WQ0021826_Residual Annual Report 2020_20210224

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00021826
Applicant/Permittee City of Roxboro
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide inforration on the person to be contacted by N B Staff
Name * Lysa Finnerty
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
14105376150
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0021826
Fbs Current Existing perrrit number
Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220
Facility Name * City of Roxboro RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report for City of Roxboro NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Forr} Engineering Fans, Specifications, Calculations, Bc.)
Roxboro NC 2020 Annual Report FINAL.pdf 8.59MB
Upload only 1 FFdocurrent (less than 250 fvB). Miltiple documents rust be combined into one FJFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/24/2021

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 24, 2021
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report for Permit No. WQ0021826
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Roxboro, NC.
If you have any questions or need additional information, please do not hesitate to contact
Thomas Warren at [phone] ext. 22 or Ryan Copeland at [phone].
Sincerely,
W�1 01_ I t
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Thomas Warren, City of Roxboro
Ryan Copeland, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF ROXBORO, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0021826
2020 ANNUAL REPORT

City of Roxboro, NC
Residuals Land Application Program
2020 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

WQ Permit #: W00021826 County Person Year 2020
Facility Name (as shown on permit) City of Roxboro WWTP & WTP NPDES No. NCO021024
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and PartB and proceed to PartC. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 250.10
Total number of acres utilized for land application during the year: 59.5
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations"
Thomas S. Warren. Assistant City Manager
ermittee Name and Title (type or print)
Signature of Preparer Date
(if different from Permittee)
2- 19—'z►
Signature of Permitt Date
21
Signa e ppli r Date
(if different from ermittee and Pre arer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
ROXBORO,NC
ROXBORO, NC WWTP AEROB. DIGESTED CAKE
MONTH/YEAR
July 2020
August 2020
TOTAL
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
846.00 Y 138.23 D 125.37
575.00 Y 111.87 D 101.46
1,421.00 Y 250.10 D 226.84
Report Date: 2/9/2021 1:37:21 PM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0021826 Laboratory:
Facility Name: ROXBORO,NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source WO # or Inc.
NPDES#: NCO021024
WWTP Name: ROXBORO WWTP
Product Type
Sample or Composite Date
AEDCAK
01/23/20
AEDCAK
07/30/20
AEDCAK
10/14/20
AEDCAK
10129/20
Parameter (mglkg dry weight)
Ceiling Conc.
Limit
Percent Solids
NA
19.40
23.10
22.40
21.60
Arsenic
75
3.76
4
5.5
4.9
Cadmium
85
0.727
1.3
1.6
1.2
Copper
4300
377
470
580
590
Chromium
NA
26.5
30
46
38
Lead
840
32.4
38
51
50
Mercury
57
0.396
0.77
0.8
<0.82
Molybdenum
75
6.24
4.1
7.5
6,6
Nickel
420
15.1
15
18
16
Selenium
100
5.09
6.7
8.1
8.2
Zinc
7500
773
870
1100
1100
Total Phosphorus
NA
19300
17000
14000
13000
TKN
NA
56200
42000
41000
40000
Ammonia -Nitrogen
NA
1870
8400
6400
5.4
Nitrate and Nitrite
NA
63.4
4.5
4.83
6.03
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* f Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1 102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/912021 1:48:38 PM For 2102 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WO Permit Number:
WQ0021826 Laboratory:
Facility Name:
ROXBORO,NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source
Inc.
NPDES # or WQ#:
NCO021024
WVVTP Name:
ROXBORO WWTP
Product Type
AEDCAK
AEDCAK
AEDCAK
AEDCAK
Sample or Composite Date
01/23/20
07/30120
10/14/20
10129/20
Parameters (mg/kg dry weight)
Aluminlurn
18900
22000
30000
31000
Calcium
10600
10000
17000
13000
Magnesium
3290
2500
3400
2600
pH (s.u.)
6.80
8.10
7.80
6.70
Potassium
4010
2200
2400
2600
Sodium
567
540
970
730
PAN
17228
14285
13585
12007
SAR (Ratio)
0.5415
0.5996
0.8385
0.7086
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1 102(26)
Printed: 2/10/20219:40:53 AM For: 2102 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
2/3/2020
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-024-0014
Project Description: Roxboro WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/24/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�a f• c•—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-024-0014
Client Project Description: Roxboro WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
70268
Roxboro WWTP
Solids
01/23/2020
11:30
01/24/2020
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

i
Waypoint.:
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46487
Synagro Central LLC/ Roxboro
Ryan Copeland
Mary Brewer
Project
Roxboro WWTP
Report Date : 02/03/2020
284 Boger Road
Information :
Received : 01/24/2020
Mocksville , NC 27028
Pam« mL 60wr
Submitted By : Ryan Copeland
Pauric ry
Report Number : 20-024-0014
REPORT OFANALYSIS
Agronomist
Lab No : 70268
Matrix:
Solids
Sample ID : Roxboro WWTP
Sampled:
1/23/2020 11:30
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
80.6
%
0.010
1
01/29/2017:05
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
1870
mg/Kg -
dry
515
1
01/31/20 12:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
63.4
mg/Kg -
dry
25.3
1
01/29/20 13:34
ZBD 4500NO3F-2011
Organic N
54100
mg/Kg -
dry
1290
1
01/31/20 10:00
CALCULATION
pH
6.8
S.U.
1
01/30/20 06:12
JSL 9045D
Total Solids
19.4
%
0.010
1
01/29/20 17:05
ADM SM-2540G
Total Kjeldahl Nitrogen
56200
mg/Kg -
dry
1290
1
01/31/20 10:00
JPJ ;M-4500-NH3C-TKl`
Phosphorus
19300
mg/Kg -
dry
25.8
1
01/29/20 17:06
JTR 6010D
Aluminum
18900
mg/Kg -
dry
25.8
1
01/29/20 17:06
JTR 6010D
Arsenic
3.76
mg/Kg -
dry
2.58
1
01/29/20 17:06
JTR 6010D
Calcium
10600
mg/Kg -
dry
129
1
01/29/20 17:06
JTR 6010D
Cadmium
0.727
mg/Kg -
dry
0.515
1
01/29/20 17:06
JTR 6010D
Chromium
26.5
mg/Kg -
dry
1.29
1
01/29/20 17:06
JTR 6010D
Copper
377
mg/Kg -
dry
1.29
1
01/29/20 17:06
JTR 6010D
Iron
19400
mg/Kg -
dry
25.8
1
01/29/20 17:06
JTR 6010D
Lead
32.4
mg/Kg -
dry
1.55
1
01/29/20 17:06
JTR 6010D
Magnesium
3290
mg/Kg -
dry
25.8
1
01/29/20 17:06
JTR 6010D
Manganese
804
mg/Kg -
dry
2.58
1
01/29/20 17:06
JTR 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

i
Waypoint.:
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46487
Synagro Central LLC/ Roxboro
Ryan Copeland
Mary Brewer
Project
Roxboro WWTP
Report Date : 02/03/2020
284 Boger Road
Information :
Received : 01/24/2020
Mocksville , NC 27028
Pam« mL 60wr
Submitted By : Ryan Copeland
Pauric ry
Report Number : 20-024-0014
REPORT OFANALYSIS
Agronomist
Lab No : 70268
Matrix: Solids
Sample ID : Roxboro WWTP
Sampled: 1/23/2020 11:30
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
0.396
mg/Kg
- dry
0.0721
1 01/29/20 12:06 TJS SW-7471B
Molybdenum
6.24
mg/Kg
- dry
1.29
1 01/29/20 17:06 JTR 6010D
Nickel
15.1
mg/Kg
- dry
1.29
1 01/29/20 17:06 JTR 6010D
Potassium
4010
mg/Kg
- dry
25.8
1 01/29/20 17:06 JTR 6010D
Selenium
5.09
mg/Kg
- dry
2.58
1 01/29/20 17:06 JTR 6010D
Sodium
567
mg/Kg
- dry
129
1 01/29/20 17:06 JTR 6010D
Zinc
773
mg/Kg
- dry
6.44
1 01/29/20 17:06 JTR 6010D
Sulfur
7220
mg/Kg
- dry
25.8
1 01/29/20 17:06 JTR 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 2-4237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46487
Customer Name: Synagro Central LLC/ Roxboro
Report Number: 20-024-0014
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 01/24/2020 13:33:31
Page 5 of 6

SAMPLING LOG # 4i�l�I�IIEa��ll�h�l��1��14i�1�i���lll�lll��l�41��f�l�l�ll�lilllll a
oo
_ gyriagro central LLC; Roxboro 13.3211
Roxdafa NVWTP
PRDJECT MANAGER: - hN
Phone:( `_�3t] ) V)_
I AGRICULTURAL -LASS, INC, CHAIN OF dCUSTODy
Road RECORD & ANALYSIS
3237 RECORD
l attest that the proper field sampling procedures
were used during the collection of these samples.
SAMPLER
A & L CUSTOMER
LAB # SAMPLE I.D.
SAMPLING
LOCA-h0N
SAMPLE
TYPE
# OF SAMPLING METHOD
CONTAINERS DATE TIME PRESERVED
METHOD
SHIPPED
Relinquished by Sampler. Date Time Recieved by: REMARKS:
?IRN COQtIA0� '[,��0 Iy 30-
Rellnqulshed by: Date 'nme Reole�e
Z i]
Relinquished by: lbate I Time Red! ed by:
SPECIAL INSTRUCTIONS:
c. monitoring purposes. PO#:
SAMPLE
ANALYSIS REQUEST
I.D.
SLi
SLR
NH _N
a
N❑ -N
a
�r�anlc
Cd
CrNI
Pb
As
Hg
Se
pH
CaCO3
uiv.
Volatile
Solids
Mo
Cl
ND -N
a
1400
100
1,00
k0or
too
1.0w
]"Oor
too
1.0or
J�w
too
1
SL1: Taal Solids (Moisture), Total Kleldahi Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iran, Aluminum, Manganese, Copper and Zlno
Page 6 of 6

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Roxboro WWTP
Lot Number:VG31063
Date Completed:08/10/2020
08/11/2020 6:40 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VG31063
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure. The LOQ has
been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VG31063-001
Description: ROXBORO WWTP Matrix: Solid
Date Sampled:07/30/2020 0715 % Solids: 23.1 08/01/2020 2011
Date Received:07/31/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 08/01/2020 2011 SRB
62017
1 350.1
(Ammonia - N ) 350.1
50 08/06/2020 1639 DMA
62563
1
(Nitrate - N ) 9056A
1 08/05/2020 1419 AMR
62554
1
(Nitrite - N ) 9056A
1 08/05/2020 1419 AMR
62552
1
(Phosphorus) 365.1
50 08/05/2020 0845 DMA
08/04/2020 1258
62258
1
(Soil pH meas) 9045D
1 08/07/2020 2322 SRB
62831
1 351.4
(TKN) 351.2
5 08/05/2020 1741 DMA
08/05/2020 1005
62372
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
23.1
%
1
Ammonia - N (gas diffusion)
350.1
8400
220
110
mg/kg
1
Nitrate - N (soluble)
9056A
3.3
2.2
0.43
mg/kg
1
Nitrite - N (soluble)
9056A
1.2
0.87
0.43
mg/kg
1
Phosphorus
7723-14-0 365.1
17000
1100
220
mg/kg
1
Soil pH measured in water @
22 ° C
9045D
8.1
su
1
TKN
351.2
42000
540
540
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
5 08/05/2020 0852 JAB2
08/01/2020 1641 62042
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
0.77 J
1.6
0.39
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 08/05/2020 1624 KSH2
08/04/2020 1422 62041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
22000
29
11
mg/kg
1
Arsenic
7440-38-2 6010D
4.0
1.1
0.36
mg/kg
1
Cadmium
7440-43-9 6010D
1.3
0.36
0.090
mg/kg
1
Calcium
7440-70-2 6010D
10000
360
45
mg/kg
1
Chromium
7440-47-3 6010D
30
0.71
0.18
mg/kg
1
Copper
7440-50-8 6010D
470
0.71
0.32
mg/kg
1
Iron
7439-89-6 6010D
17000
7.1
3.3
mg/kg
1
Lead
7439-92-1 6010D
38
0.71
0.32
mg/kg
1
Magnesium
7439-95-4 6010D
2500
360
45
mg/kg
1
Manganese
7439-96-5 6010D
760
1.1
0.42
mg/kg
1
Molybdenum
7439-98-7 6010D
4.1
2.9
0.71
mg/kg
1
Nickel
7440-02-0 6010D
15
2.9
0.75
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VG31063-001
Description: ROXBORO WWTP Matrix: Solid
Date Sampled:07/30/2020 0715 % Solids: 23.1 08/01/2020 2011
Date Received:07/31/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 08/05/2020 1624 KSH2
08/04/2020 1422 62041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
2200
360
45
mg/kg
1
Selenium
7782-49-2 6010D
6.7
1.4
0.58
mg/kg
1
Sodium
7440-23-5 6010D
540
360
45
mg/kg
1
Zinc
7440-66-6 6010D
870
3.6
0.89
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Shrn'y Fmimnmeninl'§zyices, bic.
Page I uC I
Di unen-. Numki' MBJ01&:AL
F:fir¢rve Tx='e Kr2 �I}lY.
ample Reoeipt Checklist ( RF
r
{;lic-nI- 1ICIi 6r'
l�Q
CnoicrInaaeCledbYrda[6'4L�I , I1.i ff��_0 L014:�J�]
cans off AMP-; SF,ST ❑ 0 ierr U PS Q l; c&x Otbvr;
❑ Yrsj
2NolI
- Were cusiodv seals present on N; caNrlur?
Yes
No I
=A 12.
IfciL3-AAA souls were arr%eia, were tlie,, ioinct and unbroken'?
l i Strip LD: { l7Iorine Strip IV; - _ Tea d by'
Uri ga+l �tc�mperrlua�3irccipt ! Deri� i1(C orreated) t r l ,�L upon rcc eipf ° nsillid Snap-C'up ID'71r. :� ¢n � �C. " {
4letnod; U'Rmlipeudure T3 nk gafnst Liatdcs lit Gun LU; _---- TR �„n C'uneL;Li{u7 Facror:
1AeLliod of coolant: lJ Vi�'e kt! ❑ Tee Packs ❑ I} y Icu ❑ Nouc
0 YLti
❑Tyra
1l
. li tens} ranlra of any cookT rxrceded 6-0`C- was; Project Maw.er Notified:?
I'M was Notifi.od bt; phone! QMijiI r' fWU-L[7-fo-lac (LiMle Wle).
4. la the comiliercial couricr'spackingshp attuhcx IQ 01i9 form?
g❑Teo
e
❑Teo
5, Were prDper cusmdy procediurs (relinquishcd"roucivoLD 1°ollowL:d?
Igo
6. Welt sample IDs iisred oil the coc`.',
e3
No
7. Were sans le LC15 L3", on all .58m 11r, 4:rmtminor4?
3
I❑I
LL No
S. Wa3 colled:tion date k time. Iislsxl On && C OM
9. Was calicction date & time liswd on all sample containers?
e3
❑ -No
Yes
❑ N rt
10- Did all cantaincr labs- infurrLutOua (1) ), kNw, Lim c) w i Lh .ham CO-C.?
es
❑ No
11- Wuz: tc 3N tu be perfomied- list W on ft C VX7:
Y-es
❑ No
12- Did all samples 8rrivcp in tb,� rtr"r L orkwinrrS Ior each test andr'nr in good condition
(unbroke , lids ail, ctc.)7
cs
❑ No
113. WaS ad:. UMZ SaRLple vuluno4 5lvuilabin?
'r cs
El0
14. Wac all sample€ reecivwd wiLhip LhL hold3in time or 48 huw.s, whichever calves first?
Yee
T*fn
15. WaU FloY !!JUMPIL'S L'4nLF1iRMi (rifle we) samples Not listed on C:OC'
❑ VC4
El NON
A
16. For V 0 A a:sd RSK-175 samples, ivaur bubbles prescnz }`iPCa.size:' (%"or Oinm in RiMU NT1
iannyorLiicVOA vi81s?
❑ Y cs
No
lA
17. Were all DRU,'luetalsAwtTicm saml)lcs rcccivrd at a pH of � "??
❑ Yes
1*aMTqA
1R. Wrre all cyanide samples received at a pil ? 12 and salfide samples received at a pli .> 9'2
El Yes
Q KO
C1��JQ.�
19. Were all applicable NII1.VTKN,cyuA e p G?5 (, 0.5mg'L Samples rea a msi ua
chlorine:
El Yap
Q No�0.
NA
- Were client remarkF, requests (i.e- requested diiution3, 1w15?IASD designations: etc.--)
currecLiy Lranscribed From the COC into the coluluent section in UMS?
❑ Yesl
U<o
121. VMw tic u;IIL minnher Ii9l-Oa On Liie Cxuikiiiier 10i6l? If yes, Quilte 4
Sa mplc Presvra40ur3 (Tviuslbe caPinlaleted rarallV Saanple(S) incorlWly pfe:Selved CUWitli head3pace-1
aillple(s) _.. - w=r-nrnive.d incormu.ly prczsnrvm1 rmd were atljusuNI acuydingly
in sample rece i-61ig with mL of circ lc one; 1112SO4, HNCk3, HC'1, NuOB using Sit AL'— --
Time of preser)M011 _ I F mcfe than one prc5ti,,Lv ivc is needed, please natd: in the commcncs bcluw.
SampJc(3) were received Vail?} bubbieri >6 inIrL ill diunsalef_
5auipl*s) _ were rncciv-A with TR C ? 0-5 mgi I. (Tf # 19 is no) o-3nd wrm
Fvcljusced accordijigly in sample receiving with 5odiLLIr thiosull: tto (NEiIS2 k,) witli Shealy
SIB barrode JaMs ap-ilicd b!�; — fjali:. .
C'nLtinlentx:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryand Copeland
Project Name: Roxboro
Lot Number:VJ16004
Date Completed:10/23/2020
NIM�� Mr�
10/28/2020 3:24 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VJ16004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample -001 was weighed out at 3 times the normal amount. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VJ16004-001
Description: ROXBORO N&M Matrix: Solid
Date Sampled:10/14/2020 1145 % Solids: 22.4 10/17/2020 0144
Date Received:10/15/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 10/17/2020 0144 LSH
70234
1 350.1
(Ammonia - N ) 350.1
50 10/19/2020 1648 DRD
70365
1
(Nitrate - N ) 9056A
1 10/21/2020 1913 AMR
70656
1
(Nitrite - N ) 9056A
1 10/21/2020 1913 AMR
70657
1
(Phosphorus) 365.1
100 10/20/2020 1740 DMA
10/20/2020 1300
70385
1
(Soil pH meas) 9045D
1 10/20/2020 2235 AAB
70569
1 351.4
(TKN) 351.2
10 10/21/2020 1818 DMA
10/21/2020 1201
70594
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
22.4
%
1
Ammonia - N (gas diffusion)
350.1
6400
220
120
mg/kg
1
Nitrate - N (soluble)
9056A
4.3
2.2
0.45
mg/kg
1
Nitrite - N (soluble)
9056A
0.53 J
0.89
0.45
mg/kg
1
Phosphorus
7723-14-0 365.1
14000
2200
450
mg/kg
1
Soil pH measured in water @
19.2 ° C
9045D
7.8
su
1
TKN
351.2
41000
1100
1100
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/20/2020 1340 JAB2
10/20/2020 0910
70438
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
0.80
0.35
0.085
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 10/22/2020 0127 KSH2
10/17/2020 1518
70258
2 3050B
601OD
1 10/22/2020 1351 KSH2
10/17/2020 1518
70258
3 3050B
6010D
3 10/22/2020 1355 KSH2
10/17/2020 1518
70258
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
30000
89
33
mg/kg
3
Arsenic
7440-38-2 6010D
5.5
1.1
0.37
mg/kg
1
Cadmium
7440-43-9 6010D
1.6
0.37
0.093
mg/kg
1
Calcium
7440-70-2 6010D
17000
370
46
mg/kg
1
Chromium
7440-47-3 6010D
46
0.74
0.18
mg/kg
1
Copper
7440-50-8 6010D
580
2.2
1.0
mg/kg
3
Iron
7439-89-6 6010D
22000
22
10
mg/kg
3
Lead
7439-92-1 6010D
51
2.2
1.0
mg/kg
3
Magnesium
7439-95-4 6010D
3400
370
46
mg/kg
1
Manganese
7439-96-5 6010D
870
3.3
1.3
mg/kg
3
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VJ16004-001
Description: ROXBORO N&M Matrix: Solid
Date Sampled:10/14/2020 1145 % Solids: 22.4 10/17/2020 0144
Date Received:10/15/2020
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D
1 10/22/2020 0127 KSH2
10/17/2020 1518 70258
2 3050B
601OD
1 10/22/2020 1351 KSH2
10/17/2020 1518 70258
3 3050B
601OD
3 10/22/2020 1355 KSH2
10/17/2020 1518 70258
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Molybdenum
7439-98-7 6010D
7.5 3.0
0.74
mg/kg
1
Nickel
7440-02-0 6010D
18 3.0
0.78
mg/kg
2
Potassium
7440-09-7 6010D
2400 370
46
mg/kg
1
Selenium
7782-49-2 6010D
8.1 4.4
1.8
mg/kg
3
Sodium
7440-23-5 6010D
970 370
46
mg/kg
1
Zinc
7440-66-6 6010D
1100 11
2.8
mg/kg
3
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
valy awivalukl nal SW V"V Inc. 1"WU I C. I
Dwvumcii'.Na-nM:r: 4117M1AC-1.1 T'15t�ti'c Uala :1+3��C 1$
Sample Reeci.pt Checklist ( RQ
Clicnt: SYNAGM[) Cooler Inspected hvldate, Ho-nr r l(Vl61zg of-_ y,1;GQC
McQt)S OfMcipl;
SESI ❑ C1i-cnLUF UPS © FedEx Oih.er. -
M VeSj
0 N01
11. Wore custody Weill, pr4;XatL on the 0001er? -
5re4
EINJ
OWA12.Ifcustadysnals were nrrsenr, were they h2lucl turd unhraken'?
H Strip
ID. NA
Chlorine Strip Mr TEA Tested bv:
riglril l
t01UPC0-aturc upon roceirt f Derived (CnivcLrml) lvls:pQ.-A re upon rerx[pt 1/6$Q][a S up-0ip ID: 20-2056
1.7 { 1,7 -C
NA i hA c. NA INA iC KA INN °C
Mrilhotl;
J t Gun JD' 5 _ Ilk Chu i Cormcfio ri. Fac9cw, a °C
Method ofwalEra: P1 wcq Ice ❑ ice padcc ❑ 17r 1ct ❑ 1,lcsrxi
❑ YES
❑]o
KJlA [I terniaerl,turC of airy cucrler rxCMC i�,U`C. Wd7r PY�.fcct I413n8 rfetified'?
PM WETS Nu[3fiod by: phone { ert m]I I ?ace to -race (eir,1c one).
® Yrs
❑ No
E]MA 4. Jsthe commercial courier's picking slip atrachm;d in tltis form?
i Yeq
❑ Nn
5. WEar prigwr rtntnry J,a+ ds1res(ralin vishedb- vciveil) Pcjlrrwe ?
1Z Ycs
❑ No
G. WelebmnirluTD..R Jis#ed on [he COC? T
Ytn
❑ No
17. Ware smplc Ws Jilted on all n !c con 3iu ?
® Yes
❑ No
li. Was c 11tw. ion date & tirnp listed on tJie CDC?
Yns
No
9_ WaN collection date & limo listed an al I mrnplc contabiers"
1r+:5i
❑ No
10- ]did Fall container 1ahe1 infvnnat:ion (ID, dwr, time) area luith IN; WC?
Vfvesi
LINO
11. Were La,;r4 to be P efl!673 104 -iSU 1 a:1 the COC?
� Yes
❑ No
l2. Uid aJJ Sd#1'tp[CS anVe in. tho puipcc containers fTJr eaCh _Z31t 31 lji(3 r in 1;a id caidition
(unbroken. lids url,
Yc.
❑ Nn
113. Ww, sdctTuatesa„llplc wcilumk aysilal lk?
Ll Yes
O No
J4. bbux. a J samples xccivcd w'dkln 'A the holdin; bre ur 48 hotim M�ikheVItr -Crnnes tia'st?
Ym
0 No
15. Werc any lam .les L,Ontainers lui5siiigJ::xi;L;m (circle one) simple1ti01 l:stcd an i UL"f
Y"
1�1
❑ No
16, ]err VC}.�' and l?SK-175 stapplez, were 1wb'alas present>'`pea_sir " ("r 5
NA l. omin in d ameaer}
is an Qt lha VOA Vials?
❑ Yes
tea
NA 117, Were all DR-0:nctmishtutrien' sarnplcs received al a pA of<27
❑ Yes
❑ No
®NA IS. Weir all L anidk Sam Ies reueiV'-'d kit a pi I _> L2 6,nfl sulfide sairLp m received zt a H
❑ Ym;s,
0114m�
r7� I9- WCre a 11 applica0l1 , I !7'1tNrcyanidelphr. �o 23 s ; O, SIn 'i) mpieS flea o residual
IOItiA ..
❑Yes 0 No �TiA `�. Werec-'ient rcrnarksh"ues[s(i.e. -1;qucstad dil'-i`ipns, tw15?h ED-i -Hi�,1&ti0tts_
orreetly [=scribed frrnu the COC inl(rtha coin menr.aeot:on
❑ Ycrl A Nn 12.1. Was the uuW slumber listed M tho cohtaine, ]�.bcl7 if ,es, Quot4 y 19771
�a ple Prrw-vatiau {[ ,mxr. bit mupleted for any sample(g) incorrectly pttawryMd or v4di lmr I -pace-)
Stlmple(s) NA
rere received iracrnTcctl}'rHesened an +,erg ttdlustad according]}
in sample receivirE twitlf NA _mL. ofcir2Ja arc: H2SQ-0, HNO3, H%I, N@01A using Sk pr NA _
iree of preseruadcmi NA Ir mom than one piw-sernilive is need, p.case note in the ¢ mutet7is belo+t.
SattlpJc(;} NA_ ,were received v+itlL IG Lunt ir, &ji-Lo.;r,
5slnples j TJA %yera iwaived wish TRC 7 0.5 mgf1.{ if#19 Js "n rand were
djusted Finuordingly m sainplo receiving " tb scdium thiaaulFhtr,• a,S 0)) will, Nhea[y 1p; N
H btirrcade iabek applied by; J3LVG
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Ryan Copeland
Project Name: Roxboro
Lot Number:VJ30035
Date Completed:11/13/2020
NIM�� Mr�
11/13/2020 11:04 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VJ30035
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the initial sample amount was 3X the standard procedure for the
following sample: VJ30035-001. The LOQ has been adjusted accordingly.
The following sample was diluted due to the nature of the sample matrix: VJ30035-001. This sample was
foamy so to maintain the integrity of the instrument, these samples were diluted 10 fold. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VJ30035-001
Description: ROXBORRO N+M Matrix: Solid
Date Sampled:10/29/2020 0845 % Solids: 21.6 10/31/2020 0003
Date Received:10/30/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 10/31/2020 0003 LSH
71843
3 350.1
(Ammonia - N ) 350.1
1 11/12/2020 1650 KMC
73041
1
(Nitrate - N ) 9056A
1 11/04/2020 1144 AMR
72265
1
(Nitrite - N ) 9056A
1 11/04/2020 1144 AMR
72267
1
(Phosphorus) 365.1
100 11/04/2020 1220 DMA
11/03/2020 1437
72103
1
(Soil pH meas) 9045D
1 10/30/2020 2245 AAB
71845
1 351.4
(TKN) 351.2
5 11/04/2020 1625 DMA
11/04/2020 1010
72204
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
21.6
%
1
Ammonia - N (gas diffusion)
350.1
5.4
4.6
2.4
mg/kg
3
Nitrate - N (soluble)
9056A
5.5
2.3
0.46
mg/kg
1
Nitrite - N (soluble)
9056A
0.53 J
0.93
0.46
mg/kg
1
Phosphorus
7723-14-0 365.1
13000
2300
460
mg/kg
1
Soil pH measured in water @
19 ° C
9045D
6.7
su
1
TKN
351.2
40000
580
580
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
10 11/06/20200851 JAB2
11/06/20200647
72362
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
3.4
0.82
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 11/02/2020 1818 KSH2
11/02/2020 0604
71881
2 3050B
601OD
2 11/03/2020 0913 JMH
11/02/2020 0604
71881
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
31000
60
22
mg/kg
2
Arsenic
7440-38-2 6010D
4.9
1.1
0.37
mg/kg
1
Cadmium
7440-43-9 6010D
1.2
0.37
0.094
mg/kg
1
Calcium
7440-70-2 6010D
13000
370
47
mg/kg
1
Chromium
7440-47-3 6010D
38
0.74
0.19
mg/kg
1
Copper
7440-50-8 6010D
590
1.5
0.67
mg/kg
2
Iron
7439-89-6 6010D
23000
15
6.8
mg/kg
2
Lead
7439-92-1 6010D
50
1.5
0.67
mg/kg
2
Magnesium
7439-95-4 6010D
2600
370
47
mg/kg
1
Manganese
7439-96-5 6010D
920
2.2
0.88
mg/kg
2
Molybdenum
7439-98-7 6010D
6.6
3.0
0.74
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VJ30035-001
Description: ROXBORRO N+M Matrix: Solid
Date Sampled:10/29/2020 0845 % Solids: 21.6 10/31/2020 0003
Date Received:10/30/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 11/02/2020 1818 KSH2
11/02/2020 0604 71881
2 3050B
6010D 2 11/03/2020 0913 JMH
11/02/2020 0604 71881
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
16 3.0
0.78
mg/kg
1
Potassium
7440-09-7 6010D
2600 370
47
mg/kg
1
Selenium
7782-49-2 6010D
8.2 1.5
0.60
mg/kg
1
Sodium
7440-23-5 6010D
730 370
47
mg/kg
1
Zinc
7440-66-6 6010D
1100 7.4
1.9
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
E
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Rix. ipt Checklist (SRC) (MEOOIK-115) RevSsed_9{2 AW0
�d 4lkily7+1,7� Isstj':rig Authority, Pace EN-V - IJVWL Pale 1 of a
Sample Receipt Chechlist (SRO
Client: SYNACRO L'aalerinspgctedbyldatc fps€: l lCO-0;2% Lark V,300
1'/�{'yi'TIR of rccaciiri= Pauae ClienC i,PS—, Fied (}Iher_
Y ,F T O 1, Were custody son Is ptxsont on the cooler
JNA2, if cuslodv seals were sera, were they hitact znd unbralkcn?
Yes T:n I LW
li Strip ID: ^ — Chlorine Strip IL]: �'A Tesled by, "!'
rigitial tumpmtvro upon pme€pt 1 Derived (Corrected) teraperattu%c upon receipt °'o lid Snap -Cup ID, 2a_t&SS
3.9 13.9 'C FA l "A nC NA INA + C TEA I kA aC
Method: OTemperaturr Blank LZ] Sgnins4 Br,,t:lc%L 1R Gull, ID: 5 IR Cant Correction Factor a AC,
L%i athod of cooJsnt: ❑J Well: kG ❑ 11o0 Pr r€:s ❑ lee ❑ None
❑ r es
[4] hla
❑
I lif ae,trpe_ ature of any cooler exceeded C,.O'C, was Ptojtct Maria l�foritied?
PM was Notiftod bv, phone 1 email i (circle one).
•I, 15 fne crtmmercial courier's pac:-cing slip attached wtliis fa: n?
5, Wire pamper =1edy pnxcdures (relin uislieNreceived) followed?
F Yes
No
3d.A
n Yes
Lj No
RI Yes
L No
{r_ %Vfre sarrkple lr-x linrBdl cut the C'CK7
Yes
! No
7- V.r= hamplc ID& listed rm all sample caantainers7
8, Ww cal]eetAari date & tirne listed an the CQC" �-
,I Ycs
Ljt No
0 Y
NQ
9, )Vjq co€leclinn date & Brine Fish on all sample containers k
2 Yes
NO
11), Vid id] rwata4wT Abol infprmaEnn (1D, &Ae, time) agrft %Vkh the Coo?
Vt%
i
_Lj Nu
n Nv
" -
11, V4Wctc teats to bo purfouiw%) listed Pn the COC?
12. Did all samples hrrive ilt the proper elx�#2iner5 far each lrst andlrr _n Grand canditior:
(unb cck,en: lids on. et:.)'? -
_
13. Was ade uato s3mplo volume avarrbU10
-Icy
Na
J Yes
No
14. Arere all smpder, ri ceivod i0h in ? 3 turf bnlrli ng I ime im 4fi lrcrurs, whir 1CW1- cuu Ie"e iust„
' e
i No
13, 1�'crc aft} sat opts aontainors missing+cxces� (ciroie o�1cl samples TJ�t listed on ('OC'�
# Yes
❑ No
] A
16. iror VOA and ] 1C-t" 5 mrrkp3es, wmrebp'ohleq present>wpea-size" (/-0'o-6-nm iLl diarn=r)
In any of the VOA vials? -
Yrs
'CS
No
❑ ido
f T�IA
�€4ri
3 7- W ail DROlrnetalYnut,-ient samples received at a pH of <7.�'
1 S. ',A'= ell cyanide aamples recei-ved at a pH > 12 and sulfide sampi45 rccoivcd a: a PH > V _
Yes
❑ No
❑d NA
19. Were all applicable N H�r'I`KtNticvarl HcVpbcMOM5. I 1608-a (-! O.S_r lglL) Na311I31eb Ftee at
rztiichral chlorine?
20. Were client remarke+requeVA (U., re.gucsrcd dilutions, NISJ 0.SD EcKgrwUnts, rlo,,,)
Oly"'.rly Ir�nsnri�.3M firnm the MC: into tie �mmment secttion in LlN437
�H-
DMA
21. R' ra the utwtC aU,tibCr listed on the comainer Iarel? €t�yes, CSttotc g
S,,9mple
PMe.jVfltiivn (ML3Stbr, :orrnplelerl fr,rmmy earnple(s) inccerectly pmsm-%rd or with hca6paoc.)
ple(s) ` were reu;iw 6ii;icxrTml y l,utsetved and were adLtLstod acoord inZly
in sample receiving with N* mL a= circle one, H2SO4, HNO3,1491, NY -OH usia,!� SR 8 NA
Timo of p=wvatipn NA If rare than one .jresveyative is in the opmmenrs below.
Samples) rrl — - ! were received with bubbles>6 mrn in diameter.
emit'] es(s) NA wffcTeceiivtl wi l:L TI C: > P, ;5 mgjL (if Pr I9 h nv) Alld wcm
djusted We 2Qrdut:l}' in Semple receiving with sodium #laiasulfatfi {T las C};) x ith Shealy ID, VA
IS R bancDde labels applied by. Kns Date -
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME: ROXBORO, NC WQ PERMIT #: WQ0021826 FIELD#: NC-PS-00024-0-0001- ACRES UTILIZED: 23.3
LAND OWNER: RONALD CARVER ANNUAL DRY TONS APPLIED: 97.06 SITE #: NC PS 00024 ACRES PERMITTED: 23.3
OPERATOR: RONALD CARVER PREDOMINANT SOIL SERIES: GEORGEVILLE CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 152 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(lbs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
7/27/2020
162.00 (Y)
19,400
1.136
ROAEDC
DRY
"0-<1J2"
SUR
0.5
0.30
56,200.00
1,870.00
63.40
39.144
FSH
7/28/2020
324.00(Y)
19.400
2.272
ROAEDC
DRY
"0-<1/2"
SUR
0.5
0.30
56,200.00
1,870.00
63.40
78,288
FSH
7/29/2020
108.00, (Y)
19.400
0.757
ROAEDC
DRY
"0-<1/2"
SUR
0.5
0.30
56,200.00
1,870.00
63.40
26.096
I
FSH i
9
Jul-20
594.00 (Y)
li
Total
4.165
Total
143.528 0.000
AS
CD
CU
CR�0.27�0�
HG
MO�NSAnnual
!bs/acre Applied
0.031
0.006
3.1410.221.003
0.052
6.440
160.787
Date Lbs1Ac
6,445 1 0.164 i 1.136 j 6,091 N 0,854
Permit PAN Limit (ibs/acre) 1st Crop "-
Federal C P L R (lbs/acre)**** 36.6 34.8 1,339.0 1 67.9 15.D 375.0 89.0 2,500.0
ROAEDC = ROXBORO, NC WWTP AEROB, DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0,3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 211/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: ROXBORO, NC W Q PERMIT #: W 00021826 FIELD#: NC-PS-00024-0-0002- ACRES UTILIZED: 4.4
LAND OWNER: RONALD CARVER ANNUAL DRY TONS APPLIED: 20.59 SITE #: NC PS 00024 ACRES PERMITTED: 4.4
OPERATOR: RONALD CARVER PREDOMINANT SOIL SERIES: GEORGEVILLE CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 168 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Site
I
Name of Crop Type
Gallons (G)
I
8
or Cubic Yards (Y)
Cond.
Precip
Volati-
I Mineral-
�
Ammonia
Nitrate
PAN Applied
Receiving Residual
d
a
Date or,
or Wet Tons (W )
°fo
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application k
Month
Amount UOM
Solids Dry Tons/Ac
Source
Moist
Inches
Method*
Rate'"`
Rate—
mg/kg
mg/kg
mgtkg
Crop 1 Crop 2
Crop 1 Crop 2
7/29/2020
126.00 (Y}
19.400 4.679
ROAEDC
DRY
"0-<1/2"
SUR
0.5
0.30
56,200.00
1,870.00
63.40
161.222
FSH
i
Jut-20
126.001 (Y)
Total 4.679
Total
161.222 0.000
HG
MO
Ibs/acre Applied
�AS�O007
�3.52�8
�CR�PB
0.004
0.058
�Nl
8
�SEual
7.234
180.608
Date Lbs/Ac
0.168 1 47.119 1 7.077
0.530
Permit PAN Limit (Ibs/acre) 1st Crop
Federal C P L R (lbs/acre)**** 36.6 34.8 1 339.0 267.9 15.0 1 375.0 1 89.0 2,500.0
ROAEDC = ROXBORO, NC W WTP AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pertAties for submittin false information, including the possibility of fines and impriso ent for knowing violations."
`? , ..�,
SIGNATURE OF LAND APPLIER tDATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation ***" C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: ROXBORO, NC WQ PERMIT M WQ0021826 FIELD#: NC-PS-00024-0-0003- ACRES UTILIZED:4.3
LANDOWNER: RONALD CARVER ANNUAL DRY TONS APPLIED: 20.59 SITE #: NC PS 00024 ACRES PERMITTED: 4.3
OPERATOR: RONALD CARVER PREDOMINANT SOIL SERIES: GEORGEVILLE CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 173 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
i
i
I
Name of Crop Type
or Cubic Yards m
Cond.
� Precip
Volati-
Mineral- 5
Ammonia
� Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
% Residual
Dry, Wet,
Past 24 Hrs.
Application
iization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids Dry Tons/Ac
Source
i Moist
Inches
Method*
Rate**
ri Rate -
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1 Crop 2
7/30/2020
126.00 (Y)
19AOO 4.788 � ROAEDC
DRY
"0-<1/2"
SUR
0.5
I 0.30
56,200.00
1,870.00
63.40
164.972
FSH
i
Jul-20
126.00 (Y)
k
Total 4.788
Total
164.972 0.000
AS GD
CU
CR
PB
MO
NI
�SE
ual Ibsiacre Applied
0.036 0.007
3.610
0.254
0.310
�HG
0.060
0.145
7.402
184.809
Date LbslAc
(Ibs/acre) 1st
Federal
0.167
1,339.0
0.110
0.500
2,500.0
i
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and impns nme t for knowing violations."
)0,�
�J
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: ROXBORO, NC WQ PERMIT M WQ0021826 FIELDM NC-PS-00025-0-0001-A ACRES UTILIZED: 20.2
LANDOWNER: PAUL BAILEY ANNUAL DRY TONS APPLIED: 92.41 SITE #: NC PS 00025 ACRES PERMITTED: 20.2
OPERATOR: PAUL BAILEY PREDOMINANT SOIL SERIES: GEORGEVILLE CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 211 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite (lbs/acre) Application
_Tr`op2 ­Er—opl
Month
Amount UOM
Solids Dry Tons/Ac
Source
Moist
Inches
Method*
Rate—
Rate—
mg/kg
mg/kg
mg/kg
5r—opi Crop 2
8/11/2020
250.00 (Y)
23.100 2.408
ROAEDC
DRY
110­0/2.
SUR
0.5
0.30
42,000.00
8,400.00
4.50
68.790 FSH
8/12/2020
225.00 (Y)
21100 2.167
ROAEDC 11
DRY
.10-1/2"
SUR
0.5
0.30
42,000.00
8,400.00
4.50
61.911 FSH
Aug-20
475.00 (Y)
i
Total 4,575
Total
130.701 0.000
S
SE
ZN
P
Lime Applied
Annual
�An a lbs)ameAppiled _al lb./a.,. Applied
0. 037
0.061
PAN
st
1.684
11.587 1 7.410
7.587
il
Federal C.P.L.R. (lbs/acre)**** 36,6 1 34.8 1 1,339.6-T 267,9 1 I&D 1 1 375.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
47
Co Vf4 1 �i 1-_7j
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0. 1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 211/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: ROXBORO, NG
WQ PERMIT #: WQ0021826 FIELD#: NC-PS-00025-0-0002-
LAND OWNER: PAUL BAILEY
ANNUAL DRY TONS APPLIED: 19.46 SITE #: NC PS 00025
OPERATOR: PAUL BAILEY
PREDOMINANT SOIL SERIES: GEORGEVILLE
CROP 1 NAME: FESCUE HAY (FSH)
CROP 1 MAX. PAN: 211 CROP 2 NAME:
RESIDUAL SOURCE(S): * See list at bottom of report
Page: 1
ACRES UTILIZED: 7.3
ACRES PERMITTED: 7.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
Date or or Wet Tons (W)
% Residual Dry, Wet,
Past 24 His.
Application lization
ization TKN
Nitrogen
and Nitrite
Month Amount UOM
Solids Dry Tons/Ac Source Moist
Inches
Method* Rate**
Rate— mg/kg
mg/kg
mg/kg
./12/2020 100.001
----2.665
23.100 kOAEDC
SUR 0.5
0.30 1 42,060.00
81406-00
4.50
lbs/acre Applied
Total 2.665
AS CD CU i CR PB
.007 2.50 7_0
0.021 0 5 .160 0.203
------ -T 6.665 0.122 1 36.389—F 5.653 3.067
MO
-6-02-2
3.394
M21
Name of Crop Type
PAN Applied
Receiving Residual
(lbs/acre)
Application
Crop 1 Crop 2
Crop 1 Crop 2
T6_140
FSH
Total 76.140 0.000
Lime
�
1 I I
Federal C.P.L.R. (lbs/acre)**** 36.6 1 34. 1,339.0 267.9 1, n 375.0
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
"I certify; under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
CZP,!%~ 21mILI
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0. 1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2tl/2021 DENR FORM FSF (12/2006)

SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
May 06, 2020
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Roxboro
Dear Ryan Copeland:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 20041282
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/24/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
,..
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 31

mm' y Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20041282
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 5/6/2020
CLIENT: Synagro
Project: Roxboro
WorkOrder Narrative:
20041282: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20041282-OOIA TCLP-SVOC_8270E: Surrogate outside recovery limits. Minimum method criterion of
one surrogate within established recovery limits was met.
Analytical Sequence QC Notes:
CCV 40ppm 36593 SVOC-MSTR S(8270): Surrogate outside recovery limits. Minimum method
criterion of one surrogate within established recovery limits was met.
PEST ccv 250PPB SVOC-CPEST_NPW(8081): Ending CCV exhibits outlying recoveries for several
analytes. Matrix influence possibly affected instrument calibration. Sample is ND
Original
Page 2 of 31

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 20041282
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 5/6/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL TECHNp4,1 ULES,1NC. Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Roxboro
Lab SamplelD Client Sample ID
20041282-001 Roxboro WWTP
Tag No Date Collected
4/23/2020 9:40:00 AM
Workorder
Sample Summary
WO#: 20041282
06-May-20
Date Received Matrix
4/24/2020 10:10:00 AM Sludge
Page 4 of 31

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES R PORT
ENVIRONMENTALTECHN❑L0G1ES,11+1C
Cuyahoga Falls, Ohio44223
WO#: 20041282
ArWyft cal taboralonag
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
06 May-20
Client:
Synagro
Project:
Roxboro
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
20041282-OOIA Roxboro WWTP 4/23/2020 9:40:00 AM Sludge Ignitability of Solids (SW-846: 1030)
5/1/2020 3:00:00 PM
Paint Filter Free Liquids Test (SW-846
4/29/2020 8:30:00 AM
pH (SW9045D)
4/30/2020 10:08:00 AM
Reactive Cyanide (9014/7.3.3.2)-Solid
4/27/2020 9:09:00 AM
Reactive Sulfide (9034)/7.3.4.2
4/27/2020 9:09:00 AM
TCLP Herbicides by EPA 8321B
4/29/2020 2:00:00 PM 5/2/2020 7:29:00 AM
TCLP Mercury Analysis (SW1311/7474/29/2020 2:00:00 PM
5/1/2020 9:55:00 AM 5/1/2020 1:10:00 PM
TCLP Metals Analysis (SW1311/6010:4/29/2020 2:00:00 PM
4/30/2020 9:40:00 AM 5/1/2020 2:51:39 PM
TCLP Metals Analysis (SW1311/6010:4/29/2020 2:00:00 PM
5/1/2020 1:35:46 PM
TCLP Pesticides Analysis (SW1311/8(4/29/2020 2:00:00 PM
4/30/2020 1:00:00 PM 5/4/2020 7:52:00 PM
TCLP Semi-Volatiles Analysis 4/29/2020 2:00:00 PM
4/30/2020 1:00:00 PM 5/4/2020 4:12:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
4/29/2020 2:00:00 PM 4/30/2020 1:40:00 PM
Original
Page 5 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20041282
Date Reported: 5/6/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/23/2020 9:40:00 AM
Lab ID: 20041282-OOIA
Project: Roxboro
Client Sample ID Roxboro WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: MJM
1 5/1/2020 1:10:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
5/1/2020 1:35:46 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
5/1/2020 1:35:46 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
5/1/2020 1:35:46 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
5/1/2020 1:35:46 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
5/1/2020 1:35:46 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
5/1/2020 1:35:46 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
5/1/2020 2:51:39 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2
5/4/2020 4:12:00 PM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
5/4/2020 4:12:00 PM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2
5/4/2020 4:12:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
5/4/2020 4:12:00 PM
Cresols, Total
ND
10.0
mg/L
2
5/4/2020 4:12:00 PM
Hexachloro-1,3-butadiene
ND
0.0400
mg/L
2
5/4/2020 4:12:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
5/4/2020 4:12:00 PM
Hexachloroethane
ND
0.200
mg/L
2
5/4/2020 4:12:00 PM
Nitrobenzene
ND
0.200
mg/L
2
5/4/2020 4:12:00 PM
Pentachlorophenol
ND
0.500
mg/L
2
5/4/2020 4:12:00 PM
Pyridine
ND
0.500
mg/L
2
5/4/2020 4:12:00 PM
Surr: 2-Fluorophenol
90.2
10 - 109
%Rec
2
5/4/2020 4:12:00 PM
Surr: Phenol-d6
90.0
10 - 109
%Rec
2
5/4/2020 4:12:00 PM
Surr: Nitrobenzene-d5
74.5
19 - 120
%Rec
2
5/4/2020 4:12:00 PM
Surr: 2,4,6-Tribromophenol
124
10 - 120
S %Rec
2
5/4/2020 4:12:00 PM
Surr: 2-Fluorobiphenyl
85.4
22 - 117
%Rec
2
5/4/2020 4:12:00 PM
Surr: p-Terphenyl-d14
125
34 - 116
S %Rec
2
5/4/2020 4:12:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation
exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 6 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20041282
Date Reported: 5/6/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/23/2020 9:40:00 AM
Lab ID: 20041282-OOIA
Project: Roxboro
Client Sample ID Roxboro WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
19.5
Surr: DCB
20.8
TCLP HERBICIDES BY EPA 8321B
SW8081 SW351OC Analyst: MES
0.125
mg/L
5
5/4/2020 7:52:00 PM
0.250
mg/L
5
5/4/2020 7:52:00 PM
0.0125
mg/L
5
5/4/2020 7:52:00 PM
0.0125
mg/L
5
5/4/2020 7:52:00 PM
0.0125
mg/L
5
5/4/2020 7:52:00 PM
0.0125
mg/L
5
5/4/2020 7:52:00 PM
0.0125
d mg/L
5
5/4/2020 7:52:00 PM
10 - 119
%Rec
5
5/4/2020 7:52:00 PM
10 - 119
%Rec
5
5/4/2020 7:52:00 PM
SW8321A SW1311M Analyst: BJH
2,4-D
ND
0.500
mg/L
50 5/2/2020 7:29:00 AM
2,4,5-TP
ND
0.500
mg/L
50 5/2/2020 7:29:00 AM
Surr: 2,4-Dichlorophenylacetic aci
106
70 - 130
%Rec
50 5/2/2020 7:29:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: RMT
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
MEK
ND
5.00
mg/L
50 4/30/2020 1:40:00 PM
Benzene
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
Chlorobenzene
ND
2.50
mg/L
50 4/30/2020 1:40:00 PM
Chloroform
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
Tetrachloroethene
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
Trichloroethene
ND
0.250
mg/L
50 4/30/2020 1:40:00 PM
Vinyl chloride
ND
0.100
mg/L
50 4/30/2020 1:40:00 PM
Surr: 4-Bromofluorobenzene
90.3
70 - 130
%Rec
50 4/30/2020 1:40:00 PM
Surr: Di brom ofl uorom ethane
102
70 - 130
%Rec
50 4/30/2020 1:40:00 PM
Surr: Toluene-d8
99.9
70 - 130
%Rec
50 4/30/2020 1:40:00 PM
Qualifiers: B Analyte detected in the associated
Method Blank
E Value above quantitation
range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 7 of 31

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone] WO#: 20041282
Website: http://www.settek.com Date Reported: 5/6/2020
CLIENT: Synagro
Matrix: SLUDGE
Lab ID: 20041282-OOIA
Project: Roxboro
Client Sample ID Roxboro WWTP
Tag Number:
Collection Date:
4/23/2020 9:40:00 AM
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCISOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495 mg/Kg
1
4/27/2020 9:09:00 AM
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095)
SW9095
Analyst: DHC
Free Liquid
pass
1
4/29/2020 8:30:00 AM
RCISOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
mm/sec
1
5/1/2020 3:00:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH
7.5
s.u.@20.7C
1
4/30/2020 10:08:00 AM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
4/27/2020 9:09:00 AM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 8 of 31

Summit Environmental Technologies, Inc.
Accreditation
Program
fr
3310 Win St.
SUMMIEF
Anal�7n tes Report
ENOROMMEWAL IrECHNOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20041282
Wehsite: http://www.settek.com
06 May-20
Client: Synagro
State: NW
Project: Roxboro
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20041282-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Paint Filter Free Liquids Test (SW-846: 9095)
Free Liquid
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
N
Sludge
Reactive Sulfide (9034Y7.3.4.2
Sulfide, Reactive
N
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Key
Key
NC WW SCM A Accredited
NC WW SCM N Not Accredited
Original #1
Page 9 of 31

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Anal�7n tes Report
ENVIROMMEWAL IrECHHOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
20041282
Wehsite: http://www.settek.com
06 May-20
Client: Synagro
State: NW
Project: Roxboro
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20041282-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original #1
Page 10 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43209
WO#: 20041282
06-May-20
Sample ID: MB-43209
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 4/29/2020
RunNo: 112431
lient ID: PBS
Batch ID: 43209
TestNo: SW8260 SW1311M
Analysis Date: 4/30/2020
SegNo: 2758003
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
M-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.100
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
48.6
Surr: Dibromofluoromethane
50.1
Surr: Toluene-d8
50.2
50.00 97.2 70 130
50.00 100 70 130
50.00 100 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 11 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: 43214
TCLP Silver(Ag) ND 0.500
TCLP Silver(Ag) 2.07 0.500 2.000 0 104 80 120
TCLP Silver(Ag) 1.72 0.500 2.000 0.001200 86.0 70 130
Sample ID: 20041350-004AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/30/2020
RunNo: 112443
Client ID: Batch=
Batch ID: 43214
TestNo: SW6010D SW3010A
Analysis Date: 5/1/2020
SegNo: 2759929
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Silver(Ag) 1.73 0.500
2.000 0.001200 86.2 70
130
1.722 0.232 20
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 12 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43214
WO#: 20041282
06-May-20
Sample ID: 20041350-004AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/30/2020
RunNo: 112443
Dient ID: Batch=
Batch ID: 43214
TestNo: SW6010D SW3010A
Analysis Date: 5/1/2020
SegNo: 2759929
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43218
WO#: 20041282
06-May-20
Sample ID: MB-43218
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
lient ID: PBS
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2758485
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.783
Surr: Phenol-d6
0.756
Surr: Nitrobenzene-d5
0.678
Surr: 2,4,6-Tribromophenol
1.07
Surr: 2-Fluorobiphenyl
0.779
Surr: p-Terphenyl-d14
1.13
1.000
78.3
10
109
1.000
75.6
10
109
1.000
67.8
19
120
1.000
107
10
120
1.000
77.9
22
117
1.000
113
34
116
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43218
WO#: 20041282
06-May-20
Sample ID: LCS-43218
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
Dient ID: LCSS
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2758486
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.426
0.100
0.8000
0
53.2
36.4
130
2,4,5-Trichlorophenol
0.809
0.250
0.8000
0
101
31.7
132
2,4,6-Trichlorophenol
0.796
0.250
0.8000
0
99.4
31.1
133
2,4-Dinitrotoluene
0.818
0.0500
0.8000
0
102
43.3
130
o-Cresol
0.637
0.250
0.8000
0
79.6
32.9
130
Cresols, Total
ND
5.00
1.600
0
79.8
31.7
130
Hexachloro-1,3-butadiene
0.427
0.0200
0.8000
0
53.4
31.4
130
Hexachlorobenzene
0.769
0.0500
0.8000
0
96.2
43.1
130
Hexachloroethane
0.393
0.100
0.8000
0
49.1
36.5
130
Nitrobenzene
0.584
0.100
0.8000
0
73.0
39.5
130
Pentachlorophenol
0.834
0.250
0.8000
0
104
34
130
Pyridine
0.428
0.250
0.8000
0
53.6
10
130
Surr: 2-Fluorophenol
0.851
1.000
85.1
17.1
130
Surr: Phenol-d6
0.836
1.000
83.6
10
130
Surr: Nitrobenzene-d5
0.686
1.000
68.6
32.6
130
Surr:2,4,6-Tribromophenol
1.20
1.000
120
4.43
130
Surr:2-Fluorobiphenyl
0.813
1.000
81.3
41.8
130
Surr: p-Terphenyl-d14
1.18
1.000
118
36.4
130
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43218
WO#: 20041282
06-May-20
Sample ID: 20041350-002AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
lient ID: BatchQC
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2760532
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.558
0.200
0.8000
0
69.7
33.8
126
2,4,5-Trichlorophenol
0.900
0.500
0.8000
0
113
28.7
144
2,4,6-Trichlorophenol
0.921
0.500
0.8000
0
115
12.8
153 mQC+
2,4-Dinitrotoluene
0.914
0.100
0.8000
0
114
20.4
155
o-Cresol
0.755
0.500
0.8000
0
94.4
10
148
Cresols, Total
ND
10.0
1.600
0
93.0
10
148
Hexachloro-1,3-butadiene
0.528
0.0400
0.8000
0
66.0
29
126
Hexachlorobenzene
0.913
0.100
0.8000
0
114
33.7
134
Hexachloroethane
0.540
0.200
0.8000
0
67.5
32.8
132
Nitrobenzene
0.676
0.200
0.8000
0
84.6
20
158
Pentachlorophenol
0.871
0.500
0.8000
0
109
10
176
Pyridine
ND
0.500
0.8000
0
61.8
10
130
Surr:2-Fluorophenol
0.930
1.000
93.0
3.39
130
Surr: Phenol-d6
0.946
1.000
94.6
5
130
Surr: Nitrobenzene-d5
0.797
1.000
79.7
14.5
154
Surr: 2,4,6-Tribromophenol
1.34
1.000
134
19.5
130 S
Surr:2-Fluorobiphenyl
0.938
1.000
93.8
34.4
130
Surr: p-Terphenyl-d14
1.28
1.000
128
8.86
156
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro BatchID: 43218
WO#: 20041282
06-May-20
Sample ID: 20041350-002AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
Dient ID: Batch=
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2760533
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.476
0.200
0.8000
0
59.4
33.8
126
0.5576
15.9
30
2,4,5-Trichlorophenol
0.807
0.500
0.8000
0
101
28.7
144
0.9004
11.0
30
2,4,6-Trichlorophenol
0.799
0.500
0.8000
0
99.9
12.8
153
0.9208
14.1
30 mQC+
2,4-Dinitrotoluene
0.855
0.100
0.8000
0
107
20.4
155
0.9140
6.65
30
o-Cresol
0.672
0.500
0.8000
0
84.0
10
148
0.7548
11.6
30
Cresols, Total
ND
10.0
1.600
0
83.0
10
148
0
0
30
Hexachloro-1,3-butadiene
0.492
0.0400
0.8000
0
61.5
29
126
0.5280
7.06
30
Hexachlorobenzene
0.834
0.100
0.8000
0
104
33.7
134
0.9128
8.97
30
Hexachloroethane
0.478
0.200
0.8000
0
59.8
32.8
132
0.5400
12.1
30
Nitrobenzene
0.644
0.200
0.8000
0
80.6
20
158
0.6764
4.85
30
Pentachlorophenol
0.783
0.500
0.8000
0
97.9
10
176
0.8708
10.6
30
Pyridine
ND
0.500
0.8000
0
48.0
10
130
0
0
30 m
Surr: 2-Fluorophenol
0.871
1.000
87.1
3.39
130
0
Surr: Phenol-d6
0.881
1.000
88.1
10
130
0
Surr: Nitrobenzene-d5
0.742
1.000
74.2
14.5
154
0
Surr: 2,4,6-Tribromophenol
1.25
1.000
125
19.5
130
0
Surr:2-Fluorobiphenyl
0.846
1.000
84.6
34.4
130
0
Surr: p-Terphenyl-d14
1.18
1.000
118
8.86
156
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: 43232
TCLP Mercury ND 0.00200
TCLP Mercury 0.00396 0.00200 0.00400 0 99.0 80 120
TCLP Mercury ND 0.00200
Sample ID: 20041350-004AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: Batch=
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2758994
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00514 0.00200
0.00400 0 128 75
125
S
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 18 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: 43232
TCLP Mercury 0.00515 0.00200 0.00400 0 129 75 125 0.00514 0.194 20 S
TCLP Mercury ND 0.00200
Sample ID: TCLP BLANK 2 5-1-
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: PBS
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2759005
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 19 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20041282
06-May-20
Client: Synagro
Project: Roxboro BatchID: 43232
Sample ID: M1132-43232
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: PBS
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2759012
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 31

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG Lggir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
QC SUMMARY REPORT
WO#: 20041282
06-May-20
Client: Synagro
Project: Roxboro BatchID: R112310
Sample ID: 20041280-001ADUP
SampType: DUP
TestCode: FreeLiquid_S Units:
Prep Date:
RunNo: 112310
lient ID: BatchQC
Batch ID: R112310
TestNo: SW9095
Analysis Date: 4/29/2020
SegNo: 2753993
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Free Liquid
pass
0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: R112323
Cyanide, Reactive ND 0.485
Cyanide, Reactive 9.44 0.495 10.00 0 94.4 85 115
Cyanide, Reactive ND 0.500 0.5000 0 81.0 65 135
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754434
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
8.98 0.485
10.00 0 89.8 75
125
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 22 of 31

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20041282
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com 06-May-20
Client: Synagro
Project: Roxboro BatchID: R112323
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754434
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20041299-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754435
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.35 0.490 10.00 0 93.5 75 125 8.984 3.97 10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 23 of 31

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20041282
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com 06-May-20
Client: Synagro
Project: Roxboro BatchID: R112336
Sample ID: MB-R112336
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 112336
Client ID: PBS
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755023
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R112336
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 112336
Client ID: LCSS
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755024
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
3120 25.0 3280 0 95.1 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 24 of 31

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20041282
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com 06-May-20
Client: Synagro
Project: Roxboro BatchID: R112336
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 112336
Client ID: Batch=
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755029
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3080 25.0 3280 0 93.9 75 125
Sample ID: 20041299-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 112336
Client ID: Batch=
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755030
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3180 25.0 3280 0 97.0 75 125 3080 3.19 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 25 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: R112377
pH 7.0 7.0 0 99.6 98.6 101.4
pH 7.8 7.8 0.4 5
Sample ID: PH 7 CHECK
SampType: LCS
TestCode: PH_DW(4500- Units: s.u.@21.9C
Prep Date:
RunNo: 112377
Client ID: LCSW
Batch ID: R112377
TestNo: SW9045D
Analysis Date: 4/30/2020
SegNo: 2756616
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 26 of 31

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 20041282
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http:llh settek.com 06-May-20
Client: Synagro
Project: Roxboro BatchID: R112438
Sample ID: RLC
SampType: RLC
TestCode: Mtl-ICP_NPW Units: mg/L
Prep Date:
RunNo: 112438
Client ID: Batch=
Batch ID: R112438
TestNo: SW6010D
Analysis Date: 5/1/2020
SegNo: 2758335
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
0.0207
0.0200
0.01600
0
129
70
130
TCLP
Barium(Ba)
ND
0.0200
0.02000
0
98.9
70
130
TCLP
Cadmium(Cd)
ND
0.00500
0.004000
0
99.1
70
130
TCLP
Chromium(Cr)
ND
0.0200
0.01600
0
102
70
130
TCLP
Lead(Pb)
0.0425
0.0150
0.04000
0
106
70
130
Sample ID: RLC 2
SampType: RLC
TestCode: Mtl-ICP_NPW Units: mg/L
Prep Date:
RunNo: 112438
Client ID: Batch=
Batch ID: R112438
TestNo: SW6010D
Analysis Date: 5/1/2020
SegNo: 2758336
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Selenium(Se)
0.0388 0.0250 0.04000 0 97.0 70 130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 27 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL I ECHNO LQgir,_3, INC
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX. [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: R112457
Ignitability 7.96 7.240 0 110 70 130
Ignitability non-flammable 0 0 20
Ignitability >2.2 0 0 20
Sample ID: 20041479-005ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 112457
Client ID: Batch=
Batch ID: R112457
TestNo: SW1030
Analysis Date: 5/1/2020
SegNo: 2759310
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability >2.2 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 31

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL I ECHNO Lggir,_3, INC
Cuyahoga Falls, Ohio 44223
WO#: 20041282
Arrafyt�cal iaboralorfas
TEL: [phone] FAX. [phone]
Website: http:llh settek.com
06-May-20
Client:
Synagro
Project:
Roxboro
BatchID: R112457
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Sample ID: 20041282-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 112457
Client ID: Roxboro WWTP
Batch ID: R112457
TestNo: SW1030
Analysis Date: 5/1/2020
SegNo: 2759316
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 31

DBPix Evaluation
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www.ammara.com

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 20041282 RcptNo: 1
Logged by: Jacqueline Rasile 4/24/2020 10:10:00 AM
Completed By: Jacqueline Rasile 4/24/2020 2:37:02 PM
Reviewed By: Sara E. Kidd 4/24/2020 3:59:47 PMlLA
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes d❑ No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes V No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
V
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
V
No
❑
10. Was preservative added to bottles?
Yes
❑
No
V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
V
13. Does paperwork match bottle labels?
Yes
V
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No
❑
15. Is it clear what analyses were requested?
Yes
0
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
11.4
Goodl
Not Present
Page 31 of 31

SECTION 5

1
Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number: NC 0021024
Monitoring Period: From 01/01/2020 To 3/31/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic _
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization _ Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlioahle to alternative nerformed (Class A or Class Bl complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Gen. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 61s
CFU
34826
42307
54726
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 6`'
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
(VS reduction)
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3 Option/Alt. 4
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying - Stable) (Drying - Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement rn 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties or false
certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer Name and Title Land Applier Name and Title (if applicable) (type or print)
/� 0., 2- (1.-2—Z
Signature of Prepare--er4 Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

FECAL DATA SHEET
Lab result
Log
39801
4.60
Min 34826
38095
4.58
Max 54726
47009
4.67
Geometric Mean 42307
34,826
4.54
54726
4.74
49751
4.70
35897
4.56
Average
4.63

Contact: Ryan Copeland
Report Date:
Page 1
2/4/2020
Client: Synagro
284 Boger Road
Project:
Roxboro
Mocksville, NC 27028
Date Sample Rcvd:
1/23/2020
Meritech Work Order #
01232061 Sample: Roxboro 1 Grab
1/23/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
20.1 % 1/24/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
39,801 col/g dry wt 1/23/20
494 col/g dry wt
SM 9222D
Meritech Work Order #
01232062 Sample: Roxboro 2 Grab
1/23/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
21.0 %
1/24/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
38,095 col/g dry wt
1/23/20
494 col/g dry wt
SM 9222D
Meritech Work Order #
01232063 Sample: Roxboro 3 Grab
1/23/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
23.4 %
1/24/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
47,009 col/g dry wt
1/23/20
494 col/g dry wt
SM 9222D
Meritech Work Order #
01232064 Sample: Roxboro 4 Grab
1/23/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
20.1 %
1/24/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
34,826 col/g dry wt
1/23/20
494 col/g dry wt
SM 9222D
Meritech Work Order #
01232065 Sample: Roxboro 5 Grab
1/23/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
20.1 %
1/24/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
54,726 col/g dry wt
1/23/20
494 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
= Laboratory Certification No. 165
k
Page 2
Contact: Ryan Copeland Report Date: 2/4/2020
Client: Synagro
284 Boger Road Project: Roxboro
Mocksville, NC 27028 Date Sample Rcvd: 1/23/2020
Meritech Work Order # 01232066 Sample: Roxboro 6 Grab
Parameters
Results
Analysis Date
Reporting Limit
% Total Solids
20.1 %
1/24/20
0-100 %
Fecal Coliform (Sludge)
49,751 col/g dry wt
1/23/20
508 col/g dry wt
Meritech Work Order #
01232067 Sample: Roxboro 7 Grab
Parameters
Results
Analysis Date
Reporting Limit
% Total Solids
20.1 %
1/24/20
0-100 %
Fecal Coliform (Sludge)
35,897 col/g dry wt
1/23/20
494 col/g dry wt
1/23/20
Method
SM 2540B
SM 9222D
1/23/20
Method
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data.
L boratoryRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9/18 Chain of Custody Record (COC)
� NPDES#:
Client: ,_J��%t1�;�"U Phone:
Address: "LA' (50- V-op Fax:
A)(.ICSJiLLr,— Email: I-C�PcU�1,n��
Project: �Vxga'o
P.O.#:
Attention: Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Char es ADDIV
Circle all that apply: moat Fax, Mail Std 10 a s) 3 5 Daxs zs
l MERITECH, INC.
�. ENVIRONMENTAL LABORATORIES
1 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.tlleritechlabS.com
Sample Location and/or ID #
Sampling Dates &Times
p g
Person Taking Sample (Sign/Print):sN
Lab Use Only
Start
EndComp?
Grab?
Cont,
Test(s) Required
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
'Li
z
G �
3
�3
C�
Temperature UVn
Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples must be done in the field prior to preservation.
Comments:
Compositor #
UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes No ❑
Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Hand Delivery
Relinquished by:
Time: i 3 '
n Date: z�
(rNn i� z3�
Received b Date: Time:
y'
Other
Relinquished by: Date: Time:
Received by: Date: Time:
by: Date: Time:b:
�ceiedRelinquished j '1 le& y 1r:

DIGESTER
"COOLER"
SLUDGE
ROXBORO WWTP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Nicki Dalton, Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
(Total)
Time
Out
Oven
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
(Volatile)
Time
In
Oven
(Volatile)
Time
Out
Oven
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
ANALYST
INITIALS
RPD's
if Needed
1/7/2020
1/7/2020
7
35
82.4119
117.8954
35.4835
8:47 AM
9:47 AM
82.4100
-.0019
Blank
10:55 AM
11:55 AM
82.4112
-.0012
Blank
NO
6:52 AM
1/6/2020
8
35
77.8695
113.0328
35.1633
8:47 AM
9:47 AM
78.1026
.2331
0.66
10:55 AM
11:55 AM
77.9487
.1539
66
NO
0%
1/6/2020
5
35
77.8273
111.6299
33.8026
8:47 AM
9:47 AM
78.0523
.2250
0.67
10:55 AM
11:55 AM
77.9031
.1492
66
NO
1/16/2020
1/16/2020
7
35
82.4122
116.6126
34.2004
8:40 AM
9:40 AM
82.4115
-.0007
Blank
10:46 AM
11:46 AM
82.4106
.0009
Blank
NO
6:40 AM
1/16/2020
8
35
77.8701
112.4748
34.6047
8:40 AM
9:40 AM
78.0681
.1980
0.57
10:46 AM
11:46 AM
77.9326
.1355
68
NO
0%
1/16/2020
5
35
77.8276
112.1471
34.3195
8:40 AM
9:40 AM
78.0268
.1992
0.58
10:46 AM
11:46 AM
77.8904
.1364
68
NO
1/21/2020
1/21/2020
7
35
82.4111
116.1397
33.7286
8:35 AM
9:35 AM
82.4101
-.0010
Blank
10:40 AM
11:40 AM
82.4101
.0000
Blank
NO
6:39 AM
1/20/2020
8
35
77.8696
111.9907
34.1211
8:35 AM
9:35 AM
78.0636
.1940
0.57
10:40 AM
11:40 AM
77.9328
.1308
67
NO
1%
1/20/2020
5
35
77.8270
112.1424
34.3154
8:35 AM
9:35 AM
78.0232
.1962
0.57
10:40 AM
11:40 AM
77.8907
.1325
68
NO
1/28/2020
1/28/2020
7
35
82.4118
116.5827
34.1709
8:32 AM
9:32 AM
82.4117
-.0001
Blank
11:00 AM
12:00 PM
82.4112
.0005
Blank
NO
6:24 AM
1/27/2020
8
35
77.8705
111.7495
33.8790
8:32 AM
9:32 AM
78.0583
.1878
0.55
11:00 AM
12:00 PM
77.9315
.1268
68
NO
1%
1/27/2020
5
35
77.8278
112.2249
34.3971
8:32 AM
9:32 AM
78.0182
.1904
0.55
11:00 AM
12:00 PM
77.8897
.1285
67
NO
2/4/2020
2/4/2020
7
35
82.4121
117.0654
34.6533
8:17 AM
9:17 AM
82.4114
-.0007
Blank
10:20 AM
11:20 AM
82.4115
-.0001
Blank
NO
6:15 AM
2/3/2020
8
35
77.8712
112.1523
34.2811
8:17 AM
9:17 AM
78.0502
.1790
0.52
10:20 AM
11:20 AM
77.93
.1202
67
NO
0%
2/3/2020
5
35
77.8282
112.4555
34.6273
8:17 AM
9:17 AM
78.0090
.1808
0.52
10:20 AM
11:20 AM
77.8875
.1215
67
NO
2/11/2020
2/11/2020
7
35
82.4123
119.2061
36.7938
8:15 AM
9:15 AM
82.4123
.0000
Blank
10:15 AM
11:15 AM
82.4114
.0009
Blank
NO
6:00 AM
1 2/10/2020
8
35
77.8712
111.8993
34.0281
8:15 AM
9:15 AM
78.0375
.1663
0.49
10:15 AM
10:15 AM
77.926
.1115
67
ND
0%
2/10/2020
5
35
77.8285
111.9812
34.1527
8:15 AM
9:15 AM
77.9963
.1678
0.49
10:15 AM
10:15 AM
77.8842
.1121
67
ND
VSR
0
x - Blank
2020 (First Quarter) VECTOR ATTRACTION CALCULATIONS

KIN11
503 VECTOR ATTRACTION
This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction
Formula
In - Out n .66 - .67 n -.010 n -0.01 n
In - (In x Out) - .66- (.66 x .67) - .66 - 44 - .22 - -.045 x
In - Out F- .66-66 .66 n .00 n .00 n
In - (In x Out) - .66- (.66 x .66) - .66 - .22 L= .44 - .000 x
In - Out n 0.61 - .63 n -.020 n -0.02 n
In - (In x Out) .61- (. 61 x .63) .61 - .38 .230 -0.09 x
In - Out n .60 - .63 n -.030 n -.03 n
In - (In x Out 60- (.60 x .63) .60 - .38 .22 -0.14 x
❑ 0 El
Reduction
100 0 -4.5 First Quarter
100 ❑ 0.0 Second Quarter
100 0 -9.0 Third Quarter
100 0 -14.0 Fourth Quarter
0
2020
2020
2020
2020

Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number: NC 0021024
Monitoring Period: From 04/01/2020 To 06/30/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Parameter
Allowable L-:—e-v1:ef in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x1A to the 61
CFU
22643
43870
120883
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 61s
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. I
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(dniection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
Preparer Name and Title Land Applier Name and Title (if applicable) (type or print)
Signature of Prepafer * Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

FECAL DATA SHEET
Lab result
Log
37190
4.57
Min
120883
5.08
Max
67511
4.83
Geometric Mean
28,926
4.46
34483
4.54
45643
4.66
22634
4.35
Average
4.64
22634
120883
43870

Page 1
Contact: Ryan Copeland
Report Date:
7/20/2020
Client: Synagro
284 Boger Road
Project:
Roxboro
Mocksville, NC 27028
Date Sample Rcvd:
7/9/2020
Meritech Work Order #
07092070 Sample: Roxboro 1 Grab
7/9/20
Parameters
Results
Analysis Date
Reporting_Limit
Method
% Total Solids
24.2 %
7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
37,190 col/g dry wt
7/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
07092071 Sample: Roxboro 2 Grab
7/9/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
24.0 %
7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
120,833 col/g dry wt
7/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
07092072 Sample: Roxboro 3 Grab
7/9/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
23.7 %
7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
67,511 col/g dry wt
7/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
07092073 Sample: Roxboro 4 Grab
7/9/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
24.2 %
7/14/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
28,926 col/g dry wt
7/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order # 07092074 Sample: Roxboro 5 Grab 7/9/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 26.1 % 7/14/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 34,483 col/g dry wt 7/9/20 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Ryan Copeland Report Date: 7/20/2020
Client: Synagro
284 Boger Road Project: Roxboro
Mocksville, NC 27028 Date Sample Rcvd: 7/9/2020
Meritech Work Order # 07092075 Sample: Roxboro 6 Grab 7/9/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.1 % 7/14/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 45,643 col/g dry wt 7/9/20 130 col/g dry wt SM 9222D
Meritech Work Order # 07092076 Sample: Roxboro 7 Grab 7/9/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 24.3 % 7/14/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 22,634 col/g dry wt 7/9/20 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. -"'n
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9/18 Chain of Custody Record (COC)
NPDES#:
Client: SiN hY'a Phone: 34 6b 7 - 499V
Address: n,M �.r a Rom Fax:
roc KSs1�� E ML Email: I LJELA,-'n `� )1"-A6-(t-% (,,.+l
Project: Z.XG'C-
P.O.#:
Attention: i SAX) Turn Around Time*
*RUSH work needs prior approval,
How would you li our report sent? char es AoI
Circle all that apply: Emai preferred), Fax, Mail Std 10 'a s) 3 a s z❑rs
;i M E R I T E C H, INC.
ENVIRONMENTAL LABORATORIES
i 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.111erlteCillabS.001Y1
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): P6u�M
,
Lab Use Only
Start
End
comp?
Crab?
#of
Cont.
Test(s) Required
On Ice?
'Yqs / No
pH OK?
CI OK?
Date
Time
Date
Time
2
`1�
Temperature Upon
Receipt:
i
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples must be done in the field prior to preservation. ***
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes Ll No L1
Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
`Hand Delivery
Relinquished by:
. Time:
Date:7 -�-�
Received by: Date: Time:
❑ Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
jg<eVfbyyb: � Date: i rt it/
yE, . . , ..

DIGESTER
"COOLER"
SLUDGE
ROXBORO WWTP LAB
% TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Nicki Dalton, Crystal Shotwell
DATE/TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH +WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
(Total)
Time
Out
Oven
WEIGHT
DISH +DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
(Volatile)
Time
In
Oven
(Volatile)
Time
Out
Oven
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
ANALYST
INITIALS
RPD's
if Needed
4/14/2020
4/14/2020
7
35
82.4122
116.4224
34.0102
8:39 AM
9:39 AM
82.4116
-.0006
Blank
11:01 AM
12:01 PM
82.4117
-.0001
Blank
ND
6:29 AM
4/13/2020
8
35
77.8716
112.5729
34.7013
8:39 AM
9:39 AM
78.0985
.2269
0.65
11:01 AM
12:01 PM
77.9497
.1488
66
ND
0%
4/13/2020
5
35
77.8290
112.0590
34.2300
8:39 AM
9:39 AM
78.0512
.2222
0.65
11:01 AM
12:01 PM
77.9052
.1460
66
NO
4/21/2020
4/21/2020
7
35
82.4122
116.1089
33.6967
7:56 AM
8:56 AM
82.4119
-.0003
Blank
10:02 AM
11:02 AM
82.4118
.0001
Blank
CLS
5:55 AM
4/20/2020
5
35
77.8287
111.9375
34.1088
7:56 AM
8:56 AM
78.0326
.2039
0.60
10:02 AM
11:02 AM
77.8969
.1357
67
CLS
0%
4/20/2020
8
35
77.8723
111.4726
33.6003
7:56 AM
8:56 AM
78.0747
.2024
0.60
10:02 AM
11:02 AM
77.9398
.1349
67
CLS
4/28/2020
4/28/2020
7
35
82.4112
115.8478
33.4366
8:45 AM
9:45 AM
82.4113
.0001
Blank
10:48 AM
11:48 AM
82.4101
.0012
Blank
ND
6:47 AM
1 4/27/2020
8
1 35
1 77.8709
112.6157
1 34.7448
8:45 AM
9:45 AM
1 78.0730
.2021
1 0.58
10:48 AM
11:48 AM
77.9404
1 .1326
66
ND
0%
4/27/2020
5
35
77.8275
112.5218
34.6943
8:45 AM
9:45 AM
78.0280
.2005
0.58
10:48 AM
11:48 AM
77.8957
.1323
66
ND
5/5/2020
5/5/2020
7
35
82.4123
117.2995
34.8872
8:00 AM
9:00 AM
82.4122
-.0001
Blank
10:04 AM
11:04 AM
82.4118
.0004
Blank
ND
6:07 AM
5/4/2020
8
35
77.8727
113.5050
35.6323
8:00 AM
9:00 AM
78.0686
.1959
0.55
10:04 AM
11:04 AM
77.9398
.1288
66
1 ND
0%
5/4/2020
5
35
77.8289
112.9366
35.1077
8:00 AM
9:00 AM
78.0244
1 .1955
0.56
10:04 AM
11:04 AM
77.8958
.1286
66
ND
5/12/2020
5/12/2020
7
35
82.4113
117.5917
35.1804
8:16 AM
9:16 AM
82.4106
-.0007
Blank
10:20 AM
11:20 AM
82.4108
-.0002
Blank
ND
5:50 AM
5/11/2020
8
35
77.8723
112.7568
34.8845
8:16 AM
9:16 AM
78.0519
.1796
0.51
10:20 AM
11:20 AM
77.9338
.1181
66
ND
3%
5/11/2020
5
35
77.8280
113.1500
35.3220
8:16 AM
9:16 AM
78.0319
.2039
0.58
10:20 AM
11:20 AM
77.8937
.1382
68
ND
5/19/2020
5/19/2020
7
35
82.4124
116.6818
34.2694
8:14 AM
9:14 AM
82.4113
-.0011
Blank
10:25 AM
11:25 AM
82.4113
.0000
Blank
NO
6:21 AM
5/18/2020
8
35
77.8731
112.8604
34.9873
8:14 AM
9:14 AM
78.0494
.1763
0.50
10:25 AM
11:25 AM
77.9338
.1156
66
ND
0%
5/18/2020
5
35
77.8293
111.6124
33.7831
8:14 AM
9:14 AM
78.0006
.1713
0.51
10:25 AM
11:25 AM
77.8879
.1127
66
ND
5/12/2020
5/12/2020
965
35
55.9350
90.0830
34.1480
9:42 AM
10:42 AM
55.9341
-.0009
Blank
11:34 AM
12:34 PM
55.9349
-.0008
Blank
ND
8:18 AM
5/11/2020
62
35
75.9794
110.0702
34.0908
9:42 AM
10:42 AM
76.1552
.1758
0.52
11:34 AM
12:34 PM
76.04
.1152
66
ND
0%
5/11/2020
9
35
73.4281
108.7448
35.3167
9:42 AM
10:42 AM
73.6099
1 .1818
1 0.51
11:34 AM
12:34 PM
73.4905
.1194
66
ND
x - Blank
2020 (Second Quarter) VECTOR ATTRACTION CALCULATIONS
large particle in dish
redo

KIN11
503 VECTOR ATTRACTION
This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction
Formula
In - Out n .66 - .67 n -.010 n -0.01 n
In - (In x Out) - .66- (.66 x .67) - .66 - 44 - .22 - -.045 x
In - Out F- .66-66 .66 n .00 n .00 n
In - (In x Out) - .66- (.66 x .66) - .66 - .22 L= .44 - .000 x
In - Out n 0.61 - .63 n -.020 n -0.02 n
In - (In x Out) .61- (. 61 x .63) .61 - .38 .230 -0.09 x
In - Out n .60 - .63 n -.030 n -.03 n
In - (In x Out 60- (.60 x .63) .60 - .38 .22 -0.14 x
❑ 0 El
Reduction
100 0 -4.5 First Quarter
100 ❑ 0.0 Second Quarter
100 0 -9.0 Third Quarter
100 0 -14.0 Fourth Quarter
0
2020
2020
2020
2020

Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number: NC 0021024
Monitoring Period: From 07/01/2020 To 09/30/2020
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
!I...... W...... —I.,to Oho Fnlln.v;n.r m....;tnw:nn rtnto•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6'
CFU
19305
36787
57522
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10to the 611'
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note N you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qqu�alified personnel properlyy gather and evaluate the information used to determine that the ppathogen and
vector attrac -on reduction requirements have been met. I am aware that there are significant penalties }or false
certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer Name and Title Land Applier Name and Title (if applicable) (type or print)
Signature of Prepar r* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

FECAL DATA SHEET
Lab result
Log
19305
4.29
Min 19305
57269
4.76
Max 57522
30303
4.48
Geometric Mean 36787
26,906
4.43
57522
4.76
35874
4.55
49017
4.69
Average
4.57

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 10/16/2020
Project: Roxboro
Date Sample Rcvd: 10/8/2020
Meritech Work Order #
10082051 Sample: Roxboro 1 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
25.9 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
19,305 col/g dry wt 10/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
10082052 Sample: Roxboro 2 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
22.7 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform. (SIudge)
57,269 col/g dry wt 10/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
10082053 Sample: Roxboro 3 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
23.1 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
30,303 col/g dry wt 10/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
10082054 Sample: Roxboro 4 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
22.3 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
26,906 col/gdrywt 10/9/20
130 col/gdrywt
SM 9222D
Meritech Work Order #
10082055 Sample: Roxboro 5 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
22.6 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
57,522 col/g drywt 10/9/20
130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 10/16/2020
Project: Roxboro
Date Sample Rcvd: 10/8/2020
Meritech Work Order #
10082056 Sample: Roxboro 6 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
22.3 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
35,874 col/g dry wt 10/9/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
10082057 Sample: Roxboro 7 Grab
10/8/20
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
22.4 % 10/9/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
49,017 col/g dry wt 10/9/20
130 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. J�
iaboidt-orkeepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC) NPDES#:
MERITECH, INC. Client: IV Phone:
Address: B06£2 Fax. nn
ENVIRONMENTAL LABORATORIES UIu.E Email: .._'(Z&- nEl-4-SY/uA&e�,C,y
642 Tamco Rd, Phone: [phone] Project: b
Reidsville NC 27320 Fax: [phone] P O #.
Email: info@ meritechlabs.com Attention: !� Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? CI, r es i
WWW.IYIeI"IteChlabS.COf1'1 Circle all that apply: Email referred), Fax, Mail Std 10 a 3-5 Dears z�'s
Sampling Dates & Times Person Taking Sample (Sign/Print): , t I Lab Use Only
Sample Location and/or ID # Start End �'�J
Comp? #of Test(s) Required on Ice? oK?
bate Time Date Time Grab? Cont.Yes / No ClC! OK?
F-�C��et7 F tqO-F-?7
2-�
Temperature Upon
Receipt: �'
Method of *** Dechlorination (<0.5 porn) of Ammonia, cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Shipment: Comments: Compositor #
UPS Jug #
,,Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Relinquished by: Date: Time: Received by: Date: Time:
Hand Delivery !(� �' P z , s
Other Relinquished by: Date: Time: Received by: rate: Time:
Relinquished by: Date: Time: Rec ' ed b b: �g e;� C Ti�
8 t

DIGESTER
"COOLER"
SLUDGE
ROXBORO WWTP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
Analyst: Nicki Dalton, Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
(Total)
Time
Out
Oven
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
(Volatile)
Time
In
Oven
(Volatile)
Time
Out
Oven
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
ANALYST
INITIALS
RPD's
if Needed
7/6/2020
7/6/2020
7
35
82.4118
115.8048
33.3930
8:20 AM
9:20 AM
82.4124
.0006
Blank
11:30 AM
12:30 PM
82.4109
.0015
Blank
NO
6:53 AM
7/6/2020
8
35
77.8731
110.8012
32.9281
8:20 AM
9:20 AM
78.1221
.2490
0.76
11:30 AM
12:30 PM
77.973
.1491
60
NO
2%
7/6/2020
5
35
77.8290
110.7601
32.9311
8:20 AM
9:20 AM
78.0763
.2473
0.75
11:30 AM
12:30 PM
77.9266
.1497
61
NO
7/14/2020
7/14/2020
7
35
82.4118
115.3553
32.9435
8:25 AM
9:25 AM
82.4115
-.0003
Blank
10:30 AM
11:30 AM
82.4115
.0000
Blank
NO
6:05 AM
7/13/2020
8
35
77.8726
111.7185
33.8459
8:25 AM
9:25 AM
78.0967
.2241
0.66
10:30 AM
11:30 AM
77.9568
.1399
62
NO
2%
7/13/2020
5
35
77.8288
111.5354
33.7066
8:25 AM
9:25 AM
78.0497
.2209
0.66
10:30 AM
11:30 AM
77.9116
.1381
63
NO
7/20/2020
7/20/2020
7
35
82.4117
116.4625
34.0508
8:05 AM
9:05 AM
82.4114
-.0003
Blank
10:09 AM
11:09 AM
82.4114
.0000
Blank
NO
6:20 AM
7/20/2020
8
35
77.8726
110.1414
32.2688
8:05 AM
9:05 AM
78.0752
.2026
0.63
10:09 AM
11:09 AM
77.9471
.1281
63
NO
0%
7/20/2020
5
35
77.8282
109.9816
32.1534
8:05 AM
9:05 AM
78.0266
.1984
0.62
10:09 AM
11:09 AM
77.9014
.1252
63
NO
7/27/2020
7/27/2020
7
35
82.4118
117.2006
34.7888
7:45 AM
8:45 AM
82.4117
-.0001
Blank
9:50 AM
10:05 AM
82.4115
.0002
Blank
NO
6:06 AM
7/27/2020
8
35
77.8729
110.2581
32.3852
7:45 AM
8:45 AM
78.0497
.1768
0.55
9:50 AM
10:05 AM
77.9366
.1131
64
NO
0%
7/27/2020
5
35
77.8284
113.0761
35.2477
7:45 AM
8:45 AM
78.0287
.2003
0.57
9:50 AM
10:05 AM
77.9009
.1278
64
NO
8/3/2020
8/3/2020
7
35
82.4112
116.6213
34.2101
8:35 AM
9:35 AM
82.4113
.0001
Blank
10:40 AM
11:50 AM
82.411
.0003
Blank
NO
7:10 AM
8/3/2020
8
35
77.8722
109.6674
31.7952
8:35 AM
9:35 AM
78.0464
.1742
0.55
10:40 AM
11:50 AM
77.9374
.1090
63
NO
0%
8/3/2020
5
35
77.8277
109.5986
31.7709
8:35 AM
9:35 AM
78.0011
.1734
0.55
10:40 AM
11:50 AM
77.8921
.1090
63
NO
8/10/2020
8/10/2020
7
35
82.4114
115.4550
33.0436
8:06 AM
9:06 AM
82.4116
.0002
Blank
10:20 AM
11:20 AM
82.4109
.0007
Blank
NO
6:10 AM
8/10/2020
5
35
77.8284
110.8576
33.0292
8:06 AM
9:06 AM
78.0072
.1788
0.54
10:20 AM
11:20 AM
77.8948
.1124
63
NO
0%
8/10/2020
8
35
77.8731
112.3836
34.5105
8:06 AM
9:06 AM
78.0600
.1869
0.54
10:20 AM
11:20 AM
77.9431
.1169
63
NO
VSR
0
x - Blank
2020 (Thrid Quarter) VECTOR ATTRACTION CALCULATIONS

KIN11
503 VECTOR ATTRACTION
This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction
Formula
In - Out n .66 - .67 n -.010 n -0.01 n
In - (In x Out) - .66- (.66 x .67) - .66 - 44 - .22 - -.045 x
In - Out F- .66-66 .66 n .00 n .00 n
In - (In x Out) - .66- (.66 x .66) - .66 - .22 L= .44 - .000 x
In - Out n 0.61 - .63 n -.020 n -0.02 n
In - (In x Out) .61- (. 61 x .63) .61 - .38 .230 -0.09 x
In - Out n .60 - .63 n -.030 n -.03 n
In - (In x Out 60- (.60 x .63) .60 - .38 .22 -0.14 x
❑ 0 El
Reduction
100 0 -4.5 First Quarter
100 ❑ 0.0 Second Quarter
100 0 -9.0 Third Quarter
100 0 -14.0 Fourth Quarter
0
2020
2020
2020
2020

Facility Name: City of Roxboro WWTP WQ Permit Number:
WWTP Name: Roxboro WWTP NPDES Number: _
Monitoring Period: From 10/01/2020 To 12/31/2020
WQ 0021826
NC 0021024
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
_e__�..a Ana....,, A ..» rl....., 1Pl .. ..l..a� a1,.. F n...,.s.,.. ... ..:fnrinn �1g4.s•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xlOto the 61
CFU
26667
45790
72340
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x 10 to the 6a'
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Mt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/ 15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
— explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the ppathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer Name and Title Land Applier Name and Title (if applicable) (type or print)
.---�- f- 2 -1 q _2, z r
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

FECAL DATA SHEET
Lab result
Log
57018
4.76
Min 26667
26667
4.43
Max 72340
51064
4.71
Geometric Mean 45790
38,961
4.59
72340
4.86
29412
4.47
65574
4.82
Average
4.66

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Ryan Copeland
Client: Synagro
284 B R d
Page 1
Report Date: 11/3/2020
oger oa Project: Roxboro
Mocksville, NC 27028 Date Sample Rcvd: 10/28/2020
Meritech Work Order # 10282011
Parameters
Sample: Roxboro 1 Grab
Results Analysis Date
10/28/20
Reporting Limit Method
% Total Solids
22.8 %
10/29/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
57,018 col/g dry wt
10/28/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
10282012 Sample: Roxboro 2 Grab
10/28/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
22.4 %
10/29/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
26,667 col/g dry wt
10/28/20
130 col/g dry wt
SM 9222D
Meritech Work Order # 10282013 Sample: Roxboro 3 Grab 10/28/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.5 % 10/29/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 51,064 col/g dry wt 10/28/20 130 col/g dry wt SM 9222D
Meritech Work Order # 10282014 Sample: Roxboro 4 Grab 10/28/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.1 % 10/29/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 38,961 col/g dry wt 10/28/20 130 col/g dry wt SM 9222D
Meritech Work Order # 10282015 Sample: Roxboro S Grab 10/28/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.5 % 10/29/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 72,340 col/g dry wt 10/28/20 130 col/g drywt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 11/3/2020
Project: Roxboro
Date Sample Rcvd: 10/28/2020
Meritech Work Order## 10282016 Sample: Roxboro 6 Grab 10/28/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.8 % 10/29/20 0-100 % SM 2540E
Fecal Coliform (Sludge) 29,412 col/g dry wt 10/28/20 130 col/g dry wt SM 9222D
Meritech Work Order # 10282017 Sample: Roxboro 7 Grab 10/28/20
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 24.4 % 10/29/20 0-100 % SM 2540E
Fecal Coliform (Sludge) 65,574 col/g dry wt 10/28/20 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. imalda } h �
Laboratory Rep esentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

ar9na Chain of Custody Record (COC)
J MERITECH, INC.
ENVIRONMENTAL LABORATORIES
642 Tamca Rd. Phone; 336-342-4748
Reidsville NC 27320 Fax: [phone]
Email: info@mer!techlabs.com
www.meritechiabs.com
Sampling Dates & Times
Sample Location and/or ID #
u
Start
End
Ibate
D' Z62v
F Time
U tI L1�1�'
5a-te
Time
Method of *** Uechlorination (<0.5 m) of Am
Shipment:
Comments:
0 UPS
ED Fed Ex Are these results for regulatory purl
Relinquished by; +
Hand Delivery PzY" Lin L.11 af)
Other Relinquished by:
Relinquished by:
NPDES#:
Client: Phone: ����-6A-/q
Address: �.� 05 r2e3Fax:
uACKSVILLL Email: (La-)e:6yl'Jl)CC SVAJ4G120, ,L ,
Project: 0 20
P.O.#:
Attention: Z,' •' rj .
How would you like your report sent?
Circle all that apply( Email referred), Fax, Mail
Peron Takln Sample (Sign/Prin /�
I�!°irti �[' C.. LJIilVll] I i2° o-rll �,'l3! rr �/✓
ramp? # of I
Test(s) Required
Grab? Cont.nt
4- 44�
1
Al
Phenol and TKN sa
ses? Yes LK No
Date: Tlme:
'S
Date: Time:
Rate: Tlme:
ust be done In the field prior to oreservation. ***
Turn Around Time*
*RUSH work needs prior approval,
�harues
1010 d s1 13 - 5 Days F24 88 Hrs.
Report results in: mg/L U mg/
Received by: Date;
Received by: Date:
Lab Use Only
On Ice? pH OK?
Yes / No I Cl OK?
Temperature Upon
Receipt; rL Z
y
Compositor #
Jug #
Q ug/L
Time:
Time:
ITI V ,S

ROXBORO W WTP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 2540B and 2540E
DIGESTER Analyst: Nicki Dalton, Crystal Shotwell
"COOLER"
SLUDGE
DATE/TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH +WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
(Total)
Time
Out
Oven
WEIGHT
DISH +DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
(volatile)
Time
In
Oven
(vola9le)
Time
Out
Oven
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
ANALYST
INITIALS
RPD's
if Needed
35
Blank
.0000
Blank
NO
10/7/2020
10/5/2020
8
35
77.8722
111.9267
34.0545
8:21 AM
9:28 AM
78.1252
.2530
0.74
10:30 AM
11:30 AM
77.9725
.1527
60
NO
0%
5:30 AM
10/5/2020
5
35
77.8285
112.1235
34.2950
8:21 AM
9:28 AM
78.0844
.2559
0.75
10:30 AM
11:30 AM
77.9304
.1540
60
NO
35
Blank
.0000
Blank
ND
10/12/2020
10/12/2020
8
35
77.8725
111.9893
34.1168
7:30 AM
8:30 AM
78.0885
.2160
0.63
9:33 AM
10:30 AM
77.9549
.1336
62
ND
0%
6:00 AM
10/12/2020
5
35
77.8289
111.13196
33.9907
7:30 AM
8:30 AM
78.0447
.2158
0.63
9:33 AM
10:30 AM
77.9103
.1344
62
NO
35
Blank
.0000
Blank
ND
10/20/2020
10/19/2020
8
1 35
1 77.8726
112.4705
34.5979
7:27 AM
8:27 AM
78.0672
.1946
0.56
9:28 AM
10:28 AM
77.9436
.1236
64
ND
2%
6:40 AM
10/19/2020
5
35
77.8285
112.6064
34.7779
7:27 AM
8:27 AM
78.0243
.1958
0.56
9:28 AM
10:28 AM
77.9001
.1242
63
ND
35
Blank
.0000
Blank
ND
10/27/2020
10/26/2020
9
35
73.4227
107.4332
34.0105
7:11 AM
8:11 AM
73.6176
.1949
0.57
9:16 AM
10:16 AM
73.4953
.1223
63
ND
0%
5:35 AM
10/26/2020
5
35
77.8284
112.1112
34.2828
7:11 AM
8:1 1 AM
78.0286
.2002
0.58
9:16 AM
10:16 AM
77.902
.1266
63
ND
35
1
1
Blank
.0000
Blank
ND
11/3/2020
11/2/2020
8
35
77.8721
112.3578
34.4857
7:30 AM
8:30 AM
78.0530
.1809
0.52
9:30 AM
10:30 AM
77.939
.1140
63
ND
0%
5:30 AM
11/2/2020
5
35
77.8283
111.9634
34.1351
7:30 AM
8:30 AM
78.0078
.1795
0.53
9:30 AM
10:30 AM
77.8944
.1134
63
NO
35
Blank
.0000
Blank
NO
11/9/2020
11/9/2020
8
35
77.8718
111.8151
33.9433
7:40 AM
8:40 AM
78.0401
.1683
0.50
9:41 AM
10:41 AM
77.9355
.1046
62
NO
2%
5:56 AM
11/9/2020
5
35
77.8282
111.6137
33.7855
7:40 AM
8:40 AM
77.9987
.1705
0.50
9:41 AM
10:41 AM
77.8918
.1069
63
NO
Beginning with the fourth quarter samples out lab no longer uses "blanks" in this analysis. As per
new requirements we now use "constant weights".
VSR
0
x - Blank
2020 (Fourth Quarter) VECTOR ATTRACTION CALCULATIONS

KIN11
503 VECTOR ATTRACTION
This is our worksheet showing that in using the 503.33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction
Formula
In - Out n .66 - .67 n -.010 n -0.01 n
In - (In x Out) - .66- (.66 x .67) - .66 - 44 - .22 - -.045 x
In - Out F- .66-66 .66 n .00 n .00 n
In - (In x Out) - .66- (.66 x .66) - .66 - .22 L= .44 - .000 x
In - Out n 0.61 - .63 n -.020 n -0.02 n
In - (In x Out) .61- (. 61 x .63) .61 - .38 .230 -0.09 x
In - Out n .60 - .63 n -.030 n -.03 n
In - (In x Out 60- (.60 x .63) .60 - .38 .22 -0.14 x
❑ 0 El
Reduction
100 0 -4.5 First Quarter
100 ❑ 0.0 Second Quarter
100 0 -9.0 Third Quarter
100 0 -14.0 Fourth Quarter
0
2020
2020
2020
2020

SECTION 6

Agricultural Lime Application Log
Year: 2020
Project: Roxboro
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied 11
Date Applied
PS-24-1
6.0
0.0 tons/ac.
PS-24-2
6.8
0.0 tons/ac.
PS-24-3
6.0
0.0 tons/ac.
PS-25-1A
6.5
0.0 tons/ac.
PS-25-2
6.1
0.0 tons/ac.

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL017512
Client:
Ronald Carver
Advisor:
Ryan Copeland
vo- Predictive
105 Carver Farm Rd
SYNAGRO
Roxboro, NC 27573
284 Boger Road
.'..,$' Soil Report Mehlich-3 Extraction
Mocksville, NC27028
Sampled County: Person
Links to Helpful Information
Client ID: 223450
Advisor
ID: 499503
Sampled: Received: 11/25/2020 Completed: 01/13/2021 Farm: PS-24
Sample ID: PS241
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
100
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.41 1.02 7.8 81 1.5 6.0 171 22 60 20
39
836
519
549
549
297
0.1 1
Sample ID: PS242
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
20
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.41 0.97 14.6 95 0.8 6.8 247 68 83 9
45
305
188
662
662
161
0.1 1
Sample ID: PS243
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
50
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 1.01 10.9 87 1.4 6.0 198 46 62 23
47
195
133
395
395
462
0.1 1
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO17512
Ronald Carver
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL017513
Client:
Paul Bailey
Advisor:
Ryan Copeland
vo- Predictive
2260 Haywood Bailey Rd.
SYNAGRO
Roxboro, NC 27573
284 Boger Road
.'..,$' Soil Report Mehlich-3 Extraction
Mocksville, NC27028
Sampled County: Person
Links to Helpful Information
Client ID: 107949
Advisor
ID: 499503
Sampled: Received: 11/25/2020 Completed: 01/13/2021 Farm: PS-X8/ PS-25
Sample ID: PSX81
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
50
0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.22 1.01 10.2 85 1.5 5.9 169 43 58 25
45
162
114 322
322
456
0.1 1
Sample ID: PS251A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 30
100
0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 1.02 9.6 89 1.1 6.5 49 22 64 24
26
1890 1144 235
235
294
0.1 1
Sample ID: PS252
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
80
0 0 0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.18 1.04 9.8 87 1.2 6.1 76 28 57 29
51
166
115 179
179
239
0.1 1
North Carolina
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SLO17513
Paul Bailey
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm