WQ0006101_Residual Annual Report 2020_20210224

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0006101
Applicant/Permittee City of Dunn
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide inforration on the person to be contacted by N B Staff
Name * Lysa Finnerty
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
14105376150
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00006101
Fbs Current Existing perrrit number
Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220
Facility Name * City of Dunn RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report for City of Dunn WWTP NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form} Engineering Fans, Specifications, Calculations, Bc.)
Dunn WWTP NC 2020 Annual Report FINAL.pdf 7.67MB
upload only 1 F3Fdocurrent (less than 250 MB). Multiple documents rust be corrbined into one F7Ffile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/24/2021

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 24, 2021
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report for Permit No. WQ0006101
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Dunn, NC.
If you have any questions or need additional information, please do not hesitate to contact
Heather Adams at [phone] or Matthew Carter at [phone].
Sincerely,
0-017 ". -NJ01 _ I t
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Heather Adams — City of Dunn
Matthew Carter - Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF DUNN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006101
2020 ANNUAL REPORT

City of Dunn, NC
Residuals Land Application Program
2020 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WQ0006101 County Harnett Year 2020
Facility Name (as shown on permit) Dunn W WTP & City of Dunn WTP NPDES No. NC0043176, 03-43-010
Land Application Operator S} nagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO, If NO, skip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
"Total number of application fields in the permit: 19
Total number of fields utilized for land application during the year: 11
Total amount of dry tons applied during the year for all application sites: 347.99
Total number of acres utilized for land application during the year: 100.70
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
I. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 1SA NCAC 02T .I105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." J
Heather Adams Utilities Director
Permittee Name and Title (type or print)
Signature of Preparer* Date Signwre of Land AppVr . Date
(if different from Permittee) (ii' different from Permittee and Preparer)
*Preparer is defined in 40 CPR Part 5039(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
DUNN, NC
DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
March 2020
September 2020
TOTAL
DUNN, NC WTP LIQUID
MONTH/YEAR
April 2020
August 2020
September 2020
TOTAL
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
657,200.00 G 66.59 D 60.40
719,200.00 G 72.88 D 66.10
1,376,400.00 G 139.47 D 126.50
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
483,600.00
G
86.51
D
78.47
483,600.00
G
86.51
D
78.47
198,400.00
G
35.49
D
32.19
1,165, 600.00
G
208.52
D
189.13
Report Date: 2/9/2021 2:55:23 PM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0006101 Laboratory:
Facility Name: DUNN, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO043176
WWTP Name: DUNN WWTP
Residual Analysis Data
Product Type
Sample or Composite Date
AEDLIQ
01/15/20
Parameter (mg/kg dry weight)
Ceiling Cone.
Limit
Percent Solids (°lo)
NA
2.43
Arsenic
75
<20.8
Cadmium
85
<4.17
Copper
4300
294
Chromium
NA
36.5
Lead
840
55
Mercury
57
1.55
Molybdenum
75
<10.4
Nickel
420
16.5
Selenium
100
<20.8
Zinc
7500
613
Total Phosphorus
NA
21500
TKN
NA
68800
Ammonia -Nitrogen
NA
6210
Nitrate and Nitrite
NA
1490
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer' Date
`Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/9/2021 2:55:51 PM For: 2188 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0006101
Facility Name: DUNN, NC
Residual Source
NPDES # or WQ#: NCO043176
WWTP Name: DUNN WWTP
Residual Analysis Data
Product Type
AEDLIQ
Sample or Composite Date
01/15/20
Parameters (mg/kg dry weight)
Aluminium
15000
Calcium
9290
Magnesium
2890
pH (s.u.)
5.90
Potassium
4460
Sodium
2000
PAN
23345
SAR (Ratio)
0.7218
Laboratory:
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/9/2021 2:67:10 PM For: 2188 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
1 /24/2020
Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-016-0008
Project Description: Dunn WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/16/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�a f• c•—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-016-0008
Client Project Description: Dunn WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-4500-NH3C
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
9045D
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
4500NO3F-2011
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
6010D
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
SW-7471B
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-4500-NH3C-TKN
WP
MTN
70186
Dunn WWTP
Solids
01/15/2020
01/16/2020
SM-2540G
WP
MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

i
Waypoint.:
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46789
Synagro Central LLC/ Dunn
Mary Brewer
Project
Dunn
WWTP
Report Date : 01/24/2020
284 Boger Road
Information :
Received : 01/16/2020
Mocksville , NC 27028
Pam« mL 60wr
Pauric McGroary
Report Number : 20-016-0008
REPORT OFANALYSIS
Agronomist
Lab No : 70186
Matrix:
Solids
Sample ID: Dunn WWTP
Sampled:
1/15/2020 0:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
97.6
%
0.010
1
01/21/2016:44
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
6210
mg/Kg -
dry
4170
1
01/23/20 13:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
1490
mg/Kg -
dry
199
1
01/23/20 13:37
ZBD 4500NO3F-2011
Organic N
62500
mg/Kg -
dry
10400
1
01/23/20 10:00
CALCULATION
pH
5.9
S.U.
1
01/22/20 06:20
JSL 9045D
Total Solids
2.43
%
0.010
1
01/21/20 16:44
ADM SM-2540G
Total Kjeldahl Nitrogen
68800
mg/Kg -
dry
10400
1
01/23/20 10:00
JPJ ;M-4500-NH3C-TKl`
Phosphorus
21500
mg/Kg -
dry
208
1
01/21/20 16:45
BKN 6010D
Aluminum
15000
mg/Kg -
dry
208
1
01/21/20 16:45
BKN 6010D
Arsenic
<20.8
mg/Kg -
dry
20.8
1
01/21/20 16:45
BKN 6010D
Calcium
9290
mg/Kg -
dry
1040
1
01/21/20 16:45
KKM 6010D
Cadmium
<4.17
mg/Kg -
dry
4.17
1
01/21/20 16:45
BKN 6010D
Chromium
36.5
mg/Kg -
dry
10.4
1
01/21/20 16:45
BKN 6010D
Copper
294
mg/Kg -
dry
10.4
1
01/21/20 16:45
BKN 6010D
Iron
28400
mg/Kg -
dry
208
1
01/21/20 16:45
BKN 6010D
Lead
55.0
mg/Kg -
dry
12.5
1
01/21/20 16:45
BKN 6010D
Magnesium
2890
mg/Kg -
dry
208
1
01/21/20 16:45
BKN 6010D
Manganese
261
mg/Kg -
dry
20.8
1
01/21/20 16:45
BKN 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

i
Waypoint.:
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46789
Synagro Central LLC/ Dunn
Mary Brewer
Project
Dunn WWTP
Report Date : 01/24/2020
284 Boger Road
Information :
Received : 01/16/2020
Mocksville , NC 27028
Pam« mL 60wr
Pauric McGroary
Report Number : 20-016-0008
REPORT OFANALYSIS
Agronomist
Lab No : 70186
Matrix: Solids
Sample ID: Dunn WWTP
Sampled: 1/15/2020 0:00
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
1.55
mg/Kg
- dry
0.633
1 01/20/20 13:24 TJS SW-7471B
Molybdenum
<10.4
mg/Kg
- dry
10.4
1 01/21/20 16:45 BKN 6010D
Nickel
16.5
mg/Kg
- dry
10.4
1 01/21/20 16:45 BKN 6010D
Potassium
4460
mg/Kg
- dry
208
1 01/21/20 16:45 BKN 6010D
Selenium
<20.8
mg/Kg
- dry
20.8
1 01/21/20 16:45 BKN 6010D
Sodium
2000
mg/Kg
- dry
1040
1 01/21/20 16:45 BKN 6010D
Zinc
613
mg/Kg
- dry
52.1
1 01/21/20 16:45 BKN 6010D
Sulfur
10700
mg/Kg
- dry
208
1 01/21/20 16:45 BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 2-4237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46789
Customer Name: Synagro Central LLC/ Dunn
Report Number: 20-016-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 01/16/2020 12:09:22
Page 5 of 6

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Page 6 of 6

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0006101 Laboratory:
Facility Name: DUNN, NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source WQ # or Inc.
NPDES#:
WWTP Name: DUNN WTP
Residual Analysis Data
Product Type
Sample or Composite Date
WPL
02/18/20
WPL
04/06/20
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
13.00
4.29
Arsenic
75
5.27
9.4
Cadmium
85
<0.769
<0.48
Copper
4300
33
48
Chromium
NA
24.8
42
Lead
840
14.2
15
Mercury
57
<0.121
<0.4
Molybdenum
75
<1.92
5.3
Nickel
420
11.2
16
Selenium
100
<3.85
3.3
Zinc
7500
60.8
77
Total Phosphorus
NA
838
1500
TKN
NA
4620
6500
Ammonia -Nitrogen
NA
<769
230
Nitrate and Nitrite
NA
<37.2
15.1
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, t this docu nt was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathere devaluated e information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and ' r"sonment for kp6wing violations."
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/9/2021 2:56:39 PM For: 2188 02

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0006101
Facility Name: DUNN, NC
Residual Source
NPDES # or WQ#:
WWTP Name: DUNN WTP
Residual Analysis Data
Laboratory:
PACE ANALYTICAL; Waypoint Analytical Virginia
Inc.
Product Type
WPL
WPL
Sample or Composite Date
02/18/20
04/06/20
Parameters (mg/kg dry weight)
Aluminium
48500
130000
Calcium
908
1100
Magnesium
1670
1700
pH (s.u.)
5.90
6.00
Potassium
1130
1600
Sodium
<192
1100
PAN
<2270
2638
SAR (Ratio)
0.3133
0.9989
"I certify, under penalty of w, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly g r d and evalu ted the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fine nd i priso�ment r knowing violations."
gnature of P arer ` Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/9/2021 3:23:28 PM For: 2188 02 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
2/28/2020
Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-051-0003
Project Description: Dunn WTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/20/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-051-0003
Client Project Description: Dunn WTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
70533
Dunn WTP
Solids
02/18/2020
09:00
02/20/2020
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

�'
WayP
7621
Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46789
Synagro Central LLC/ Dunn
Melvin
Goad
Mary Brewer
Project
Dunn
WTP
Report Date : 02/28/2020
284 Boger Road
Information :
Received : 02/20/2020
Mocksville , NC 27028
P��G mL 60wr
Submitted By : Melvin Goad
Pauric ry
Report Number : 20-051-0003
REPORT OFANALYSIS
Agronomist
Lab No : 70533
Matrix:
Solids
Sample ID: Dunn WTP
Sampled:
2/18/2020 9:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
87.0
%
0.010
1
02/25/2017:02
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
<769
mg/Kg -
dry
769
1
02/27/20 13:30
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<37.2
mg/Kg -
dry
37.2
1
02/24/20 13:42
ZBD 4500NO3F-2011
Organic N
4620
mg/Kg -
dry
1920
1
02/27/20 10:30
CALCULATION
pH
5.9
S.U.
1
02/26/20 06:51
JSL 9045D
Total Solids
13.0
%
0.010
1
02/25/20 17:02
ADM SM-2540G
Total Kjeldahl Nitrogen
4620
mg/Kg -
dry
1920
1
02/27/20 10:30
JPJ ;M-4500-NH3C-TKI`
Phosphorus
838
mg/Kg -
dry
38.5
1
02/24/20 17:25
KKM 6010D
Aluminum
48500
mg/Kg -
dry
38.5
1
02/24/20 17:25
KKM 6010D
Arsenic
5.27
mg/Kg -
dry
3.85
1
02/24/20 17:25
KKM 6010D
Calcium
908
mg/Kg -
dry
192
1
02/24/20 17:25
KKM 6010D
Cadmium
<0.769
mg/Kg -
dry
0.769
1
02/24/20 17:25
KKM 6010D
Chromium
24.8
mg/Kg -
dry
1.92
1
02/24/20 17:25
KKM 6010D
Copper
33.0
mg/Kg -
dry
1.92
1
02/24/20 17:25
KKM 6010D
Iron
22100
mg/Kg -
dry
38.5
1
02/24/20 17:25
KKM 6010D
Lead
14.2
mg/Kg -
dry
2.31
1
02/24/20 17:25
KKM 6010D
Magnesium
1670
mg/Kg -
dry
38.5
1
02/24/20 17:25
KKM 6010D
Manganese
838
mg/Kg -
dry
3.85
1
02/24/20 17:25
KKM 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

�'
WayP
7621
Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46789
Synagro Central LLC/ Dunn
Melvin Goad
Mary Brewer
Project
Dunn WTP
Report Date : 02/28/2020
284 Boger Road
Information :
Received : 02/20/2020
Mocksville , NC 27028
P��G mL 60wr
Submitted By : Melvin Goad
Pauric ry
Report Number : 20-051-0003
REPORT OFANALYSIS
Agronomist
Lab No : 70533
Matrix: Solids
Sample ID: Dunn WTP
Sampled: 2/18/2020 9:00
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
<0.121
mg/Kg
- dry
0.121
1 02/24/20 15:15 TJS SW-7471B
Molybdenum
<1.92
mg/Kg
- dry
1.92
1 02/24/20 17:25 KKM 6010D
Nickel
11.2
mg/Kg
- dry
1.92
1 02/24/20 17:25 KKM 6010D
Potassium
1130
mg/Kg
- dry
38.5
1 02/24/20 17:25 KKM 6010D
Selenium
<3.85
mg/Kg
- dry
3.85
1 02/24/20 17:25 KKM 6010D
Sodium
<192
mg/Kg
- dry
192
1 02/25/20 12:20 KKM 6010D
Zinc
60.8
mg/Kg
- dry
9.62
1 02/24/20 17:25 KKM 6010D
Sulfur
2480
mg/Kg
- dry
38.5
1 02/24/20 17:25 KKM 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46789
Customer Name: Synagro Central LLC/ Dunn
Report Number: 20-051-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 02/20/2020 13:02:02
Page 5 of 6

fib' i
A 1lllllllllllll�lllll� 6225¢23
1111111111��111� 48
11l�lllll Svnadso CenSraV V_LG; Dunn
p� A� Riohmnr4 Dunn WTP rl� �
to" ow ft
0766 f wwrnrrrrd
�1
� v / . ' - .� � I • tom" � ]y g --- wrrn-irw�
�. p""Re
00 CN, - a PH JM
tilft"WIh
1 � ,
copper and Eno '
k' S cie-:- ,
Page 6 of 6

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Melvin Goad
Project Name: Dunn WTP NC
Project Number: #2188
Lot Number:VD07020
Date Completed:04/14/2020
04/17/2020 12:54 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VD07020
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Phosphorus
The method blank for analytical batch 50964 contained the phosphorus greater than the acceptance
criteria. The associated sample contained detections for this analyte at concentrations greater than 1 OX
the value found in the method blank; therefore sample results are not impacted. The data has been
reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VD07020-001
Description: Dunn NC WTP Matrix: Solid
Date Sampled:04/06/2020 0900 % Solids: 4.29 04/08/2020 0043
Date Received:04/07/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 04/08/2020 0043 MOM
50147
1 350.1
(Ammonia - N ) 350.1
1 04/13/2020 1310 SLC
50851
1
(Nitrate - N ) 9056A
1 04/09/2020 1911 HKL
50610
1
(Nitrite - N ) 9056A
1 04/09/2020 1911 HKL
50611
1
(Phosphorus) 365.1
2 04/13/2020 1631 DMA
04/13/2020 1215
50872
1
(Soil pH meas) 9045D
1 04/09/2020 2129 SRB
50573
1 351.4
(TKN) 351.2
1 04/14/2020 1429 DMA
04/14/2020 0940 50881
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.29
%
1
Ammonia - N (gas diffusion)
350.1
230
23
12
mg/kg
1
Nitrate - N (soluble)
9056A
13
12
0.57
mg/kg
1
Nitrite - N (soluble)
9056A
2.1 J
4.7
0.45
mg/kg
1
Phosphorus
7723-14-0 365.1
1500
230
47
mg/kg
1
Soil pH measured in water @
21.5 ° C
9045D
6.0
su
1
TKN
351.2
6500
580
580
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 04/10/2020 1210 KSH2
04/10/2020 0300
50363
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
1.7
0.40
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 04/09/2020 1746 KSH2
04/08/2020 1523 50361
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
130000
150
57
mg/kg
1
Arsenic
7440-38-2 6010D
9.4
5.7
1.9
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.9
0.48
mg/kg
1
Calcium
7440-70-2 6010D
1100 J
1900
240
mg/kg
1
Chromium
7440-47-3 6010D
42
3.8
0.95
mg/kg
1
Copper
7440-50-8 6010D
48
3.8
1.7
mg/kg
1
Iron
7439-89-6 6010D
31000
38
17
mg/kg
1
Lead
7439-92-1 6010D
15
3.8
1.7
mg/kg
1
Magnesium
7439-95-4 6010D
1700 J
1900
240
mg/kg
1
Manganese
7439-96-5 6010D
1500
5.7
2.2
mg/kg
1
Molybdenum
7439-98-7 6010D
5.3 J
15
3.8
mg/kg
1
Nickel
7440-02-0 6010D
16
15
4.0
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VD07020-001
Description: Dunn NC WTP Matrix: Solid
Date Sampled:04/06/2020 0900 % Solids: 4.29 04/08/2020 0043
Date Received:04/07/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 04/09/2020 1746 KSH2
04/08/2020 1523 50361
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
1600 J
1900
240
mg/kg
1
Selenium
7782-49-2 6010D
3.3 J
7.6
3.1
mg/kg
1
Sodium
7440-23-5 6010D
1100 J
1900
240
mg/kg
1
Zinc
7440-66-6 6010D
77
19
4.7
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
F.
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Strati, Crvir4:ili:anr=I S rvices, lot,
QOPLurtcmNuinLerUaL)]W.-Id Pip
Sample Receipt Checklist (SRC) l I1btLivC�:¢:$'b�1L$
Client: Sy'nagrk, CoolerIrtSPeetetiby,'daJC ,1)7,'Mil) �
���` � 0$4oC �: 'D670?Q
11pleant of*eraint: ❑ '. LEI C[iolrt t�t}S ❑ FedlSx tither;
0 Yes No 1. �4'ere ra .dy 5�� is present an i1e� —
Yns Igo NA 2- If Cu�bdu sc�Js wtr� tSre��srtt ulcer th ill rind llnbmken�
pH Strip lll: 1�1A ChIorirc Strip IDz N _ Ceslyd by-
[irrgma[ te�nlx�, rurc upon rceaiprl ]7a [ve i {Cor,xxted} tern,]OMPArc upon receipt °foSolid Ana LuD ] -203
�! i�lA ,+7.a h'A rJ,q �[ lV }tlA u P p I
lvJelhod, ❑ry'cmperaFufe Blank IZIAgainm i3otrJta IR Gate Ill 3. !>t {`,air Carcttion FaCtilr: G °C
Method Cr Cr,pla.11t' ® %VCt lice ❑ le- Packs d Due Ice O Nona
Yes [I No MINA
3, IFtcm eMM1111 Oran Coo0'l=rexroeded 6.C,'�as PI'Vicet M2nager lqi tifie�D
f'h+I was Notified � t ,
by, 13 C'no J pilail . fine {e irol One).
l Ye3 ❑ No it NA a. Is rltx commercial eau:•ier's pacAin� sli a�acllecE to this forr_t?
Ycs. No 5. are roper u,sfody proced ,ms (relinquishcdlieuGivcd)fnJlUwe(1?
' No 6, flare siunple IDa listed on tte COC7
® Ycs N0 7. WOre sample JTUS 1JSU7J on all sample contai ftry
VMs ❑ lea S. Was ct]llpcxiDrl tlaoe lime iistod an the Cocf
❑ Yes 0 Nti 9. Vas o411ecrion date $ time I.Sted4ni aJl €atrp'JCcnri
ycs _ ❑ 1qo 10. ON all catr4rirtc_ Ja[,c] in(4yrMariim (ID, dai tius�} g�ree v�itli the { {}C?
® YPg i No 1 '„ iVcre fists t+, b� pertomted l iste'l rrn the Coc?
® '+,� ❑ No 12. Nit a]I Salr ift a:=ike in di,: pr4)pff evntainet; for eacEt tetit rr4d'or in gaud condition
(11ri ol:arr, lids out, t tc.)7 _
WJ I`es U Ml 13_ Vans aderltlate 4;il vOJume avai_abk?
Yes 11 No 14.kVineall afilcsreoeitic
Yvs dwithin341heholdirtirgoar4Shour,whicbrv�rcorresfirst?
Idle, J S. V'cre a balm Ir,� ca,t;eirters missin�fcxcesS (nirclC onej�arrp]e� 7dor listed an �t��
❑ Yes ❑ No Wi NA 16. For VO.4 and RSK-175 Simples, ',vcre bubbles present = w::eL-sins" (1�a"ai 5mm in r7itrme#er)
In anY of the WA S'i o IS`?
Y" No NA 17. 14'are all DR17lruetais+'nutrient sampl s recoived au(a ] I of � 2?
!� Yes Q'Jo NA I S- �1'e�c all c aeeide sample€€ receat a H> 12 and €.ulftde wamples %Ceivcd at a H
© Y" ❑ No � NA 19. ere all aPPii(W c M H.,r i KWcy'an idoipI10n. b535 (< 0-5rrrP/r Q same ea t'rce of rc�lduai
ehl[uiue
❑Yes d No [ 1 q 2[)-'1Jerec1icnt rgnat slrcgttesls{i,e. quested dilu�itues, ll4S}MSJ`)dc5i83rat[e311, crc..,j
Corr-mct[y transcribed fron, the C{}C iru , the comment section in I'mS?
❑ Y:a 1�22J 21. Was 'a uutu Durn4Gr [isWd on the oa Itainar la2,ol? If ycr Qu,,#e N.
:tampit V'mservation (Lhlfi'. lse cnrr,Pleted for aaly 3RMp[e(5j incorrectly prel Qr sit Il ansptua,)
araplr(s
sarnpre or were racei+'{x[ incorrectly crewx+'cd and we--e adjusted xcca�jV ly
sampler ci `�ul�= yp'ith NA_ML of circle octet l-12S,04, JAN03, 'NU Nppli tLrting SR 9 NA
ilnt Of pres4:Na1101-L NA If Irrorc 111him one C,r,,servadvw is noe'& 1, plcast note iiI [he corrunents belr,,v
arrpJe(.R} NA _
imple�(s) NA
WiMe received with bubblt_fi >6 mrrr in dl.Emeter.
_~ wex� receivtd wii]a 1'R�' � 0.5 m�rJl. {Tip 19 ie +r� t and we rp
ljtlstetl a boAngiy in sample c=vin6with sodium thic,suICHtp (NEI,5,031 wi*Ll Shcaiy JL): NA
—Me liabcla applied by, B %A(J
Corarrtonts
Date: 0071X20
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

FACILITY NAME: DUNN, NC
LAND OWNER: RAY N DELORES EDWARDS
OPERATOR: RAY N DELORES EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
Mnv rRr'MW
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: W00006101 FIELD#: NC-CU-00010-0-0001-
ANNUAL DRY TONS APPLIED: 43.58 SITE #: NC CU 00010
PREDOMINANT SOIL SERIES: AUTRYVILLE
CROP 1 MAX. PAN: 270 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 7.6
ACRES PERMITTED: 7.6
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
Amount
UOM
3/30/2020
18,600.OD
(G)
2.430
0.248
DUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
11.579
BCH
3/31/2020
148,800.00
(G)
2.430
1.984
DUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
92.631
BCH
Mar-20
167,400.00
(G)
4/6/2020
148,800.00
(G)
4.290
3.503
DUWPL
DRY
"0-<112"
SUR I
D.5
0.40
6,500.00
230.00
15.10
18.480
BCH
Apr-20
148,800.00
(G)
Total 5.735
local o.vuu
AS CD CU
CR
PB HG
MO NI SE
ZN P Lime Applied
Annual Ibs/acre Applied 1.64 0.159 0.022 9
DA57
0.351 0.010
0.084 0.186 0.116
3.276 106.481 Date
Lbs/Ac
Cumulative Ibs/acre Applied 0.198
0.027 2.398 0.457
0.482 0.013
0,108
0.228
0.155 4.537
Permit PAN Limit (Ibs/acre) 1st Cropx
270
Federal C.P.L.R. (Ibs/acre)**** 36.6
34.8 1,339.0
267.9 15.0
375.0 89.0 2,500.0
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
"I certify, tinder penalty of law, that this document was prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that the a 11gniflcant p ]ties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
f?�
Z �
SIGNATURE OF LAND APPLIER
DATE
NR = Not Reported or Not Required
*** Mineralization Rates: Compost-0.1, Anaerobicaliy digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation
*"** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
*"*** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021
DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: RAY N DELORES EDWARDS
OPERATOR: RAY N DELORES EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0006101 FIELD#: NC-CU-00010-0-DD03-
ANNUAL DRY TONS APPLIED: 48.35 SITE #: NC CU 00010
PREDOMINANT SOIL SERIES: AUTRYVILLE
CROP 1 MAX. PAN: 270 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 6.3
ACRES PERMITTED: 6.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia Nitrate PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization TKN
Nitrogen and Nitrite (lbs/acre) Application
Month
Solids Dry Tons/Ac
Source
Moist
Inches
Method*
Rate*`
Rate*** mglkg
mglkg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
:=
UOM
3/30/2020
148,800.00
(G)
2A30 2.393
DUAEDL
DRY
1'0-<1/2"
SUR
0.5
0.30 68,800.00
6,210.00 1,490,00 111.745
BCH
Mar-20
148,800.00
(G)
4/7/2020
186,000.00
(G)
4.290 �1 5.282
DUWPL
DRY
"D-<1/2"
SUR
0.5
1 0.40 1 6,500.00
230.00 1 15.10 1 27.867
BCH
Apr-20
186,000.00
(G)
I
1
Total 7.675-'---
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there a ig �c t penalties submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER ATE
NR = Not Reported or Not Required * * Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 **** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: RAY N DELORES EDWARDS
OPERATOR: RAY N DELORES EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
uav rRrIPN
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
W Q PERMIT #: W 00006101 FIELD#: NC-CU-00010-0-OOD4-
ANNUAL DRY TONS APPLIED: 46.72 SITE #: NC CU 00010
PREDOMINANT SOIL SERIES: AUTRYVILLE
CROP 1 MAX. PAN: 270 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 11.0
ACRES PERMITTED: 11.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate-
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
3/27/2020
105,400.00
(G)
2.430
0.971
DUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
45.333
BCH
3/28/2020
93,000.00
(G)
2.430
0.857
DUAEDL
DRY
110-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
40.000
BCH
Mar-20
198,400.00
(G)
4/8/2020
142,600.00
(G)
4.290 I
2.319
DUWPL
DRY
"0-<1/2"
SUR
0.5
0.40
6,500.00
230.00
15.10
12.236
BCH
4/9/2020
6,200.00
(G)
4.290
0.101
DUWPL
DRY
"0-<1/2"
SUR
0.5
0.40
6,500.00
230.00
15.10
0.532
BCH
l - Apr-2 0
148,800.00
(G)
Total 4.248
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
[Annual lbs/acre Applied 0.122 0.01 B 1 1.307 0.337 0.274 1 0.008 0.064 0.138 0.092 2.613 85.848 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.202 1 0.028 1 2.859 0.337 1 0.547 1 0.014 1 0.114 0.226 0.172 5.227
Permit PAN Limit (Ibs/acre) 1st Crop 270
Federal G P L R (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 1 375.0 89.0 2,500.0
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
9 certify, under penalty of law, that this document was prepared cinder my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are signi caries for so 'tting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation "*** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (1212006)

FACILITY NAME: DUNN, NC
LAND OWNER: RAY N DELORES EDWARDS
OPERATOR: RAY N DELORES EDWARDS
CROP 1NAME: BERMUDAGRASS,COASTAL -
"AV IRf Nl
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0006101 FIELD#: NC-CU-00010-0-0005-
ANNUAL DRY TONS APPLIED: 14.45 SITE M NC CU 00010
PREDOMINANT SOIL SERIES: AUTRYVILLE
CROP 1 MAX. PAN: 270 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 6.8
ACRES PERMITTED: 6.8
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia Nitrate
PAN Applied Receiving Residual
Date or
or Wet Tons (W)
% Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization TKN
Nitrogen and Nitrite
(Ibs/acre) Application
Crop 1 Crop 2 Crop 1 Crop 2
Month
Solids Dry Tons/Ac Source
Moist
Inches
Method*
Rate**
Rate*** mg/kg
mg/kg mg/kg
Amount
UOM
3/27/2020
142,600.00
(G)
2,430 2.125 DUAEDL
DRY
"0-�112"
SUR
0.5
0.30 68,800.00
6,210.00 1,490.00
99.215 BCH
Mar-20
142,600.ot,
(G)
Annual Ibs/acre Applied
Total 2.125
AS CD I CU I CR
0.088 0.018 1 1.249 F 0.155
49 1 0.026 1 2.412 1 0.155
PB HG I MO NI SE ZN P Lime Applied
0.234 0.007 I 0.044 0.070 0.088 2.605 91.374 t Date Lbs/Ac
0.082 1 0.136 1 0.149 1 4.563
Permit PAN Limit (Ibs/acre) 1st Crop
Federal C P L R (Ibs/acre)**** 36 6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in acc07dance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there ar, aiica.penalties for ybmittin false information, including the possibility of fines and imprison ien for knowing violations."
SIGNATURE OF LAND APPLIER — DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injectionlincorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: HAROLD EDRIDGE
OPERATOR: HAROLD ELDRIDGE
CROP 1NAME: BERMUDAGRASS,COASTAL -
DagTI IP lRCPN
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0006101 FIELD#: NC-CU-00034-0-0001-
ANNUAL DRY TONS APPLIED: 11.94 SITE #: NC CU 00034
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP 1 MAX. PAN: 224 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 4.8
ACRES PERMITTED: 4.8
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond. Precip
Volati- Mineral-
Ammonia
Nitrate PAN Applied Receiving Residual
Date or
or Wet Tons (W) % Residual
Dry, Wet, Past 24 Hrs.
Application
lization ization TKN
Nitrogen
and Nitrite (Ibs/acre) Application
Month
Amount UOM Solids Dry Tons/Ac Source
Moist Inches
Method*
Rate* Rate*** mg/kg
mg/kg
mg/kg Crop 1 Crop 2 Crop 1 Crop 2
9/8/2020
117,800.00
(G) 2A30 2.487 DUAEDL
DRY 110-<1/2"
SUR
0.5 0.30 68,800.00
6,210.00
1,490.00 116.110
BCP
Sep-20
117,800.00
(G)
Total 2.487
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.103 0.021 1.462 0.182 0.274 O.D08 OA52 0.082 0.103 3.049 106.934 Date LbslAc
Ibs/acre Applied 0.435 0.101 11.626 1 1.837 1 1.641 1 0.066 1 0.435 1 0.945 1 0.380
Permit PAN Limit (Ibs/acre) 1st Crop "'
Federal C.P.L.R. (Ibslacre)`*** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are sign$ ena ies for sub ding false information, including the possibility offines and imprisonment for knowing violations."
..
SIGNATURE OF LAND APPLIER ATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation * `* C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injectiontlncorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: HAROLD EDRIDGE
OPERATOR: HAROLD ELDRIDGE
CROPINAME:BERMUDAGRASS,COASTAL-
uov trzrtu
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQOD06101 FIELD#: NC-CU-00034-0-0002-
ANNUAL DRY TONS APPLIED: 12.57 SITE #: NC CU 00034
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP 1 MAX. PAN: 299 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 4.0
ACRES PERMITTED: 4.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip Volati-
Mineral-
Ammonia Nitrate PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs. Application lization
ization TKN
Nitrogen and Nitrite (Ibs/acre) Application
Month
Solids DryTons/Ac
Source
Moist
Inches Method* Rate**
Rate*** mg/kg
mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Amount
UOM
9/15/2020
124,000.00
(G)
2.430 i 3.141
DUAEDL
DRY
"0-<1/2" SUR 0.5
0.30 68,800.00
6,210.00 1,490.00 146.665
BCH
,
Sep-20
124,000.00
(G)
Total 3.141
AS CD GU CR PB HG MO NI SE ZN P Lime Applied
Annual its/acre Applied 0.131 0.026 1 1.8471 0,229 1 0.346 1 0.010 1 0,065 1 0.104 1 0.131 3,851 135.074 Date Lbs1Ac
IbslacreApplied 0.41E 0.093 9.914 1.588 ( 1.387 1 0.059 0.378 0,776 I 0.371 @ 17.585
Limit (Ibs/acre) 1st Crop II 9 i
1,39.0 2,500.0
Federal C P L R (Ibs/acre)** 34.8 267.9 I !
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are .f - t p aloes for subm false information, including the possibility of fines and impr on lent for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation **'* C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ** * See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: HAROLD EDRIDGE
OPERATOR: HAROLD ELDRIDGE
CROPINAME:BERMUDAGRASS,COASTAL-
DACTI IR /riRP\
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0006101 FIELD#: NC-CU-00034-0-0003-
ANNUAL DRY TONS APPLIED: 14.49 SITE* NC CU 00034
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP 1 MAX. PAN: 224 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 4.3
ACRES PERMITTED: 4.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
i
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia Nitrate PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization TKN
Nitrogen and Nitrite (Ibs/acre) Application
Month
Solids Dry Tons/Ac
Source
Moist
Inches
Method'*
Rate**
Rate*** mglkg
mglkg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Amount
UOM
9/8/2020
74,400.00
(G)
2.430 1.753
DUAEDL
DRY
110-<112"
SUR
0.5
0.30 68,800.00
6,210.00 n 1,490.00 81.860
BCP
9/9/2020
24,800.00
(G)
2.430 0.584
DUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30 1 68,800.00
6,210.00 1,490.00 27.287
BCP
Sep-20
99,200.00
(G)
9l9/202
24,800.00
0
""
SUR
0.5
0.40 6,500.00
230.00 15.10
BCP
1 Sep-20
24,800.00
(G)
Total 3.369
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.117 0.020 1.474 0.257 0.288 0.008 717 0.060 0.110 0.104 3.025 103.616 Date Lbs/Ac
T-7777—
f`i—i dntiv the/acres Annlierl 0.468 0.105 11.738 1.939 1.667 0.068 0.457 1.043 0.390 1 20.927
Permit PAN Limit (Ibs/acre) 1st Crop 224
Federal C.P.L.R. (Ibslacre)**** 36.6 34.8 1,339.0 2677-7 15.0 375.0 89.0 2,500.0
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there fint penaltie ubmitting False information, including the possibility of fines and impriso ment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injectiontlncorporation 1.0 ** * See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: DUNN, NC
LAND OWNER: HAROLD EDRIDGE
OPERATOR: HAROLD ELDRIDGE
CROPINAME:BERMUDAGRASS,COASTAL-
POCTI IP tPr'P\
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0006101 FIELD#: NC-CU-00034-0-0004-
ANNUAL DRY TONS APPLIED: 32.20 SITE #: NC CU 00034
PREDOMINANT SOIL SERIES: NORFOLK
CROP 1 MAX. PAN: 219 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 6.2
ACRES PERMITTED: 6.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mglkg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
9/1112020
49,600.00
(G)
2.430
0.811
DUAEDL
DRY
1.0-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
37.849
BCP
9/14/2020
93,000.00
(G)
2.430
1.520
DUAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
68,800.00
6,210.00
1,490.00
70.967
BCP
Sep-20
142,600.00
(G)
a
9/11/2020
24,800.00
(G)
4.290
0.716
DUWPL
DRY
110-<1/2"
SUR
0.5
0.40
6,500.00
230.00
15.10
3.776
BCP
9/16/2020
74,400.00
(G)
4.290
2.147
DUWPL
DRY
110-<1/2"
SUR
0.5
0.40
6,500.00
230.00
15.10
11.327
BCP
Sep-20
99,200.00
(G)
Total 6.194
AS CD I CU CR PB HG MO NI SE ZN P Lime Applied
Annuallbs/acre Applied 0.151 OA22 1.645 0.411 0.342 0.01D 0,079 0.169 0.116 3.298 106.803 Date Lbs1Ac
Cumulative Ihc7acre Annlied 0.519 0.109 11.691 2.065 1.739 0.066 0.460 1.062 0.405 20.826
Permit PAN Limit (Ibs/acre) 1st Crop -'
Federal C P L R (lbslacre)**** 36.6 34.8 1,339.0 1 267.9 15.D 375.0 89.0 2,500.0
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are �p'n'i/�ant penalties for st fitting false information, including the possibility of fines and imprisonment for
knowing violations."
' SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed:2/1/2021 DENR FORM FSF (1212006)

FACILITY NAME: DUNN, NO
LAND OWNER: HAROLD EDRIDGE
OPERATOR: HAROLD ELDRIDGE
CROP INAME: BERMUDAGRASS,COASTAL -
41Av 1RrW
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT#: WQ0006101 FIELD#: NC-CU-00034-0-0005-
ANNUAL DRY TONS APPLIED: 37.18 SITE #: NC CU 00034
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP I MAX. PAN: 299 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 9.7
ACRES PERMITTED: 9.7
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
I
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia Nitrate
PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 His.
Application lization
ization TKN
Nitrogen and Nitrite
(Ibs/acre) Application
Month
Solids ° DryTons/Ac
Source
Moist
Inches
Method* Rate**
Rate*** mg/kg
mg/kg mg/kg
Amount
UOM
Crop 1
Crop 2 Crop 1
Crop 2
9/11/2020
124,000.00
(G)
2.430 1.295
DUAEDL
DRY
110-<112"
SUR 0.5
0.30 68,800.00
6,210.00 1,490.00
60.481
BCH
9/14/2020
111,600.00
(G)
2,430 1.166
DUAEDL
DRY
110-<1/2"
SUR 0.5
0.30 68,800.00
6,210.00 1,490.00
54.433
BCH
Sep-20
235,600.00
(G)
I —
9/16/2020
74,400.00
(G)
4.290 1.372
DUWPL
DRY
"0-<1J2"
SUR 0.5
0.40 6,500.00
230.00 15.10
7.240
BCH
:1
Sep-20
74,400.00
(G)
I
_[
Ibs/acre Applied
Applied
Total 3.833 ,..1a1
CD I CU CR PB I HG I MO I NI
0.022 1 1.579 1 0.295 0.312 1 0A09 0.066 0.125
0.106 I 12.025 1 1.907 1 1.745 I 0.066
SE ZN
0.111 S 3.229
0.395 1 21
Lime Applied
Date I t
Permit PAN Limit (Ibs/acre) 1st Crop ; 299
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
DUAEDL = DUNN, NC W WTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are ant enalties for bmitting false information, including the possibility of fines and imprison ent f r knowing violations."
F
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required ** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation ** * C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injectionfincorporation 1.0 ""* See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME: DUNN, NC WQ PERMIT #: WQ0035207 FIELD#: NC-HA-OOX48-0-0001- ACRES UTILIZED: 25.0
LAND OWNER: MONROE LEE ANNUAL DRY TONS APPLIED: 36,60 SITE #: NC HA 0OX48 ACRES PERMITTED: 25.0
OPERATOR: MONROE LEE PREDOMINANT SOIL SERIES: NORFOLK CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP) CROP 1 MAX. PAN: 118 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
s
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
% s
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite (Ibs/acre)
Application
Month
Amount UOM
Solids Dry Tons/Ac
Source
Moist
Inches
i Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1
Crop 2
8/26/2020
68,200.00 (G)
4.290 0.488
DUWPL
SUR
0.5
0.40
6,500.00
230.00
15.10
2.575
FSP
8/27/2020
136,400.00 (G)
4.290 0.976
DUWPL
SUR
0.5
OAO
6,500.00
230.00
15.10
5.150
FSP
Aug-20
204,600.00 (G)
Total 1.464
Total
7.725 0.000
AS
CD
CU
CR
PB
HG
MO
NI
�O�
ZNLime
Applied
Annual Ibslacre
Applied
0.028
0.001
0.141
0.123
0.044
0.001
0.016
0.047
00.225
4.392
Date
Lbs/Ac
itive Ibs/acre Applied 0.028 0.001 ( 0.141 0.123 0.044 0.001 I 0.016 0.047 ¢ 0.010 0.225 Y
PAN Limit (Ibslacre) 1st Crop` ¢ L Y 118
C P_I _R_ (Ihsiacrel**** 36.6 34.8 1,339.0 26Z9 15.0 375.0 89.0 2,500.0 s
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are sigcpficAnt nalties for siaornitting false information, including the possibility of fines and imprisonment for knowing violations."
/7
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: DUNN, NC WQ PERMIT #: W00035207 FIELD#: NC-HA-OOX48-0-0002- ACRES UTILIZED: 15,0
LAND OWNER: MONROE LEE ANNUAL DRY TONS APPLIED: 49.91 SITE #: NC HA 0OX48 ACRES PERMITTED: 15.0
OPERATOR: MONROE LEE PREDOMINANT SOIL SERIES: NORFOLK CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: BERMUDAGRASS, COASTAL - CROP 1 MAX. PAN: 219 CROP 2 NAME: CROP 2 MAX. PAN:
u nv IRru\
RESIDUAL SOURCE(S): * See list at bottom of report
--��
Gallons (G)
Site
y
a
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre) Application'
Month i
Amount UOM
Solids
i
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate *
Rate*
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
8/27/2020
62,000,00 (G)
4.290
0.739 � DUWPL
SUR
0.5
0.40
6,500.00
230.00
15.10
3.901 �
BCH
8/28/2020
217,000.00 (G)
4,290
2.588 DUWPL
SUR
0.5
0.40
6,500.00
230.00
15.10
13.655
BCH
Aug-20
279,000.00 (G)
Total 3.327
Total
17.556 0.000
AS�%D
CU
CR
PB
HG
MO
NI
SEAnnual
Ibsiacre Applied
0.063
0.319
0.280
0.100
0.003
0.035
0.106
0.022
0.512
9.982
Date Lbs/Ac
bs/acre Applied 0.063
19 —0.280 0.100 0.003 R 0.035 � 0.106 ' 0.022 1 0.512
Permit PAN Limit (Ibs/acre) 1st Crop, ± - -
Federal C P L R (Ibs/acre)*""* 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0E 2,500.0
DUWPL = DUNN, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are si cant penalties fo rm tt
m. false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
" Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation ***" C.P.L.R.: Cumulative Pollutant Loading Rate
"* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***"" See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

SECTION 4

SUMM111 Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOL0C4r;S,INC Cuyahoga Falls, Ohio44223
Arraly0ca1 Laboralorfas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
February 07, 2020
Melvin Goad
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: DUNN WWTP
Dear Melvin Goad: Order No.: 20010926
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/16/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20010926
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/7/2020
CLIENT: Synagro
Project: DUNN WWTP
WorkOrder Narrative:
20010926: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20010926-OOIA TCLP-SVOC-CPEST(8081B): Bracketing CCVs were out of range for some analytes.
All samples within the sequence are non -detect for all analytes.
20010926-OOIA TCLP-SVOC_8270E: Possible low bias for 1,4-Dichlorobenzene and
Hexachloroethane due to low recovery in LCS-41607.
20010926-OOIA F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
Analytical Sequence QC Notes:
CCV-108374 VOC-MSTR_NPW(8260): The VOC CCV (Batch R108374) exhibited high recovery fo
Chlorobenzene and Tetrachloroethene; All samples were ND.
Original
Page 2 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 20010926
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/7/2020
CLIENT: Synagro
Project: DUNN WWTP
LCS-41570 TCLP-SVOC-CPEST_TCLP(8081): LCS-41570 demonstrated high recovery for analyte
Endrin, suggesting a potential high bias for recovery of this analyte. All samples in this batch are non -
detect for Endrin.
LCS TCLP-SVOC-Herb_TCLP: LCS exhibited high recovery, associated samples are ND for all
analytes of interest.
LCS-R108707 F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
Original
Page 3 of 32

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 20010926
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 2/7/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 32

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL TECHNp4,1 ULES,1NC. Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: DUNN WWTP
Lab SamplelD Client Sample ID
20010926-001 DUNN WWTP
Tag No Date Collected
1/15/2020 10:00:00 AM
Workorder
Sample Summary
WO#: 20010926
07-Feb-20
Date Received Matrix
1/16/2020 9:55:00 AM Sludge
Page 5 of 32

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES "PORT
ENVIRONMENTALTECHN❑L0G1ES,11+1C
Cuyahoga Falls, Ohio44223
WO#:
20010926
ArWyft cal taboralonag
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Feb-20
Client:
Synagro
Project:
DUNN WWTP
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
20010926-OOIA DUNN WWTP 1/15/2020 10:00:00 AM Sludge Flashpoint Determination (1010)
1/30/2020 11:50:49 AM
pH (SW9045D)
2/3/2020 3:53:37 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
2/3/2020 5:24:00 PM
Reactive Sulfide (9034)/7.3.4.2
2/3/2020 5:24:00 PM
TCLP Herbicides by EPA 8321B
1/17/2020 5:00:00 PM
1/24/2020 3:19:00 AM
TCLP Mercury Analysis (SW1311/7471/17/2020 5:00:00 PM
1/20/2020 2:25:00 PM
1/23/2020 3:25:00 PM
TCLP Metals Analysis (SW1311/6010:1/17/2020 5:00:00 PM
1/20/2020 12:20:00 PM
1/22/2020 1:30:02 PM
TCLP Pesticides Analysis (SW1311/8(1/17/2020 5:00:00 PM
1/20/2020 3:30:00 PM
1/23/2020 11:40:00 PM
TCLP Semi-Volatiles Analysis 1/17/2020 5:00:00 PM
1/21/2020 3:30:00 PM
1/24/2020 7:47:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/17/2020 5:00:00 PM
1/22/2020 6:00:00 PM
Original
Page 6 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RCI
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
31.2
Surr: Phenol-d6
34.2
Surr: Nitrobenzene-d5
48.0
SW7470A SW7470A Analyst: MJM
0.00500 mg/L 1 1/23/2020 3:25:00 PM
SW6010D SW301OA Analyst: EAM
1.25
mg/L
1
1/22/2020 1:30:02 PM
12.5
mg/L
1
1/22/2020 1:30:02 PM
0.250
mg/L
1
1/22/2020 1:30:02 PM
0.500
mg/L
1
1/22/2020 1:30:02 PM
1.25
mg/L
1
1/22/2020 1:30:02 PM
0.125
mg/L
1
1/22/2020 1:30:02 PM
1.25
mg/L
1
1/22/2020 1:30:02 PM
SW1010
Analyst: TAH
Z °F
1
1/30/2020 11:50:49 AM
SW8270 SW351OC Analyst: SFG
0.200
QL- mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.100
mg/L
2
1/24/2020 7:47:00 PM
10.0
mg/L
2
1/24/2020 7:47:00 PM
0.0400
mg/L
2
1/24/2020 7:47:00 PM
0.100
mg/L
2
1/24/2020 7:47:00 PM
0.200
QL- mg/L
2
1/24/2020 7:47:00 PM
0.200
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
0.500
mg/L
2
1/24/2020 7:47:00 PM
10 - 109
%Rec
2
1/24/2020 7:47:00 PM
10 - 109
m %Rec
2
1/24/2020 7:47:00 PM
19 - 120
%Rec
2
1/24/2020 7:47:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 7 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: 2,4,6-Tribromophenol 54.1 10 - 120 %Rec 2
Surr: 2-Fluorobiphenyl 44.7 22 - 117 %Rec 2
Surr: p-Terphenyl-d14 82.4 34 - 116 %Rec 2
NOTES:
Possible low bias for 1,4-Dichlorobenzene and Hexachloroethane due to low recovery in LCS-41607.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
75.3
Surr: DCB
102
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 76.5
SW351OC Analyst: SFG
1/24/2020 7:47:00 PM
1/24/2020 7:47:00 PM
1/24/2020 7:47:00 PM
SW8081 Analyst: SEK
0.125
mg/L
5
1/23/2020 11:40:00 PM
0.250
mg/L
5
1/23/2020 11:40:00 PM
0.0125iQC+(QDmg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
0.0125
dQC+
mg/L
5
1/23/2020 11:40:00 PM
10 - 119
%Rec
5
1/23/2020 11:40:00 PM
10 - 119
%Rec
5
1/23/2020 11:40:00 PM
SW8321A SW1311M Analyst: BJH
0.500 mg/L 50 1/24/2020 3:19:00 AM
0.500 mg/L 50 1/24/2020 3:19:00 AM
70 - 130 %Rec 50 1/24/2020 3:19:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260 SW1311M Analyst: RMT
TCLP VOLATILES
ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L 50 1/22/2020 6:00:00 PM
1,2-Dichloroethane
ND
0.250
mg/L 50 1/22/2020 6:00:00 PM
MEK
ND
5.00
mg/L 50 1/22/2020 6:00:00 PM
Benzene
ND
0.250
mg/L 50 1/22/2020 6:00:00 PM
Carbon tetrachloride ND
0.250
mg/L 50 1/22/2020 6:00:00 PM
Chlorobenzene
ND
2.50
QC+ mg/L 50 1/22/2020 6:00:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
U Samples with CaleVal < MDL
Page 8 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010926
Date Reported: 2/7/2020
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2020 10:00:00 AM
Lab ID:
20010926-OOIA
Project:
DUNN WWTP
Client Sample ID DUNN WWTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: RMT
TCLP VOLATILES ANALYSIS
Chloroform
ND
0.250
mg/L
50
1/22/2020 6:00:00 PM
Tetrachloroethene
ND
0.250
QC+ mg/L
50
1/22/2020 6:00:00 PM
Trichloroethene
ND
0.250
mg/L
50
1/22/2020 6:00:00 PM
Vinyl chloride
ND
0.100
mg/L
50
1/22/2020 6:00:00 PM
Surr: 4-Bromofluorobenzene
101
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
Surr: Di brom ofl uorom ethane
97.9
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
Surr: Toluene-d8
94.1
70 - 130
%Rec
50
1/22/2020 6:00:00 PM
RCI
SW9014
Analyst: CXS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495
mg/Kg
1
2/3/2020 5:24:00 PM
RCI
SW9045D
Analyst: VVK
PH (SW9045D)
pH
6.2
s.u.@20.00
1
2/3/2020 3:53:37 PM
RCI
SW9034
Analyst: CXS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
2/3/2020 5:24:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 9 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal�7n tes Report
ENOROMMEWAL IrECHNOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20010926
Website: http://www.settek.com
07-Feb-20
Client: Synagro
State: NW
Project: DUNN WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010926-OOIA Sludge
Flashpoint Determination (1010)
Flashpoint (1407)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034Y7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original #1
Page 10 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal�7n tes Report
ENVIROMMEWAL IrECHHOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20010926
Website: http://www.settek.com
07-Feb-20
Client: Synagro
State: NW
Project: DUNN WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010926-OOIA Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Original #1
Page 11 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010926
07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108355
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2574864
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
MEK ND 1.00
Surr: 4-Bromofluorobenzene 507 500.0 101 70 130
Surr: Dibromofluoromethane 517 500.0 103 70 130
Surr: Toluene-d8 499 500.0 99.8 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 12 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010926
07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108374
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2576732
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
518
Surr: Dibromofluoromethane
477
Surr: Toluene-d8
468
500.0 104 70 130
500.0 95.3 70 130
500.0 93.6 70 130
QC+
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010926
07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108319
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2572614
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
501
Surr: Dibromofluoromethane
485
Surr: Toluene-d8
482
500.0 100 70 130
500.0 97.0 70 130
500.0 96.3 70 130
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 32

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20010926
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Feb-20
Client:
Synagro
Project:
DUNN WWTP
BatchID: 41527
TCLP Mercury ND 0.00200
TCLP Mercury 0.00425 0.00200 0.00400 0 106 80 120
TCLP Mercury ND 0.00200
Sample ID: 20010863-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00472 0.00200
0.00400 0.000110 115 75
125
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 15 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41527
Sample ID: 20010863-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
NOTES:
Sample ID in raw data was typed incorrectly.
Sample ID: 20010863-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578129
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00469 0.00200 0.00400 0.000110 114 75 125 0.00472 0.638 20
NOTES:
Sample ID in raw data was typed incorrectly.
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 16 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010926
07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41546
Sample ID: MB-41546
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108321
Client ID: PBS
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2572816
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-41546
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108321
Client ID: LCSS
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2572817
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.96
0.500
2.000
0
98.2
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
96.8
80
120
TCLP Cadmium(Cd)
1.86
0.100
2.000
0
92.8
80
120
TCLP Chromium(Cr)
1.95
0.200
2.000
0
97.6
80
120
TCLP Lead(Pb)
1.95
0.500
2.000
0
97.7
80
120
TCLP Selenium(Se)
2.13
0.0500
2.000
0
106
80
120
TCLP Silver(Ag)
1.99
0.500
2.000
0
99.5
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41546
Sample ID: 20010911-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575565
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Cadmium(Cd)
2.18
0.100
2.000
0.001870
109
70
130
TCLP Chromium(Cr)
1.94
0.200
2.000
0
97.1
70
130
TCLP Lead(Pb)
1.89
0.500
2.000
0.07361
90.9
70
130
Sample ID: 20010911-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575566
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Cadmium(Cd) 2.20 0.100 2.000 0.001870 110 70 130 2.176 1.20 20
TCLP Chromium(Cr) 1.96 0.200 2.000 0 98.0 70 130 1.943 0.876 20
TCLP Lead(Pb) 1.93 0.500 2.000 0.07361 92.7 70 130 1.892 1.85 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 18 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: 41570B
Sample ID: MB-41570
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: PBS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581728
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
dQC+
gamma-BHC
ND
0.000500
dQC+
Heptachlor
ND
0.000500
dQC+
Heptachlor epoxide
ND
0.000500
dQC+
Methoxychlor
ND
0.000500
dQC+
Surr: TCMX
601
1000 60.1 10 119
Surr: DCB
1030
1000 103 10 119
Sample ID: LCS-41570
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: LCSS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581729
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.790
0.000500
0.500
0
158
10
130
SmQC-
gamma-BHC
0.482
0.000500
0.500
0
96.5
10
130
QC+
Heptachlor
0.516
0.000500
0.500
0
103
10
130
mQC+
Heptachlor epoxide
0.576
0.000500
0.500
0
115
10
130
QC+
Methoxychlor
0.789
0.000500
0.500
0
158
10
178
mQC+
Surr: TCMX
793
1000
79.3
10
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 19 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WWTP BatchID: 41607
WO#: 20010926
07-Feb-20
Sample ID: 20010822-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: BatchQC
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586256
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.259
0.200
0.8000
0
32.4
15.2
124
QMR
2,4,5-Trichlorophenol
0.681
0.500
0.8000
0
85.2
30.6
152
2,4,6-Trichlorophenol
0.662
0.500
0.8000
0
82.7
27.6
150
2,4-Dinitrotoluene
0.893
0.100
0.8000
0
112
58
141
o-Cresol
ND
0.500
0.8000
0
61.6
26.9
132
Cresols, Total
ND
10.0
1.600
0
62.4
27.6
132
Hexachloro-1,3-butadiene
0.278
0.0400
0.8000
0
34.7
-5.3
156
QMR
Hexachlorobenzene
0.657
0.100
0.8000
0
82.1
54.3
142
Hexachloroethane
0.227
0.200
0.8000
0
28.4
1.92
131
QMR
Nitrobenzene
0.483
0.200
0.8000
0
60.4
21
135
Pentachlorophenol
0.899
0.500
0.8000
0
112
47.4
134
Pyridine
ND
0.500
0.8000
0
41.8
-10.3
64.2
m
Surr:2-Fluorophenol
0.489
1.000
48.9
9.77
146
Surr: Phenol-d6
0.525
1.000
52.5
20.7
130
Surr: Nitrobenzene-d5
0.581
1.000
58.1
13.9
156
Surr:2,4,6-Tribromophenol
0.942
1.000
94.2
27.3
183
Surr:2-Fluorobiphenyl
0.622
1.000
62.2
21.4
153
Surr: p-Terphenyl-d14
1.02
1.000
102
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WWTP BatchID: 41607
WO#: 20010926
07-Feb-20
Sample ID: 20010822-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: BatchQC
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586257
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.397
0.200
0.8000
0
49.6
15.2
124
0.2588
42.2
30 R
2,4,5-Trichlorophenol
0.741
0.500
0.8000
0
92.6
30.6
152
0.6812
8.38
30
2,4,6-Trichlorophenol
0.793
0.500
0.8000
0
99.2
27.6
150
0.6616
18.1
30
2,4-Dinitrotoluene
0.944
0.100
0.8000
0
118
58
141
0.8932
5.57
30
o-Cresol
0.613
0.500
0.8000
0
76.7
26.9
132
0.4924
21.9
30
Cresols, Total
ND
10.0
1.600
0
76.6
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.470
0.0400
0.8000
0
58.7
-5.3
156
0.2776
51.4
30 R
Hexachlorobenzene
0.728
0.100
0.8000
0
91.0
54.3
142
0.6568
10.3
30
Hexachloroethane
0.378
0.200
0.8000
0
47.2
1.92
131
0.2272
49.7
30 R
Nitrobenzene
0.584
0.200
0.8000
0
73.0
21
135
0.4832
18.8
30
Pentachlorophenol
0.984
0.500
0.8000
0
123
47.4
134
0.8992
9.01
30
Pyridine
ND
0.500
0.8000
0
44.7
-10.3
64.2
0
0
30 m
Surr: 2-Fluorophenol
0.581
1.000
58.1
9.77
146
0
Surr: Phenol-d6
0.650
1.000
65.0
20.7
130
0
Surr: Nitrobenzene-d5
0.682
1.000
68.2
13.9
156
0
Surr:2,4,6-Tribromophenol
1.02
1.000
102
27.3
183
0
Surr:2-Fluorobiphenyl
0.755
1.000
75.5
21.4
153
0
Surr: p-Terphenyl-d14
1.07
1.000
107
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WWTP BatchID: 41607
WO#: 20010926
07-Feb-20
Sample ID: MB-41607
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: PBS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581886
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.383
Surr: Phenol-d6
0.386
Surr: Nitrobenzene-d5
0.373
Surr: 2,4,6-Tribromophenol
0.640
Surr: 2-Fluorobiphenyl
0.375
Surr: p-Terphenyl-d14
0.859
1.000
38.3
10
109
1.000
38.6
10
109
1.000
37.3
19
120
1.000
64.0
10
120
1.000
37.5
22
117
1.000
85.9
34
116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WWTP BatchID: 41607
WO#: 20010926
07-Feb-20
Sample ID: LCS-41607
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: LCSS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581887
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.213
0.100
0.8000
0
26.7
36.4
130 S
2,4,5-Trichlorophenol
0.610
0.250
0.8000
0
76.3
31.7
132
2,4,6-Trichlorophenol
0.642
0.250
0.8000
0
80.2
31.1
133
2,4-Dinitrotoluene
0.822
0.0500
0.8000
0
103
43.3
130
o-Cresol
0.448
0.250
0.8000
0
56.0
32.9
130
Cresols, Total
ND
5.00
1.600
0
58.1
31.7
130
Hexachloro-1,3-butadiene
0.263
0.0200
0.8000
0
32.9
31.4
130
Hexachlorobenzene
0.597
0.0500
0.8000
0
74.7
43.1
130
Hexachloroethane
0.188
0.100
0.8000
0
23.5
36.5
130 S
Nitrobenzene
0.438
0.100
0.8000
0
54.7
39.5
130
Pentachlorophenol
0.705
0.250
0.8000
0
88.1
34
130
Pyridine
0.255
0.250
0.8000
0
31.9
10
130
Surr: 2-Fluorophenol
0.434
1.000
43.4
17.1
130
Surr: Phenol-d6
0.482
1.000
48.2
10
130
Surr: Nitrobenzene-d5
0.506
1.000
50.6
32.6
130
Surr: 2,4,6-Tribromophenol
0.831
1.000
83.1
4.43
130
Surr: 2-Fluorobiphenyl
0.521
1.000
52.1
41.8
130
Surr: p-Terphenyl-d14
0.834
1.000
83.4
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 23 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010926
07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R108707
Sample ID: LCS-R108707
SampType: LCS
TestCode: FlashPt_S(10 Units: °F
Prep Date:
RunNo: 108707
Client ID: LCSS
Batch ID: R108707
TestNo: SW1010
Analysis Date: 1/30/2020
SegNo: 2595868
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (140°F)
134
135.4 0 99.1 98 102
Z
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R108838
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_DW(4500- Units: s.u.@20.1C
Prep Date:
RunNo: 108838
Client ID: LCSW
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601762
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 20010989-006ADUP
SampType: DUP
TestCode: pH_DW(4500- Units: s.u.@21.2C
Prep Date:
RunNo: 108838
Client ID: Batch=
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601769
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.6 7.6 0.4 5 H
NOTES:
pH is an EPA field recommended parameter. Per 40 CFR 136.3, hold time is 15 minutes from collection.
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 25 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R108838
Sample ID: LCS-R108838
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@19.9C
Prep Date:
RunNo: 108838
Client ID: LCSS
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601750
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.4C
Prep Date:
RunNo: 108838
Client ID: LCSS
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601867
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.9 90 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 26 of 32

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20010926
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Feb-20
Client:
Synagro
Project:
DUNN WWTP
BatchID: R109015
Cyanide, Reactive ND 0.500
Cyanide, Reactive 9.29 0.495 10.00 0 92.9 85 115
Sample ID: RLC-R109015
SampType: RLC
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611492
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
0.557 0.500 0.5000 0 ill 50 150
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 27 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R109015
Sample ID: 20010790-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611506
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.22 0.490 10.00 0 92.2 81.6 122
Sample ID: 20010790-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611507
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.08 0.481 10.00 0 90.8 81.6 122 9.218 1.47 5
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 28 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R109050
Sample ID: 20010790-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109050
Client ID: Batch=
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612561
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4520 25.0 4800 0 94.2 80 120
Sample ID: 20010790-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109050
Client ID: Batch=
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612562
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4460 25.0 4800 0 92.9 80 120 4520 1.34 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 29 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010926
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Feb-20
Client: Synagro
Project: DUNN WWTP BatchID: R109050
Sample ID: MB-R109050
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109050
Client ID: PBW
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612556
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R109050
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109050
Client ID: LCSW
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612557
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4560 25.0 4800 0 95.0 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 30 of 32

DBPix Evaluatio -
Eieq S mrnit Environmental Technologies, Inc. Req>estlhain ofustodyIllStreeC ForSurwrdt Erivironmenl'al Technologies, Inc use only
Cu toga Falls, Ohio 44223 Tel: 330.253,8211 Fax: 3K253.448qalysis
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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGa1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 20010926 RcptNo: 1
Logged by: Jacqueline Rasile 1/16/2020 9:55:00 AM
1.f•
Completed By: Jesseca E. Westfall 1/19/2020 7:11:35 PM �{G
Reviewed By:
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑ No ❑d NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑ No ❑0 NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
V
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
V
No
❑
10. Was preservative added to bottles?
Yes
❑
No
V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
V
13. Does paperwork match bottle labels?
Yes
V
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No
❑
15. Is it clear what analyses were requested?
Yes
0
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
melted ice
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
18.7
Goodl
Not Present
Page 32 of 32

SUMM111
ENVIRONMENTAL TECHNOLOMZ3. INC
Arraly0ca1 Laboralorfas
February 10, 2020
Melvin Goad
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: DUNN WTP
Dear Melvin Goad:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 20010927
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/16/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20010927
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/10/2020
CLIENT: Synagro
Project: DUNN WTP
WorkOrder Narrative:
20010927: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20010927-OOIA TCLP-SVOC-CPEST(8081B): Bracketing CCVs were out of range for some analytes.
All samples within the sequence are non -detect for all analytes.
20010927-OOIA TCLP-SVOC_8270E: Possible low bias for 1,4-Dichlorobenzene and
Hexachloroethane due to low recovery in LCS-41607.
20010927-OOIA TCLP-SVOC_8270E: Sample exhibits high recoveries for all surrogates. Possibly
doubled spiked by extractions analyst. Sample was ND for all compounds.
20010927-OOIA F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
Analytical Sequence QC Notes:
Revision v1
Page 2 of 32

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20010927
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 2/10/2020
CLIENT: Synagro
Project: DUNN WTP
CCV-108374 VOC-MSTR_NPW(8260): The VOC CCV (Batch R108374) exhibited high recovery for
Chlorobenzene and Tetrachloroethene; All samples were ND.
LCS-41570 TCLP-SVOC-CPEST(808113): LCS-41570 demonstrated high recovery for analyte Endrin,
suggesting a potential high bias for recovery of this analyte. All samples in this batch are non -detect for
Endrin.
LCS TCLP-SVOC-Herb: LCS exhibited high recovery, associated samples are ND for all analytes of
interest.
LCS-RIO8707 F1ashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to
250 RPM as required by the method.
REVISED REPORT: 2/10/20 Corrected Project & Sample IDs
Revision vl
Page 3 of 32

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� Wo#: 20010927
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: htm:11www.settek.co Date: 2/10/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 32

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL TECHNp4,1 ULES,1NC. Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: DUNN WTP
Lab SampleID Client Sample ID
20010927-001 DUNN WTP
Tag No Date Collected
1/15/2020 12:00:00 PM
Workorder
Sample Summary
WO#: 20010927
l0-Feb-20
Date Received Matrix
1/16/2020 9:15:00 AM Sludge
Page 5 of 32

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES "PORT
ENVIRONMENTALTECHN❑LOG1ES,11+1C
Cuyahoga Falls, Ohio44223
Wo#:
20010927
ArWyft cal taboralonag
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
10-Feb-20
Client:
Synagro
Project:
DUNN WTP
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
20010927-OOIA DUNN WTP 1/15/2020 12:00:00 PM Sludge Flashpoint Determination (1010)
1/30/2020 11:50:49 AM
pH (SW9045D)
2/3/2020 3:53:37 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
2/3/2020 5:24:00 PM
Reactive Sulfide (9034)/7.3.4.2
2/3/2020 5:24:00 PM
TCLP Herbicides by EPA 8321B
1/17/2020 5:00:00 PM
1/24/2020 4:12:00 AM
TCLP Mercury Analysis (SW1311/7471/17/2020 5:00:00 PM
1/20/2020 2:25:00 PM
1/23/2020 3:27:00 PM
TCLP Metals Analysis (SW1311/6010:1/17/2020 5:00:00 PM
1/20/2020 12:20:00 PM
1/22/2020 1:33:21 PM
TCLP Pesticides Analysis (SW1311/8(1/17/2020 5:00:00 PM
1/20/2020 3:30:00 PM
1/24/2020 12:15:00 AM
TCLP Semi-Volatiles Analysis 1/17/2020 5:00:00 PM
1/21/2020 3:30:00 PM
1/24/2020 8:22:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/17/2020 5:00:00 PM
1/22/2020 6:30:00 PM
Revision vl
Page 6 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010927
Date Reported: 2/10/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/15/2020 12:00:00 PM
Lab ID: 20010927-OOIA
Project: DUNN WTP
Client Sample ID DUNN WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RCI
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
133
Surr: Phenol-d6
120
Surr: Nitrobenzene-d5
142
SW7470A SW7470A Analyst: MJM
0.00200 mg/L 1 1/23/2020 3:27:00 PM
SW6010D SW301OA Analyst: EAM
0.500
mg/L
1
1/22/2020 1:33:21
PM
5.00
mg/L
1
1/22/2020 1:33:21
PM
0.100
mg/L
1
1/22/2020 1:33:21
PM
0.200
mg/L
1
1/22/2020 1:33:21
PM
0.500
mg/L
1
1/22/2020 1:33:21
PM
0.0500
mg/L
1
1/22/2020 1:33:21
PM
0.500
mg/L
1
1/22/2020 1:33:21
PM
SW1010
Analyst:
TAH
Z °F
1
1/30/2020 11:50:49 AM
SW8270 SW351OC Analyst: SFG
0.500
QL-
mg/L
5
1/24/2020 8:22:00 PM
1.25
mg/L
5
1/24/2020 8:22:00 PM
1.25
mg/L
5
1/24/2020 8:22:00 PM
0.250
mg/L
5
1/24/2020 8:22:00 PM
25.0
mg/L
5
1/24/2020 8:22:00 PM
0.100
mg/L
5
1/24/2020 8:22:00 PM
0.250
mg/L
5
1/24/2020 8:22:00 PM
0.500
QL-
mg/L
5
1/24/2020 8:22:00 PM
0.500
mg/L
5
1/24/2020 8:22:00 PM
1.25
mg/L
5
1/24/2020 8:22:00 PM
1.25
mg/L
5
1/24/2020 8:22:00 PM
10 - 109
S
%Rec
5
1/24/2020 8:22:00 PM
10 - 109
S
%Rec
5
1/24/2020 8:22:00 PM
19 - 120
S
%Rec
5
1/24/2020 8:22:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision v1
U Samples with CaleVal < MDL
Page 7 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010927
Date Reported: 2/10/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/15/2020 12:00:00 PM
Lab ID: 20010927-OOIA
Project: DUNN WTP
Client Sample ID DUNN WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: 2,4,6-Tribromophenol 168 10 - 120 S %Rec 5
Surr: 2-Fluorobiphenyl 136 22 - 117 S %Rec 5
Surr: p-Terphenyl-d14 229 34 - 116 S %Rec 5
NOTES:
Possible low bias for 1,4-Dichlorobenzene and Hexachloroethane due to low recovery in LCS-41607.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
110
Surr: DCB
122
TCLP HERBICIDES BY EPA 8321B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 76.4
SW351OC Analyst: SFG
1/24/2020 8:22:00 PM
1/24/2020 8:22:00 PM
1/24/2020 8:22:00 PM
SW8081 Analyst: SEK
0.125
mg/L
5
1/24/2020 12:15:00 AM
0.250
mg/L
5
1/24/2020 12:15:00 AM
0.0125iQC+(QDmg/L
5
1/24/2020 12:15:00 AM
0.0125
dQC+
mg/L
5
1/24/2020 12:15:00 AM
0.0125
dQC+
mg/L
5
1/24/2020 12:15:00 AM
0.0125
dQC+
mg/L
5
1/24/2020 12:15:00 AM
0.0125
dQC+
mg/L
5
1/24/2020 12:15:00 AM
10 - 119
%Rec
5
1/24/2020 12:15:00 AM
10 - 130
%Rec
5
1/24/2020 12:15:00 AM
SW8321A SW1311M Analyst: BJH
0.500 mg/L 50 1/24/2020 4:12:00 AM
0.500 mg/L 50 1/24/2020 4:12:00 AM
70 - 130 %Rec 50 1/24/2020 4:12:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260 SW1311M Analyst: RMT
TCLP VOLATILES
ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L 50 1/22/2020 6:30:00 PM
1,2-Dichloroethane
ND
0.250
mg/L 50 1/22/2020 6:30:00 PM
MEK
ND
5.00
mg/L 50 1/22/2020 6:30:00 PM
Benzene
ND
0.250
mg/L 50 1/22/2020 6:30:00 PM
Carbon tetrachloride ND
0.250
mg/L 50 1/22/2020 6:30:00 PM
Chlorobenzene
ND
2.50
QC+ mg/L 50 1/22/2020 6:30:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits Revision v1
RL
Reporting Detection Limit
U Samples with CaleVal < MDL
Page 8 of 32

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20010927
Date Reported: 2/10/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/15/2020 12:00:00 PM
Lab ID: 20010927-OOIA
Project: DUNN WTP
Client Sample ID DUNN WTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: RMT
TCLP VOLATILES ANALYSIS
Chloroform
ND
0.250
mg/L
50
1/22/2020 6:30:00 PM
Tetrachloroethene
ND
0.250
QC+ mg/L
50
1/22/2020 6:30:00 PM
Trichloroethene
ND
0.250
mg/L
50
1/22/2020 6:30:00 PM
Vinyl chloride
ND
0.100
mg/L
50
1/22/2020 6:30:00 PM
Surr: 4-Bromofluorobenzene
100
70 - 130
%Rec
50
1/22/2020 6:30:00 PM
Surr: Di brom ofl uorom ethane
95.8
70 - 130
%Rec
50
1/22/2020 6:30:00 PM
Surr: Toluene-d8
95.3
70 - 130
%Rec
50
1/22/2020 6:30:00 PM
RCI
SW9014
Analyst: CXS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.490
mg/Kg
1
2/3/2020 5:24:00 PM
RCI
SW9045D
Analyst: VVK
PH (SW9045D)
pH
5.9
[e-mail]
1
2/3/2020 3:53:37 PM
RCI
SW9034
Analyst: CXS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
2/3/2020 5:24:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision v1
U Samples with CaleVal < MDL
Page 9 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal�7n tes Report
ENOROMMEWAL IrECHNOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20010927
Website: http://www.settek.com
10-Feb-20
Client: Synagro
State: NW
Project: DUNN WTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010927-OOIA Sludge
Flashpoint Determination (1010)
Flashpoint (1407)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034Y7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Version #2
Page 10 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal�7n tes Report
EMOROMMEWAL IrECHHOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20010927
Website: http://www.settek.com
10-Feb-20
Client: Synagro
State: NW
Project: DUNN WTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20010927-001A Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Version #2
Page 11 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010927
10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108355
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2574864
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
MEK ND 1.00
Surr: 4-Bromofluorobenzene 507 500.0 101 70 130
Surr: Dibromofluoromethane 517 500.0 103 70 130
Surr: Toluene-d8 499 500.0 99.8 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 12 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010927
10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108374
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2576732
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
518
Surr: Dibromofluoromethane
477
Surr: Toluene-d8
468
500.0 104 70 130
500.0 95.3 70 130
500.0 93.6 70 130
QC+
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010927
10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41501
Sample ID: MB-41501
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 1/17/2020
RunNo: 108319
Client ID: PBS
Batch ID: 41501
TestNo: SW8260 SW1311M
Analysis Date: 1/22/2020
SegNo: 2572614
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
501
Surr: Dibromofluoromethane
485
Surr: Toluene-d8
482
500.0 100 70 130
500.0 97.0 70 130
500.0 96.3 70 130
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 32

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20010927
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
10-Feb-20
Client:
Synagro
Project:
DUNN WTP
BatchID: 41527
TCLP Mercury ND 0.00200
TCLP Mercury 0.00425 0.00200 0.00400 0 106 80 120
TCLP Mercury ND 0.00200
Sample ID: 20010863-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00472 0.00200
0.00400 0.000110 115 75
125
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Revision V 1
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 15 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41527
Sample ID: 20010863-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
NOTES:
Sample ID in raw data was typed incorrectly.
Sample ID: 20010863-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/20/2020
RunNo: 108386
Client ID: Batch=
Batch ID: 41527
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2020
SegNo: 2578129
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00469 0.00200 0.00400 0.000110 114
NOTES:
Sample ID in raw data was typed incorrectly.
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
75 125 0.00472 0.638
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
20
Revision vl
Page 16 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010927
10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41546
Sample ID: MB-41546
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108321
Client ID: PBS
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2572816
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-41546
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108321
Client ID: LCSS
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2572817
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.96
0.500
2.000
0
98.2
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
96.8
80
120
TCLP Cadmium(Cd)
1.86
0.100
2.000
0
92.8
80
120
TCLP Chromium(Cr)
1.95
0.200
2.000
0
97.6
80
120
TCLP Lead(Pb)
1.95
0.500
2.000
0
97.7
80
120
TCLP Selenium(Se)
2.13
0.0500
2.000
0
106
80
120
TCLP Silver(Ag)
1.99
0.500
2.000
0
99.5
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41546
Sample ID: 20010911-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575565
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Cadmium(Cd)
2.18
0.100
2.000
0.001870
109
70
130
TCLP Chromium(Cr)
1.94
0.200
2.000
0
97.1
70
130
TCLP Lead(Pb)
1.89
0.500
2.000
0.07361
90.9
70
130
Sample ID: 20010911-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/20/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41546
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575566
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Cadmium(Cd) 2.20 0.100 2.000 0.001870 110 70 130 2.176 1.20 20
TCLP Chromium(Cr) 1.96 0.200 2.000 0 98.0 70 130 1.943 0.876 20
TCLP Lead(Pb) 1.93 0.500 2.000 0.07361 92.7 70 130 1.892 1.85 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 18 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: 41570B
Sample ID: MB-41570
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: PBS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581728
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
dQC+
gamma-BHC
ND
0.000500
dQC+
Heptachlor
ND
0.000500
dQC+
Heptachlor epoxide
ND
0.000500
dQC+
Methoxychlor
ND
0.000500
dQC+
Surr: TCMX
601
1000 60.1 10 119
Surr: DCB
1030
1000 103 10 119
Sample ID: LCS-41570
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: LCSS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581729
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.790
0.000500
0.500
0
158
10
130
SmQC-
gamma-BHC
0.482
0.000500
0.500
0
96.5
10
130
QC+
Heptachlor
0.516
0.000500
0.500
0
103
10
130
mQC+
Heptachlor epoxide
0.576
0.000500
0.500
0
115
10
130
QC+
Methoxychlor
0.789
0.000500
0.500
0
158
10
178
mQC+
Surr: TCMX
793
1000
79.3
10
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Revision vl
Page 19 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WTP BatchID: 41607
WO#: 20010927
10-Feb-20
Sample ID: 20010822-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: BatchQC
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586256
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.259
0.200
0.8000
0
32.4
15.2
124
QMR
2,4,5-Trichlorophenol
0.681
0.500
0.8000
0
85.2
30.6
152
2,4,6-Trichlorophenol
0.662
0.500
0.8000
0
82.7
27.6
150
2,4-Dinitrotoluene
0.893
0.100
0.8000
0
112
58
141
o-Cresol
ND
0.500
0.8000
0
61.6
26.9
132
Cresols, Total
ND
10.0
1.600
0
62.4
27.6
132
Hexachloro-1,3-butadiene
0.278
0.0400
0.8000
0
34.7
-5.3
156
QMR
Hexachlorobenzene
0.657
0.100
0.8000
0
82.1
54.3
142
Hexachloroethane
0.227
0.200
0.8000
0
28.4
1.92
131
QMR
Nitrobenzene
0.483
0.200
0.8000
0
60.4
21
135
Pentachlorophenol
0.899
0.500
0.8000
0
112
47.4
134
Pyridine
ND
0.500
0.8000
0
41.8
-10.3
64.2
m
Surr:2-Fluorophenol
0.489
1.000
48.9
9.77
146
Surr: Phenol-d6
0.525
1.000
52.5
20.7
130
Surr: Nitrobenzene-d5
0.581
1.000
58.1
13.9
156
Surr:2,4,6-Tribromophenol
0.942
1.000
94.2
27.3
183
Surr:2-Fluorobiphenyl
0.622
1.000
62.2
21.4
153
Surr: p-Terphenyl-d14
1.02
1.000
102
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WTP BatchID: 41607
WO#: 20010927
10-Feb-20
Sample ID: 20010822-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: BatchQC
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586257
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.397
0.200
0.8000
0
49.6
15.2
124
0.2588
42.2
30 R
2,4,5-Trichlorophenol
0.741
0.500
0.8000
0
92.6
30.6
152
0.6812
8.38
30
2,4,6-Trichlorophenol
0.793
0.500
0.8000
0
99.2
27.6
150
0.6616
18.1
30
2,4-Dinitrotoluene
0.944
0.100
0.8000
0
118
58
141
0.8932
5.57
30
o-Cresol
0.613
0.500
0.8000
0
76.7
26.9
132
0.4924
21.9
30
Cresols, Total
ND
10.0
1.600
0
76.6
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.470
0.0400
0.8000
0
58.7
-5.3
156
0.2776
51.4
30 R
Hexachlorobenzene
0.728
0.100
0.8000
0
91.0
54.3
142
0.6568
10.3
30
Hexachloroethane
0.378
0.200
0.8000
0
47.2
1.92
131
0.2272
49.7
30 R
Nitrobenzene
0.584
0.200
0.8000
0
73.0
21
135
0.4832
18.8
30
Pentachlorophenol
0.984
0.500
0.8000
0
123
47.4
134
0.8992
9.01
30
Pyridine
ND
0.500
0.8000
0
44.7
-10.3
64.2
0
0
30 m
Surr: 2-Fluorophenol
0.581
1.000
58.1
9.77
146
0
Surr: Phenol-d6
0.650
1.000
65.0
20.7
130
0
Surr: Nitrobenzene-d5
0.682
1.000
68.2
13.9
156
0
Surr:2,4,6-Tribromophenol
1.02
1.000
102
27.3
183
0
Surr:2-Fluorobiphenyl
0.755
1.000
75.5
21.4
153
0
Surr: p-Terphenyl-d14
1.07
1.000
107
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WTP BatchID: 41607
WO#: 20010927
10-Feb-20
Sample ID: MB-41607
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: PBS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581886
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.383
Surr: Phenol-d6
0.386
Surr: Nitrobenzene-d5
0.373
Surr: 2,4,6-Tribromophenol
0.640
Surr: 2-Fluorobiphenyl
0.375
Surr: p-Terphenyl-d14
0.859
1.000
38.3
10
109
1.000
38.6
10
109
1.000
37.3
19
120
1.000
64.0
10
120
1.000
37.5
22
117
1.000
85.9
34
116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: DUNN WTP BatchID: 41607
WO#: 20010927
10-Feb-20
Sample ID: LCS-41607
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
lient ID: LCSS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581887
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.213
0.100
0.8000
0
26.7
36.4
130 S
2,4,5-Trichlorophenol
0.610
0.250
0.8000
0
76.3
31.7
132
2,4,6-Trichlorophenol
0.642
0.250
0.8000
0
80.2
31.1
133
2,4-Dinitrotoluene
0.822
0.0500
0.8000
0
103
43.3
130
o-Cresol
0.448
0.250
0.8000
0
56.0
32.9
130
Cresols, Total
ND
5.00
1.600
0
58.1
31.7
130
Hexachloro-1,3-butadiene
0.263
0.0200
0.8000
0
32.9
31.4
130
Hexachlorobenzene
0.597
0.0500
0.8000
0
74.7
43.1
130
Hexachloroethane
0.188
0.100
0.8000
0
23.5
36.5
130 S
Nitrobenzene
0.438
0.100
0.8000
0
54.7
39.5
130
Pentachlorophenol
0.705
0.250
0.8000
0
88.1
34
130
Pyridine
0.255
0.250
0.8000
0
31.9
10
130
Surr: 2-Fluorophenol
0.434
1.000
43.4
17.1
130
Surr: Phenol-d6
0.482
1.000
48.2
10
130
Surr: Nitrobenzene-d5
0.506
1.000
50.6
32.6
130
Surr: 2,4,6-Tribromophenol
0.831
1.000
83.1
4.43
130
Surr: 2-Fluorobiphenyl
0.521
1.000
52.1
41.8
130
Surr: p-Terphenyl-d14
0.834
1.000
83.4
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 23 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20010927
10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R108707
Sample ID: LCS-R108707
SampType: LCS
TestCode: FlashPt_S(10 Units: °F
Prep Date:
RunNo: 108707
Client ID: LCSS
Batch ID: R108707
TestNo: SW1010
Analysis Date: 1/30/2020
SegNo: 2595868
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (140°F)
134
135.4 0 99.1 98 102
Z
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R108838
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_DW(4500- Units: s.u.@20.1C
Prep Date:
RunNo: 108838
Client ID: LCSW
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601762
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 20010989-006ADUP
SampType: DUP
TestCode: pH_DW(4500- Units: s.u.@21.2C
Prep Date:
RunNo: 108838
Client ID: Batch=
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601769
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.6 7.6 0.4 5 H
NOTES:
pH is an EPA field recommended parameter. Per 40 CFR 136.3, hold time is 15 minutes from collection.
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Revision vl
Page 25 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R108838
Sample ID: LCS-R108838
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@19.9C
Prep Date:
RunNo: 108838
Client ID: LCSS
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601750
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.4C
Prep Date:
RunNo: 108838
Client ID: LCSS
Batch ID: R108838
TestNo: SW9045D
Analysis Date: 2/3/2020
SegNo: 2601867
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.9 90 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 26 of 32

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20010927
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
10-Feb-20
Client:
Synagro
Project:
DUNN WTP
BatchID: R109015
Cyanide, Reactive ND 0.500
Cyanide, Reactive 9.29 0.495 10.00 0 92.9 85 115
Sample ID: RLC-R109015
SampType: RLC
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611492
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
0.557 0.500 0.5000 0 ill 50 150
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 27 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R109015
Sample ID: 20010790-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611506
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.22 0.490 10.00 0 92.2 81.6 122
Sample ID: 20010790-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109015
Client ID: Batch=
Batch ID: R109015
TestNo: SW9014
Analysis Date: 2/3/2020
SegNo: 2611507
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.08 0.481 10.00 0 90.8 81.6 122 9.218 1.47 5
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R109050
Sample ID: 20010790-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109050
Client ID: Batch=
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612561
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4520 25.0 4800 0 94.2 80 120
Sample ID: 20010790-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109050
Client ID: Batch=
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612562
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4460 25.0 4800 0 92.9 80 120 4520 1.34 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 32

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20010927
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 10-Feb-20
Client: Synagro
Project: DUNN WTP BatchID: R109050
Sample ID: MB-R109050
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109050
Client ID: PBW
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612556
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R109050
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109050
Client ID: LCSW
Batch ID: R109050
TestNo: SW9034
Analysis Date: 2/3/2020
SegNo: 2612557
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4560 25.0 4800 0 95.0 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 30 of 32

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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGa1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 20010927 RcptNo: 1
Logged by: Jacqueline Rasile 1/16/2020 9:15:00 AM
1.f•
Completed By: Jesseca E. Westfall 1/19/2020 7:13:49 PM �{G
Reviewed By:
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑ No ❑d NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑ No ❑0 NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
V
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
V
No
❑
10. Was preservative added to bottles?
Yes
❑
No
V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
V
13. Does paperwork match bottle labels?
Yes
V
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No
❑
15. Is it clear what analyses were requested?
Yes
0
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
melted ice
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
18.7
Goodl
Not Present
Page 32 of 32

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Dunn WWTP WQ Permit Number: WQ 0006101
WWTP Name: City of Dunn WWTP NPDES Number: NC 0043176
Monitoring Period: From 01/01/20 To 12/31/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
TF., -1;.. hIo+...,i+o,.,,.,+;<. ,.f,,, .,....1 Y(`l—A.,,-1-1—ill fnun »itn o+la+a•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6"
MPN
MPN/g
Coliform
power per gram
of total solids
<30,100
<34,700
<35,500
CFU/g
0
IX/yr.
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/1.5A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.I 107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32/15A NCAC 02T1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02'f.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Donrie Dukes, WWTP Supervisor
Pr arer Name and Title ( type or print)
t
,t ee AQLA-g Z-?
Signature ofPreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1.102 (26)

Cameron Testing Services, Inc. Laboratory Report
lied Synagro CT8 Prnje
Projec ; Dunn WV"iP Regutatary
Sample Information
Sarrti fad'-T M. Goad 03117120 Recal red
Analyses and Results
2003-121
yus
J. Cameron apt,
CL
Lab ID Sample 10 x a M
Anafyle
ROSUIt
iY
2003-121 -01
Fee. Coliiarm-S
<35500
cru4
355co
=18nO ERf
e 02
<30100
CFUIQ
MI00
-03
<35500
1;Fuio
myco
-04
<35500
CFU19
35500
-05
<35500
cFwg
m5oo
-06
<35600
CM11;
361500
-o7
<35500
C uIQ
35500
Geoman
<34700
2003-121 -01 3ludof Gr
TS (%)
2,82%
O.G1
03117120 ERR
-02
3-32%
a.at
-03
2,82%
001
-04
Z 82%
c.0,
-05
2.82%
OV
«06
2,82%
0,01
-07
2.82%
0.01
Report -
Review IV c

Cameron Testing Services, Inc.
NC VVWiGW Cei1 9.554 NC PITHS �Cer At 107799 US EPA, NGO' 315
Eli:
d . Fax:
4G 27028 lv�:
Mel'.. — �--
Sample Information
x �
E E }
~ 0
rrM aya W;&yri a cwra. corn
336-909-WT
sonarare
Numbor of bottles
i)
saw Temp
X1
ice (Y/N)
Rush (YIN)
Chain of Custody
Page of
CTS lair use only
Lab 1D
out
Requested Analysis
Pmarvatives: (U)rrpreserved; H(C)I, CTS Lab
H2(S)O4, HENP3, (Ha)Tl=asus"ate, Na{O)H, �❑
Other (x). lr: tV

CAMERON TESTING SERVICES
Sample Preservation Check -In Sheet
Project # 061)3 --/
Checked In By:
Date:
Temp ,9, `j °C
Ti .
Driver:
Client
Delivered
CTS
arnpled
CTS
Pickup
US Mail
I
FedEx
General
Courier
UPS
Sample No
Matrix
Grab,
Container
Checked for Preservative by p
No Change
Red H<2
p (Red)
DW I W 15
C G
P G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / W W / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
p / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
DW / WW / S
C / G
P / G
None
HCL
H2SO4
HNO3
Phos
COMMENTS:

Black River Wastewater Treatment Plant
City of Dunn
2020
Sept. 2020 Vector Attraction
Rec.—.81
Holding Tank—.66
.81 - .66 = 53.5%
81 - (.81x.66)

SECTION 6

Agricultural Lime Application Log
Year: 2020
Protect: Dunn
Field
Soil
Lime Recommendation
Tons/Acre
Date
(state -county -site
-field)
PH
(from soil analysis)
Applied
Applied
NC-CU-10-01
6.7
O.OT/AC
N/A
N/A
NC-CU-10-03
6.4
O.OT/AC
N/A
N/A
NC-CU-10-04
6.7
O.OT/AC
N/A
N/A
NC-CU-10-05
6.5
O.OT/AC
N/A
N/A
NC-CU-34-01
6.6
O.OT/AC
N/A
N/A
NC-CU-34-02
6.6
O.OT/AC
N/A
N/A
NC-CU-34=03
6.6
O.OT/AC
N/A
N/A
NC-CU-34-04
6.6
O.OT/AC
N/A
N/A
NC-CU-34-05
6.6
O.OT/AC
N/A
N/A
* Ag lime will be applied when ff
when field
and crop conditions are suitable.

SECTION 7

Page 1 of 1
Report No: 20-086-0554
Account No: 46849
Advisor: Synagro Central LLC/ PWC
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint'(D
ANALYTICAL
Client: Ray Edwards
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: 66-10
Date Received: 03/26/2020
Date of Report: 03/27/2020
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
24568 1-5
CU-10-1
MIN
6.7
0.3
302
23
25
94
1243
1243
150
7.7
96
68
26
0.5 0
Crop Recommendations:
1- Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
50
P205
0
K20
160
S
17
Mn
2
Mn-AI
63
Zn
0
Cu
0
B
0
Mg
0
Last Crop
24569 1-5
CU-10-2
MIN
6.7
0.2
225
33
15
94
233
233
65
3.9
94
62
27
0.9 0
Crop Recommendations:
1- Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
50
P205
0
K20
160
S
22
Mn
2
Mn-AI
63
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
24570 1-5
CU-10-3
MIN
6.4
0.3
72
19
17
94
110
110
30
3.2
92
60
28
1.1 0
Crop Recommendations:
1- Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
50
P205
30
K20
160
S
21
Mn
2
Mn-AI
67
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
24571 1-5
CU-10-4
MIN
6.7
0.2
147
16
12
63
360
360
100
3.8
94
64
27
1.1 0
Crop Recommendations:
1- Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
50
P205
0
K20
160
S
23
Mn
2
Mn-AI
44
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
24572 1-5
CU-10-5
MIN
6.5
0.3
135
20
19
119
328
328
75
4.1
93
62
27
1.1 0
Crop Recommendations:
1- Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
50
P205
0
K20
160
S
20
Mn
2
Mn-AI
81
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL017500
Client:
Harold Eldridge
Advisor:
Ryan Copeland
Predictive
8373 Rhodes Pond Rd
SYNAGRO
Dunn, NC 28334
284 Boger Road
.'..,$' Soil Report Mehlich-3 Extraction
Mocksville, NC27028
_
Sampled County: Cumberland
Links to Helpful Information
Client ID: 295037
Advisor
ID: 499503
Sampled: Received: 11/25/2020 Completed: 01/13/2021 Farm: CU-34
Sample ID: CU341
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 10
200
0 0
pH$
0
0
0
Note: 12 Note:
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.22 1.17 6.3 89 0.7 6.6 58 16 56 32
31
64
46
235
235
137
0.1 2
Sample ID: CU342
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0
200
0 0
pH$
0
0
0
Note: 12 Note:
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.27 1.21 6.4 89 0.7 6.6 63 16 56 31
30
65
47
247
247
142
0.1 2
Sample ID: CU343
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0
200
0 0
pH$
0
0
0
Note: 12 Note:
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.27 1.18 6.5 89 0.7 6.6 74 16 57 31
31
66
47
261
261
150
0.1 2
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL017500
Harold Eldridge
Page 2 of 3
Sample ID: CU344
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0
180-220 0
200
0
0
pH$
0
0 0
Note: 12 Note: $
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.22 1.17 6.3
89 0.7 6.6 69 15
57 31
35
60
44
199
199
149 0.1
2
Sample ID: CU345
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0
180-220 0
190
0
0
pH$
0
0 0
Note: 12 Note: $
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.32 1.14 7.0
89 0.8 6.6 110 18
57 31
35
67
48
254
254
189 0.0

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO17500
Harold Eldridge
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm