WQ0018525_Residual Annual Report 2020_20210224

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?*
Annual Report Year*
Permit Number (IR)*
Applicant/Permittee
Email Notifications
........................................................................................................................................................................
Does this need review by the hydrogeologist?*
Regional Office
CO Reviewer
Admin Reviewer
* Annual Report
* Residual Annual Report
r Additional Information
r Other
2020
WQ0018525
Barnes Environmental Waste and Hauling, Inc.
0 Yes r No
Wilmington

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd
.......................................................... ronc su_ -
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
........ ......... ..........................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363121396
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
W00018525
Fbs Current Existing perm number
Applicant/Permittee Address*
PO Box654, Newport, NC 28570
Facility Name *
Barnes Environmental RLAP
Please provide comments/notes on your current submittal below.
2020 Class B Annual Report WQ0018525
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Barnes Environmental 2020 Annual Report
29.79M6
WQ0018525.pdf
Upload only 1 PCFdocurrent (less than 250 M3). Miltiple docurrents must be combined into one PDF file unless file is larger than
upload linit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
ew"2W �W'&"fe
Submission Date 2/24/2021

2020 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2021

willcox&mebe
SOIL SOLUTIONS
February 24, 2021
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9th Floor, Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2020 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling, Inc.
WMSS, Inc. Project No. 15-02 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental
Waste and Hauling, Inc. (Barnes Environmental Waste). WMSS compiled this report using
data gathered during the compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this Iland application
program please do not hesitate to contact Mr. Steve Barnes, with Barnes Environmental
Waste 252-241-5014 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/ResiduaIs Operator
#22753
Enclosure(s)
cc Barnes Environmental Waste
Shared\WMSS Projects12015115-02 Barnes Environmental12020 Annual Report12020 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summertield Road/ SummerField, NC 27358 / Rob 336.339.9128 or
Martin 336.312,1396 / www.wiltcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
H Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00018525 County:
Carteret
Year: 2620
racility Name tas shown on permit): Barnes Environmental Waste and Hauling, Inc.
Land Application'Qperator: Steven M. Barnes .Phone:. [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yves: ❑ No - If No, skip Part A, and Part 9 and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
number of.
Total number of fields.utilized for lam
Total amount of dry tons applied during the
Total number of acres utilized for lam
Part B - Annual Com Hance Statement:
;ion fields in the permitj 6
lioation during tli� year; 5
for all application sites: .29612.
Facility was compliant during calendar.year 2020 with all conditions of the land application permit
(including but not limited to items 1.-13 below) issued by the Division of Water Quality. El 'Yes ❑ No
If no please, provide a written description Whythe facility was not compliant, the dates, and explain -corrective
action taken.
1) only- residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at'least 6,0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three _(3) cop.ies
of laboratory results are attached.
4) Annual TCLLP analysis (if required) was -performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in I5A NCAC 02T ,1105(a) or the -Pollutant
Loading Rates in 15A NCAC 02T .1 i05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 Ill we're complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements'in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the pernnit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface wafers has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of la-v, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for.subinitting false information, including the
possibility of fines and imprisonment.for knowing violations."
Steven M. Barnes, President �� _1-96 , - l
Permittee Name and Title (type or print) Signature of Permittee Yate
Signature of Preparer* Date Signature of rand Applier Date
(if different from Permittee) (if different from Permittee and Preparer):
* Preparer is defined in 40 CFR Part 503,9 (r) and 15A NCAC 02T .1:102 (26)
DENR FORM AM i9mfrf m

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

Permit Number WOODIS525
Facility Name Barnes Environmental
NPD5S # See Below
WWTP Name See Below
RE91DUAl . ANAI MMS i1ATA
ANNUAL RESIAUAL.SAMPLINC SUMMARY FORM
Attach Mis roan (o the ccrrespondina laheraiegranalysts,
Please notelhat pourparmit,mayContain adddlanal parameters to be analyzed lhan.tlmv required m be svmmarizad on ihts:form
Laboratory 1) Environment 1. Inc,
2 Environmental Chemists, Iris_
3
Woes r
W❑OON059
W00013676 I W00005173
I V1-15-17 I VMr-13 I V1-14 -13
I Nmnnnmem4
I V-Z-13
IWC:0006863
VI-0219
WWrP Name
Allanlic Stallon
Beanons Reach Cape Royal
I CC Sass I Cedar paint Colony by Sea
Dunesrape
Eight 112 Marina
Genesis Candor
Hampton Suiles
Compm ed1Grab
01109/20
01/09120 1011W20
10/06120 10/20120 01l02120
01102/20
03126120
02/04120
01l02120
PCrccnt SOWS
0.63
2.12 1.67
Z68 1.97 1.27
1.33
0.73
212
1.81
Arsenic
.250
270
28.10
27.10
52,30
2.50
2.50
7.60
4.50
2.50
Cadmium
O.S1
1.00
22.90
18_10
24.'60
1.30
0,51
1.10
1.10
0.50
copper
606.00
1.341.00
349.00'
9.93.00
563:00
324.00
493.00
1.159.00
643.00
1,175.00
Lead
13.00
16.00
44.00
18,10
24.60
13.00
9A0
28.00
16.00
4.10
Mercury
0.12
0.19
0.96
0,57
0.al
0.21
0.12
0.62
0.28
4_i5
Ainlyhdenum
5_00
5.00
22.90
18.10
24.60
5.00
7-00
5.00
7,00
T.00
Nickel
13.00
10.00
22.90
18.10
24.60
16.00
9.00
10.00
13,00
12,00
Selenium
5,00
1 5.00
22,90
18.10
24.60
5.00
5.00
5.00
5.00
S.Da
Zinc
96600
1a26.00
2,980.00
1.090A0
1,130.00
1.969.00
606.00
2,318.00
1.245.00
776.00
TKN
61.040.00
71,550.00
55.400,00
60,500.00
54,600,00
69,320.00
77,700,00
50.630.00
62.970.00
21.110,00
Ammonia -Nitrogen
58A3
1,980.00
6,160.00
2.73
12,700,00
637.20
71320
59.82
2;340,00
1,445.00
Nitrate•Nitrngen
167.00
9.77
237.00
939.00.
7.04
1,98
3.9Z
144.60
.141.50
6.95
Total Phosphorus
14,840,00
18,730,00
1S,000-00
15.100.00
17,400:00
11,550.00 1
15.810.00 1
17.290.00
7.603.00
12,780.00
1�&, j 1�21
(SIGNATURE OF PREPARER) DATE
I cer5fy, under penalty of law,lhat this documenl-was prepared under my direction or supervision in, accordance with a system designed
to aasurethat qualifred personnel property gathered and evaluated the information submitted I am aware that Were, are significant
penat0es for submitting false information. including the possibi4y.00ines and imprisonment for knowing violations,
Page 1

PerrokNumber VVGOO18525.
Facility Name Same& EWronrnerital
NPDES# See Below
VVWTP Name See Below
RESMUAL ANALYSIS DATA
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach thii form to the carrsprnrdmg iaagratory analysis:
Please note that-yourperreit may contain addlignat paramaiam to be anaq zed titan those regeored to tra swema&id an this form.
Laboratory III EniilronmeM 1. lrie
2 Environmental Chemists .lnc..
3)
NPDES# W00013027
Vl-i47
W00007103
WQo01 m
Vi-12-17
WQOD24756
VI-20-15
W WTP Name Sea Isle Pfanla5on
Sea Spray
Sound of the Sea
SOuthWnds.Candas
Summer Winds
The Grove
Whater Inn
Composs�ed/Grab 02127120
02/04/20
03110/20
0=7120
01114120'
02171l20
11105/20
Pasent solids 0-57
1,11
1.06
1.20
1.54.
1.65'
0.39
Arsenic
2.50
2.50
2.50
2 50
2.50
3.40
2.50.
Cadmium
'2.00
0.50
OA7
0.96
0.79
0.50
0.50
Copper
249.00
1,015.00
969.OD
786.00
599.00.
'83.00,
712.,DD-
Lead
48;00
13.00
.16.00
15.00
10,00
2.90
6.90
Mercury
0.17
0.29
0.12
0.23
0.17
0.08
0.12
Mplybd6num
Nickel
5.00
moo
5.00
11.00
5.00
7.00
5.00
.9.00
5.00
1 i0.00
5.00
7.00.
6.00
$.00
Selenium
5.00
5.00.
SAO
5.00
5.00:
5.00
5:00
Tmc
Turf
1.27-1.00
38,490.00
871.00
58.140.00
968,00
60.080.00
1.2B4.00
47,690.00
2,062.00
64.410.00
382.OG
59,700:00
854.00
33.540.00
Ammonla-Mitrogen
46.64
.362.10
2.937.00
30.4
1.651.00
2,572-00
66.61
Mrale-Nitrogen,
Total Phosphorus
48.62
17,290.00
.1143
T760.00
3.99
14.800.00,
29.92
14.520.00
67.78
16.840.00
7.92
17100.00
337.00
13,520.00
(SIGNATURE 4F PREPARER) DATE r /
l certify, udder penalty of law; that dilsdocument was preparers under mfdlrecdon orsupervision, in accordance with a system designed
!b assure that gtialdied persanrlel pnpkly gathered and evaluated the infarmafion submitted. I am aware that there are significant
pertallies for submiiting'false Worrnation, including the possibility dffines.and imprisonment iarknowing violations.
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 9, 2020
Permit No. WQ0018525
Atlantic Station 0.63 % Solids
12AI H (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0,723
61,040.000
I22.080
Phosphorus
0.263
14,840.000
29,680
Potassium
0.449
4,481.000
8.962
PAN (injected)*
0.270
2,695.700
5.391
PAN (surface)*
0,243
2,432.200
4.864
Ammonia Nitrogen
0.053
58.430
0.117
Calcium
3.558
42,992.000
85.984
Calcium Carbonate E .
---
---
Magnesium
---
2.913.000
5.826
Sodium
---
26,750.000
53.500
Sulfur
___
___
---
Nitrate N 1 Nitrite N
---
157.800
0,316
Barium
---
---
---
SAR
2.67
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M !K )
Aluminum
---
4,464.00
8.928
Arsenic
---
2,50
0.005
75
Cadmium
--- 1
0.57
0.001
85
Chromium
---
17.000
---
---
Copper
---
606.00
1,212
4,300
Lead
---
13.00
0.026
840
Mercury
---
0.12
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
13.00
0.026
420
Selenium
---
5.00
0.010
100
Zinc
---
966.00
1.932
7,500
Environment I, Incorporated 108A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization state)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
ATLANTIC STATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
Aluminum, (dry wt. basis), mglkg
4464
02/03/20
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/04/20
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
42992
01/31/20
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.57
01/30/20
MTM
311313-04
Copper (dry wt. basis), mg/kg
606
02/03/20
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mglkg
17
01/31/20
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
13
01/29/20
MTM
3113E-04
Magnesium (dry wt. basis), mg/kg
2913
02/03/20
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.12
01/16/20
MTM
EPA7471B
Nickel (dry wt. basis), mglkg
13
02/03/20
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4481
02/03/20
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
02/05/20
MTM
31138-04
Sodium (dry wt. basis), mg/kg
26750
02/03/20
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
966
02/03/20
LFJ
EPA200.7
Total Solids, %
0.63
01/13/20
KDS
254OG-11
TKN (dry wt.), mg/kg
c 61040
01/23/20
AKS
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg
c 58.43
01/14/20
DTL
350.1 Rz-93
Phosphorus, T. (dry wt.), mglkg
c 14840
01/14/20
BLD
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 157.8
01/14/20
TLH
353.2 IU-93
Plant Available Nitrogen, mg/kg
24580
01/23/20
SEJ
Molybdenum (dry wt. basis), mg/kg
<5.0
01/31/20
LFJ
EPA200.7
Drinking Water rD: 37715
Wastewater 10; 10
PHONE [phone]
FAX [phone]
ID#: 108 A
DATE COLLECTED: 01/09/20
DATE REPORTED : 02/14/20
RF,VIEWFJi >
n Uncertified data. DWR done not offer non -aqueous certification for Chia analytical procedure.

CHAIN OF CUSTODY. RECORD
Environment i, Inc.
Pace _ 1 of 1
PA- Box 7085,114 palanont Dr,
Greenville, NC 27858
D E -nON
CHLORINE NaAPALQEDATCALLEanoN.
eavironmentlinc.com
Phone [phone] • Fax (Z52).756-0633
CHL:ORINM
CHECK (iA8)
pH
CLIENT: lop,.A Week:7
LTV Ca LPL La. 1tiai.
�••l
CONTAINERIYPF- PIG
ATI..ANTIC STATION (6'ORTII�
NE
:P P P
P p I'
CHEMiCALPFiESER►IATION
AUL DAN FORTIN
FORTIN.CONTRACT SERVICES
p.O. BOX 4188
—
m
in
A NONE" D NAOH
EMERALD ALD ISLE NC 28594,
o` E -
uu
E-HCL
OW)393-8720
ui-w o.
a;o
coB'-FiNO.
Lu
0-Fz60, F-ZINC ACETATEINAOH
<
G - NATHIOSULFATE
COLLECTION
a� �� Z Z
SAMPLEt OCAiiON• DA
TIME
�o a l;. F z 4
CLASSIRCATIOR
WASTEWATER (NPDES}
DRiNKINGWATER
DARIGW.
SOLIDWASTESECTION'
CHAIN OF CUSTODY (SEAL), MAINTAINED
D U RI N CYEHN MENTID ELIVERY
JJ N
I
SAMPLES COLLECTED 8`F
IHE
(Ple se Pra)
�e
. .
SAMPLES RECEiVEO IN LAB AT °CTi
RE I DUISHED BY.(S1G.) (SAMPLFR) . AiFlil
REC Y(SIG j
1, DAI hyn.mE
OOMIuZENTS:
�
ISHED BY (51G) DAR-J iME
REGEVEI) BY (SIG.
DATEMME
RELJNQIIISHED BY:(SIG.) DATEMW;
RECENED"BY SSIG)
DATEIiIME.
Sampler must place a°C°.for composite sample or a "G° for. .
PLEASE READ:Instruetiori,s for completing this form on the.reverse side.
Grab sample in the blocks above for each..parameter requested. N O 3 7 5 8.6"6
- 2
FORM n5

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 9, 2020
Permit No. WQ0018525
Beacons Reach 2.12 % Solids
6.6 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Top
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.155
71,550.000
143.100
Phosphorus
1.873
18,730.000
37A60
Potassium
0.621
6,213,000
12A26
PAN (injected)`
2.286
22,860.770
45.722
PAN (surface)*
2.187
21,870,770
43.742
Ammonia Nitrogen
0.198
1,980,000
3.960
Calcium
3.491
34,909.000
69.819
Calcium Carbonate E .
---
Magnesium
---
3,273.000
6.546
Sodium
---
9,096.000
18.192
Sulfur
Nitrate N / Nitrite N
---
9.770
0.020
Barium
---
---
---
SAR
1.81
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3,187.00
6.374
Arsenic
---
2.70
0.005
75
Cadmium
---
1.000
0.002
85
Chromium
---
13.000
---
---
Capper
---
1,341.00
2.682
4,300
Lead
---
16.00
0.032
840
Mercury
---
0.19
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
10.00
0.020
420
Selenium
---
5.00
0.010
100
Zinc
---
1,126.00
2252
7,500
Environment 14 554A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

r
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
BEACON'S REACH I/POND (HYDROTECH)
ATTN: DON O'MARA
HYDROT'ECH
P.O. SOX 4602
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting)
6.6
01/09/20
TMR
4500HB-11
Aluminum, (dry wt. basis), mglkg
3187
02/03/20
LFJ
EPA200.7
Arsenic (dry wt. basis), mglkg
2.7
02/04/20
N1TM
3113E-04
Calcium (dry wt. basis), mglkg
34909
01/31/20
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.0
01/30/20
MTM
3113E-04
Copper (dry wt. basis), mg/kg
1341
02/03/20
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
13
01/31/20
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
16
01/29/20
N1TM
3113B-04
Magnesium (dry wt. basis), mg/kg
3273
02/03/20
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.19
01/16/20
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
10
02/03/20
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
6213
02/03/20
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
C 5.0
02/05/20
MTM
311313-04
Sodium (dry wt. basis), mg/ltg
9096
02/03/20
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1126
02/03/20
LFJ
EPA200.7
Total Solids, %
2.12
01/13120
KDS
254OG-11
TICN (dry wt.), mg/kg
c 71550
01/23/20
AILS
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg
c 1980
01/14/20
DTL
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 18730
01/14/20
BLD
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 9.77
01/14/20
TLH
353.2 112-93
Molybdenum (dry wt. basis), mg/kg
5
01/31/20
LFJ
EPA200.7
Drinking Water ID: 37715
WaetewdtGr ID: 10
PHONE [phone]
FAX [phone]
ID#: 554 A
DATE COLLECTED: 01/09/20
DATE REPORTED : 02/14/20
REVIEWE"
c Uncertified data. DWR does not offer non -aqueous certification for thin analytical procedure.

CHAIN OF CUSTODY RECORD
Environment 1,Inc.
PA_ Box 7085' 114 Oakmont Dr.
Greenville, WC 27858
environmentlinc.com
DISH4FEC-nON.
Phone {252) 756-6208: • Fax [phone]
CM,OREqE
CLIENT: 554 A Week: s
❑w
IP
4A4���Za
BEP,COWS-REACE1 IIPOND iHYDAOTECR)
NONE
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P
P P P P
ATTN.- DON O'MARA
HYDRO.1'IECH
JA
JA JA
p_O_.BOg 4602
A A
A A
E M ERALD ISLE NC 28594.
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[phone]
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SAMPLELOCATION DATE TIME
a o
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lodge Sample f-�- f�GjcU
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iHED BY (SIG.) (SAMPLER) DATEffIME R .8Y(SIG.)
G4iHED {51G}, DATEIIIME REG BY.(Sl
3HED BY (SIG:) DATEi1ME RECEIVED BY (S a)
PLEASE READ instructions for completing this farm on the. reverse: side.
FORM'#5
Page 1 of 1
CHLORINE NEUTRALIZED AT COU-EC11ON
pH CHECK (LAB)
CONTAINERTYPE, PIG.
CHEMICALPBESERVAnON
A -NONE D-NAOH
B-HNO3 E-HCL
w
C - H25O, F: ZINC AwrATEmAOH
G-NATHIOSULFATE
ii
CIAABSIF0fl0N:
WASTEWATEA(NPDES)
DAINI(INGWAW
L ) DWR/GVV
SOLIDWASTESECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURINPMENT/DELIVERY
Y.. N
SAMPLES COLLECTED BY_
(Please Punt) .
SAMPLES RECENED IN LABAT EJ `o' °C
Sampler must place.a "C° for composite: sample.or a "G" for
Grab sample in the blocks above for -each parameter requested. N D 375315

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment PIant
Date Sampled: October 13, 2020
Permit No. WQ0018525
Cave Royal Dolphin, 1.67 % Solids
7.62 EH
Parameter
%
Mg/Kg Dry Weight
(% x 10,OOp)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
5.540
35,400.000
110.800
Phosphorus
1.500
15,000.000
30.000
Potassium
0.114
1,144,000
2.288
PAN (injected)`
2.117
21,169,000
42.338
PAN (surface)*
1.809
18,089.000
36.178
Ammonia Nitrogen
0.616
6,160.000
12,320
Calcium
2.110
21,100.000
42.200
Calcium Carbonate E .
---
---
Magnesium
---
1,520.000s.040
Sodium
---
3,700.000
7.400
Sulfur
Nitrate N / Nitrite N
---
237.000
0.474
Barium
---
Chloride
---
Iron
---
_--
_--
Aluminum
---
9,100.00
18,200
Arsenic
---
28.10
0.056
Cadmium
---
22.90
0,046
Chromium
---
39.500
---
Co er
---
349.00
0.698
Lead
---
44.00
0.088
Mercury
---
0.958
0.002
Molybdenum
---
2290
0.046
Nickel
---
22.90
0.046
Selenium
---
22.90
0.046
Zinc
---
2,980.00
5.960
EUVirochem # 2020-17443
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.86
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 > 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington. Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report: Nov 02, 2020
Post Office Box 4188
Customer PO #:
Emerald Isle NC
28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2020-17443
Project ID: Cape Royal Dolphin
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
2044605 Site: Sludge
10/13/2020 8:45 AM Solid/Sludge Kevin Stanley
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
9100mg/kg
10/2012020
Arsenic
EPA 200.7
28.1 mg/kg
10/20/2020
Cadmium
EPA 200.7
<22.9 mg/kg
10/20/2020
Calcium
EPA 200.7
21100 mg/kg
10/20/2020
Chromium
EPA 200.7
39.5mg/kg
10/20/2020
Copper
EPA 200.7
349 mg/kg
10/20/2020
Lead
EPA 200.7
44.0 mg/kg
10/20/2020
Magnesium
EPA 200.7
1520mg/kg
10/20/2020
Molybdenum
EPA 200.7
<22.9 mg/kg
10/20/2020
Nickel
EPA 200.7
<22.9 mg/kg
10/20/2020
Potassium
EPA 200.7
<1144 mg/kg
10/20/2020
Selenium
EPA 200.7
<22.9 mg/kg
10/20/2020
Sodium
EPA 200.7
3700 mg/kg
10/20/2020
Zinc
EPA 200.7
2980 mg/kg
10/20/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
237 mg/kg
10/14/2020
Total Solids (%)
SM 2540 B
1.67 %
10/14/2020
pH
SM 4500 H B
7.62 units
10/27/2020
Ammonia Nitrogen
SM 4500 NH3 C
6160 mg/kg
10/15/2020
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
55400 mg/kg
10/15/2020
Total Phosphorus
SM 4500 P F
15000 mg/kg
10/19/2020
Mercury
Sw845 7471 B
<0.958 mg/kg
10/30/2020
Comment: Sludge residuals,
except pH, reported on a dry weight basis, pH reported on an as received basis.
Reviewed by:
Report #.: 2020-17443 P— 0 �r 9

Environmental Chemist, Inc., Wilmington, NC tab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
l Date: 4
Client: I`�Y}`lri --C�,�v aID,5J 20 Report Number: 2(�-1�4�
Receipt of sample:
SCHEM PickuW Client Delivery ©
1UPS ❑ FedEx ❑ Other ❑
❑ YES
10
NO
N/A
1. Were custody seals present on the cooler?
❑ YES
❑
NO
N/A 12,
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank I Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 IR Gun Correction Factor T. 0.0
❑ YES
10
NO
3. if temperature of cooler exceeded VC, was Project Mgr./QA notified?
YES
J11
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
10
NO
7. Were collection date and time listed on the COC?
iT YES
❑
NO
S. Were tests to be performed listed on the COC?
YE5
❑
NO
9. Did samples arrive in proper containers for each test?
YESO
10. Did samples arrive in good condition for each test?
YESO
11. Was adequate sample volume availableT
O
12. Were samples received within proper holding time for requested tests?
O
13. Were acid preserved samples received at a pH of <2?
YES
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
I YES
10
NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): Hz504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Vote: Notify customer service Immediately for incorrectly preserved samples. Obtain a new sample or
iotify the state lab if directed to analyzed by the customer. who was notified, date and time: _
/olatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
'C

6602 Windmill Way ton, NC
ming
ENVIRONMENTAL CHEMISTS, INCOFFICE: 9 0-3 2-0223'IFAX 910 392-4424$
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Fortin Contract Services PROJECT NAME: Cape Royal Dolphin REPORT NO:
ADDRESS: Post Office Box 4188 CONTACT NAME: Dan Fortin PO NO:
Emerald Isle, NC 28694 REPORT TO: PHONEIFAX'
COPY TO: email:
Sampled l3 : 1 _ SAMPLE TYPE: I = influent, E - Effl t loll - W it
IdentificationSample
CompositeEffluent -
ION NIMMMM-
Effluent - Grab
-Ma Ju November
�
=MEN
mm-=
mm�=
„ m
4
n
E°
o a
r
g W
in
m?
uen
PRESERVATION
,
-
e , ST
-
Stream,
SO = Soil, SL = Sludge, Other:
ANALYSES REQUESTED
i
a
o
o
0
BOD, TSS, NO2
G
G
C
P
�'xi
h
NH3, Total Phos, TN, TKN, NO3
G
G
C
P
G
G
-G7
ye
Fecal
G
C
P
G
G
C
P
G
G
X
TDS, Chloride
C
P
G
G
SLu
G6�5
C
P
G
G
Transfer Relinquished By: DatefTime Received By: Daterrime
2.
Temperature when RKeDeivea °C: } Accepted: eject Resample Requested:
Delivered = _ _ _Received By -
Date: 12-I3-LID Time:
Comments:_Due March, July, Nov. TURNAROUND:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 6, 2020
Permit No. WQ0018525
CC Sass 2.68 % Solids
6.22 DH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.050
60,500,000
121.000
Phosphorus
1.510
15.100.000
30.200
Potassium
0.277
2,770.000
5.540
PAN (injected)*
L909
19,091.6I1s8.183
PAN (surface)*
1.909
19,089.746
38.179
Ammonia Nitrogen
0.000
3.730
0.007
Calcium
2.140
21,400.000
42.800
Calcium Carbonate E .
---
---
Magnesium
---
3,570.000
7.140
Sodium
---
5,300.000
10.600
Sulfur
---
___
---
Nitrate N / Nitrite N
---
939.000
1.878
Barium
---
---
---
SAR
1.44
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,620.00
5.240
Arsenic
---
27.I0
0.054
75
Cadmium
---
18.10
0.036
85
Chromium
---
30.800
0.062
---
Copper
---
993.00
1.986
4,300
Lead
---
18.10
0.036
840
Mercury
---
0.567
0.001
57
Molybdenum
---
18.10
0.036
75
Nickel
---
18.10
0.036
420
Selenium
---
18.10
0,036
100
Zinc
---
L,090.00
2.I80
7,500
Cnvirochem ff 2020-16943
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammania N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910,347.5843 Lab/Fax
info@envi ronmen talchemi sts. cam
Fortin Contract Services
Date of Report: Oct 21, 2020
Post Office Box 4188
Customer PO #:
Emerald Isle NC
28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2020-16943
Project ID: CCSASS
Lab ID Sample ID:
Collect DatelTlme Matrix Sampled by
20-43338 Site: Sludge
10/6/2020 9:15 AM Solid/Sludge Kevin Stanley
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
2620mg/kg
10/12/2020
Arsenic
EPA 200.7
27.1 mg/kg
10/12/2020
Cadmium
EPA 200.7
<18.1 mg/kg
10/12/2020
Calcium
EPA 200.7
21400 mg/kg
10/12/2020
Chromium
EPA 200.7
30.8 mg/kg
10/12/2020
Copper
EPA 200.7
993 mg/kg
10/12/2020
Lead
EPA 200.7
<18.1 mg/kg
10112/2020
Magnesium
EPA 200.7
3570mg/kg
10/12/2020
Molybdenum
EPA 200.7
<18.1 mg/kg
10/12/2020
Nickel
EPA 200.7
<18.1 mg/kg
10/12/2020
Potassium
EPA 200.7
2770 mg/kg
10/12/2020
Selenium
EPA 200.7
<18.1 mg/kg
10/12/2020
Sodium
EPA 200.7
5300 mg/kg
10/1612020
Zinc
EPA 200.7
1090 mg/kg
10/12/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
939mg/kg
10/09/2020
Total Solids (%)
SM 2540 B
2,68 %
10/07/2020
pH
SM 4500 H B
6.22 units
10/13/2020
Ammonia Nitrogen
SM 4500 NH3 c
<3.73 mg/kg
10/08/2020
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
60500 mg/kg
10/09/2020
Total Phosphorus
SM 4500 P F
15100 mg/kg
10/09/2020
Mercury
SW8467471B
<0.567mg/kg
10/07/2020
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by:
Report #:: 2020-16943 D- 0 -f o

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: Ccspv-"_:�S
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Date: 1 d kJ 2D Report Number: Zu--- 1 n4 3
Receipt of sample:
❑ YES ❑ NO
ECHEM PickupA Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑
IN N/A 1. Were custody seals present on the cooler?
❑ YES
ID NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor "C: 0.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
S. Were sample ID's listed on the COC?
YES
YES
❑ NO
❑ NO
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the CDC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume availableT
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a pH of <27
❑ YES
© NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
Rk YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCl NaOH
If more than one preservative is needed, notate in comments below
Note: !Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC, QA.002 Rev 1

Analytical & Consulting Chemists
CLIENT: Fortin Contract Services
ADDRESS: PO BOX 4188
EMERALD ISLE, NC 28694
Sampled By:
Sample Identification
Influent
1.
2.
Temperature when
Delivered By:--
Comments:
Fti \ }`�"' � ® E T " L E I T ' INC OFFICE 910-392-0 23 FIAX 910-3 2-4424
NCDE:NR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: CCSASS
REPORT NO-
Z49 —16 1 q
CONTACT NAME:
PO NO:
REPORT TO: Dan Fortin
PHONE/FAX:
COPY TO:
email:
SAMPLE TYPE: I = Influent,
E = Effluent,W
= Well,
ST = Stream, SO =
Soil, SL = Sludge, Other:
action
m g _
o PRESERVATION
06
o° o a r E
m= 7Cft-1
3
0
0 O
ANALYSIS REQUESTED
ime
Tem
cn
_ _
O
I
G G
X
BOD, TSS
C P
G
X
TKN, O&G
C P
G G
C P
G G
00
C �
I
X
CBOD, TSS, NO2
P
L
G G
X
TKN, NO2+NO3, NO3
C P
3
r
G
X
FECAL
Is
C P
G G
C P
G I G
C P
G I G
cepted:
"Received By:
me
11: 00
Received Ely: Date/Time
rc� -,,- zd /x
Resample Requested:
Date 9 6 —Z'D �Time:
TURNAROUND:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 20, 2020
Permit No. WQ0018525
Cedar Point 1.97 % Solids
7.42 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.460
54,600.000
109.200
Phosphorus
1.740
17,400.000
34.800
Potassium
0,355
3,550.000
7.100
PAN (injected)*
2.528
25,277.040
50554
PAN (surface)*
1.893
18,927.040
37.854
Ammonia Nitrogen
1.270
12,700.000
25.400
Calcium
3.320
33,200.000
66.400
Calcium Carbonate E .
---
---
---
Magnesium
---
3,390.000
6.780
Sodium
---
4.360.000
8.720
Sulfur
---
---
._.
Nitrate N / Nitrite N
---
7.040
0.014
Barium
---
---
Chloride
---
....
---
Iron
---
---
---
Aluminum
---
9,640,00
19.280
Arsenic
---
52.30
0.105
Cadmium
---
24.60
0.049
Chromium
---
28.800
---
Copper
---
563.00
1.126
Lead
---
24.60
0.049
Mercury
---
0.81
0.002
Molybdenum
---
24.60
0.049
Nickel
---
24.60
0.049
Selenium
---
24,60
0.049
Zinc
---
1,130.00
2.260
Envirochem# 2020-17839
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or c detection limits are listed as detection limits
for calculation purposes.
SAR
0.85
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347,5843 Lab/Fax
info@environmentalchemists,com
Fortin Contract Services Date of Report: Nov 13, 2020
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report #: 2020-17839
Project ID: Cedar Point Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
20-45525 Site: Sludge 10/20/2020 8:35 AM Solid/Sludge Client
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7
9640mg/kg
11/04/2020
Arsenic
EPA 200.7
52.3mglkg
11/10/2020
Cadmium
EPA 2007
<24.6 mg/kg
11/04/2020
Calcium
EPA 200.7
33200 mg/kg
11/04/2020
Chromium
EPA 200.7
28.8mglkg
11/04/2020
Copper
EPA 200.7
563 mg/kg
11/04/2020
Lead
EPA 200.7
<24.6 mg/kg
11/04/2020
Magnesium
EPA 2007
3390mglkg
11/04/2020
Molybdenum
EPA 200.7
<24.6 mg/kg
11/04/2020
Nickel
EPA 200.7
<24.6mg/kg
11/04/2020
Potassium
EPA 200.7
3550 mg/kg
11/0412020
Selenium
EPA 200.7
<24.6mglkg
11/04/2020
Sodium
EPA 200.7
4360 mg/kg
11/04/2020
Zinc
EPA 200.7
1130 mglkg
11 /04/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
7.04mg/kg
10/21/2020
Total Solids (%)
SM 2540 B
1.97 %
10/26/2020
pH
SM 4500 H S
7.42 units
10/27/2020
Ammonia Nitrogen
SM 4500 NH3 C
12700 mg/kg
10/21/2020
Total Kjeldahl Nitrogen (TKN)
SM 4500 arg B
54600 mg/kg
10/22/2020
Total Phosphorus
SM 4500 P F
17400 mg/kg
10/21/2020
Mercury
SW046 7471B
<0.812 mg/kg
10/30/2020
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by:
Reporl M: 2020-17s39 Paoe 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392,0223
Sample Receipt Checklist
Client: Date: 0 b Report Number: � Q — -CL�� C!
Receipt of sample:
ECHEM Pickup Client Delivery ElUPS ElFedEx ❑ Other ❑
❑ YES
❑ NO
N/A 1. Were custody seals present on the cooler?
❑ YES
El NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank 7 Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 lR Gun Correction Factor °C: 0.0
❑ YES
I E7 NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
I ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
tq YES
❑ NO
9. Did samples arrive in proper containers for
YES
❑ NO
each test?
10. Did samples arrive in good condition for each test?
YES
❑ NO
11, Was adequate sample volume availableT
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
IS. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *#
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
ID NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation, (Must be completed for any sample(s) incorrectly preserved or with headspace)
ISample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°C

Analytical & Consulting Chemists
CLIENT: Fortin Contract Services
ADDRESS:
ENVIRONMENTAL CHEMISTS ngton, NC 28405
1 OFFICE- 910-3 2-0223 FiAX 910-392-4424
NCDENR: DWO CERTIFICATION 4 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: Cedar Point WWTP REPORT NO: D.�) I� 8
ACT NAME: Dan Fortin
PO NO:
REPORT TO: Dan Fortin PHONEIFAX:
COPY TO: email:
Sampled 13 SAMPLE TYPE• ! -Influent E - Effl W -
Sample Identification
Collection
1
'
M
r�
- uent, - Well, ST = Stream, SO = Soil, SL = Sludge, Other:
B
e
in
PRESERVATION
Q
o`
p
r 5
o
m m
z
o
0
o
u�7
ANALYSIS REQUESTED
tip
�+
gz
i
=
=
s
I
a
c°� _
"JEMN
im
W'JJJ,TKN,
NH3,NO3
Fecal Coliform
�NM1111111i
MMMMI
Iloilo
MM
MM
Monosson
Transfer Relinquished By: DatefTime Received By: Date/Time
9=30 - ,� 0 - zo �o
7.
Temperature when Received ° : 4. Accepted: Rejected: Resampie Requested:
Delivered By:Received B Date:c� Z� ` ��7 Time:
Comments: TURNAROUND:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2020
Permit No. WQ0018525
ColonyBy The Sea 1.27 % Solids
12.25 pH (taken from lime stabilization event)
Parameter
%
MgIKg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.932
69,320.000
138.640
Phosphorus
1.155
11,550.000
23.100
Potassium
0.315
3,152.000
6.304
PAN (injected)*
2.124
21,244.020
42.488
PAN (surface)*
2.093
20,925.420
41.851
Ammonia Nitrogen
0.064
637.200
1.274
Calcium
3.523
35,226.000
70.452
Calcium Carbonate E .
---
---
Magnesium
---
4,157.000
8.314
Sodium
---
6,312.000
11624
Sulfur
Nitrate N / Nitrite N
---
1.980
0.004
Barium
---
---
---
L SAR
0.95
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3,958.00
7.916
Arsenic
---
2.50
0.005
75
Cadmium
---
1.30
0,003
85
Chromium
---
22.000
---
---
Co er
---
324.00
0.648
4,300
Lead
---
13,00
0.026
840
Mercury
---
0.21
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
16.00
0.032
420
Selenium
---
5.00
0.010
100
Zinc
---
1,969.00
3.938
7,500
Environment 1 # 616A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
COLONY BY THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mgllcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mglkg
Plant Available Nitrogen, mglkg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
3958
02/03/20
LFJ
EPA200.7
<2.5
02/04/20
MTM
311313-04
35226
01/31/20
LFJ
EPA200.7
1.3
01/30/20
MTM
3113B-04
324
02/03/20
LFJ
EPA200.7
22
01/31/20
LFJ
EPA200.7
13
01/29/20
1VITM
3113B-04
4157
02/03/20
LFJ
EPA200.7
0.21
01/16/20
MTM
EPA7471B
16
02/03/20
LFJ
EPA200.7
3152
02/03/20
LFJ
EPA200.7
C 5.0
02/05/20
MTM
3113E-04
6312
02/03/20
LFJ
EPA200.7
1969
02/03/20
LFJ
EPA200.7
1.27
01/06/20
MAR
2540G-11
c 69320
01/23/20
AKS
351.2 112-93
c 637.2
01/06/20
AKS
350.1 R2-93
c 11550
01/14/20
BLD
365.4-74
c 1.98
01/08/20
DTL
353.2 R2-93
20925
01/23/20
SEJ
5
01/31/20
LFJ
EPA200.7
Drinking Water ID: 3771.5
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 616 A
DATE.COLLECTED: 01/02/20
DATE REPORTED : 02/14/20
REVIEWED//BT y
c Uncertified data. DWR dose not offer non-aqueoua certification for this analytical procedure.

OF CUSTODY RECORD
Environment I, Inc.
P.O. Bo7.7085,114 Oakmont Dr.
Greenville,.NC 27859
environmentlinc.com
wSWFECI'ION
Phone [phone] • Fax [phone]
CHLORINE
CLIENT: 616 A wed 5
w
COLONY BY THE SEA MDROTECH1
NONE
P
P
P P
P
P
A'ITN: DON 0'11'IARA
HYDROTECH
A
A
A A
A
A
P.O- BOX 4602
EMERALD ISLE NC 28594
o
[phone]
3 _j
Ld "o
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-`•
x�
��
<
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COLLECTION
J
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c7
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aC
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¢
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SAMPLELOCA'ROK
BATE
TIME
iludg _ Sample
-2A
AEUNCLIISHFD BY
DATEMME
`Z=2d
zl
R BY [SIG.�ti jam. DATEIIIME
RELINQUISHED BY (Sa)
DATEITIME
RECEIVED BY (SIG.) DATEliiME
REUNQUISHED BY, (SIG)
I DATERIME
RECIENED BY.(SIG.) DATFJIIME
_6 T d1
Page 1 of 1
CHLORINE NEUTRAUIEDAT COLLECTION
pH CHECK (LAB)
CONTAINERTYPE, PIG
CHEMICALPRESERVATION
A -NONE D-.NAOH
UJ
cn
B-HNO, E-HCL
C-H1SO, F - ZJNC ACE-rATEINAOH
G - NATHIOSUiFATE
d
CLASSIRCATION:
WASTEWATER(NPOES)
DRINKINGWATEI
DWPVGW
SOLID WASTE SECTION
CHAIN OF CUSTODY- (SEAL) MAINTAINED
DURI NI PMENT/DELIVERY
Y, N
SAMPLES COLLECTED BY:
(Please Print} .
SAMPLES RECENED IN LABATQa—_°C
PLEASE READ I nstnlctiorls for completing Phis farm°on,the reverse side. Sampier must place a "C" iorcomposite sample or.a V for
Crab sample in the`blocks.above for each parameter, requested. NO 174521
FORM

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2020
Permit No. WQ0018525
Dunescape 1.33 % Solids
7.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002}
Nitrogen (TKN)
7.770
77,700.000
155.400
Phosphorus
1.581
15,810.000
31.620
Potassium
0.649
6,490.000
12.980
PAN (injected)*
2.381
23,813,220
47.626
PAN (surface)*
2.346
23,456.620
46.913
Ammonia Nitrogen
0.071
713.200
1.426
Calcium
4.581
45,807.000
91.614
Calcium Carbonate E .
---
---
---
Magnesium
---
4,748,000
9.496
Sodium
---
6,678.000
13.356
Sulfur
---
---
Nitrate N / Nitrite N
---
3.980
0.008
Barium
---
---
---
SAR
0.91
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,347.00
4.694
Arsenic
---
2.50
0.005
75
Cadmium
---
0.51
0.001
85
Chromium
---
7.000
---
---
Copper
---
493.00
0.986
4,300
Lead
---
9.40
0.019
840
Mercury
---
0.12
0.000
57
Molybdenum
---
7.00
0.014
75
Nickel
---
9.00
0.018
420
Selenium
---
5.00
0.010
100
Zinc
---
606.00
1.212
7,500
Environment 1 ff 556 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application;
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Drinking Water ID: 37715
ae ewa ar
;.
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
DUNESCAPE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mglkg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.4
01/02/20
GNB
4500HB-11
2347
01/08/20
LFJ
EPA200.7
<2.5
01/08/20
MTM
311313-04
45807
01/08/20
LFJ
EPA200.7
0.51
01/08/20
MTM
31138-04
493
01/08/20
LFJ
EPA200.7
7
01/08/20
LFJ
EPA200.7
9.4
01/07/20
MTM
3113E-04
4748
01/08/20
LFJ
EPA200.7
0.12
01/16/20
MTM
EPA7471B
9
01/08/20
LFJ
EPA200.7
6490
01/08/20
LFJ
EPA200.7
<5.0
01/09/20
MTM
3113E-04
6678
01/08/20
LFJ
EPA200.7
606
01/08/20
LFJ
EPA200.7
1.33
01/06/20
MAR
2540G-11
c 77700
01/23/20
AKS
351.2 R2-93
c 713.2
01/06/20
AKS
350.1 112-93
c 15810
01/14/20
BLD
365.4-74
c 3,98
01/08/20
DTL
353.2 112-93
7
01/08/20
LFJ
EPA200.7
PHONE [phone]
FAX [phone]
ID##: 556 A
DATE COLLECTED: 01/02/20
DATE REPORTED : 01/24/20
3 �
f ;
REVIEWED )BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

CHAIN OF CUSTODY RECORD
1 1
Environment 1, Inc.
page of
P.O..Box 7085.114 Oakmont Dr
Greenville; NC 27858
DISU*MCTION
CHLgAINENEUTRALIZEDATCQLLEcnoN.
environmentliac.com
phone [phone] • Fax [phone]
CHLORINE
pH CHECK (LAB)
CLIENT. 556 A Week: 4
W
CONTAINERTYPE, PIG
DUNESCAPE 0ELYDROTEC11)
NONE
P P
P P. P P
P
A'ITN::.ON O'MARA
. D.
CHEMICALPRESEWATION
kVDRUTECH
A A
A A A A
:A
P.O, BOX 46❑2
A - NONE D - NAOH
EMERALD ISLE NC 28594:r-
L
C B-HNO, E-HCL
[phone]
W a ¢ o z
0
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z
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a G-IVATHIOSULFAII=
COLLECTION
¢¢ ,� o c
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SAMPLELOCAI-ION DATE WEs-
o r
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�
CLASSIFICATION
Sindge.Sampie J z-zo
$"
WASTEWATER (NPDE8)
DRINKINGWATER
L) DWRIGW
SOLID WASTE SECTION{
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
N
SAMPLES COLLECTED BY:
(Please Print)
BY (SIG.) (SAMPLER) I
BY
ATErfIME ` COMMENTS:
SAMPLES RECEIVED IN LABAT :S - 7 °C
RplNQUISHEDBY(SIG) ynl C1i11Y1L i1GVG1Y�J �vnw.f
Sampler must place a °C" for composite Sample or a "G°for
PLEASE fiEAI) I nstructions fior completing this form on the reverse side_ Grab sample in the blocks above for eachparameter requested. N 0 3.74652 .

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 26, 2020
Permit No. WQ0018525
Eight 1/2 Marina 0.73 % Solids
12.27 vH {taken from lime stabilization)
Parameter -T
11
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002) :1
Nitrogen (TKN)
2.438
50,630.000
101.260
Phosphorus
0.244
17,290.000
34.580
Potassium
0.349
3,028.000
6.056
PAN (injected)*
0.752
7,524.446
15.049
PAN (surface)*
0.748
7,476.556
14,953
Ammonia Nitrogen
0.010
59.820
0.120
Calcium
50,607.000
101.214
Calcium Carbonate E .
---
---
---
Magnesium
---
M25.000
6,050
Sodium
---
12,658.000
25.316
Sulfur
---
---
Nitrate N / Nitrite N
---
144.600
0.289
Barium
---
---
---
SA R
1.26
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
5,243.00
10.486
Arsenic
---
7.60
0.015
75
Cadmium
---
1.10
0.002
85
Chromium
---
27.000
---
---
Copper
---
1,159.00
2.3I8
4,300
Lead
---
28.00
0.056
840
Mercury
---
0.62
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
10.00
0.020
420
Selenium
---
5.00
0.010
100
Zinc
---
2,318.00
4.636
7,500
Environment 1 # 196A
*Determination of PIant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or < detection limits are listed as detection Iimits
for calculation purposes.

Environment 1, Incorporated
_P.O. BOX 7085 i 14; OAKMONT DRIVE
GREENVILLE;- N C 27835-7085 MONE
(252) 75670633
EIGHT & ONE-HALF MARINA(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
5243
04/01/20
MTM EPA200.7
7.6
04/13/20
MTM 3113B-04
50607
04/01/20
MTM EPA200.7
1.1
04/03/20
MTM 3113B-04
1159
04/01/20
MTM EPA200.7
27
04/01/20
MTM EPA200.7
28
04/03/20
MTM 3113E-04
3025
04/01/20
MTM EPA200.7
0.62
04/16/20
MTM EPA7471B
10
04/01I20
MTM EPA200.7
3028
04/01/20
MTM EPA200.7
< 5.0
04/14/20
MTM 3113B-04
12658
04/01/20
MTM EPA200.7
2318
04/01/20
MTM EPA200.7
0.73
03/27/20
KDS 2540G-11
c 50630
03/3V20
TLH 351.2 R2-93
c 59.82
04/01/20
AKS 350.1 R2-93
c 17290
03/31/20
AKS 365.4-74
c 144.6
03/31/20
DTL 353.2 R2-93
20403
04/06/20
SEJ
< 5.0
04/01/20
MTM EPA200.7
ID#: 196 A
DATE COLLECTEDt 03/26/20
DATE REPO TED : 04/23/20
a�
REVIEWED BY:
c 9ncextilied data. DWR does not offer non -aqueous cartifi.cation for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 4, 2020
Permit No. WQ0018525
Genesis Condos 2.12 % Solids
6.4 pH
Parameter
-
%
I ]
Mg/Kg Dry Weight
- (% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.297
62,970.000
125.940
Phosphorus
0.760
7,603.000
15.206
Potassium
0.506
5,057,000
10.114
PAN (injected)*
2.067
20,670.500
41.341
PAN (surface)*
1950
19,500.500
39.001
Ammonia Nitrogen
0.234
1 2,340.000
4.680
Calcium
4.960
49,598.000
99.196
Calcium Carbonate Eq.
---
---
_-.
Ma ncsium
---
4,481.000
8.962
Sodium
---
6,248.000
12.496
Sulfur
-__
Nitrate N / Nitrite N
---
l4 L500
0.283
Barium
---
---
---
SAR
1.05
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
1881.00
5.762
Arsenic
---
4.50
0.009
75
Cadmium
---
1.10
0.002
85
Chromium
---
19.000
---
---
Copper
---
643.00
1.286
4,300
Lead
---
18.00
0.036
840
Mercury
---
0.28
0.001
57
Molybdenum
---
7.00
0.014
75
Nickel
---
13.00
0,026
420
Selenium
---
5.00
0.010
100
Zinc
---
1,245.00
2.490
7,500
Environment l # 68 C
'Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

M_ • • J
GENESIS CONDO ASSOCIATION(HYDROTECH
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg(kg
Zinc (dry wt. basis), ing/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg(kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.4
02/04/20
GNB
4500HB-11
2881
02/28/20
LFJ
EPA200.7
4.5
02/17/20
MTM
3113E-04
49598
02/14/20
LFJ
EPA200.7
1.1
02/24/20
MTM
3113E-04
643
02/14/20
LFJ
EPA200.7
19
02/26/20
LFJ
EPA200.7
18
02/21/20
MTM
311311-04
4481
02/28/20
LFJ
EPA200.7
0.28
02/7,7/20
MTM
EPA7471B
13
02/14/20
LFJ
EPA200.7
5057
02/14/20
LFJ
EPA200.7
5.0
02/18/20
MTM
3113E-04
6248
02/14/20
LFJ
EPA200.7
1245
02/26/20
LFJ
EPA200.7
2.12
02/04/20
KDS
2540G-11
c 62970
02/11/20
TLH
351.2 112-93
c 2340
02/11/20
AKS
350.1 R2-93
c 7603
02/10/20
DTL
365.4-74
c 141.5
02/11/20
BLD
353.2 R2-93
7
02/14/20
LFJ
EPA200.7
DiInkiag Water ID: 37.715t
Waafe�a ter 77P.i 10
_. PHONE [phone]B
FAX.. (252) 756_-6633
iD#: 68 C
DATE COLLECTED: 02/04/20
DATE REPOR ED : 03/02/20
REVIEWED BY:
c Racartified data. DWR does not otter non-aquacus cextification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2020
Permit No. WQ0018525
Hampton Suites 1.81 % Solids
6.40 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
2.111
21,110.000
42.220
Phosphorus
1.278
I2,780.000
25.560
Potassium
0.299
2,989.000
5.978
PAN (injected)*
0.735
7,351.450
14.703
PAN (surface)*
0.663
6,628.950
13.258
Ammonia Nitrogen
0.145
1,445.000
2.890
Calcium
5.099
50,987,000
101,974
Calcium Carbonate E .
---
---
Magnesium
---
2,318.000
4.636
Sodium
---
26,I09.000
52.218
Sulfur
---
___
Nitrate N / Nitrite N
---
6.950
0.014
Barium
---
---
SAR
4.12
Chloride
---
___
_
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
1696.000
3.392
Arsenic
---
2.50
0.005
75
Cadmium
---
0.50
0.001
85
Chromium
---
6.000
---
--
Copper
---
1,175.00
2.350
4,300
Lead
---
4.10
0.008
840
Mercury
---
0.15
0,000
57
Molybdenum
---
7.00
0.014
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
776.00
1.552
7,500
Environment 1, Incorporated 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes_

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
HAMPTON INN (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/lcg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mgllcg
ivlercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg1k9
Sodium (dry wt, basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/lcg
Sludge Analysis Method
Sample Date Analyst Code
6.4
01/02/20
GNB
4500HB-11
1696
01/08/20
LFJ
EPA200.7
<2.5
01/08/20
MTM
3113E-04
50987
01/08/20
LFJ
EPA200.7
<0.5
01/08/20
MTM
31138-04
1175
01/08/20
LFJ
EPA200.7
6
01/08/20
LFJ
EPA200.7
4.1
01/07/20
MTM
31138-04
2318
01/08/20
LFJ
EPA200.7
0.15
01/16/20
MTM
EPA74718
12
01/08/20
LFJ
EPA200.7
2989
01/08/20
LFJ
EPA200.7
<5.0
01/09/20
MTM
3113E-04
26109
01/08/20
LFJ
EPA200.7
776
01/08/20
LFJ
EPA200.7
1.81
01/06/20
MAR
254OG-11
c 21110
01/09/20
DTL
351.2 R2-93
c 1445
01/06/20
AKS
350.1 R2-93
c 12780
01/09/20
TLH
365.4-74
c 6.95
01/08/20
DTL
353.2 R2-93
7
01/08/20
LFJ
EPA200.7
Drinking Water IDS 37715
Wastewater IDS 10
a
PHONE [phone]
FAX [phone]
ID#: 551 A
DATE COLLECTED: 01/02/20
DATE REPORTED : 01/22/20
s �
REVIEWEI
c uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment i, Inc.
P.O. Box 7085, 114 Oakmont Dr.
GreenviUe,NC 27958
environmentlinc.-com
phone [phone] • Fax [phone]
CLIENT- 551 A week- 4
HAN[PT0N M. WyDROTECM
Ate: DON O'MARA
HYDROTECH
p.0. BOX 4602
FMERAi b IsLE NC 28594
(252) 72-5 .249
SAMPLELOCAnON
BY
BY (SIG.)
BY (SIG.I
CHAIN OF CUSTODY RECORD
CHLOPJNE
NONE
A A.
A
A
A
A
A
—z
rn
�
E
D- 8
COLLEUON J �,
S
_
-4
o
a�
z
DATE TUNE a o
l
RECEIVED BY (SIG:) `
Page 1 of 1
CHLOR1NE,NEUTRWUED AT COLLECTION
pH CHECK(LAB)
CONTAINERTYPE PIG
CHEMICALPRESERVATION
A -NONE D-NAOH
E S-HNO, E-HCL
LU C-HzSO, F-ZINCACECATEnmH
a G-NATHIOSULPATE
d
CLASSIFICATION
WASTEWATER(NMES)'
DRINI(INGWATER.
DWFIIGW
SOLID WASTESECTION
CHAIN OF CUSTODY (SEAL): MAINTAINED
DURINGkPMENTIDELIVERY .
Y N
SAMPLES 0,01-L:CTED BY
(Please RMq
SAMPLES RECEIVED IN LABAT, 9—a-°C
Sampler must place -a "V10r.cornposite sample or. a OW for
PLEASE READ Instructions for compiling this form 0n the reverse side_ Grab sample. in the blocks above for each parameter requested: p 37055
FARM #5
7777..

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 26, 2020
Permit No. WQ0018525
Harker's Point 0.46 % Solids
12.26 pH (Taken from Lime Stabilization)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg[Kg x 0.002)
Nitrogen (TKN)
6.158
61,580.000
123.160
Phosphorus
2.158
21,580.000
43.160
Potassium
1.074
10,737.000
21.474
PAN (infected)*
1.855
18,551.862
37.I04
PAN (surface)*
1.851
18,511,932
37.024
Ammonia Nitrogen
0.008
79.860
0.160
Calcium
2.046
20,459.000
40.918
Calcium Carbonate E .
.._
---
---
Magnesium
---
7,005.000
I4.010
Sodium
---
34,635.000
69.270
Sulfur
---
__-
Nitrate N / Nitrite N
---
21.960
0.044
Barium
---
---
---
SAR
3.60
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
2162.000
4.324
Arsenic
---
4.70
0.009
75
Cadmium
---
0.99
0.002
85
Chromium
-.-
9.000
---
---
Copper
---
368.00
0.736
4,300
Lead
---
20.00
0.040
840
Mercury
---
0.37
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
--- 1
8.00
0.016
420
Selenium
---
5A0
0,010
100
Zinc
---
1,111.00
2.222
7,500
Environment 1, Incorporated 95S
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits
for calculation purposes.

HARKERIS POINT SUBDIVISION(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOIL 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date. Analyst Code
2162
04/O1/20
MTM
EPA200.7
4.7
04/13/20
MTM
3113B-04
20459
04/01/20
MTM
EPA200.7
0.99
04/03/20
MTM
3113E-04
368
04/01/20
MTM
EPA200.7
9
04/01/20
MTM
EPA200.7
20
04/03/20
MTM
3113B-04
7005
04/01/20
MTM
EPA200.7
0.37
04/16/20
MTM
EPA7471B
8
04/01/20
MTM
EPA200.7
10737
04/01/20
MTM
EPA200.7
< 5.0
04/14/20
MTM
3113E-04
34635
04/01/20
MTM
EPA200.7
1111
04/01/20
MTM
EPA200.7
0.46
03/27/20
KDS
2540G-11
c 61580
03/31/20
TLH
351.2 R2-93
c 79.86
04/01/20
AKS
350.1 R2-93
c 21580
03/31/20
AKS
365.4-74
c 21.96
03/31/20
DTL
353.2 R2-93
24662
04/06/20
SEJ
< 5.0
04/O1/20
MTM
EPA200.7
Priak'ing y7ater IP7s 37-7•'15
➢ bAi texatex ID x .T..0
:PHONE [phone]
_ FAX [phone]
ID#: 9S S
DATE COLLECTED: 03/26/20
DATE REPORTED : 04/23/20
I
REVIEWED�Y: 2 �- 'P
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 17, 2020
Permit No. WQ0018525
Mariners Point 1.84 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
—(Mg/Kg -(Mg/Kgx 0.002)
Nitrogen (TKN)
4.854
48,540.000
97.080
Phosphorus
2.058
20,580.000
41.160
Potassium
0382
3,823.000
7.646
PAN (injected)*
1.596
15,957.370
31.915
PAN (surface)*
1.497
14,966,370
29.933
Ammonia Nitrogen
0.198
I.982.000
3.964
Calcium
4.086
40,863.000
81.726
Calcium Carbonate E .
---
---
Magnesium
---
3.388.000
6.776
Sodium
---
27,048.000
54.096
Sulfur
__-
---
Nitrate N / Nitrite N
---
7.970
0.016
Barium
---
---
---
SAR
L 4.68
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,515.00
5.030
Arsenic
---
2.50
0.005
75
Cadmium
---
0.91
0.002
85
Chromium
---
9.000
---
---
Copper
---
1,178.00
2.356
4,300
Lead
---
11.00
0.022
840
Mercury
---
0.21
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
8.00
0,016
420
Selenium
---
5.60
0.011
100
Zinc
---
1,495.00
2.990
7,500
Environment 1 # 307
"Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

Emw'o mum % hmp mUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
MARINERS POINT (BUCK)
C/O M.R. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mgllcg
Calcium (dry wt. basis), mgllcg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mgllcg
Lead (dry weight basis), mg/kg
Magnesium (dry wt, basis), mgllcg
Mercury ((try wt. basis), mgllcg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mgllcg
Sodium Adsorption Ratio (talc)
Total Solids, %
TKN (dry Nvt.), mg/kg
Ammonite Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mgllcg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis R-Cethod
Sample pate Analyst Code
7.1
12/17/20
KD5
4500HI1-11
2515
12/23/20
LFJ
EPA200.7
<2.5
12/28/20
NAB
3113B-04
40863
(2/23/20
LFJ
EPA200.7
0.9I
12/23/20
MTM
3113B-04
1178
12/23/20
LFJ
EPA200,7
9
12/23/20
LFJ
EPA200.7
11
12/23/20
MPB
3113B-04
3388
12/23/20
LFJ
EPA200.7
0.21
01/05/21
MTNI
EPA7471B
8
12/23/20
LFJ
EPA200.7
3823
12/29/20
LFJ
EPA200.7
5.6
01/11/21
NAB
EPA200.8
27048
12/23/20
LFJ
EPA200.7
1495
12/23/20
LFJ
EPA200.7
34.6
1.84
12/21/20
JMS
254OG-11
c 48540
12/23/20
TLH
351.2 R2-93
c 1982
12/21/20
ICES
350.1 R2-93
c 20580
12/23/20
ICES
365.4-74
e 7.97
12/21/20
TLH
353.2 112-93
<5.0
12/23/20
LFJ
EPA200.7
Drinking Water ID3 37715
Wastewater YDi 10
PHONE [phone]
FAX [phone]
ID#: 307
DATE COLLECTED: 12/17/20
DATE REPORTED : 01/12/21.
REVIEWED BY: fL
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

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Environment I, Inc.
P-O. Box 7085, 114 Oakmont Dr.
f Tr�Pnvi11P NC.. 17R71R
CHAIN OF CUSTODY RECORD
Page 1 of 1
environment 1 i ne.com
DISINFECTION
Phone [phone] e Fax [phone]
CHLORINE !NEUTRALIZED AT COLLECTION
Ll CxLolzllyE
pH CHECK (LAB)
CLIENT: 307 Week: 18
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P
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CONTAINER TYPE, PIG
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NONE
O MR. STANLEY BUCK
45 BELGRADE-SWANSBORO RD.
kYS'VIL,LE NC 28555
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CLASSIFICATION;
WASTEWATER(NPOES)
DRINKINGWATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
QUR{NG IPMENTIQELIVERY
N
SAMPLES COLLECTED BY:
(Phase Print)
SAMPLES RECEIVED IN LABAT 1,7 �C
RELIN UISH BY (SIG.) (SANIPLER)
DATENIME
RECEIVED BY (SIG.)
DATEITIME
COMMENTS:
REUNQU ED BY (SIG.)
DATEWE
RECEIVED BY (SIG.)
DATEfnME
RELINQUISHED BY (SIG.)
DATFfnME
RECEIVED BY (SIG.)
DATEIEIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G for
FORM "s Grab sample in the blocks above for each parameter requested. N2 372810

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2020
Permit No. WQ0018525
McGinnis Point 0.69 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
(°/u x 10,000)
Pounds/Dry Ton
(Mg/,Kg(Mg/,Kg x 0.002)
Nitrogen (TKN)
5.843
58,430.000
116.860
Phosphorus
1.741
17,410.000
34.820
Potassium
0.299
2,989.000
5.978
PAN (injected)*
I.762
17,617.740
35.235
PAN (surface)*
1.756
17,557.190
35.114
Ammonia Nitrogen
0.012
121.100
0.242
Calcium
5.408
54,079.000
1.08.158
Calcium Carbonate E .
---
---
Magnesium
---
6,I83,000
12.366
Sodium
---
26.775.000
53.550
Sulfur
---
---
---
Nitrate N / Nitrite N
---
3.970
0.008
Barium
---
---
---
SAR
2.41
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
6,169.00
12.338
Arsenic
---
2.50
0.005
75
Cadmium
---
0.64
0.001
85
Chromium
---
22.000
---
---
Copper
---
1,538.00
3.076
4,300
Lead
---
19.00
0.038
840
Mercury
---
0.22
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.90
0.012
100
Zinc
---
1,082.00
2.164
7,500
Environment I # 555 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT OLIVE
GREENVILLE, N.C. 27858
MCGINNIS POINT (HYDROTECH)
ATTN. DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mg/lcg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mglkg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mglkg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TIN (dry wt.), mg/lcg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mgllcg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.1
01/02/20
GNB
4500HB-11
6169
01/08/20
LFJ
EPA200.7
< 2.5
01/08/20
MTM
3113E-04
54079
01/08/20
LFJ
EPA200.7
0.64
01/08/20
MTM
311313-04
1538
01/08/20
LFJ
EPA200.7
22
01/08/20
LFJ
EPA200.7
19
01/07/20
MTM
3113E-04
6183
01/08/20
LFJ
EPA200.7
0.22
01/16/20
MTM
EPA7471B
11
01/08/20
LFJ
EPA200.7
2989
01/08/20
LFJ
EPA200.7
5.9
01/09/20
MTM
3113B-04
26775
01/08/20
LFJ
EPA200.7
1082
01/08/20
LFJ
EPA200.7
0.69
01/06/20
MAR
2540G-11
c 58430
01/09/20
DTL
351.2 R2-93
c 121.1
01/06/20
AILS
350.1 112-93
c 17410
01/09/20
TLH
365.4-74
c 3.97
01/08/20
DTL
353.2 R2-93
C 5.0
01/08/20
LFJ
EPA200.7
Drinking Water ID: 37715
.WaateWa.ter �D 10
PHONE [phone]
FAX [phone]
ID#: 555 A
DATE COLLECTED: 01/02/20
DATE REPORTED : 01/22/20
REVIEWED B F
c Uncertified data. DWR does not offer non-aqueoua certification for this analytical procedure.

_..__._.._ .._----
.__......�
CHAIN OF CUSTODY RECORD 1
Environment fine.
page 1 of
P:O. Box 7085., 114 Oakmont Dr-
Greenvilie,.NC'?7855
DISINFECTION
{
CHLORINE NEIITRAIMATWLLECTION
environment] inc.eorn
Phone [phone] + Fax [phone]
CHLORINE
V.
pH CHECK (LAB]
CLIENT: 555 A Week: 4'
CONTAINERiYPe PIG
MCGn,lm$ POINT IHYDROTECS)
NONE;'-
P_ P P P
P p
ATTN: DON O'MARA
CHEMICALPRESERVATION
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A A A, A
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P.oi BOX 4602
EMERALD ISLE NC-, 28594.
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SAMPLES RECEIVED.IN LAB AT=
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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RLISIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2020
Permit No. WQ0018525
NC Aquarium at Pine 1.34 % Solids
Knoll Shores 12.03 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
4.127
41,270.000
82.540
Phosphorus
2.566
25,660.000
51.320
Potassium
0.345
3,445.000
6.890
PAN (injected)*
1,256
12,559.940
25.120
PAN (surface)*
1.244
12,435.690
24.871
Ammonia Nitrogen
0.025
248.500
0.497
Calcium
5.460
54,596.000
109.192
Calcium Carbonate E .
---
---
---
Magnesium
---
5,844.000
11.688
Sodium
---
33,677.000
67.354
Sulfur
---
---
Nitrate N / Nitrite N
---
4,990
0.010
Barium
---
---
---
SAR
4.23
Chloride
_-_
___
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
2,401,00
4.802
Arsenic
---
2.80
0.006
75
Cadmium
---
46.00
0.092
85
Chromium
---
31.000
---
---
Copper
---
767.00
1.534
4,300
Lead
---
19I.00
0.382
840
Mercury
---
0.18
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
35.00
0.070
420
Selenium
---
5.00
0.010
100
Zinc
---
1,427.00
2.854
7,500
Environment 14 444 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

NNATumimW
114 OAKMON7 DRIVE
GREENVII_I_E, N.C. 27858
NC AQUARIUM AT PINE KNOLL SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 41.88
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/lcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), nig/Icg
Cadmium (dry wt. basis), rng/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/Icg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mglicg
Sodium (dry wt. basis), mg/Icg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/Icg
Anmionin Nitrogen (dry wt.),mg/lrg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mgllcg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), nig/lig
Sludge
Analysis
Method
Sample
Date
Analyst
Code
2401
03/04/20
Ll<J
EPA200.7
2.8
03/05/26
MTNI
3113E-04
54596
03/04/20
LFJ
EPA200.7
46
03/19/20
MTM
3113B-04
767
03/04/20
LFJ
EPA200.7
31
03/16/20
LFJ
EPA200,7
191
03/04/20
iVITM
311313-04
5844
03/04/20
LFJ
EPA200.7
0.18
03/23/20
MTM
EPA7471B
35
03/16/20
LFJ
EPA200.7
3445
03/04/20
LCJ
EPA200.7
<5.0
03/09/20
MTM
3113B-04
33677
03/04/20
LF.1
EPA200.7
1427
03/04/20
LFJ
EPA200.7
1.34
02/27/20
JM5
2540G-11
c 41270
03/04/20
DTL
35t.2 R2-93
c 248,5
03/03/20
BLD
350.1 R2-93
c 25660
03/04/20
AKS
365.4-74
c 4.99
03/02/20
AKS
353.2 R2-93
12436
03/06/20
SE 1
<5.0
03/04/20
LFJ
EPA200.7
Drinking Water ID 37715
Wastewater ID, 1D
PHONE [phone]
FAX [phone]
ID# : 444 A
DATE COLLECTED: 02/27/20
DATE REPORTED : 03/27/20
M
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Boh--7085, 114 Oakmont Dr.
Gmnville. NC 27858 page 1 of
e'
env irontnent I inc.com
DISNI;ECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE
Ij
pH CHECK (LAB)
CLIENT: 444 A Week: 9
ZUV
NC AQUARIUM AT PINE KNOLL SHORES
NOINTE
P
P
P
P
P
p
CONTAINER TYPE, PIG
MR. DAN FORTIN
L�
FORTIN CONTRACT SERVICES
P.O. BOX 4188
A
A
A
A
A
A
CHEMICALPRESI RVATION
EMERALD ISLE NC 28594
PO
A - NONE D - NAOH
[phone]
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GHAIN OF CUSTODY (SEAL) MAINTAINED
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Y N
SAMPLES COLLECTED BY:
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SAMPLES RECEIVED IN LABAT5 1:9 °C
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DATE/TIME
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DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a °C" for composite sample or a "G' for
FORA 5 Grab sample in the blocks above for each parameter requested. N 9 376248

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 23, 2020
Permit No. WQ0018525
Ocean Club 1.60 % Solids
12.03 nH (taken from lime stabilization eventl
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.787
57,870.000
115.740
Phosphorus
1.845
I8,450.000
36.900
Potassium
0.641
6.413.000
I2.826
PAN (injected)*
1.904
19.043.600
38.087
PAN (surface)*
1.784
17,844.600
35.689
Ammonia Nitrogen
0.240
2,398.000
4.796
Calcium
3,553
35,526,000
71.052
Calcium Carbonate E .
---
---
Magnesium
---
3,851.000
7.702
Sodium
---
11,892.000
23.784
Sulfur
---
___
---
Nitrate N / Nitrite N
--
4.000
0.008
Barium
---
---
SAR
2.02
Chloride
---
---
---
Iron
---
---
---
g Concen.
1�tg/Kg)
Aluminum
---
1,702.00
3.404
Arsenic
---
2.50
0.005
75
Cadmium
---
0.66
0.001
85
Chromium
---
11Q00
___
---
Copper
---
379.00
0.758
4,300
Lead
---
8.30
0.017
840
Mercury
0.15
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
14.00
0.028
420
Selenium
---
5.00
0.010
100
Zinc
---
1,549.00
3.098
L 7,500
Environment I # 404 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environment 1, Incorporated
Drinkiiig Water IDs, 3171Sj
- _ Wast-ewater SAt 14.
PHONE (252)`756 6208
TAX (252) 756.003
P.O. [iOR 7085,1'14_0AKMONT'DRIVE
dREENVILLE, N.C. 27835-7085 -
OCEAN CLUB (FORTIN)
MR.. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt, basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
1702
02/28/20
LFJ
EPA200,7
< 2.5
02/17/20
MTM
3113E-04
35526
02/14/20
LFJ
EPA200.7
0.66
02/24/20
MTM
3113B-04
379
02/14/20
LFJ
EPA200.7
12
02/26/20
LFJ
EPA200.7
8.3
02/21/20
MTM
3113B-04
3851
02/28/20
LFJ
EPA200.7
0.15
02/06/20
MTM
EPA7471B
14
02/14/20
LFJ
EPA200.7
6413
02/14/20
LFJ
EPA200.7
< 5.0
02/18/20
MTM
311313-04
11892
02/14/20
LFJ
EPA200.7
1549
02/26/20
LFJ
EPA200.7
1.60
01/27/20
KDS
2540G-11
c 57870
OV28/20
TLH
351.2 R2-93
c 2398
OV28/20
AKS
350.1 R2-93
c 18450
01/28/20
BLD
365.4-74
c 4.00
01/28/20
DTL
353.2 R2-93
11845
OV79/20
SEJ
< 5.0
02/14/20
LFJ
EPA200.7
ID#: 404 A
DATE COLLECTED; 01/23/20
DATE REPORTED : 03/02/20
REVIEWED BY: '�y
c Uncertified data. DWR does not offer non -aqueous cartitication lox this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 9, 2020
Permit No. WQ0018525
Pebble Beach 1.83 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
8.216
82,160.000
164,320
Phosphorus
1.223
12,230.000
24.460
Potassium
0.433
4,330.000
8.660
PAN (injected)*
2.715
2,464.097
4.928
PAN (surface)*
2.537
2,435.542
4.871
Ammonia Nitrogen
0.357
3,571.000
7.142
Calcium
2.828
28,280.000
56.560
Calcium Carbonate E .
---
___
---
Magnesium
---
3,624.000
7.248
Sodium
---
6,608.000
13.216
Sulfur
---
Nitrate N / Nitrite N
---
6.900
0.014
Barium
---
---
---
SAR
1.33
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,422.000
4.844
Arsenic
---
2.30
0.005
75
Cadmium
---
0.88
0.002
85
Chromium
---
10.000
---
---
Copper
---
484.00
0.968
4,300
Lead
---
12.00
0.024
840
Mercury
---
0.19
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
1,880.00
3.760
7,500
Environment 14 287A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Drinking Water ID: 37715
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PEBBLE BEACH (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mgllcg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/lig
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.1
01/09/20
TMR
4500HB-11
2422
02/03/20
LFJ
EPA200.7
<2.5
02/04/20
MTM
311313-04
28280
01/31/20
LFJ
EPA200.7
0.88
01/30/20
MTM
3113E-04
484
02/03/20
LFJ
EPA200.7
10
01/31/20
LFJ
EPA200.7
12
01/29/20
MTM
3113B-04
3624
02/03/20
LFJ
EPA200.7
0.19
01/16/20
MTM
EPA7471B
11
02/03/20
LFJ
EPA200.7
4330
02/03/20
LFJ
EPA200.7
< 5.0
02/05/20
MTM
3113E-04
6608
02/03/20
LFJ
EPA200.7
1880
02/03/20
LFJ
EPA200.7
1.83
01/13/20
KDS
254OG-11
c 82160
01/23/20
AKS
351.2 R2-93
c 3571
01/14/20
DTL
350.1 112-93
c 12230
01/14/20
BLD
365.4-74
c 6.90
01/14/20
TLH
353.2 R2-93
25369
01/23/20
SEJ
<5.0
01/31/20
LFJ
EPA200.7
PHONE [phone]
FAX [phone]
ID#: 287 A
DATE COLLECTED: 01/09/20
DATE REPORTED : 02/14/20
REVIEWED B
c Uncertified data. 13WR does not offer non-aqueauu certification for this analytical procedure.

CHAIN OF CUSTODY RECORD
Environment I,;Lnc.
P.O. Box 7085, 114 Oakmont Dr.
Greenvil e,.NC 27858
DISINFECTION
envi.ronmeralinc.com
Phone [phone] - Fax [phone]
CHLORWE
287 A Week- 8
CLIENT:Uv
a a ��
PEBBLE BEACI (HYDROTECH)
NONE
P P P P P P P
ATLN: DON OIAIARA
HYDROTECH
A A A A. A A A
P.O. BOX 4602
EMERALD ISLEVC 28594.
o
.J L
Z w
_
diy,_ L
�
.z b
{2S2p 775-2319
Z = � — o z
G o
so
z
COLLECTION
S.Zn . d
�,
O c. d
o
" ¢
¢
Z, a+
SAMPLELOCAnON DATE TIME
fudge Sample
jELMMQUGHED BY (SIG:) (SAMPLER) DATEIITME RECEiV (SIG.) .
Rf:UNQLf(5HmBY(SICti) DA R Cal
RpJNQUISHQ3 BY (SIG.) DATEMME.. RECEIVED BY
PLEASE READ Instructions for completing this form on the reverse side:
FORM #5
01
Page >< of I
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
CONTAINERI YK NG
CHEM[CALPRESERVAIION
A -NONE D-NAOH
c!3
B-HNO, E-MCL
LU
C - HP, . F - ZiNC ACETATFtNAOH
G - NATWOSULFATE
CLASSIRCATKA"
WASTEWATER.(WDES)
DRIWNGWATER .
DWRIGW
S4UQWASTESEGnON.
CHAIN Of CUSTODY (SEAL) MAINTAINED
DURING SHIPMENTMELIVERY
N
SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECENM IN LABAT—P—(,°C
:DATFJTIME
Sampler mustplace.a "C" far composite sample or a "G" for
Grab sample. in the blocks above for, each -parameter requested: N 2' 3753.76

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 16, 2020
Permit No. WQ0018525
Peppertree 0.43 % Solids
12.24 DH (taken from lime stahilizatinn eventl
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.784
57,840.000
115.680
Phosphorus
1.568
15,680.000
31.360
Potassium
0.198
1,978.000
3.956
PAN (injected)*
1.788
17,878.681
35.757
PAN (surface)*
1.785
17,852.766
35.706
Ammonia Nitrogen
0.005
51.830
0.104
Calcium
6.264
62,638.000
125,276
Calcium Carbonate E .
---
---
___
Ma nesium
---
2,995.000
5.990
Sodium
---
10,307.000
20.614
Sulfur
---
___
Nitrate N / Nitrite N
---
490.400
0.981
Barium
---
---
---
SAR
0.71
Chloride
---
___
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
4,712.000
9.424
Arsenic
---
2.70
0.005
75
Cadmium
---
1.10
0.002
85
Chromium
---
22.000
---
---
Copper
---
702.00
1.404
4,300
Lead
---
13.00
0.026
840
Mercury
---
0.62
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
13.00
0.026
420
Selenium
---
5.00
0.010
100
Zinc
---
1,814.00
3.628
7,500
Environment l # 129 C
`Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PEPPERTREE RESORTS (FORTIN)
ATTN: MR. DAN FORTIN
P.O. BOX 1068
ATLANTIC BEACH :NC 28512
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mglkg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mglkg
Total Solids, %
TICN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt,), mglkg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mgllcg
Sludge Analysis Method
Sample Date Analyst Code
4712
02/03/20
LFJ
EPA200.7
2.7
02/04/20
MTM
311313-04
62638
01/31/20
LFJ
El PA200.7
1.1
01/30/20
MTM
3113E-04
702
02/03/20
LFJ
EPA200.7
22
01/31/20
LFJ
EPA200.7
13
01/29/20
MTM
3113E-04
2995
02/03/20
LFJ
EPA200.7
0.62
02/06/20
MTM
EPA7471B
13
02/03/20
LFJ
EPA200.7
1978
02/03/20
LFJ
EPA200.7
<5.0
02/05/20
MTM
3113B-04
10307
02/03/20
LFJ
EPA200.7
1814
02/03/20
LFJ
EPA200.7
0.43
01/16/20
KDS
254OG-11
c 57840
01/23/20
AKS
351.2 R2-93
c 51.83
01/21/20
DTL
350.1 R2-93
c 15680
01/23/20
TLH
365.4-74
c 490.4
01/21/20
TLH
353.2 R2-93
23632
01/24/20
SEJ
<5.0
01/31/20
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 1f4
1,-AVy-
PHONE [phone]
FAX [phone]
ID#: 129 C
DATE COLLECTED: 01/16/20
DATE REPORTED : 02/14/20
REVIEWE
e Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc.
P.O. Box 7085,114 Oakmont Dr.
Greenville, NC 27858
environment I inc.corn
Pbone [phone] w Fax (252) 756-OC33
CLIENT: 129 C Week: 8
PEPPERTREE RESORTS (FORTIN)
ATTN: MR..DAN FORTIN
P.O. BOX 1068
ATLANTIC BEACH NC.28512
[phone].
SAMPLELOCATION
ledge Sample
COLLECTION
DATE I TIME
RELINQUISHED BY (SIG.) (SAMPLER)
ISO
BY (SIG.) I
RE! INQUiSHED BY (SIG.)
CHAIN OF CUSTODY RECORD
DISINFECTION
CHLORINE
w
ONE P P P P P P
A A A A A A
�a
�a
s La z w z L
so
0 9M �� ¢
2N O
v s h a Z. w
00 �a
4
VA -
BY (SIG.)
RECEIVED BY (SIG,)
COMMENTS:
Paae 1 of 1
CHLORINE NEUTRAL®AT COLLECTION
pH CHECK (LAB)
CONTAINERTYPE, P1G
CHEMICAL PRESERVATION
A -NONE
D-NAOH
m
LU
B-HNO,
E-HCL
co
w
C - HZSO,
F - ZINC ACEfATElNAOH
G-NATHIOSULFATE
C
CLASSIMPTlON:
WASTEWATER (NPDES)
DRINKINGWATER
DWRfGW
SOLID WASTE SECTION
CHAIN OF -CUSTODY. (SEAL) MAINTAINED
DURINGSHCL
IPMENT/DELIVERY
N
SAMPLES COLLECTED BY.
(Please PdA� . C—
SAMPLESSRECEIVED IN LABAT_L:�_°C
Sampler must place a V for composite sampie. or a "G" for
PLEASE READ Instructions for completing this form on the reverse side. Grab sample in the blacks above for each parameter requested. N U 375412
FORM 45

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2020
Permit No. WQ0018525
Point Emerald Villas 1.14 % Solids
8.1 pH
Parameter
%
Mg/Kg Dry Weigbt
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.254
56,100.000
112.200
Phosphorus
1.482
17,050.000
34.100
Potassium
0.273
2,789,000
5.578
PAN (injected)*
1.636
16,363900
32.728
PAN (surface)*
1.619
16,193.400
32.387
Ammonia Nitrogen
0.034
77.810
0.156
Calcium
4.028
17,787.000
35.574
Calcium Carbonate 1 _
---
..-
Ma nesium
---
2,168.000
4.336
Sodium
---
21,266.000
42.532
Sulfur
---
_--
---
Nitrate N / Nitrite N
---
364.100
0.728
Barium
---
---
---
SAIL
4.27
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
6,5t3.00
13.026
Arsenic
---
2.50
0.005
75
Cadmium
---
0.96
0.002
85
Chromium
---
21.000
---
---
Copper
---
696.00
1392
4,300
Lead
---
72.00
0.144
840
Mercury
---
0.20
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
2,116.00
4.232
7,500
Environment 14 348 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environment 1
POINT EMERALD VILLAS (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.D. SOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
PA, Units
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
8.1
03/05/20
TMR
4500HB-11
6513
03/18/20
LFJ
EPA200.7
< 2.5
03/31/20
MTM
3113E-04
17787
03/18/20
LFJ
EPA200.7
0.96
03/20/20
MTM
3113B-04
696
03/1.8/20
LFJ
EPA200.7
21
03/18/20
LFJ
EPA200.7
72
03/18/20
MTM
3113E-04
2168
03/18/20
LFJ
EPA200.7
0.20
03/23/20
MTM
EPA7471B
11
03/18/20
LFJ
EPA200.7
2789
03/18/20
LFJ
EPA200.7
< 5.0
04/01/20
MTM
3113E-04
21266
03/18/20
LFJ
EPA200.7
2116
03/18/20
LFJ
EPA200.7
1.14
02/27/20
JMS
2540G-11
c 56100
03/06/20
TLH
351.2 R2-93
c 77.81
03/06/20
AKS
350.1 R2-93
c 17050
03/06/20
AKS
365.4-74
c 364.1
03/11/20
AKS
353.2 112-93
< 5.0
03/18/20
LFJ
EPA200.7
Drinking Water xD4 3.77:1-51
ID#: 348 A
DATE COLLECTED: 02/27/20
DATE REPORTED : 04/03/20
V
V'
REV...,". V
a Uncertified data. DWR does not offer noa-aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 13, 2020
Permit No. WQ0018525
Queens Court 2.00 % Solids
6.94 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.370
63.700.000
127.400
Phosphorus
0.998
9,980.000
19.960
Potassium
0.380
3,800.000
7.600
PAN (injected)*
2.236
22,360.100
44.720
PAN (surface)*
2.005
20,045.100
40.090
Ammonia Nitrogen
0.463
4,630.000
9.260
Calcium
1.360
13,600.000
27.200
Calcium Carbonate E .
---
---
---
Magnesium
---
2,840.000
5.680
Sodium
....
9,250.000
18.500
Sulfur
Nitrate N / Nitrite N
---
9.100
0.018
Barium
---
---
---
SAR
2.66
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
F(M /K )
Aluminum
---
2,580.00
5.160
Arsenic
---
25.00
0.050
75
Cadmium
---
25.00
0.050
85
Chromium
---
25,040
___
---
Copper
---
590.00
1.180
4,300
Lead
---
25.00
0.050
840
Mercury
---
0.85
0.002
57
Molybdenum
---
25.00
0.050
75
Nickel
---
25.00
0.050
420
Selenium
---
25.00
0.050
100
Zinc
---
1,930.00
3.860
7,500
Envirochem # 2020-17442
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
a � ' 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
•�"t ' ' 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: Nov 02, 2020
Post Office Box 4188 Customer PO #•
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report #• 2020-17442
Project ID: Queens Court
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
20-44602 Site: Sludge 10/13/2020 9:25 AM Solid/Sludge Kevin Stanley
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+ N itri te-N itrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total K)eldahl Nitrogen (TKN)
Total Phosphorus
Mercury
Comment:
Reviewed by
Method
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200,7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
S W846 7471 B
Results
2580 mglkg
<25.0 mg/kg
<25.0 mg/kg
13600 mglkg
<25,0 mg/kg
590 mg/kg
<25.0 mg/kg
2840 mg/kg
<25.0 mg/kg
<25.0 mg/kg
3800 mg/kg
<25.0 mg/kg
9250 mg/kg
1930 mg/kg
9.10 mg/kg
2.00 %
6.94 units
4830 mg/kg
63700 mg/kg
9980 mg/kg
<0.850 mglkg
Date Analyzed
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/20/2020
10/ 14/2020
10/14/2020
10/27/2020
10/15/2020
10/15/2020
10/19/2020
10/30/2020
Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
t
Report #:: 2020-17442 Pane 9 of 7

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910,392.0223
Sample Receipt Checklist
Client: YI n s7QL' {(� SC-�• 3 ZC�
Date: � � �J Report Number:
Receipt of sample:
ECHEM Pickup 9 Client Delivery ❑ 1 UPS ❑ FedEx ❑ Other ❑
❑ YES
❑
NO
N/A 11. Were custody seats present on the cooler?
❑ YES
❑
NO
N/A 2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt c °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
iR Gun ID: Thomas Traceable SIN 192511657 iR Gun Correction Factor °C: 0.0
❑ YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
S. Were sample iD's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
10
NO
19. Did samples arrive in proper containers for each test?
YES
❑
NO
110. Did samples arrive in good condition for each test?
YES
❑
NO
Ill. Was adequate sample volume availableT
YES
ElNQ
12. Were samples received within proper holding time for requested tests?
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
ElNO
114. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0,5 m/L? *"
❑ YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any samples) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HC1 NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

ENVIRONMENTAL CHEMISTS, IN OFFICE: 2-02l31=AX910-3 2-44 4�
`�
Analytical & Consulting Chemists NCDENR. DWQ CERTIFICATION # 94 NCDIIHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Fortin Contract Services PROJECT NAME: Queens Court REPORT NO: IL
ADDRESS: PO Box 4188 CONTACT NAME: Dan Fortin PO NO:
Emerald Isle, NC 28594 REPORT TO: PHONEIFAX:
COPY TO: email:
Sampled By: �_. 1 SAMPLE TYPE: I = Influent E - Effl t W = W
Sample Identification
Effiluent-Cornf asite
-
-GrabEffluent
.-�--
Transfer
1.
2.
Temperature when Receive °C:
Delivered By:
Comments:
uen
,
ell, 5T
=
Stream,
SO = Soil, 31_ = Sludge, Other:
E'
U
V 4
r
U
m
z
PRESERVATION
ANALYSIS REQUESTED
i
Z.
u
x
=
y
0
P
BOD, TSS, NO2
G
G
G
P
G
L. � C
NH3, Total Phos, TN, NO3, `E`KN
C
P
4�6(?�
Fecal
G
C
P
G
G
C
P
G
IMS, CHLORIDE
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Date/Time Received By: Dateffime
1u- 0 - I5 - 13-1 O f/. o
��'
e]ected: Resample Requested:
eived By-_— _ Date: it) - 13--?0 Time:
TURNAROUND:

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plaint
Date Sampled: February 4, 2020
Permit No. WQ0018525
Sands Villas 2.26 % Solids
6.9 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.484
74,840.000
149.680
Phosphorus
1.003
10,030.000
20.060
Potassium
0.238
2,381.000
4.762
PAN (injected)*
2.434
24,343.600
48.687
PAN (surface)*
2.362
23,621.600
47.243
Ammonia Nitrogen
0.144
1,444.000
2.888
Calcium
3.374
33,744.000
67.488
Calcium Carbonate E .
---
---
Magnesium
---
3,169.000
6.338
Sodium
---
3,829.000
7.658
Sulfur
Nitrate N / Nitrite N
---
880.800
1.762
Barium
---
---
---
SAR
0.80
Chloride
_--
___
Iron
---
---
---
Ceiling Concen.
(M 1K )
Aluminum
---
2,364.00
4.728
Arsenic
---
2.60
0.005
75
Cadmium
---
0.73
0.001
85
Chromium
---
11.000
---
---
Copper
---
339.00
0,678
4,300
Lead
---
7.50
0.015
840
Mercury
---
0.23
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.0I0
100
Zinc
---
1,055.00
2.110
7,500
Environment 14 559
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environment 1, Incorporated
ID#: 559
SANDS VILLA (HYDROTECH)
DON OINARA
HYDROTECH DATE COLLECTED: 02/04/20
P.O. BOX 4602 DATE REPORTED : 03/09/20
EMERALD ISLE ,NC 28594
REVIEWBID BY ✓ i
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mng/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
SIudge Analysis Method
Sample Date Analyst Code
6.9
02/04/20
GNB
4500HB-11
2364
02/28/20
LFJ
EPA200.7
2.6
02/28/20
MTM
3113B-04
33744
02/29/20
LFJ
EPA200.7
0.73
02/26/20
MTM
3113E-04
339
02/26/20
LFJ
EPA200.7
11
02/29/20
LFJ
EPA200.7
7.5
02/25/20
MTM
3113B-04
3169
02/28/20
LFJ
EPA200.7
0.23
02/27/20
MTM
EPA7471B
11
02/29/20
LFJ
EPA200.7
2381
02/29/20
LFJ
EPA200.7
< 5.0
03/03/20
MTM
3113E-04
3829
02/29/20
LFJ
EPA200.7
1055
02/29/20
LFJ
EPA200.7
2.26
02/04/20
KDS
254OG-11
c 74840
02/11/20
TLH
351.2 112-93
c 1444
02/11/20
AKS
350.1 R2-93
c 10030
02/10/20
DTL
365.4-74
c 880.8
02/11/20
BLD
353.2 R2-93
< 5.0
02/29/20
LFJ
EPA200.7
c Uncertified data. DWR does not offer non -aqueous eertifieatiaa for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2020
Permit No. WQ0018525
Sea Isle Plantation 0.51 % Solids
12.09 DH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weigbt
(% x 10,000}
Pounds/Dry Ton
(Mg/Ke x 0.002)
Nitrogen (TKN)
1.917
38,490.000
76980
Phosphorus
0.675
17,290.000
34.580
Potassium
0.452
4,941.000
9.882
PAN (injected)*
0.585
5,852.768
11.706
PAN (surface)*
0.581
5,813.948
11.628
Ammonia Nitrogen
0.008
46.640
0.093
Calcium
4.831
35,034.000
70.068
Calcium Carbonate E _
---
---
Magnesium
---
3,454,000
6.908
Sodium
---
21,700.000
43.400
Sulfur
---
..-_
Nitrate N 1 Nitrite N
---
48.620
0.097
Barium
---
---
---
SAR
2.11
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3,141.00
6.282
Arsenic
---
2.50
0.005
75
Cadmium
---
2.00
0.004
85
Chromium
---
21.000
---
---
Copper
---
249.00
0.498
4,300
Lead
---
48.00
0.096
840
Mercury
---
0.17
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
18.00
0.036
420
Selenium
---
5.00
0.010
1 100
Zinc
---
1,271.00
2.542
71500
Environment l # 96A
"Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Emwohmmid % hmpu8nUd
114 OAKMONT [DRIVE;
GRE=ENVILLE, N.C. 27858
SEA ISLE PLANTATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/Icg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry ivt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/Icg
Mercury (dry wt, basis), mg/Icg
Nickel (dry wt. basis), mg/Icg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %s
TKN (dry wt.), mgllcg
Ammonia Nitrogen (dry wt.),ing/lcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
rviolybde:umi (dry wt, basis), mg/kg
Sludge
Analysis
Method
Sample
Date
Analyst
Code
3141
03/04/20
LFJ
EPA200.7
<2.5
03/05/20
MTM
3113B-04
35034
03/04/20
LFJ
EPA200.7
2.0
03/06/20
MTM
3113B-04
249
03/04/20
LFJ
EPA200.7
21
03/16/20
LFJ
EPA200.7
48
03/04/20
MTM
3113B-04
3454
03/04/20
LFJ
EPA200.7
0.17
03/23/20
MTM
EPA7471B
18
03/16/20
LFJ
EPA200.7
4941
03/04/20
LRI
EPA200.7
<5.0
03/09/20
MTIV1
3113B-04
21700
03/04/20
LFJ
EPA200.7
1271
03/04/20
LFJ
EPA200.7
0.51
02/27/20
JMS
254OG-11
c 38490
03/04/20
DTL
351.2 112-93
c 46.64
03/03/20
BLD
350.1 112-93
c 17290
03/04/20
AKS
365.4-74
c 48.62
03/02/20
AKS
353.2 112-93
11605
03/06/20
SEJ
<5.0
03/04/20
L14J
EPA200.7
Drinking Water IDe 37115
Wastewater IDr 10
PHONE [phone]
FAX [phone]
ID#: 96 A
DATE COLLECTED: 02/27/20
DATE REPORTED : 03/27/20
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for thin analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr. Page 1 of 1
i reenville. NC 27858 V
en viron rnent l inc-corn
DISINFECTION
CHLORINE NEWRALIZEDATCOLLECTION
Phone [phone] e Par• [phone]
CHLORINE
Ij
CLIENT: 96 A Week: 8
UV
pH CHECK (LAB)
A ISLE PLANTATION (FORTIN)
NONE
P
P
P
P
P
P
CONTAINER TYPE, P/G
t. DAN FORTIN
CHEMICAL PRESERVATION
1RTIN CONTRACT SERVICES
). BOX 4188
A
A
A
A
A
A
IERALD ISLE NC 28594
7 0
A - NONE D - NAOH
'2) 393-872U
z
Z
_
L
�
_ B- HNO, E HCL
rr J
0 0
ur
rC o
w
z
o
Z
oc
w C-H,SO, F- ZINC ACETATE/NAOH
COLLECTION
¢
o¢
Lb�
0
y
o
a
'
o
�`
a
O
a
G
< G-NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
Sludge Sample
*7120�•
3�
4
L..
vu
'..
x.r
CLASSIFICATION:
JWASTEWATER (NPDES)
DRINKING WATER
DWRiGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
MENT/DELIVERY
DURI��U
N
SAMPLES COLLECTED BY'
( lease Print)
4 l 5-TAN
SAMPLES RECEIVED IN LAB AT °C
� INQUISHED=(SIGAI4fPLER)
RECEIVED BY .1
COMMENTS:
h�QATETIME
4ATE/TIME
INQUISHED BY (SIG.)
AT�ME
RECEIVED BY {51G.)
DATEIIIME
RELINQUISHED BY (SIG.)
DATEIIIME
RECEIVED BY {SIG.} _T
DATE FPME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C' for composite sample or a "G for
FORM ws Grab sample in the blocks above for each parameter requested. N 2 375426

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 4, 2020
Permit No. WQ0018525
Sea_ Sr ray 1.11 % Solids
7.2 pH
Parameter
%
Mg/Kg Dry Weight
Pounds/Dry Ton
(M /K x 0.002)
Nitrogen (TKN)
2.885
58,I40.000
116.280
Phosphorus
0.416
7,760.000
15.520
Potassium
0.100
4,154.000
8.308
PAN (injected)*
0.889
8,890.130
17.780
PAN (surface)*
0.873
8,731.130
17.462
Ammonia Nitrogen
0.032
362.100
0.724
Calcium
3.890
43,266.000
86.532
Calcium Carbonate E .
---
---
Magnesium
---
3,185.000
6.370
Sodium
---
7,439.000
14.878
Sulfur
Nitrate N / Nitrite N
---
11.930
0.024
Barium
---
---
SAR
0.98
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2.797.00
5.594
Arsenic
---
2.50
0.005
75
Cadmium
---
0.50
0.001
85
Chromium
---
12.000
---
---
Copper
---
1,015.00
2.030
4,300
Lead
---
13.00
0.026
840
Mercury
---
0.29
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
871.00
1.742
7,500
Environment I N 560
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environment 1. Incorporated
g6z'7005; iia'_anKnnoNrDRIVE
-
.ENUILLE, N.C:'27835-7085 --
A PLACE AT TfEE BEACH II(HYDROTECH)
DON OIMARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.2
02//04/20
GNB
4500HB-11
2797
02/28/20
LFJ
EPA200.7
< 2.5
02/28/20
MTM
3113E-04
43266
02/29/20
LFJ
EPA200.7
< 0.5
02/26/20
MTM
3113E-04
1015
02/26/20
LFJ
EPA200.7
12
02/29/20
LFJ
EPA200.7
13
02/25/20
MTM
3113B-04
3185
02/28/20
LFJ
EPA200.7
0.29
02/27/20
MTM
EPA7471B
11
02/29/20
LFJ
EPA200.7
4154
02/29/20
LFJ
EPA200.7
< 5.0
03/03/20
MTM
311313-04
7439
02/29/20
LFJ
EPA200.7
871
02/29/20
LFJ
EPA200.7
1.11
02/04/20
KDS
254OG-11
c 59140
02/11/20
TLH
351.2 R2-93
c 326.1
02/11/20
AKS
350.1 R2-93
c 7760
02/10/20
DTL
365.4-74
c 11.93
02/11/20
BLD
353.2 R2-93
< 5.0
02/29/20
LFJ
EPA200.7
ID#: 560
DATE COLLECTED: 02/04/20
DATE REPORTED 03/09/20
x \1
REVIEWED BY:
e Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 10, 2020
Permit No. WQ0018525
Sound Of The Sea 1.06 % Solids
5.6 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
2.885
60,080.000
120.160
Phosphorus
0.416
14,800.000
29.600
Potassium
0.100
10,771.000
21.542
PAN (injected)*
0.888
8,882.190
17.764
PAN (surface)*
0.872
8,723.190
17.446
Ammonia Nitrogen
0.032
2,937.000
5.874
Calcium
3.890
11,489.000
22.978
Calcium Carbonate Eq.
---
---
Magnesium
---
2,891.000
5.782
Sodium
---
16,809.000
33.618
Sulfur
---
---
Nitrate N / Nitrite N
---
3.990
0.008
Barium
---
---
---
SAR
3.73
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
1,648.00
3.296
Arsenic
---
2.50
0.005
75
Cadmium
---
0.87
0.002
85
Chromium
---
6.000
---
---
Copper
---
969.00
1.938
4,300
Lead
---
16.00
0.032
840
Mercury
---
0.12
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
7.00
0.014
420
Selenium
---
5.00
OA10
100
Zinc
---
968.00
1.936
7,500
Environment 14 561
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

SOUND OF THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, 110
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
5.6
03/10/20
MAR
4500HB-11
1648
03/18/20
LFJ
EPA200.7
< 2.5
03/31/20
MTM
3113B-04
11489
03/18/20
LFJ
EPA200.7
0.87
03/20/20
MTM
3113B-04
969
03/18/20
LFJ
EPA200.7
6
03/18/20
LFJ
EPA200.7
16
03/18/20
MTM
3113B-04
2891
03/18/20
LFJ
EPA200.7
0.12
03/23/20
MTM
EPA7471B
7
03/18/20
LFJ
EPA200.7
10771
03/18/20
LFJ
EPA200.7
< 5.0
04/01/20
MTM
311313-04
16809
03/18/20
LFJ
EPA200.7
968
03/18/20
LFJ
EPA200.7
1.06
03/11/20
KDS
2540G11
c 60080
03/18/20
TLH
351.2 R2-93
c 2937
03/17/20
BLD
350.1 R2-93
c 14800
03/18/20
BLD
365.4-74
c 3.99
03/18/20
DTL
353.2 R2-93
< 5.0
03/18/20
LFJ
EPA200.7
Drinking Water xbr 33715
ID#: 561
DATE COLLECTED: 03/10/20
DATE REPORTED : 04/03/20
REVIEWVY
T
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2020
Permit No. WQ0018525
Southwinds Condominiums 1.20 % Solids
7.3 PH
Parameter
IF
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002
Nitrogen (TKN)
4.769
47,690,000
95.380
Phosphorus
1.452
14,520.000
29.040
Potassium
0.301
3,006.000
6.012
PAN (injected)*
1.455
14,549,860
29.100
PAN (surface)*
1.440
14,397.760
28.796
Ammonia Nitrogen
0.030
304.200
0.608
Calcium
4.971
49,707.000
99.414
Calcium Carbonate E .
---
---
Magnesium
---
2,892.000
5.784
Sodium
---
6,373.000
12.746
Sulfur
---
---
Nitrate N 1 Nitrite N
---
29.920
0.060
Barium
---
---
---
SAR
L 0.82
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
5765.000
11.530
Arsenic
---
2.50
0.005
75
Cadmium
---
0.96
0.002
85
Chromium
---
18.000
---
--
Copper
---
786.00
1.572
4,300
Lead
---
15.00
0.030
840
Mercury
---
0.23
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
9.00
0.018
420
Selenium
---
5.00
0.010
100
,Zinc
---
1,284.00
2.568
7,500
Environment 1 # 562 B
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SOUTHWINDS (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (slot to be used for reporting)
Aliuniimm, (thy wt. basis), mg/kg
Arsenic (dry wt. basis), mg/Icg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), inglkg
Chromium, T.(dry wt, basis),mg/kg
Lead (dry weight basis), mg/lig
Magnesium (dry wt, basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/Icg
Potassium (dry wt. basis), mg/lig
Selenium (dry wt. basis), mg/lig
Sodium (dry wt. basis), mg/lig
Zinc (dry wt. basis), mg/Icg
Total Solids,
TKN (dry wt,), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), n1g/Icg
Nitrate -Nitrite (dry wt.), nag/leg
Molybdenum (dry wt, basis), mg/kg
Sludge
Analysis
Method
Sample
hate
Analyst
Code
7.3
02/28/20
TMR
4500HB-11
5765
03/04/20
LFJ
EPA200.7
C 2.5
03/05/20
119TNI
311313-04
49707
03/04/20
LFJ
EPA200.7
0.9fi
03/06/20
MTM
3113B-04
786
03/04/20
LF3
EPA200.7
18
03/16/20
LFJ
EPA200.7
15
03/04/20
MTM
311313-04
2892
03/04/20
LFJ
EPA200.7
0.23
03/23/20
MTM
EPA7471B
9
03/16/20
LFJ
EPA200.7
3006
03/04/20
LFJ
EPA200.7
C 5.0
03/09/20
MTM
311313-04
6373
03/04/20
LFJ
EPA200.7
1284
03/04/20
LFJ
EPA200.7
1.20
02/27/20
JMS
254OG-11
e 47690
03/04/20
DTL
351.2 R2-93
c 304.2
03/03/20
BLD
350.1 R2-93
c 14520
03/04/20
AKS
365.4-74
c 29.92
03/02/20
AKS
353.2 112-93
C 5.0
03/04/20
LFJ
EPA200.7
Drinking Water ID, 37715
Wastewater ID, 16
PHONE [phone]
FAX [phone]
ID#: 562 B
DATE COLLECTED: 02/27/20
DATE REPORTED : 03/27/20
i�
REVIEWED BY: 24S
c Uncartified data. DWR does not offer non-agueoua certification for this analytical procedure.

Environment 1. Isic. CHAIN OF CUSTODY RECORD
P.O. Box 70-�8-�5. 114 Oakmont Dr. Page 1 of 1
Gree0v-ffre Z 27955
environment] inc.com
DISINFECTION
Phone [phone] FaX [phone]
CHLORINE NEUTRALIZED AT COLLECTION
CHLORLNE
Ij
pH CHECK (LAB)
CLIENT: s62 B Week- s
Ij UV
P
P
P
P
P
P
P
C4NTAINERTYPE,P/G
QUTHWINDS (HYDROTECH)
NONE
ON O'MARA
A
A
A
A
A
A
A
CHEMICALPRESERVAl1ON
YDROTECH
.O. BOX 4602
MERALD ISLE NC 28594
�- z
E 4
A•NONE D•NAOH
:52} 725-2319
U
Ld zo
�
O
2
cCn
LU
B . HNO, E - HCL
�"- C-H,SO, F- ZINC ACETATE/NAOH
COLLECTION
� R7
o
�
M 8
�' tz
LL
o
C
a
7
O
r
s
uE
E�
d
Z
¢ G-NATHIOSULFATE
���
SAMPLE LOCATION
DATE
TIME
K
Y`<`"
'?
Slud a Sample
5
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWRIGW
SOLID WAS TIE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING
APMENTlDELIVERY
N
SAMPLES COLLECTED BY
(Please Print)
SAMPLES RECEIVED IN LAB AT
RELINQUISHED BY (SIG.) (SAMPLER)
DATErTME
RECEIV
Y (SIG.)
TETIME
COMMENTS:
`
�74
n-
RELI Q 'SHED BY (SIG.)
OATEMME
RECEIVED BY (SI
DATE111ME
RELINQUISHED BY (SIG.)
DATE! T IME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this farm on the reverse side. Sampler must place a `�C" for composite sample or a "G" for
Fonts �� Grab sample in the blocks above for each parameter requested. N U 374527

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 14, 2020
Permit No. WQ0018525
Summer Winds 1.54 % Solids
6.2 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.441
64,410.000
128.820
Phosphorus
1.684
16,840.000
33.680
Potassium
0.477
4,765,000
9.530
PAN (injected)*
2.055
20,546.480
41.093
PAN (surface)*
1.972
I9,720.980
39.442
Ammonia Nitrogen
0.165
1,651.000
3.302
Calcium
5.502
55,020.000
110.040
Calcium Carbonate E .
---
---
Magnesium
---
5,084.000
10.168
Sodium
---
19,642.000
39.284
Sulfur
---
__.
Nitrate N / Nitrite N
---
67.780
0.136
Barium
---
___
SA R
2.66
Chloride
---
---
---
Iron
---
---
---
g Ceilin Concen.
(Mg/Kg)
Aluminum
---
2,407.00
4.814
Arsenic
---
2.50
0.005
75
Cadmium
---
0.79
0.002
85
Chromium
---
7.000
---
---
Copper
---
599.00
1.198
4,300
Lead
---
10.00
0.020
840
Mercury
---
0.17
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
10.00
0.020
420
Selenium
---
5.00
0.010
100
Zinc
---
2,062.00
4.124
7,500
Environment I # 119A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Efiwo'TOEH(M % hmpufflUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SWNC MASTER OWNERS ASSOC, INC
ATTN: DON O'MARA
HYDROTECH; SUMMER WINDS
P.O. BOX 4602
EMERALD ISLE ,NC 26594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mgllcg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mgllcg
Magnesium (dry wt. basis), mglkg
Mercury (dry wt. basis), mgllcg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %s
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mgllcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.2
01/14/20
TMR
4500HB-11
2407
02/03/20
LFJ
EPA200.7
<2.5
02/04/20
MTM
31138-04
55020
01/31/20
LFJ
EPA200.7
0.79
01/30/20
MTM
3113B-04
599
02/03/20
LFJ
EPA200.7
7
01/31/20
LFJ
EPA200.7
10
01/29/20
MTM
3113E-04
5084
02/03/20
LFJ
EPA200.7
0.17
02/06/20
MTM
EPA7471B
10
02/03/20
LFJ
EPA200.7
4765
02/03/20
LFJ
EPA200.7
< 5.0
02/05/20
MTM
3113E-04
19642
02/03/20
LFJ
EPA200.7
2062
02/03/20
LFJ
EPA200.7
1.54
01/15/20
KDS
254OG-11
c 64410
01/17/20
TLH
351.2 R2-93
c 1651
01/16/20
BLD
350.1 R2-93
c 16940
01/17/20
BLD
365.4-74
c 67.78
01/16/20
DTL
353.2 112-93
<5.0
01/31/20
LFJ
EPA200.7
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
ID#: 119 A
DATE COLLECTED: 01/14/20
DATE REPORTED : 02/14/20
REVIEWED47�
�y f`
. f L! ✓
c Uncertified data. DWR does not otter non -aqueous certification for thin analytical procedure.

mm r-RAIN OF CUSTODY RECORD
Environment 1, Inc.
P.O. Box M85. 114 Oakmont Dr_
Greenville, NC 27858
environment 1 inc xom
Phone [phone] • Fax [phone]
CLIENT: 119 A week: 5
SWNC MASTER OWNERS ASSOC, INC
ATTN. DON O'MARA
HYDROTECH; SU11IlV1ER WINDS
P.O..BOX 4602
EMERALD ISLE NC 28594
[phone]
COULECTION
SAMPLELOCATION D___+ATE TIME
- 74 1 GSS Z
BY (SIG) (SAMPLER)
BY (SIG.) _f I
DATFJTIME
BY (SfG.) DAME
DISINFECTION
Ij CHLORINE
UV
61-NONE
P
P P
P
P
P
P
A
A A
A
A
A
A
�o
u ,v 9 co
Z�
'z u'
CrU
-
.M
z
co
Q1 �
oEr,6
0
S
RECENM
RECEIVED BY (SIG.)
COMMENTS:
Page 1 of 1
CHLORINE NEt 1TRA III) AT COU-ECTION
pH CHECK (LAB)
COITAINERTYPE. PIG
CHEMICALPRESERVATION
A -NONE D-NAOH
LU
S-HNO, E-HCL
r C H2SO, F - ZINC ACETATE/NAOH
¢ G-NATHIOSULFATE
Q
a
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWRIGW
SOUDWASTESECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENTIDELIVERY
N
SAMPLES COLLECTED BY:
(Phase Pont)
SAMPLES RECEIVED IN tABAT L4 ('10 °C
Sampler must place a "C" for composite sample or a "G" for
PLEASE READ Instructions for competing This form an the reverse side. Grab sample in the blocks above for each parameter requested. NO 374849

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 11, 2020
Permit No. WQ0024756
The Grove WWTP 1.65 % Solids
6.6 pR
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.970
59,700.000
119.400
Phosphorus
1.210
12,100.000
24.200
Potassium
0.359
3,592.000
7.184
PAN (infected)*
1.993
19,928.320
39.857
PAN (surface)*
1.849
18,492.320
36.985
Ammonia Nitrogen
0.287
2,872.000
5.744
Calcium
2.663
26,632.000
53.264
Calcium Carbonate E .
---
---
Magnesium
---
2,056.000
4.112
Sodium
---
6,535.000
13.070
Sulfur
---
---
Nitrate N / Nitrite N
---
7.920
0.016
Barium
---
---
SAR
1.33
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
1075.000
2.150
Arsenic
---
3.40
0.007
75
Cadmium
---
0.50
0.001
85
Chromium
---
7.000
---
---
Copper
---
83.00
0.166
4,300
Lead
---
2.90
0.006
840
Mercury
---
0.08
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
7.00
0.014
420
Selenium
---
5.00
0.010
100
Zinc
---
382.00
0.764
7,500
Environment 14 549 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environment 1} Incorporated
Drsnkiug S9at;er ills 3-7�715
:-.r.L.OVA-Iuuuj, llY-VNn1Y1VIY 1_U IV a.-..--.----'-- - --- - `_---
GREE14VILLE,14c 27b95=70e5 _ . -
THE GROVE WWTP (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mgfkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt, basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.6
02/11/20
TMR
4500HR-11
1075
02/28/20
LFJ
EPA200.7
3.4
02/28/20
MTM
3113B-04
26632
02/29/20
LFJ
EPA200.7
< 0.5
02/26/20
MTM
3113E-04
83
02/26/20
LFJ
EPA200.7
7
02/29/20
LFJ
EPA200.7
2.9
02/25/20
MTM
3113B-04
2056
02/28/20
LFJ
EPA200.7
0.08
02/27/20
MTM
EPA7471B
7
02/29/20
LFJ
EPA200.7
3592
02/29/20
LFJ
EPA200.7
< 5.0
03/03/20
MTM
3113B-04
6535
02/29/20
LFJ
EPA200.7
382
02/29/20
LFJ
EPA200.7
1.65
02/12/20
MAR
2540G11
c 59700
02/14/20
BLD
351.2 R2-93
c 2872
02/13/20
DTL
350.1 R2-93
c 12100
02/14/20
TLH
365.4-74
c 7.92
02/13/20
TLH
353.2 112-93
< 5.0
02/29/20
LFJ
EPA200.7
1D#: 549 A
DATE COLLECTED: 02/11/20
DATE REPORTED 03/09/20
REVIEWED B V
c Uncertified data. DWR does not offer moo -aqueous certification for thin analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 5, 2020
Permit No. WQ0018525
Whaler Inn 0.39 % Solids
7.4 pH
Parameter
%
I Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
1.601
33,540.000
67.080
Phosphorus
0.397
13,520,000
27.040
Potassium
0.399
4,784.000
9.568
PAN (injected)*
0.534
5,344.200
10.688
PAN (surface)*
0.520
5,199.200
10.398
Ammonia Nitrogen
0.029
66.610
0.133
Calcium
5.591
45,578.000
91.156
Calcium Carbonate E .
---
---
Magnesium
---
3,403.000
6.806
Sodium
---
88,217.000
176.434
Sulfur
___
---
Nitrate N / Nitrite N
---
337.000
0.674
Barium
---
---
---
SAR
6.69
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
1,627.00
3.254
Arsenic
---
2.50
0.005
75
Cadmium
---
0.50
0.001
85
Chromium
---
5.000
___
---
Copper
---
712.00
1.424
4,300
Lead
---
6.90
0.014
840
Mercury
---
0.12
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
6.00
0.012
420
Selenium
---
5.00
0.010
100
Zinc
---
854.00
1.708
7,500
Environment 19 70A
*Determination of PIant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

RmAmM W % hCopumUd
114 OAKMONT DRIVE
GREENVILLE. N.C. 27858
THE WHALER INN (BUCK)
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mgllcg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt. basis),mg/1%
Lead (dry weight basis), mg/Icg
Magnesium (dry wt. basis), mg/Icg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mgllcg
Total Solids, %
TKN (dry wt.), mg/lcg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mgllcg
Nitrate -Nitrite (dry wt.), mg/lcg
Plant Available Nitrogen, mgllcg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Melhod
Sample Date Analyst Code
7.4
11/05/20
ICDS
4500HB-11
1627
11/12/20
LFJ
EPA200.7
<2.5
11/16/20
NI TM
311313-04
45578
11/12/20
LFJ
EPA200.7
<0.5
11/11/20
MTIM
311313-04
712
11/12/20
LFJ
EPA200.7
5
11/12/20
LFJ
EPA200.7
6.9
11/12/20
MTM
311313-04
3403
11/12/20
LFJ
EPA200.7
0.12
11/23/20
MTIM
EPA7471B
6
11/12/20
LFJ
EPA200.7
4784
11/12/20
LFJ
EPA200.7
<5.0
11/17/20
1y1TM
31I3B-04
88217
11/12/20
LFJ
EPA200.7
854
11/12/20
LFJ
EPA200.7
0.39
11/10/20
ICDS
254OG-1I
c 33540
11/10/20
DTL
351.2 R2-93
c 66.61
11/11/20
ICES
350.1 R2-93
c 13520
11/10/20
DTL
365.4-74
c 337.0
11/09/20
DTL
353.2 R2-93
7065
11/13/20
SE.1
<5.0
11/12/20
LFJ
EPA200.7
Drinking Water TDi 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
ID#: 70 A
DATE COLLECTED: 11/05/20
DATE REPORTED : 11/24/20
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

G
Environment I, Inc. GRAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr.
f;rpi-nvillP N( ?7QSR Page 1 Of I
env ironment I inc.com
DISINFECTION
Phone [phone] e Fax [phone]
CHLORINE
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
CLIENT: 70 A Week: S
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DURING SR MENVDELIVERY
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SAMPLES RECEIVED IN LABKi i _ °C
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DATEMME
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PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "T for
FORM 45 Grab sample in the blocks above for each parameter requested. N0 374869

PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING

ANNUAL PATHOGEN AND VECTOR ATTRACTION.REDUCTXON r,ORM (02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number WQ0018525
WWTP Name: SEE ATTACHED LIST NPDIa;S Number: SEE ATTACHED
Monitoring Period: From 1/1/2020 To 12/31/2020
Pathogent Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ 1 Alt R (Alk Treatment) ❑ Alt, C (Prior Testing)❑
Alt.D (No Prior Test) Li Process to Further Reduce Ptttho o s ❑Ix
If applicable to alternative pet'forrmed (Ciflss A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Dry,'itt E] Heat Treatment ❑ Tltetttto hi1ic ❑
Beta Ray [IGaw!jia Ray ❑. Pasteu s:. ..
- rization ❑
;lass B: Alt. (1) Fecal Density ❑
flicable to alternative performed (Class,B
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mly) Indicate "Process to
ig ❑ T Com7.
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Parameter in Sludge iExcee-
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2 x t0 to the MPN
6th power
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Fecal Caliform total solids
1000 mpn pee grain
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(in lieu offecal total solid (dry
0
monitoring data::
Frequency Sample . na u
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yp
Vector Attraction Reduction (15A.NCAC 02T .1107) _ Pleasc indicate alternative performed:
Alt. I (VS .reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day beach) ❑ Alt. 4 (Spec. Oz uptake) p
Alt. 5 (14=0ay Aerobic) ❑ Alt. 6 (Alk. Stabilization (l Alt T(Drying - Stable) 111 Alt. 8 (Diy ng - Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 1.0 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CEI RTfFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law; that the pathogen requirements in 15A NCAC 02T .1106.and the -
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15.A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This -determination has been mole under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. f am aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes, President
Prep , er Name and Title (type or print) Land Applies Name and Title (if applicable)(type or pt int)
Signature of Prepares* Vate Signature o g f Land Appller (!f applicable) Date
*Pieparer is defined in 40 CFR Patt 503.9(r•) acid 15A NCAC 2T .1102 (26)
DEER FORM Pl/RF 09T ii9/1>MF1 '

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2020 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit # WQ 0018526
RESIDUALS APPLICATION
2020 APPLICATION
SUMMARY
Will Turner
Site WT
2020
1
6.20
83,500
5.99
37.81
0.00
2020
2
5.00
108,500
5.83
39.09
1.70
2020
3
8.00
119,000
7.60
29.66
0.11
2020
5
2.60
1 80,500
3.98
36.09
17.03
2020
6
19087,500
5.72
57.91
9.33
Totals
Total Gallons 479,000
WWTP - Metric Tons 26.41

FIELD APPLICATION SUMMARIES

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
BARNES ENVIRONMENTAL WASTE
2020 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-01 6.2 ACRES TOTAL CALLONS 52,000
Swim IL
R2.,h
Ef
---
-----------
---
-----------
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------
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00
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111
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11
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JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2020 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-02 5.0 ACRES TOTAL GALLONS 101,500
-----------------
------------
---
--
-------
----------
---------
--------
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-------
---------
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0
14,000
7,000
0
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0 3,500
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0
0
0
0
0
0
0
0
0 0
0
0
0
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0 0
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0
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0 3,500
0
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0
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JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2020 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-03 8.0 ACRES TOTAL GALLONS 84,000
Alantic
Station
Beacons
Reach
CC Sass
Ca a Royal
Dolphin
Cedar
Point
B
Colon t'
The Sea
Ham ton
Suites
Dunesca a
Ei ht 112
Marina
Emerald
Plantation
Genesis
Condos
Harkers
Point
Island
Beach
Kin brid a
mi
l[
Manner's
Point
McGinnis
Paint
NC
Aquarium
7,000
3,500
7,000
3,500
3,500
3,500
3,500
3,500
7,000
7,000
7,000
7,000
14,000
21,000
3,500
0
0
0
7,000
0
1 3,500
0
3,500
0 1
0 1
0
3,500
77000
0
7,000
21,000
3,500
0
0
0
7,000
0
3,500
0
3,500
0
0
0
3,500
7,000
0
7,000
0
0
0
1 0
0
0
0
0
0
0
0
0
0
0
0
0
Sands
Villa
SCa Island
Plantation
Sea
Spray
--
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---------
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: 111
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JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2020 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-05 2.6 ACRES TOTAL GALLONS 66,500
----
-------------
----
---
----------
-----------------
------
-----------
--------
------------
-----
-------
----------
11
14,000
0
0
0
0
3,500 0
21,000
3,500
0
0
3,500
0
0
0
0
0
0
0
0
3,500
0
0 0
0
0
0
0
0
0
0
0
0
0
-
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JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2020 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-06 2.9 ACRES TOTAL GALLONS 87,500
-
----------------
---------------
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----
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0
0
1
0
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0
0
0
0
0
0
0
0
0 0
0
0
1 0
0

FIELD LOADING RATE REPORTS

ANNUAL .LAND APPLICATION FIELD SUMMARY FORM
Facility Marne: Barges'environmentalwasle&.Hauline Permit # W00018525 Anneal Dry Tons Applied: 5.99
Owner: Will Turner Operator. Steve Barnes Cation Exchange Capacity ( non 503): 2.2
Site #: WT Field:#: 1 Acres Utilized: 6.20 Acres Permitted: 6.20
Application. Method'*: S Volatilization Rate**: 05 Mineralization Rate: 30 % Predominant Soil'Series: GoA
- • • • � •-• • • - - -- ._.._-E:ic's�in�:: e:bv_:e .:eri-3=ir.': -:�i:�.c:u:::c;:...r-.a. :... ......................"R..»_.-,... _,.., .. - • - - - - - - �•-•-• - ._.._._.-._._._._.-. ,_.-..-.-._.._ _ ....... _._.. - - -• ..-.._ • - .. _.......... - -
2020
2020
2020
2020
2020
2020
1 3.000
14,000
3,500
2100
3,500
7,000
484
2,258
565.
-3,387
565
4129
1 0.63
2.12
2.68
1.65
1.60
2.00
1 0.01
0120
.0.06
0.23
0.04
0.09
AtraaticStation
13cacansRmctt
CC5ass
Tltr d-C W'WTPP
Occen.Club
QucensCoua
G/D
G/D
WD
G/D
G/D
GA)
0.000
0.001
0.003
0.002
0.0001
0.005
0.000
0.000
'0.002
0A00
0.000
0.005
10.015
0.535
0.125
0,039
0.029
0.111
10.000
0.006
0.002
0.001
0.001
0.005.
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.062:
0,002
0.002
3.000
0.005.
0,000
0,004
0.002
0.003
0.001
0.005
10.000
0,002
0.002
0.002
0.000
0,005
10.025
0A56.
0.138
0,178
0.117
0.363
1 0-,06
8.73
2.41
8.62
1 1.34
3.77
0.38
7.48
1.9.1
5.64
1.39
1.88
Com
Corn
Corn
Coro
Cdrn
Corn
I.55
28:57
163
27:83
436
12.00
0.011
0.79
0,00
1.34.
O..IS
0.87
0.00
0:00
0.12
0:00
0:00
0.00
2020
31.500
.5,081
1.54
033
Summer unds
GM
0.002
0.001
0.391
01107
0.000.10.003
0.007
.0.003
1.346
1217
10.99
Cote
42.03
1.08
0.04
TOW
83,500
Annual lbdacre 0.013 0.008
IZ45
0,922 0:000 0.015 0.022 0.015 2.615.
37.81 0.00
29.66
I:imeA
Current.Cumalative lbsthare 0.08 0.05
21.11
0:36 0.0I 0.13 021 0.12 27_73
147 50
Permit PAN Limit Ist/2nd Crop Date, Lbs/Ac
Prior Years Cumulative lbs/.atre0:07- 0:05
19.86
0:34 0.01 0.11 0 19 0.10 25,11
Perraittr-im lt-"*R 36.
1338•
267 15 NIA . 374 89 2498
•
"L certify, under penalty of. law , that this document vas prepared under my direction or supervision in accordance witkasystern
designed toassure that qualified.persodnel properly, gathered and evaluated
the information submitted. I. amaware thatfhere are
significant penalties for submitting ialseinfennation, including the possibility offines and iinprisonmeat for knowing viblati6n&"
"Application -Method: S - Surface, IN-
Injection, INC -.incorporation
amm of Land AppHE D to
s*Valagiizadon Race: Surface - 045 Injection/incorporation - 1.0
***GP.L.R: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF.(TI2002) Mod:

ANNUAL LAND .APPLICATION FIELD•SUMMARY FORM
Facility N3Mr: Barons £Quito lal Waste& Hatilingr Permit#: 4Y00018525
Owner: Will Turner Operator: Steve Barnes
Site 8: WT Ficld #: 2 Acres Utilized: 5.00
Application Method*: 8 Volatilization Rate**: 0.5
Annual Dry Tons Applied: SA3
Cation Exchange Capacity ( non 503). 6.8
Acres Permitted: 5.00
Mineralization Rate: 30 % Predominant Soil Series: GoA
ci�f�ic
Si�g��'-�
E2•�`i`.F�
`• . C1=�.:
:€��r�
ii.'l:'.'�t`.e?�;7k:t:;�
.. ssi+tl4a€�c`
�
:=S31�i
=€=>E 1gi
e?:`;ii:i`2
� c?ci
. '•. ,.r ;:.
•... ....................::::E
_:=r 2=:=?3::c2c3:c:i�;=
::=:_:.::¢_:E:::e::_:ic3
;e:i:;:e
'•,y�'•
:::::: - -- .:-:.-
•._.- :..•...;_:..:,;:::::::::::_::::::::::::::::::_:
2020
14,000
2,800
2.1-2
0.25
Beacons Reach
G/D.
0 001
0,000
0.664.
0.008
0.000
0,002
-0.005
0.002
0.557
.10.83
9.27
Coasat
35.42
0.98
0.W
2020
7,000
1,400
2.68
0.16
CCSass
G/D
0.008
0.006
0.3-11
0.006
0.000
0.006.
0.006
0.006
0.341
5.97
4.73
Coastal
1&93
0.00
0.29
2020
3,50Q
700
1.97
0.06
Cedar Point
G/D
0.0.06
0.003'
0.065
'0:003
0.000
0-003
0.003
0.003
A130
2.18
2.00
Coastal
628
146
0.0.0
2020
3,500
100
1.81
0.05
Hzm.wl)5uites
G/D
.0:000
0.0001
0.1241
0,000
-0.000
0.001
0.001
0.00.1,
0.082
0.70
1.35
Coastal
2,23•
0.15
.0.00
2020
10500
2,100
1.33
0_12
Dust -Pa
G/D
0.001
0.0001
0.115
-0.002
0.000
0.002
0.002
0:001
0.141
5.46
3.68
Coastal
18;10
0_ 17
0-0.0
2020
3,500
700
1.34
0.04
NCAq{-m=az
q
G/D
0.000
0.004
0.060
0.015
0.000
0,000
0.003•
0.000
. 0.112.
0.97
2.01
Coastal
3.23
0.02
0.60
2020
7,000
1,400
1.60
0.04
1 PC- Club
G/D
0.000
0,000
0-071
0.002
0.000
.0.001
0.003
0.001
0.289
333
3-45.
Coastal
10.81
0.45
0.00
-2020
28,000
5.600
0.43
0,10
P°➢>f"O0
G/D
0.001
0-000
0.141
0.003.
0..000
0.00.1
0.003
0.001
0.364
3.59
3.15
Coastal
11.62
0.0.1
0.1.6
2020
7,000
'1,400
2.00
0.12
QyeansC-
G/D
0,000
0.006-
0.138
0.006
0.000
0.006
0.006
0.006
0.451
4.68
2.33
Coasw,l
14.88
1;08
0.60
2020
2020
2020
2020
3,500
10,500
7,000
3;500
700
2.100
I;400
7.00:
0:51
1.11
1,06
0.39
0.01
0.10
0.06
0.01
s- hie PWdwi"
sea spray
5ound4f;]cccSca
W"alerrna
CAD
G/D
G/D.
G/D
0.000
0.000
0.000
0.000
0.000
0.000
0.000
O.000
0.007
0.197
0.120
0.016
0.001
0.003
0.002
01000.
0.000
-0.000
0.000
0.000
0.000:
0.001
0.001
0.000
0.001
0:002
9.001
0.000
0.000
0.001
0.001
0.000
0.038
0.169
0.120
0.019
0.17
1.08
0.12
1.70
0-51
1.5.1
-1.83
0.3I
Coastal
'Eoasial
Coastal
Ryo
1.15
11.30
7.44
076
0-00
'0:07
0.36
0.00,
0.00
0.00
0.00. .
0:01
Total
108,500
AnnuaIl&slacre 0.025 0.019 2.029 0:050 0.001 0.023 0.034 0.023 2$14 39A9 1.70 36.13
Current Cumulativc lbskere 1.87 0.10 77A6 25.08 0.46 031 1.00 0.65 92.43 299. 50 Permit PAN Lirnt lst/2nd Crap
Prior Ymrs Cumulative lbslacre 1.85 0.08 75.13 25.03 0.46 0.29 0 97 0:63 89.61
PcrmittC-P..1..IL"* 36 34 1 1338 267 15 N!A 374 89 2498
"'I certify, under penalty of lain; that this document was.prepared under my dircction or supervision in accordance with a system
designed to assure-that-qualif ed personnel properly gathered and cvaltiated the information submitted I am ululate that'there are
significant penaltiet for submitting false inforinati4n, including the possibility:oF fines and imprisonment for Imowing violations."
LimeApp.
Date
L6s14
X oy2,7- *Applicadon_Method: S - Surface, IN - in w4on,-1NC = Incorporation
( ignature.of Land Applie Date **Volatilizaiion Rate: Surface - 0-5,.Injectioriltricorpo6tibti - I.0
*"*C.P.L.R..: Cumulative Pollutant,Loading Rate
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Namt: Barrie+ Emiroamentai Waste& tlauleae Permit-4: W000I8525
Owner. Will Turner
Site -#: WT
Operator. Steve Barnes
Field 9: 3 Acres Utilized: 8.00
Application Method*: S Volatilization Ratc**: 0.5
Annual Dry Tons Applied: 7.60
Cation Exchange Capacity ( oon 503): 8:2
Acres Permitted: 8.00
Mineralization Rate: 30. % Predomina ut Soil Series: GoA
.
?`
F �i'
eii (t41 �`4`i3'
di
fro .
0.
€fii ii ieii
., i.'
.:`• , �c.
i�`lii;
��``
iiSaueie
's.�
::�..=k
• ::i:15;::,:-'�•K"1
e:
i%•0
�a�y
.hiR�'!=
1:.::i!
2020
14,000
1,750
0..63
0.05
AdmdcSlatim
G/D
0.000
0.000'
0.056
0.001
0.000
0.600
0.001
0.000
0.089
0.11
0.11
136
Caasw
Rye
5.61
0.01
Ot01
2020
21.000
2,625
2:12
0.23
Bens Reach
G/D
0.601
0.000
0.622
0.007
0.000
0,002
.0.005
0.002
0.523
10.15
8.69
Coastal
33.21
0:92
0.00
'2020
3,500
438
269
0:05
CC Sass
GID
0:003
0.002
0-097
0.002
0.020'
0.002
0.002
OA02
0..107
1.87
1.48
Coastal
5.92
0;00'
0.09
2020
7.000
875
1.81
0.07
Hampton5uitcs
G/D
.0.000
01000
0.155
O.oal
0:000-
0.001
0:002
0.001
0.102
0.88
3.69
Ccasta[
2.79
0.I9
0:60
2020
3;500
438
0.73
0,01'
"Eight iifl Mari=
G/D
.0.000
0.000
0:03 !
0.00:1
0.000
16,000
10.000
0.000
0;062
0:20
0.46
Coastal
1.35
0.00
0.00
2020
3.500.
438
212
0:04
Genesi5Condos
G/D
0.000
0.000'
0.050
0.001
0.000
0,00t
0.001.
0.000
0.096
1.51
0.59
Caastsl
a:BT
0.18
0.01
2020
3500
43$
1.84
0.63
MarinersAoint
G/D
0.000
0.000
0:079
0.001
a.A.0
6,000
0.001
0.000
0.1.00
1.00.
1.38
Coastal
3.26
0.13
0.00
2020
7,600
875
0.69
0.03
McGinnis Mik
O/O
0.000
0.00.0
0.077
0.001
0.00a
0.000
0.601
0-0001
0.054
0.86
1
0.88.
CKSW
194
0.01
0.00
2020
10,500
1,313
1.83
112
P-212-2-i
GM
0-001
0.000
0.097.
0.002
0.000
0.001.
0.1102
0.001
0.377
.0.49
2.45
Coastal
16.46
0:72
0.00
2020
2020
7,000
3.5W
875
438
2.00
0,51
0.07
0.01
.Queens Coup
S-Ulc,Ptatnation
G/D
G/D
0.004
.0:000-
0.004
0.000
0.096
0.005
0_004
0.001
0.000
0.000'
0.004
0.000
0.004
0,000
0.004
0.000
0.282.
0.024
1.93
0.11
1-46'
0.32
Coaswl
Coastal
930
0.72
0.68
0:00
0.00
0.00
2020
7,006
&IS
1.06
0.04
56undOfThe Sa
G/D
.0.000
0,000
6.075
0.00,
0.000.
0.000
0.'001
0.000
0,075
0.67
1.14
Coanat
4.65
0.23
0.00
2020
28,000
3-500
1.54
0.22
$LffmarWinds
On
0:001
0.060
0.269
0.004
'0.000
6.002
0.004
0.002
0:927
8.87
In
Coastal
28'.95
0:74
0.03
Total
119,000
Annual Ibs/acre 0.011 0.007 I.699 0.927 0.000 0.014 0.023 0.014 2.817
Current Cumulative lbs/acre 1 0.20.1 0.40 62-37 1 0.97 -0.01 124 0.63 0.21 66.07
.P'rior-Xears Cumulative lbs/acre 0.19 0:39 60.67 0.94 0.01 0.23 0.61 0.24 63.25
]Wmitt CP.%.R.11" 36 34 I338. 2G7 IS 1 NA 374 89 2498
"I certifj; inder•penalty oflav ;!bat this dacurhent was prepared under my. direction or supervision in accordance with a-systcm
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there arc
sigtufrcantpenalties. for submittilnefalse;iiiformation, Including the possibility of fines and. imprisonment forlmowing'violations;"
29,66 .0.11
299 50
29.47 ='
Permit PAN Limt 1st/2nd Crop
1.imc A
Date
Lbs/A
X ZO&Q &; ._1 *Application. Method: S �Surface,.M -Injection; 9NC-1hcorporatfon
( mre afLend Applier I7aie **Volatilization Rate: Surface - 0.5, lnjection4ncorporati. 1.0
***C.F.L.R: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR'FORM F5F (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: 132rnrsEnvironmental Waste& Halllinir Permit . W00018525
Owner: Will Turner
Annual Dry Tons'Applied: 3.98
Operator. Steve Barnes Cation Exchange Capacity ( non 503): 5.9
Site #: WT Field #: 5
Acres Utilized: 2.60'
Acres Permitted:
2.60
Application' Method*: S
Volatilization Rate**: 0.5
Mineralization Rate:
30 % Predominant Soil Series: GoA
202-0
14,000,
5,385.
0.63
0.14
AdanticSmtion.
G/D
6.001
0.000
0.17I
0.004-.1
0.000
0.0.01
0.004.
0:001
0.273
1 0.69
4.20
Coastal
17.27.
0.02
1 0.04
pe Royal
2020
3,500
1,146
1.67
0.09
Dolphin
G/D
0.005
0,004
0,065
0.008
0.000
0.004
0.004
0.004
0.559
339
2.8I
Rye
I0.39
1.15
.0.044
v oay y e
2020:
3;500
1,346
1.27
0.0.7
Sea
G/D
0.000
0.000
0.046
0.002
0.000-
0,00.1
0.002
0.001
0291
2.98
1.65
Coastal
9.88.
'0.09
-0:00
2020
21,000
8,077
1.33
0.45
Dunescape
GID
0.002
10.000
0.442
1 0.009
0-0001
0.006
-0.008
0.604
4.543.
21.01
14.16
ca=w
69.61
-0.64
1 0A0
2020
3,500
1,346
1 0.73
0.04
Eight 1/2Marina
G/D
0,001
0.000
0.095
1.0.002
0:000
'0.00.0
0:001
1 0,000
0.190
6.61
1
1.42
Coastal
4.1-5
D.00
O.Ol
2020
3,500
1,346
0 A6
0.03
Hatkets Point
G/D
0.000
0.000
0.019
1 0.001
O.00O
0:000
0.0.-C
0.000
0.057
0.96
1.11
Coastal
3.19
0.0D
0.00
otnt c
2020
3,500
1,3446
1.14
0.06
Vinas
Gm
0.00.0
0.000
0.089
0.009
0.000
0.001
0.001
0.001
0.271
2.07
2.1.9
Coastal
7.18
0.01
0.05.
2020
3,500
1,346
2.00
0.11
QutwsCourt
G/D
0.006
0.006
0.132
0.006
0:000
0.006
0_006
0.006
0.433
4:54
224
Coastal
14.34
1.04
O:OQ
2020
10,500
4,038
1.11
0.19
5easpray
G1I7
0.001
0.000
0.379
0.005
0.000
0.002
0,004
0.002
0,326
3,26
2.90
coasw-
21.74
0.14..
0.00
2020
14,000
5,385
I,54
0:35
Summer Winds
1G/D
0,002
0:001.
0.4.14
0.00.7
0.000
0.003
0600.7
0.003
1.:426
13.64
11.65.
Aye
44.54
1.14
0.05'
Annuallbslacre 0.018 0.012 1 1.$54 10,052 10.001 0.025 0.038 0.023 14,359 36.09 117.03
Current Cumulative lbs/acre 0.084 0.055 17.145 0.411 0.008 0.126 1 0.252 OA20 25.171 299 50
Prior Years Cumulative IN/acre 0.066 0.043. 15.291 0359 0.007 0.10I 0.214 0.097 20.812
Permitt C.P.L.R.*** 36 34 1338 267 15 N!A 3.r4 89 2498
"I certify.,: under penalty of law, that this document was prepared under my direction or supervision in accordance with asystera
designed. to assure, that qualified personnel properly gathered and evaluated the information submitted. I am aware that there:are
signif cant -penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations:"
x
(Sl ature of Land Applier D e
443x lame
xmit PAN Lunt Ist/2nd Cron Date ]
*Application Method: S - Surface, IN - Ipicction,1NQ-- Incorporatiop
**Volatilization Rate: Surface - 0.5, Injecdon/lncorporation- I,0
***C.P.L.R.: Cumu.Wive.PollutantI_oading.Raie
WMSS, PLLC
DENNR FORM 'FSF (712002) Mod.

Owner:
ANNUAL LAND APPLICATION HELD SUMMARY FORM
Facility Name- H.rne Environmentnl waste•&_Ranline Permit & W00018525
Will Turner Operator: Steya Dames,
Site#: NVT Field#: 6 Acres Utilized: 2.90
Application Method*: S VolatMaition hate**: 0.5
Annual Dry Tons Applied: 6.72
Cation Exchange Capacity ( non 503)> 6.7
Acres Permitted: 2.90
Mineralization Rate: 30 %
Predominant Sell.Seriem GoA
t Date:::
T
::..�y
''
_
l+zs'='Sands
:::is��fi�I:
s�
.tlt`..�.'.'
';tks'-s:
;=it~li
:=�'.u==i�i}=_2€k[=::Ala}�s.'syR;''�Zsi•"•'
1'ili•.
.�
�'.€�'•E
�.te•'' ..••1
-'��
::=ice:
-
'Nl•13-
.
2020
21,000
7,241
2.12
0.64
B-r* Peach
01D
0.003
0.001
1.717
0.020
0.000
0.006
0.013
0.006
1.442
18.67
9.33
23,99
Caastal
Frye
91.61
2.54
0.01
2020
I0,500
3,621
1:33
0.20
Ounescape
GM
0.001
0.000
0.198
0.004
0.000
0:003
-0,004
0,002
0.243
9.42
6.35
Coastal
3121
629
0.00
2020
14.000
4,929
'1.60
0.32
Ocean Club
G/D
10.002.
0.000
0.244
0.005
0.000
0.001
0009
0.003
0.998
1I50
11.89
CoaW
3728
1.S4
0:00
2020.
10.500
3,621
1.93
0:28
Pe6Lleaeach
CjD
0,M]
0.060
0.267
0.007
0.000
0.003
0.006
0-003
1.039
1.35
6.76
Consul
45.40
L97
A00
2020
7.000
2,414
-226
0.23
San& Vill0.s
GID
0.001
0 000
0.154
0.003.
0.000
-0.002
0.045
0.002
0-480
10.75
4:56
Coasttl
34.05
1 1166
0.40
2020
10.500
3;62I
O;S1
0.08
Sea Isla Plantation
Cril]
0:000
0.000
0.038
.0.007
0.000
0,001
0.003
0.001
0:196.
0.90
2.66
Ca=l
5:93
001
0.01
2020
7.000
2,414
1.06
0.11
SoundOfThakSm
-GID
0.001
0-000
0.207
0.003
0.000
0.001
0.001
1 0.001
0.207
1.86'
3-16
Caasw
12.82
O.fi3
0.00
2020
7.000
7-414
1.20
0.12
a
Condominiums
G/D'.
0.001
0.000
0.190
0.004
0.000'
0.001
0.002.
0,001
0.310
3.48
3.5,1
Coairsl
IL52
0.07
0.01
TOW
87,500
AnnualIbs/acre 0.010 0.003 3.016 0,054 0.001 0.021 0.043 .0.020 4,914 157.91 9.33 6287
Current Cumulative lWacre 0.088 '0:051 22A68 0.520 0.009 0,142 0.330 0.156 34:018 299 50 Permit PAN Limt istr2nd Crop
Prior Years Cumulative.ibs/scrc 0.078 0:048 19AS2 b 466 A.008 L0.122 0.187 0.136 29.104
PannittC:P.L.R***J 36 1 34 1339 2fi7 15 NIA 374 89 249$
"I certify, trader penalty oflaw, that this document was prepared under my direction orsupervision�in accordance with a system
designed to assure that qualified personnel propcdy.gathered and evaluated Ihe information submitted. I am aware that there.are
significant penalties for submitting false information, including the possibility of fu= and'imprisontnent'for knoMng violations:"
1.imeA
Date
Lbd A
*Application Method-. 5 - Surface; D4 - Injection, URIC. -incorporation
CS' ure of Land Applier) ` Date "Volatilization Rate: Surface - 0.5,1njeetion/lricorporation-1.0
***C.P_LR-: Cumulative Pollutant loading Rate
vuMSS. PLLC. DENR FORM.FSF'(712002) Mod.

SOIL ANALYSIS REPORTS

Page 1 of 1
Report No: 20-052-0796
Account No: 08361
Advisor: Willcox & Mabe Soil Solutions, PLLC
7231 B. Summerfiield Rd
Summerfield NC 27358
0
waypoint"' ANALYTICAL
Client: Steve Barnes
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypo i nta na lyti ca l.co m
Farm:
Date Received; 02/21/2020
Date of Report: 02/24/2020
Lab No Field 1D
Sample 1D
Soil Class 141114% tW/V pH
Ac
P-1
K 1
S-1
Mn-1
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
.ESP Na SS-1 NO3 N
03226
WT-01
MIN
0.6
5.7
0.5
200
12
21
100
75
75
125
2.4
81
61
15
1.6 0
Crop Recommendations:
Rec Uom
Lime (nacre)
N
P205
K20
S
Mn
Mn Al
Zn
Cu
B
M9
Last Crop
1- Corn
Iblacre
0.5
160
0
119
20
0
81
0
0
1.5
0
03227
WT 02
MIN
0.8
6.4
0.5
239
8
29
31
95
95
370
5.9
91
83
7
1.0 0.1
Crop Recommendations:
Rec Uom
Lime (nacre)
N
P205
K20
S
Mn
Mn-AI
Zn
Cu
B
Mg
Last Crop
1- Corn
Iblacre
0.0
160
0
129
20
0
29
0
0
1.2
0
03228
WT-03
MIN
1.3
7.4
0.0
197
6
33
31
323
323
1125
10.8
101
95
5
0.7 0.1
Crop Recommendations:
Rec Uom
Lime (nacre)
N
P2 05
K20
S
Mn
Mn Al
Zn
Cu
B
Mg
Last Crop
1- Corn
Iblacre
0.0
160
0
134
20
10
14
0
0
0
0
03229
WT-05
MIN
0.6
7.7
0.0
275
6
31
31
543
543
520
8.3
100
94
5
0.5 0
Crop Recommendations:
Rec Uom
Lime (nacre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu
B
Mg
Last Crop
1- Com
Iblacre
0.0
160
0
134
20
10
10
0
0
1.2
0
03230
WT-06
MIN
0.7
7.6
0.0
272
6
33
31
693
693
870
8.5
101
93
7
0.8 0.1
Crop Recommendations:
Rec Uom
Lime (nacre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu
B
Mg
Last Crop
1- Corn
Iblacre
0.0
160
0
134
20
10
11
0
0
1.2
0
Comment:
Test result units = CEO and Na in meg1100cm3; NO3 N in mg1dm3; WN in g1cm3
North Carolina Division of Water Quality Certification #257. Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared t)y: Waypoint Analytical Virginia, Inc.