223
Arrafytical Lahprelprly*
TEL: [phone] FAX.- [phone]
WO#:
18061305
Wehsite: http://www.settek.com
24 Jul-l8
Client: Synagro
State: NW
Project: Oxford TCLP 2018
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
18061305-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-d14
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Toluene-d8
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original # 1
Page 10 of 27

sumfoill Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOOl>=S, INC Cuyahoga Falls, Ohio 44223
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com
QC SUMMARY REPORT
WO#: 18061305
24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: 32833
Sample ID mb-32833
SampType: MBLK
TestCode: tclp-voc-MST Units: mg/L
Prep Date: 7/1/2018
RunNo: 86054
Client ID: PBS
Batch ID: 32833
TestNo: SW8260B SW1311M
Analysis Date: 7/3/2018
SegNo: 1616959
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
50.0
Surr: Dibromofluoromethane
48.7
Surr: Toluene-d8
51.3
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
50.00 100 70
50.00 97.5 70
50.00 103 70
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
130
130
130
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 11 of 27

sumfoill Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOO17=3, INC Cuyahoga Falls, Ohio 44223
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com
QC SUMMARY REPORT
WO#: 18061305
24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: 32833
Sample ID MB-32833
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 7/1/2018
RunNo: 85971
Client ID: PBS
Batch ID: 32833
TestNo: SW8260B SW1311M
Analysis Date: 7/2/2018
SegNo: 1615558
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
488
Surr: Dibromofluoromethane
412
Surr: Toluene-d8
509
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
500.0 97.6 70
500.0 82.4 70
500.0 102 70
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
130
130
130
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 27

sumfoill
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOOlfS, INC
Cuyahoga Falls, Ohio 44223
WO#: 18061305
Analyllaal 4ab#fafvrie5
TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com
24-Jul-18
Client:
Synagro
Project:
Oxford TCLP 2018
BatchID: 32855
TCLP Mercury ND 0.00200
TCLP Mercury 0.00363 0.00200 0.00400 0 90.8 80 120
TCLP Mercury 0.00391 0.00200 0.00400 0 97.8 75 125
Sample ID 18061322-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 7/3/2018
RunNo: 86042
Client ID: BatchQC
Batch ID: 32855
TestNo: SW7470A SW7470A
Analysis Date: 7/3/2018
SegNo: 1616628
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00381 0.00200
0.00400 0 95.2 75
125
0.00391 2.59 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Original
Page 13 of 27

sumfoill Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOO47=3, INC Cuyahoga Falls, Ohio 44223
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Oxford TCLP 2018 BatchID: 32855
WO#: 18061305
24-Jul-18
Sample ID 18061322-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 7/3/2018
RunNo: 86042
client ID: BatchQC
Batch ID: 32855
TestNo: SW7470A SW7470A
Analysis Date: 7/3/2018
SegNo: 1616628
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 14 of 27

sumfoill
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOOlfS, INC
Cuyahoga Falls, Ohio 44223
WO#: 18061305
Analyllaal 4ab#fafvrie5
TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com
24-Jul-18
Client:
Synagro
Project:
Oxford TCLP 2018
BatchID: 32886
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 365 500.0 73.1 20 140
2,4-D
ND
1.00 0.500
0 72.9
62.6
125
2,4,5-TP
ND
0.500 0.500
0 78.9
52.5
128
Surr: DCAA
449
500.0
89.9
20
140
Sample ID 18061305-001ams
SampType: ms
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 7/3/2018
RunNo: 86440
Client ID: Oxford TCLP 2018
Batch ID: 32886
TestNo: SW8151A SW8151A
Analysis Date: 7/11/2018
SegNo: 1632760
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00
0.500 0 82.7 37
105
2,4,5-TP
ND 0.500
0.500 0 86.7 38
106
Surr: DCAA
486
500.0 97.1 20
140
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 15 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOL001fS, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#fatvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: 32886
Sample ID 18061305-001amsd
SampType: msd
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 7/3/2018
RunNo: 86440
Client ID: Oxford TCLP 2018
Batch ID: 32886
TestNo: SW8151A SW8151A
Analysis Date: 7/11/2018
SegNo: 1632761
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 84.9 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 89.6 38 106 0 0 30
Surr: DCAA 502 500.0 100 20 140 0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 16 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOLOOl>=S, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R85806
Sample ID 18061330-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 85806
Client ID: BatchQC
Batch ID: R85806
TestNo: SW9014
Analysis Date: 6/25/2018
SegNo: 1608659
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.74 0.500 10.00 0 97.4 81.6 122
Sample ID 18061330-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 85806
Client ID: BatchQC
Batch ID: R85806
TestNo: SW9014
Analysis Date: 6/25/2018
SegNo: 1608660
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.62 0.500 10.00 0 96.2 81.6 122 9.739 1.20 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 17 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOLOOl>=S, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R85806
Sample ID MB-R85806
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 85806
Client ID: PBW
Batch ID: R85806
TestNo: SW9014
Analysis Date: 6/25/2018
SegNo: 1608644
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R85806
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 85806
Client ID: LCSW
Batch ID: R85806
TestNo: SW9014
Analysis Date: 6/25/2018
SegNo: 1608645
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.91 0.500 10.00 0 99.1 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 18 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOLOOlfS, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#fafvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R85822
Sample ID 18061330-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 85822
Client ID: BatchQC
Batch ID: R85822
TestNo: SW9034
Analysis Date: 6/25/2018
SegNo: 1609030
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4630 25.0 4800 40.00 95.6 80 120
Sample ID 18061330-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 85822
Client ID: BatchQC
Batch ID: R85822
TestNo: SW9034
Analysis Date: 6/25/2018
SegNo: 1609031
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4740 25.0 4800 40.00 97.9 80 120 4630 2.35 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOL001fS, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#fafvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,-",.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R85822
Sample ID MB-R85822
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 85822
Client ID: PBW
Batch ID: R85822
TestNo: SW9034
Analysis Date: 6/25/2018
SegNo: 1609015
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R85822
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 85822
Client ID: LCSW
Batch ID: R85822
TestNo: SW9034
Analysis Date: 6/25/2018
SegNo: 1609016
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4660 25.0 4800 0 97.1 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 20 of 27

sumfoill Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOO17=3, INC Cuyahoga Falls, Ohio 44223
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com
QC SUMMARY REPORT
WO#: 18061305
24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R86179
Sample ID CHECK 7
SampType: LCS
TestCode: PH_S(9045D) Units: s.u.@22.3C
Prep Date:
RunNo: 86179
Client ID: LCSS
Batch ID: R86179
TestNo: SW9045D
Analysis Date: 7/9/2018
SegNo: 1623498
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.0 0 99.6
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
90 110
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 21 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOLOOlfS, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R86179
Sample ID CHECK 7
SampType: LCS
TestCode: PH_0IL(9045 Units: s.u.@22.2C
Prep Date:
RunNo: 86179
Client ID: LCSW
Batch ID: R86179
TestNo: SW9045D
Analysis Date: 7/9/2018
SegNo: 1622920
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.3 90 110
Sample ID 18070425-001ADUP
SampType: DUP
TestCode: pH_Oil(9045 Units: s.u.@22.9C
Prep Date:
RunNo: 86179
Client ID: BatchQC
Batch ID: R86179
TestNo: SW9045D
Analysis Date: 7/9/2018
SegNo: 1623459
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 5.4 0 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
5.3 0.7 10
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 22 of 27

mfoill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL TECHNOL001fS, INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Analyllaal 4ab#falvrie5 TEL: [phone] FAX.- [phone]
Website: http://n-m,n,.settek.com 24-Jul-18
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R86179
Sample ID LCS-R86179
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.8C
Prep Date:
RunNo: 86179
Client ID: LCSW
Batch ID: R86179
TestNo: SW9045D
Analysis Date: 7/9/2018
SegNo: 1622722
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Sample ID 18061704-005ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.8C
Prep Date:
RunNo: 86179
Client ID: BatchQC
Batch ID: R86179
TestNo: SW9045D
Analysis Date: 7/9/2018
SegNo: 1622724
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.9
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
6.8 0.4 5
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 27

sumfoill
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOOlfS, INC
Cuyahoga Falls, Ohio 44223
WO#: 18061305
Analyllaal 4ab#fafvrie5
TEL: [phone] FAX. [phone]
Website: http://n-m,n,.settek.com
24-Jul-18
Client:
Synagro
Project:
Oxford TCLP 2018
BatchID: R86713
Ignitability 7.41 7.240 0 102 70 130
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Sample ID 18070827-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 86713
Client ID: BatchQC
Batch ID: R86713
TestNo: SW1030
Analysis Date: 7/23/2018
SegNo: 1645848
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 24 of 27

sumfoill
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOL004ES, INC
Cuyahoga Falls, Ohio 44223
WO#: 18061305
Analyllaal 4ab#fafvrie5
TEL: [phone] FAX. [phone]
Website: http://n-m,n,.settek.com
24-Jul-18
Client:
Synagro
Project:
Oxford TCLP 2018
BatchID: R86713
Ignitability non-flammable 0 0 20
Sample ID 18070849-002ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 86713
Client ID: BatchQC
Batch ID: R86713
TestNo: SW1030
Analysis Date: 7/23/2018
SegNo: 1645852
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 25 of 27

AGQACOC338 Rev.0
EtF. ' Dates"ID O S
SUMMIT naiysig request 1 Chain of Custodyas10 r�nn sn.re4. For Summit Envlmnmental Technologies, Inc, use only
Guyal o nellk eMo A4743
�M wa .n
ge1of1
Page 26 of 27

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
F"VIRONME14TAL7ECHNOLAGJES,INQ. Cuyahoga Falls, Ohio44223 Sample Log -In Check List
—.... ArrafyNcal Lahpralor es TEL: [phone] FAX. [phone]
Website: http://`"-m,-",.settek.com
Client Name: SYN-NC-27028 Work Order Number: 18061305 RcptNo: 1
Logged by: Christopher Livengood 6/22/2018 10:20:00 AM '
Completed By: Christopher Livengood 6/22/2018 1:47:05 PM
Reviewed By: Jennifer Woolf 6/25/2018 12:30:58 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present?
Yes d❑
No ❑
NA ❑
4. Shipping container/cooler in good condition?
Yes d❑
No ❑
Custody seals intact on shipping container/cooler?
Yes ❑
No ❑
Not Present ❑d
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes V
No ❑
NA ❑
6. Were all samples received at a temperature of >0' C to 6.0°C
Yes V
No ❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
0
No ❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
V
No ❑
10. Was preservative added to bottles?
Yes
❑
No ❑
NA V
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑
No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No V
13. Does paperwork match bottle labels?
Yes
V
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No ❑
15. Is it clear what analyses were requested?
Yes
0
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑
NA V
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Additional sample rec'd on 7-13-18/10:25 via UPS in cooler w/ ice temp. of 4.2'
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
14.3
Goodl
Not Present
Page 27 of 27

SECTION 5

Facility Name: City of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NC0025054
Monitoring Period: From l/l/2020 To 3/31/2020
Pathogen Reduction (40 CFR 503-32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Ir ......Y.....M1., Fr ..11 ........ k:.,a n.—P--A !('lnec A nr Clove M o nlata tha fnild—Ina M""Unrina dafg•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Exece-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'
MPN
MPN/g
Coliform
power per gram
of total solids
18405
40908
88608
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
T explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Prepa�ame an itle (type or print)
ignature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Date:
Project:
Date Sample Rcvd:
Page 1Report
1/27/2020
Oxford
1/16/2020
Meritech Work Order #
01162036 Sample: Oxford 1 Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.58 %
1/21/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
25,316 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
01162037 Sample: Oxford 2 Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.63 %
1/21/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
18,405 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
01162038 Sample: Oxford 3 Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.64 %
1/21/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
42,683 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
01162039 Sample: Oxford 4 Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.58 %
1/21/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
88,608 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order # 01162040 Sample: Oxford 5 Grab 1/16/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.58 % 1/21/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 50,633 col/g dry wt 1/16/20 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Ryan Copeland Report Date: 1/27/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 1/16/2020
Meritech Work Order # 01162041 Sample: Oxford 6 Grab 1/16/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.57 % 1/21/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 50,955 col/g dry wt 1/16/20 130 col/g dry wt SM 9222D
Meritech Work Order # 01262042 Sample: Oxford 7 Grab 1/16/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.66 % 1/21/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 42,169 col/g dry wt 1/16/20 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Lbboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9/18 Chain of Custody Record (COC)
NPDES#:
Client: S`�!�Ni� Phone: �36 "�(�U�`'��19�
M ERITECH INC.
Address: Z�y o�� .�tp Fax:
ENVIRONMENTAL LABORATORIES
'�ot.1�SUI�CC N�- Email: �L��E� P SYAf4"C
i 642TamcoRd. Phone: [phone]
Project: 1yCL-0
. Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
p
Attention: `�PC� l.Onfrl3c44) Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es ADDIV
www.meritechiabs.com
Circle all that apply: Ema�l(preferred), Fax, Mail Std 10 s) 3s 2rs
Sampling Dates & Times
P g
Person Taking Sample (Sign/Print): �w ` �^
�r, M
Lab Use Only
Sample Location and/or ID #
Start
End
comp?
# of
Test(s) Required
On Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yes / No
Cl OK?
Z
37
3�
�q
o
Temperature Upon
Receipt:
Method of
*** Dechlorination
(<0.5 p m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
Shipment:
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes 0 No ❑
Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Hand Delivery
Relinquished by: Z� Date: i Time: )
I ' N o _ �1� ZL; �Z w
Received by: Date: Time:
Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab: Da Time:
Time:
�, r Lk

Contact: Ryan Copeland Report Date: 2/18/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 1/16/2020
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 01162051 Sample: Oxford Grab 1/16/20
Total Solids Volatile Solids % Volatile Solids
Week 1 0.980 0.630 0.646
Week 2
0.910
0.600
0.657
Week 3
0.810
0.520
0.645
Week 4
0.780
0.500
0.639
Week 5
0.730
0.470
0.644
Van Kleeck Reduction (%): 1.10
I hereby certify that I have reviewed and approve these data.
Lab rator Represent tive
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9/18 Chain of Custody Record (COC)
NPDES#:
Client: (, j,o�g(� p Phone: 336 - 6y7 -ggcl �
Address: L 2 Fax:
LOCfC UIL—L- I `— Email: VLCUPC1 w & S 'JtihGTw
Project: OXFOW
P.O.#:
Attention: Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es A I
Circle all that apply: E a (preferred), Fax, Mail Std 10 a s) 3 5 Da�rs z�rs
M E R I T E C H, INC.
ENVIRONMENTAL LABORATORIES
i 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
. Email: [e-mail]
WWW.merlteCillabS.COm
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): R _ �C�+A�" ,a � 1) q
r[
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test(s) Required
on Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
I
y5
C.
tF►=Lu E,Jr To ? v.
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples must be done in the field prior to preservation. ***
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes No ❑
Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Hand Delivery
Relinquished by: Date: ( Time: I Z, n
�� N �nE�A^ (It, Zu L
Received by: Date: Time:
❑ Other
—
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab:
Date: j �1nnTime: ->

%VS R
(older, more conservative method)
%VS in 0.6460 Enter in
VS out
t 0.6440 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 0.87
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in

1 � i 1 i I 1 I 1
Facility Name: City of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NCO025054
Monitoring Period: From 4/1/2020 To 6/30/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
rr _ _.1_ ..l.l.. 4....14.. ..a3., r..t ,,,7 f.-l.. A .... r'l— RN ..n ..lufn +h. f.11—. i4nrl eert tints•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61
MPN
MPN/g
Coliform
power per gram
of total solids
1113
2410
2919
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/I5A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. I
Option/Alt. 2
Option/Alt_ 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Prep r Nam d Title (type or print)
ignature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 4/14/2020
Project: Oxford
Date Sample Rcvd: 4/2/2020
Meritech Work Order #
04022067 Sample: Oxford 1 Grab
4/2/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
6.90 % 4/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,108 col/g dry wt 4/2/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
04022068 Sample: Oxford 2 Grab
4/2/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
6.90 % 4/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
1,713 col/g dry wt 4/2/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
04022069 Sample: Oxford 3 Grab
4/2/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
6.43 % 4/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,404 col/g dry wt 4/2/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
04022070 Sample: Oxford 4 Grab
4/2/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
6.22 % 4/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,923 col/g dry wt 4/2/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
04022071 Sample: Oxford 5 Grab
4/2/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
5.71 % 4/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,866 col/g dry wt 4/2/20
130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 04022072 Sample: Oxford 6 Grab
Parameters Results Analysis Date
% Total Solids 6.78 % 4/7/20
Fecal Coliform (Sludge) 2,682 col/g dry wt 4/2/20
Page 2
Report Date: 4/14/2020
Project: Oxford
Date Sample Rcvd: 4/2/2020
4/2/20
Reporting Limit Method
0-100 % SM 2540B
130 col/g dry wt SM 9222D
Meritech Work Order # 04022073 Sample: Oxford 7 Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 7.22 % 4/7/20 0-100 %
Fecal Coliform (Sludge) 2,959 col/g dry wt 4/2/20 130 col/g dry wt
4/2/20
Method
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data. n(JLX, d=CzJU
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016
Chain of Custody Record (COC)
NPDES#:
Client: Phone: ��'(- gyp
r
Address: ��'�A I.7tt1-0- �O� Fax:
e��u�,hJil.l�t �� Email:
Project:
P.O.#:
Attention: Turn Around Time*
�_,l � tNn
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emai (preferred), Fax, Mail Stcl 10 a s) s 24�s
--_.l
M ERITECH1 INC.
C
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): ��, rr'
Lab Use Only
Start
End
comp?
Grab?
# of
Cont.
Test(s)
Required
On Ice? Yes
/ No
pH OK?
Cl OK?
Date
Time
Date
Time
ox o a
z 'Z�
��
- - L- 7
4
5
1\
Temperature Upon Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
UPS
Q, Fed Ex
Are these results for regulatory purposes? Yes No Chi
Report results in: mg/L
❑ mg/kg
�Jlu�g#
EJ ug/L El
Hand Delivery
Relinquished by: Date: Time: `
Ise o { ti l0 1
v ,
Received by:
Date:
Time:
Other
Relinquished by: Date: Time:
Received by:
Date:
Time:
Relinquished by: Date: Time:
eceived b b: ate: C
Tim G
M

Contact: Ryan Copeland Report Date: 5/4/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 4/2/2020
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 04022066 Sample: Oxford Grab 4/2/20
Total Solids Volatile Solids % Volatile Solids
Week 1 1.13 0.600 0.534
Week 2
Week 3
Week 4
1.13
0.940
1.24
Week 5 1.15
Van Kleeck Reduction (%): -16.98
� ..
IN-MI7
0.700
/1101111
I hereby certify that have reviewed and approve these data.
0.584
0.655
0.566
0.573
*La"oraory"Repre&saenta`tive�
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9 2016
Chain of Custody Record (COC)
_ NPDES#:
Client: -2'jN�? Phone: 3♦J"VU�'yyy
MERITECH INC,
Address: 2?�A Soiry- Rr om Fax:
ENVIRONMENTAL LABORATORIES
ti��� N W LLIr I��
V 1 v Email:-
642 Tamco Rd. Phone: [phone]
Project: t/appp
•ktReidsville
NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: 1h'(-,Ui
Turn Around Time*
How would you like your report sent? *RUSH
work needs prior approval.
WWW.merlteCillabS.COm
Circle all that apply: Email referred), Fax, Mail Std 10
s)s zs
�-J
Sampling Dates &Times
Person Taking Sample (Sign/Print):
�•`�w ❑PuVvq'0
Lab Use Only
Sample Location
and/or ID # Start End
Date Time
Comp?
# of
Test (s ) Required
On Ice? Yes
pH OK?
Date Time
Grab?
Cont.
/ No
CI OK?
�NL
il)EtJLIJ (a
AYAI�� C"YFWE
L1,Z�Zu
.�S�iM
L
I
�� LJJc r
DJL\)T I D fJ
T—T
Temperature Upon Receipt:
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Shipment:
Comments:
Compositor #
a UPS
❑ Fed Ex
Are these results for regulatory purposes? Yes
No ❑ Report results in: mg/L I mg/kg
Jug #
❑ ug/L
Fj Hand Delivery
Relinquished by: P Date: Time:
l � J��e1AOD Z
` Received by: Date:
Time:
Other
Relinquished by: Date: Time:
I�..�
Received by: Date:
Time:
Relinquished by: Date: Time:
ceived by 16ate:
:qz' v
i
G�

%VS R
(older, more conservative method)
%VS in 0.5340 Enter in
VS out
t 0.5730 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= -17.10
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in

Facility Name: City of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NCO025054
Monitoring Period: From 7/1/2020 To 9/30/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tr..—19,..,1.1.. t., ..lto...,nti..n —f--A hr'l— A — I) c i21 n mnlntu tha fnlln. A..—itnrina rinta-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Gen. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61b
MPN
MPN/g
Coliform
power per gram
of total solids
297
310
325
CFU/g
0
4/Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis WWTP Superintendent
Prep me and T' e (type or print)
11
i ature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Page 1
Contact: Ryan Copeland Report Date: 7/20/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 7/9/2020
Meritech Work Order #
07092062 Sample: Oxford 1 Grab
7/9/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.06 % 7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<297 col/g dry wt 7/9/20
297 col/g dry wt
SM 9222D
Meritech Work Order #
07092063 Sample: Oxford 2 Grab
7/9/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.04 % 7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<299 col/g dry wt 7/9/20
299 col/g dry wt
SM 9222D
Meritech Work Order #
07092064 Sample: Oxford 3 Grab
7/9/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.80 % 7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<325 col/g dry wt 7/9/20
325 col/g dry wt
SM 9222D
Meritech Work Order #
07092065 Sample: Oxford 4 Grab
7/9/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.92 % 7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<311 col/g dry wt 7/9/20
311 col/g dry wt
SM 9222D
Meritech Work Order #
07092066 Sample: Oxford 5 Grab
7/9/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.81 % 7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<323 col/g dry wt 7/9/20
323 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Ryan Copeland Report Date: 7/20/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 7/9/2020
Meritech Work Order # 07092067 Sample: Oxford 6 Grab 7/9/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.94 % 7/14/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <309 col/g dry wt 7/9/20 309 col/g dry wt SM 9222D
Meritech Work Order # 07092068 Sample: Oxford 7 Grab 7/9/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.95 % 7/14/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <308 col/g dry wt 7/9/20 308 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. 4ozz'&
aboratory Rep res tative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8r9r18 Chain of Custody Record (COC)
NPDES#:
S�Nac
MERITECH INC.
Client: Phone:
1
Address: Z,gU f?O&E(L f >r'o Fax:
ENVIRONMENTAL LABORATORIES
I/V10LV-S1JiLi6 ILL Email: 2 oeF-L rn L SYNAc4-0 ,ice
i 642 Tamco Rd. Phone: [phone]
Project: Dii'FOM
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: r YAN Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es Aoolv
www.meritechlabs.com
Circle all that apply: Ema'I(preferred), Fax, Mail Stcl 10d s) 3-5 Da�rs 1 24L---J48Hrs
Sampling Dates & Times
Person Taking Sample (Sign/Print): �%� hr`+ C-f'$Ar�`
T''I
Lab Use Only/
Sample Location and/or ID #
Start
End
Com ?
p
#of
on Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Test(s)
Required
Yes / No
Cl OK?
yy
/
FeLAL
lll� G'M
Z
j
ca
t�
I
y
jl'L?(Lo 3o Oh`(
1 rUW E(fFLUC
50 AM
n` O�Ji l lil �J
l f
Temperature Upon
Receipt:
*** Dechlorination
***
Method of
(<0.5 pp of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Shipment:
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes No
Report results in: mg/L ❑ mg/kg ❑ ug/L El
Hand Delivery
Time:
Relinquished by: Date: �, /y•
��{v
'`'/rJ G(�f� 7��j
Received
Rived b . Date: Time:
y
❑ Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
a ^IJate: i
lip

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland ReportDate: 8/13/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 7/9/2020
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 07092069 Sample: Oxford Grab 7/9/20
Total Solids Volatile Solids % Volatile Solids
Week 1 0.890 0.520 0.578
Week 2
0.960
0.600
0.624
Week 3
1.01
0.620
0.605
Week 4
1.07
0.620
0.581
Week 5 1.07
Van Kleeck Reduction [%]: -9.07
0.640
I hereby certify that I have reviewed and approve these data.
0.599
pz&—
Labordtory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

019/16 Chain of Custody Record (COC) NPDES#:
1
M E R ITE C H, INC. client: Phone:
Address: Fax:
ENVIRONMENTAL LABORATORIES :, I: , Email.
i 642 Tamco Rd. Phone; 336-342-4748 Project: i I !'
Reidsville NC 27320 Fax: [phone] P.O.#:
Email: [e-mail] Attention: � ��- �.> (:,; , , rt �,��1 r;
Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es a I
Www.meritechlabs.eom 1 Std 10d s) 3-5 nay5 Z�rs
Circle all that apply: I'{preferredJ, Fax, Mail II_��
Sampling Dates & Times Person Taking Sample [Sign/PrintJ: l Lab Use Only
Sample Location and/or ID # Start End
comp? #of Test(s) Required les N pH ?
Date Time Date Time Grab? Cont. Yes / No Cl OK?
I
l
l
Temperature upon
Receipt:
Method of *** Dechlorination (<0,5 p m) of Ammonia, Cyanide, Phenol and TKN samples done in the field prior to resrvatl
Comments: Compositor #e
Shipment:
❑ up
Jug #
❑ , Fed Ex Are these results for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Relinquished by: Date; Time: Received b Hand Delivery i . r � � ;+ I . Y� bate: Time:
❑ Other Relinquished by: Date: Time: Received by: Date: Time:
Relinquished by: Date: Time: �qceivedgF ab: -j ate: Ti
l; I ••Dl�

%VS R
(older, more conservative method)
%VS in 0.5780 Enter in
VS out
t 0.5990 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR=
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in

Facility Name: City Of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPIDES Number: NC 0025054
Monitoring Period: From 10/1/2020 To 12/31/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 021.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l /A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
,s ....,.+....,+.,.,....+Sa... ,..,..,:.8..., 0.1 !t''l.. o A ...- Cl... M .. ntnto th.. fnilnavinn ,nnnitnrinff alai-•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 66
MPN
MPN/g
Coliform
power per gram
of total solids
214
239
312
CFU/g
0
4 /Yr
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis WWTP Superintendent
Prepa me and itle (type or print)
ignature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Prepares is defined in 40 CFR Part 5039(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 10/16/2020
Project: Oxford
Date Sample Rcvd: 10/8/2020
Meritech Work Order #
10082043 Sample: Oxford 1 Grab
10/8/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.85 %
10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<236 col/g dry wt
10/8/20
236 col/g dry wt
SM 9222D
Meritech Work Order #
10082044 Sample:
Oxford 2 Grab
10/8/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
2.91 %
10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<312 cal/g dry wt
10/8/20
312 col/g dry wt
SM 9222D
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
10082045 Sample: Oxford 3 Grab
Results Analysis Date
3.79 % 10/9/20
<240 col/g dry wt 10/8/20
Reporting Limit
0-100 %
240 col/g dry wt
10/8/20
Method
SM 2540B
SM 9222D
Meritech Work Order #
10082046 Sample: Oxford 4 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.91 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<232 col/g dry wt 10/8/20
232 col/g dry wt
SM 9222D
Meritech Work Order #
10082047 Sample. Oxford 5 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
4.08 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<223 col/g dry wt 10/8/20
223 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
teI.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 10082048 Sample: Oxford 6 Grab
Parameters Results Analysis Date
% Total Solids 4.01 % 10/9/20
Fecal Coliform (Sludge) <227 col/g dry wt 10/8/20
Meritech Work Order # 10082049 Sample: Oxford 7 Grab
Parameters Results Analysis Date
% Total Solids 4.25 % 10/9/20
Fecal Coliform (Sludge) <214 col/g dry wt 10/8/20
Page 2
Report Date: 10/16/2020
Project: Oxford
Date Sample Rcvd: 10/8/2020
10/8/20
Reporting Limit Method
0-100 % SM 2540E
227 col/gdry wt SM9222D
10/8/20
Reporting Limit Method
0-100 % SM 2540E
214 col/gdry wt SM9222D
I hereby certify that have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

$�971e
Chain of Custody Record (COC)
NPDES#:
M E R (TECH, INC.
Client: Phone:
Address: S13q uywa, om Fax:
ENVIRONMENTAL LABORATORIES
n
U �LGc IBC, Email: Ve-oPE A&
642 Tamco Rd. Phone: [phone]
Project:_QXRAQ
'A"
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: info@ meritechlabs.com
Attention: Y ND
Turn Around Time*
How would you like your report sent?
*RUSH work needs prior approval,
WWW.rYleritechlabs.com
C iar es A I v
Circle all that apply Emai (preferred), Fax, Mall 5td is s} 3._5 Days 2s
Sampling Dates & Times
Person Taking Sample (Sign/Print): !`-f AM
Lab Use Only
Sample Location and/or ID # Start End
Date
Comp? #of Test(s) Required
On Ice? pH OK?
Time Date Time
Grab? Cont.
Yes / No Cl OK?
r0Y /w
rem (.-rr0'J
2LVA
3Lis,
S
)
Temperature Upon
Method of
° "* Dechlorination (<0.5 pin) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Receipt:
Shipment:
Comments:
Compositor #
UPS
Jug #
❑ Aed Ex
Are these results for regulatory purposes? Yes LV
No ❑ Report results in: mg/L ❑
mg/kg ❑ ug/L
Hand Delivery
Relinquished by: [ Date: Time;
�r\/ � �(7�g-�
Rived b
Received y:
Date: Time;
❑ Other
Relinquished by; Date: Time;
Received by:
Date: Time:
Relinquished by; Date: Time;
Rec ' by ab: G
Q t : G Z e:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Ryan Copeland Report Date: 11/11/2020
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 10/8/2020
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 10082050 Sample: Oxford Grab 10/8/20
Total Solids Volatile Solids % Volatile Solids
Week 1. 1.46 0.800 0.551
Week 2 1.32 0.740 0.561
Week 3 1.59 0.880 0.556
Week 4 1.44 0.800 0.555
Week 5 1.60
Van Kleeck Reduction (%): 8.59
I hereby certify that I have reviewed and approve these data.
0.529
Laboratory Representative
642 Tannco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC) NPDES#:
Client: Phone:
M E R IT E C H, INC. Address: Z &a& &/�o Fax:
ENVIRONMENTAL LABORATORIES a LLE Email: I`L0p6VV11 GS i
642 Tamco Rd. Phone: [phone] ����
Project: _
Reidsville NC 27320 Fax: [phone] P.O.#:
Email: [e-mail] Attention: m (-nPE(^M Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es Anni
WWw.I"1"leritechlabs,COIYI Circle all that apply: 0ma(preferred), Fax, Mail std a.o s) 3 5 Da s 24-48Hrs
Sampling Dates & Times person Taking Sample (Sign/Print):
p g � Lab Use Only
Sample Location and/or iD # Start End
Comp? #of Test(s) Required On Ice? pH CI OK?
Date Time pate Time Grabs Cont. �f s / No 7
1 �r FL.V l` rL
Temperature Upon
Receipt:
Method o� *** Dechlorination <0.5 p m of Ammonia, Cyanide, Phenol and TKN sam les must be done In the field prior to reservation. *** a o
Shipment: Comments: Compositor #
Ll ups
!ug #
U Fed Ex Are these results for regulatory purposes? Yes No L7 Report results in: mg/L 0 mg/kg 0 ug/L
Hand Delivery Relinquished by: ,/—C �p Date:`'0_evTime: 0. Received by: Date: Time:
Q Other Relinquished by: Date: V Time; Received by: Date: Time:
Relinquished by: Date: Time: R ved Lab:

%VS R
(older, more conservative method)
%VS in 0.5510 Enter in
VS out
t 0.5290 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 8.48
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in

SECTION 6

Agricultural Lime Application Log
Year: 2020
Project: OXFORD
Field
(state -county -site -field code) I
Soil pH
Lime Requirement
I (from soil analysis)
Tons/Acre
Applied 11
Date Applied
NC-GR-60-2 IF-7-771
0.0 tons/ac.
NC-GR-60-5 6.6 0.0 tons/ac.
NC-GR-60-6 6.8 0.0 tons/ac.
0.1 tons/ac.
0.1 tons/ac.
0.0 tons/ac.
0.3 tons/ac.
0.3 tons/ac.
0.0 tons/ac.
1.0 tons/ac.
0.7 tons/ac.
0.8 tons/ac.
0.4 tons/ac.
0.0 tons/ac.

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL017497
Client: Jake Isley
Advisor:
Ryan Copeland
vo- Predictive
4520 Townsville Rd
SYNAGRO
Bullock, NC 27507
284 Boger Road
.'..,$' Soil Report Mehlich-3 Extraction
Mocksville, NC27028
Sampled County: Granville
Links to Helpful Information
Client ID: 451747
Advisor
ID: 499503
Sampled: Received: 11/25/2020 Completed: 01/13/2021 Farm: GR-60
Sample ID: GR602
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 30
100 0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.51 0.98 11.6 93 0.8 6.7 48 18 65 27
35
1238 750
295
295
256
0.1 1
Sample ID: GR605
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
100 0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.46 1.01 11.1 92 0.9 6.6 122 19 65 26
30
2016 1217
647
647
268
0.1 1
Sample ID: GR606
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
100 0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 0.94 13.8 94 0.9 6.8 178 21 68 25
37
1586 957
1046
1046
424
0.2 1
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO17497
Jake Isley
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm