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HomeMy WebLinkAboutNC0026051_Pretreatment_Annual_Report_20210227POTW: NPDES #: WWTP: Reporting Period: Pretreatment Annual Report Durham County Triangle WWTP NC0026051 Triangle Wastewater Treatment Plant January 1, 2020 to December 31, 2020 Person to contact Regarding this report: Amy Moore Phone #: 919-560-9035 I certify that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based upon my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. },o,o4A,L /1/);I,21 Amy laore Date Laboratory & Compliance Manager DocuSign Envelope ID: DC036976-38AC-4819-9004-0029DAAB2668 POTW: NPDES #: WWTP: Reporting Period: Pretreatment Annual Report Durham County Triangle WWTP NC0026051 Triangle Wastewater Treatment Plant January 1, 2020 to December 31, 2020 Person to contact Regarding this report: Amy Moore Phone #: 919-560-9035 I certify that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based upon my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. �DocuSigned by: loticketiS IAa�«1 �tegjjxey Date Deputy Director of E&ES/POTW Director 2/27/2021 DURHAM COUNTY PRETREATMENT ANNUAL REPORT NARRATIVE GENERAL PROGRAM INFORMATION: Durham County submitted revisions to the Enforcement Response Plan (ERP) on February 11, 2020 in response to the Dental Amalgam Rule, that was approved February 13, 2020. Durham County submitted a revision of the Long Term Monitoring Plan (LTMP) to the Division on September 5, 2013, that was approved by the Division on October 8, 2013. Durham County submitted a revision of the Sewer Use Ordinance (SUO) to the Division on December 18, 2012. A letter was received from the Division on January 28, 2013, requesting additional information. The additional information was submitted March 21, 2013 and approved by the Division on April 3, 2013. The Industrial Waste Survey (IWS) was submitted to the Division on March 9, 2016. The Division requested additional information that was submitted on May 27, 2016. The IWS was approved by the Division on May 31, 2016. Durham County submitted a revision of the Headwork's Analysis (HWA) on March 16, 2018, that was approved by the Division on May 2, 2018. A copy of the "Pretreatment Program Info Database" is included. GENERAL PERMIT INFORMATION: During the reporting period the following Industrial User Permits were issued, modified, or renewed: • Biogen, IUP DC-080 was renewed with an effective date of August 24, 2020. The permit was received by the Division on September 3, 2020. • Novan, IUP DC-084 was dropped from the program as of December 21, 2020. The request to remove Novan from the program was received by the Division on December 21, 2020 and approved by email on February 21, 2021. • TriPharm Services, Inc. dba Alcami Corporation, IUP DC-106 was issued with an effective date of October 18, 2020. The permit was received by the Division on September 18, 2020. • United Therapeutics Corporation, IUP DC-053 was renewed with an effective date of May 25, 2020. The permit was received by the Division on May 26, 2020 and approved by email on September 2, 2020. SIU INFORMATION: 1. AstraZeneca (formerly Pearl Therapeutics) (IUP DC-078) — No permit violations occurred at this facility. 2. Aurobindo USA (IUP DC-089) — No permit violations occurred at this facility. 3. Biogen (1UP DC-080) — No permit violations occurred at this facility. 4. Cintas (IUP DC-037) — Cintas was issued a Notice of Violation on April 24, 2020 for exceeding the daily maximum of Oil and Grease (polar) on March 13, 2020. The Notice of Violation was issued in accordance with the ERP. 5. Cree, Inc. (IUP DC-076) — No permit violations occurred at this facility. 6. Cree RTP (IUP DC-040) — Cree RTP was issued a Notice of Violation on January 7, 2020 for failure to provide notification to Durham County of an acid - separation piping installation and failure to provide engineering certification as required per an Authorization to Construct issued on September 27, 2019. The Notice of Violation was issued in accordance with the ERP. 7. JMC (IUP DC-023) — JMC is no longer discharging process flow. All chemicals and process equipment has been removed from the site. The pretreatment system remains on site in the event it needs to be used in ground water remediation/removal of chromium. Monthly flow reports were submitted but no monitoring was conducted at the site in 2020. No permit violations occurred at this facility. 8. Micross (IUP DC-085) — Micross was issued a Notice of Violation on August 29, 2020 for exceeding the daily maximum for mercury on June 15, 2020. The Notice of Violation was issued in accordance with the ERP. 9. Novan (IUP DC-084) — Novan was issued a Notice of Violation on February 12, 2020 for late reporting. The permit requires the summary of the monthly flow rate be submitted by the last day of the following month. The report for December 2020 was received on February 6, 2020. Novan decommissioned all process equipment on June 30, 2020. A close-out inspection was conducted on July 10, 2020. The Notice of Violation was issues in accordance with the ERP. 10. Phononic (IUP DC-075) — Phononic was issued a Notice of Violation on August 29, 2020, for exceeding the daily maximum for nickel on June 18, 2020. Filters on the pretreatment unit were replaced, additional samples were taken and Phononic returned to compliance. The Notice of Violation was issued in accordance with the ERP. 11. PowerSecure (IUP DC-095) — PowerSecure was issued a Notice of Violation on October 10, 2020 for the failure to monitor for the first semiannual period of 2020. Monitoring was conducted twice in November 2020. The Notice of Violation was issued in accordance with the ERP. 12. SCM Metal (IUP DC-005) — No permit violations occurred at this facility. 13. TriPharm Services (IUP DC-106) — No permit violations occurred at this facility. 14. United Therapeutics (IUP DC-053) — United Therapeutics was issued a Notice of Violation on September 25, 2020 for exceeding the daily maximum of acetone on July 10, 2020 and for exceeding the monthly average of acetone for July 2020. United Therapeutics was issued a Notice of Violation on November 30, 2020 for exceeding the monthly average for acetone in September 2020. United Therapeutics discovered that a holding tank prior to discharge was the source of the elevated acetone. United Therapeutics stopped discharge and hauled away process wastewater until the tank was emptied and cleaned. The contents of the tank were removed and hauled off site via hazardous waste disposal. Additional samples were collected for acetone in October and November 2020. United Therapeutics is currently in Significant Non -Compliance for exceeding the monthly average Technical Review Criteria for the second semiannual period of 2020. The Notices of Violation were issued in accordance with the ERP. WASTE REDUCTION ACTIVITIES: The Triangle Wastewater Treatment Plant participates in the following waste reduction activities: 1. Recycling of plastic, glass, aluminum, newspaper and corrugated cardboard. 2. Recycling of used pens, markers, mechanical pencils, highlighters, scotch tape dispensers and cores, and ink jet cartridges. 3. Recycling of used batteries. 4. Secondary containment for bulk storage of chemicals. 5. Recycling of used oil. 6. Reduction of paper generation. 7. Reduction of power consumption via automation. Logic controls are present that operates the rotors used for aeration as well as the intensity of the Ultraviolet Disinfection System. Permit applications and inspection reports were reviewed for industrial waste reduction activities information. The codes used in Part V, Waste Reduction Information of the Industrial Waste Survey and Permit Application are used here. A copy of the code and description is attached for reference. Industry Name Code or description of waste reduction activity AstraZeneca (formerly Pearl Therapeutics) Aurobindo W19, W34, W36, W55, W62, W71 Biogen W13, W33, W34, W36, W39, W99 Cintas W13, W52 Cree W24, W32, W33, W34, W36, W39, W51, W54, W55, W58, W67 Cree RTP JMC W24, W52, W81 Micross W21, W23, W33, W34, W36 Novan W14, W55, W61, W62, W72 Phononic W34 PowerSecure W3, W24, W31, W32, W34, W36 W39 United Therapeutics W25, W52, W54, W55 WASTE REDUCTION CODES: SCM W24, W32, W33, W34, W36, W51, W54, W55 W13 Improved maintenance scheduling recordkeeping, or procedures W14 Changed production schedule to minimize equipment and feedstock changeovers W19 Other changes in operating practices (explain briefly in comments) W21 Instituted procedures to ensure that materials do not stay in inventory beyond shelf -life W22 Began to test outdated material -continue to use if still effective W23 Eliminated shelf -life requirements for stable materials W24 Instituted better labeling procedures W25 Instituted clearinghouse to exchange materials that would otherwise be discarded W29 Other changes in Inventory control (explain briefly in comments) W31 Improved storage or stacking procedures W32 Improved procedures for loading, unloading and transfer operations W33 Installed overflow alarms or automatic shutoff valves W34 Installed secondary containment W35 Installed vapor recovery systems W36 Implemented inspection or monitoring program of potential spill or leak sources W39 Other spill and leak prevention (explain briefly in comments) W41 Increased purity of raw materials W42 Substituted raw materials W49 Other raw material modifications (explain briefly in comments) W51 Instituted recirculation within a process W52 Modified equipment, layout, or piping W53 Use of a different process catalyst W54 Instituted better controls on operating bulk containers to minimize discarding of empty containers W55 Changed from small volume containers to bulk containers to minimize discarding of empty containers W58 Other process modifications (explain briefly in comments) W59 Modified stripping / cleaning equipment W60 Changed to mechanical stripping / cleaning devices (from solvents or other materials) W61 Changed to aqueous cleaners (from solvents or other materials) W62 Reduced the number of solvents used to make waste more amenable to recycling W63 Modified containment procedures for cleaning units W64 Improved draining procedures W65 Redesigned parts racks to reduce drag out W66 Modified or installed rinse systems W67 Improved rinse equipment design W68 Improved rinse equipment operation W71 Other cleaning and degreasing operation (explain briefly in comments) W72 Modified spray systems or equipment W73 Substituted coating materials used W74 Improved application techniques W75 Changed from spray to other system W78 Other surface preparation and finishing (explain briefly in comments) W81 Changed product specifications W82 Modified design or composition of product W83 Modified packaging W89 Other product modifications (explain briefly in comments) W99 Other (specify in comments) Additional Information: PowerSecure was in SNC for failure to sample for the first semi-annual period of 2020. Subsequent sampling was conducted and met permit limits in November 2020. The Public Notice is included with this submittal and will be posted in the Durham -Herald Sun. Proof of publication will be sent to the Division of Water Resources as soon as it is available. United Therapeutics was in SNC for exceeding the monthly average Technical Review Criteria for acetone during the second semiannual period. Subsequent acetone sampling was conducted and met permit limits The Public Notice is included with this submittal and will be posted in the Durham -Herald Sun. Proof of publication will be sent to the Division of Water Resources as soon as it is available. Dental Amalgam Information: Durham County mailed eight (8) One Time Compliance Reports for Dental Amalgam to Dentists in the service area and received eight completed forms. Forms are retained at the Triangle Wastewater Treatment Plant for review upon request. Pretreatment Program Info Database for Program Name Durham County WWTP Name Triangle Program Approval Date Pretreatment Status Region County NPDES Number NPDES Effective Date NPDES Expire Date POTW is Primary WWTP Design Flow mgd WWTP SIU's WWTP CIU's date Inactive 14 13 07/06/1995 Full RRO Durham NC0026051 12/01/2011 04/30/2016 TRUE 12.0000 Program Sills Program CIUs printed on: 12/22/2020 Stream Information 7Q10 Flow cfs / mgd 1Q10 Flow cfs / mgd Stream Classification ws-iv Basin Number CPF05 Receiving Stream Name NORTHEAST CREEK IWC % at 7Q10 100.00 0 / 0.00 0.00 / 0.00 Last PAR Rec 03/03/2020 Current Fiscal 03/04/2020 Year PCI Done Last Audit on 07/27/2016 % Design mgd is SIU permitted 14 13 11.85 PAR Due Date 03/01/2021 Audit Year Next20/21 Permitted SIU flow (mgd) [Pt_SIU) mercury 1631 required yes 1.422 Date Next Due 04/01/2023 04/01/2021 Date Received by DWR 03/16/2018 09/05/2013 03/14/2016 12/20/2012 02/11/2020 Date Approved 05/02/2018 10/08/2013 05/31/2016 04/03/2013 02/13/2020 Adopt Date Required Date Adopted 03/11/2013 Info in this Box from Pt Contacts PT_Pro g.Prime Formal Name Phonel ext Fax Date Date Date Attended Attended Attended HWA Wksp IUP Wksp PAR Wksp Ms. Stephanie Brixey I 11919-560-9034 I 1919-544-8590 1 16/22/2011 11/23/2007 sbrixey@dconc.gov Deputy Director of E&ES/POTW 5926 NC Hwy 55 E 27713 Ms. Amy Moore 'Prim 11919-560-9035 l 1919-544-8590 II 2/9/2012 14/18/2012 11/19/2012 I ajmoore@dconc.gov LABORATORY & COMPLIANCE Ms. Laura Melton I 11919-560-9042 1 1919-544-8590 1 I I Imelton@dconc.gov Pretreatment Project Coordinator 5926 Highway 55 East 27713 J f Pretreatment Related NOVs from DWQ 3/24/2004 PAR -failure to enforce-nov/orders for SNC DWR Central Office Contact DWR Regional Contact Kristen Litzenburger Cheng Zhang Chapter 9, PAR Guidance Pretreatment Performance Summary (PPS) 1. Pretreatment Town Name: Durham County 2. "Primary" NPDES Number NC00 26051 or Non Di scharge Permit # if applicable => 3. PAR begin Date, please enter 01 /01 /yy or 07/01 /yy 4. PAR end Date, please enter 06/30/yy or 12/31/yy 5. Total number of SI Us, includes CI Us 6. Number ofClUs 7. Enter the Higher Number, either 7a. Number of SI Us not sampled by POTW 7b. Number of SIUs not inspected by POTW 3. => 1 / 1 /2020 4. => 12/31/2020 5. => 14 6. => 13 (7a) or (7b) here => 1 7a. => 1 7b. => 0 8. Number of SIUswith no IUP, or with an expired IUP 8. _> 9. Total Number of SIUs in SNC due to either I U Reporting violations or IUP Limit violations. To avoid double counting some SIUs Enter (9a + 9b) - 9c here => 0 2 Enter the Number of SIUs in SNC for : 9a. I U Reporting vi of ati ons 9a. => 1 9b. I U P Limit violations 9b. => 1 9c. Both IU Reporting & Limit violations 9c. => 0 10. Number of SI Us i n SNC due to I U Reporting vi of ati ons that were not sampled or inspected by POTW 10. => 0 11. Number of SlUs in SNC dueto violation of 11.=> 0 Compl i ance Schedule due dates 12. Number NOVs, NNCs, AOs, or similar assesed to SIUs 12. => 8 13. Number Civil or Criminal Penalties assessed to SIUs 13. => 0 14. Number of SIUs included in public notice 14. => 2 15. Number of SIUsfrom which penalties collected 15. => 0 16. Total Amount of Civil Penalties Collected 16. => $ 0 17. Total Number of SI Us on a compl i ance schedule 17. => 0 This Column for office use only EPA WENDB PSSD PSED SI US CI us NOIN NOCM PSNC MSNC SNPS SNIN SSNC FENF JUDI SVPu I UPN sOCs Foot Notes: AO CI U CO IUP NNC Administrative Order Categorical Industrial User Consent Order Industrial User Pretreatment Permit Notice of Non -Compliance NOV PAR POTW SI U SNC Noticeof Violation Pretreatment Annual Report Public Operated Treatment Works Significant Industrial User Significant Non -Compliance, formerly RNC Pretreatment Annual Report (PAR) Significant Non -Compliance Report (SNCR) WWTP = Wastewater Treatment Rant, use separate form for each WWTP. SIU = Significant Industrial User SNC = Significant Non -Compliance PAR covers this calendar year => Control A uthority=Program=Town Name => WWTP Name => N PD ES # => A SNCR Form must be submitted with every PAR, please write"None" if you had No SIUs in SNC during calendar year 2020 Durham County Triangle WWTP N C0026051 I UP # Pipe # I ndustry Name Parameter or "Reporting" SNC? (Yes/No) for each 6-month period. Jan. - June July - Dec. DC-075 001 PowerSecure Reporting Yes No DC-053 001 United Therapeutics Acetone No Yes Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SI Us behind this page . Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years. EVERY SNC M UST be explained in the Narrative, How was, is, or will it be resolved? REPEAT SNCs are serious matters that M UST be explai ned i n the Narrative. Form name: PAR,SNCR,2001 Date Revised: 1/4/2001 h istg1fg IP1 REPORT Durham County 2013 2014 2015 2016 2017 2018 2019 1st half 1 2nd half 1st half 1 2nd half 1st half 1 2nd half 1st half 1 2nd half 1st half 1 2nd half 1st half 1 2nd half 1st half 1 2nd half JMC (USA), Inc. IUP # DC-023 IUP Status: Active Pipe # 001 Chromium failure to sample I I PreviousNames: I I SIU Word Description: metals-433-Cr metal production XI XI Phononic IUP # DC-075 Pipe # 001 IUP Status: Active Reporting I PreviousNames: I XI SIU Word Description: Subpart A Aurobindo USA PreviousNames: IUP # DC-089 Pipe # 001 IUP_Status: Active PRINTED ON: 12/16/2020 Acetone I I SIU Word Description: 439 D+E An 'X' in a semi-annual period indicates snc for the period for the respective parameter. This information is compiled from many sources, and has not been verified. Contact the local pretreatment coordinator or state pretreatment staff if errors are noted. PAGE 27 Public Notice Durham County in accordance with Federal and State Regulations, is hereby giving public notice. Listed below are users in significant noncompliance with national pretreatment regulations (40 CFR Part 403), state pretreatment regulations (15 NCAC 2H.0900), or local pretreatment regulations during January 2020 through December 2020. PowerSecure, located at 4058 Stirrup Creek Drive and regulated by significant industrial user permit number DC-095 was in status of significant noncompliance for failure to monitor for the first semiannual period of January through June 2020. A written notification title "Notice of Violation" was sent to the user's authorized representative requiring them to notify the County of the cause of the violation. Subsequent sampling was conducted in 2020 and met the permit limits. United Therapeutics Corporation, located at 55 TW Alexander Drive and regulated by significant industrial user permit number DC-053 was in status of significant noncompliance for exceeding the permit limitation for acetone in the second semiannual period of July through December 2020. A written notification titled "Notice of Violation" was sent to the user's authorized representative requiring them to notify the County of the cause of the violation. Subsequent acetone sampling completed in 2020 met the permit limit. POTW=> NPDES#=> IUP Count 1 2 3 4 5 6 7 8 10 11 12 13 14 Allocation Table Headworks last approved: Allocation Table updated: Permits last modified: 05/02/18 02/01/21 12/21/20 TWWTP Allocation Table Printed: 2/27/2021, 9:52 PM Page 1 of 5 TriangleWWTP NC0026051 Industry INDUSTRY NAMES Permit (pleaselist alphabetidy) number Type Renewal Modification Date Pipe of Effective Effective Permit number Industry Date Date Expires FLOW Permit Limits BOD Permit Limits MGD gal/day Conc. Load mg/I I bsiday AstraZeneca Pharmaceutics DC-078 001 439 D& E Pharmaceutical 01/01/17 01/31/18 12/31/21 0.0020 2,000 Aurobindo USA DC-089 001 439 D&E Pharmaceutical 10/09/19 10/08/24 0.0390 39,000 monitor Biogen DC-080 001 439 C,D& E Pharmaceutical 08/24/20 08/23/25 0.2500 250,000 _ monitor Cintas DC-037 • 001 Full Service Laundry Facility 11/05/17 11/01/22 0.1200 120,000 monitor Cree(008, 009) DC-076 469 Semi Conductor Mfg. 08/01/19 07/31/24 0.4510 451,000 _ Cree 008 008 (Combined Discharge) monitor Cree 009 009 (Combined Discharge) monitor _ Cree RTP DC-040 012 469 Semi Conductor Mfg. 08/01/19 07/31/24 0.3290 329,000 JMC (USA) Inc DC-023 001 433 Cr Metal Production 07/02/17 07/01/22 0.0100 10,000 _ MicrossAdvanced DC-085 001 469 E R&D Semiconductor 10/21/19 10/20/24 0.0750 75,000 Phononic DC-075 001 469 A Semi Conductor Mfg. 03/08/18 03/06/23 0.0200 20,000 _ PowerSerure DC-095 • 001 433 Metal Finisher 11/13/19 11/12/24 0.0060 6,000 SCM Metals DC-005 001 471.104A Powder Former 07/01/16 06/30/21 0.0500 50,000 _ TriPharm DC-106 001 439 D& E Pharmaceutical 10/18/20 10/17/23 0.0050 5,000 monitor United Therapeutics DC-053 001 (Combined Discharge) 05/25/20 05/24/25 0.0500 50,000 _ monitor 002 Pharmaceutical Column Totals=> 1 1.4070 1,407,0001 0 B asi s=> MAHL from HWA (Ibs/day) => Uncontrollable Loading (I bs/day) => .otal Allowable for Industry (MAIL) (Ibs/day) => Total Permitted to Industry (Ibs/day) => MAIL left (Ibsiday) _> 'ercent A l l ow. Ind. (MAIL) still available (%) => Percent MAHL still available (%) _> 5 Percent MAHL (I bs/day) => NPDES Permitted Flow=> NPDES 12.0000 5.3100 6.6900 1.4070 5.2830 79.0 0/0 44.0 0.6000 Design 20016 8281 11735 0 11735 100.0 % 58.6 1001 POTW=> NPDES#=> IUP Count 1 2 3 4 5 6 7 8 10 11 12 13 14 Allocation Table Headworks last approved: Allocation Table updated: Permits last modified: 05/02/18 02/01/21 12/21/20 TWWTP Allocation Table Printed: 2/27/2021, 9:52 PM Page 2 of 5 TriangleWWTP NC0026051 Industry INDUSTRY NAMES Permit (please list alphabetidy) number Pipe number TSS Permit Limits Ammonia Permit Limits Arsenic Permit Limits Cadmium Permit Limits Chromium Permit Limits Copper Permit Limits Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day AstraZeneca Pharmaceutics DC-078 001 Aurobindo USA DC-089 001 monitor monitor _ monitor monitor Biogen DC-080 001 monitor monitor monitor Cintas DC-037 001 monitor _ monitor _ monitor monitor monitor Cree (008, 009) DC-076 Cree 008 008 monitor _ monitor monitor monitor Cree 009 009 monitor Cree RTP DC-040 012 monitor monitor monitor monitor monitor JMC (USA) Inc DC-023 001 monitor 0.0250 0.0021 0.6500 0.0542 0.7000 0.0584 MicrossAdvanced DC-085 001 _ monitor _ monitor monitor Phononic DC-075 001 PowerSecure DC-095 001 _ 0.0700 0.0035 1.7100 0.0856 2.0700 0.1036 SCM Metals DC-005 001 monitor 0.5000 0.2085 TriPharm DC-106 001 monitor monitor monitor United Therapeutics DC-053 001 monitor monitor monitor 002 Column Totals => J 0 0 0.0000 0.0056 0.1398 0.3705 B asi s=> MAHL from HWA (Ibs/day) => Uncontrollable Loadi ng (I bs/day) => .otal Allowable for Industry (MAIL) (Ibs/day) => Total Permitted to Industry (I bs/day) => MAIL left (Ibs/day) _> 'ercent A l l ow. Ind. (MAIL) still available (%) => Percent MAHL still available (%) _> 5 Percent MAHL (I bs/day) => Design 25020 9964 15056 0 15056 100.0 % 60.2 1251 Design 2502.00 1306.42 1195.58 0.00 1195.58 100.0 % 47.8 125.10 Stream Std 0.8962 0.1329 0.7633 0.0000 0.7633 100.0 % 85.2 0.0448 Stream Std 0.2987 0.0133 0.2854 0.0056 0.2799 98.0 % 93.7 0.0149 Stream Std 4.8465 0.1771 4.6694 0.1398 4.5296 97.0 % 93.5 0.2423 AS/Nit/TF inhibition 23.6589 1.9308 21.7281 0.3705 21.3576 98.3 % 90.3 1.1829 POTW=> NPDES#=> IUP Count 1 2 3 4 5 6 7 8 10 11 12 13 14 Allocation Table Headworks last approved: Allocation Table updated: Permits last modified: 05/02/18 02/01/21 12/21/20 TWWTP Allocation Table Printed: 2/27/2021, 9:52 PM Page 3 of 5 TriangleWWTP NC0026051 Industry INDUSTRY NAMES Permit (please list alphabeticly) number Pipe number Cyanide Permit Limits Lead Permit Limits Mercury Permit Limits Molybdenum Permit Limits Nickel Permit Limits Conc. Load mg/I I bs/day Conc. Load mg/I I bs/da, Conc. Load mg/I I bs/day Conc. Load nr I bs/day Conc. Load m /I I bsiday AstraZeneca Pharmaceutics DC-078 001 0.000142 0.000002 Aurobindo USA DC-089 001 monitor 0.000142 0.000046 _ monitor Biogen DC-080 001 0.0400 0.0834 0.000142 0.000296 monitor Cintas DC-037 001 _ monitor 0.000142 0.000142 _ monitor monitor Cree (008, 009) DC-076 0.000142 0.000534 Cree 008 008 monitor monitor monitor _ 0.4570 monitor Cree 009 009 monitor monitor Cree RTP DC-040 012 monitor 0.000142 0.000390 _ monitor monitor JMC (USA) Inc DC-023 001 0.0300 0.0025 0.1600 0.0133 0.000142 0.000012 monitor 0.2000 0.0167 MicrossAdvanced DC-085 001 monitor monitor 0.000142 0.000089 _ monitor monitor Phononic DC-075 001 0.000142 0.000024 monitor 0.0200 PowerSecure DC-095 001 0.5000 0.0250 0.4300 0.0215 0.000142 0.000007 _ monitor 1.0000 0.0500 SCM Metals DC-005 001 0.0300 0.0125 0.1000 0.0417 0.000142 0.000059 monitor monitor TriPharm DC-106 001 0.000142 0.000006 _ monitor United Therapeutics DC-053 001 monitor 0.000142 0.000059 monitor 002 Column Totals => I 0.1234 0.07661 0.001666 0.4570 I 0.0867 B asi s=> MAHL from HWA (Ibs/day) => Uncontrollable Loadi ng (I bs/day) => .otal Allowable for Industry (MAIL) (Ibs/day) => Total Permitted to I ndustry (I bs/day) => MAIL left (Ibsiday) _> 'ercent A l l ow. Ind. (MAIL) still available (%) => Percent MAHL still available (%) _> 5 Percent MAHL (I bs/day) => Stream Std 0.7950 0.0221 0.7728 0.1234 0.6494 84.0 % 81.7 0.0397 Stream Std 3.1596 0.1949 2.9647 0.0766 2.8882 97.4 % 91.4 0.1580 NPDES 0.025829 0.003543 0.022286 0.001666 0.020619 92.5 % 79.8 0.001291 Sludge Ceiling HASL 22.9553 0.3366 22.6188 0.4570 22.1618 98.0 % 96.5 1.1478 Stream Std 2.4843 0.3321 2.1522 0.0867 2.0655 96.0 % 83.1 0.1242 POTW=> NPDES#=> IUP Count 1 2 3 4 5 6 7 8 10 11 12 13 14 Allocation Table Headworks last approved: Allocation Table updated: Permits last modified: 05/02/18 02/01/21 12/21/20 TWWTP Allocation Table Printed: 2/27/2021, 9:52 PM Page 4 of 5 TriangleWWTP NC0026051 Industry INDUSTRY NAMES Permit (please list alphabetidy) number Pipe number Selenium Permit Limits Silver Permit Limits Zinc Permit Limits Total Nitrogen Permit Limits Total Phos. Permit Limits Conc. Load mg/I I bs/day Conc. Load mg/I I bs/da Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day AstraZeneca Pharmaceutics DC-078 001 I Aurobindo USA DC-089 001 monitor _ monitor monitor Biogen DC-080 001 _ monitor _ monitor monitor Cintas DC-037 001 monitor _ monitor _ monitor monitor Cree (008, 009) DC-076 _ _ Cree 008 008 monitor - monitor monitor _ monitor monitor Cree 009 009 Cree RTP DC-040 012 monitor - monitor monitor _ monitor monitor JMC (USA) Inc DC-023 001 0.0900 0.0075 _ 0.0467 _ monitor monitor MicrossAdvanced DC-085 001 monitor monitor _ monitor monitor Phononic DC-075 001 _ _ PowerSecure DC-095 001 0.2400 0.0120 1.4800 0.0741 SCM Metals DC-005 001 monitor - monitor _ monitor monitor TriPharm DC-106 001 _ monitor _ monitor monitor United Therapeutics DC-053 001 _ monitor _ monitor monitor 002 Column Totals => 1 0.0000 0.01951 0.12081 0.00 1 0.00 B asi s=> MAHL from HWA (Ibs/day) => Uncontrollable Loadi ng (I bs/day) => .otal Allowable for Industry (MAIL) (Ibs/day) => Total Permitted to I ndustry (I bs/day) => MAIL left (Ibs/day) _> 'ercent A l l ow. Ind. (MAIL) still available (%) => Percent MAHL still available (%) _> 5 Percent MAHL (I bs/day) => Sludge Ceiling HASL 0.4219 0.0930 0.3289 0.0000 0.3289 100.0 % 78.0 0.0211 AS/Nit/TF inhibition 12.3224 0.0443 12.2781 0.0195 12.2585 99.8 % 99.5 0.6161 AS/Nit/TF inhibition 49.2894 18.1304 31.1590 0.1208 31.0382 99.6 % 63.0 2.4645 Design 4003.2000 1988.6492 2014.55 0.00 2014.55 100.0 % 50.3 200.16 Design 650.00 238.92 411.08 0.00 411.08 100.0 63.2 32.5000 POTW=> NPDES#=> IUP Count 1 2 3 4 5 6 7 8 10 11 12 13 14 Allocation Table Headworks last approved: Allocation Table updated: Permits last modified: 05/02/18 02/01/21 12/21/20 TWWTP Allocation Table TriangleWWTP NC0026051 Industry INDUSTRY NAMES Permit (please list alphabetidy) number Pipe number Chloride Permit Limits Fluoride Permit Limits Conc. Load mg/I I bs/day Conc. Load mg/I I bs/day AstraZeneca Pharmaceutics DC-078 001 Aurobindo USA DC-089 001 monitor monitor Biogen DC-080 001 monitor _ monitor Cintas DC-037 001 monitor monitor Cree (008, 009) DC-076 _ 26.3294 Cree 008 008 monitor monitor Cree 009 009 monitor _ monitor Cree RTP DC-040 012 monitor 7.0000 19.2070 JMC (USA) Inc DC-023 001 monitor monitor MicrossAdvanced DC-085 001 monitor 6.0000 3.7530 Phononic DC-075 001 PowerSecure DC-095 001 SCM Metals DC-005 001 monitor _ monitor TriPharm DC-106 001 monitor monitor United Therapeutics DC-053 001 monitor _ monitor 002 Column Totals => I 0.00001 49.2894 B asi s=> MAHL from HWA (Ibs/day) => Uncontrollable Loadi ng (I bs/day) => .otal Allowable for Industry (MAIL) (Ibs/day) => Total Permitted to I ndustry (I bs/day) => MAIL left (Ibsiday) _> 'ercent Al low. Ind. (MAIL) still available (%) => Percent MAHL still available (%) _> 5 Percent MAHL (I bs/day) => Stream Std 16179.5562 3844.2251 12335.3311 0.0000 12335.3311 100.0 % 76.2 808.9778 NPDES 100.3290 31.7881 68.5409 49.2894 19.2515 28.1 % 19.2 5.0164 Printed: 2/27/2021, 9:52 PM Page 5 of 5 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result / Limit Mass /Limit Acetone 02/24/2020 S AstraZeneca022420Se1 0.168 / 20.7 mg/L f Feb 2020 Week 4 0.168 / mg/L Feb 2020 Average 0.168 / 8.2 mg/L 2020 Quarter 1 0.168 / mg/L 2020 1st 6 Months (Avg) 0.168 / mg/L 2020 1st 6...(Max) 0.168 / mg/L 2020 1st 6...(Min) 0.168 / mg/L 2020 1st 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S AstraZeneca0120F1ow 0.000731 / MGD / 02/28/2020 S AstraZeneca0220F1ow 0.000295 / MGD / 03/30/2020 S AstraZeneca0320F1ow 0.00019 / MGD / 04/30/2020 S AstraZeneca0420F1ow 0.000225 / MGD / 05/31/2020 S AstraZeneca0520F1ow 0.000036 / MGD / 06/30/2020 S AstraZeneca0620F1ow 0.000038 / MGD / Jan 2020 Week 4 0.000731 / MGD / Feb 2020 Week 4 0.000295 / MGD / Mar 2020 Week 4 0.00019 / MGD / Apr 2020 Week 4 0.000225 / MGD / May 2020 Week 4 0.000036 / MGD / Jun 2020 Week 4 0.000038 / MGD / Jan 2020 Average 0.000731 / 0.002000 MGD / Feb 2020 Average 0.000295 / 0.002000 MGD / Mar 2020 Average 0.00019 / 0.002000 MGD / Apr 2020 Average 0.000225 / 0.002000 MGD / May 2020 Average 0.000036 / 0.002000 MGD / Jun 2020 Average 0.000038 / 0.002000 MGD / 2020 Quarter 1 0.000405 / MGD / 2020 Quarter 2 0.0001 / MGD / 2020 1st 6 Months (Avg) 0.000253 / MGD / 2020 1st 6...(Max) 0.000731 / MGD / Wednesday, February 24, 2021 10:46:50PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result / Limit Mass /Limit Average Flow for Month 2020 1st 6...(Min) 0.000036 / 2020 1st 6 ...(Count) 6 / MGD Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit COD 01/06/2020 P AstraZeneca010620PO < 7.5 / mg/L < / TW 02/24/2020 S AstraZeneca022420Se1 < 7.5 / mg/L < / f Jan 2020 Week 1 < 7.5 / mg/L < / Feb 2020 Week 4 < 7.5 / mg/L < / Jan 2020 Average < 7.5 / mg/L < / Feb 2020 Average < 7.5 / mg/L < / 2020 Quarter 1 < 7.5 / mg/L < / 2020 1st 6 Months (Avg) < 7.5 / mg/L < / 2020 1st 6 ...(Max) < 7.5 / mg/L < / 2020 1st 6 ...(Min) < 7.5 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 02/24/2020 S AstraZeneca022420Se1 < 0.0005 / 20.7 f Feb 2020 Week 4 < 0.0005 / Feb 2020 Average < 0.0005 / 8.2 2020 Quarter 1 < 0.0005 / 2020 1st 6 Months (Avg) < 0.0005 / 2020 1st 6 ...(Max) < 0.0005 / 2020 1st 6 ...(Min) < 0.0005 / 2020 1st 6 ...(Count) 1 / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / Wednesday, February 24, 2021 10:46:50PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # cyo # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 # 0 0.00 0 0.00 0 0.00 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Isopropyl acetate 02/24/2020 S AstraZeneca022420Se1 < 0.0005 / 20.7 mg/L < / f Feb 2020 Week 4 < 0.0005 / mg/L < / Feb 2020 Average < 0.0005 / 8.2 mg/L < / 2020 Quarter 1 < 0.0005 / mg/L < / 2020 1st 6 Months (Avg) < 0.0005 / mg/L < / 2020 1st 6 ...(Max) < 0.0005 / mg/L < / 2020 1st 6 ...(Min) < 0.0005 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Mercury - LL 01/06/2020 P AstraZeneca010620PO 0.000001 / 0.000142 mg/L / TWHg 02/24/2020 S AstraZeneca022420Se1 0.000002 / 0.000142 mg/L / f 05/04/2020 P AstraZeneca050420PO 0.000001 / 0.000142 mg/L / TWHg Jan 2020 Week 1 0.000001 / mg/L / Feb 2020 Week 4 0.000002 / mg/L / May 2020 Week 1 0.000001 / mg/L / Jan 2020 Average 0.000001 / mg/L / Feb 2020 Average 0.000002 / mg/L / May 2020 Average 0.000001 / mg/L / 2020 Quarter 1 0.000002 / mg/L / 2020 Quarter 2 0.000001 / mg/L / 2020 1st 6 Months (Avg) 0.000001 / mg/L / 2020 1st 6 ...(Max) 0.000002 / mg/L / Wednesday, February 24, 2021 10:46:50PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 2020 1st 6 ...(Min) 0.000001 / 2020 1st 6 ...(Count) 3 / mg/L Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 04 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Methylene Chloride 02/24/2020 S AstraZeneca022420Se1 < 0.001 / 3 mg/L < / f Feb 2020 Week 4 < 0.001 / mg/L < / Feb 2020 Average < 0.001 / 0.7 mg/L < / 2020 Quarter 1 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.001 / mg/L < / 2020 1st 6 ...(Max) < 0.001 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit n-Amyl acetate 02/24/2020 S AstraZeneca022420Se1 < 0.001 / 20.7 mg/L < / f Feb 2020 Week 4 < 0.001 / mg/L < / Feb 2020 Average < 0.001 / 8.2 mg/L < / 2020 Quarter 1 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.001 / mg/L < / 2020 1st 6 ...(Max) < 0.001 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:46:50PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit pH 01/06/2020 P AstraZeneca010620PO 7.4 / 6 - 10 SU / TW 02/24/2020 S AstraZeneca022420Se1 6.7 / 6 - 10 SU / f Jan 2020 Week 1 7.4 / SU / Feb 2020 Week 4 6.7 / SU / Jan 2020 Average 7.4 / SU / Feb 2020 Average 6.7 / SU / 2020 Quarter 1 7.05 / SU / 2020 1st 6 Months (Avg) 7.05 / SU / 2020 1st 6 ...(Max) 7.4 / SU / 2020 1st 6 ...(Min) 6.7 / SU / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit VOC 01/06/2020 P AstraZeneca010620PO < 0.0025 / mg/L < / TW Jan 2020 Week 1 < 0.0025 / mg/L < / Jan 2020 Average < 0.0025 / mg/L < / 2020 Quarter 1 < 0.0025 / mg/L < / 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:46:50PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 01/31/2020 P Aurobindo013120POT 0.217 / 5.59 mg/L W 02/28/2020 S Aurobindo022820Se1f < 0.003 / 5.59 mg/L < / Jan 2020 Week 4 0.217 / mg/L / Feb 2020 Week 4 < 0.003 / mg/L < / Jan 2020 Average 0.217 / 2.21 mg/L / Feb 2020 Average < 0.003 / 2.21 mg/L < / 2020 Quarter 1 < 0.11 / mg/L < / 2020 1st 6 Months (Avg) < 0.1098 / mg/L < / 2020 1st 6 ...(Max) 0.217 / mg/L / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ammonia 01/31/2020 P Aurobindo013120POT 24.9 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 26.1 / mg/L / Jan 2020 Week 4 24.9 / mg/L / Feb 2020 Week 4 26.1 / mg/L / Jan 2020 Average 24.9 / mg/L / Feb 2020 Average 26.1 / mg/L / 2020 Quarter 1 25.5 / mg/L / 2020 1st 6 Months (Avg) 25.5 / mg/L / 2020 1st 6 ...(Max) 26.1 / mg/L / 2020 1st 6 ...(Min) 24.9 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/16/2020 S Aurobindo0120F1ow 0.00498 / MGD 02/18/2020 S Aurobindo0220F1ow 0.005516 / MGD 03/24/2020 S Aurobindo0320F1ow 0.011688 / MGD 04/16/2020 S Aurobindo0420F1ow 0.008911 / MGD Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 1 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 05/21/2020 S Aurobindo0520F1ow 0.00871 / MGD 06/26/2020 S Aurobindo0620F1ow 0.003936 / MGD Jan 2020 Week 3 0.00498 / MGD Feb 2020 Week 3 0.005516 / MGD Mar 2020 Week 4 0.011688 / MGD Apr 2020 Week 3 0.008911 / MGD May 2020 Week 3 0.00871 / MGD Jun 2020 Week 4 0.003936 / MGD Jan 2020 Average 0.00498 / 0.039 MGD Feb 2020 Average 0.005516 / 0.039 MGD Mar 2020 Average 0.011688 / 0.039 MGD Apr 2020 Average 0.008911 / 0.039 MGD May 2020 Average 0.00871 / 0.039 MGD Jun 2020 Average 0.003936 / 0.039 MGD 2020 Quarter 1 0.007395 / MGD 2020 Quarter 2 0.007186 / MGD 2020 1st 6 Months (Avg) 0.007290 / MGD 2020 1st 6 ...(Max) 0.011688 / MGD 2020 1st 6 ...(Min) 0.003936 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit BOD 01/31/2020 P Aurobindo013120POT 281 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 175 / mg/L / Jan 2020 Week 4 281 / mg/L / Feb 2020 Week 4 175 / mg/L / Jan 2020 Average 281 / mg/L / Feb 2020 Average 175 / mg/L / 2020 Quarter 1 228 / mg/L / 2020 1st 6 Months (Avg) 228 / mg/L / 2020 1st 6 ...(Max) 281 / mg/L / 2020 1st 6 ...(Min) 175 / mg/L / Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 2 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit BOD 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result /Limit Mass /Limit Cadmium 01/31/2020 P Aurobindo013120POT < 0.00008 / mg/L < / W 02/28/2020 S Aurobindo022820Se1f < 0.00008 / mg/L < / Jan 2020 Week 4 < 0.00008 / mg/L < / Feb 2020 Week 4 < 0.00008 / mg/L < / Jan 2020 Average < 0.00008 / mg/L < / Feb 2020 Average < 0.00008 / mg/L < / 2020 Quarter 1 < 0.00008 / mg/L < / 2020 1st 6 Months (Avg) < 0.00008 / mg/L < / 2020 1st 6 ...(Max) < 0.00008 / mg/L < / 2020 1st 6 ...(Min) < 0.00008 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Chloride 01/31/2020 P Aurobindo013120POT 61 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 37 / mg/L / Jan 2020 Week 4 61 / mg/L / Feb 2020 Week 4 37 / mg/L / Jan 2020 Average 61 / mg/L / Feb 2020 Average 37 / mg/L / 2020 Quarter 1 49 / mg/L / 2020 1st 6 Months (Avg) 49 / mg/L / 2020 1st 6 ...(Max) 61 / mg/L / 2020 1st 6 ...(Min) 37 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit COD 01/31/2020 P Aurobindo013120POT 995 / mg/L W 02/28/2020 S Aurobindo022820Se1f 508 / mg/L Jan 2020 Week 4 995 / mg/L Feb 2020 Week 4 508 / mg/L Jan 2020 Average 995 / mg/L Feb 2020 Average 508 / mg/L 2020 Quarter 1 751.5 / mg/L Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 3 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit COD 2020 1st 6 Months (Avg) 751.5 / mg/L 2020 1st 6 ...(Max) 995 / mg/L 2020 1st 6 ...(Min) 508 / mg/L 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result / Limit Mass / Limit Copper 01/31/2020 P Aurobindo013120POT 0.055 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 0.077 / mg/L / Jan 2020 Week 4 0.055 / mg/L / Feb 2020 Week 4 0.077 / mg/L / Jan 2020 Average 0.055 / mg/L / Feb 2020 Average 0.077 / mg/L / 2020 Quarter 1 0.066 / mg/L / 2020 1st 6 Months (Avg) 0.066 / mg/L / 2020 1st 6 ...(Max) 0.077 / mg/L / 2020 1st 6 ...(Min) 0.055 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Cyanide 01/31/2020 P Aurobindo013120POT < 0.003 / mg/L < / W 02/28/2020 S Aurobindo022820Se1f < 0.003 / mg/L < / Jan 2020 Week 4 < 0.003 / mg/L < / Feb 2020 Week 4 < 0.003 / mg/L < / Jan 2020 Average < 0.003 / mg/L < / Feb 2020 Average < 0.003 / mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.003 / mg/L < / 2020 1st 6 ...(Max) < 0.003 / mg/L < / 2020 1st 6 ...(Min) < 0.003 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 01/31/2020 P Aurobindo013120POT < 0.003 / 5.59 mg/L < / W Jan 2020 Week 4 < 0.003 / mg/L < / Jan 2020 Average < 0.003 / 2.21 mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 4 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 01/31/2020 P Aurobindo013120POT 0.13 / mg/L / W 02/28/2020 S Aurobindo022820Se1f < 0.05 / mg/L < / Jan 2020 Week 4 0.13 / mg/L / Feb 2020 Week 4 < 0.05 / mg/L < / Jan 2020 Average 0.13 / mg/L / Feb 2020 Average < 0.05 / mg/L < / 2020 Quarter 1 < 0.09 / mg/L < / 2020 1st 6 Months (Avg) < 0.09 / mg/L < / 2020 1st 6 ...(Max) 0.13 / mg/L / 2020 1st 6 ...(Min) < 0.05 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result /Limit Mass /Limit Isopropyl acetate 01/31/2020 P Aurobindo013120POT < 0.003 / 5.59 mg/L < / W Jan 2020 Week 4 < 0.003 / mg/L < / Jan 2020 Average < 0.003 / 2.21 mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 5 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass /Limit Mercury - LL 02/27/2020 S Aurobindo022720Se1f 0.000078 / 0.000142 mg/L / Hg 05/24/2020 P Aurobindo050420POT 0.000023 / 0.000142 mg/L / WHg Feb 2020 Week 4 0.000078 / mg/L / May 2020 Week 4 0.000023 / mg/L / Feb 2020 Average 0.000078 / mg/L / May 2020 Average 0.000023 / mg/L / 2020 Quarter 1 0.000078 / mg/L / 2020 Quarter 2 0.000023 / mg/L / 2020 1st 6 Months (Avg) 0.000050 / mg/L / 2020 1st 6 ...(Max) 0.000078 / mg/L / 2020 1st 6 ...(Min) 0.000023 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit Methylene Chloride 01/31/2020 P Aurobindo013120POT < 0.003 / 0.81 mg/L < / W 02/28/2020 S Aurobindo022820Se1f < 0.003 / 0.81 mg/L < / Jan 2020 Week 4 < 0.003 / mg/L < / Feb 2020 Week 4 < 0.003 / mg/L < / Jan 2020 Average < 0.003 / 0.18 mg/L < / Feb 2020 Average < 0.003 / 0.18 mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.003 / mg/L < / 2020 1st 6 ...(Max) < 0.003 / mg/L < / Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 6 of 11 Aurobindo USA # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Methylene Chloride 2020 2020 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.003 / 2 / Months Sampled : 2 0 0 0 0 mg/L 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 01/31/2020 02/28/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 P Aurobindo013120POT W S Aurobindo022820Se1f Week 4 Week 4 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit n-Amyl acetate 01/31/2020 Jan 2020 Jan 2020 2020 2020 2020 2020 2020 P Aurobindo013120POT W Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.003 / 5.59 0.003 / 0.003 / 2.21 0.003 / 0.003 / 0.003 / 0.003 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 7 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 # Sample Date SamplelD Result/Limit Mass /Limit Nitrogen, Total 01/31/2020 P Aurobindo013120POT 25.9 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 35.8 / mg/L / Jan 2020 Week 4 25.9 / mg/L / Feb 2020 Week 4 35.8 / mg/L / Jan 2020 Average 25.9 / mg/L / Feb 2020 Average 35.8 / mg/L / 2020 Quarter 1 30.85 / mg/L / 2020 1st 6 Months (Avg) 30.85 / mg/L / 2020 1st 6 ...(Max) 35.8 / mg/L / 2020 1st 6 ...(Min) 25.9 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Oil & Grease, Total 01/31/2020 P Aurobindo013120POT 5 / 200 mg/L / W 02/28/2020 S Aurobindo022820Se1f < 2.5 / 200 mg/L < / Jan 2020 Week 4 5 / mg/L / Feb 2020 Week 4 < 2.5 / mg/L < / Jan 2020 Average 5 / mg/L / Feb 2020 Average < 2.5 / mg/L < / 2020 Quarter 1 < 3.75 / mg/L < / 2020 1st 6 Months (Avg) < 3.75 / mg/L < / 2020 1st 6 ...(Max) 5 / mg/L / 2020 1st 6 ...(Min) < 2.5 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 8 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 01/31/2020 P Aurobindo013120POT 8.6 / 6.0 - 10.0 SU W 02/28/2020 S Aurobindo022820Se1f 8.5 / 6.0 - 10.0 SU Jan 2020 Week 4 8.6 / SU Feb 2020 Week 4 8.5 / SU Jan 2020 Average 8.6 / SU Feb 2020 Average 8.5 / SU 2020 Quarter 1 8.55 / SU 2020 1st 6 Months (Avg) 8.55 / SU 2020 1st 6 ...(Max) 8.6 / SU 2020 1st 6 ...(Min) 8.5 / SU 2020 1st 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Temperature 01/31/2020 P Aurobindo013120POT 9 / 66 °C / W 02/28/2020 S Aurobindo022820Se1f 11 / 66 °C / Jan 2020 Week 4 9 / °C / Feb 2020 Week 4 11 / °C / Jan 2020 Average 9 / °C / Feb 2020 Average 11 / °C / 2020 Quarter 1 10 / °C / 2020 1st 6 Months (Avg) 10 / °C / 2020 1st 6 ...(Max) 11 / °C / 2020 1st 6 ...(Min) 9 / °C / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 9 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 01/31/2020 P Aurobindo013120POT 12 / mg/L W 02/28/2020 S Aurobindo022820Se1f 7.41 / mg/L Jan 2020 Week 4 12 / mg/L Feb 2020 Week 4 7.41 / mg/L Jan 2020 Average 12 / mg/L Feb 2020 Average 7.41 / mg/L 2020 Quarter 1 9.705 / mg/L 2020 1st 6 Months (Avg) 9.705 / mg/L 2020 1st 6 ...(Max) 12 / mg/L 2020 1st 6 ...(Min) 7.41 / mg/L 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result/Limit Mass/Limit TSS 01/31/2020 P Aurobindo013120POT 162 / mg/L / W 02/28/2020 S Aurobindo022820Se1f 106 / mg/L / Jan 2020 Week 4 162 / mg/L / Feb 2020 Week 4 106 / mg/L / Jan 2020 Average 162 / mg/L / Feb 2020 Average 106 / mg/L / 2020 Quarter 1 134 / mg/L / 2020 1st 6 Months (Avg) 134 / mg/L / 2020 1st 6 ...(Max) 162 / mg/L / 2020 1st 6 ...(Min) 106 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit VOC 02/28/2020 S Aurobindo022820Se1f < 0.0025 / mg/L < / Feb 2020 Week 4 < 0.0025 / mg/L < / Feb 2020 Average < 0.0025 / mg/L < / 2020 Quarter 1 < 0.0025 / mg/L < / 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Zinc Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 10 of 11 Aurobindo USA SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc 01/31/2020 P Aurobindo013120POT 0.305 / mg/L W 02/28/2020 S Aurobindo022820Se1f 0.258 / mg/L Jan 2020 Week 4 0.305 / mg/L Feb 2020 Week 4 0.258 / mg/L Jan 2020 Average 0.305 / mg/L Feb 2020 Average 0.258 / mg/L 2020 Quarter 1 0.282 / mg/L 2020 1st 6 Months (Avg) 0.282 / mg/L 2020 1st 6 ...(Max) 0.305 / mg/L 2020 1st 6 ...(Min) 0.258 / mg/L 2020 1st 6 ...(Count) 2 / Wednesday, February 24, 2021 10:47:55PM * Indicates Violation ** Indicates TRC Violation Page 11 of 11 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 01/28/2020 P Biogen012820POTW < 0.025 / 12.19 mg/L < 0.0147 / lbs/day Jan 2020 Week 4 < 0.025 / mg/L < 0.0147 / lbs/day Jan 2020 Average < 0.025 / 4.83 mg/L < 0.0147 / lbs/day 2020 Quarter 1 < 0.025 / mg/L < 0.0147 / lbs/day 2020 1st 6 Months (Avg) < 0.025 / mg/L < 0.0147 / lbs/day 2020 1st 6 ...(Max) < 0.025 / mg/L < 0.0147 / lbs/day 2020 1st 6 ...(Min) < 0.025 / mg/L < 0.0147 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ammonia 01/28/2020 P Biogen012820POTW 3 / mg/L 1.7684 / lbs/day 02/11/2020 S Biogen021120Self 2.1 / mg/L 1.9167 / lbs/day Jan 2020 Week 4 3 / mg/L 1.7684 / lbs/day Feb 2020 Week 2 2.1 / mg/L 1.9167 / lbs/day Jan 2020 Average 3 / mg/L 1.7684 / lbs/day Feb 2020 Average 2.1 / mg/L 1.9167 / lbs/day 2020 Quarter 1 2.55 / mg/L 1.8426 / lbs/day 2020 1st 6 Months (Avg) 2.55 / mg/L 1.8426 / lbs/day 2020 1st 6 ...(Max) 3 / mg/L 1.9167 / lbs/day 2020 1st 6 ...(Min) 2.1 / mg/L 1.7684 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S Biogen0120Flow 0.0777 / 0.375 MGD / 02/29/2020 S Biogen0220F1ow 0.080874 / 0.375 MGD / 03/31/2020 S Biogen0320F1ow 0.0687 / 0.375 MGD / 04/30/2020 S Biogen0420Flow 0.067245 / 0.375 MGD / 05/31/2020 S Biogen0520Flow 0.082814 / 0.375 MGD / 06/30/2020 S Biogen0620Flow 0.087378 / 0.375 MGD / Jan 2020 Week 4 0.0777 / MGD / Feb 2020 Week 4 0.080874 / MGD / Mar 2020 Week 4 0.0687 / MGD / Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Apr 2020 Week 4 0.067245 / MGD May 2020 Week 4 0.082814 / MGD Jun 2020 Week 4 0.087378 / MGD Jan 2020 Average 0.0777 / 0.250 MGD Feb 2020 Average 0.080874 / 0.250 MGD Mar 2020 Average 0.0687 / 0.250 MGD Apr 2020 Average 0.067245 / 0.250 MGD May 2020 Average 0.082814 / 0.250 MGD Jun 2020 Average 0.087378 / 0.250 MGD 2020 Quarter 1 0.075758 / MGD 2020 Quarter 2 0.079146 / MGD 2020 1st 6 Months (Avg) 0.077452 / MGD 2020 1st 6 ...(Max) 0.087378 / MGD 2020 1st 6 ...(Min) 0.067245 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit BOD 01/28/2020 P Biogen012820POTW 107 / mg/L 63.073 / lbs/day 02/11/2020 S Biogen021120Self 11.6 / mg/L 10.588 / lbs/day Jan 2020 Week 4 107 / mg/L 63.073 / lbs/day Feb 2020 Week 2 11.6 / mg/L 10.588 / lbs/day Jan 2020 Average 107 / mg/L 63.073 / lbs/day Feb 2020 Average 11.6 / mg/L 10.588 / lbs/day 2020 Quarter 1 59.3 / mg/L 36.831 / lbs/day 2020 1st 6 Months (Avg) 59.3 / mg/L 36.831 / lbs/day 2020 1st 6 ...(Max) 107 / mg/L 63.073 / lbs/day 2020 1st 6 ...(Min) 11.6 / mg/L 10.588 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Cadmium 01/28/2020 P Biogen012820POTW < 0.00008 / mg/L < 0.000044 / lbs/day 02/11/2020 S Biogen021120Self < 0.0005 / mg/L < 0.000456 / lbs/day Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Cadmium Jan 2020 Week 4 < 0.00008 / mg/L < 0.000044 / lbs/day Feb 2020 Week 2 < 0.0005 / mg/L < 0.000456 / lbs/day Jan 2020 Average < 0.00008 / mg/L < 0.000044 / lbs/day Feb 2020 Average < 0.0005 / mg/L < 0.000456 / lbs/day 2020 Quarter 1 < 0.00029 / mg/L < 0.00025 / lbs/day 2020 1st 6 Months (Avg) < 0.00029 / mg/L < 0.000250 / lbs/day 2020 1st 6 ...(Max) < 0.0005 / mg/L < 0.000456 / lbs/day 2020 1st 6 ...(Min) < 0.00008 / mg/L < 0.000044 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Chloride 01/28/2020 P Biogen012820POTW 93 / mg/L 54.8208 / lbs/day 02/11/2020 S Biogen021120Self 66.3 / mg/L 60.514 / lbs/day Jan 2020 Week 4 93 / mg/L 54.8208 / lbs/day Feb 2020 Week 2 66.3 / mg/L 60.514 / lbs/day Jan 2020 Average 93 / mg/L 54.8208 / lbs/day Feb 2020 Average 66.3 / mg/L 60.514 / lbs/day 2020 Quarter 1 79.65 / mg/L 57.6674 / lbs/day 2020 1st 6 Months (Avg) 79.65 / mg/L 57.6674 / lbs/day 2020 1st 6 ...(Max) 93 / mg/L 60.5140 / lbs/day 2020 1st 6 ...(Min) 66.3 / mg/L 54.8208 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit COD 01/28/2020 P Biogen012820POTW 02/11/2020 S Biogen021120Self Jan 2020 Week 4 Feb 2020 Week 2 Jan 2020 Average Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 145 / mg/L 85.47 / lbs/day 67.3 / mg/L 61.43 / lbs/day 145 / mg/L 85.47 / lbs/day 67.3 / mg/L 61.43 / lbs/day 145 / mg/L 85.47 / lbs/day 67.3 / mg/L 61.43 / lbs/day 106.2 / mg/L 73.45 / lbs/day 106.2 / mg/L 73.45 / lbs/day 145 / mg/L 85.47 / lbs/day 67.3 / mg/L 61.43 / lbs/day 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 01/28/2020 P Biogen012820POTW < 0.003 / 12.19 mg/L < 0.0015 / lbs/day Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 3 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate Jan 2020 Week 4 < 0.003 / mg/L < 0.0015 / lbs/day Jan 2020 Average < 0.003 / 4.83 mg/L < 0.0015 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 Months (Avg) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Max) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 01/28/2020 P Biogen012820POTW < 0.01 / mg/L < 0.0029 / lbs/day 02/11/2020 S Biogen021120Self < 0.05 / mg/L < 0.0456 / lbs/day Jan 2020 Week 4 < 0.01 / mg/L < 0.0029 / lbs/day Feb 2020 Week 2 < 0.05 / mg/L < 0.0456 / lbs/day Jan 2020 Average < 0.01 / mg/L < 0.0029 / lbs/day Feb 2020 Average < 0.05 / mg/L < 0.0456 / lbs/day 2020 Quarter 1 < 0.03 / mg/L < 0.0243 / lbs/day 2020 1st 6 Months (Avg) < 0.03 / mg/L < 0.0243 / lbs/day 2020 1st 6 ...(Max) < 0.05 / mg/L < 0.0456 / lbs/day 2020 1st 6 ...(Min) < 0.01 / mg/L < 0.0029 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Isopropyl acetate 01/28/2020 P Biogen012820POTW < 0.003 / 12.19 mg/L < 0.0015 / lbs/day Jan 2020 Week 4 < 0.003 / mg/L < 0.0015 / lbs/day Jan 2020 Average < 0.003 / 4.83 mg/L < 0.0015 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 Months (Avg) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Max) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass /Limit Mercury - LL 02/11/2020 S Biogen021120Self 0.000005 / 0.000142 mg/L / 05/04/2020 P Biogen050420POTWH 0.000007 / 0.000142 mg/L / g Feb 2020 Week 2 0.000005 / mg/L / May 2020 Week 1 0.000007 / mg/L / Feb 2020 Average 0.000005 / mg/L / May 2020 Average 0.000007 / mg/L / 2020 Quarter 1 0.000005 / mg/L / 2020 Quarter 2 0.000007 / mg/L / 2020 1st 6 Months (Avg) 0.000006 / mg/L / 2020 1st 6 ...(Max) 0.000007 / mg/L / 2020 1st 6 ...(Min) 0.000005 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Methylene Chloride 01/28/2020 P Biogen012820POTW < 0.003 / 1.77 mg/L < 0.001474 / lbs/day Jan 2020 Week 4 < 0.003 / mg/L < 0.001474 / lbs/day Jan 2020 Average < 0.003 / 0.41 mg/L < 0.001474 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.001474 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.001474 / lbs/day 2020 1st 6 ...(Max) < 0.003 / mg/L < 0.001474 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.001474 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Molybdenum 01/28/2020 P Biogen012820POTW < 0.001 / mg/L < 0.0006 / lbs/day Jan 2020 Week 4 < 0.001 / mg/L < 0.0006 / lbs/day Jan 2020 Average < 0.001 / mg/L < 0.0006 / lbs/day 2020 Quarter 1 < 0.001 / mg/L < 0.0006 / lbs/day 2020 1st 6 Months (Avg) < 0.001 / mg/L < 0.0006 / lbs/day 2020 1st 6 ...(Max) < 0.001 / mg/L < 0.0006 / lbs/day 2020 1st 6 ...(Min) < 0.001 / mg/L < 0.0006 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass/Limit n-Amyl acetate 01/28/2020 P Biogen012820POTW < 0.003 / 12.19 mg/L < 0.0015 / lbs/day Jan 2020 Week 4 < 0.003 / mg/L < 0.0015 / lbs/day Jan 2020 Average < 0.003 / 4.83 mg/L < 0.0015 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Max) < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.0015 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Nitrate -Nitrite 02/11/2020 S Biogen021120Self 1 / mg/L 0.885 / lbs/day Feb 2020 Week 2 1 / mg/L 0.885 / lbs/day Feb 2020 Average 1 / mg/L 0.885 / lbs/day Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 2020 2020 2020 2020 2020 Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) mg/L mg/L mg/L mg/L 0.885 / 0.885 / 0.885 / 0.885 / 1 / lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 01/28/2020 02/11/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 P Biogen012820POTW S Biogen021120Self Week 4 Week 2 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 8.75 / 6.9 / 8.75 / 6.9 / 8.75 / 6.9 / 7.83 / 7.83 / 8.75 / 6.9 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 5.158 / 6.298 / 5.158 / 6.298 / 5.158 / 6.298 / 5.728 / 5.728 / 6.298 / 5.158 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 01/28/2020 02/11/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: P Biogen012820POTW S Biogen021120Self Week 4 Week 2 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 5 20.1 5 20.1 5 20.1 12.55 12.55 20.1 5 2 / 200 mg/L / 200 mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L Months Sampled : 0 0 0 0 2 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 Quarters Sampled : 1 #0/0 0.00 # Over Qt Avg C : 0 0.00 0.00 # Over Qt Avg C TRC : 0 0.00 0.00 # Over Qtr Avg M : 0 0.00 0.00 # Over Qtr Avg M TRC : 0 0.00 Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 01/28/2020 02/11/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: P Biogen012820POTW S Biogen021120Self Week 4 Week 2 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 7.6 6.8 7.6 6.8 7.6 6.8 7.2 7.2 7.6 6.8 2 / 5.5 - 10.5 / 5.5 - 10.5 Months Sampled : 0 0 0 0 SU SU SU SU SU SU SU SU SU SU 2 Weeks Sampled : 2 #0/0 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtAvg C: # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result / Limit Mass / Limit Temperature 01/28/2020 Jan 2020 Jan 2020 2020 2020 2020 2020 2020 P Biogen012820POTW Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) Sample # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: Count : 1 0 0 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 18 / 66 18 / 18 / 18 / 18 / 18 / 18 / 1 / Months Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 °C °C °C °C °C °C °C # Over Wk Avg C : # Over Wk Avg C TRC : # Over Wk Avg M : # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result / Limit Mass /Limit TKN Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN 02/11/2020 S Biogen021120Self Feb 2020 Week 2 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 5.9 / mg/L 5.9 / mg/L 5.9 / mg/L 5.9 / mg/L 5.9 / mg/L 5.9 / mg/L 5.9 / mg/L 5.385 / lbs/day 5.385 / lbs/day 5.385 / lbs/day 5.385 / lbs/day 5.385 / lbs/day 5.385 / lbs/day 5.385 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass /Limit Total Phosphorus 01/28/2020 P Biogen012820POTW 1.38 / mg/L 0.8135 / lbs/day 02/11/2020 S Biogen021120Self 1 / mg/L 0.9127 / lbs/day Jan 2020 Week 4 1.38 / mg/L 0.8135 / lbs/day Feb 2020 Week 2 1 / mg/L 0.9127 / lbs/day Jan 2020 Average 1.38 / mg/L 0.8135 / lbs/day Feb 2020 Average 1 / mg/L 0.9127 / lbs/day 2020 Quarter 1 1.19 / mg/L 0.8631 / lbs/day 2020 1st 6 Months (Avg) 1.19 / mg/L 0.8631 / lbs/day 2020 1st 6 ...(Max) 1.38 / mg/L 0.9127 / lbs/day 2020 1st 6 ...(Min) 1 / mg/L 0.8135 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit TSS 01/28/2020 P Biogen012820POTW 02/11/2020 S Biogen021120Self Jan 2020 Week 4 Feb 2020 Week 2 Jan 2020 Average Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 136 / mg/L 80.168083 / lbs/day 13.3 / mg/L 12.139304 / lbs/day 136 / mg/L 80.168083 / lbs/day 13.3 / mg/L 12.139304 / lbs/day 136 / mg/L 80.168083 / lbs/day 13.3 / mg/L 12.139304 / lbs/day 74.7 / mg/L 46.153693 / lbs/day 74.7 / mg/L 46.1537 / lbs/day 136 / mg/L 80.168083 / lbs/day 13.3 / mg/L 12.139304 / lbs/day 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit VOC 02/11/2020 S Biogen021120Self Feb 2020 Week 2 0.005 / 0.005 / mg/L mg/L Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 Biogen SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit VOC Feb 2020 Average 0.005 / mg/L 2020 Quarter 1 0.005 / mg/L 2020 1st 6 Months (Avg) 0.005 / mg/L 2020 1st 6 ...(Max) 0.005 / mg/L 2020 1st 6 ...(Min) 0.005 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit Zinc 01/28/2020 P Biogen012820POTW 1.37 / mg/L 0.807576 / lbs/day 02/11/2020 S Biogen021120Self 0.638 / mg/L 0.582321 / lbs/day Jan 2020 Week 4 1.37 / mg/L 0.807576 / lbs/day Feb 2020 Week 2 0.638 / mg/L 0.582321 / lbs/day Jan 2020 Average 1.37 / mg/L 0.807576 / lbs/day Feb 2020 Average 0.638 / mg/L 0.582321 / lbs/day 2020 Quarter 1 1.004 / mg/L 0.694949 / lbs/day 2020 1st 6 Months (Avg) 1.004 / mg/L 0.694949 / lbs/day 2020 1st 6 ...(Max) 1.37 / mg/L 0.807576 / lbs/day 2020 1st 6 ...(Min) 0.638 / mg/L 0.582321 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Wednesday, February 24, 2021 10:48:57PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 02/27/2020 S Cintas022720Se1f 0.898 / mg/L Feb 2020 Week 4 0.898 / mg/L Feb 2020 Average 0.898 / mg/L 2020 Quarter 1 0.898 / mg/L 2020 1st 6 Months (Avg) 0.898 / mg/L 2020 1st 6 ...(Max) 0.898 / mg/L 2020 1st 6 ...(Min) 0.898 / mg/L 2020 1st 6 ...(Count) 1 / 0.541216 / lbs/day 0.541216 / lbs/day 0.541216 / lbs/day 0.541216 / lbs/day 0.541216 / lbs/day 0.541216 / lbs/day 0.541216 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass /Limit Ammonia 01/03/2020 S Cintas010320Se1f 23.4 / mg/L 14.5376 / lbs/day 02/18/2020 P Cintas021820POTW 6.1 / mg/L 3.5062 / lbs/day 02/27/2020 S Cintas022720Se1f 5.9 / mg/L 3.5559 / lbs/day 03/13/2020 S Cintas031320Se1f 1.9 / mg/L 1.0292 / lbs/day 04/14/2020 S Cintas041420Se1f 1.1 / mg/L 0.5446 / lbs/day 05/12/2020 S Cintas051220Se1f 9.7 / mg/L 4.7283 / lbs/day 06/12/2020 S Cintas061220Se1f 7.4 / mg/L 3.7412 / lbs/day Jan 2020 Week 1 23.4 / mg/L 14.5376 / lbs/day Feb 2020 Week 3 6.1 / mg/L 3.5062 / lbs/day Mar 2020 Week 2 1.9 / mg/L 1.0292 / lbs/day Feb 2020 Week 4 5.9 / mg/L 3.5559 / lbs/day Apr 2020 Week 2 1.1 / mg/L 0.5446 / lbs/day May 2020 Week 2 9.7 / mg/L 4.7283 / lbs/day Jun 2020 Week 2 7.4 / mg/L 3.7412 / lbs/day Jan 2020 Average 23.4 / mg/L 14.5376 / lbs/day Feb 2020 Average 6 / mg/L 3.5311 / lbs/day Mar 2020 Average 1.9 / mg/L 1.0292 / lbs/day Apr 2020 Average 1.1 / mg/L 0.5446 / lbs/day May 2020 Average 9.7 / mg/L 4.7283 / lbs/day Jun 2020 Average 7.4 / mg/L 3.7412 / lbs/day 2020 Quarter 1 9.33 / mg/L 5.6572 / lbs/day 2020 Quarter 2 6.07 / mg/L 3.0047 / lbs/day 2020 1st 6 Months (Avg) 7.93 / mg/L 4.5204 / lbs/day 2020 1st 6 ...(Max) 23.4 / mg/L 14.5376 / lbs/day 2020 1st 6 ...(Min) 1.1 / mg/L 0.5446 / lbs/day 2020 1st 6 ...(Count) 7 / 7 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S Cintas0120F1ow 0.052694 / 0.180 MGD 02/29/2020 S Cintas0220F1ow 0.060971 / 0.180 MGD Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 1 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 03/31/2020 S Cintas0320F1ow 0.055568 / 0.180 MGD 04/30/2020 S Cintas0420F1ow 0.050403 / 0.180 MGD 05/31/2020 S Cintas0520F1ow 0.052634 / 0.180 MGD 06/30/2020 S Cintas0620F1ow 0.05954 / 0.180 MGD Jan 2020 Week 4 0.052694 / MGD Feb 2020 Week 4 0.060971 / MGD Mar 2020 Week 4 0.055568 / MGD Apr 2020 Week 4 0.050403 / MGD May 2020 Week 4 0.052634 / MGD Jun 2020 Week 4 0.05954 / MGD Jan 2020 Average 0.052694 / 0.120 MGD Feb 2020 Average 0.060971 / 0.120 MGD Mar 2020 Average 0.055568 / 0.120 MGD Apr 2020 Average 0.050403 / 0.120 MGD May 2020 Average 0.052634 / 0.120 MGD Jun 2020 Average 0.05954 / 0.120 MGD 2020 Quarter 1 0.056411 / MGD 2020 Quarter 2 0.054192 / MGD 2020 1st 6 Months (Avg) 0.055302 / MGD 2020 1st 6 ...(Max) 0.060971 / MGD 2020 1st 6 ...(Min) 0.050403 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit BOD 01/03/2020 S Cintas010320Se1f 326 / mg/L 202.532 / lbs/day 01/31/2020 P Cintas013120POTW 1150 / mg/L / 02/18/2020 P Cintas021820POTW 299 / mg/L 171.863 / lbs/day 02/27/2020 S Cintas022720Se1f 590 / mg/L 355.587 / lbs/day 03/03/2020 P Cintas030320POTW 168 / mg/L / 03/13/2020 S Cintas031320Se1f 610 / mg/L 330.416 / lbs/day 04/14/2020 S Cintas041420Se1f 152 / mg/L 75.249 / lbs/day 04/23/2020 P Cintas042320POTW 241 / mg/L / 05/05/2020 P Cintas050520POTW 371 / mg/L / Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 2 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit BOD 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f 06/16/2020 P Cintas061620POTW Jan 2020 Week 1 Jan 2020 Week 4 Feb 2020 Week 3 Feb 2020 Week 4 Mar 2020 Week 1 Mar 2020 Week 2 Apr 2020 Week 2 May 2020 Week 1 Apr 2020 Week 4 May 2020 Week 2 Jun 2020 Week 2 Jun 2020 Week 3 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 279 / mg/L 323 / mg/L 314 / mg/L 136 / lbs/day 163.299 / lbs/day 326 / mg/L 202.532 / lbs/day 1150 / mg/L 299 / mg/L 171.863 / lbs/day 590 / mg/L 355.587 / lbs/day 168 / mg/L 610 / mg/L 330.416 / lbs/day 152 / mg/L 75.249 / lbs/day 371 / mg/L 241 / mg/L 279 / mg/L 136 / lbs/day 323 / mg/L 163.299 / lbs/day 314 / mg/L 738 / mg/L 202.532 / lbs/day 444.5 / mg/L 263.725 / lbs/day 389 / mg/L 330.416 / lbs/day 196.5 / mg/L 75.249 / lbs/day 325 / mg/L 136 / lbs/day 318.5 / mg/L 163.299 / lbs/day 523.8 / mg/L 265.1 / lbs/day 280 / mg/L 124.85 / lbs/day 401.9 / mg/L 204.993 / lbs/day 1150 / mg/L 355.587 / lbs/day 152 / mg/L 12 / 7 / Sample Date SamplelD Result/Limit Mass/Limit Cadmium 02/27/2020 S Cintas022720Se1f 0.0012 / mg/L 0.000723 / lbs/day Feb 2020 Week 4 0.0012 / mg/L 0.000723 / lbs/day Feb 2020 Average 0.0012 / mg/L 0.000723 / lbs/day 2020 Quarter 1 0.0012 / mg/L 0.000723 / lbs/day 2020 1st 6 Months (Avg) 0.0012 / mg/L 0.000723 / lbs/day 2020 1st 6 ...(Max) 0.0012 / mg/L 0.000723 / lbs/day 2020 1st 6 ...(Min) 0.0012 / mg/L 0.000723 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Chloride 01/03/2020 S Cintas010320Se1f 125 / mg/L 77.6579 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 3 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chloride 02/18/2020 P Cintas021820POTW 116 / mg/L Jan 2020 Week 1 125 / mg/L Feb 2020 Week 3 116 / mg/L Jan 2020 Average 125 / mg/L Feb 2020 Average 116 / mg/L 2020 Quarter 1 120.5 / mg/L 2020 1st 6 Months (Avg) 120.5 / mg/L 2020 1st 6 ...(Max) 125 / mg/L 2020 1st 6 ...(Min) 116 / mg/L 2020 1st 6 ...(Count) 2 / 66.676 / lbs/day 77.6579 / lbs/day 66.676 / lbs/day 77.6579 / lbs/day 66.676 / lbs/day 72.1669 / lbs/day 72.1669 / lbs/day 77.6579 / lbs/day 66.6760 / lbs/day 2 / Sample Date SamplelD Result/Limit Mass/Limit Chromium 01/03/2020 S Cintas010320Se1f < 0.003 / mg/L < 0.001553 / lbs/day 02/27/2020 S Cintas022720Se1f 0.006 / mg/L 0.003496 / lbs/day 03/13/2020 S Cintas031320Se1f 0.006 / mg/L 0.003196 / lbs/day 04/14/2020 S Cintas041420Se1f < 0.003 / mg/L < 0.001238 / lbs/day 05/12/2020 S Cintas051220Se1f 0.006 / mg/L 0.002876 / lbs/day 06/12/2020 S Cintas061220Se1f 0.007 / mg/L 0.003539 / lbs/day Jan 2020 Week 1 < 0.003 / mg/L < 0.001553 / lbs/day Feb 2020 Week 4 0.006 / mg/L 0.003496 / lbs/day Mar 2020 Week 2 0.006 / mg/L 0.003196 / lbs/day Apr 2020 Week 2 < 0.003 / mg/L < 0.001238 / lbs/day May 2020 Week 2 0.006 / mg/L 0.002876 / lbs/day Jun 2020 Week 2 0.007 / mg/L 0.003539 / lbs/day Jan 2020 Average < 0.003 / mg/L < 0.001553 / lbs/day Feb 2020 Average 0.006 / mg/L 0.003496 / lbs/day Mar 2020 Average 0.006 / mg/L 0.003196 / lbs/day Apr 2020 Average < 0.003 / mg/L < 0.001238 / lbs/day May 2020 Average 0.006 / mg/L 0.002876 / lbs/day Jun 2020 Average 0.007 / mg/L 0.003539 / lbs/day 2020 Quarter 1 < 0.005 / mg/L < 0.002748 / lbs/day 2020 Quarter 2 < 0.005 / mg/L < 0.002551 / lbs/day 2020 1st 6 Months (Avg) < 0.005 / mg/L < 0.002650 / lbs/day 2020 1st 6 ...(Max) 0.007 / mg/L 0.003539 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.001238 / lbs/day 2020 1st 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass/Limit Copper 01/03/2020 S Cintas010320Se1f 02/27/2020 S Cintas022720Se1f 0.089 / mg/L 0.055292 / lbs/day 0.064 / mg/L 0.038813 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 4 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Copper 03/13/2020 S Cintas031320Se1f 0.052 04/14/2020 S Cintas041420Se1f 0.042 05/12/2020 S Cintas051220Se1f 0.12 06/12/2020 S Cintas061220Se1f 0.094 Jan 2020 Week 1 0.089 Feb 2020 Week 4 0.064 Mar 2020 Week 2 0.052 Apr 2020 Week 2 0.042 May 2020 Week 2 0.12 Jun 2020 Week 2 0.094 Jan 2020 Average 0.089 Feb 2020 Average 0.064 Mar 2020 Average 0.052 Apr 2020 Average 0.042 May 2020 Average 0.12 Jun 2020 Average 0.094 2020 Quarter 1 0.068 2020 Quarter 2 0.085 2020 1st 6 Months (Avg) 0.077 2020 1st 6 ...(Max) 0.12 2020 1st 6 ...(Min) 0.042 2020 1st 6 ...(Count) 6 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.028167 / lbs/day 0.020793 / lbs/day 0.058495 / lbs/day 0.047524 / lbs/day 0.055292 / lbs/day 0.038813 / lbs/day 0.028167 / lbs/day 0.020793 / lbs/day 0.058495 / lbs/day 0.047524 / lbs/day 0.055292 / lbs/day 0.038813 / lbs/day 0.028167 / lbs/day 0.020793 / lbs/day 0.058495 / lbs/day 0.047524 / lbs/day 0.040757 / lbs/day 0.04227 / lbs/day 0.041514 / lbs/day 0.058495 / lbs/day 0.020793 / lbs/day 6 / Sample Date SamplelD Result/Limit Mass/Limit Fluoride 01/03/2020 S Cintas010320Se1f < 0.05 / mg/L < 0.0311 / lbs/day 02/18/2020 P Cintas021820POTW 0.2 / mg/L 0.115 / lbs/day 02/27/2020 S Cintas022720Se1f < 0.05 / mg/L < 0.0301 / lbs/day 03/13/2020 S Cintas031320Se1f < 0.05 / mg/L < 0.0271 / lbs/day 04/14/2020 S Cintas041420Se1f 0.31 / mg/L 0.1535 / lbs/day 05/12/2020 S Cintas051220Se1f < 0.05 / mg/L < 0.0244 / lbs/day 06/12/2020 S Cintas061220Se1f < 0.05 / mg/L < 0.0253 / lbs/day Jan 2020 Week 1 < 0.05 / mg/L < 0.0311 / lbs/day Feb 2020 Week 3 0.2 / mg/L 0.115 / lbs/day Feb 2020 Week 4 < 0.05 / mg/L < 0.0301 / lbs/day Mar 2020 Week 2 < 0.05 / mg/L < 0.0271 / lbs/day Apr 2020 Week 2 0.31 / mg/L 0.1535 / lbs/day May 2020 Week 2 < 0.05 / mg/L < 0.0244 / lbs/day Jun 2020 Week 2 < 0.05 / mg/L < 0.0253 / lbs/day Jan 2020 Average < 0.05 / mg/L < 0.0311 / lbs/day Feb 2020 Average < 0.13 / mg/L < 0.0725 / lbs/day Mar 2020 Average < 0.05 / mg/L < 0.0271 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 5 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Fluoride Apr 2020 Average 0.31 / mg/L 0.1535 / lbs/day May 2020 Average < 0.05 / mg/L < 0.0244 / lbs/day Jun 2020 Average < 0.05 / mg/L < 0.0253 / lbs/day 2020 Quarter 1 < 0.09 / mg/L < 0.0508 / lbs/day 2020 Quarter 2 < 0.14 / mg/L < 0.0677 / lbs/day 2020 1st 6 Months (Avg) < 0.11 / mg/L < 0.0581 / lbs/day 2020 1st 6 ...(Max) 0.31 / mg/L 0.1535 / lbs/day 2020 1st 6 ...(Min) < 0.05 / mg/L < 0.0244 / lbs/day 2020 1st 6 ...(Count) 7 / 7 / Sample Date SamplelD Result/Limit Mass/Limit Lead 01/03/2020 S Cintas010320Se1f 0.011 / mg/L 0.006834 / lbs/day 02/27/2020 S Cintas022720Se1f 0.0108 / mg/L 0.006509 / lbs/day 03/13/2020 S Cintas031320Se1f 0.011 / mg/L 0.005958 / lbs/day 04/14/2020 S Cintas041420Se1f < 0.0025 / mg/L < 0.001238 / lbs/day 05/12/2020 S Cintas051220Se1f 0.012 / mg/L 0.005849 / lbs/day 06/12/2020 S Cintas061220Se1f 0.016 / mg/L 0.008089 / lbs/day Jan 2020 Week 1 0.011 / mg/L 0.006834 / lbs/day Feb 2020 Week 4 0.0108 / mg/L 0.006509 / lbs/day Mar 2020 Week 2 0.011 / mg/L 0.005958 / lbs/day Apr 2020 Week 2 < 0.0025 / mg/L < 0.001238 / lbs/day May 2020 Week 2 0.012 / mg/L 0.005849 / lbs/day Jun 2020 Week 2 0.016 / mg/L 0.008089 / lbs/day Jan 2020 Average 0.011 / mg/L 0.006834 / lbs/day Feb 2020 Average 0.0108 / mg/L 0.006509 / lbs/day Mar 2020 Average 0.011 / mg/L 0.005958 / lbs/day Apr 2020 Average < 0.0025 / mg/L < 0.001238 / lbs/day May 2020 Average 0.012 / mg/L 0.005849 / lbs/day Jun 2020 Average 0.016 / mg/L 0.008089 / lbs/day 2020 Quarter 1 0.0109 / mg/L 0.006434 / lbs/day 2020 Quarter 2 < 0.0102 / mg/L < 0.005059 / lbs/day 2020 1st 6 Months (Avg) < 0.0106 / mg/L < 0.005746 / lbs/day 2020 1st 6 ...(Max) 0.016 / mg/L 0.008089 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.001238 / lbs/day 2020 1st 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass/Limit Mercury 03/25/2020 S Cintas032520Se1fHg 0 / mg/L Mar 2020 Week 4 0 / mg/L Mar 2020 Average 0 / mg/L Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 6 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury 2020 Quarter 1 0 / mg/L 2020 1st 6 Months (Avg) 0.00000 / mg/L 2020 1st 6 ...(Max) 0.00000 / mg/L 2020 1st 6 ...(Min) 0.00000 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 01/03/2020 S Cintas010320Se1f 0 / mg/L 0.0193 / lbs/day 02/27/2020 S Cintas022720Se1f 0 / mg/L 0.0294 / lbs/day 03/13/2020 S Cintas031320Se1f 0 / mg/L 0.0157 / lbs/day 04/14/2020 S Cintas041420Se1f 0 / mg/L 0.0109 / lbs/day 05/12/2020 S Cintas051220Se1f 0 / mg/L 0.0102 / lbs/day 06/12/2020 S Cintas061220Se1f 0 / mg/L 0.0116 / lbs/day Jan 2020 Week 1 0 / mg/L 0.0193 / lbs/day Feb 2020 Week 4 0 / mg/L 0.0294 / lbs/day Mar 2020 Week 2 0 / mg/L 0.0157 / lbs/day Apr 2020 Week 2 0 / mg/L 0.0109 / lbs/day May 2020 Week 2 0 / mg/L 0.0102 / lbs/day Jun 2020 Week 2 0 / mg/L 0.0116 / lbs/day Jan 2020 Average 0 / mg/L 0.0193 / lbs/day Feb 2020 Average 0 / mg/L 0.0294 / lbs/day Mar 2020 Average 0 / mg/L 0.0157 / lbs/day Apr 2020 Average 0 / mg/L 0.0109 / lbs/day May 2020 Average 0 / mg/L 0.0102 / lbs/day Jun 2020 Average 0 / mg/L 0.0116 / lbs/day 2020 Quarter 1 0 / mg/L 0.0215 / lbs/day 2020 Quarter 2 0 / mg/L 0.0109 / lbs/day 2020 1st 6 Months (Avg) 0.029 / mg/L 0.0162 / lbs/day 2020 1st 6 ...(Max) 0.049 / mg/L 0.0294 / lbs/day 2020 1st 6 ...(Min) 0.021 / mg/L 0.0102 / lbs/day 2020 1st 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass /Limit Nickel 01/03/2020 S Cintas010320Se1f 02/27/2020 S Cintas022720Se1f 03/13/2020 S Cintas031320Se1f 04/14/2020 S Cintas041420Se1f 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f Jan 2020 Week 1 0.013 / mg/L 0.008076 / lbs/day 0.0194 / mg/L 0.011692 / lbs/day 0.022 / mg/L 0.011917 / lbs/day 0.022 / mg/L 0.010891 / lbs/day 0.021 / mg/L 0.010237 / lbs/day 0.024 / mg/L 0.012134 / lbs/day 0.013 / mg/L 0.008076 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 7 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nickel Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 Jan 2020 Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 2020 2020 2020 2020 2020 2020 Week 4 Week 2 Week 2 Week 2 Week 2 Average Average Average Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.0194 0.022 0.022 0.021 0.024 0.013 0.0194 0.022 0.022 0.021 0.024 0.0181 0.0223 0.0202 0.024 0.013 6 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.011692 0.011917 0.010891 0.010237 0.012134 0.008076 0.011692 0.011917 0.010891 0.010237 0.012134 0.010562 0.011087 0.010825 0.012134 0.008076 6 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 01/03/2020 02/18/2020 02/27/2020 03/13/2020 04/14/2020 05/12/2020 06/12/2020 Jan 2020 Feb 2020 Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 Jan 2020 Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 2020 2020 S Cintas010320Se1f P Cintas021820POTW S Cintas022720Se1f S Cintas031320Se1f S Cintas041420Se1f S Cintas051220Se1f S Cintas061220Se1f Week 1 Week 3 Week 4 Week 2 Week 2 Week 2 Week 2 Average Average Average Average Average Average Quarter 1 Quarter 2 0 / 0.1 / 0 / 0 / 0.1 / 0 / 0 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.056 0.057 0.029 0.031 0.01 0.097 0.042 0.056 0.057 0.029 0.031 0.01 0.097 0.042 0.056 0.043 0.031 0.01 0.097 0.042 0.043 0.05 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 8 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 2020 2020 2020 2020 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.1 / 0.2 / 0.0 / 7 / mg/L mg/L mg/L 0.046 / 0.097 / 0.010 / 7 / lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit Nitrogen, Total 01/03/2020 02/27/2020 03/13/2020 04/14/2020 05/12/2020 06/12/2020 Jan 2020 Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 Jan 2020 Feb 2020 Mar 2020 Apr 2020 May 2020 Jun 2020 2020 2020 2020 2020 2020 2020 S Cintas010320Se1f S Cintas022720Se1f S Cintas031320Se1f S Cintas041420Se1f S Cintas051220Se1f S Cintas061220Se1f Week 1 Week 4 Week 2 Week 2 Week 2 Week 2 Average Average Average Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 67.4 / 17.2 / 12.2 / 7 / 39.4 / 19.8 / 67.4 / 17.2 / 12.2 / 7 / 39.4 / 19.8 / 67.4 / 17.2 / 12.2 / 7 / 39.4 / 19.8 / 32.27 / 22.07 / 27.17 / 67.4 / 7 / 6 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 41.873 / 10.366 / 6.608 / 3.465 / 19.206 / 10.01 / 41.873 / 10.366 / 6.608 / 3.465 / 19.206 / 10.01 / 41.873 / 10.366 / 6.608 / 3.465 / 19.206 / 10.01 / 19.616 / 10.894 / 15.255 / 41.873 / 3.465 / 6/ lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, HEM (Polar) 01/03/2020 S Cintas010320Se1f 02/18/2020 P Cintas021820POTW 02/27/2020 S Cintas022720Se1f 03/13/2020 S Cintas031320Se1f 04/14/2020 S Cintas041420Se1f 04/23/2020 S Cintas042320Se1f 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f 32.5 / 100 2.5 / 100 45.7 / 100 221 / 100 7.5 / 100 12.8 / 100 18.1 / 100 54.9 / 100 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 20.191057 / 1.436982 / 27.542938 / * * 119.708257 / 3.712968 / 5.091643 / 8.822959 / 27.755837 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 9 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, HEM (Polar) Jan 2020 Week 1 32.5 / mg/L 20.191057 / lbs/day Feb 2020 Week 3 < 2.5 / mg/L < 1.436982 / lbs/day Feb 2020 Week 4 45.7 / mg/L 27.542938 / lbs/day Mar 2020 Week 2 221 / mg/L 119.708257 / lbs/day Apr 2020 Week 2 7.5 / mg/L 3.712968 / lbs/day Apr 2020 Week 4 12.8 / mg/L 5.091643 / lbs/day May 2020 Week 2 18.1 / mg/L 8.822959 / lbs/day Jun 2020 Week 2 54.9 / mg/L 27.755837 / lbs/day Jan 2020 Average 32.5 / mg/L 20.191057 / lbs/day Feb 2020 Average < 24.1 / mg/L < 14.48996 / lbs/day Mar 2020 Average 221 / mg/L 119.708257 / lbs/day Apr 2020 Average 10.2 / mg/L 4.402306 / lbs/day May 2020 Average 18.1 / mg/L 8.822959 / lbs/day Jun 2020 Average 54.9 / mg/L 27.755837 / lbs/day 2020 Quarter 1 < 75.4 / mg/L < 42.219808 / lbs/day 2020 Quarter 2 23.3 / mg/L 11.345852 / lbs/day 2020 1st 6 Months (Avg) < 49.4 / mg/L < 26.7828 / lbs/day 2020 1st 6 ...(Max) 221 / mg/L 119.708257 / lbs/day 2020 1st 6 ...(Min) < 2.5 / mg/L < 1.436982 / lbs/day 2020 1st 6 ...(Count) 8 / 8 / Sample Count : 8 Months Sampled : 6 Weeks Sampled : 8 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 1 12.50 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 1 12.50 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Oil & Grease, SGT-HEM (Non -Polar) 01/03/2020 S Cintas010320Se1f 10.4 / 100 mg/L 6.4611 / lbs/day 02/18/2020 P Cintas021820POTW < 2.5 / 100 mg/L < 1.437 / lbs/day 02/27/2020 S Cintas022720Se1f 11.4 / 100 mg/L 6.8707 / lbs/day 03/13/2020 S Cintas031320Se1f 45.3 / 100 mg/L 24.5375 / lbs/day 04/14/2020 S Cintas041420Se1f < 2.5 / 100 mg/L < 1.2377 / lbs/day 04/23/2020 S Cintas042320Se1f < 2.5 / 100 mg/L < 0.9945 / lbs/day 05/12/2020 S Cintas051220Se1f 5.5 / 100 mg/L 2.681 / lbs/day 06/12/2020 S Cintas061220Se1f 13.6 / 100 mg/L 6.8758 / lbs/day Jan 2020 Week 1 10.4 / mg/L 6.4611 / lbs/day Feb 2020 Week 3 < 2.5 / mg/L < 1.437 / lbs/day Feb 2020 Week 4 11.4 / mg/L 6.8707 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 10 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, SGT-HEM (Non -Polar) Mar 2020 Week 2 45.3 / mg/L 24.5375 / lbs/day Apr 2020 Week 2 < 2.5 / mg/L < 1.2377 / lbs/day Apr 2020 Week 4 < 2.5 / mg/L < 0.9945 / lbs/day May 2020 Week 2 5.5 / mg/L 2.681 / lbs/day Jun 2020 Week 2 13.6 / mg/L 6.8758 / lbs/day Jan 2020 Average 10.4 / mg/L 6.4611 / lbs/day Feb 2020 Average < 7 / mg/L < 4.1538 / lbs/day Mar 2020 Average 45.3 / mg/L 24.5375 / lbs/day Apr 2020 Average < 2.5 / mg/L < 1.1161 / lbs/day May 2020 Average 5.5 / mg/L 2.681 / lbs/day Jun 2020 Average 13.6 / mg/L 6.8758 / lbs/day 2020 Quarter 1 < 17.4 / mg/L < 9.8266 / lbs/day 2020 Quarter 2 < 6 / mg/L < 2.9472 / lbs/day 2020 1st 6 Months (Avg) < 11.7 / mg/L < 6.3869 / lbs/day 2020 1st 6 ...(Max) 45.3 / mg/L 24.5375 / lbs/day 2020 1st 6 ...(Min) < 2.5 / mg/L < 0.9945 / lbs/day 2020 1st 6 ...(Count) 8 / 8 / Sample Count : 8 Months Sampled : 6 Weeks Sampled : 8 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 01/03/2020 S Cintas010320Se1f 7.2 / 6.0 - 10.5 SU / 02/18/2020 P Cintas021820POTW 7.2 / 6.0 - 10.5 SU / 02/27/2020 S Cintas022720Se1f 6.5 / 6.0 - 10.5 SU / 03/13/2020 S Cintas031320Se1f 6.8 / 6.0 - 10.5 SU / 03/25/2020 S Cintas032520SelfHg 6.9 / 6.0 - 10.5 SU / 04/14/2020 S Cintas041420Se1f 7.1 / 6.0 - 10.5 SU / 04/23/2020 S Cintas042320Se1f 7 / 6.0 - 10.5 SU / 05/12/2020 S Cintas051220Se1f 7.1 / 6.0 - 10.5 SU / 06/12/2020 S Cintas061220Se1f 7.1 / 6.0 - 10.5 SU / Jan 2020 Week 1 7.2 / SU / Feb 2020 Week 3 7.2 / SU / Feb 2020 Week 4 6.5 / SU / Mar 2020 Week 2 6.8 / SU / Mar 2020 Week 4 6.9 / SU / Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 11 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH Apr 2020 Week 2 Apr 2020 Week 4 May 2020 Week 2 Jun 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 7.1 7 7.1 7.1 7.2 6.85 6.85 7.05 7.1 7.1 6.92 7.08 6.99 7.2 6.5 9 SU SU SU SU SU SU SU SU SU SU SU SU SU SU SU Sample Count : 9 Months Sampled : 6 Weeks Sampled : 9 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Silver 02/27/2020 S Cintas022720Se1f < 0.0025 / mg/L < 0.001507 / lbs/day Feb 2020 Week 4 < 0.0025 / mg/L < 0.001507 / lbs/day Feb 2020 Average < 0.0025 / mg/L < 0.001507 / lbs/day 2020 Quarter 1 < 0.0025 / mg/L < 0.001507 / lbs/day 2020 1st 6 Months (Avg) < 0.0025 / mg/L < 0.001507 / lbs/day 2020 1st 6 ...(Max) < 0.0025 / mg/L < 0.001507 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.001507 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Temperature 01/03/2020 S Cintas010320Se1f 27.2 / 66 °C 02/18/2020 P Cintas021820POTW 22.8 / 66 °C 02/27/2020 S Cintas022720Se1f 27.9 / 66 °C 03/13/2020 S Cintas031320Se1f 30.7 / 66 °C Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 12 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Temperature 03/25/2020 S Cintas032520Se1fHg 04/14/2020 S Cintas041420Se1f 04/23/2020 S Cintas042320Se1f 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f Jan 2020 Week 1 Feb 2020 Week 3 Feb 2020 Week 4 Mar 2020 Week 2 Mar 2020 Week 4 Apr 2020 Week 2 Apr 2020 Week 4 May 2020 Week 2 Jun 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 30 / 66 °C 31.7 / 66 °C 31.2 / 66 °C 31.9 / 66 °C 34.3 / 66 °C 27.2 / °C 22.8 / °C 27.9 / °C 30.7 / °C 30 / °C 31.7 / °C 31.2 / °C 31.9 / °C 34.3 / °C 27.2 / °C 25.4 / °C 30.4 / °C 31.5 / °C 31.9 / °C 34.3 / °C 27.7 / °C 32.3 / °C 29.7 / °C 34.3 / °C 22.8 / °C 9 / Sample Count : 9 Months Sampled : 6 Weeks Sampled : 9 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit TKN 01/03/2020 S Cintas010320Se1f 67.3 / mg/L 41.811 / lbs/day 01/31/2020 P Cintas013120POTW 55.8 / mg/L / 02/18/2020 P Cintas021820POTW 22.3 / mg/L 12.818 / lbs/day 02/27/2020 S Cintas022720Se1f 17.2 / mg/L 10.366 / lbs/day 03/03/2020 P Cintas030320POTW 185 / mg/L / Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 13 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN 03/13/2020 S Cintas031320Se1f 04/14/2020 S Cintas041420Se1f 04/23/2020 P Cintas042320POTW 05/05/2020 P Cintas050520POTW 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f 06/16/2020 P Cintas061620POTW Jan 2020 Week 1 Jan 2020 Week 4 Feb 2020 Week 3 Feb 2020 Week 4 Mar 2020 Week 1 Mar 2020 Week 2 Apr 2020 Week 2 Apr 2020 Week 4 May 2020 Week 1 May 2020 Week 2 Jun 2020 Week 2 Jun 2020 Week 3 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 12.1 / mg/L 7 / mg/L 14.1 / mg/L 21.7 / mg/L 39.2 / mg/L 19.7 / mg/L 34.2 / mg/L 67.3 / mg/L 55.8 / mg/L 22.3 / mg/L 17.2 / mg/L 185 / mg/L 12.1 / mg/L 7 / mg/L 14.1 / mg/L 21.7 / mg/L 39.2 / mg/L 19.7 / mg/L 34.2 / mg/L 61.55 / mg/L 19.75 / mg/L 98.55 / mg/L 10.55 / mg/L 30.45 / mg/L 26.95 / mg/L 59.95 / mg/L 22.65 / mg/L 41.3 / mg/L 185 / mg/L 7 / mg/L 12 / 6.554 / lbs/day 3.465 / lbs/day 19.108 / lbs/day 9.96 / lbs/day 41.811 / lbs/day 12.818 / lbs/day 10.366 / lbs/day 6.554 / lbs/day 3.465 / lbs/day 19.108 / lbs/day 9.96 / lbs/day 41.811 / lbs/day 11.592 / lbs/day 6.554 / lbs/day 3.465 / lbs/day 19.108 / lbs/day 9.96 / lbs/day 17.887 / lbs/day 10.844 / lbs/day 14.869 / lbs/day 41.811 / lbs/day 7 / Sample Date SamplelD Result/Limit Mass/Limit Total Phosphorus 01/03/2020 S Cintas010320Se1f 6.6 / mg/L 4.1003 / lbs/day 01/31/2020 P Cintas013120POTW 5.71 / mg/L / 02/18/2020 P Cintas021820POTW 2.25 / mg/L 1.2933 / lbs/day 02/27/2020 S Cintas022720Se1f 1.7 / mg/L 1.0246 / lbs/day 03/03/2020 P Cintas030320POTW 10.8 / mg/L / 03/13/2020 S Cintas031320Se1f 1.3 / mg/L 0.7042 / lbs/day 04/14/2020 S Cintas041420Se1f 0.37 / mg/L 0.1832 / lbs/day 04/23/2020 P Cintas042320POTW 1.16 / mg/L / Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 14 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 05/05/2020 P Cintas050520POTW 2.3 / mg/L 05/12/2020 S Cintas051220Se1f 2.9 / mg/L 06/12/2020 S Cintas061220Se1f 2.5 / mg/L 06/16/2020 P Cintas061620POTW 3.33 / mg/L Jan 2020 Week 1 6.6 / mg/L Jan 2020 Week 4 5.71 / mg/L Feb 2020 Week 3 2.25 / mg/L Feb 2020 Week 4 1.7 / mg/L Mar 2020 Week 1 10.8 / mg/L Mar 2020 Week 2 1.3 / mg/L Apr 2020 Week 2 0.37 / mg/L Apr 2020 Week 4 1.16 / mg/L May 2020 Week 1 2.3 / mg/L May 2020 Week 2 2.9 / mg/L Jun 2020 Week 2 2.5 / mg/L Jun 2020 Week 3 3.33 / mg/L Jan 2020 Average 6.155 / mg/L Feb 2020 Average 1.975 / mg/L Mar 2020 Average 6.05 / mg/L Apr 2020 Average 0.765 / mg/L May 2020 Average 2.6 / mg/L Jun 2020 Average 2.915 / mg/L 2020 Quarter 1 4.727 / mg/L 2020 Quarter 2 2.093 / mg/L 2020 1st 6 Months (Avg) 3.41 / mg/L 2020 1st 6 ...(Max) 10.8 / mg/L 2020 1st 6 ...(Min) 0.37 / mg/L 2020 1st 6 ...(Count) 12 / 1.4136 / lbs/day 1.2639 / lbs/day 4.1003 / lbs/day 1.2933 / lbs/day 1.0246 / lbs/day 0.7042 / lbs/day 0.1832 / lbs/day 1.4136 / lbs/day 1.2639 / lbs/day 4.1003 / lbs/day 1.1589 / lbs/day 0.7042 / lbs/day 0.1832 / lbs/day 1.4136 / lbs/day 1.2639 / lbs/day 1.7806 / lbs/day 0.9536 / lbs/day 1.4262 / lbs/day 4.1003 / lbs/day 7 / Sample Date SamplelD Result/Limit Mass /Limit TSS 01/03/2020 S Cintas010320Se1f 108 / mg/L 67.096434 / lbs/day 01/31/2020 P Cintas013120POTW 1416 / mg/L / 02/18/2020 P Cintas021820POTW 116 / mg/L 66.675965 / lbs/day 02/27/2020 S Cintas022720Se1f 226 / mg/L 136.207963 / lbs/day 03/03/2020 P Cintas030320POTW 43 / mg/L / 03/13/2020 S Cintas031320Se1f 242 / mg/L 131.083249 / lbs/day 04/14/2020 S Cintas041420Se1f 41.3 / mg/L 20.446077 / lbs/day 04/23/2020 P Cintas042320POTW 84 / mg/L / 05/05/2020 P Cintas050520POTW 48 / mg/L / 05/12/2020 S Cintas051220Se1f 179 / mg/L 87.254681 / lbs/day 06/12/2020 S Cintas061220Se1f 50.4 / mg/L 25.480768 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 15 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TSS 06/16/2020 P Cintas061620POTW 774 / mg/L Jan 2020 Week 1 108 / mg/L Jan 2020 Week 4 1416 / mg/L Feb 2020 Week 3 116 / mg/L Feb 2020 Week 4 226 / mg/L Mar 2020 Week 1 43 / mg/L Mar 2020 Week 2 242 / mg/L Apr 2020 Week 2 41.3 / mg/L Apr 2020 Week 4 84 / mg/L May 2020 Week 1 48 / mg/L May 2020 Week 2 179 / mg/L Jun 2020 Week 2 50.4 / mg/L Jun 2020 Week 3 774 / mg/L Jan 2020 Average 762 / mg/L Feb 2020 Average 171 / mg/L Mar 2020 Average 142.5 / mg/L Apr 2020 Average 62.7 / mg/L May 2020 Average 113.5 / mg/L Jun 2020 Average 412.2 / mg/L 2020 Quarter 1 358.5 / mg/L 2020 Quarter 2 196.1 / mg/L 2020 1st 6 Months (Avg) 277.3 / mg/L 2020 1st 6 ...(Max) 1416 / mg/L 2020 1st 6 ...(Min) 41.3 / mg/L 2020 1st 6 ...(Count) 12 / 67.096434 / lbs/day 66.675965 / lbs/day 136.207963 / lbs/day 131.083249 / lbs/day 20.446077 / lbs/day 87.254681 / lbs/day 25.480768 / lbs/day 67.096434 / lbs/day 101.441964 / lbs/day 131.083249 / lbs/day 20.446077 / lbs/day 87.254681 / lbs/day 25.480768 / lbs/day 100.265903 / lbs/day 44.393842 / lbs/day 76.3207 / lbs/day 136.207963 / lbs/day 7 / Sample Date SamplelD Result / Limit Mass/Limit VOC 02/27/2020 S Cintas022720Se1f 0.0452 / mg/L / Feb 2020 Week 4 0.0452 / mg/L / Feb 2020 Average 0.0452 / mg/L / 2020 Quarter 1 0.0452 / mg/L / 2020 1st 6 Months (Avg) 0.0452 / mg/L / 2020 1st 6 ...(Max) 0.0452 / mg/L / 2020 1st 6 ...(Min) 0.0452 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result / Limit Mass/Limit Zinc 01/03/2020 S Cintas010320Se1f 0.85 / mg/L 0.528074 / lbs/day 02/27/2020 S Cintas022720Se1f 1.07 / mg/L 0.644878 / lbs/day 03/13/2020 S Cintas031320Se1f 1 / mg/L 0.541666 / lbs/day Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 16 of 17 Cintas Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc 04/14/2020 S Cintas041420Se1f 05/12/2020 S Cintas051220Se1f 06/12/2020 S Cintas061220Se1f Jan 2020 Week 1 Feb 2020 Week 4 Mar 2020 Week 2 Apr 2020 Week 2 May 2020 Week 2 Jun 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.75 / mg/L 0.85 / mg/L 1.3 / mg/L 0.85 / mg/L 1.07 / mg/L 1 / mg/L 0.75 / mg/L 0.85 / mg/L 1.3 / mg/L 0.85 / mg/L 1.07 / mg/L 1 / mg/L 0.75 / mg/L 0.85 / mg/L 1.3 / mg/L 0.973 / mg/L 0.967 / mg/L 0.97 / mg/L 1.3 / mg/L 0.75 / mg/L 6 / 0.371297 / lbs/day 0.414338 / lbs/day 0.657242 / lbs/day 0.528074 / lbs/day 0.644878 / lbs/day 0.541666 / lbs/day 0.371297 / lbs/day 0.414338 / lbs/day 0.657242 / lbs/day 0.528074 / lbs/day 0.644878 / lbs/day 0.541666 / lbs/day 0.371297 / lbs/day 0.414338 / lbs/day 0.657242 / lbs/day 0.57154 / lbs/day 0.480959 / lbs/day 0.526249 / lbs/day 0.657242 / lbs/day 0.371297 / lbs/day 6 / Wednesday, February 24, 2021 10:50:27PM * Indicates Violation ** Indicates TRC Violation Page 17 of 17 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 02/25/2020 S CreeP8022520Se1f Feb 2020 Week 4 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.22 / mg/L 0.22 / mg/L 0.22 / mg/L 0.22 / mg/L 0.22 / mg/L 0.22 / mg/L 0.22 / mg/L 0.50457 / lbs/day 0.50457 / lbs/day 0.50457 / lbs/day 0.50457 / lbs/day 0.50457 / lbs/day 0.50457 / lbs/day 0.50457 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass /Limit Ammonia 02/20/2020 P CreeP8022020POTW 24.9 / mg/L 76.6288 / lbs/day 02/25/2020 S CreeP8022520Se1f 24.2 / mg/L 55.5027 / lbs/day Feb 2020 Week 3 24.9 / mg/L 76.6288 / lbs/day Feb 2020 Week 4 24.2 / mg/L 55.5027 / lbs/day Feb 2020 Average 24.55 / mg/L 66.0657 / lbs/day 2020 Quarter 1 24.55 / mg/L 66.0657 / lbs/day 2020 1st 6 Months (Avg) 24.55 / mg/L 66.0657 / lbs/day 2020 1st 6 ...(Max) 24.9 / mg/L 76.6288 / lbs/day 2020 1st 6 ...(Min) 24.2 / mg/L 55.5027 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date Sump/ern Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S CreeP80120F1ow 0.31536 / MGD / 02/29/2020 S CreeP80220F1ow 0.329263 / MGD / 03/31/2020 S CreeP80320F1ow 0.321631 / MGD / 04/30/2020 S CreeP80420F1ow 0.306336 / MGD / 05/31/2020 S CreeP80520F1ow 0.274947 / MGD / 06/30/2020 S CreeP80620F1ow 0.37728 / MGD / Jan 2020 Week 4 0.31536 / MGD / Feb 2020 Week 4 0.329263 / MGD / Mar 2020 Week 4 0.321631 / MGD / Apr 2020 Week 4 0.306336 / MGD / May 2020 Week 4 0.274947 / MGD / Jun 2020 Week 4 0.37728 / MGD / Jan 2020 Average 0.31536 / MGD / Feb 2020 Average 0.329263 / MGD / Mar 2020 Average 0.321631 / MGD / Apr 2020 Average 0.306336 / MGD / May 2020 Average 0.274947 / MGD / Jun 2020 Average 0.37728 / MGD / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Dute SamplelD Result /Limit Mass /Limit Average Flow for Month 2020 Quarter 1 0.322085 / MGD 2020 Quarter 2 0.319521 / MGD 2020 1st 6 Months (Avg) 0.320803 / MGD 2020 1st 6 ...(Max) 0.37728 / MGD 2020 1st 6 ...(Min) 0.274947 / MGD 2020 1st 6 ...(Count) 6 / Sample Date SamplelD Result/Limit Mass/Limit Barium 02/25/2020 S CreeP8022520Se1f 0.019 / mg/L 0.0436 / lbs/day Feb 2020 Week 4 0.019 / mg/L 0.0436 / lbs/day Feb 2020 Average 0.019 / mg/L 0.0436 / lbs/day 2020 Quarter 1 0.019 / mg/L 0.0436 / lbs/day 2020 1st 6 Months (Avg) 0.019 / mg/L 0.0436 / lbs/day 2020 1st 6 ...(Max) 0.019 / mg/L 0.0436 / lbs/day 2020 1st 6 ...(Min) 0.019 / mg/L 0.0436 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Dute SamplelD Result/Limit Mass /Limit Cadmium 02/25/2020 S CreeP8022520Se1f < 0.0005 / mg/L < 0.001147 / lbs/day Feb 2020 Week 4 < 0.0005 / mg/L < 0.001147 / lbs/day Feb 2020 Average < 0.0005 / mg/L < 0.001147 / lbs/day 2020 Quarter 1 < 0.0005 / mg/L < 0.001147 / lbs/day 2020 1st 6 Months (Avg) < 0.0005 / mg/L < 0.001147 / lbs/day 2020 1st 6 ...(Max) < 0.0005 / mg/L < 0.001147 / lbs/day 2020 1st 6 ...(Min) < 0.0005 / mg/L < 0.001147 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Chloride 02/20/2020 P CreeP8022020POTW 02/25/2020 S CreeP8022520Se1f Feb 2020 Week 3 Feb 2020 Week 4 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 200 / mg/L 615.492 / lbs/day 157 / mg/L 360.0795 / lbs/day 200 / mg/L 615.492 / lbs/day 157 / mg/L 360.0795 / lbs/day 178.5 / mg/L 487.7858 / lbs/day 178.5 / mg/L 487.7858 / lbs/day 178.5 / mg/L 487.786 / lbs/day 200 / mg/L 615.492 / lbs/day 157 / mg/L 360.0795 / lbs/day 2 / 2 / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Chromium 02/25/2020 S CreeP8022520Se1f < 0.003 / mg/L < 0.005734 / lbs/day Feb 2020 Week 4 < 0.003 / mg/L < 0.005734 / lbs/day Feb 2020 Average < 0.003 / mg/L < 0.005734 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.005734 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Max) < 0.003 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Copper 02/25/2020 S CreeP8022520Se1f 0.031 / mg/L 0.071099 / lbs/day Feb 2020 Week 4 0.031 / mg/L 0.071099 / lbs/day Feb 2020 Average 0.031 / mg/L 0.071099 / lbs/day 2020 Quarter 1 0.031 / mg/L 0.071099 / lbs/day 2020 1st 6 Months (Avg) 0.031 / mg/L 0.071099 / lbs/day 2020 1st 6 ...(Max) 0.031 / mg/L 0.071099 / lbs/day 2020 1st 6 ...(Min) 0.031 / mg/L 0.071099 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Cyanide 02/20/2020 P CreeP8022020POTW < 0.003 / mg/L < 0.007694 / lbs/day 02/25/2020 S CreeP8022520Se1f < 0.004 / mg/L < 0.009174 / lbs/day Feb 2020 Week 3 < 0.003 / mg/L < 0.007694 / lbs/day Feb 2020 Week 4 < 0.004 / mg/L < 0.009174 / lbs/day Feb 2020 Average < 0.003 / mg/L < 0.008434 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.008434 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.008434 / lbs/day 2020 1st 6 ...(Max) < 0.004 / mg/L < 0.009174 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.007694 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result / Limit Mass/Limit Fluoride 02/20/2020 P CreeP8022020POTW 2.01 / mg/L 6.1857 / lbs/day 02/25/2020 S CreeP8022520Se1f 3 / mg/L 6.8805 / lbs/day Feb 2020 Week 3 2.01 / mg/L 6.1857 / lbs/day Feb 2020 Week 4 3 / mg/L 6.8805 / lbs/day Feb 2020 Average 2.51 / mg/L 6.5331 / lbs/day 2020 Quarter 1 2.51 / mg/L 6.5331 / lbs/day Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6...(Count) 2.51 / mg/L 3 / mg/L 2.01 / mg/L 2 / 6.5331 / lbs/day 6.8805 / lbs/day 6.1857 / lbs/day 2 / Sample Date SamplelD Result / Limit Mass / Limit Lead 02/25/2020 S CreeP8022520Se1f < 0.0025 / mg/L < 0.005734 / lbs/day Feb 2020 Week 4 < 0.0025 / mg/L < 0.005734 / lbs/day Feb 2020 Average < 0.0025 / mg/L < 0.005734 / lbs/day 2020 Quarter 1 < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 Months (Avg) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Max) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date Sump/ern Result / Limit Mass/Limit Mercury - LL 02/25/2020 S CreeP8022520Se1f 0.000017 / mg/L / 06/01/2020 P CreeP8060120POTW 0.000126 / mg/L / Hg Feb 2020 Week 4 0.000017 / mg/L / Jun 2020 Week 1 0.000126 / mg/L / Feb 2020 Average 0.000017 / mg/L / Jun 2020 Average 0.000126 / mg/L / 2020 Quarter 1 0.000017 / mg/L / 2020 Quarter 2 0.000126 / mg/L / 2020 1st 6 Months (Avg) 0.000072 / mg/L / 2020 1st 6 ...(Max) 0.000126 / mg/L / 2020 1st 6 ...(Min) 0.000017 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 02/25/2020 S CreeP8022520Se1f < 0.003 / mg/L < 0.0057 / lbs/day Feb 2020 Week 4 < 0.003 / mg/L < 0.0057 / lbs/day Feb 2020 Average < 0.003 / mg/L < 0.0057 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.0057 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.0057 / lbs/day 2020 1st 6 ...(Max) < 0.003 / mg/L < 0.0057 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.0057 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 4 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Nickel 02/25/2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 S CreeP8022520Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) • 0.0025 / • 0.0025 / • 0.0025 / • 0.0025 / • 0.0025 / • 0.0025 / • 0.0025 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L • 0.005734 / • 0.005734 / • 0.005734 / • 0.005734 / • 0.005734 / • 0.005734 / • 0.005734 / 1 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 02/20/2020 P CreeP8022020POTW Feb 2020 Week 3 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) mg/L mg/L mg/L mg/L mg/L mg/L mg/L 6.586 / 6.586 / 6.586 / 6.586 / 6.586 / 6.586 / 6.586 / 1 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result/Limit Mass /Limit Nitrogen, Total 02/20/2020 02/25/2020 Feb 2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 P CreeP8022020POTW S CreeP8022520Se1f Week 3 Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 30.8 / 31.5 / 30.8 / 31.5 / 31.15 / 31.15 / 31.15 / 31.5 / 30.8 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 94.786 / 72.245 / 94.786 / 72.245 / 83.516 / 83.516 / 83.516 / 94.786 / 72.245 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result/Limit Mass /Limit Oil & Grease, Total P S 02/20/2020 02/25/2020 Feb 2020 Feb 2020 Feb 2020 2020 CreeP8022020POTW CreeP8022520Se1f Week 3 Week 4 Average Quarter 1 17 / 7.5 / 17 / 7.5 / 12.25 / 12.25 / mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 5 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Dute SamplelD Result /Limit Mass /Limit Oil & Grease, Total 2020 1st 6 Months (Avg) 12.25 / mg/L 2020 1st 6 ...(Max) 17 / mg/L 2020 1st 6 ...(Min) 7.5 / mg/L 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result / Limit Mass / Limit pH 02/20/2020 P CreeP8022020POTW 02/25/2020 S CreeP8022520Se1f Feb 2020 Week 3 Feb 2020 Week 4 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 9.3 /5.0-10.5 SU / 8.3 /5.0-10.5 SU / 9.3 / SU / 8.3 / SU / 8.8 / SU / 8.8 / SU / 8.8 / SU / 9.3 / SU / 8.3 / SU / 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C: 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Dute SamplelD Result/Limit Mass /Limit Selenium 02/25/2020 S CreeP8022520Se1f < 0.005 / mg/L < 0.011468 / lbs/day Feb 2020 Week 4 < 0.005 / mg/L < 0.011468 / lbs/day Feb 2020 Average < 0.005 / mg/L < 0.011468 / lbs/day 2020 Quarter 1 < 0.005 / mg/L < 0.011468 / lbs/day 2020 1st 6 Months (Avg) < 0.005 / mg/L < 0.011468 / lbs/day 2020 1st 6 ...(Max) < 0.005 / mg/L < 0.011468 / lbs/day 2020 1st 6 ...(Min) < 0.005 / mg/L < 0.011468 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Silver 02/25/2020 S CreeP8022520Se1f < 0.0025 / mg/L < 0.005734 / lbs/day Feb 2020 Week 4 < 0.0025 / mg/L < 0.005734 / lbs/day Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 6 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Silver Feb 2020 Average < 0.0025 / mg/L < 0.005734 / lbs/day 2020 Quarter 1 < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 Months (Avg) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Max) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Min) < 0.0025 / mg/L < 0.005734 / lbs/day 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit Temperature 02/20/2020 P CreeP8022020POTW 14 / 66 °C / 02/25/2020 S CreeP8022520Se1f 18.8 / 66 °C / Feb 2020 Week 3 14 / °C / Feb 2020 Week 4 18.8 / °C / Feb 2020 Average 16.4 / °C / 2020 Quarter 1 16.4 / °C / 2020 1st 6 Months (Avg) 16.4 / °C / 2020 1st 6 ...(Max) 18.8 / °C / 2020 1st 6 ...(Min) 14 / °C / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit TKN 02/20/2020 P CreeP8022020POTW 28.7 / mg/L 88.323 / lbs/day Feb 2020 Week 3 28.7 / mg/L 88.323 / lbs/day Feb 2020 Average 28.7 / mg/L 88.323 / lbs/day 2020 Quarter 1 28.7 / mg/L 88.323 / lbs/day 2020 1st 6 Months (Avg) 28.7 / mg/L 88.323 / lbs/day 2020 1st 6 ...(Max) 28.7 / mg/L 88.323 / lbs/day 2020 1st 6 ...(Min) 28.7 / mg/L 88.323 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Total Phosphorus Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 7 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 02/20/2020 02/25/2020 Feb 2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 P CreeP8022020POTW S CreeP8022520Se1f Week 3 Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 1.62 / 1.8 / 1.62 / 1.62 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 4.9855 / 4.1283 / 4.9855 / 4.1283 / 4.5569 / 4.5569 / 4.5569 / 4.9855 / 4.1283 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result/Limit Mass /Limit VOC 02/25/2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 S CreeP8022520Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 3.7 / 3.7 / 3.7 / 3.7 / 3.7 / 3.7 / 3.7 / l / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit Zinc 02/25/2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 S CreeP8022520Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.26 / 0.26 / 0.26 / 0.26 / 0.26 / 0.26 / 0.26 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.59631 / 0.59631 / 0.59631 / 0.59631 / 0.59631 / 0.59631 / 0.59631 / 1 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 01/31/2020 S 02/29/2020 S 03/31/2020 S 04/30/2020 S CreeP90120F1ow CreeP90220F1ow CreeP90320F1ow CreeP90420F1ow 0.039444 / 0.043998 / 0.044278 / 0.045603 / MGD MGD MGD MGD Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 8 of 8 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 05/31/2020 S CreeP90520F1ow 0.051925 / MGD 06/30/2020 S CreeP90620F1ow 0.050982 / MGD Jan 2020 Week 4 0.039444 / MGD Feb 2020 Week 4 0.043998 / MGD Mar 2020 Week 4 0.044278 / MGD Apr 2020 Week 4 0.045603 / MGD May 2020 Week 4 0.051925 / MGD Jun 2020 Week 4 0.050982 / MGD Jan 2020 Average 0.039444 / MGD Feb 2020 Average 0.043998 / MGD Mar 2020 Average 0.044278 / MGD Apr 2020 Average 0.045603 / MGD May 2020 Average 0.051925 / MGD Jun 2020 Average 0.050982 / MGD 2020 Quarter 1 0.042573 / MGD 2020 Quarter 2 0.049503 / MGD 2020 1st 6 Months (Avg) 0.046038 / MGD 2020 1st 6 ...(Max) 0.051925 / MGD 2020 1st 6 ...(Min) 0.039444 / MGD 2020 1st 6 ...(Count) 6 / Sample Date SamplelD Result/Limit Mass/Limit Chloride 02/25/2020 S CreeP9022520Se1f 30.4 / mg/L / Feb 2020 Week 4 30.4 / mg/L / Feb 2020 Average 30.4 / mg/L / 2020 Quarter 1 30.4 / mg/L / 2020 1st 6 Months (Avg) 30.4 / mg/L / 2020 1st 6 ...(Max) 30.4 / mg/L / 2020 1st 6 ...(Min) 30.4 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Copper 02/25/2020 S CreeP9022520Se1f 0.019 / mg/L / Feb 2020 Week 4 0.019 / mg/L / Feb 2020 Average 0.019 / mg/L / 2020 Quarter 1 0.019 / mg/L / 2020 1st 6 Months (Avg) 0.019 / mg/L / 2020 1st 6 ...(Max) 0.019 / mg/L / 2020 1st 6 ...(Min) 0.019 / mg/L / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 02/20/2020 P CreeP9022020POTW < 0.05 / mg/L < / 02/25/2020 S CreeP9022520Se1f 0.9 / mg/L / Feb 2020 Week 3 < 0.05 / mg/L < / Feb 2020 Week 4 0.9 / mg/L / Feb 2020 Average < 0.48 / mg/L < / 2020 Quarter 1 < 0.48 / mg/L < / 2020 1st 6 Months (Avg) < 0.48 / mg/L < / 2020 1st 6 ...(Max) 0.9 / mg/L / 2020 1st 6 ...(Min) < 0.05 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 02/25/2020 S CreeP9022520Se1f 0.000006 / mg/L / 06/01/2020 P CreeP9060120POTW 0.000058 / mg/L / Hg Feb 2020 Week 4 0.000006 / mg/L / Jun 2020 Week 1 0.000058 / mg/L / Feb 2020 Average 0.000006 / mg/L / Jun 2020 Average 0.000058 / mg/L / 2020 Quarter 1 0.000006 / mg/L / 2020 Quarter 2 0.000058 / mg/L / 2020 1st 6 Months (Avg) 0.000032 / mg/L / 2020 1st 6 ...(Max) 0.000058 / mg/L / 2020 1st 6 ...(Min) 0.000006 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Muss/Limit Molybdenum 02/20/2020 P CreeP9022020POTW < 0 / mg/L < / Feb 2020 Week 3 < 0 / mg/L < / Feb 2020 Average < 0 / mg/L < / 2020 Quarter 1 < 0 / mg/L < / 2020 1st 6 Months (Avg) < 0.000 / mg/L < / 2020 1st 6 ...(Max) < 0.000 / mg/L < / 2020 1st 6 ...(Min) < 0.000 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result / Limit Mass /Limit Oil & Grease, Total 02/20/2020 P CreeP9022020POTW 02/25/2020 S CreeP9022520Se1f 19 / 9.2 / mg/L mg/L Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total Feb 2020 Week 3 Feb 2020 Week 4 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 19 / mg/L 9.2 / mg/L 14.1 / mg/L 14.1 / mg/L 14.1 / mg/L 19 / mg/L 9.2 / mg/L 2 / Sample Date SamplelD Result/Limit Mass/Limit pH 02/20/2020 P CreeP9022020POTW 02/25/2020 S CreeP9022520Se1f Feb 2020 Week 3 Feb 2020 Week 4 Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 7.4 /5.0-10.5 SU / 6.9 /5.0-10.5 SU / 7.4 / SU / 6.9 / SU / 7.2 / SU / 7.2 / SU / 7.15 / SU / 7.4 / SU / 6.9 / SU / 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Temperature 02/25/2020 S CreeP9022520Se1f 16.7 / °C Feb 2020 Week 4 16.7 / °C Feb 2020 Average 16.7 / °C 2020 Quarter 1 16.7 / °C 2020 1st 6 Months (Avg) 16.7 / °C 2020 1st 6 ...(Max) 16.7 / °C 2020 1st 6 ...(Min) 16.7 / °C 2020 1st 6 ...(Count) 1 / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: All Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 01/31/2020 S Cree0120F1ow 0.354804 / 0.600 MGD 02/29/2020 S Cree0220F1ow 0.373262 / 0.600 MGD 03/31/2020 S Cree0320F1ow 0.365909 / 0.600 MGD 04/30/2020 S Cree0420F1ow 0.351939 / 0.600 MGD 05/31/2020 S Cree0520F1ow 0.326872 / 0.600 MGD 06/30/2020 S Cree0620F1ow 0.428262 / 0.600 MGD Jan 2020 Week 4 0.354804 / MGD Feb 2020 Week 4 0.373262 / MGD Mar 2020 Week 4 0.365909 / MGD Apr 2020 Week 4 0.351939 / MGD May 2020 Week 4 0.326872 / MGD Jun 2020 Week 4 0.428262 / MGD Jan 2020 Average 0.354804 / 0.451 MGD Feb 2020 Average 0.373262 / 0.451 MGD Mar 2020 Average 0.365909 / 0.451 MGD Apr 2020 Average 0.351939 / 0.451 MGD May 2020 Average 0.326872 / 0.451 MGD Jun 2020 Average 0.428262 / 0.451 MGD 2020 Quarter 1 0.364658 / MGD 2020 Quarter 2 0.369024 / MGD 2020 1st 6 Months (Avg) 0.366841 / MGD 2020 1st 6 ...(Max) 0.428262 / MGD 2020 1st 6 ...(Min) 0.326872 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 02/25/2020 S Cree022520Se1f 2.8 / 8.0 mg/L / Feb 2020 Week 4 2.8 / mg/L / Feb 2020 Average 2.8 / 7.0 mg/L / 2020 Quarter 1 2.8 / mg/L / 2020 1st 6 Months (Avg) 2.8 / mg/L / 2020 1st 6 ...(Max) 2.8 / mg/L / 2020 1st 6 ...(Min) 2.8 / mg/L / Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3 Cree, Inc.(A11) # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: All Sample Date SamplelD Result /Limit Mass /Limit Fluoride 2020 1st 6...(Count) Sample Count : 0 0 0 0 0 0 1 % 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : Months Sampled : 0 0 0 0 1 Weeks Sampled : 1 % # % 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 % 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 02/25/2020 06/12/2020 Feb 2020 Jun 2020 Feb 2020 Jun 2020 2020 2020 2020 2020 2020 2020 S Cree022520Se1f P Cree061220POTWHg Week 4 Week 2 Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 % 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.000016 0.000118 0.000016 0.000118 0.000016 0.000118 0.000016 0.000118 0.000067 0.000118 0.000016 2 / 0.000142 mg/L / 0.000142 mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L / mg/L Months Sampled : 0 0 0 0 2 % 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 % 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 2 % 0.00 0.00 0.00 0.00 Sample Date SamplelD Result/Limit Mass /Limit Oil & Grease, Total 02/25/2020 S Feb 2020 Feb 2020 2020 2020 2020 Cree022520Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 7.7 / 200.0 7.7 / 7.7 / 7.7 / 7.7 / 7.7 / mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: All Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 7.7 / mg/L 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:51:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 02/26/2020 S CreeRTPP12022620Se 0.22 / mg/L if Feb 2020 Week 4 0.22 / mg/L Feb 2020 Average 0.22 / mg/L 2020 Quarter 1 0.22 / mg/L 2020 1st 6 Months (Avg) 0.22 / mg/L 2020 1st 6 ...(Max) 0.22 / mg/L 2020 1st 6 ...(Min) 0.22 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit Ammonia 02/26/2020 S CreeRTPP12022620Se 5.7 / mg/L / if 04/21/2020 CreeRTPP12042120P 4 / mg/L / OTW Feb 2020 Week 4 5.7 / mg/L / Apr 2020 Week 3 4 / mg/L / Feb 2020 Average 5.7 / mg/L / Apr 2020 Average 4 / mg/L / 2020 Quarter 1 5.7 / mg/L / 2020 Quarter 2 4 / mg/L / 2020 1st 6 Months (Avg) 4.85 / mg/L / 2020 1st 6 ...(Max) 5.7 / mg/L / 2020 1st 6 ...(Min) 4 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass /Limit Average Flow for Month 01/16/2020 S CreeRTPP120120F1ow 0.11754 / 0.469 MGD / 02/28/2020 S CreeRTPP120220F1ow 0.124424 / 0.469 MGD / 04/16/2020 S CreeRTPP120420F1ow 0.120519 / 0.469 MGD / 05/21/2020 S CreeRTPP120520F1ow 0.132038 / 0.469 MGD / 06/18/2020 S CreeRTPP120620F1ow 0.151028 / 0.469 MGD / Jan 2020 Week 3 0.11754 / MGD / Feb 2020 Week 4 0.124424 / MGD / Apr 2020 Week 3 0.120519 / MGD / May 2020 Week 3 0.132038 / MGD / Jun 2020 Week 3 0.151028 / MGD / Jan 2020 Average 0.11754 / 0.329 MGD / Feb 2020 Average 0.124424 / 0.329 MGD / Apr 2020 Average 0.120519 / 0.329 MGD / May 2020 Average 0.132038 / 0.329 MGD / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Jun 2020 Average 0.151028 / 0.329 MGD 2020 Quarter 1 0.120982 / MGD 2020 Quarter 2 0.134528 / MGD 2020 1st 6 Months (Avg) 0.12911 / MGD 2020 1st 6 ...(Max) 0.151028 / MGD 2020 1st 6 ...(Min) 0.11754 / MGD 2020 1st 6 ...(Count) 5 / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Barium 02/26/2020 S CreeRTPP12022620Se 0.018 / mg/L / if Feb 2020 Week 4 0.018 / mg/L / Feb 2020 Average 0.018 / mg/L / 2020 Quarter 1 0.018 / mg/L / 2020 1st 6 Months (Avg) 0.018 / mg/L / 2020 1st 6 ...(Max) 0.018 / mg/L / 2020 1st 6 ...(Min) 0.018 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result /Limit Mass /Limit Cadmium 02/26/2020 S CreeRTPP12022620Se < 0.0005 / if Feb 2020 Week 4 < 0.0005 / Feb 2020 Average < 0.0005 / 2020 Quarter 1 < 0.0005 / 2020 1st 6 Months (Avg) < 0.0005 / 2020 1st 6 ...(Max) < 0.0005 / 2020 1st 6 ...(Min) < 0.0005 / 2020 1st 6 ...(Count) 1 / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / mg/L < / Sample Date SamplelD Result/Limit Mass/Limit Chloride Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Chloride 02/26/2020 S CreeRTPP12022620Se 282 / mg/L if 04/21/2020 CreeRTPP12042120P 111 / mg/L OTW Feb 2020 Week 4 282 / mg/L Apr 2020 Week 3 111 / mg/L Feb 2020 Average 282 / mg/L Apr 2020 Average 111 / mg/L 2020 Quarter 1 282 / mg/L 2020 Quarter 2 111 / mg/L 2020 1st 6 Months (Avg) 196.5 / mg/L 2020 1st 6 ...(Max) 282 / mg/L 2020 1st 6 ...(Min) 111 / mg/L 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result / Limit Mass /Limit Chromium 02/26/2020 S CreeRTPP12022620Se < 0.003 / mg/L < / if Feb 2020 Week 4 < 0.003 / mg/L < / Feb 2020 Average < 0.003 / mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.003 / mg/L < / 2020 1st 6 ...(Max) < 0.003 / mg/L < / 2020 1st 6 ...(Min) < 0.003 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Copper 02/26/2020 S CreeRTPP12022620Se 0.032 / mg/L / if Feb 2020 Week 4 0.032 / mg/L / Feb 2020 Average 0.032 / mg/L / 2020 Quarter 1 0.032 / mg/L / 2020 1st 6 Months (Avg) 0.032 / mg/L / 2020 1st 6 ...(Max) 0.032 / mg/L / 2020 1st 6 ...(Min) 0.032 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Cyanide 02/26/2020 S CreeRTPP12022620Se < 0.004 / if mg/L Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 3 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Cyanide 04/21/2020 CreeRTPP12042120P < 0.003 / mg/L < / OTW Feb 2020 Week 4 < 0.004 / mg/L < / Apr 2020 Week 3 < 0.003 / mg/L < / Feb 2020 Average < 0.004 / mg/L < / Apr 2020 Average < 0.003 / mg/L < / 2020 Quarter 1 < 0.004 / mg/L < / 2020 Quarter 2 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.003 / mg/L < / 2020 1st 6 ...(Max) < 0.004 / mg/L < / 2020 1st 6 ...(Min) < 0.003 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Fluoride 02/26/2020 S CreeRTPP12022620Se 1.8 / 8.0 mg/L if 04/21/2020 CreeRTPP12042120P 1.38 / 8.0 mg/L OTW Feb 2020 Week 4 1.8 / mg/L Apr 2020 Week 3 1.38 / mg/L Feb 2020 Average 1.8 / 7.0 mg/L Apr 2020 Average 1.38 / 7.0 mg/L 2020 Quarter 1 1.8 / mg/L 2020 Quarter 2 1.38 / mg/L 2020 1st 6 Months (Avg) 1.59 / mg/L 2020 1st 6 ...(Max) 1.8 / mg/L 2020 1st 6 ...(Min) 1.38 / mg/L 2020 1st 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Lead 02/26/2020 S CreeRTPP12022620Se < 0.0025 / if Feb 2020 Week 4 < 0.0025 / mg/L mg/L Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Lead Feb 2020 Average < 0.0025 / mg/L < / 2020 Quarter 1 < 0.0025 / mg/L < / 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 02/26/2020 S CreeRTPP12022620Se 0.000086 / mg/L / if 04/20/2020 P CreeRTPP12042020P 0.000003 / mg/L / OTWHg Feb 2020 Week 4 0.000086 / mg/L / Apr 2020 Week 3 0.000003 / mg/L / Feb 2020 Average 0.000086 / 0.000142 mg/L / Apr 2020 Average 0.000003 / 0.000142 mg/L / 2020 Quarter 1 0.000086 / mg/L / 2020 Quarter 2 0.000003 / mg/L / 2020 1st 6 Months (Avg) 0.000045 / mg/L / 2020 1st 6 ...(Max) 0.000086 / mg/L / 2020 1st 6 ...(Min) 0.000003 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 02/26/2020 S CreeRTPP12022620Se < 0.003 / mg/L < / If 04/21/2020 CreeRTPP12042120P < 0.001 / mg/L < / OTW Feb 2020 Week 4 < 0.003 / mg/L < / Apr 2020 Week 3 < 0.001 / mg/L < / Feb 2020 Average < 0.003 / mg/L < / Apr 2020 Average < 0.001 / mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 2020 Quarter 2 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.002 / mg/L < / 2020 1st 6 ...(Max) < 0.003 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Nickel 02/26/2020 S CreeRTPP12022620Se < 0.0025 / mg/L < / if Feb 2020 Week 4 < 0.0025 / mg/L < / Feb 2020 Average < 0.0025 / mg/L < / 2020 Quarter 1 < 0.0025 / mg/L < / 2020 1st 6 Months (Avg) < 0.0025 / mg/L < / 2020 1st 6 ...(Max) < 0.0025 / mg/L < / 2020 1st 6 ...(Min) < 0.0025 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Nitrate -Nitrite 04/21/2020 CreeRTPP12042120P 3.4 / mg/L / OTW Apr 2020 Week 3 3.4 / mg/L / Apr 2020 Average 3.4 / mg/L / 2020 Quarter 2 3.4 / mg/L / 2020 1st 6 Months (Avg) 3.4 / mg/L / 2020 1st 6 ...(Max) 3.4 / mg/L / 2020 1st 6 ...(Min) 3.4 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Nitrogen, Total 02/26/2020 S CreeRTPP12022620Se 14.2 / mg/L / if 04/21/2020 CreeRTPP12042120P 19.3 / mg/L / OTW Feb 2020 Week 4 14.2 / mg/L / Apr 2020 Week 3 19.3 / mg/L / Feb 2020 Average 14.2 / mg/L / Apr 2020 Average 19.3 / mg/L / 2020 Quarter 1 14.2 / mg/L / 2020 Quarter 2 19.3 / mg/L / 2020 1st 6 Months (Avg) 16.75 / mg/L / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 19.3 / mg/L 14.2 / mg/L 2 / Sample .Date SamplelD Result/Limit Mass /Limit Oil & Grease, Total 02/26/2020 S CreeRTPP12022620Se < 2.5 / 200 mg/L < / if 04/21/2020 CreeRTPP12042120P < 2.5 / 200 mg/L < / OTW Feb 2020 Week 4 < 2.5 / mg/L < / Apr 2020 Week 3 < 2.5 / mg/L < / Feb 2020 Average < 2.5 / mg/L < / Apr 2020 Average < 2.5 / mg/L < / 2020 Quarter 1 < 2.5 / mg/L < / 2020 Quarter 2 < 2.5 / mg/L < / 2020 1st 6 Months (Avg) < 2.5 / mg/L < / 2020 1st 6 ...(Max) < 2.5 / mg/L < / 2020 1st 6 ...(Min) < 2.5 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over QtrAvg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtrAvg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 02/26/2020 S CreeRTPP12022620Se 6.7 / 5.0 - 10.5 SU / if 04/21/2020 CreeRTPP12042120P 8.9 / 5.0 - 10.5 SU / OTW Feb 2020 Week 4 6.7 / SU / Apr 2020 Week 3 8.9 / SU / Feb 2020 Average 6.7 / SU / Apr 2020 Average 8.9 / SU / 2020 Quarter 1 6.7 / SU / 2020 Quarter 2 8.9 / SU / 2020 1st 6 Months (Avg) 7.8 / SU / 2020 1st 6 ...(Max) 8.9 / SU / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit pH 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 6.7 / 2 / Months Sampled : 2 0 0 0 0 SU 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Selenium 02/26/2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 S CreeRTPP12022620Se if Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.005 / 0.005 / 0.005 / 0.005 / 0.005 / 0.005 / 0.005 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit Silver 02/26/2020 Feb 2020 Feb 2020 2020 2020 2020 2020 2020 S CreeRTPP12022620Se if Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.0025 0.0025 / 0.0025 / 0.0025 / 0.0025 / 0.0025 / 0.0025 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result / Limit Mass /Limit Temperature 02/26/2020 04/21/2020 Feb 2020 Apr 2020 S CreeRTPP12022620Se if CreeRTPP12042120P OTW Week 4 Week 3 17.8 / 66 21 / 66 17.8 / 21 / °C °C °C °C Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Temperature Feb 2020 Apr 2020 2020 2020 2020 2020 2020 2020 Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 17.8 / °C 21 / °C 17.8 / °C 21 / °C 19.4 / °C 21 / °C 17.8 / °C 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit TKN 04/21/2020 CreeRTPP12042120P 15.9 / mg/L / OTW Apr 2020 Week 3 15.9 / mg/L / Apr 2020 Average 15.9 / mg/L / 2020 Quarter 2 15.9 / mg/L / 2020 1st 6 Months (Avg) 15.9 / mg/L / 2020 1st 6 ...(Max) 15.9 / mg/L / 2020 1st 6 ...(Min) 15.9 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Total Phosphorus 02/26/2020 S CreeRTPP12022620Se 1.5 / mg/L / if 04/21/2020 CreeRTPP12042120P 2.37 / mg/L / OTW Feb 2020 Week 4 1.5 / mg/L / Apr 2020 Week 3 2.37 / mg/L / Feb 2020 Average 1.5 / mg/L / Apr 2020 Average 2.37 / mg/L / 2020 Quarter 1 1.5 / mg/L / 2020 Quarter 2 2.37 / mg/L / 2020 1st 6 Months (Avg) 1.935 / mg/L / 2020 1st 6 ...(Max) 2.37 / mg/L / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 Cree, Inc.(RTP) SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 1.5 / mg/L 2 / Sample Date SamplelD Result /Limit Mass /Limit VOC 02/26/2020 S CreeRTPP12022620Se 0.19 / mg/L / if Feb 2020 Week 4 0.19 / mg/L / Feb 2020 Average 0.19 / mg/L / 2020 Quarter 1 0.19 / mg/L / 2020 1st 6 Months (Avg) 0.19 / mg/L / 2020 1st 6 ...(Max) 0.19 / mg/L / 2020 1st 6 ...(Min) 0.19 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Zinc 02/26/2020 S CreeRTPP12022620Se 0.26 / mg/L / if Feb 2020 Week 4 0.26 / mg/L / Feb 2020 Average 0.26 / mg/L / 2020 Quarter 1 0.26 / mg/L / 2020 1st 6 Months (Avg) 0.26 / mg/L / 2020 1st 6 ...(Max) 0.26 / mg/L / 2020 1st 6 ...(Min) 0.26 / mg/L / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:52:40PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 JMC (USA), Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 01/31/2020 S JMC0120F1ow 0.000159 / MGD 02/29/2020 S JMCO220F1ow 0.000248 / MGD 03/31/2020 S JMC0320F1ow 0.000133 / MGD 04/30/2020 S JMC0420F1ow 0.00004 / MGD 05/31/2020 S JMC0520F1ow 0.000094 / MGD 06/30/2020 S JMC0620F1ow 0.000034 / MGD Jan 2020 Week 4 0.000159 / MGD Feb 2020 Week 4 0.000248 / MGD Mar 2020 Week 4 0.000133 / MGD Apr 2020 Week 4 0.00004 / MGD May 2020 Week 4 0.000094 / MGD Jun 2020 Week 4 0.000034 / MGD Jan 2020 Average 0.000159 / 0.01 MGD Feb 2020 Average 0.000248 / 0.01 MGD Mar 2020 Average 0.000133 / 0.01 MGD Apr 2020 Average 0.00004 / 0.01 MGD May 2020 Average 0.000094 / 0.01 MGD Jun 2020 Average 0.000034 / 0.01 MGD 2020 Quarter 1 0.00018 / MGD 2020 Quarter 2 0.000056 / MGD 2020 1st 6 Months (Avg) 0.000118 / MGD 2020 1st 6 ...(Max) 0.000248 / MGD 2020 1st 6 ...(Min) 0.000034 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:53:55PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 01/21/2020 S Micross012120Se1f 02/25/2020 P Micross022520POTW Jan 2020 Week 3 Feb 2020 Week 4 Jan 2020 Average Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6...(Count) 0.021 / mg/L 0.032 / mg/L 0.021 / mg/L 0.032 / mg/L 0.021 / mg/L 0.032 / mg/L 0.026 / mg/L 0.026 / mg/L 0.032 / mg/L 0.021 / mg/L 2 / 0.003586 / lbs/day 0.005693 / lbs/day 0.003586 / lbs/day 0.005693 / lbs/day 0.003586 / lbs/day 0.005693 / lbs/day 0.00464 / lbs/day 0.004640 / lbs/day 0.005693 / lbs/day 0.003586 / lbs/day 2 / Sample Date SamplelD Result/Limit Mass/Limit Ammonia 01/21/2020 S Micross012120Se1f 1.9 / mg/L 0.3324 / lbs/day 02/25/2020 P Micross022520POTW 7.5 / mg/L 1.3385 / lbs/day Jan 2020 Week 3 1.9 / mg/L 0.3324 / lbs/day Feb 2020 Week 4 7.5 / mg/L 1.3385 / lbs/day Jan 2020 Average 1.9 / mg/L 0.3324 / lbs/day Feb 2020 Average 7.5 / mg/L 1.3385 / lbs/day 2020 Quarter 1 4.7 / mg/L 0.8354 / lbs/day 2020 1st 6 Months (Avg) 4.7 / mg/L 0.8354 / lbs/day 2020 1st 6 ...(Max) 7.5 / mg/L 1.3385 / lbs/day 2020 1st 6 ...(Min) 1.9 / mg/L 0.3324 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Average Flow for Month 01/31/2020 S Micross0120F1ow 0.022944 / 0.100 MGD / 02/29/2020 S Micross0220F1ow 0.021913 / 0.100 MGD / 03/31/2020 S Micross0320F1ow 0.026079 / 0.100 MGD / 04/30/2020 S Micross0420F1ow 0.027935 / 0.100 MGD / 05/31/2020 S Micross0520F1ow 0.03299 / 0.100 MGD / 06/30/2020 S Micross0620F1ow 0.036317 / 0.100 MGD / Jan 2020 Week 4 0.022944 / MGD / Feb 2020 Week 4 0.021913 / MGD / Mar 2020 Week 4 0.026079 / MGD / Apr 2020 Week 4 0.027935 / MGD / May 2020 Week 4 0.03299 / MGD / Jun 2020 Week 4 0.036317 / MGD / Jan 2020 Average 0.022944 / 0.075 MGD / Feb 2020 Average 0.021913 / 0.075 MGD / Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Mar 2020 Average 0.026079 / 0.075 MGD Apr 2020 Average 0.027935 / 0.075 MGD May 2020 Average 0.03299 / 0.075 MGD Jun 2020 Average 0.036317 / 0.075 MGD 2020 Quarter 1 0.023645 / MGD 2020 Quarter 2 0.032414 / MGD 2020 1st 6 Months (Avg) 0.028030 / MGD 2020 1st 6 ...(Max) 0.036317 / MGD 2020 1st 6 ...(Min) 0.021913 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Cadmium 01/21/2020 S Micross012120Se1f < 0.0002 / mg/L < 0.000035 / lbs/day 02/25/2020 P Micross022520POTW < 0.00008 / mg/L < 0.000013 / lbs/day Jan 2020 Week 3 < 0.0002 / mg/L < 0.000035 / lbs/day Feb 2020 Week 4 < 0.00008 / mg/L < 0.000013 / lbs/day Jan 2020 Average < 0.0002 / mg/L < 0.000035 / lbs/day Feb 2020 Average < 0.00008 / mg/L < 0.000013 / lbs/day 2020 Quarter 1 < 0.00014 / mg/L < 0.000024 / lbs/day 2020 1st 6 Months (Avg) < 0.00014 / mg/L < 0.000024 / lbs/day 2020 1st 6 ...(Max) < 0.0002 / mg/L < 0.000035 / lbs/day 2020 1st 6 ...(Min) < 0.00008 / mg/L < 0.000013 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Chloride 01/21/2020 S Micross012120Se1f 02/25/2020 P Micross022520POTW Jan 2020 Week 3 Feb 2020 Week 4 Jan 2020 Average Feb 2020 Average 2020 Quarter 1 22 / mg/L 3.8485 / lbs/day 75 / mg/L 13.3851 / lbs/day 22 / mg/L 3.8485 / lbs/day 75 / mg/L 13.3851 / lbs/day 22 / mg/L 3.8485 / lbs/day 75 / mg/L 13.3851 / lbs/day 48.5 / mg/L 8.6168 / lbs/day Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Chloride 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6...(Count) 48.5 / mg/L 75 / mg/L 22 / mg/L 2 / 8.6168 / lbs/day 13.3851 / lbs/day 3.8485 / lbs/day 2 / Sample Date SamplelD Result / Limit Mass / Limit Chromium 01/21/2020 S Micross012120Se1f 0.003 / mg/L 0.000525 / lbs/day 02/25/2020 P Micross022520POTW < 0.001 / mg/L < 0.000178 / lbs/day Jan 2020 Week 3 0.003 / mg/L 0.000525 / lbs/day Feb 2020 Week 4 < 0.001 / mg/L < 0.000178 / lbs/day Jan 2020 Average 0.003 / mg/L 0.000525 / lbs/day Feb 2020 Average < 0.001 / mg/L < 0.000178 / lbs/day 2020 Quarter 1 < 0.002 / mg/L < 0.000352 / lbs/day 2020 1st 6 Months (Avg) < 0.002 / mg/L < 0.000352 / lbs/day 2020 1st 6 ...(Max) 0.003 / mg/L 0.000525 / lbs/day 2020 1st 6 ...(Min) < 0.001 / mg/L < 0.000178 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Copper 01/21/2020 S Micross012120Se1f 0.03 / mg/L 0.005248 / lbs/day 02/25/2020 P Micross022520POTW 0.037 / mg/L 0.006603 / lbs/day Jan 2020 Week 3 0.03 / mg/L 0.005248 / lbs/day Feb 2020 Week 4 0.037 / mg/L 0.006603 / lbs/day Jan 2020 Average 0.03 / mg/L 0.005248 / lbs/day Feb 2020 Average 0.037 / mg/L 0.006603 / lbs/day 2020 Quarter 1 0.034 / mg/L 0.005926 / lbs/day 2020 1st 6 Months (Avg) 0.034 / mg/L 0.005926 / lbs/day 2020 1st 6 ...(Max) 0.037 / mg/L 0.006603 / lbs/day 2020 1st 6 ...(Min) 0.03 / mg/L 0.005248 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result / Limit Mass/Limit Cyanide 01/21/2020 S Micross012120Se1f 0.009 / mg/L 0.001574 / lbs/day 02/25/2020 P Micross022520POTW < 0.003 / mg/L < 0.000446 / lbs/day Jan 2020 Week 3 0.009 / mg/L 0.001574 / lbs/day Feb 2020 Week 4 < 0.003 / mg/L < 0.000446 / lbs/day Jan 2020 Average 0.009 / mg/L 0.001574 / lbs/day Feb 2020 Average < 0.003 / mg/L < 0.000446 / lbs/day Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 3 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Cyanide 2020 Quarter 1 < 0.006 / mg/L < 0.00101 / lbs/day 2020 1st 6 Months (Avg) < 0.006 / mg/L < 0.001010 / lbs/day 2020 1st 6 ...(Max) 0.009 / mg/L 0.001574 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.000446 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Fluoride 01/21/2020 S Micross012120Se1f 0.98 / mg/L 0.1714 / lbs/day 02/25/2020 P Micross022520POTW 0.6 / mg/L 0.1071 / lbs/day Jan 2020 Week 3 0.98 / mg/L 0.1714 / lbs/day Feb 2020 Week 4 0.6 / mg/L 0.1071 / lbs/day Jan 2020 Average 0.98 / mg/L 0.1714 / lbs/day Feb 2020 Average 0.6 / mg/L 0.1071 / lbs/day 2020 Quarter 1 0.79 / mg/L 0.1393 / lbs/day 2020 1st 6 Months (Avg) 0.79 / mg/L 0.1393 / lbs/day 2020 1st 6 ...(Max) 0.98 / mg/L 0.1714 / lbs/day 2020 1st 6 ...(Min) 0.6 / mg/L 0.1071 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Lead 01/21/2020 S Micross012120Se1f 0.0056 / mg/L 0.00098 / lbs/day 02/25/2020 P Micross022520POTW 0.0025 / mg/L 0.000452 / lbs/day Jan 2020 Week 3 0.0056 / mg/L 0.00098 / lbs/day Feb 2020 Week 4 0.0025 / mg/L 0.000452 / lbs/day Jan 2020 Average 0.0056 / mg/L 0.00098 / lbs/day Feb 2020 Average 0.0025 / mg/L 0.000452 / lbs/day 2020 Quarter 1 0.0041 / mg/L 0.000716 / lbs/day 2020 1st 6 Months (Avg) 0.0041 / mg/L 0.000716 / lbs/day 2020 1st 6 ...(Max) 0.0056 / mg/L 0.000980 / lbs/day 2020 1st 6 ...(Min) 0.0025 / mg/L 0.000452 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 01/23/2020 S Micross012320Se1fHg 0.000033 / 0.000142 mg/L 01/28/2020 S Micross012820Se1fHg 0.000006 / 0.000142 mg/L 02/24/2020 P Micross022420POTW 0.000141 / 0.000142 mg/L Hg 06/15/2020 P Micross061520POTW 0.000188 / 0.000142 mg/L * Hg * Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL Jan 2020 Week 4 0.00002 / mg/L Feb 2020 Week 4 0.000141 / mg/L Jun 2020 Week 3 0.000188 / mg/L Jan 2020 Average 0.00002 / mg/L Feb 2020 Average 0.000141 / mg/L Jun 2020 Average 0.000188 / mg/L 2020 Quarter 1 0.00006 / mg/L 2020 Quarter 2 0.000188 / mg/L 2020 1st 6 Months (Avg) 0.000092 / mg/L 2020 1st 6 ...(Max) 0.000188 / mg/L 2020 1st 6 ...(Min) 0.000006 / mg/L 2020 1st 6 ...(Count) 4 / Sample Count : 4 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 1 25.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 1 25.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit Molybdenum 01/21/2020 S Micross012120Se1f 0.014 / mg/L 0.0024 / lbs/day 02/25/2020 P Micross022520POTW 0.02 / mg/L 0.0036 / lbs/day Jan 2020 Week 3 0.014 / mg/L 0.0024 / lbs/day Feb 2020 Week 4 0.02 / mg/L 0.0036 / lbs/day Jan 2020 Average 0.014 / mg/L 0.0024 / lbs/day Feb 2020 Average 0.02 / mg/L 0.0036 / lbs/day 2020 Quarter 1 0.017 / mg/L 0.003 / lbs/day 2020 1st 6 Months (Avg) 0.017 / mg/L 0.0030 / lbs/day 2020 1st 6 ...(Max) 0.020 / mg/L 0.0036 / lbs/day 2020 1st 6 ...(Min) 0.014 / mg/L 0.0024 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Nickel 01/21/2020 S Micross012120Se1f 0.0212 / mg/L 0.003709 / lbs/day 02/25/2020 P Micross022520POTW 0.0029 / mg/L 0.000516 / lbs/day Jan 2020 Week 3 0.0212 / mg/L 0.003709 / lbs/day Feb 2020 Week 4 0.0029 / mg/L 0.000516 / lbs/day Jan 2020 Average 0.0212 / mg/L 0.003709 / lbs/day Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Nickel Feb 2020 2020 2020 2020 2020 2020 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 0.0029 / 0.012 / 0.0120 / 0.0212 / 0.0029 / 2 / mg/L mg/L mg/L mg/L mg/L 0.000516 / 0.002112 / 0.002112 / 0.003709 / 0.000516 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 01/21/2020 02/25/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 S Micross012120Se1f P Micross022520POTW Week 3 Week 4 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.9 / 1.4 / 0.9 / 1.4 / 0.9 / 1.4 / 1.1 / 1.1 / 1.4 / 0.9 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.156 / 0.243 / 0.156 / 0.243 / 0.156 / 0.243 / 0.199 / 0.199 / 0.243 / 0.156 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 01/21/2020 02/25/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 S Micross012120Se1f P Micross022520POTW Week 3 Week 4 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 10.1 / 15.9 / 10.1 / 15.9 / 10.1 / 15.9 / 13 / 13 / 15.9 / 10.1 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1.767 / 2.838 / 1.767 / 2.838 / 1.767 / 2.838 / 2.302 / 2.302 / 2.838 / 1.767 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 01/21/2020 02/25/2020 Jan 2020 Feb 2020 S Micross012120Se1f P Micross022520POTW Week 3 Week 4 0.75 / 200 2.5 / 200 0.75 / 2.5 / mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total Jan 2020 Average < 0.75 / mg/L < / Feb 2020 Average < 2.5 / mg/L < / 2020 Quarter 1 < 1.63 / mg/L < / 2020 1st 6 Months (Avg) < 1.63 / mg/L < / 2020 1st 6 ...(Max) < 2.5 / mg/L < / 2020 1st 6 ...(Min) < 0.75 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 01/21/2020 S Micross012120Se1f 02/25/2020 P Micross022520POTW Jan 2020 Week 3 Feb 2020 Week 4 Jan 2020 Average Feb 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 8.8 /5.5-10.5 SU / 8.7 /5.5-10.5 SU / 8.8 / SU / 8.7 / SU / 8.8 / SU / 8.7 / SU / 8.75 / SU / 8.75 / SU / 8.8 / SU / 8.7 / SU / 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SrunplelD Result /Limit Mass /Limit Silver 01/21/2020 S Micross012120Se1f < 0.0001 / mg/L 0.000009 / lbs/day Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result / Limit Mass /Limit Silver 02/25/2020 P Micross022520POTW < 0.0003 / mg/L < 0.000045 / lbs/day Jan 2020 Week 3 < 0.0001 / mg/L < 0.000009 / lbs/day Feb 2020 Week 4 < 0.0003 / mg/L < 0.000045 / lbs/day Jan 2020 Average < 0.0001 / mg/L < 0.000009 / lbs/day Feb 2020 Average < 0.0003 / mg/L < 0.000045 / lbs/day 2020 Quarter 1 < 0.0002 / mg/L < 0.000027 / lbs/day 2020 1st 6 Months (Avg) < 0.0002 / mg/L < 0.000027 / lbs/day 2020 1st 6...(Max) < 0.0003 / mg/L < 0.000045 / lbs/day 2020 1st 6...(Min) < 0.0001 / mg/L < 0.000009 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result / Limit Mass/Limit Temperature 01/21/2020 S Micross012120Self 11.7 / 66 °C / 02/25/2020 P Micross022520POTW 17 / 66 °C / Jan 2020 Week 3 11.7 / °C / Feb 2020 Week 4 17 / °C / Jan 2020 Average 11.7 / °C / Feb 2020 Average 17 / °C / 2020 Quarter 1 14.4 / °C / 2020 1st 6 Months (Avg) 14.4 / °C / 2020 1st 6...(Max) 17 / °C / 2020 1st 6...(Min) 11.7 / °C / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Tin 01/21/2020 S Micross012120Se1f < 0.001500000 / mg/L < 0.000262397 / lbs/day 02/25/2020 P Micross022520POTW < 0.012500000 / mg/L < 0.002230846 / lbs/day Jan 2020 Week 3 < 0 / mg/L < 0 / lbs/day Feb 2020 Week 4 < 0 / mg/L < 0 / lbs/day Jan 2020 Average < 0 / mg/L < 0 / lbs/day Feb 2020 Average < 0 / mg/L < 0 / lbs/day 2020 Quarter 1 < 0 / mg/L < 0 / lbs/day Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Tin 2020 2020 2020 2020 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 0 / 0 / 0 / 2 / mg/L mg/L mg/L 0 / 0 / 0 / 2 / lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit TKN 01/21/2020 02/25/2020 Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 S Micross012120Se1f P Micross022520POTW Week 3 Week 4 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 9.2 / 14.6 / 9.2 / 14.6 / 9.2 / 14.6 / 11.9 / 11.9 / 14.6 / 9.2 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1.609 / 2.606 / 1.609 / 2.606 / 1.609 / 2.606 / 2.107 / 2.108 / 2.606 / 1.609 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 01/21/2020 S 02/25/2020 P Jan 2020 Feb 2020 Jan 2020 Feb 2020 2020 2020 2020 2020 2020 Micross012120Se1f Micross022520POTW Week 3 Week 4 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 1.9 / 1.61 / 1.9 / 1.61 / 1.9 / 1.61 / 1.755 / 1.755 / 1.9 / 1.61 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.3324 / 0.2873 / 0.3324 / 0.2873 / 0.3324 / 0.2873 / 0.3099 / 0.3099 / 0.3324 / 0.2873 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass /Limit VOC 01/21/2020 Jan 2020 Jan 2020 2020 2020 2020 S Micross012120Se1f Week 3 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 0.01 / 0.01 / 0.01 / 0.01 / 0.01 / 0.01 / mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit VOC 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.01 / mg/L 1 / Sample Date SamplelD Result /Limit Mass /Limit Zinc 01/21/2020 S Micross012120Se1f 0.392 / mg/L 0.068573 / lbs/day 02/25/2020 P Micross022520POTW < 0.205 / mg/L < 0.036497 / lbs/day Jan 2020 Week 3 0.392 / mg/L 0.068573 / lbs/day Feb 2020 Week 4 < 0.205 / mg/L < 0.036497 / lbs/day Jan 2020 Average 0.392 / mg/L 0.068573 / lbs/day Feb 2020 Average < 0.205 / mg/L < 0.036497 / lbs/day 2020 Quarter 1 < 0.298 / mg/L < 0.052535 / lbs/day 2020 1st 6 Months (Avg) < 0.298 / mg/L < 0.052535 / lbs/day 2020 1st 6 ...(Max) 0.392 / mg/L 0.068573 / lbs/day 2020 1st 6 ...(Min) < 0.205 / mg/L < 0.036497 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Wednesday, February 24, 2021 10:55:02PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 Novan, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 04/06/2020 P Novan040620POTW 6.7 / mg/L Apr 2020 Week 1 6.7 / mg/L Apr 2020 Average 6.7 / mg/L 2020 Quarter 2 6.7 / mg/L 2020 1st 6 Months (Avg) 6.7 / mg/L 2020 1st 6 ...(Max) 6.7 / mg/L 2020 1st 6 ...(Min) 6.7 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass /Limit Average Flow for Month 01/31/2020 S Novan0120Flow 02/29/2020 S Novan0220F1ow 03/31/2020 S Novan0320F1ow 04/30/2020 S Novan0420F1ow 05/31/2020 S Novan0520F1ow 06/30/2020 S Novan0620F1ow Jan 2020 Week 4 Feb 2020 Week 4 Mar 2020 Week 4 Apr 2020 Week 4 May 2020 Week 4 Jun 2020 Week 4 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.00047 / MGD 0.000515 / MGD 0.00019 / MGD 0.000164 / MGD 0.000153 / MGD 0.000187 / MGD 0.00047 / MGD 0.000515 / MGD 0.00019 / MGD 0.000164 / MGD 0.000153 / MGD 0.000187 / MGD 0.00047 / MGD 0.000515 / MGD 0.00019 / MGD 0.000164 / MGD 0.000153 / MGD 0.000187 / MGD 0.000392 / MGD 0.000168 / MGD 0.000280 / MGD 0.000515 / MGD 0.000153 / MGD 6 / Sample Date SamplelD Result /Limit Mass /Limit Cadmium 01/23/2020 S Novan012320Se1f < 0.00008 / mg/L < / 04/06/2020 P Novan040620POTW < 0.00008 / mg/L < / Jan 2020 Week 4 < 0.00008 / mg/L < / Apr 2020 Week 1 < 0.00008 / mg/L < / Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5 Novan, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Cadmium Jan 2020 Average < 0.00008 / mg/L < / Apr 2020 Average < 0.00008 / mg/L < / 2020 Quarter 1 < 0.00008 / mg/L < / 2020 Quarter 2 < 0.00008 / mg/L < / 2020 1st 6 Months (Avg) < 0.00008 / mg/L < / 2020 1st 6 ...(Max) < 0.00008 / mg/L < / 2020 1st 6 ...(Min) < 0.00008 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit COD 01/23/2020 S Novan012320Se1f 04/06/2020 P Novan040620POTW Jan 2020 Week 4 Apr 2020 Week 1 Jan 2020 Average Apr 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 549 / mg/L 818 / mg/L 549 / mg/L 818 / mg/L 549 / mg/L 818 / mg/L 549 / mg/L 818 / mg/L 683.5 / mg/L 818 / mg/L 549 / mg/L 2 / Sample Date SamplelD Result/Limit Mass/Limit Copper 01/23/2020 S Novan012320Se1f 0.071 / mg/L / 04/06/2020 P Novan040620POTW 0.134 / mg/L / Jan 2020 Week 4 0.071 / mg/L / Apr 2020 Week 1 0.134 / mg/L / Jan 2020 Average 0.071 / mg/L / Apr 2020 Average 0.134 / mg/L / 2020 Quarter 1 0.071 / mg/L / 2020 Quarter 2 0.134 / mg/L / 2020 1st 6 Months (Avg) 0.103 / mg/L / 2020 1st 6 ...(Max) 0.134 / mg/L / 2020 1st 6 ...(Min) 0.071 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result / Limit Mass/Limit Mercury - LL Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5 Novan, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 01/23/2020 S Novan012320Se1fHg 0.000032 / 0.000142 mg/L 04/06/2020 P Novan040620POTWH 0.000045 / 0.000142 mg/L g Jan 2020 Week 4 0.000032 / mg/L Apr 2020 Week 1 0.000045 / mg/L Jan 2020 Average 0.000032 / mg/L Apr 2020 Average 0.000045 / mg/L 2020 Quarter 1 0.000032 / mg/L 2020 Quarter 2 0.000045 / mg/L 2020 1st 6 Months (Avg) 0.000039 / mg/L 2020 1st 6 ...(Max) 0.000045 / mg/L 2020 1st 6 ...(Min) 0.000032 / mg/L 2020 1st 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 01/23/2020 S Novan012320Se1f < 0.001 / mg/L Jan 2020 Week 4 < 0.001 / mg/L Jan 2020 Average < 0.001 / mg/L 2020 Quarter 1 < 0.001 / mg/L 2020 1st 6 Months (Avg) < 0.001 / mg/L 2020 1st 6 ...(Max) < 0.001 / mg/L 2020 1st 6 ...(Min) < 0.001 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit pH 01/23/2020 S Novan012320Se1f 8.1 / 6.0 - 10.0 SU / 04/06/2020 P Novan040620POTW 6.2 / 6.0 - 10.0 SU / Jan 2020 Week 4 8.1 / SU / Apr 2020 Week 1 6.2 / SU / Jan 2020 Average 8.1 / SU / Apr 2020 Average 6.2 / SU / 2020 Quarter 1 8.1 / SU / Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5 Novan, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 6.2 / SU 7.15 / SU 8.1 / SU 6.2 / SU 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit Silver 01/23/2020 S Novan012320Se1f < 0.0003 / mg/L < / Jan 2020 Week 4 < 0.0003 / mg/L < / Jan 2020 Average < 0.0003 / mg/L < / 2020 Quarter 1 < 0.0003 / mg/L < / 2020 1st 6 Months (Avg) < 0.0003 / mg/L < / 2020 1st 6 ...(Max) < 0.0003 / mg/L < / 2020 1st 6 ...(Min) < 0.0003 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Temperature 01/23/2020 S Novan012320Se1f 04/06/2020 P Novan040620POTW Jan 2020 Week 4 Apr 2020 Week 1 Jan 2020 Average Apr 2020 Average 2020 Quarter 1 2020 Quarter2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 15 / 66 °C 22 / 66 °C 15 / °C 22 / °C 15 / °C 22 / °C 15 / °C 22 / °C 18.5 / °C 22 / °C 15 / °C 2 / Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5 Novan, Inc. # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 0 0 0 0 0 0 2 Months Sampled : 2 # 0.00 # Over Mo Avg C : 0 0.00 0.00 # Over Mo Avg C TRC : 0 0.00 0.00 # Over Mo Avg M : 0 0.00 0.00 # Over Mo Avg M TRC : 0 0.00 0.00 0.00 # Over Wk Avg C : # Over Wk Avg C TRC : # Over Wk Avg M : # Over Wk Avg M TRC : Weeks Sampled : # 0 0 0 0 2 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 01/23/2020 04/06/2020 Jan 2020 Apr 2020 Jan 2020 Apr 2020 2020 2020 2020 2020 2020 2020 S Novan012320Se1f P Novan040620POTW Week 4 Week 1 Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 9.46 / 16.7 / 9.46 / 16.7 / 9.46 / 16.7 / 9.46 / 16.7 / 13.08 / 16.7 / 9.46 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result / Limit Mass /Limit VOC 01/23/2020 Jan 2020 Jan 2020 2020 2020 2020 2020 2020 S Novan012320Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.538 / 0.538 / 0.538 / 0.538 / 0.538 / 0.538 / 0.538 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit Zinc 01/23/2020 Jan 2020 Jan 2020 2020 2020 2020 2020 2020 S Novan012320Se1f Week 4 Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 0.301 / 0.301 / 0.301 / 0.301 / 0.301 / 0.301 / 0.301 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5 Wednesday, February 24, 2021 10:55:54PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1 Phononic SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 01/31/2020 S Phononic0120F1ow 0.006335 / MGD 02/29/2020 S Phononic0220F1ow 0.006106 / MGD 03/02/2020 P Phononic030220POT 0.000002 / MGD WHg 03/31/2020 S Phononic0320F1ow 0.005799 / MGD 04/30/2020 S Phononic0420F1ow 0.006729 / MGD 05/31/2020 S Phononic0520F1ow 0.006964 / MGD 06/30/2020 S Phononic0620F1ow 0.00511 / MGD Jan 2020 Week 4 0.006335 / MGD Feb 2020 Week 4 0.006106 / MGD Mar 2020 Week 1 0.000002 / MGD Mar 2020 Week 4 0.005799 / MGD Apr 2020 Week 4 0.006729 / MGD May 2020 Week 4 0.006964 / MGD Jun 2020 Week 4 0.00511 / MGD Jan 2020 Average 0.006335 / 0.020 MGD Feb 2020 Average 0.006106 / 0.020 MGD Mar 2020 Average 0.002901 / 0.020 MGD Apr 2020 Average 0.006729 / 0.020 MGD May 2020 Average 0.006964 / 0.020 MGD Jun 2020 Average 0.00511 / 0.020 MGD 2020 Quarter 1 0.004561 / MGD 2020 Quarter 2 0.006268 / MGD 2020 1st 6 Months (Avg) 0.005292 / MGD 2020 1st 6 ...(Max) 0.006964 / MGD 2020 1st 6 ...(Min) 0.000002 / MGD 2020 1st 6 ...(Count) 7 / Sample Count : 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Bismuth 01/20/2020 S Phononic012020Se1f 0.164 / mg/L 02/14/2020 S Phononic021420Se1f 0.037 / mg/L 03/02/2020 P Phononic030220POT < 0.05 / mg/L W 03/13/2020 S Phononic031320Se1f 0.091 / mg/L Wednesday, February 24, 2021 10:56:53PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5 Phononic SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Bismuth 04/10/2020 S Phononic041020Se1f 05/18/2020 S Phononic051820Se1f 06/18/2020 S Phononic061820Se1f Jan 2020 Week 3 Feb 2020 Week 2 Mar 2020 Week 1 Mar 2020 Week 2 Apr 2020 Week 2 May 2020 Week 3 Jun 2020 Week 3 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average Jun 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.054 0.125 0.044 0.164 0.037 0.05 0.091 0.054 0.125 0.044 0.164 0.037 0.071 0.054 0.125 0.044 0.086 0.074 0.081 0.164 0.037 7 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 04/17/2020 S Phononic041720Se1fH 0.000002 / 0.000142 mg/L g Apr 2020 Week 3 0.000002 / mg/L Apr 2020 Average 0.000002 / mg/L 2020 Quarter 2 0.000002 / mg/L 2020 1st 6 Months (Avg) 0.000002 / mg/L 2020 1st 6 ...(Max) 0.000002 / mg/L 2020 1st 6 ...(Min) 0.000002 / mg/L 2020 1st 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:56:53PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5 Phononic SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 04/10/2020 S Phononic041020Se1f < 0.003 / mg/L < 0.0002 / lbs/day Apr 2020 Week 2 < 0.003 / mg/L < 0.0002 / lbs/day Apr 2020 Average < 0.003 / mg/L < 0.0002 / lbs/day 2020 Quarter 2 < 0.003 / mg/L < 0.0002 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.0002 / lbs/day 2020 1st 6 ...(Max) < 0.003 / mg/L < 0.0002 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.0002 / lbs/day 2020 1st 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Nickel 01/20/2020 S Phononic012020Se1f 0.111 / mg/L 0.011216 / 0.02 lbs/day 02/14/2020 S Phononic021420Se1f 0.128 / mg/L 0.010484 / 0.02 lbs/day 03/02/2020 P Phononic030220POT 0.121 / mg/L / 0.02 W 03/13/2020 S Phononic031320Se1f 0.105 / mg/L 0.007034 / 0.02 lbs/day 04/10/2020 S Phononic041020Se1f 0.111 / mg/L 0.007545 / 0.02 lbs/day 05/18/2020 S Phononic051820Se1f 0.155 / mg/L 0.01937 / 0.02 lbs/day 06/18/2020 S Phononic061820Se1f 0.752 / mg/L 0.043206 / 0.02 lbs/day 06/25/2020 S Phononic062520Se1f 0.076 / mg/L 0.003239 / 0.02 lbs/day Jan 2020 Week 3 0.111 / mg/L 0.011216 / lbs/day Feb 2020 Week 2 0.128 / mg/L 0.010484 / lbs/day Mar 2020 Week 1 0.121 / mg/L / Mar 2020 Week 2 0.105 / mg/L 0.007034 / lbs/day Apr 2020 Week 2 0.111 / mg/L 0.007545 / lbs/day May 2020 Week 3 0.155 / mg/L 0.01937 / lbs/day Jun 2020 Week 3 0.752 / mg/L 0.043206 / lbs/day Jun 2020 Week 4 0.076 / mg/L 0.003239 / lbs/day Jan 2020 Average 0.111 / mg/L 0.011216 / lbs/day Feb 2020 Average 0.128 / mg/L 0.010484 / lbs/day Mar 2020 Average 0.113 / mg/L 0.007034 / lbs/day Apr 2020 Average 0.111 / mg/L 0.007545 / lbs/day May 2020 Average 0.155 / mg/L 0.01937 / lbs/day Jun 2020 Average 0.414 / mg/L 0.023222 / lbs/day 2020 Quarter 1 0.1163 / mg/L 0.009578 / lbs/day 2020 Quarter 2 0.2735 / mg/L 0.01834 / lbs/day 2020 1st 6 Months (Avg) 0.1949 / mg/L 0.014585 / lbs/day 2020 1st 6 ...(Max) 0.752 / mg/L 0.043206 / lbs/day 2020 1st 6 ...(Min) 0.076 / mg/L / 2020 1st 6 ...(Count) 8 / 7 / * Wednesday, February 24, 2021 10:56:53PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5 Phononic SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 8 Months Sampled : 6 Weeks Sampled : 8 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 1 12.50 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 1 12.50 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit pH 03/02/2020 P Phononic030220POT 7.1 / 5.5 - 10 SU W 05/27/2020 S Phononic052720Se1f 6.3 / 5.5 - 10 SU / Mar 2020 Week 1 7.1 / SU / May 2020 Week 4 6.3 / SU / Mar 2020 Average 7.1 / SU / May 2020 Average 6.3 / SU / 2020 Quarter 1 7.1 / SU / 2020 Quarter 2 6.3 / SU / 2020 1st 6 Months (Avg) 6.7 / SU / 2020 1st 6 ...(Max) 7.1 / SU / 2020 1st 6 ...(Min) 6.3 / SU / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Tellurium 01/20/2020 S Phononic012020Se1f 02/14/2020 S Phononic021420Se1f 03/02/2020 P Phononic030220POT W 03/13/2020 S Phononic031320Se1f 04/10/2020 S Phononic041020Se1f 05/18/2020 S Phononic051820Se1f 06/18/2020 S Phononic061820Se1f Jan 2020 Week 3 Feb 2020 Week 2 Mar 2020 Week 1 0.559 / mg/L 0.357 / mg/L 0.281 / mg/L 0.257 / mg/L 0.567 / mg/L 0.201 / mg/L 0.323 / mg/L 0.559 / mg/L 0.357 / mg/L 0.281 / mg/L Wednesday, February 24, 2021 10:56:53PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5 Phononic SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Tellurium Mar 2020 Week 2 0.257 / mg/L Apr 2020 Week 2 0.567 / mg/L May 2020 Week 3 0.201 / mg/L Jun 2020 Week 3 0.323 / mg/L Jan 2020 Average 0.559 / mg/L Feb 2020 Average 0.357 / mg/L Mar 2020 Average 0.269 / mg/L Apr 2020 Average 0.567 / mg/L May 2020 Average 0.201 / mg/L Jun 2020 Average 0.323 / mg/L 2020 Quarter 1 0.364 / mg/L 2020 Quarter 2 0.364 / mg/L 2020 1st 6 Months (Avg) 0.364 / mg/L 2020 1st 6 ...(Max) 0.567 / mg/L 2020 1st 6 ...(Min) 0.201 / mg/L 2020 1st 6 ...(Count) 7 / Wednesday, February 24, 2021 10:56:53PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result / Limit Mass /Limit Aluminum 03/02/2020 P PowerSecure030220P 6.18 / mg/L OTW Mar 2020 Week 1 6.18 / mg/L Mar 2020 Average 6.18 / mg/L 2020 Quarter 1 6.18 / mg/L 2020 1st 6 Months (Avg) 6.18 / mg/L 2020 1st 6...(Max) 6.18 / mg/L 2020 1st 6...(Min) 6.18 / mg/L 2020 1st 6 ...(Count) 1 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S PowerSecure0120F1ow 0.001113 / MGD 02/29/2020 S PowerSecure0220F1ow 0.001397 / MGD 03/31/2020 S PowerSecure0320F1ow 0.001283 / MGD 04/30/2020 S PowerSecure0420F1ow 0.000875 / MGD 05/31/2020 S PowerSecure0520F1ow 0.001022 / MGD 06/30/2020 S PowerSecure0620F1ow 0.006432 / MGD Jan 2020 Week 4 0.001113 / MGD Feb 2020 Week 4 0.001397 / MGD Mar 2020 Week 4 0.001283 / MGD Apr 2020 Week 4 0.000875 / MGD May 2020 Week 4 0.001022 / MGD Jun 2020 Week 4 0.006432 / MGD Jan 2020 Average 0.001113 / 0.006 MGD Feb 2020 Average 0.001397 / 0.006 MGD Mar 2020 Average 0.001283 / 0.006 MGD Apr 2020 Average 0.000875 / 0.006 MGD May 2020 Average 0.001022 / 0.006 MGD Jun 2020 Average 0.006432 / 0.006 MGD * 2020 Quarter 1 0.001264 / MGD 2020 Quarter 2 0.002776 / MGD 2020 1st 6 Months (Avg) 0.002020 / MGD 2020 1st 6...(Max) 0.006432 / MGD 2020 1st 6...(Min) 0.000875 / MGD 2020 1st 6 ...(Count) 6 / Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 1 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 6 Months Sampled : 6 # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 1 16.67 # Over Wk Avg C : # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Weeks Sampled : 6 Quarters Sampled : 2 # % # 0 0.00 # Over Qt Avg C : 0 0.00 0 0.00 # Over Qt Avg C TRC : 0 0.00 0 0.00 # Over Qtr Avg M : 0 0.00 0 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cadmium 03/02/2020 P PowerSecure030220P < 0.00008 / 0.11 mg/L < / OTW Mar 2020 Week 1 < 0.00008 / mg/L < / Mar 2020 Average < 0.00008 / 0.07 mg/L < / 2020 Quarter 1 < 0.00008 / mg/L < / 2020 1st 6 Months (Avg) < 0.00008 / mg/L < / 2020 1st 6 ...(Max) < 0.00008 / mg/L < / 2020 1st 6 ...(Min) < 0.00008 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Chromium 03/02/2020 P PowerSecure030220P < 0.001 / 2.77 mg/L < / OTW Mar 2020 Week 1 < 0.001 / mg/L < / Mar 2020 Average < 0.001 / 1.71 mg/L < / 2020 Quarter 1 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.001 / mg/L < / 2020 1st 6 ...(Max) < 0.001 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 2 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass /Limit Copper 03/02/2020 P PowerSecure030220P 0.423 / 3.38 mg/L / OTW Mar 2020 Week 1 0.423 / mg/L / Mar 2020 Average 0.423 / 2.07 mg/L / 2020 Quarter 1 0.423 / mg/L / 2020 1st 6 Months (Avg) 0.423 / mg/L / 2020 1st 6 ...(Max) 0.423 / mg/L / 2020 1st 6 ...(Min) 0.423 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Cyanide 03/02/2020 P PowerSecure030220P < 0.003 / 0.60 mg/L < / OTW Mar 2020 Week 1 < 0.003 / mg/L < / Mar 2020 Average < 0.003 / 0.50 mg/L < / 2020 Quarter 1 < 0.003 / mg/L < / 2020 1st 6 Months (Avg) < 0.003 / mg/L < / 2020 1st 6 ...(Max) < 0.003 / mg/L < / 2020 1st 6 ...(Min) < 0.003 / mg/L < / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 3 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass /Limit Lead 03/02/2020 P PowerSecure030220P < 0.0003 / 0.69 mg/L < / OTW Mar 2020 Week 1 < 0.0003 / mg/L < / Mar 2020 Average < 0.0003 / 0.43 mg/L < / 2020 Quarter 1 < 0.0003 / mg/L < / 2020 1st 6 Months (Avg) < 0.0003 / mg/L < / 2020 1st 6 ...(Max) < 0.0003 / mg/L < / 2020 1st 6 ...(Min) < 0.0003 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Mercury - LL 06/01/2020 P PowerSecure060120P 0.000002 / mg/L / OTWHg Jun 2020 Week 1 0.000002 / mg/L / Jun 2020 Average 0.000002 / mg/L / 2020 Quarter 2 0.000002 / mg/L / 2020 1st 6 Months (Avg) 0.000002 / mg/L / 2020 1st 6 ...(Max) 0.000002 / mg/L / 2020 1st 6 ...(Min) 0.000002 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 03/02/2020 P PowerSecure030220P < 0.001 / OTW Mar 2020 Week 1 < 0.001 / mg/L mg/L Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 4 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum Mar 2020 Average < 0.001 / mg/L < / 2020 Quarter 1 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.001 / mg/L < / 2020 1st 6 ...(Max) < 0.001 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Nickel 03/02/2020 P PowerSecure030220P 0.0063 / 1.30 mg/L OTW Mar 2020 Week 1 0.0063 / mg/L Mar 2020 Average 0.0063 / 1.00 mg/L 2020 Quarter 1 0.0063 / mg/L 2020 1st 6 Months (Avg) 0.0063 / mg/L 2020 1st 6 ...(Max) 0.0063 / mg/L 2020 1st 6 ...(Min) 0.0063 / mg/L 2020 1st 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 03/02/2020 P PowerSecure030220P 7.36 / 6.0 - 10.0 SU OTW Mar 2020 Week 1 7.36 / SU Mar 2020 Average 7.36 / SU 2020 Quarter 1 7.36 / SU 2020 1st 6 Months (Avg) 7.36 / SU 2020 1st 6 ...(Max) 7.36 / SU 2020 1st 6 ...(Min) 7.36 / SU 2020 1st 6 ...(Count) 1 / Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 5 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass /Limit Silver 03/02/2020 P PowerSecure030220P < 0.0003 / 0.43 mg/L < / OTW Mar 2020 Week 1 < 0.0003 / mg/L < / Mar 2020 Average < 0.0003 / 0.24 mg/L < / 2020 Quarter 1 < 0.0003 / mg/L < / 2020 1st 6 Months (Avg) < 0.0003 / mg/L < / 2020 1st 6 ...(Max) < 0.0003 / mg/L < / 2020 1st 6 ...(Min) < 0.0003 / mg/L < / 2020 1st 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Zinc 03/02/2020 P PowerSecure030220P 0.316 / 2.61 mg/L / OTW Mar 2020 Week 1 0.316 / mg/L / Mar 2020 Average 0.316 / 1.48 mg/L / 2020 Quarter 1 0.316 / mg/L / 2020 1st 6 Months (Avg) 0.316 / mg/L / 2020 1st 6 ...(Max) 0.316 / mg/L / 2020 1st 6 ...(Min) 0.316 / mg/L / 2020 1st 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 6 of 7 PowerSecure SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:59:13PM * Indicates Violation ** Indicates TRC Violation Page 7 of 7 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ammonia 01/28/2020 S SCM012820Se1f 02/07/2020 S SCM020720Se1f 04/30/2020 P SCM043020POTW Jan 2020 Week 4 Feb 2020 Week 1 Apr 2020 Week 4 Jan 2020 Average Feb 2020 Average Apr 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 6.7 / mg/L 4.4 / mg/L 2.7 / mg/L 6.7 / mg/L 4.4 / mg/L 2.7 / mg/L 6.7 / mg/L 4.4 / mg/L 2.7 / mg/L 5.55 / mg/L 2.7 / mg/L 4.6 / mg/L 6.7 / mg/L 2.7 / mg/L 3 / 2.9754 / lbs/day 1.6672 / lbs/day 0.245 / lbs/day 2.9754 / lbs/day 1.6672 / lbs/day 0.245 / lbs/day 2.9754 / lbs/day 1.6672 / lbs/day 0.245 / lbs/day 2.3213 / lbs/day 0.245 / lbs/day 1.6292 / lbs/day 2.9754 / lbs/day 0.2450 / lbs/day 3 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 01/31/2020 S SCM0120F1ow 0.012976 / 0.080 MGD / 02/28/2020 S SCM0220F1ow 0.010925 / 0.080 MGD / 03/31/2020 S SCM0320F1ow 0.006334 / 0.080 MGD / 04/30/2020 S SCM0420F1ow 0.00874 / 0.080 MGD / 05/31/2020 S SCM0520F1ow 0.010232 / 0.080 MGD / 06/30/2020 S SCM0620F1ow 0.009608 / 0.080 MGD / Jan 2020 Week 4 0.012976 / MGD / Feb 2020 Week 4 0.010925 / MGD / Mar 2020 Week 4 0.006334 / MGD / Apr 2020 Week 4 0.00874 / MGD / May 2020 Week 4 0.010232 / MGD / Jun 2020 Week 4 0.009608 / MGD / Jan 2020 Average 0.012976 / 0.050 MGD / Feb 2020 Average 0.010925 / 0.050 MGD / Mar 2020 Average 0.006334 / 0.050 MGD / Apr 2020 Average 0.00874 / 0.050 MGD / May 2020 Average 0.010232 / 0.050 MGD / Jun 2020 Average 0.009608 / 0.050 MGD / 2020 Quarter 1 0.010078 / MGD / 2020 Quarter 2 0.009174 / MGD / 2020 Quarter 2 0.010232 / MGD / 2020 Quarter 2 0.009174 / MGD / 2020 Quarter 2 0.010232 / MGD / 2020 1st 6 Months (Avg) 0.009803 / MGD / Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 2020 1st 6 ...(Max) 0.012976 / MGD 2020 1st 6 ...(Min) 0.006334 / MGD 2020 1st 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 5 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Cadmium 01/28/2020 S SCM012820Se1f < 0.0005 / mg/L < 0.000222 / lbs/day 02/07/2020 S SCM020720Se1f < 0.0005 / mg/L < 0.000189 / lbs/day 04/30/2020 P SCM043020POTW < 0.00008 / mg/L < 0.000007 / lbs/day Jan 2020 Week 4 < 0.0005 / mg/L < 0.000222 / lbs/day Feb 2020 Week 1 < 0.0005 / mg/L < 0.000189 / lbs/day Apr 2020 Week 4 < 0.00008 / mg/L < 0.000007 / lbs/day Jan 2020 Average < 0.0005 / mg/L < 0.000222 / lbs/day Feb 2020 Average < 0.0005 / mg/L < 0.000189 / lbs/day Apr 2020 Average < 0.00008 / mg/L < 0.000007 / lbs/day 2020 Quarter 1 < 0.0005 / mg/L < 0.000206 / lbs/day 2020 Quarter 2 < 0.00008 / mg/L < 0.000007 / lbs/day 2020 1st 6 Months (Avg) < 0.00036 / mg/L < 0.000139 / lbs/day 2020 1st 6 ...(Max) < 0.0005 / mg/L < 0.000222 / lbs/day 2020 1st 6 ...(Min) < 0.00008 / mg/L < 0.000007 / lbs/day 2020 1st 6 ...(Count) 3 / 3 / Sample Date SamplelD Result/Limit Mass/Limit Chloride 01/28/2020 S SCM012820Se1f 02/07/2020 S SCM020720Se1f 04/30/2020 P SCM043020POTW Jan 2020 Week 4 Feb 2020 Week 1 Apr 2020 Week 4 Jan 2020 Average Feb 2020 Average Apr 2020 Average 2020 Quarter 1 18.4 / mg/L 8.1712 / lbs/day 12.4 / mg/L 4.6984 / lbs/day 13 / mg/L 1.1798 / lbs/day 18.4 / mg/L 8.1712 / lbs/day 12.4 / mg/L 4.6984 / lbs/day 13 / mg/L 1.1798 / lbs/day 18.4 / mg/L 8.1712 / lbs/day 12.4 / mg/L 4.6984 / lbs/day 13 / mg/L 1.1798 / lbs/day 15.4 / mg/L 6.4348 / lbs/day Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chloride 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 13 / mg/L 14.6 / mg/L 18.4 / mg/L 12.4 / mg/L 3 / 1.1798 / lbs/day 4.6832 / lbs/day 8.1712 / lbs/day 1.1798 / lbs/day 3 / Sample Date SamplelD Result/Limit Mass/Limit Copper 01/28/2020 S SCM012820Se1f 0.174 / 0.75 mg/L 0.077271 / lbs/day 02/07/2020 S SCM020720Se1f 0.016 / 0.75 mg/L 0.006138 / lbs/day 04/30/2020 P SCM043020POTW 0.07 / 0.75 mg/L 0.006362 / lbs/day 05/15/2020 S SCM051520Se1f 0.025 / 0.75 mg/L 0.00438 / lbs/day Jan 2020 Week 4 0.174 / mg/L 0.077271 / lbs/day Feb 2020 Week 1 0.016 / mg/L 0.006138 / lbs/day Apr 2020 Week 4 0.07 / mg/L 0.006362 / lbs/day May 2020 Week 3 0.025 / mg/L 0.00438 / lbs/day Jan 2020 Average 0.174 / 0.50 mg/L 0.077271 / lbs/day Feb 2020 Average 0.016 / 0.50 mg/L 0.006138 / lbs/day Apr 2020 Average 0.07 / 0.50 mg/L 0.006362 / lbs/day May 2020 Average 0.025 / 0.50 mg/L 0.00438 / lbs/day 2020 Quarter 1 0.095 / mg/L 0.041705 / lbs/day 2020 Quarter 2 0.047 / mg/L 0.005371 / lbs/day 2020 1st 6 Months (Avg) 0.071 / mg/L 0.023538 / lbs/day 2020 1st 6 ...(Max) 0.174 / mg/L 0.077271 / lbs/day 2020 1st 6 ...(Min) 0.016 / mg/L 0.004380 / lbs/day 2020 1st 6 ...(Count) 4 / 4 / Sample Count : 4 Months Sampled : 4 Weeks Sampled : 4 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over QtrAvg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtrAvg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cyanide 02/07/2020 S SCM020720Se1f < 0.004 / 0.04 mg/L < 0.001516 / lbs/day 04/30/2020 P SCM043020POTW < 0.003 / 0.04 mg/L < 0.000227 / lbs/day Feb 2020 Week 1 < 0.004 / mg/L < 0.001516 / lbs/day Apr 2020 Week 4 < 0.003 / mg/L < 0.000227 / lbs/day Feb 2020 Average < 0.004 / 0.03 mg/L < 0.001516 / lbs/day Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Cyanide Apr 2020 Average < 0.003 / 0.03 mg/L < 0.000227 / lbs/day 2020 Quarter 1 < 0.004 / mg/L < 0.001516 / lbs/day 2020 Quarter 2 < 0.003 / mg/L < 0.000227 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.000871 / lbs/day 2020 1st 6 ...(Max) < 0.004 / mg/L < 0.001516 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < 0.000227 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 02/07/2020 S SCM020720Se1f < 0.05 / mg/L < 0.0189 / lbs/day 04/30/2020 P SCM043020POTW < 0.05 / mg/L < 0.0045 / lbs/day Feb 2020 Week 1 < 0.05 / mg/L < 0.0189 / lbs/day Apr 2020 Week 4 < 0.05 / mg/L < 0.0045 / lbs/day Feb 2020 Average < 0.05 / mg/L < 0.0189 / lbs/day Apr 2020 Average < 0.05 / mg/L < 0.0045 / lbs/day 2020 Quarter 1 < 0.05 / mg/L < 0.0189 / lbs/day 2020 Quarter 2 < 0.05 / mg/L < 0.0045 / lbs/day 2020 1st 6 Months (Avg) < 0.05 / mg/L < 0.0117 / lbs/day 2020 1st 6 ...(Max) < 0.05 / mg/L < 0.0189 / lbs/day 2020 1st 6 ...(Min) < 0.05 / mg/L < 0.0045 / lbs/day 2020 1st 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Lead 01/28/2020 S SCM012820Se1f < 0.0025 / 0.20 mg/L < 0.00111 / lbs/day 02/07/2020 S SCM020720Se1f < 0.0025 / 0.20 mg/L < 0.000947 / lbs/day 04/30/2020 P SCM043020POTW < 0.0003 / 0.20 mg/L < 0.000023 / lbs/day 05/15/2020 S SCM051520Se1f < 0.0025 / 0.20 mg/L < 0.000447 / lbs/day Jan 2020 Week 4 < 0.0025 / mg/L < 0.00111 / lbs/day Feb 2020 Week 1 < 0.0025 / mg/L < 0.000947 / lbs/day Apr 2020 Week 4 < 0.0003 / mg/L < 0.000023 / lbs/day May 2020 Week 3 < 0.0025 / mg/L < 0.000447 / lbs/day Jan 2020 Average < 0.0025 / 0.10 mg/L < 0.00111 / lbs/day Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 4 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Lead Feb 2020 Apr 2020 May 2020 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 4 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.0025 0.0003 0.0025 0.0025 0.0014 0.0019 0.0025 0.0003 4 Months Sampled : 0 0 0 0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L • 0.000947 / • 0.000023 / • 0.000447 / • 0.001029 / • 0.000235 / • 0.000632 / 0.001110 / • 0.000023 / 4 / 4 Weeks Sampled : 0/0 # 0.00 # Over Wk Avg C : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Wk Avg M TRC : 0 4 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 01/28/2020 S 02/07/2020 S 04/29/2020 P Jan 2020 Feb 2020 Apr 2020 Jan 2020 Feb 2020 Apr 2020 2020 2020 2020 2020 2020 2020 SCM012820Se1f SCM020720Se1f SCM042920POTWHg Week 4 Week 1 Week 4 Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.000007 0.000003 0.000001 0.000007 0.000003 0.000001 0.000007 0.000003 0.000001 0.000005 0.000001 0.000004 0.000007 0.000001 3 / 0.000142 / 0.000142 / 0.000142 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 5 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall:: 001 Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Molybdenum 01/28/2020 S SCM012820Se1f < 0.003 / mg/L < 0.0011 / lbs/day 02/07/2020 S SCM020720Se1f 0.169 / mg/L 0.064 / lbs/day 04/30/2020 P SCM043020POTW < 0.001 / mg/L < 0.0001 / lbs/day Jan 2020 Week 4 < 0.003 / mg/L < 0.0011 / lbs/day Feb 2020 Week 1 0.169 / mg/L 0.064 / lbs/day Apr 2020 Week 4 < 0.001 / mg/L < 0.0001 / lbs/day Jan 2020 Average < 0.003 / mg/L < 0.0011 / lbs/day Feb 2020 Average 0.169 / mg/L 0.064 / lbs/day Apr 2020 Average < 0.001 / mg/L < 0.0001 / lbs/day 2020 Quarter 1 < 0.086 / mg/L < 0.0326 / lbs/day 2020 Quarter 2 < 0.001 / mg/L < 0.0001 / lbs/day 2020 1st 6 Months (Avg) < 0.058 / mg/L < 0.0217 / lbs/day 2020 1st 6 ...(Max) 0.169 / mg/L 0.0640 / lbs/day 2020 1st 6 ...(Min) < 0.001 / mg/L < 0.0001 / lbs/day 2020 1st 6 ...(Count) 3 / 3 / Sample Date SamplelD Result/Limit Mass /Limit Nickel 01/28/2020 S SCM012820Se1f 02/07/2020 S SCM020720Se1f 04/30/2020 P SCM043020POTW Jan 2020 Week 4 Feb 2020 Week 1 Apr 2020 Week 4 Jan 2020 Average Feb 2020 Average Apr 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) < 0.0025 / mg/L < 0.00111 / lbs/day 0.0776 / mg/L 0.029403 / lbs/day 0.0011 / mg/L 0.000102 / lbs/day < 0.0025 / mg/L < 0.00111 / lbs/day 0.0776 / mg/L 0.029403 / lbs/day 0.0011 / mg/L 0.000102 / lbs/day < 0.0025 / mg/L < 0.00111 / lbs/day 0.0776 / mg/L 0.029403 / lbs/day 0.0011 / mg/L 0.000102 / lbs/day < 0.0401 / mg/L < 0.015257 / lbs/day 0.0011 / mg/L 0.000102 / lbs/day < 0.0271 / mg/L < 0.010205 / lbs/day 0.0776 / mg/L 0.029403 / lbs/day 0.0011 / mg/L 0.000102 / lbs/day 3 / 3 / Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 6 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 01/28/2020 02/07/2020 04/30/2020 Jan 2020 Feb 2020 Apr 2020 Jan 2020 Feb 2020 Apr 2020 2020 2020 2020 2020 2020 2020 S SCM012820Se1f S SCM020720Se1f P SCM043020POTW Week 4 Week 1 Week 4 Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.5 0.7 0.4 0.5 0.7 0.4 0.5 0.7 0.4 0.6 0.4 0.5 0.7 0.4 3 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.218 0.25 0.033 0.218 0.25 0.033 0.218 0.25 0.033 0.234 0.033 0.167 0.250 0.033 3 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 01/28/2020 02/07/2020 04/30/2020 Jan 2020 Feb 2020 Apr 2020 Jan 2020 Feb 2020 Apr 2020 2020 2020 2020 2020 2020 2020 S SCM012820Se1f S SCM020720Se1f P SCM043020POTW Week 4 Week 1 Week 4 Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 14.3 10.6 4.6 14.3 10.6 4.6 14.3 10.6 4.6 12.45 4.6 9.83 14.3 4.6 3 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 6.35 4.016 0.417 6.35 4.016 0.417 6.35 4.016 0.417 5.183 0.417 3.595 6.350 0.417 3 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 01/28/2020 02/07/2020 04/30/2020 Feb 2020 Jan 2020 Apr 2020 S SCM012820Se1f S SCM020720Se1f P SCM043020POTW Week 1 Week 4 Week 4 9.2 / 200 2.5 / 200 2.5 / 200 2.5 / 9.2 / 2.5 / mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 7 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total Jan 2020 Average 9.2 / mg/L / Feb 2020 Average < 2.5 / mg/L < / Apr 2020 Average < 2.5 / mg/L < / 2020 Quarter 1 < 5.85 / mg/L < / 2020 Quarter 2 < 2.5 / mg/L < / 2020 1st 6 Months (Avg) < 4.73 / mg/L < / 2020 1st 6 ...(Max) 9.2 / mg/L / 2020 1st 6 ...(Min) < 2.5 / mg/L < / 2020 1st 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 01/28/2020 S SCM012820Se1f 02/07/2020 S SCM020720Se1f 04/30/2020 P SCM043020POTW 05/15/2020 S SCM051520Se1f Jan 2020 Week 4 Feb 2020 Week 1 Apr 2020 Week 4 May 2020 Week 3 Jan 2020 Average Feb 2020 Average Apr 2020 Average May 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 6.9 /6.0-10.5 SU / 6.6 /6.0-10.5 SU / 7.4 /6.0-10.5 SU / 6.8 /6.0-10.5 SU / 6.9 / SU / 6.6 / SU / 7.4 / SU / 6.8 / SU / 6.9 / SU / 6.6 / SU / 7.4 / SU / 6.8 / SU / 6.75 / SU / 7.1 / SU / 6.93 / SU / 7.4 / SU / 6.6 / SU / 4 / / Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 8 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 4 Months Sampled : 4 Weeks Sampled : 4 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Selenium 01/28/2020 S SCM012820Se1f < 0.005 / mg/L < 0.00222 / lbs/day 02/07/2020 S SCM020720Se1f < 0.005 / mg/L < 0.001895 / lbs/day 04/30/2020 P SCM043020POTW < 0.0005 / mg/L < 0.000045 / lbs/day Jan 2020 Week 4 < 0.005 / mg/L < 0.00222 / lbs/day Feb 2020 Week 1 < 0.005 / mg/L < 0.001895 / lbs/day Apr 2020 Week 4 < 0.0005 / mg/L < 0.000045 / lbs/day Jan 2020 Average < 0.005 / mg/L < 0.00222 / lbs/day Feb 2020 Average < 0.005 / mg/L < 0.001895 / lbs/day Apr 2020 Average < 0.0005 / mg/L < 0.000045 / lbs/day 2020 Quarter 1 < 0.005 / mg/L < 0.002057 / lbs/day 2020 Quarter 2 < 0.0005 / mg/L < 0.000045 / lbs/day 2020 1st 6 Months (Avg) < 0.0035 / mg/L < 0.001387 / lbs/day 2020 1st 6 ...(Max) < 0.005 / mg/L < 0.002220 / lbs/day 2020 1st 6 ...(Min) < 0.0005 / mg/L < 0.000045 / lbs/day 2020 1st 6 ...(Count) 3 / 3 / Sample Date SamplelD Result/Limit Mass /Limit Temperature 01/28/2020 S SCM012820Se1f 13.5 / 66 °C / 02/07/2020 S SCM020720Se1f 14.3 / 66 °C / 04/30/2020 P SCM043020POTW 19 / 66 °C / 05/15/2020 S SCM051520Se1f 22.1 / 66 °C / Jan 2020 Week 4 13.5 / °C / Feb 2020 Week 1 14.3 / °C / Apr 2020 Week 4 19 / °C / May 2020 Week 3 22.1 / °C / Jan 2020 Average 13.5 / °C / Feb 2020 Average 14.3 / °C / Apr 2020 Average 19 / °C / May 2020 Average 22.1 / °C / 2020 Quarter 1 13.9 / °C / 2020 Quarter 2 20.6 / °C / 2020 1st 6 Months (Avg) 17.2 / °C / 2020 1st 6 ...(Max) 22.1 / °C / Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 9 of 11 SCM Metal Products, Inc. # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Temperature 2020 2020 1st 6 ...(Min) 1st 6 ...(Count) Sample Count : 0 0 0 0 0 0 4 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 13.5 / 4 / Months Sampled : 0 0 0 0 °C 4 Weeks Sampled : 4 #0/0 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtAvg C: # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit TKN 01/28/2020 02/07/2020 04/30/2020 Jan 2020 Feb 2020 Apr 2020 Jan 2020 Feb 2020 Apr 2020 2020 2020 2020 2020 2020 2020 S SCM012820Se1f S SCM020720Se1f P SCM043020POTW Week 4 Week 1 Week 4 Average Average Average Quarter 1 Quarter 2 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 13.8 / 10 / 4.24 / 13.8 / 10 / 4.24 / 13.8 / 10 / 4.24 / 11.9 / 4.24 / 9.35 / 13.8 / 4.24 / 3 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 6.128 / 3.789 / 0.385 / 6.128 / 3.789 / 0.385 / 6.128 / 3.789 / 0.385 / 4.959 / 0.385 / 3.434 / 6.128 / 0.385 / 3 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 01/28/2020 S 02/07/2020 S 04/30/2020 P Jan 2020 Feb 2020 Apr 2020 Jan 2020 Feb 2020 Apr 2020 2020 2020 SCM012820Se1f SCM020720Se1f SCM043020POTW Week 4 Week 1 Week 4 Average Average Average Quarter 1 Quarter 2 2.9 / 1.5 / 0.902 / 2.9 / 1.5 / 0.902 / 2.9 / 1.5 / 0.902 / 2.2 / 0.902 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1.2879 / 0.5684 / 0.0819 / 1.2879 / 0.5684 / 0.0819 / 1.2879 / 0.5684 / 0.0819 / 0.9281 / 0.0819 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 10 of 11 SCM Metal Products, Inc. SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 2020 1st 6 Months (Avg) 1.767 / mg/L 2020 1st 6 ...(Max) 2.9 / mg/L 2020 1st 6 ...(Min) 0.902 / mg/L 2020 1st 6 ...(Count) 3 / 0.6460 / lbs/day 1.2879 / lbs/day 0.0819 / lbs/day 3 / Sample Date SamplelD Result / Limit Mass / Limit VOC 01/28/2020 S SCM012820Se1f 0.0194 / mg/L / 02/07/2020 S SCM020720Se1f 0.109 / mg/L / Jan 2020 Week 4 0.0194 / mg/L / Feb 2020 Week 1 0.109 / mg/L / Jan 2020 Average 0.0194 / mg/L / Feb 2020 Average 0.109 / mg/L / 2020 Quarter 1 0.0642 / mg/L / 2020 1st 6 Months (Avg) 0.0642 / mg/L / 2020 1st 6 ...(Max) 0.109 / mg/L / 2020 1st 6 ...(Min) 0.0194 / mg/L / 2020 1st 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass /Limit Zinc 01/28/2020 S SCM012820Se1f 02/07/2020 S SCM020720Se1f 04/30/2020 P SCM043020POTW Jan 2020 Week 4 Feb 2020 Week 1 Apr 2020 Week 4 Jan 2020 Average Feb 2020 Average Apr 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 0.53 / mg/L 0.235367 / lbs/day 0.069 / mg/L 0.02622 / lbs/day 0.386 / mg/L 0.035032 / lbs/day 0.53 / mg/L 0.235367 / lbs/day 0.069 / mg/L 0.02622 / lbs/day 0.386 / mg/L 0.035032 / lbs/day 0.53 / mg/L 0.235367 / lbs/day 0.069 / mg/L 0.02622 / lbs/day 0.386 / mg/L 0.035032 / lbs/day 0.3 / mg/L 0.130793 / lbs/day 0.386 / mg/L 0.035032 / lbs/day 0.328 / mg/L 0.098873 / lbs/day 0.53 / mg/L 0.235367 / lbs/day 0.069 / mg/L 0.026220 / lbs/day 3 / 3 / Wednesday, February 24, 2021 8:49:30PM * Indicates Violation ** Indicates TRC Violation Page 11 of 11 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result / Limit Mass /Limit Ammonia 02/11/2020 S UTP1021120Se1f 03/19/2020 P UTP1031920POTW Feb 2020 Week 2 Mar 2020 Week 3 Feb 2020 Average Mar 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 4 / mg/L 1.1 / mg/L 4 / mg/L 1.1 / mg/L 4 / mg/L 1.1 / mg/L 2.55 / mg/L 2.55 / mg/L 4 / mg/L 1.1 / mg/L 2 / 0.2167 / lbs/day 0.2167 / lbs/day 0.2167 / lbs/day 0.2167 / lbs/day 0.2167 / lbs/day 0.2167 / lbs/day Sample Date SamplelD Result / Limit Mass/Limit Average Flow for Month 01/31/2020 S UTP10120Flow 0.026748 / MGD / 02/28/2020 S UTP10220Flow 0.023949 / MGD / 03/31/2020 S UTP10320Flow 0.025252 / MGD / 04/30/2020 S UTP10420Flow 0.022558 / MGD / 05/31/2020 S UTP10520Flow 0.023476 / MGD / 06/30/2020 S UTP10620Flow 0.029907 / MGD / Jan 2020 Week 4 0.026748 / MGD / Feb 2020 Week 4 0.023949 / MGD / Mar 2020 Week 4 0.025252 / MGD / Apr 2020 Week 4 0.022558 / MGD / May 2020 Week 4 0.023476 / MGD / Jun 2020 Week 4 0.029907 / MGD / Jan 2020 Average 0.026748 / 0.050 MGD / Feb 2020 Average 0.023949 / 0.050 MGD / Mar 2020 Average 0.025252 / 0.050 MGD / Apr 2020 Average 0.022558 / 0.050 MGD / May 2020 Average 0.023476 / MGD / Jun 2020 Average 0.029907 / MGD / 2020 Quarter 1 0.025316 / MGD / 2020 Quarter 2 0.026692 / MGD / 2020 Quarter 2 0.022558 / MGD / 2020 Quarter 2 0.026692 / MGD / 2020 Quarter 2 0.022558 / MGD / 2020 1st 6 Months (Avg) 0.025315 / MGD / 2020 1st 6 ...(Max) 0.029907 / MGD / 2020 1st 6...(Min) 0.022558 / MGD / 2020 1st 6 ...(Count) 6 / / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 1 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 6 Months Sampled : 6 # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Weeks Sampled : 6 Quarters Sampled : 5 # % # 0 0.00 # Over Qt Avg C : 0 0.00 0 0.00 # Over Qt Avg C TRC : 0 0.00 0 0.00 # Over Qtr Avg M : 0 0.00 0 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit BOD 02/11/2020 S UTP1021120Se1f 03/19/2020 P UTP1031920POTW Feb 2020 Week 2 Mar 2020 Week 3 Feb 2020 Average Mar 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 92.1 / mg/L / 72.1 / mg/L 14.203 / lbs/day 92.1 / mg/L / 72.1 / mg/L 14.203 / lbs/day 92.1 / mg/L / 72.1 / mg/L 14.203 / lbs/day 82.1 / mg/L 14.203 / lbs/day 82.1 / mg/L 14.203 / lbs/day 92.1 / mg/L 14.203 / lbs/day 72.1 / mg/L / 2 / 1 / Sample .Date SamplelD Result / Limit Mass / Limit Cadmium 02/11/2020 S UTP1021120Se1f < 0.0005 / mg/L < / 03/19/2020 P UTP1031920POTW < 0.00008 / mg/L < 0.000015 / lbs/day Feb 2020 Week 2 < 0.0005 / mg/L < / Mar 2020 Week 3 < 0.00008 / mg/L < 0.000015 / lbs/day Feb 2020 Average < 0.0005 / mg/L < / Mar 2020 Average < 0.00008 / mg/L < 0.000015 / lbs/day 2020 Quarter 1 < 0.00029 / mg/L < 0.000015 / lbs/day 2020 1st 6 Months (Avg) < 0.00029 / mg/L < 0.000015 / lbs/day 2020 1st 6 ...(Max) < 0.0005 / mg/L < 0.000015 / lbs/day 2020 1st 6 ...(Min) < 0.00008 / mg/L < / 2020 1st 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Chloride 02/11/2020 S UTP1021120Se1f 03/19/2020 P UTP1031920POTW Feb 2020 Week 2 Mar 2020 Week 3 Feb 2020 Average Mar 2020 Average 43.3 / mg/L 33 / mg/L 43.3 / mg/L 33 / mg/L 43.3 / mg/L 33 / mg/L 6.5007 / 6.5007 / 6.5007 / lbs/day lbs/day lbs/day Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 2 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chloride 2020 Quarter 1 38.15 / mg/L 2020 1st 6 Months (Avg) 38.15 / mg/L 2020 1st 6 ...(Max) 43.3 / mg/L 2020 1st 6 ...(Min) 33 / mg/L 2020 1st 6 ...(Count) 2 / 6.5007 / lbs/day 6.5007 / lbs/day 6.5007 / lbs/day Sample Date SamplelD Result/Limit Mass/Limit COD 02/11/2020 S UTP1021120Se1f 03/19/2020 P UTP1031920POTW Feb 2020 Week 2 Mar 2020 Week 3 Feb 2020 Average Mar 2020 Average 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 296 / mg/L / 158 / mg/L 31.12 / lbs/day 296 / mg/L / 158 / mg/L 31.12 / lbs/day 296 / mg/L / 158 / mg/L 31.12 / lbs/day 227 / mg/L 31.12 / lbs/day 227 / mg/L 31.12 / lbs/day 296 / mg/L 31.12 / lbs/day 158 / mg/L / 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Cyanide 02/11/2020 S UTP1021120Se1f < 0.004 / mg/L < / 03/19/2020 P UTP1031920POTW < 0.003 / mg/L < 0.000492 / lbs/day Feb 2020 Week 2 < 0.004 / mg/L < / Mar 2020 Week 3 < 0.003 / mg/L < 0.000492 / lbs/day Feb 2020 Average < 0.004 / mg/L < / Mar 2020 Average < 0.003 / mg/L < 0.000492 / lbs/day 2020 Quarter 1 < 0.003 / mg/L < 0.000492 / lbs/day 2020 1st 6 Months (Avg) < 0.003 / mg/L < 0.000492 / lbs/day 2020 1st 6 ...(Max) < 0.004 / mg/L < 0.000492 / lbs/day 2020 1st 6 ...(Min) < 0.003 / mg/L < / 2020 1st 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Fluoride 02/11/2020 S UTP1021120Se1f < 0.05 / mg/L < / 03/19/2020 P UTP1031920POTW < 0.05 / mg/L < 0.0098 / lbs/day Feb 2020 Week 2 < 0.05 / mg/L < / Mar 2020 Week 3 < 0.05 / mg/L < 0.0098 / lbs/day Feb 2020 Average < 0.05 / mg/L < / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 3 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Dute SamplelD Result /Limit Mass /Limit Fluoride Mar 2020 Average < 0.05 / mg/L < 0.0098 / lbs/day 2020 Quarter 1 < 0.05 / mg/L < 0.0098 / lbs/day 2020 1st 6 Months (Avg) < 0.05 / mg/L < 0.0098 / lbs/day 2020 1st 6 ...(Max) < 0.05 / mg/L < 0.0098 / lbs/day 2020 1st 6 ...(Min) < 0.05 / mg/L < / 2020 1st 6 ...(Count) 2 / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 01/28/2020 S UTP1012820Se1fHg 0.000004 / 0.000142 mg/L / 02/11/2020 S UTP1021120Se1f 0.000026 / 0.000142 mg/L / 03/17/2020 S UTP1031720Se1f 0.000002 / 0.000142 mg/L / 03/18/2020 P UTP1031820POTWHg 0.00003 / 0.000142 mg/L / 04/21/2020 S UTP1042120Se1f 0.000006 / 0.000142 mg/L / 05/08/2020 S UTP1050820Se1ffig 0.00001 / 0.000142 mg/L / Feb 2020 Week 2 0.000026 / mg/L / Jan 2020 Week 4 0.000004 / mg/L / Mar 2020 Week 3 0.000016 / mg/L / Apr 2020 Week 3 0.000006 / mg/L / May 2020 Week 2 0.00001 / mg/L / Jan 2020 Average 0.000004 / mg/L / Feb 2020 Average 0.000026 / mg/L / Mar 2020 Average 0.000016 / mg/L / Apr 2020 Average 0.000006 / mg/L / May 2020 Average 0.00001 / mg/L / 2020 Quarter 1 0.000016 / mg/L / 2020 Quarter 2 0.000008 / mg/L / 2020 1st 6 Months (Avg) 0.000013 / mg/L / 2020 1st 6 ...(Max) 0.00003 / mg/L / 2020 1st 6 ...(Min) 0.000002 / mg/L / 2020 1st 6 ...(Count) 6 / / Sample Count : 6 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Dute SamplelD Result/Limit Mass /Limit Molybdenum Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 4 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 0.003 / 0.001 / 0.003 / 0.001 / 0.003 / 0.001 / 0.002 / 0.002 / 0.003 / 0.001 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.0002 / 0.0002 / 0.0002 / 0.0002 / 0.0002 / 0.0002 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit Nitrate -Nitrite 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 0.7 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.138 / 0.138 / 0.138 / 0.138 / 0.138 / 0.138 / 1 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) lst 6 ...(Count) 22.7 / 8.24 / 22.7 / 8.24 / 22.7 / 8.24 / 15.47 / 15.47 / 22.7 / 8.24 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1.623 / 1.623 / 1.623 / 1.623 / 1.623 / 1.623 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 5 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 02/11/2020 S UTP1021120Se1f < 2.5 / 200 mg/L < / 03/19/2020 P UTP1031920POTW < 2.5 / 200 mg/L < / Feb 2020 Week 2 < 2.5 / mg/L < / Mar 2020 Week 3 < 2.5 / mg/L < / Feb 2020 Average < 2.5 / mg/L < / Mar 2020 Average < 2.5 / mg/L < / 2020 Quarter 1 < 2.5 / mg/L < / 2020 1st 6 Months (Avg) < 2.5 / mg/L < / 2020 1st 6 ...(Max) < 2.5 / mg/L < / 2020 1st 6 ...(Min) < 2.5 / mg/L < / 2020 1st 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit pH 01/28/2020 S UTP1012820Se1f {g 02/11/2020 S UTP1021120Se1f 03/17/2020 S UTP1031720Se1f 03/19/2020 P UTP1031920POTW 04/21/2020 S UTP1042120Se1f 05/08/2020 S UTP1050820Se1f {g Jan 2020 Week 4 Feb 2020 Week 2 Mar 2020 Week 3 Apr 2020 Week 3 May 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 6.7 /5.5-10 SU / 7.4 /5.5-10 SU / 6.4 /5.5-10 SU / 7.7 /5.5-10 SU / 7.7 /5.5-10 SU / 7.5 /5.5-10 SU / 6.7 / SU / 7.4 / SU / 7.05 / SU / 7.7 / SU / 7.5 / SU / 6.7 / SU / 7.4 / SU / 7.05 / SU / 7.7 / SU / 7.5 / SU / 7.05 / SU / 7.6 / SU / 7.23 / SU / 7.7 / SU / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 6 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 6.4 / SU 6 / Sample Count : 6 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Temperature 01/28/2020 S UTP1012820Se1flg 02/11/2020 S UTP1021120Se1f 03/17/2020 S UTP1031720Se1f 03/19/2020 P UTP1031920POTW 04/21/2020 S UTP1042120Se1f 05/08/2020 S UTP1050820Se1flg Jan 2020 Week 4 Feb 2020 Week 2 Mar 2020 Week 3 Apr 2020 Week 3 May 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average 2020 Quarter 1 2020 Quarter 2 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 18.8 / 66 °C / 19.7 / 66 °C / 19.7 / 66 °C / 19 / 66 °C / 20.9 / 66 °C / 22 / 66 °C / 18.8 / °C / 19.7 / °C / 19.4 / °C / 20.9 / °C / 22 / °C / 18.8 / °C / 19.7 / °C / 19.4 / °C / 20.9 / °C / 22 / °C / 19.3 / °C / 21.5 / °C / 20.0 / °C / 22 / °C / 18.8 / °C / 6 / / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 7 of 9 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 0 0 0 0 0 0 6 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : Months Sampled : 0 0 0 0 5 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 5 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit TKN 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 22 / 7.54 / 22 / 7.54 / 22 / 7.54 / 14.77 / 14.77 / 22 / 7.54 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1.485 / 1.485 / 1.485 / 1.485 / 1.485 / 1.485 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit Total Phosphorus 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 2.8 / 1.48 / 2.8 / 1.48 / 2.8 / 1.48 / 2.14 / 2.14 / 2.8 / 1.48 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.2915 / 0.2915 / 0.2915 / 0.2915 / 0.2915 / 0.2915 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit TSS 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average 53.6 / 56 / 53.6 / 56 / 53.6 / 56 / mg/L mg/L mg/L mg/L mg/L mg/L 11.031485 / 11.031485 / 11.031485 / lbs/day lbs/day lbs/day Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 8 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TSS 2020 Quarter 1 2020 1st 6 Months (Avg) 2020 1st 6 ...(Max) 2020 1st 6 ...(Min) 2020 1st 6 ...(Count) 54.8 / mg/L 54.8 / mg/L 56 / mg/L 53.6 / mg/L 2 / 11.031485 / lbs/day 11.0315 / lbs/day 11.031485 / lbs/day Sample Date SamplelD Result/Limit Mass/Limit VOC 02/11/2020 S UTP1021120Se1f 0.0879 / mg/L / Feb 2020 Week 2 0.0879 / mg/L / Feb 2020 Average 0.0879 / mg/L / 2020 Quarter 1 0.0879 / mg/L / 2020 1st 6 Months (Avg) 0.0879 / mg/L / 2020 1st 6 ...(Max) 0.0879 / mg/L / 2020 1st 6 ...(Min) 0.0879 / mg/L / 2020 1st 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Zinc 02/11/2020 03/19/2020 Feb 2020 Mar 2020 Feb 2020 Mar 2020 2020 2020 2020 2020 2020 S UTP1021120Se1f P UTP1031920POTW Week 2 Week 3 Average Average Quarter 1 1st 6 Months (Avg) 1st 6 ...(Max) 1st 6 ...(Min) 1st 6 ...(Count) 0.45 / mg/L 0.269 / mg/L 0.052991 / lbs/day 0.45 / mg/L / 0.269 / mg/L 0.052991 / lbs/day 0.45 / mg/L 0.269 / mg/L 0.36 / mg/L 0.360 / mg/L 0.45 / mg/L 0.269 / mg/L 2 / 0.052991 / lbs/day 0.052991 / lbs/day 0.052991 / lbs/day 0.052991 / lbs/day 1 / 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit Acetone 01/28/2020 S UTP2012820Se1f 02/11/2020 S UTP2021120Se1f 03/17/2020 S UTP2031720Se1f 04/21/2020 S UTP2042120Se1f 05/08/2020 S UTP2050820Se1f Jan 2020 Week 4 9.6 / 20.7 mg/L 4.34 / 20.7 mg/L 6.57 / 20.7 mg/L 0.348 / 20.7 mg/L 5.4 / 20.7 mg/L 9.6 / mg/L Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 9 of 9 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit Acetone Feb 2020 Week 2 4.34 / mg/L Mar 2020 Week 3 6.57 / mg/L Apr 2020 Week 3 0.348 / mg/L May 2020 Week 2 5.4 / mg/L Jan 2020 Average 9.6 / 8.2 mg/L Feb 2020 Average 4.34 / 8.2 mg/L Mar 2020 Average 6.57 / 8.2 mg/L Apr 2020 Average 0.348 / 8.2 mg/L May 2020 Average 5.4 / 8.2 mg/L 2020 Quarter 1 6.837 / mg/L 2020 Quarter 2 2.874 / mg/L 2020 1st 6 Months (Avg) 5.252 / mg/L 2020 1st 6 ...(Max) 9.6 / mg/L 2020 1st 6 ...(Min) 0.348 / mg/L 2020 1st 6 ...(Count) 5 / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 1 20.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 01/28/2020 S UTP2012820Se1f 02/11/2020 S UTP2021120Se1f 03/17/2020 S UTP2031720Se1f 04/21/2020 S UTP2042120Se1f 05/08/2020 S UTP2050820Se1f Jan 2020 Week 4 Feb 2020 Week 2 Mar 2020 Week 3 Apr 2020 Week 3 May 2020 Week 2 Jan 2020 Average Feb 2020 Average Mar 2020 Average Apr 2020 Average May 2020 Average 2020 Quarter 1 < 0.05 / 20.7 mg/L < / < 0.05 / 20.7 mg/L < / < 0.05 / 20.7 mg/L < / < 0.05 / 20.7 mg/L < / < 0.05 / 20.7 mg/L < / < 0.05 / mg/L < / < 0.05 / mg/L < / < 0.05 / mg/L < / < 0.05 / mg/L < / < 0.05 / mg/L < / < 0.05 / 8.2 mg/L < / < 0.05 / 8.2 mg/L < / < 0.05 / 8.2 mg/L < / < 0.05 / 8.2 mg/L < / < 0.05 / 8.2 mg/L < / < 0.05 / mg/L < / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 1 of 4 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result / Limit Mass /Limit Ethyl acetate 2020 Quarter 2 < 0.05 / mg/L < / 2020 1st 6 Months (Avg) < 0.05 / mg/L < / 2020 1st 6...(Max) < 0.05 / mg/L < / 2020 1st 6...(Min) < 0.05 / mg/L < / 2020 1st 6 ...(Count) 5 / / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit Isopropyl acetate 01/28/2020 S UTP2012820Se1f < 0.05 / 20.7 mg/L < / 02/11/2020 S UTP2021120SeIf < 0.05 / 20.7 mg/L < / 03/17/2020 S UTP2031720Se1f < 0.05 / 20.7 mg/L < / 04/21/2020 S UTP2042120Se1f < 0.05 / 20.7 mg/L < / 05/08/2020 S UTP2050820Se1f < 0.05 / 20.7 mg/L < / Jan 2020 Week 4 < 0.05 / mg/L < / Feb 2020 Week 2 < 0.05 / mg/L < / Mar 2020 Week 3 < 0.05 / mg/L < / Apr 2020 Week 3 < 0.05 / mg/L < / May 2020 Week 2 < 0.05 / mg/L < / Jan 2020 Average < 0.05 / 8.2 mg/L < / Feb 2020 Average < 0.05 / 8.2 mg/L < / Mar 2020 Average < 0.05 / 8.2 mg/L < / Apr 2020 Average < 0.05 / 8.2 mg/L < / May 2020 Average < 0.05 / 8.2 mg/L < / 2020 Quarter 1 < 0.05 / mg/L < / 2020 Quarter 2 < 0.05 / mg/L < / 2020 1st 6 Months (Avg) < 0.05 / mg/L < / 2020 1st 6...(Max) < 0.05 / mg/L < / 2020 1st 6...(Min) < 0.05 / mg/L < / 2020 1st 6 ...(Count) 5 / / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 2 of 4 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Count : 5 Months Sampled : 5 # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Weeks Sampled : 5 Quarters Sampled : 2 # % # 0 0.00 # Over Qt Avg C : 0 0.00 0 0.00 # Over Qt Avg C TRC : 0 0.00 0 0.00 # Over Qtr Avg M : 0 0.00 0 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Methylene Chloride 01/28/2020 S UTP2012820Se1f < 0.001 / 3 mg/L < / 02/11/2020 S UTP2021120Se1f < 0.001 / 3 mg/L < / 03/17/2020 S UTP2031720Se1f < 0.001 / 3 mg/L < / 04/21/2020 S UTP2042120Se1f < 0.001 / 3 mg/L < / 05/08/2020 S UTP2050820Se1f < 0.001 / 3 mg/L < / Jan 2020 Week 4 < 0.001 / mg/L < / Feb 2020 Week 2 < 0.001 / mg/L < / Mar 2020 Week 3 < 0.001 / mg/L < / Apr 2020 Week 3 < 0.001 / mg/L < / May 2020 Week 2 < 0.001 / mg/L < / Jan 2020 Average < 0.001 / 0.7 mg/L < / Feb 2020 Average < 0.001 / 0.7 mg/L < / Mar 2020 Average < 0.001 / 0.7 mg/L < / Apr 2020 Average < 0.001 / 0.7 mg/L < / May 2020 Average < 0.001 / 0.7 mg/L < / 2020 Quarter 1 < 0.001 / mg/L < / 2020 Quarter 2 < 0.001 / mg/L < / 2020 1st 6 Months (Avg) < 0.001 / mg/L < / 2020 1st 6 ...(Max) < 0.001 / mg/L < / 2020 1st 6 ...(Min) < 0.001 / mg/L < / 2020 1st 6 ...(Count) 5 / / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit n-Amyl acetate 01/28/2020 S UTP2012820Se1f < 0.025 / 20.7 mg/L < / 02/11/2020 S UTP2021120Se1f < 0.025 / 20.7 mg/L < / Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 3 of 4 United Therapeutics Corporation SAMPLE OVERVIEW 1/1/2020 To 6/30/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit n-Amyl acetate 03/17/2020 S UTP2031720Se1f < 0.025 / 20.7 mg/L < / 04/21/2020 S UTP2042120Se1f < 0.025 / 20.7 mg/L < / 05/08/2020 S UTP2050820Se1f < 0.025 / 20.7 mg/L < / Jan 2020 Week 4 < 0.025 / mg/L < / Feb 2020 Week 2 < 0.025 / mg/L < / Mar 2020 Week 3 < 0.025 / mg/L < / Apr 2020 Week 3 < 0.025 / mg/L < / May 2020 Week 2 < 0.025 / mg/L < / Jan 2020 Average < 0.025 / 8.2 mg/L < / Feb 2020 Average < 0.025 / 8.2 mg/L < / Mar 2020 Average < 0.025 / 8.2 mg/L < / Apr 2020 Average < 0.025 / 8.2 mg/L < / May 2020 Average < 0.025 / 8.2 mg/L < / 2020 Quarter 1 < 0.025 / mg/L < / 2020 Quarter 2 < 0.025 / mg/L < / 2020 1st 6 Months (Avg) < 0.025 / mg/L < / 2020 1st 6 ...(Max) < 0.025 / mg/L < / 2020 1st 6 ...(Min) < 0.025 / mg/L < / 2020 1st 6 ...(Count) 5 / / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 8:50:54PM * Indicates Violation ** Indicates TRC Violation Page 4 of 4 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 08/17/2020 S AstraZeneca081720Se1 < 0.025 / 20.7 mg/L < / f 10/26/2020 P AstraZeneca102620PO < 0.025 / 20.7 mg/L < / TW Aug 2020 Week 3 < 0.025 / mg/L < / Oct 2020 Week 4 < 0.025 / mg/L < / Aug 2020 Average < 0.025 / 8.2 mg/L < / Oct 2020 Average < 0.025 / 8.2 mg/L < / 2020 Quarter 3 < 0.025 / mg/L < / 2020 Quarter 4 < 0.025 / mg/L < / 2020 2nd 6 Months (Avg) < 0.025 / mg/L < / 2020 2nd 6 ...(Max) < 0.025 / mg/L < / 2020 2nd 6 ...(Min) < 0.025 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/31/2020 S AstraZeneca0720F1ow 0.000939 / MGD 08/31/2020 S AstraZeneca0820F1ow 0.00042 / MGD 09/30/2020 S AstraZeneca0920F1ow 0.000205 / MGD 10/31/2020 S AstraZeneca1020F1ow 0.000746 / MGD 11/30/2020 S AstraZeneca1120Flow 0.000294 / MGD 12/31/2020 S AstraZeneca1220F1ow 0.000077 / MGD Jul 2020 Week 4 0.000939 / MGD Aug 2020 Week 4 0.00042 / MGD Sep 2020 Week 4 0.000205 / MGD Oct 2020 Week 4 0.000746 / MGD Nov 2020 Week 4 0.000294 / MGD Dec 2020 Week 4 0.000077 / MGD Jul 2020 Average 0.000939 / 0.002000 MGD Aug 2020 Average 0.00042 / 0.002000 MGD Sep 2020 Average 0.000205 / 0.002000 MGD Oct 2020 Average 0.000746 / 0.002000 MGD Nov 2020 Average 0.000294 / 0.002000 MGD Dec 2020 Average 0.000077 / 0.002000 MGD Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 1 of 6 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 2020 Quarter 3 0.000521 / MGD 2020 Quarter 4 0.000372 / MGD 2020 2nd 6 Months (Avg) 0.000447 / MGD 2020 2nd 6 ...(Max) 0.000939 / MGD 2020 2nd 6 ...(Min) 0.000077 / MGD 2020 2nd 6 ...(Count) 6 / Sample Count : 1 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # rye # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit COD 08/17/2020 S AstraZeneca081720Se1 < 7.5 / mg/L < / f 10/26/2020 P AstraZeneca102620PO < 7.5 / mg/L < / TW Aug 2020 Week 3 < 7.5 / mg/L < / Oct 2020 Week 4 < 7.5 / mg/L < / Aug 2020 Average < 7.5 / mg/L < / Oct 2020 Average < 7.5 / mg/L < / 2020 Quarter 3 < 7.5 / mg/L < / 2020 Quarter 4 < 7.5 / mg/L < / 2020 2nd 6 Months (Avg) < 7.5 / mg/L < / 2020 2nd 6 ...(Max) < 7.5 / mg/L < / 2020 2nd 6 ...(Min) < 7.5 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 08/17/2020 S AstraZeneca081720Se1 < 0.0025 / 20.7 mg/L < / f 10/26/2020 P AstraZenecal02620PO < 0.0025 / 20.7 mg/L < / TW Aug 2020 Week 3 < 0.0025 / mg/L < / Oct 2020 Week 4 < 0.0025 / mg/L < / Aug 2020 Average < 0.0025 / 8.2 mg/L < / Oct 2020 Average < 0.0025 / 8.2 mg/L < / 2020 Quarter 3 < 0.0025 / mg/L < / Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 2 of 6 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate 2020 Quarter 4 < 0.0025 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0025 / mg/L < / 2020 2nd 6 ...(Max) < 0.0025 / mg/L < / 2020 2nd 6 ...(Min) < 0.0025 / mg/L < / 2020 2nd 6 ...(Count) 2 / / 1 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit Isopropyl acetate 08/17/2020 S AstraZeneca081720Se1 < 0.0025 / 20.7 mg/L < / f 10/26/2020 P AstraZeneca102620PO < 0.0025 / 20.7 mg/L < / TW Aug 2020 Week 3 < 0.0025 / mg/L < / Oct 2020 Week 4 < 0.0025 / mg/L < / Aug 2020 Average < 0.0025 / 8.2 mg/L < / Oct 2020 Average < 0.0025 / 8.2 mg/L < / 2020 Quarter 3 < 0.0025 / mg/L < / 2020 Quarter 4 < 0.0025 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0025 / mg/L < / 2020 2nd 6 ...(Max) < 0.0025 / mg/L < / 2020 2nd 6 ...(Min) < 0.0025 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 10/26/2020 P AstraZeneca102620PO < 0.000001 / 0.000142 mg/L < / TWHg Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 3 of 6 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL Oct 2020 Week 4 < 0.000001 / mg/L < / Oct 2020 Average < 0.000001 / mg/L < / 2020 Quarter 4 < 0.000001 / mg/L < / 2020 2nd 6 Months (Avg) < 0.000001 / mg/L < / 2020 2nd 6 ...(Max) < 0.000001 / mg/L < / 2020 2nd 6 ...(Min) < 0.000001 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Count : I 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Methylene Chloride 08/17/2020 S AstraZeneca081720Se1 < 0.003 / 3 mg/L < / f 10/26/2020 P AstraZeneca102620PO < 0.003 / 3 mg/L < / TW Aug 2020 Week 3 < 0.003 / mg/L < / Oct 2020 Week 4 < 0.003 / mg/L < / Aug 2020 Average < 0.003 / 0.7 mg/L < / Oct 2020 Average < 0.003 / 0.7 mg/L < / 2020 Quarter 3 < 0.003 / mg/L < / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 4 of 6 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit n-Amyl acetate 08/17/2020 S AstraZeneca081720Se1 < 0.003 / 20.7 mg/L < / f 10/26/2020 P AstraZeneca102620PO < 0.003 / 20.7 mg/L < / TW Aug 2020 Week 3 < 0.003 / mg/L < / Oct 2020 Week 4 < 0.003 / mg/L < / Aug 2020 Average < 0.003 / 8.2 mg/L < / Oct 2020 Average < 0.003 / 8.2 mg/L < / 2020 Quarter 3 < 0.003 / mg/L < / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 08/17/2020 S AstraZeneca081720Se1 7.7 / 6 - 10 SU / f 10/26/2020 P AstraZeneca102620PO 7.3 / 6 - 10 SU / TW Aug 2020 Week 3 7.7 / SU / Oct 2020 Week 4 7.3 / SU / Aug 2020 Average 7.7 / SU / Oct 2020 Average 7.3 / SU / 2020 Quarter 3 7.7 / SU / 2020 Quarter 4 7.3 / SU / 2020 2nd 6 Months (Avg) 7.5 / SU / 2020 2nd 6 ...(Max) 7.7 / SU / 2020 2nd 6 ...(Min) 7.3 / SU / 2020 2nd 6 ...(Count) 2 / / Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 5 of 6 AstraZeneca Pharmaceuticals LP SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:45:20PM * Indicates Violation ** Indicates TRC Violation Page 6 of 6 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 08/27/2020 S Aurobindo082720Se1f 0.341 / 5.59 mg/L Aug 2020 Week 4 0.341 / mg/L Aug 2020 Average 0.341 / 2.21 mg/L 2020 Quarter 3 0.341 / mg/L 2020 2nd 6 Months (Avg) 0.341 / mg/L 2020 2nd 6 ...(Max) 0.341 / mg/L 2020 2nd 6 ...(Min) 0.341 / mg/L 2020 2nd 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ammonia 08/27/2020 S Aurobindo082720Se1f 40.5 / mg/L / 09/24/2020 P Aurobindo092420POT 4.3 / mg/L / W Aug 2020 Week 4 40.5 / mg/L / Sep 2020 Week 4 4.3 / mg/L / Aug 2020 Average 40.5 / mg/L / Sep 2020 Average 4.3 / mg/L / 2020 Quarter 3 22.4 / mg/L / 2020 2nd 6 Months (Avg) 22.4 / mg/L / 2020 2nd 6 ...(Max) 40.5 / mg/L / 2020 2nd 6 ...(Min) 4.3 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/16/2020 S Aurobindo0720F1ow 0.001883 / MGD 08/21/2020 S Aurobindo0820F1ow 0.002085 / MGD 09/17/2020 S Aurobindo0920F1ow 0.003512 / MGD 10/22/2020 S Aurobindo1020F1ow 0.004124 / MGD 11/18/2020 S Aurobindo1120Flow 0.006343 / MGD 12/16/2020 S Aurobindo1220F1ow 0.00249 / MGD Ju12020 Week 3 0.001883 / MGD Aug 2020 Week 3 0.002085 / MGD Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 1 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Sep 2020 Week 3 0.003512 / MGD Oct 2020 Week 4 0.004124 / MGD Nov 2020 Week 3 0.006343 / MGD Dec 2020 Week 3 0.00249 / MGD Jul 2020 Average 0.001883 / 0.039 MGD Aug 2020 Average 0.002085 / 0.039 MGD Sep 2020 Average 0.003512 / 0.039 MGD Oct 2020 Average 0.004124 / 0.039 MGD Nov 2020 Average 0.006343 / 0.039 MGD Dec 2020 Average 0.00249 / 0.039 MGD 2020 Quarter 3 0.002493 / MGD 2020 Quarter 4 0.004319 / MGD 2020 2nd 6 Months (Avg) 0.003406 / MGD 2020 2nd 6 ...(Max) 0.006343 / MGD 2020 2nd 6 ...(Min) 0.001883 / MGD 2020 2nd 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit BOD 08/27/2020 S Aurobindo082720Se1f 09/24/2020 P Aurobindo092420POT W Aug 2020 Week 4 Sep 2020 Week 4 Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 86 / mg/L 50.2 / mg/L 86 / mg/L 50.2 / mg/L 86 / mg/L 50.2 / mg/L 68.1 / mg/L 68.1 / mg/L 86 / mg/L 50.2 / mg/L 2 / Sample Date SamplelD Result/Limit Mass/Limit Cadmium Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 2 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Cadmium 08/27/2020 S Aurobindo082720Se1f < 0.00008 / mg/L < / 09/24/2020 P Aurobindo092420POT < 0.00008 / mg/L < / W Aug 2020 Week 4 < 0.00008 / mg/L < / Sep 2020 Week 4 < 0.00008 / mg/L < / Aug 2020 Average < 0.00008 / mg/L < / Sep 2020 Average < 0.00008 / mg/L < / 2020 Quarter 3 < 0.00008 / mg/L < / 2020 2nd 6 Months (Avg) < 0.00008 / mg/L < / 2020 2nd 6 ...(Max) < 0.00008 / mg/L < / 2020 2nd 6 ...(Min) < 0.00008 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Chloride 08/27/2020 S Aurobindo082720Se1f 09/24/2020 P Aurobindo092420POT W Aug 2020 Week 4 Sep 2020 Week 4 Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 50.5 / mg/L 21.5 / mg/L 50.5 / mg/L 21.5 / mg/L 50.5 / mg/L 21.5 / mg/L 36 / mg/L 36 / mg/L 50.5 / mg/L 21.5 / mg/L 2 / Sample Date SamplelD Result/Limit Mass/Limit COD 08/27/2020 S Aurobindo082720Se1f 279 / mg/L / 09/24/2020 P Aurobindo092420POT 89 / mg/L / W Aug 2020 Week 4 279 / mg/L / Sep 2020 Week 4 89 / mg/L / Aug 2020 Average 279 / mg/L / Sep 2020 Average 89 / mg/L / 2020 Quarter 3 184 / mg/L / 2020 2nd 6 Months (Avg) 184 / mg/L / 2020 2nd 6 ...(Max) 279 / mg/L / 2020 2nd 6 ...(Min) 89 / mg/L / 2020 2nd 6 ...(Count) 2 / / Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 3 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Copper 08/27/2020 S Aurobindo082720Se1f 0.034 / mg/L 09/24/2020 P Aurobindo092420POT 0.027 / mg/L W Aug 2020 Week 4 0.034 / mg/L Sep 2020 Week 4 0.027 / mg/L Aug 2020 Average 0.034 / mg/L Sep 2020 Average 0.027 / mg/L 2020 Quarter 3 0.031 / mg/L 2020 2nd 6 Months (Avg) 0.031 / mg/L 2020 2nd 6 ...(Max) 0.034 / mg/L 2020 2nd 6 ...(Min) 0.027 / mg/L 2020 2nd 6 ...(Count) 2 / Sample Date SamplelD Result/Limit Mass/Limit Cyanide 08/27/2020 S Aurobindo082720Se1f < 0.003 / mg/L < / 09/24/2020 P Aurobindo092420POT < 0.003 / mg/L < / W Aug 2020 Week 4 < 0.003 / mg/L < / Sep 2020 Week 4 < 0.003 / mg/L < / Aug 2020 Average < 0.003 / mg/L < / Sep 2020 Average < 0.003 / mg/L < / 2020 Quarter 3 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Ethyl acetate 08/27/2020 S Aurobindo082720Se1f < 0.005 / 5.59 mg/L < / Aug 2020 Week 4 < 0.005 / mg/L < / Aug 2020 Average < 0.005 / 2.21 mg/L < / 2020 Quarter 3 < 0.005 / mg/L < / 2020 2nd 6 Months (Avg) < 0.005 / mg/L < / 2020 2nd 6 ...(Max) < 0.005 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 4 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 # % # % # iyo # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 # Sample Date SamplelD Result/Limit Mass /Limit Fluoride 08/27/2020 S Aurobindo082720Se1f < 0.05 / mg/L < / 09/24/2020 P Aurobindo092420POT < 0.05 / mg/L < / W Aug 2020 Week 4 < 0.05 / mg/L < / Sep 2020 Week 4 < 0.05 / mg/L < / Aug 2020 Average < 0.05 / mg/L < / Sep 2020 Average < 0.05 / mg/L < / 2020 Quarter 3 < 0.05 / mg/L < / 2020 2nd 6 Months (Avg) < 0.05 / mg/L < / 2020 2nd 6 ...(Max) < 0.05 / mg/L < / 2020 2nd 6 ...(Min) < 0.05 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Isopropyl acetate 08/27/2020 S Aurobindo082720Se1f < 0.005 / 5.59 mg/L < / Aug 2020 Week 4 < 0.005 / mg/L < / Aug 2020 Average < 0.005 / 2.21 mg/L < / 2020 Quarter 3 < 0.005 / mg/L < / 2020 2nd 6 Months (Avg) < 0.005 / mg/L < / 2020 2nd 6 ...(Max) < 0.005 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 5 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 08/27/2020 S Aurobindo082720Se1f 0.000087 / 0.000142 mg/L 10/05/2020 P Aurobindo100520POT 0.000036 / 0.000142 mg/L WHg Aug 2020 Week 4 0.000087 / mg/L Oct 2020 Week 1 0.000036 / mg/L Aug 2020 Average 0.000087 / mg/L Oct 2020 Average 0.000036 / mg/L 2020 Quarter 3 0.000087 / mg/L 2020 Quarter 4 0.000036 / mg/L 2020 2nd 6 Months (Avg) 0.000062 / mg/L 2020 2nd 6 ...(Max) 0.000087 / mg/L 2020 2nd 6 ...(Min) 0.000036 / mg/L 2020 2nd 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Methylene Chloride 08/27/2020 S Aurobindo082720Se1f < 0.005 / 0.81 mg/L < / Aug 2020 Week 4 < 0.005 / mg/L < / Aug 2020 Average < 0.005 / 0.18 mg/L < / 2020 Quarter 3 < 0.005 / mg/L < / 2020 2nd 6 Months (Avg) < 0.005 / mg/L < / 2020 2nd 6 ...(Max) < 0.005 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 6 of 11 Aurobindo USA # Over Daily C # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 08/27/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S Aurobindo082720Se1f P Aurobindo092420POT W Week 4 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 0.001 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result/Limit Mass /Limit n-Amyl acetate 08/27/2020 Aug 2020 Aug 2020 2020 2020 2020 2020 2020 S Aurobindo082720Se1f Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 1 0.00 0.00 0.00 0.00 0.00 0.00 0.005 / 5.59 0.005 / 0.005 / 2.21 0.005 / 0.005 / 0.005 / 0.005 / 1 / Months Sampled : # Over MoAvg C: # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 Weeks Sampled : 1 # % # 0 0.00 # Over Wk Avg C : 0 0.00 0 0.00 # Over Wk Avg C TRC : 0 0.00 0 0.00 # Over Wk Avg M : 0 0.00 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 08/27/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 S Aurobindo082720Se1f P Aurobindo092420POT W Week 4 Week 4 Average Average Quarter 3 0.3 / 0.2 / 0.3 / 0.2 / 0.3 / 0.2 / 0.3 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 7 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 2020 2020 2020 2020 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.3 / 0.3 / 0.2 / 2 / mg/L mg/L mg/L Sample Date SamplelD Result / Limit Mass / Limit Nitrogen, Total 08/27/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S Aurobindo082720Se1f P Aurobindo092420POT W Week 4 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 78 / 15.3 / 78 / 15.3 / 78 / 15.3 / 46.65 / 46.65 / 78 / 15.3 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 08/27/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: S Aurobindo082720Se1f < P Aurobindo092420POT W Week 4 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 2.5 / 200 6 / 200 2.5 6 2.5 6 4.25 4.25 6 2.5 2 Months Sampled : 0 0 0 0 1 2 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 8 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 08/27/2020 S Aurobindo082720Se1f 8.4 / 6.0 - 10.0 SU 09/24/2020 P Aurobindo092420POT 8.2 / 6.0 - 10.0 SU W Aug 2020 Week 4 8.4 / SU Sep 2020 Week 4 8.2 / SU Aug 2020 Average 8.4 / SU Sep 2020 Average 8.2 / SU 2020 Quarter 3 8.3 / SU 2020 2nd 6 Months (Avg) 8.3 / SU 2020 2nd 6 ...(Max) 8.4 / SU 2020 2nd 6 ...(Min) 8.2 / SU 2020 2nd 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Temperature 08/27/2020 S Aurobindo082720Se1f 09/24/2020 P Aurobindo092420POT W Aug 2020 Week 4 Sep 2020 Week 4 Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 29 / 66 °C / 26 / 66 °C / 29 / °C / 26 / °C / 29 / °C / 26 / °C / 27.5 / °C / 27.5 / °C / 29 / °C / 26 / °C / 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 9 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN 08/27/2020 09/24/2020 S Aurobindo082720Se1f P Aurobindo092420POT W Aug 2020 Week 4 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 77.7 / 15.1 / 77.7 / 15.1 / 77.7 / 15.1 / 46.4 / 46.4 / 77.7 / 15.1 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result/Limit Mass /Limit Total Phosphorus 08/27/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S Aurobindo082720Se1f P Aurobindo092420POT W Week 4 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 8.42 / 3.88 / 8.42 / 3.88 / 8.42 / 3.88 / 6.15 / 6.15 / 8.42 / 3.88 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result/Limit Mass /Limit TSS 08/27/2020 S Aurobindo082720Se1f 09/24/2020 P Aurobindo092420POT W Aug 2020 Week 4 Sep 2020 Week 4 Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 122 / 47 / 122 / 47 / 122 / 47 / 84.5 / 84.5 / 122 / 47 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 10 of 11 Aurobindo USA SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc 08/27/2020 S Aurobindo082720Se1f 0.159 / mg/L 09/24/2020 P Aurobindo092420POT 0.32 / mg/L W Aug 2020 Week 4 0.159 / mg/L Sep 2020 Week 4 0.32 / mg/L Aug 2020 Average 0.159 / mg/L Sep 2020 Average 0.32 / mg/L 2020 Quarter 3 0.24 / mg/L 2020 2nd 6 Months (Avg) 0.240 / mg/L 2020 2nd 6 ...(Max) 0.32 / mg/L 2020 2nd 6 ...(Min) 0.159 / mg/L 2020 2nd 6 ...(Count) 2 / Wednesday, February 24, 2021 10:43:59PM * Indicates Violation ** Indicates TRC Violation Page 11 of 11 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 09/29/2020 P Biogen092920POTW 0.0918 / 12.19 mg/L Sep 2020 Week 4 0.0918 / mg/L Sep 2020 Average 0.0918 / 4.83 mg/L 2020 Quarter 3 0.0918 / mg/L 2020 2nd 6 Months (Avg) 0.0918 / mg/L 2020 2nd 6 ...(Max) 0.0918 / mg/L 2020 2nd 6 ...(Min) 0.0918 / mg/L 2020 2nd 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 0.068 / lbs/day 0.068 / lbs/day 0.068 / lbs/day 0.068 / lbs/day 0.0680 / lbs/day 0.0680 / lbs/day 0.0680 / lbs/day 1 / 1 Quarters Sampled : 1 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : # 0 0.00 0 0.00 0 0.00 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ammonia 08/20/2020 S Biogen082020Se1f 1.3 / mg/L 3.0634 / lbs/day 09/29/2020 P Biogen092920POTW 1.9 / mg/L 1.4071 / lbs/day Aug 2020 Week 3 1.3 / mg/L 3.0634 / lbs/day Sep 2020 Week 4 1.9 / mg/L 1.4071 / lbs/day Aug 2020 Average 1.3 / mg/L 3.0634 / lbs/day Sep 2020 Average 1.9 / mg/L 1.4071 / lbs/day 2020 Quarter 3 1.3 / mg/L 3.0634 / lbs/day 2020 Quarter 3 1.9 / mg/L 1.4071 / lbs/day 2020 Quarter 3 1.3 / mg/L 3.0634 / lbs/day 2020 Quarter 3 1.9 / mg/L 1.4071 / lbs/day 2020 2nd 6 Months (Avg) 1.6 / mg/L 2.2353 / lbs/day 2020 2nd 6 ...(Max) 1.9 / mg/L 3.0634 / lbs/day 2020 2nd 6 ...(Min) 1.3 / mg/L 1.4071 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Average Flow for Month 07/31/2020 S Biogen0720F1ow 0.09304 / 0.375 MGD 08/31/2020 S Biogen0820F1ow 0.087956 / 0.375 MGD 09/30/2020 S Biogen0920F1ow 0.077921 / 0.375 MGD 10/31/2020 S Biogen1020Flow 0.071654 / 0.375 MGD 11/30/2020 S Biogen1120Flow 0.067742 / 0.375 MGD Jul 2020 Week 4 0.09304 / MGD Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 1 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Aug 2020 Week 4 0.087956 / MGD Sep 2020 Week 4 0.077921 / MGD Oct 2020 Week 4 0.071654 / MGD Nov 2020 Week 4 0.067742 / MGD Jul 2020 Average 0.09304 / 0.250 MGD Aug 2020 Average 0.087956 / 0.250 MGD Sep 2020 Average 0.077921 / 0.250 MGD Oct 2020 Average 0.071654 / 0.250 MGD Nov 2020 Average 0.067742 / 0.250 MGD 2020 Quarter 3 0.09304 / MGD 2020 Quarter 3 0.082939 / MGD 2020 Quarter 3 0.09304 / MGD 2020 Quarter 3 0.082939 / MGD 2020 Quarter 4 0.069698 / MGD 2020 2nd 6 Months (Avg) 0.079663 / MGD 2020 2nd 6 ...(Max) 0.09304 / MGD 2020 2nd 6 ...(Min) 0.067742 / MGD 2020 2nd 6 ...(Count) 5 / Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 5 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit BOD 08/20/2020 S Biogen082020Self 25.7 / mg/L 60.561 / lbs/day 09/29/2020 P Biogen092920POTW 76.5 / mg/L 56.655 / lbs/day Aug 2020 Week 3 25.7 / mg/L 60.561 / lbs/day Sep 2020 Week 4 76.5 / mg/L 56.655 / lbs/day Aug 2020 Average 25.7 / mg/L 60.561 / lbs/day Sep 2020 Average 76.5 / mg/L 56.655 / lbs/day 2020 Quarter 3 25.7 / mg/L 60.561 / lbs/day 2020 Quarter 3 76.5 / mg/L 56.655 / lbs/day 2020 Quarter 3 25.7 / mg/L 60.561 / lbs/day 2020 Quarter 3 76.5 / mg/L 56.655 / lbs/day 2020 2nd 6 Months (Avg) 51.1 / mg/L 58.608 / lbs/day 2020 2nd 6 ...(Max) 76.5 / mg/L 60.561 / lbs/day 2020 2nd 6 ...(Min) 25.7 / mg/L 56.655 / lbs/day Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 2 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit BOD 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result /Limit Mass /Limit Cadmium 09/29/2020 P Biogen092920POTW < 0.00008 / mg/L < 0.000056 / lbs/day Sep 2020 Week 4 < 0.00008 / mg/L < 0.000056 / lbs/day Sep 2020 Average < 0.00008 / mg/L < 0.000056 / lbs/day 2020 Quarter 3 < 0.00008 / mg/L < 0.000056 / lbs/day 2020 2nd 6 Months (Avg) < 0.00008 / mg/L < 0.000056 / lbs/day 2020 2nd 6 ...(Max) < 0.00008 / mg/L < 0.000056 / lbs/day 2020 2nd 6 ...(Min) < 0.00008 / mg/L < 0.000056 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Chloride 08/20/2020 S Biogen082020Se1f 35.5 / mg/L 83.6546 / lbs/day 09/29/2020 P Biogen092920POTW 37 / mg/L 27.4019 / lbs/day Aug 2020 Week 3 35.5 / mg/L 83.6546 / lbs/day Sep 2020 Week 4 37 / mg/L 27.4019 / lbs/day Aug 2020 Average 35.5 / mg/L 83.6546 / lbs/day Sep 2020 Average 37 / mg/L 27.4019 / lbs/day 2020 Quarter 3 35.5 / mg/L 83.6546 / lbs/day 2020 Quarter 3 37 / mg/L 27.4019 / lbs/day 2020 Quarter 3 35.5 / mg/L 83.6546 / lbs/day 2020 Quarter 3 37 / mg/L 27.4019 / lbs/day 2020 2nd 6 Months (Avg) 36.25 / mg/L 55.5282 / lbs/day 2020 2nd 6 ...(Max) 37 / mg/L 83.6546 / lbs/day 2020 2nd 6 ...(Min) 35.5 / mg/L 27.4019 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit COD 08/20/2020 S Biogen082020Se1f 42.8 / mg/L 100.86 / lbs/day 09/29/2020 P Biogen092920POTW 108 / mg/L 79.98 / lbs/day Aug 2020 Week 3 42.8 / mg/L 100.86 / lbs/day Sep 2020 Week 4 108 / mg/L 79.98 / lbs/day Aug 2020 Average 42.8 / mg/L 100.86 / lbs/day Sep 2020 Average 108 / mg/L 79.98 / lbs/day 2020 Quarter 3 42.8 / mg/L 100.86 / lbs/day 2020 Quarter 3 108 / mg/L 79.98 / lbs/day 2020 Quarter 3 42.8 / mg/L 100.86 / lbs/day Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 3 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit COD 2020 Quarter 3 108 / mg/L 2020 2nd 6 Months (Avg) 75.4 / mg/L 2020 2nd 6 ...(Max) 108 / mg/L 2020 2nd 6 ...(Min) 42.8 / mg/L 2020 2nd 6 ...(Count) 2 / 79.98 / lbs/day 90.42 / lbs/day 100.86 / lbs/day 79.98 / lbs/day 2 / Sample Date SamplelD Result/Limit Mass/Limit Cyanide 08/20/2020 S Biogen082020Se1f < 0.004 / mg/L < 0.009426 / lbs/day Aug 2020 Week 3 < 0.004 / mg/L < 0.009426 / lbs/day Aug 2020 Average < 0.004 / mg/L < 0.009426 / lbs/day 2020 Quarter 3 < 0.004 / mg/L < 0.009426 / lbs/day 2020 2nd 6 Months (Avg) < 0.004 / mg/L < 0.009426 / lbs/day 2020 2nd 6 ...(Max) < 0.004 / mg/L < 0.009426 / lbs/day 2020 2nd 6 ...(Min) < 0.004 / mg/L < 0.009426 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Fluoride 08/20/2020 S Biogen082020Se1f < 0.05 / mg/L < 0.1178 / lbs/day 09/29/2020 P Biogen092920POTW < 0.05 / mg/L < 0.037 / lbs/day Aug 2020 Week 3 < 0.05 / mg/L < 0.1178 / lbs/day Sep 2020 Week 4 < 0.05 / mg/L < 0.037 / lbs/day Aug 2020 Average < 0.05 / mg/L < 0.1178 / lbs/day Sep 2020 Average < 0.05 / mg/L < 0.037 / lbs/day 2020 Quarter 3 < 0.05 / mg/L < 0.1178 / lbs/day 2020 Quarter 3 < 0.05 / mg/L < 0.037 / lbs/day 2020 Quarter 3 < 0.05 / mg/L < 0.1178 / lbs/day 2020 Quarter 3 < 0.05 / mg/L < 0.037 / lbs/day 2020 2nd 6 Months (Avg) < 0.05 / mg/L < 0.0774 / lbs/day 2020 2nd 6 ...(Max) < 0.05 / mg/L < 0.1178 / lbs/day 2020 2nd 6 ...(Min) < 0.05 / mg/L < 0.0370 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 08/20/2020 S Biogen082020Se1f 0.000002 / 0.000142 mg/L 11/10/2020 P Biogen111020POTWH 0.000011 / 0.000142 mg/L g Aug 2020 Week 3 0.000002 / mg/L Nov 2020 Week 2 0.000011 / mg/L Aug 2020 Average 0.000002 / mg/L Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 4 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL Nov 2020 2020 2020 2020 2020 2020 2020 Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : I 2 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: 0 0 0 0 0 0 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.000011 0.000002 0.000011 0.000007 0.000011 0.000002 2 / Months Sampled : 2 0 0 0 0 mg/L mg/L mg/L mg/L mg/L mg/L 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 2 Quarters Sampled : 2 #0/0 0.00 # Over Qt Avg C : 0 0.00 0.00 # Over Qt Avg C TRC : 0 0.00 0.00 # Over Qtr Avg M : 0 0.00 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Methylene Chloride 09/29/2020 Sep 2020 Sep 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: P Biogen092920POTW Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 1 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.25 / 1.77 0.25 / 0.25 / 0.41 0.25 / 0.25 / 0.25 / 0.25 / 1 / Months Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 mg/L mg/L mg/L mg/L mg/L mg/L mg/L # Over Wk Avg C : # Over Wk Avg C TRC : # Over Wk Avg M : # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 0.185148 / 0.185148 / 0.185148 / 0.185148 / 0.185148 / 0.185148 / 0.185148 / 1 / 1 0.00 0.00 0.00 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 08/20/2020 09/29/2020 Aug 2020 Sep 2020 S Biogen082020Se1f P Biogen092920POTW Week 3 Week 4 mg/L mg/L mg/L mg/L 1.037 / 0.733 / 1.037 / 0.733 / lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 5 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.4 / 1 / 0.7 / 0.7 / 1.0 / 0.4 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L 1.037 / 0.733 / 0.885 / 0.885 / 1.037 / 0.733 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 08/20/2020 09/29/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 2020 2020 2020 S Biogen082020Se1f P Biogen092920POTW Week 3 Week 4 Average Average Quarter 3 Quarter 3 Quarter 3 Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 4.3 6.72 4.3 6.72 4.3 6.72 4.3 6.72 4.3 6.72 5.51 6.72 4.3 2 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 10.133 4.977 10.133 4.977 10.133 4.977 10.133 4.977 10.133 4.977 7.555 10.133 4.977 2 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 08/20/2020 09/29/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 2020 2020 2020 S Biogen082020Se1f P Biogen092920POTW < Week 3 Week 4 Average Average Quarter 3 Quarter 3 Quarter 3 Quarter 3 2nd 6 Months (Avg) < 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2 / 200 / 200 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 6 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 4 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit pH 08/20/2020 S Biogen082020Se1f 5.98 / 5.5 - 10.5 SU / 09/29/2020 P Biogen092920POTW 7.3 / 5.5 - 10.5 SU / Aug 2020 Week 3 5.98 / SU / Sep 2020 Week 4 7.3 / SU / Aug 2020 Average 5.98 / SU / Sep 2020 Average 7.3 / SU / 2020 Quarter 3 5.98 / SU / 2020 Quarter 3 7.3 / SU / 2020 Quarter 3 5.98 / SU / 2020 Quarter 3 7.3 / SU / 2020 2nd 6 Months (Avg) 6.64 / SU / 2020 2nd 6 ...(Max) 7.3 / SU / 2020 2nd 6 ...(Min) 5.98 / SU / 2020 2nd 6 ...(Count) 2 / / Sample Count : I 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 4 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Temperature 09/29/2020 P Biogen092920POTW Sep 2020 Week 4 Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 26 / 66 °C / 26 / °C / 26 / °C / 26 / °C / 26 / °C / 26 / °C / 26 / °C / 1 / / Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 7 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 1 # Over Daily C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Daily M : 0 0.00 # Over Daily M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 # Over MoAvg C: # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : Months Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 # Over WkAvg C: # Over Wk Avg C TRC : # Over WkAvg M: # Over Wk Avg M TRC : Weeks Sampled : # 0 0 0 0 1 Quarters Sampled : 1 0.00 # Over Qt Avg C : 0 0.00 0.00 # Over Qt Avg C TRC : 0 0.00 0.00 # Over Qtr Avg M : 0 0.00 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit TKN 08/20/2020 09/29/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S Biogen082020Se1f P Biogen092920POTW Week 3 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 3.8 / 5.73 / 3.8 / 5.73 / 3.8 / 5.73 / 4.77 / 4.77 / 5.73 / 3.8 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 8.955 / 4.244 / 8.955 / 4.244 / 8.955 / 4.244 / 6.599 / 6.599 / 8.955 / 4.244 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit Total Phosphorus 08/20/2020 S 09/29/2020 P Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 2020 2020 2020 Biogen082020Se1f Biogen092920POTW Week 3 Week 4 Average Average Quarter 3 Quarter 3 Quarter 3 Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 1.42 / 1.1 / 1.42 / 1.1 / 1.42 / 1.1 / 1.42 / 1.1 / 1.42 / 1.26 / 1.42 / 1.1 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 2.5921 / 1.0516 / 2.5921 / 1.0516 / 2.5921 / 1.0516 / 2.5921 / 1.0516 / 2.5921 / 1.0516 / 1.8219 / 2.5921 / 1.0516 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit TSS 08/20/2020 09/29/2020 Aug 2020 S Biogen082020Se1f P Biogen092920POTW Week 3 9.3 / 143 / 9.3 / mg/L mg/L mg/L 21.915143 / 105.904656 / 21.915143 / lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 8 of 9 Biogen SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TSS Sep 2020 Week 4 143 / mg/L Aug 2020 Average 9.3 / mg/L Sep 2020 Average 143 / mg/L 2020 Quarter 3 9.3 / mg/L 2020 Quarter 3 143 / mg/L 2020 Quarter 3 9.3 / mg/L 2020 Quarter 3 143 / mg/L 2020 2nd 6 Months (Avg) 76.2 / mg/L 2020 2nd 6 ...(Max) 143 / mg/L 2020 2nd 6 ...(Min) 9.3 / mg/L 2020 2nd 6 ...(Count) 2 / 105.904656 / lbs/day 21.915143 / lbs/day 105.904656 / lbs/day 21.915143 / lbs/day 105.904656 / lbs/day 21.915143 / lbs/day 105.904656 / lbs/day 63.9099 / lbs/day 105.904656 / lbs/day 21.915143 / lbs/day 2 / Sample Date SamplelD Result / Limit Mass / Limit Zinc 08/20/2020 S Biogen082020Se1f 0.204 / mg/L 0.480719 / lbs/day 09/29/2020 P Biogen092920POTW 0.388 / mg/L 0.28735 / lbs/day Aug 2020 Week 3 0.204 / mg/L 0.480719 / lbs/day Sep 2020 Week 4 0.388 / mg/L 0.28735 / lbs/day Aug 2020 Average 0.204 / mg/L 0.480719 / lbs/day Sep 2020 Average 0.388 / mg/L 0.28735 / lbs/day 2020 Quarter 3 0.204 / mg/L 0.480719 / lbs/day 2020 Quarter 3 0.388 / mg/L 0.28735 / lbs/day 2020 Quarter 3 0.204 / mg/L 0.480719 / lbs/day 2020 Quarter 3 0.388 / mg/L 0.28735 / lbs/day 2020 2nd 6 Months (Avg) 0.296 / mg/L 0.384034 / lbs/day 2020 2nd 6 ...(Max) 0.388 / mg/L 0.480719 / lbs/day 2020 2nd 6 ...(Min) 0.204 / mg/L 0.287350 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Wednesday, February 24, 2021 10:42:35PM * Indicates Violation ** Indicates TRC Violation Page 9 of 9 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 07/10/2020 S Cintas071020Se1f 0.56 / mg/L Ju12020 Week 2 0.56 / mg/L Jul 2020 Average 0.56 / mg/L 2020 Quarter 3 0.56 / mg/L 2020 2nd 6 Months (Avg) 0.56 / mg/L 2020 2nd 6 ...(Max) 0.56 / mg/L 2020 2nd 6 ...(Min) 0.56 / mg/L 2020 2nd 6 ...(Count) 1 / 0.092474 / lbs/day 0.092474 / lbs/day 0.092474 / lbs/day 0.092474 / lbs/day 0.092474 / lbs/day 0.092474 / lbs/day 0.092474 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass /Limit Ammonia 07/10/2020 S Cintas071020Se1f 0.16 / mg/L 0.0264 / lbs/day 08/04/2020 S Cintas080420Se1f 1.3 / mg/L 0.57 / lbs/day 08/11/2020 P Cintas081120POTW 18.7 / mg/L / 09/18/2020 S Cintas091820Se1f 4.4 / mg/L 2.5404 / lbs/day 10/06/2020 S Cintas100620Se1f 9.5 / mg/L 4.924 / lbs/day 11/06/2020 S Cintas110620Self 16.3 / mg/L 8.442 / lbs/day 12/11/2020 S Cintas121120Self 1.7 / mg/L 1.0236 / lbs/day Jul 2020 Week 2 0.16 / mg/L 0.0264 / lbs/day Aug 2020 Week 1 1.3 / mg/L 0.57 / lbs/day Aug 2020 Week 2 18.7 / mg/L / Sep 2020 Week 3 4.4 / mg/L 2.5404 / lbs/day Oct 2020 Week 1 9.5 / mg/L 4.924 / lbs/day Nov 2020 Week 1 16.3 / mg/L 8.442 / lbs/day Dec 2020 Week 2 1.7 / mg/L 1.0236 / lbs/day Jul 2020 Average 0.16 / mg/L 0.0264 / lbs/day Aug 2020 Average 10 / mg/L 0.57 / lbs/day Sep 2020 Average 4.4 / mg/L 2.5404 / lbs/day Oct 2020 Average 9.5 / mg/L 4.924 / lbs/day Nov 2020 Average 16.3 / mg/L 8.442 / lbs/day Dec 2020 Average 1.7 / mg/L 1.0236 / lbs/day 2020 Quarter 3 6.14 / mg/L 1.0456 / lbs/day 2020 Quarter 4 9.17 / mg/L 4.7965 / lbs/day 2020 2nd 6 Months (Avg) 7.44 / mg/L 2.9211 / lbs/day 2020 2nd 6 ...(Max) 18.7 / mg/L 8.4420 / lbs/day 2020 2nd 6 ...(Min) 0.16 / mg/L / 2020 2nd 6 ...(Count) 7 / 6 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/31/2020 S Cintas0720F1ow 0.057278 / 0.180 MGD 08/31/2020 S Cintas0820F1ow 0.060637 / 0.180 MGD Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 1 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 09/30/2020 S Cintas0920F1ow 0.065836 / 0.180 MGD 10/31/2020 S Clntas1020Flow 0.061402 / 0.180 MGD 11/30/2020 S Cintas1120F1ow 0.051741 / 0.180 MGD 12/31/2020 S Cintas1220F1ow 0.052085 / 0.180 MGD Jul 2020 Week 4 0.057278 / MGD Aug 2020 Week 4 0.060637 / MGD Sep 2020 Week 4 0.065836 / MGD Oct 2020 Week 4 0.061402 / MGD Nov 2020 Week 4 0.051741 / MGD Dec 2020 Week 4 0.052085 / MGD Ju12020 Average 0.057278 / 0.120 MGD Aug 2020 Average 0.060637 / 0.120 MGD Sep 2020 Average 0.065836 / 0.120 MGD Oct 2020 Average 0.061402 / 0.120 MGD Nov 2020 Average 0.051741 / 0.120 MGD Dec 2020 Average 0.052085 / 0.120 MGD 2020 Quarter 3 0.06125 / MGD 2020 Quarter 4 0.055076 / MGD 2020 2nd 6 Months (Avg) 0.058163 / MGD 2020 2nd 6 ...(Max) 0.065836 / MGD 2020 2nd 6 ...(Min) 0.051741 / MGD 2020 2nd 6 ...(Count) 6 / Sample Count : L Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit BOD 07/10/2020 S Cintas071020Se1f 07/21/2020 P Cintas072120POTW 08/04/2020 S Cintas080420Se1f 08/11/2020 P Cintas081120POTW 09/18/2020 S Cintas091820Se1f 09/24/2020 P Cintas092420POTW 10/06/2020 S Cintas100620Se1f 10/20/2020 P Cintas102020POTW 11/06/2020 S Cintas110620Self 227 / mg/L 654 / mg/L 218 / mg/L 320 / mg/L 279 / mg/L 343 / mg/L 113 / mg/L 230 / mg/L 405 / mg/L 37.485 / 95.582 / 161.084 / 58.57 / 209.755 / lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 2 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit BOD 11/24/2020 P Cintas112420POTW 12/11/2020 P Cintas121120POTW 12/11/2020 S Cintas121120Self Ju12020 Week 2 Jul 2020 Week 3 Aug 2020 Week 1 Aug 2020 Week 2 Sep 2020 Week 3 Sep 2020 Week 4 Oct 2020 Week 1 Nov 2020 Week 1 Oct 2020 Week 3 Nov 2020 Week 4 Dec 2020 Week 2 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average Nov 2020 Average Dec 2020 Average 2020 Quarter3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 361 / mg/L 497 / mg/L 79.6 / mg/L 47.928 / lbs/day 227 / mg/L 37.485 / lbs/day 654 / mg/L / 218 / mg/L 95.582 / lbs/day 320 / mg/L / 279 / mg/L 161.084 / lbs/day 343 / mg/L / 113 / mg/L 58.57 / lbs/day 405 / mg/L 209.755 / lbs/day 230 / mg/L / 361 / mg/L / 288.3 / mg/L 47.928 / lbs/day 440.5 / mg/L 37.485 / lbs/day 269 / mg/L 95.582 / lbs/day 311 / mg/L 161.084 / lbs/day 171.5 / mg/L 58.57 / lbs/day 383 / mg/L 209.755 / lbs/day 288.3 / mg/L 47.928 / lbs/day 340.2 / mg/L 98.05 / lbs/day 280.9 / mg/L 105.418 / lbs/day 310.6 / mg/L 101.734 / lbs/day 654 / mg/L 209.755 / lbs/day 79.6 / mg/L 12 / 6 / Sample .Date SamplelD Result / Limit Mass/Limit Cadmium 07/10/2020 S Cintas071020Se1f 0.001 / mg/L 0.000165 / lbs/day Jul 2020 Week 2 0.001 / mg/L 0.000165 / lbs/day Jul 2020 Average 0.001 / mg/L 0.000165 / lbs/day 2020 Quarter 3 0.001 / mg/L 0.000165 / lbs/day 2020 2nd 6 Months (Avg) 0.001 / mg/L 0.000165 / lbs/day 2020 2nd 6 ...(Max) 0.001 / mg/L 0.000165 / lbs/day 2020 2nd 6 ...(Min) 0.001 / mg/L 0.000165 / lbs/day 2020 2nd 6 ...(Count) I / 1 / Sample Date SamplelD Result/Limit Mass/Limit Chloride 08/11/2020 P Cintas081120POTW Aug 2020 Week 2 156 / 156 / mg/L mg/L Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 3 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chloride Aug 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 156 / mg/L 156 / mg/L 156 / mg/L 156 / mg/L 156 / mg/L 1 / Sample Date SamplelD Result/Limit Mass/Limit Chromium 07/10/2020 S Cintas071020Se1f < 0.003 / mg/L < 0.000413 / lbs/day 08/04/2020 S Cintas080420Se1f < 0.003 / mg/L < 0.001096 / lbs/day 09/18/2020 S Cintas091820Se1f 0.017 / mg/L 0.009815 / lbs/day 10/06/2020 S Cintas100620Se1f < 0.003 / mg/L < 0.001296 / lbs/day 11/06/2020 S Cintas110620Se1f 0.013 / mg/L 0.006733 / lbs/day 12/11/2020 S Cintas121120Self 0.006 / mg/L 0.003552 / lbs/day Jul 2020 Week 2 < 0.003 / mg/L < 0.000413 / lbs/day Aug 2020 Week 1 < 0.003 / mg/L < 0.001096 / lbs/day Sep 2020 Week 3 0.017 / mg/L 0.009815 / lbs/day Oct 2020 Week 1 < 0.003 / mg/L < 0.001296 / lbs/day Nov 2020 Week 1 0.013 / mg/L 0.006733 / lbs/day Dec 2020 Week 2 0.006 / mg/L 0.003552 / lbs/day Jul 2020 Average < 0.003 / mg/L < 0.000413 / lbs/day Aug 2020 Average < 0.003 / mg/L < 0.001096 / lbs/day Sep 2020 Average 0.017 / mg/L 0.009815 / lbs/day Oct 2020 Average < 0.003 / mg/L < 0.001296 / lbs/day Nov 2020 Average 0.013 / mg/L 0.006733 / lbs/day Dec 2020 Average 0.006 / mg/L 0.003552 / lbs/day 2020 Quarter 3 < 0.007 / mg/L < 0.003775 / lbs/day 2020 Quarter 4 < 0.007 / mg/L < 0.00386 / lbs/day 2020 2nd 6 Months (Avg) < 0.007 / mg/L < 0.003818 / lbs/day 2020 2nd 6 ...(Max) 0.017 / mg/L 0.009815 / lbs/day 2020 2nd 6 ...(Min) < 0.003 / mg/L < 0.000413 / lbs/day 2020 2nd 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass /Limit Copper 07/10/2020 S Cintas071020Se1f 08/04/2020 S Cintas080420Se1f 09/18/2020 S Cintas091820Se1f 10/06/2020 S Cintas100620Se1f 11/06/2020 S Cintas110620Se1f 12/11/2020 S Cintas121120Self 0.052 / mg/L 0.008587 / lbs/day 0.066 / mg/L 0.028938 / lbs/day 0.18 / mg/L 0.103925 / lbs/day 0.039 / mg/L 0.020214 / lbs/day 0.13 / mg/L 0.067329 / lbs/day 0.081 / mg/L 0.048771 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 4 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Copper Jul 2020 Week 2 0.052 Aug 2020 Week 1 0.066 Sep 2020 Week 3 0.18 Oct 2020 Week 1 0.039 Nov 2020 Week 1 0.13 Dec 2020 Week 2 0.081 Jul 2020 Average 0.052 Aug 2020 Average 0.066 Sep 2020 Average 0.18 Oct 2020 Average 0.039 Nov 2020 Average 0.13 Dec 2020 Average 0.081 2020 Quarter 3 0.099 2020 Quarter 4 0.083 2020 2nd 6 Months (Avg) 0.091 2020 2nd 6 ...(Max) 0.18 2020 2nd 6 ...(Min) 0.039 2020 2nd 6 ...(Count) 6 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.008587 0.028938 0.103925 0.020214 0.067329 0.048771 0.008587 0.028938 0.103925 0.020214 0.067329 0.048771 0.04715 0.045438 0.046294 0.103925 0.008587 6 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass/Limit Fluoride 07/10/2020 S Cintas071020Se1f < 0.05 / mg/L < 0.0083 / lbs/day 08/04/2020 S Cintas080420Se1f < 0.05 / mg/L < 0.0219 / lbs/day 08/11/2020 P Cintas081120POTW 0.15 / mg/L / 09/18/2020 S Cintas091820Se1f < 0.05 / mg/L < 0.0289 / lbs/day 10/06/2020 S Cintas100620Se1f < 0.05 / mg/L < 0.0259 / lbs/day 11/06/2020 S Cintas110620Self < 0.05 / mg/L < 0.0259 / lbs/day 12/11/2020 S Cintas121120Self < 0.05 / mg/L < 0.0301 / lbs/day Jul 2020 Week 2 < 0.05 / mg/L < 0.0083 / lbs/day Aug 2020 Week 1 < 0.05 / mg/L < 0.0219 / lbs/day Aug 2020 Week 2 0.15 / mg/L / Sep 2020 Week 3 < 0.05 / mg/L < 0.0289 / lbs/day Oct 2020 Week 1 < 0.05 / mg/L < 0.0259 / lbs/day Nov 2020 Week 1 < 0.05 / mg/L < 0.0259 / lbs/day Dec 2020 Week 2 < 0.05 / mg/L < 0.0301 / lbs/day Jul 2020 Average < 0.05 / mg/L < 0.0083 / lbs/day Aug 2020 Average < 0.1 / mg/L < 0.0219 / lbs/day Sep 2020 Average < 0.05 / mg/L < 0.0289 / lbs/day Oct 2020 Average < 0.05 / mg/L < 0.0259 / lbs/day Nov 2020 Average < 0.05 / mg/L < 0.0259 / lbs/day Dec 2020 Average < 0.05 / mg/L < 0.0301 / lbs/day 2020 Quarter 3 < 0.08 / mg/L < 0.0197 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 5 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 2020 Quarter 4 < 0.05 / mg/L < 0.0273 / lbs/day 2020 2nd 6 Months (Avg) < 0.06 / mg/L < 0.0235 / lbs/day 2020 2nd 6 ...(Max) 0.15 / mg/L 0.0301 / lbs/day 2020 2nd 6 ...(Min) < 0.05 / mg/L < / 2020 2nd 6 ...(Count) 7 / 6 / Sample Date SamplelD Result/Limit Mass/Limit Lead 07/10/2020 S Cintas071020Se1f 0.011 / mg/L 0.001816 / lbs/day 08/04/2020 S Cintas080420Se1f 0.0072 / mg/L 0.003157 / lbs/day 09/18/2020 S Cintas091820Se1f 0.022 / mg/L 0.012702 / lbs/day 10/06/2020 S Cintas100620Se1f < 0.0025 / mg/L < 0.001296 / lbs/day 11/06/2020 S Cintas110620Self 0.016 / mg/L 0.008287 / lbs/day 12/11/2020 S Cintas121120Self 0.008 / mg/L 0.004817 / lbs/day Ju12020 Week 2 0.011 / mg/L 0.001816 / lbs/day Aug 2020 Week 1 0.0072 / mg/L 0.003157 / lbs/day Sep 2020 Week 3 0.022 / mg/L 0.012702 / lbs/day Oct 2020 Week 1 < 0.0025 / mg/L < 0.001296 / lbs/day Nov 2020 Week 1 0.016 / mg/L 0.008287 / lbs/day Dec 2020 Week 2 0.008 / mg/L 0.004817 / lbs/day Ju12020 Average 0.011 / mg/L 0.001816 / lbs/day Aug 2020 Average 0.0072 / mg/L 0.003157 / lbs/day Sep 2020 Average 0.022 / mg/L 0.012702 / lbs/day Oct 2020 Average < 0.0025 / mg/L < 0.001296 / lbs/day Nov 2020 Average 0.016 / mg/L 0.008287 / lbs/day Dec 2020 Average 0.008 / mg/L 0.004817 / lbs/day 2020 Quarter 3 0.0134 / mg/L 0.005892 / lbs/day 2020 Quarter 4 < 0.0088 / mg/L < 0.0048 / lbs/day 2020 2nd 6 Months (Avg) < 0.0111 / mg/L < 0.005346 / lbs/day 2020 2nd 6 ...(Max) 0.022 / mg/L 0.012702 / lbs/day 2020 2nd 6 ...(Min) < 0.0025 / mg/L < 0.001296 / lbs/day 2020 2nd 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass /Limit Mercury 07/10/2020 S Cintas071020Se1f < 0 / mg/L < 0 / lbs/day Jul 2020 Week 2 < 0 / mg/L < 0 / lbs/day Jul 2020 Average < 0 / mg/L < 0 / lbs/day 2020 Quarter 3 < 0 / mg/L < 0 / lbs/day 2020 2nd 6 Months (Avg) < 0.00000 / mg/L < 0.000000 / lbs/day 2020 2nd 6 ...(Max) < 0.00000 / mg/L < 0.000000 / lbs/day 2020 2nd 6 ...(Min) < 0.00000 / mg/L < 0.000000 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 6 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury 2020 2nd 6 ...(Count) Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 08/11/2020 P Cintas081120POTWH 0.000095 / 0.000142 mg/L / g Aug 2020 Week 2 0.000095 / mg/L / Aug 2020 Average 0.000095 / mg/L / 2020 Quarter 3 0.000095 / mg/L / 2020 2nd 6 Months (Avg) 0.000095 / mg/L / 2020 2nd 6 ...(Max) 0.000095 / mg/L / 2020 2nd 6 ...(Min) 0.000095 / mg/L / 2020 2nd 6 ...(Count) 1 / / r Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Molybdenum 07/10/2020 S Cintas071020Se1f 08/04/2020 S Cintas080420Se1f 09/18/2020 S Cintas091820Se1f 10/06/2020 S Cintas100620Self 11/06/2020 S Cintas110620Se1f 12/11/2020 S Cintas121120Self Ju12020 Week 2 Aug 2020 Week 1 Sep 2020 Week 3 Oct 2020 Week 1 Nov 2020 Week 1 Dec 2020 Week 2 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average Nov 2020 Average Dec 2020 Average 0 / mg/L 0.0054 / lbs/day 0 / mg/L 0.011 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.003 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.0126 / lbs/day 0 / mg/L 0.0054 / lbs/day 0 / mg/L 0.011 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.003 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.0126 / lbs/day 0 / mg/L 0.0054 / lbs/day 0 / mg/L 0.011 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.003 / lbs/day 0 / mg/L 0.0104 / lbs/day 0 / mg/L 0.0126 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 7 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 2020 Quarter 3 0 / mg/L 2020 Quarter 4 0 / mg/L 2020 2nd 6 Months (Avg) 0.020 / mg/L 2020 2nd 6 ...(Max) 0.033 / mg/L 2020 2nd 6 ...(Min) 0.006 / mg/L 2020 2nd 6 ...(Count) 6 / 0.0089 / lbs/day 0.0087 / lbs/day 0.0088 / lbs/day 0.0126 / lbs/day 0.0030 / lbs/day 6 / Sample Date SamplelD Result/Limit Mass/Limit Nickel 07/10/2020 S Cintas071020Se1f 0.019 / mg/L 0.003138 / lbs/day 08/04/2020 S Cintas080420Se1f 0.021 / mg/L 0.009207 / lbs/day 09/18/2020 S Cintas091820Se1f 0.027 / mg/L 0.015589 / lbs/day 10/06/2020 S Cintas100620Se1f 0.012 / mg/L 0.00622 / lbs/day 11/06/2020 S Cintas110620Self 0.045 / mg/L 0.023306 / lbs/day 12/11/2020 S Cintas121120Self 0.015 / mg/L 0.009032 / lbs/day Ju12020 Week 2 0.019 / mg/L 0.003138 / lbs/day Aug 2020 Week 1 0.021 / mg/L 0.009207 / lbs/day Sep 2020 Week 3 0.027 / mg/L 0.015589 / lbs/day Oct 2020 Week 1 0.012 / mg/L 0.00622 / lbs/day Nov 2020 Week 1 0.045 / mg/L 0.023306 / lbs/day Dec 2020 Week 2 0.015 / mg/L 0.009032 / lbs/day Ju12020 Average 0.019 / mg/L 0.003138 / lbs/day Aug 2020 Average 0.021 / mg/L 0.009207 / lbs/day Sep 2020 Average 0.027 / mg/L 0.015589 / lbs/day Oct 2020 Average 0.012 / mg/L 0.00622 / lbs/day Nov 2020 Average 0.045 / mg/L 0.023306 / lbs/day Dec 2020 Average 0.015 / mg/L 0.009032 / lbs/day 2020 Quarter 3 0.0223 / mg/L 0.009311 / lbs/day 2020 Quarter 4 0.024 / mg/L 0.012853 / lbs/day 2020 2nd 6 Months (Avg) 0.0232 / mg/L 0.011082 / lbs/day 2020 2nd 6 ...(Max) 0.045 / mg/L 0.023306 / lbs/day 2020 2nd 6 ...(Min) 0.012 / mg/L 0.003138 / lbs/day 2020 2nd 6 ...(Count) 6 / 6 / Sample Date SamplelD Result/Limit Mass /Limit Nitrate -Nitrite 07/10/2020 S Cintas071020Self 08/04/2020 S Cintas080420Self 08/11/2020 P Cintas081120POTW 09/18/2020 S Cintas091820Self 10/06/2020 S Cintas100620Self 11/06/2020 S Cintas110620Se1f 0 / mg/L 0.1 / mg/L 0.2 / mg/L 0.1 / mg/L 0.1 / mg/L 0.2 / mg/L 0.003 / lbs/day 0.022 / lbs/day 0.057 / lbs/day 0.043 / lbs/day 0.093 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 8 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 12/11/2020 Jul 2020 Aug 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 Dec 2020 Jul 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 2020 S Cintas121120Self Week 2 Week 1 Week 2 Week 3 Week 1 Week 1 Week 2 Average Average Average Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0 / 0 / 0 / 0.1 / 0.1 / 0.1 / 0.2 / 0.0 / 7 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.012 0.003 0.022 0.057 0.043 0.093 0.012 0.003 0.022 0.057 0.043 0.093 0.012 0.027 0.049 0.038 0.093 6 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 07/10/2020 08/04/2020 08/11/2020 09/18/2020 10/06/2020 11/06/2020 12/11/2020 Jul 2020 Aug 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 Dec 2020 Jul 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 S Cintas071020Se1f S Cintas080420Se1f P Cintas081120POTW S Cintas091820Se1f S Cintas100620Se1f S Cintas110620Self S Cintas121120Self Week 2 Week 1 Week 2 Week 3 Week 1 Week 1 Week 2 Average Average Average Average Average 13.8 14 66.1 18.6 25.1 32.2 15.6 13.8 14 66.1 18.6 25.1 32.2 15.6 13.8 40.05 18.6 25.1 32.2 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 2.279 / 6.138 10.739 / 13.01 / 16.677 / 9.393 / 2.279 / 6.138 / 10.739 / 13.01 / 16.677 / 9.393 / 2.279 / 6.138 / 10.739 / 13.01 / 16.677 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 9 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total Dec 2020 Average 15.6 / mg/L 2020 Quarter 3 28.13 / mg/L 2020 Quarter 4 24.3 / mg/L 2020 2nd 6 Months (Avg) 26.49 / mg/L 2020 2nd 6 ...(Max) 66.1 / mg/L 2020 2nd 6 ...(Min) 13.8 / mg/L 2020 2nd 6 ...(Count) 7 / 9.393 / lbs/day 6.385 / lbs/day 13.027 / lbs/day 9.706 / lbs/day 16.677 / lbs/day 6 / Sample Date SamplelD Result/Limit Mass /Limit Oil & Grease, HEM (Polar) 07/10/2020 S Cintas071020Se1f 12.1 / 100 mg/L 1.998097 / lbs/day 08/04/2020 S Cintas080420Se1f 10.8 / 100 mg/L 4.735265 / lbs/day 08/11/2020 P Cintas081120POTW < 2.5 / 100 mg/L < / 09/18/2020 S Cintas091820Se1f 23.9 / 100 mg/L 13.79894 / lbs/day 10/06/2020 S Cintas100620Se1f 6.3 / 100 mg/L 3.26538 / lbs/day 11/06/2020 S Cintas110620Self 6.6 / 100 mg/L 3.418232 / lbs/day 12/11/2020 S Cintas121120Self < 2.5 / 100 mg/L < 1.505287 / lbs/day Ju12020 Week 2 12.1 / mg/L 1.998097 / lbs/day Aug 2020 Week 1 10.8 / mg/L 4.735265 / lbs/day Aug 2020 Week 2 < 2.5 / mg/L < / Sep 2020 Week 3 23.9 / mg/L 13.79894 / lbs/day Oct 2020 Week 1 6.3 / mg/L 3.26538 / lbs/day Nov 2020 Week 1 6.6 / mg/L 3.418232 / lbs/day Dec 2020 Week 2 < 2.5 / mg/L < 1.505287 / lbs/day Ju12020 Average 12.1 / mg/L 1.998097 / lbs/day Aug 2020 Average < 6.7 / mg/L < 4.735265 / lbs/day Sep 2020 Average 23.9 / mg/L 13.79894 / lbs/day Oct 2020 Average 6.3 / mg/L 3.26538 / lbs/day Nov 2020 Average 6.6 / mg/L 3.418232 / lbs/day Dec 2020 Average < 2.5 / mg/L < 1.505287 / lbs/day 2020 Quarter 3 < 12.3 / mg/L < 6.844101 / lbs/day 2020 Quarter 4 < 5.1 / mg/L < 2.729633 / lbs/day 2020 2nd 6 Months (Avg) < 9.2 / mg/L < 4.78687 / lbs/day 2020 2nd 6 ...(Max) 23.9 / mg/L 13.798940 / lbs/day 2020 2nd 6 ...(Min) < 2.5 / mg/L < / 2020 2nd 6 ...(Count) 7 / 6 / Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 10 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # cyo # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Oil & Grease, SGT-HEM (Non -Polar) 07/10/2020 S Cintas071020Se1f 8.2 / 100 mg/L 1.3541 / lbs/day 08/04/2020 S Cintas080420Se1f < 2.5 / 100 mg/L < 1.0961 / lbs/day 08/11/2020 P Cintas081120POTW < 2.5 / 100 mg/L < / 09/18/2020 S Cintas091820Se1f 6.2 / 100 mg/L 3.5796 / lbs/day 10/06/2020 S Cintas100620Se1f < 2.5 / 100 mg/L < 1.2958 / lbs/day 11/06/2020 S Cintas110620Se1f 16.8 / 100 mg/L 8.701 / lbs/day 12/11/2020 S Cintas121120Self < 2.5 / 100 mg/L < 1.5053 / lbs/day Ju12020 Week 2 8.2 / mg/L 1.3541 / lbs/day Aug 2020 Week 1 < 2.5 / mg/L < 1.0961 / lbs/day Aug 2020 Week 2 < 2.5 / mg/L < / Sep 2020 Week 3 6.2 / mg/L 3.5796 / lbs/day Oct 2020 Week 1 < 2.5 / mg/L < 1.2958 / lbs/day Nov 2020 Week 1 16.8 / mg/L 8.701 / lbs/day Dec 2020 Week 2 < 2.5 / mg/L < 1.5053 / lbs/day Ju12020 Average 8.2 / mg/L 1.3541 / lbs/day Aug 2020 Average < 2.5 / mg/L < 1.0961 / lbs/day Sep 2020 Average 6.2 / mg/L 3.5796 / lbs/day Oct 2020 Average < 2.5 / mg/L < 1.2958 / lbs/day Nov 2020 Average 16.8 / mg/L 8.701 / lbs/day Dec 2020 Average < 2.5 / mg/L < 1.5053 / lbs/day 2020 Quarter 3 < 4.9 / mg/L < 2.01 / lbs/day 2020 Quarter 4 < 7.3 / mg/L < 3.834 / lbs/day 2020 2nd 6 Months (Avg) < 5.9 / mg/L < 2.9220 / lbs/day 2020 2nd 6 ...(Max) 16.8 / mg/L 8.7010 / lbs/day 2020 2nd 6 ...(Min) < 2.5 / mg/L < / 2020 2nd 6 ...(Count) 7 / 6 / Sample Count : 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 11 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 07/10/2020 S Cintas071020Se1f 7.1 / 6.0 - 10.5 SU 08/04/2020 S Cintas080420Se1f 7 / 6.0 - 10.5 SU 08/11/2020 P Cintas081120POTW 7.6 / 6.0 - 10.5 SU 09/18/2020 S Cintas091820Se1f 7 / 6.0 - 10.5 SU 10/06/2020 S Cintas100620Se1f 7.3 / 6.0 - 10.5 SU 11/06/2020 S Cintas110620Se1f 7.2 / 6.0 - 10.5 SU 12/11/2020 S Cintas121120Self 8.8 / 6.0 - 10.5 SU Ju12020 Week 2 7.1 / SU Aug 2020 Week 1 7 / SU Aug 2020 Week 2 7.6 / SU Sep 2020 Week 3 7 / SU Oct 2020 Week 1 7.3 / SU Nov 2020 Week 1 7.2 / SU Dec 2020 Week 2 8.8 / SU Ju12020 Average 7.1 / SU Aug 2020 Average 7.3 / SU Sep 2020 Average 7 / SU Oct 2020 Average 7.3 / SU Nov 2020 Average 7.2 / SU Dec 2020 Average 8.8 / SU 2020 Quarter 3 7.18 / SU 2020 Quarter 4 7.77 / SU 2020 2nd 6 Months (Avg) 7.43 / SU 2020 2nd 6 ...(Max) 8.8 / SU 2020 2nd 6 ...(Min) 7 / SU 2020 2nd 6 ...(Count) 7 / 1 Sample Count : 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit Silver 07/10/2020 S Cintas071020Se1f < 0.0025 / mg/L < 0.000413 / lbs/day Jul 2020 Week 2 < 0.0025 / mg/L < 0.000413 / lbs/day Jul 2020 Average < 0.0025 / mg/L < 0.000413 / lbs/day 2020 Quarter 3 < 0.0025 / mg/L < 0.000413 / lbs/day 2020 2nd 6 Months (Avg) < 0.0025 / mg/L < 0.000413 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 12 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Silver 2020 2nd 6 ...(Max) < 0.0025 / mg/L < 0.000413 / lbs/day 2020 2nd 6 ...(Min) < 0.0025 / mg/L < 0.000413 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Temperature 07/10/2020 S Cintas071020Se1f 37.3 / 66 °C / 08/04/2020 S Cintas080420Se1f 36.1 / 66 °C / 08/11/2020 P Cintas081120POTW 30.6 / 66 °C / 09/18/2020 S Cintas091820Se1f 25.5 / 66 °C / 10/06/2020 S Cintas100620Se1f 33.4 / 66 °C / 11/06/2020 S Cintas110620Self 28.2 / 66 °C / 12/11/2020 S Cintas121120Self 25.3 / 66 °C / Ju12020 Week 2 37.3 / °C / Aug 2020 Week 1 36.1 / °C / Aug 2020 Week 2 30.6 / °C / Sep 2020 Week 3 25.5 / °C / Oct 2020 Week 1 33.4 / °C / Nov 2020 Week 1 28.2 / °C / Dec 2020 Week 2 25.3 / °C / Ju12020 Average 37.3 / °C / Aug 2020 Average 33.4 / °C / Sep 2020 Average 25.5 / °C / Oct 2020 Average 33.4 / °C / Nov 2020 Average 28.2 / °C / Dec 2020 Average 25.3 / °C / 2020 Quarter 3 32.4 / °C / 2020 Quarter 4 29 / °C / 2020 2nd 6 Months (Avg) 30.9 / °C / 2020 2nd 6 ...(Max) 37.3 / °C / 2020 2nd 6 ...(Min) 25.3 / °C / 2020 2nd 6 ...(Count) 7 / / Sample Count : 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over QtrAvg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtrAvg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 13 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN 07/10/2020 07/21/2020 08/04/2020 08/11/2020 09/18/2020 09/24/2020 10/06/2020 10/20/2020 11/06/2020 11/24/2020 12/11/2020 12/11/2020 Jul 2020 Jul 2020 Aug 2020 Aug 2020 Sep 2020 Sep 2020 Oct 2020 Oct 2020 Nov 2020 Nov 2020 Dec 2020 Jul 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 2020 S Cintas071020Se1f P Cintas072120POTW S Cintas080420Se1f P Cintas081120POTW S Cintas091820Se1f P Cintas092420POTW S Cintas100620Se1f P Cintas102020POTW S Cintas110620Se1f P Cintas112420POTW P Cintas121120POTW S Cintas121120Self Week 2 Week 3 Week 1 Week 2 Week 3 Week 4 Week 1 Week 3 Week 1 Week 4 Week 2 Average Average Average Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 13.7 / mg/L 33.8 / mg/L 14 / mg/L 65.9 / mg/L 18.5 / mg/L 19.6 / mg/L 25 / mg/L 23.5 / mg/L 32.1 / mg/L 32.2 / mg/L 8.48 / mg/L 15.6 / mg/L 13.7 / mg/L 33.8 / mg/L 14 / mg/L 65.9 / mg/L 18.5 / mg/L 19.6 / mg/L 25 / mg/L 23.5 / mg/L 32.1 / mg/L 32.2 / mg/L 12.04 / mg/L 23.75 / mg/L 39.95 / mg/L 19.05 / mg/L 24.25 / mg/L 32.15 / mg/L 12.04 / mg/L 27.58 / mg/L 22.81 / mg/L 25.20 / mg/L 65.9 / mg/L 8.48 / mg/L 12 / 2.262 6.138 10.681 12.958 16.625 9.393 2.262 6.138 10.681 12.958 16.625 9.393 2.262 6.138 10.681 12.958 16.625 9.393 6.361 12.992 9.676 16.625 6 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 07/10/2020 S 07/21/2020 08/04/2020 08/11/2020 P S P Cintas071020Se1f Cintas072120POTW Cintas080420Se1f Cintas081120POTW mg/L mg/L mg/L mg/L 0.2477 / 0.4823 / lbs/day lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 14 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 09/18/2020 S 09/24/2020 P 10/06/2020 S 10/20/2020 P 11/06/2020 S 11/24/2020 P 12/11/2020 P 12/11/2020 S Jul 2020 Jul 2020 Aug 2020 Aug 2020 Sep 2020 Sep 2020 Oct 2020 Oct 2020 Nov 2020 Nov 2020 Dec 2020 Jul 2020 Aug 2020 Sep 2020 Oct 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 2020 Cintas091820Se1f Cintas092420POTW Cintas100620Se1f Cintas102020POTW Cintas 110620Se1f Cintas 112420POTW Cintas 121120POTW Cintas 121120Self Week 2 Week 3 Week 1 Week 2 Week 3 Week 4 Week 1 Week 3 Week 1 Week 4 Week 2 Average Average Average Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 2.1 / mg/L 2.41 / mg/L 3 / mg/L 3.35 / mg/L 3.4 / mg/L 2.69 / mg/L 4.86 / mg/L 1.4 / mg/L 1.5 / mg/L 3.07 / mg/L 1.1 / mg/L 4.56 / mg/L 2.1 / mg/L 2.41 / mg/L 3 / mg/L 3.35 / mg/L 3.4 / mg/L 2.69 / mg/L 3.13 / mg/L 2.285 / mg/L 2.83 / mg/L 2.255 / mg/L 3.175 / mg/L 3.045 / mg/L 3.13 / mg/L 2.457 / mg/L 3.117 / mg/L 2.787 / mg/L 4.86 / mg/L 1.1 / mg/L 12 / 1.2125 1.5549 1.7609 0.843 0.2477 0.4823 1.2125 1.5549 1.7609 0.843 0.2477 0.4823 1.2125 1.5549 1.7609 0.843 0.6475 1.3863 1.0169 1.7609 6 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit TSS 07/10/2020 07/21/2020 08/04/2020 08/11/2020 09/18/2020 09/24/2020 10/06/2020 10/20/2020 S Cintas071020Se1f P Cintas072120POTW S Cintas080420Se1f P Cintas081120POTW S Cintas091820Se1f P Cintas092420POTW S Cintas100620Se1f P Cintas102020POTW 97.6 / 1000 / 89.5 / 110 / 315 / 262 / 95.7 / 150 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 16.116883 / 39.241318 / 181.868879 / 49.60268 / lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 15 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TSS 11/06/2020 S Cintas110620Se1f 11/24/2020 P Cintas112420POTW 12/11/2020 P Cintas121120POTW 12/11/2020 S Cintas121120Self Ju12020 Week 2 Ju12020 Week 3 Aug 2020 Week 1 Aug 2020 Week 2 Sep 2020 Week 3 Sep 2020 Week 4 Oct 2020 Week 1 Oct 2020 Week 3 Nov 2020 Week 1 Nov 2020 Week 4 Dec 2020 Week 2 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average Nov 2020 Average Dec 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 591 / mg/L 195 / mg/L 496 / mg/L 348 / mg/L 97.6 / mg/L 1000 / mg/L 89.5 / mg/L 110 / mg/L 315 / mg/L 262 / mg/L 95.7 / mg/L 150 / mg/L 591 / mg/L 195 / mg/L 422 / mg/L 548.8 / mg/L 99.8 / mg/L 288.5 / mg/L 122.9 / mg/L 393 / mg/L 422 / mg/L 312.4 / mg/L 312.6 / mg/L 312.5 / mg/L 1000 / mg/L 89.5 / mg/L 12 / 306.087174 / lbs/day 209.535895 / lbs/day 16.116883 / lbs/day 39.241318 / lbs/day 181.868879 / lbs/day 49.60268 / lbs/day 306.087174 / lbs/day 209.535895 / lbs/day 16.116883 / lbs/day 39.241318 / lbs/day 181.868879 / lbs/day 49.60268 / lbs/day 306.087174 / lbs/day 209.535895 / lbs/day 79.075693 / lbs/day 188.408583 / lbs/day 133.742 / lbs/day 306.087174 / lbs/day 6 / Sample Date SamplelD Result/Limit Mass/Limit VOC 07/10/2020 S Cintas071020Se1f 0.01 / mg/L / Jul 2020 Week 2 0.01 / mg/L / Jul 2020 Average 0.01 / mg/L / 2020 Quarter 3 0.01 / mg/L / 2020 2nd 6 Months (Avg) 0.01 / mg/L / 2020 2nd 6 ...(Max) 0.01 / mg/L / 2020 2nd 6 ...(Min) 0.01 / mg/L / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Zinc 07/10/2020 S Cintas071020Se1f 1.2 / mg/L 0.198158 / lbs/day Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 16 of 17 Cintas Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc 08/04/2020 S Cintas080420Se1f 09/18/2020 S Cintas091820Se1f 10/06/2020 S Cintas100620Se1f 12/11/2020 S Cintas121120Self Ju12020 Week 2 Aug 2020 Week 1 Sep 2020 Week 3 Oct 2020 Week 1 Dec 2020 Week 2 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average Dec 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.92 / mg/L 0.96 / mg/L 0.47 / mg/L 0.83 / mg/L 1.2 / mg/L 0.92 / mg/L 0.96 / mg/L 0.47 / mg/L 0.83 / mg/L 1.2 / mg/L 0.92 / mg/L 0.96 / mg/L 0.47 / mg/L 0.83 / mg/L 1.027 / mg/L 0.65 / mg/L 0.876 / mg/L 1.2 / mg/L 0.47 / mg/L 5 / 0.403374 / lbs/day 0.554267 / lbs/day 0.243608 / lbs/day 0.499755 / lbs/day 0.198158 / lbs/day 0.403374 / lbs/day 0.554267 / lbs/day 0.243608 / lbs/day 0.499755 / lbs/day 0.198158 / lbs/day 0.403374 / lbs/day 0.554267 / lbs/day 0.243608 / lbs/day 0.499755 / lbs/day 0.385267 / lbs/day 0.371681 / lbs/day 0.379833 / lbs/day 0.554267 / lbs/day 0.198158 / lbs/day 5 / Wednesday, February 24, 2021 10:40:30PM * Indicates Violation ** Indicates TRC Violation Page 17 of 17 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Ammonia 08/14/2020 S CreeP8081420Se1f 13 10/27/2020 CreeP8102720POTW 11.9 Aug 2020 Week 2 13 Oct 2020 Week 4 11.9 Aug 2020 Average 13 Oct 2020 Average 11.9 2020 Quarter 3 13 2020 Quarter 4 11.9 2020 2nd 6 Months (Avg) 12.45 2020 2nd 6 ...(Max) 13 2020 2nd 6 ...(Min) 11.9 2020 2nd 6 ...(Count) 2 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 42.067 / lbs/day 42.067 / lbs/day 42.067 / lbs/day 42.067 / lbs/day 42.067 / lbs/day 42.0670 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/31/2020 S CreeP80720F1ow 08/31/2020 S CreeP80820F1ow 09/30/2020 S CreeP80920F1ow 10/31/2020 S CreeP81020F1ow Ju12020 Week 4 Aug 2020 Week 4 Sep 2020 Week 4 Oct 2020 Week 4 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.400329 / MGD 0.372909 / MGD 0.382608 / MGD 0.341903 / MGD 0.400329 / MGD 0.372909 / MGD 0.382608 / MGD 0.341903 / MGD 0.400329 / MGD 0.372909 / MGD 0.382608 / MGD 0.341903 / MGD 0.385282 / MGD 0.341903 / MGD 0.374437 / MGD 0.400329 / MGD 0.341903 / MGD 4 / Sample Date SamplelD Result/Limit Mass /Limit Barium 08/14/2020 S CreeP8081420Se1f 0.025 / mg/L 0.0809 / lbs/day Aug 2020 Week 2 0.025 / mg/L 0.0809 / lbs/day Aug 2020 Average 0.025 / mg/L 0.0809 / lbs/day 2020 Quarter 3 0.025 / mg/L 0.0809 / lbs/day 2020 2nd 6 Months (Avg) 0.025 / mg/L 0.0809 / lbs/day 2020 2nd 6 ...(Max) 0.025 / mg/L 0.0809 / lbs/day Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Barium 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.025 / mg/L 1 / 0.0809 / lbs/day 1 / Sample Date SamplelD Result /Limit Mass /Limit Chloride 08/14/2020 S CreeP8081420Se1f 86.6 / mg/L 280.2307 / lbs/day 10/27/2020 CreeP8102720POTW 100 / mg/L / Aug 2020 Week 2 86.6 / mg/L 280.2307 / lbs/day Oct 2020 Week 4 100 / mg/L / Aug 2020 Average 86.6 / mg/L 280.2307 / lbs/day Oct 2020 Average 100 / mg/L / 2020 Quarter 3 86.6 / mg/L 280.2307 / lbs/day 2020 Quarter 4 100 / mg/L / 2020 2nd 6 Months (Avg) 93.3 / mg/L 280.231 / lbs/day 2020 2nd 6 ...(Max) 100 / mg/L 280.2307 / lbs/day 2020 2nd 6 ...(Min) 86.6 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Cyanide 08/14/2020 S CreeP8081420Se1f 0.018 / mg/L 0.058247 / lbs/day 10/27/2020 CreeP8102720POTW < 0.003 / mg/L < / Aug 2020 Week 2 0.018 / mg/L 0.058247 / lbs/day Oct 2020 Week 4 < 0.003 / mg/L < / Aug 2020 Average 0.018 / mg/L 0.058247 / lbs/day Oct 2020 Average < 0.003 / mg/L < / 2020 Quarter 3 0.018 / mg/L 0.058247 / lbs/day 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.010 / mg/L < 0.058247 / lbs/day 2020 2nd 6 ...(Max) 0.018 / mg/L 0.058247 / lbs/day 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result / Limit Mass/Limit Fluoride 08/14/2020 S CreeP8081420Se1f 1.3 / mg/L 4.2067 / lbs/day 10/27/2020 CreeP8102720POTW 1.53 / mg/L / Aug 2020 Week 2 1.3 / mg/L 4.2067 / lbs/day Oct 2020 Week 4 1.53 / mg/L / Aug 2020 Average 1.3 / mg/L 4.2067 / lbs/day Oct 2020 Average 1.53 / mg/L / Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 2020 Quarter 3 1.3 / mg/L 2020 Quarter 4 1.53 / mg/L 2020 2nd 6 Months (Avg) 1.42 / mg/L 2020 2nd 6 ...(Max) 1.53 / mg/L 2020 2nd 6 ...(Min) 1.3 / mg/L 2020 2nd 6 ...(Count) 2 / 4.2067 / lbs/day 4.2067 / lbs/day 4.2067 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 08/14/2020 S CreeP8081420Se1f 0.000004 / mg/L / 10/27/2020 P CreeP8102720POTW 0.000048 / mg/L / Hg Aug 2020 Week 2 0.000004 / mg/L / Oct 2020 Week 4 0.000048 / mg/L / Aug 2020 Average 0.000004 / mg/L / Oct 2020 Average 0.000048 / mg/L / 2020 Quarter 3 0.000004 / mg/L / 2020 Quarter 4 0.000048 / mg/L / 2020 2nd 6 Months (Avg) 0.000026 / mg/L / 2020 2nd 6 ...(Max) 0.000048 / mg/L / 2020 2nd 6 ...(Min) 0.000004 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Nitrate -Nitrite 10/27/2020 CreeP8102720POTW 2.3 / mg/L / Oct 2020 Week 4 2.3 / mg/L / Oct 2020 Average 2.3 / mg/L / 2020 Quarter 4 2.3 / mg/L / 2020 2nd 6 Months (Avg) 2.3 / mg/L / 2020 2nd 6 ...(Max) 2.3 / mg/L / 2020 2nd 6 ...(Min) 2.3 / mg/L / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Nitrogen, Total 08/14/2020 S CreeP8081420Se1f 17 / mg/L 55.011 / lbs/day 10/27/2020 CreeP8102720POTW 20.1 / mg/L / Aug 2020 Week 2 17 / mg/L 55.011 / lbs/day Oct 2020 Week 4 20.1 / mg/L / Aug 2020 Average 17 / mg/L 55.011 / lbs/day Oct 2020 Average 20.1 / mg/L / Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 2020 Quarter 3 17 / mg/L 2020 Quarter 4 20.1 / mg/L 2020 2nd 6 Months (Avg) 18.55 / mg/L 2020 2nd 6 ...(Max) 20.1 / mg/L 2020 2nd 6 ...(Min) 17 / mg/L 2020 2nd 6 ...(Count) 2 / 55.011 / lbs/day 55.011 / lbs/day 55.011 / lbs/day Sample Date SamplelD Result/Limit Mass/Limit Oil & Grease, Total 10/27/2020 CreeP8102720POTW < 2.5 / mg/L Oct 2020 Week 4 < 2.5 / mg/L Oct 2020 Average < 2.5 / mg/L 2020 Quarter 4 < 2.5 / mg/L 2020 2nd 6 Months (Avg) < 2.5 / mg/L 2020 2nd 6 ...(Max) < 2.5 / mg/L 2020 2nd 6 ...(Min) < 2.5 / mg/L 2020 2nd 6 ...(Count) 1 / < / < / < / Sample Date SamplelD Result/Limit Mass /Limit pH 08/14/2020 S CreeP8081420Se1f 9.4 / 5.0 - 10.5 SU / 10/27/2020 CreeP8102720POTW 8.3 / 5.0 - 10.5 SU / Aug 2020 Week 2 9.4 / SU / Oct 2020 Week 4 8.3 / SU / Aug 2020 Average 9.4 / SU / Oct 2020 Average 8.3 / SU / 2020 Quarter 3 9.4 / SU / 2020 Quarter 4 8.3 / SU / 2020 2nd 6 Months (Avg) 8.85 / SU / 2020 2nd 6 ...(Max) 9.4 / SU / 2020 2nd 6 ...(Min) 8.3 / SU / 2020 2nd 6 ...(Count) 2 / / 1 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 008 Sample Date SamplelD Result /Limit Mass /Limit Temperature 08/14/2020 S CreeP8081420Se1f 25.7 / 66 °C 10/27/2020 CreeP8102720POTW 24 / 66 °C Aug 2020 Week 2 25.7 / °C Oct 2020 Week 4 24 / °C Aug 2020 Average 25.7 / °C Oct 2020 Average 24 / °C 2020 Quarter 3 25.7 / °C 2020 Quarter 4 24 / °C 2020 2nd 6 Months (Avg) 24.9 / °C 2020 2nd 6 ...(Max) 25.7 / °C 2020 2nd 6 ...(Min) 24 / °C 2020 2nd 6 ...(Count) 2 / 1 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit TKN 10/27/2020 CreeP8102720POTW 17.8 / mg/L / Oct 2020 Week 4 17.8 / mg/L / Oct 2020 Average 17.8 / mg/L / 2020 Quarter 4 17.8 / mg/L / 2020 2nd 6 Months (Avg) 17.8 / mg/L / 2020 2nd 6 ...(Max) 17.8 / mg/L / 2020 2nd 6 ...(Min) 17.8 / mg/L / 2020 2nd 6 ...(Count) I / / Sample Date SamplelD Result/Limit Mass/Limit Zinc 08/14/2020 S CreeP8081420Se1f 0.32 / mg/L 1.035494 / lbs/day Aug 2020 Week 2 0.32 / mg/L 1.035494 / lbs/day Aug 2020 Average 0.32 / mg/L 1.035494 / lbs/day 2020 Quarter 3 0.32 / mg/L 1.035494 / lbs/day 2020 2nd 6 Months (Avg) 0.32 / mg/L 1.03549 / lbs/day 2020 2nd 6 ...(Max) 0.32 / mg/L 1.035494 / lbs/day 2020 2nd 6 ...(Min) 0.32 / mg/L 1.035494 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 07/31/2020 S CreeP90720F1ow 0.049382 08/14/2020 S CreeP90820F1ow 0.049797 09/30/2020 S CreeP90920F1ow 0.052401 10/31/2020 P CreeP91020F1ow 0.055614 Ju12020 Week 4 0.049382 Aug 2020 Week 2 0.049797 Sep 2020 Week 4 0.052401 Oct 2020 Week 4 0.055614 Jul 2020 Average 0.049382 Aug 2020 Average 0.049797 Sep 2020 Average 0.052401 Oct 2020 Average 0.055614 2020 Quarter 3 0.050527 2020 Quarter 4 0.055614 2020 2nd 6 Months (Avg) 0.051799 2020 2nd 6 ...(Max) 0.055614 2020 2nd 6 ...(Min) 0.049382 2020 2nd 6 ...(Count) 4 MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD MGD Sample Date SamplelD Result / Limit Mass/Limit Fluoride 08/14/2020 S CreeP9081420Se1f < 0.05 / mg/L < / 10/27/2020 P CreeP9102720POTW < 0.05 / mg/L < / Aug 2020 Week 2 < 0.05 / mg/L < / Oct 2020 Week 4 < 0.05 / mg/L < / Aug 2020 Average < 0.05 / mg/L < / Oct 2020 Average < 0.05 / mg/L < / 2020 Quarter 3 < 0.05 / mg/L < / 2020 Quarter 4 < 0.05 / mg/L < / 2020 2nd 6 Months (Avg) < 0.05 / mg/L < / 2020 2nd 6 ...(Max) < 0.05 / mg/L < / 2020 2nd 6 ...(Min) < 0.05 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass /Limit Mercury - LL 08/14/2020 S CreeP9081420Se1f 0.000025 / mg/L 10/27/2020 P CreeP9102720POTW 0.000013 / mg/L Hg Aug 2020 Week 2 0.000025 / mg/L Oct 2020 Week 4 0.000013 / mg/L Aug 2020 Average 0.000025 / mg/L Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL Oct 2020 Average 0.000013 / mg/L 2020 Quarter 3 0.000025 / mg/L 2020 Quarter 4 0.000013 / mg/L 2020 2nd 6 Months (Avg) 0.000019 / mg/L 2020 2nd 6 ...(Max) 0.000025 / mg/L 2020 2nd 6 ...(Min) 0.000013 / mg/L 2020 2nd 6 ...(Count) 2 / Sample Date SamplelD Result/Limit Mass /Limit Molybdenum 10/27/2020 P CreeP9102720POTW < 0.001 / mg/L < / Oct 2020 Week 4 < 0.001 / mg/L < / Oct 2020 Average < 0.001 / mg/L < / 2020 Quarter 4 < 0.001 / mg/L < / 2020 2nd 6 Months (Avg) < 0.001 / mg/L < / 2020 2nd 6 ...(Max) < 0.001 / mg/L < / 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Oil & Grease, Total 10/27/2020 P CreeP9102720POTW < 2.5 / mg/L < / Oct 2020 Week 4 < 2.5 / mg/L < / Oct 2020 Average < 2.5 / mg/L < / 2020 Quarter 4 < 2.5 / mg/L < / 2020 2nd 6 Months (Avg) < 2.5 / mg/L < / 2020 2nd 6 ...(Max) < 2.5 / mg/L < / 2020 2nd 6 ...(Min) < 2.5 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit pH 08/14/2020 S CreeP9081420Se1f 10/27/2020 P CreeP9102720POTW Aug 2020 Week 2 Oct 2020 Week 4 Aug 2020 Average Oct 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 7.4 /5.0-10.5 SU / 7.3 /5.0-10.5 SU / 7.4 / SU / 7.3 / SU / 7.4 / SU / 7.3 / SU / 7.4 / SU / 7.3 / SU / 7.35 / SU / Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 009 Sample Date SamplelD Result /Limit Mass /Limit pH 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 7.4 / SU 7.3 / SU 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Temperature 08/14/2020 10/27/2020 Aug 2020 Oct 2020 Aug 2020 Oct 2020 2020 2020 2020 2020 2020 2020 S CreeP9081420Se1f P CreeP9102720POTW Week 2 Week 4 Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 26.2 / 23 / 26.2 / 23 / 26.2 / 23 / 26.2 / 23 / 24.6 / 26.2 / 23 / 2 / °C °C °C °C °C °C °C °C °C °C °C 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Ou fall: All Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 07/31/2020 S Cree0720F1ow 0.449711 / 0.600 MGD 08/31/2020 S Cree0820F1ow 0.422706 / 0.600 MGD 09/30/2020 S Cree0920F1ow 0.435009 / 0.600 MGD 10/31/2020 S Cree1020F1ow 0.397517 / 0.600 MGD Ju12020 Week 4 0.449711 / MGD Aug 2020 Week 4 0.422706 / MGD Sep 2020 Week 4 0.435009 / MGD Oct 2020 Week 4 0.397517 / MGD Ju12020 Average 0.449711 / 0.451 MGD Aug 2020 Average 0.422706 / 0.451 MGD Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: All Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Sep 2020 Average 0.435009 / 0.451 MGD Oct 2020 Average 0.397517 / 0.451 MGD 2020 Quarter 3 0.435809 / MGD 2020 Quarter 4 0.397517 / MGD 2020 2nd 6 Months (Avg) 0.426236 / MGD 2020 2nd 6 ...(Max) 0.449711 / MGD 2020 2nd 6 ...(Min) 0.397517 / MGD 2020 2nd 6 ...(Count) 4 / Sample Count : 4 Months Sampled : 4 Weeks Sampled : 4 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 08/14/2020 S Cree081420Se1f 1.15 / 8.0 mg/L / 10/27/2020 P Cree102720POTW 1.32 / 8.0 mg/L / Aug 2020 Week 2 1.15 / mg/L / Oct 2020 Week 4 1.32 / mg/L / Aug 2020 Average 1.15 / 7.0 mg/L / Oct 2020 Average 1.32 / 7.0 mg/L / 2020 Quarter 3 1.15 / mg/L / 2020 Quarter 4 1.32 / mg/L / 2020 2nd 6 Months (Avg) 1.24 / mg/L / 2020 2nd 6 ...(Max) 1.32 / mg/L / 2020 2nd 6 ...(Min) 1.15 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 1 of 2 Cree, Inc.(A11) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: All Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 08/14/2020 S Cree081420Se1f 0.000006 / 0.000142 mg/L 10/27/2020 P Cree102720POTW 0.000043 / 0.000142 mg/L Aug 2020 Week 2 0.000006 / mg/L Oct 2020 Week 4 0.000043 / mg/L Aug 2020 Average 0.000006 / mg/L Oct 2020 Average 0.000043 / mg/L 2020 Quarter 3 0.000006 / mg/L 2020 Quarter 4 0.000043 / mg/L 2020 2nd 6 Months (Avg) 0.000025 / mg/L 2020 2nd 6 ...(Max) 0.000043 / mg/L 2020 2nd 6 ...(Min) 0.000006 / mg/L 2020 2nd 6 ...(Count) 2 / 1 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:37:58PM * Indicates Violation ** Indicates TRC Violation Page 2 of 2 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Ammonia 08/14/2020 S CreeRTPP12081420Se 2.7 / mg/L if 11/19/2020 P CreeRTPP12111920PO 2.3 / mg/L TW Aug 2020 Week 2 2.7 / mg/L / Nov 2020 Week 3 2.3 / mg/L / Aug 2020 Average 2.7 / mg/L / Nov 2020 Average 2.3 / mg/L / 2020 Quarter 3 2.7 / mg/L / 2020 Quarter 4 2.3 / mg/L / 2020 2nd 6 Months (Avg) 2.5 / mg/L / 2020 2nd 6 ...(Max) 2.7 / mg/L / 2020 2nd 6 ...(Min) 2.3 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result / Limit Mass /Limit Average Flow for Month 07/16/2020 S CreeRTPP120720F1ow 0.160066 / 0.469 MGD 08/21/2020 S CreeRTPP120820F1ow 0.15684 / 0.469 MGD 09/17/2020 S CreeRTPP120920F1ow 0.153263 / 0.469 MGD 10/22/2020 S CreeRTPP121020F1ow 0.131828 / 0.469 MGD Ju12020 Week 3 0.160066 / MGD Aug 2020 Week 3 0.15684 / MGD Sep 2020 Week 3 0.153263 / MGD Oct 2020 Week 4 0.131828 / MGD Ju12020 Average 0.160066 / 0.329 MGD Aug 2020 Average 0.15684 / 0.329 MGD Sep 2020 Average 0.153263 / 0.329 MGD Oct 2020 Average 0.131828 / 0.329 MGD 2020 Quarter 3 0.156723 / MGD 2020 Quarter 4 0.131828 / MGD 2020 2nd 6 Months (Avg) 0.150499 / MGD 2020 2nd 6 ...(Max) 0.160066 / MGD 2020 2nd 6 ...(Min) 0.131828 / MGD 2020 2nd 6 ...(Count) 4 / Sample Count : 4 Months Sampled : 4 Weeks Sampled : 4 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 1 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Chloride 08/14/2020 S CreeRTPP12081420Se if 11/19/2020 P CreeRTPP12111920P0 TW Aug 2020 Week 2 Nov 2020 Week 3 Aug 2020 Average Nov 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 12.2 / mg/L 119 / mg/L 12.2 / 119 / 12.2 / 119 / 12.2 / 119 / 65.6 / 119 / 12.2 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result / Limit Mass /Limit Cyanide 08/14/2020 S CreeRTPP12081420Se < 0.004 / mg/L < / If 11/19/2020 P CreeRTPP12111920PO < 0.003 / mg/L < / TW Aug 2020 Week 2 < 0.004 / mg/L < / Nov 2020 Week 3 < 0.003 / mg/L < / Aug 2020 Average < 0.004 / mg/L < / Nov 2020 Average < 0.003 / mg/L < / 2020 Quarter 3 < 0.004 / mg/L < / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) < 0.004 / mg/L < / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass /Limit Fluoride 08/14/2020 S CreeRTPP12081420Se 0.37 / 8.0 mg/L / if 11/19/2020 P CreeRTPP12111920PO 0.93 / 8.0 mg/L / TW Aug 2020 Week 2 0.37 / mg/L / Nov 2020 Week 3 0.93 / mg/L / Aug 2020 Average 0.37 / 7.0 mg/L / Nov 2020 Average 0.93 / 7.0 mg/L / 2020 Quarter 3 0.37 / mg/L / 2020 Quarter 4 0.93 / mg/L / Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 2 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 2020 2nd 6 Months (Avg) 0.65 / mg/L 2020 2nd 6 ...(Max) 0.93 / mg/L 2020 2nd 6 ...(Min) 0.37 / mg/L 2020 2nd 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Mercury - LL 08/14/2020 S CreeRTPP12081420Se 0.000002 / mg/L / if 11/19/2020 P CreeP12111920POTW 0.00001 / mg/L / Hg Aug 2020 Week 2 0.000002 / mg/L / Nov 2020 Week 3 0.00001 / mg/L / Aug 2020 Average 0.000002 / 0.000142 mg/L / Nov 2020 Average 0.00001 / 0.000142 mg/L / 2020 Quarter 3 0.000002 / mg/L / 2020 Quarter 4 0.00001 / mg/L / 2020 2nd 6 Months (Avg) 0.000006 / mg/L / 2020 2nd 6 ...(Max) 0.00001 / mg/L / 2020 2nd 6 ...(Min) 0.000002 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 08/14/2020 S CreeRTPP12081420Se < 0.003 / mg/L < / if Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 3 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Molybdenum 11/19/2020 P CreeRTPP12111920PO < 0.001 / mg/L < / TW Aug 2020 Week 2 < 0.003 / mg/L < / Nov 2020 Week 3 < 0.001 / mg/L < / Aug 2020 Average < 0.003 / mg/L < / Nov 2020 Average < 0.001 / mg/L < / 2020 Quarter 3 < 0.003 / mg/L < / 2020 Quarter 4 < 0.001 / mg/L < / 2020 2nd 6 Months (Avg) < 0.002 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Nitrate -Nitrite 11/19/2020 P CreeRTPP12111920PO 2 / mg/L / TW Nov 2020 Week 3 2 / mg/L / Nov 2020 Average 2 / mg/L / 2020 Quarter 4 2 / mg/L / 2020 2nd 6 Months (Avg) 2.0 / mg/L / 2020 2nd 6 ...(Max) 2.0 / mg/L / 2020 2nd 6 ...(Min) 2.0 / mg/L / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result / Limit Mass /Limit Nitrogen, Total 08/14/2020 S CreeRTPP12081420Se 22.1 / mg/L / If 11/19/2020 P CreeRTPP12111920PO 14.4 / mg/L / TW Aug 2020 Week 2 22.1 / mg/L / Nov 2020 Week 3 14.4 / mg/L / Aug 2020 Average 22.1 / mg/L / Nov 2020 Average 14.4 / mg/L / 2020 Quarter 3 22.1 / mg/L / 2020 Quarter 4 14.4 / mg/L / 2020 2nd 6 Months (Avg) 18.25 / mg/L / 2020 2nd 6 ...(Max) 22.1 / mg/L / 2020 2nd 6 ...(Min) 14.4 / mg/L / 2020 2nd 6 ...(Count) 2 / / Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 4 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 11/19/2020 P CreeRTPP12111920PO < 2.5 / 200 mg/L < / TW Nov 2020 Week 3 < 2.5 / mg/L < / Nov 2020 Average < 2.5 / mg/L < / 2020 Quarter 4 < 2.5 / mg/L < / 2020 2nd 6 Months (Avg) < 2.5 / mg/L < / 2020 2nd 6 ...(Max) < 2.5 / mg/L < / 2020 2nd 6 ...(Min) < 2.5 / mg/L < / 2020 2nd 6 ...(Count) 1 / / 1 Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 08/14/2020 S CreeRTPP12081420Se 8.5 / 5.0 - 10.5 SU / if 11/19/2020 P CreeRTPP12111920PO 7.3 / 5.0 - 10.5 SU / TW Aug 2020 Week 2 8.5 / SU / Nov 2020 Week 3 7.3 / SU / Aug 2020 Average 8.5 / SU / Nov 2020 Average 7.3 / SU / 2020 Quarter 3 8.5 / SU / 2020 Quarter 4 7.3 / SU / 2020 2nd 6 Months (Avg) 7.9 / SU / 2020 2nd 6 ...(Max) 8.5 / SU / 2020 2nd 6 ...(Min) 7.3 / SU / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 5 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Temperature 08/14/2020 S CreeRTPP12081420Se 26.3 / 66 °C if 11/19/2020 P CreeRTPP12111920PO 14 / 66 °C TW Aug 2020 Week 2 26.3 / °C Nov 2020 Week 3 14 / °C Aug 2020 Average 26.3 / °C Nov 2020 Average 14 / °C 2020 Quarter 3 26.3 / °C 2020 Quarter 4 14 / °C 2020 2nd 6 Months (Avg) 20.2 / °C 2020 2nd 6 ...(Max) 26.3 / °C 2020 2nd 6 ...(Min) 14 / °C 2020 2nd 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 # Sample Date SamplelD Result/Limit Mass/Limit TKN 11/19/2020 P CreeRTPP12111920PO 12.4 / mg/L / TW Nov 2020 Week 3 12.4 / mg/L / Nov 2020 Average 12.4 / mg/L / 2020 Quarter 4 12.4 / mg/L / 2020 2nd 6 Months (Avg) 12.4 / mg/L / 2020 2nd 6 ...(Max) 12.4 / mg/L / 2020 2nd 6 ...(Min) 12.4 / mg/L / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Total Phosphorus 11/19/2020 P CreeRTPP12111920PO 1.68 / mg/L / TW Nov 2020 Week 3 1.68 / mg/L / Nov 2020 Average 1.68 / mg/L / 2020 Quarter 4 1.68 / mg/L / 2020 2nd 6 Months (Avg) 1.68 / mg/L / Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 6 of 7 Cree, Inc.(RTP) SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 012 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 1.68 / mg/L 1.68 / mg/L 1 / Wednesday, February 24, 2021 10:35:29PM * Indicates Violation ** Indicates TRC Violation Page 7 of 7 JMC (USA), Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 07/31/2020 S JMC0720F1ow 0.00001 / MGD 08/31/2020 S JMC0820F1ow 0.000088 / MGD 09/30/2020 S JMC0920F1ow 0.000037 / MGD 10/31/2020 S JMC1020F1ow 0.000006 / MGD 11/30/2020 S JMC1120F1ow 0.000011 / MGD 12/31/2020 S JMC1220F1ow 0.000093 / MGD Jul 2020 Week 4 0.00001 / MGD Aug 2020 Week 4 0.000088 / MGD Sep 2020 Week 4 0.000037 / MGD Oct 2020 Week 4 0.000006 / MGD Nov 2020 Week 4 0.000011 / MGD Dec 2020 Week 4 0.000093 / MGD Jul 2020 Average 0.00001 / 0.01 MGD Aug 2020 Average 0.000088 / 0.01 MGD Sep 2020 Average 0.000037 / 0.01 MGD Oct 2020 Average 0.000006 / 0.01 MGD Nov 2020 Average 0.000011 / 0.01 MGD Dec 2020 Average 0.000093 / 0.01 MGD 2020 Quarter 3 0.000045 / MGD 2020 Quarter 4 0.000037 / MGD 2020 2nd 6 Months (Avg) 0.000041 / MGD 2020 2nd 6 ...(Max) 0.000093 / MGD 2020 2nd 6 ...(Min) 0.000006 / MGD 2020 2nd 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:33:47PM * Indicates Violation ** Indicates TRC Violation Page 1 of 1 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 07/14/2020 S Micross071420Se1f 08/27/2020 P Micross082720POTW Ju12020 Week 2 Aug 2020 Week 4 Jul 2020 Average Aug 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.035 / mg/L 0.017 / mg/L 0.035 / mg/L 0.017 / mg/L 0.035 / mg/L 0.017 / mg/L 0.026 / mg/L 0.026 / mg/L 0.035 / mg/L 0.017 / mg/L 2 / 0.012872 / lbs/day 0.011767 / lbs/day 0.012872 / lbs/day 0.011767 / lbs/day 0.012872 / lbs/day 0.011767 / lbs/day 0.01232 / lbs/day 0.012320 / lbs/day 0.012872 / lbs/day 0.011767 / lbs/day 2 / Sample Date SamplelD Result / Limit Mass/Limit Ammonia 07/14/2020 S Micross071420Se1f 2.3 / mg/L 0.8459 / lbs/day 08/27/2020 P Micross082720POTW 2.4 / mg/L 1.6613 / lbs/day Ju12020 Week 2 2.3 / mg/L 0.8459 / lbs/day Aug 2020 Week 4 2.4 / mg/L 1.6613 / lbs/day Jul 2020 Average 2.3 / mg/L 0.8459 / lbs/day Aug 2020 Average 2.4 / mg/L 1.6613 / lbs/day 2020 Quarter 3 2.35 / mg/L 1.2536 / lbs/day 2020 2nd 6 Months (Avg) 2.35 / mg/L 1.2536 / lbs/day 2020 2nd 6 ...(Max) 2.4 / mg/L 1.6613 / lbs/day 2020 2nd 6 ...(Min) 2.3 / mg/L 0.8459 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Average Flow for Month 07/14/2020 S Micross071420Se1fHg 0.000016 / 0.100 MGD / 07/31/2020 S Micross0720F1ow 0.04263 / 0.100 MGD / 08/14/2020 S Micross081420Se1fHg 0.000004 / 0.100 MGD / 08/31/2020 S Micross0820F1ow 0.049871 / 0.100 MGD / 09/30/2020 S Micross0920F1ow 0.042707 / 0.100 MGD / 10/31/2020 S Micross1020F1ow 0.036106 / 0.100 MGD / 11/30/2020 S Micross1120Flow 0.028333 / 0.100 MGD / 12/31/2020 S Micross1220F1ow 0.021172 / 0.100 MGD / Jul 2020 Week 2 0.000016 / MGD / Jul 2020 Week 4 0.04263 / MGD / Aug 2020 Week 2 0.000004 / MGD / Aug 2020 Week 4 0.049871 / MGD / Sep 2020 Week 4 0.042707 / MGD / Oct 2020 Week 4 0.036106 / MGD / Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 1 of 7 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Nov 2020 Week 4 0.028333 / MGD Dec 2020 Week 4 0.021172 / MGD Jul 2020 Average 0.021323 / 0.075 MGD Aug 2020 Average 0.024938 / 0.075 MGD Sep 2020 Average 0.042707 / 0.075 MGD Oct 2020 Average 0.036106 / 0.075 MGD Nov 2020 Average 0.028333 / 0.075 MGD Dec 2020 Average 0.021172 / 0.075 MGD 2020 Quarter 3 0.027046 / MGD 2020 Quarter 4 0.028537 / MGD 2020 2nd 6 Months (Avg) 0.027605 / MGD 2020 2nd 6 ...(Max) 0.049871 / MGD 2020 2nd 6 ...(Min) 0.000004 / MGD 2020 2nd 6 ...(Count) 8 / Sample Count : r 8 Months Sampled : 6 Weeks Sampled : 8 Quarters Sampled : 2 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Chloride 07/14/2020 S Micross071420Se1f 18 / mg/L 6.62 / lbs/day 08/27/2020 P Micross082720POTW 22.5 / mg/L 15.5744 / lbs/day Ju12020 Week 2 18 / mg/L 6.62 / lbs/day Aug 2020 Week 4 22.5 / mg/L 15.5744 / lbs/day Ju12020 Average 18 / mg/L 6.62 / lbs/day Aug 2020 Average 22.5 / mg/L 15.5744 / lbs/day 2020 Quarter 3 20.25 / mg/L 11.0972 / lbs/day 2020 2nd 6 Months (Avg) 20.25 / mg/L 11.0972 / lbs/day 2020 2nd 6 ...(Max) 22.5 / mg/L 15.5744 / lbs/day 2020 2nd 6 ...(Min) 18 / mg/L 6.6200 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Chromium 07/14/2020 S Micross071420Se1f 0.001 / mg/L 0.000463 / lbs/day 08/27/2020 P Micross082720POTW < 0.001 / mg/L < 0.000692 / lbs/day Jul 2020 Week 2 0.001 / mg/L 0.000463 / lbs/day Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 2 of 7 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Chromium Aug 2020 Week 4 < 0.001 / mg/L < 0.000692 / lbs/day Jul 2020 Average 0.001 / mg/L 0.000463 / lbs/day Aug 2020 Average < 0.001 / mg/L < 0.000692 / lbs/day 2020 Quarter 3 < 0.001 / mg/L < 0.000578 / lbs/day 2020 2nd 6 Months (Avg) < 0.001 / mg/L < 0.000578 / lbs/day 2020 2nd 6 ...(Max) 0.001 / mg/L 0.000692 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < 0.000463 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Copper 07/14/2020 S Micross071420Se1f 0.049 / mg/L 0.018021 / lbs/day 08/27/2020 P Micross082720POTW 0.017 / mg/L 0.01149 / lbs/day Ju12020 Week 2 0.049 / mg/L 0.018021 / lbs/day Aug 2020 Week 4 0.017 / mg/L 0.01149 / lbs/day Jul 2020 Average 0.049 / mg/L 0.018021 / lbs/day Aug 2020 Average 0.017 / mg/L 0.01149 / lbs/day 2020 Quarter 3 0.033 / mg/L 0.014756 / lbs/day 2020 2nd 6 Months (Avg) 0.033 / mg/L 0.014756 / lbs/day 2020 2nd 6 ...(Max) 0.049 / mg/L 0.018021 / lbs/day 2020 2nd 6 ...(Min) 0.017 / mg/L 0.011490 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Fluoride 07/14/2020 S Micross071420Se1f 08/27/2020 P Micross082720POTW Ju12020 Week 2 Aug 2020 Week 4 Jul 2020 Average Aug 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.67 / mg/L 0.2464 / lbs/day 1.7 / mg/L 1.1767 / lbs/day 0.67 / mg/L 0.2464 / lbs/day 1.7 / mg/L 1.1767 / lbs/day 0.67 / mg/L 0.2464 / lbs/day 1.7 / mg/L 1.1767 / lbs/day 1.19 / mg/L 0.7116 / lbs/day 1.19 / mg/L 0.7116 / lbs/day 1.7 / mg/L 1.1767 / lbs/day 0.67 / mg/L 0.2464 / lbs/day 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Mercury - LL 09/11/2020 S Micross091120SelfHg 0.000008 / 0.000142 mg/L 11/11/2020 P Micross111120POTW 0.000008 / 0.000142 mg/L Hg Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 3 of 7 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 11/11/2020 S 12/23/2020 S Sep 2020 Nov 2020 Dec 2020 Sep 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 2020 Micross111120SelfHg Micross122320Se1fHg Week 2 Week 2 Week 4 Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 r4 0.00 # Over Mo Avg C : 0.00 # Over Mo Avg C TRC : 0.00 # Over Mo Avg M : 0.00 # Over Mo Avg M TRC : 0.00 0.00 0.000008 / 0.000142 0.000004 / 0.000142 0.000008 0.000008 0.000004 0.000008 0.000008 0.000004 0.000008 0.000007 0.000007 0.000008 0.000004 4 / Months Sampled : 0 0 0 0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 3 Weeks Sampled : 3 # 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Nickel 07/14/2020 08/27/2020 Jul 2020 Aug 2020 Jul 2020 Aug 2020 2020 2020 2020 2020 2020 S Micross071420Se1f P Micross082720POTW Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.0157 / 0.002 / 0.0157 / 0.002 / 0.0157 / 0.002 / 0.0089 / 0.0089 / 0.0157 / 0.002 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.005774 / 0.001384 / 0.005774 / 0.001384 / 0.005774 / 0.001384 / 0.003579 / 0.003579 / 0.005774 / 0.001384 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 07/14/2020 08/27/2020 Jul 2020 S Micross071420Se1f P Micross082720POTW Week 2 1.5 / 0.9 / 1.5 / mg/L mg/L mg/L 0.552 / 0.637 / 0.552 / lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 4 of 7 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite Aug 2020 Week 4 Jul 2020 Average Aug 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.9 / 1.5 / 0.9 / 1.2 / 1.2 / 1.5 / 0.9 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.637 / 0.552 / 0.637 / 0.594 / 0.594 / 0.637 / 0.552 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample .Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 08/27/2020 Aug 2020 Aug 2020 2020 2020 2020 2020 2020 P Micross082720POTW Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 8.8 / 8.8 / 8.8 / 8.8 / 8.8 / 8.8 / 8.8 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L 6.091 / 6.091 / 6.091 / 6.091 / 6.091 / 6.091 / 6.091 / 1 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 08/27/2020 Aug 2020 Aug 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: P Micross082720POTW Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 2.5 / 200 2.5 / 2.5 / 2.5 / 2.5 / 2.5 / 2.5 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 Months Sampled : 1 Weeks Sampled : 0/0 # % # 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 0.00 1 0.00 0.00 0.00 0.00 # Over QtAvg C: # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit pH Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 5 of 7 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Date SamplelD Result /Limit Mass /Limit pH 07/14/2020 08/14/2020 08/27/2020 Jul 2020 Aug 2020 Aug 2020 Jul 2020 Aug 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: S Micross071420Se1f S Micross081420Se1fHg P Micross082720POTW Week 2 Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 ' 3 0/0 0.00 # Over Mo Avg C : 0.00 # Over Mo Avg C TRC : 0.00 # Over Mo Avg M : 0.00 # Over Mo Avg M TRC 0.00 0.00 8.3 7.2 7.4 8.3 7.2 7.4 8.3 7.3 7.63 7.63 8.3 7.2 3 / 5.5 - 10.5 / 5.5 - 10.5 / 5.5 - 10.5 Months Sampled : 2 0 0 0 0 SU SU SU SU SU SU SU SU SU SU SU SU 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 3 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Temperature 07/14/2020 08/14/2020 08/27/2020 Jul 2020 Aug 2020 Aug 2020 Jul 2020 Aug 2020 2020 2020 2020 2020 2020 S Micross071420Se1f S Micross081420SelfHg P Micross082720POTW Week 2 Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 22.9 23.9 25 22.9 23.9 25 22.9 24.5 23.9 23.9 25 22.9 3 / 66 / 66 / 66 °C °C °C °C °C °C °C °C °C °C °C °C Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 6 of 7 Micross Advanced Interconnect Technology, LLC SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: '001 Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Quarters Sampled : 1 Sample Date SamplelD Result/Limit Mass/Limit Tin 07/14/2020 S Micross071420Se1f 0.003050000 / mg/L 0.001121721 / lbs/day Jul 2020 Week 2 0 / mg/L 0 / lbs/day Jul 2020 Average 0 / mg/L 0 / lbs/day 2020 Quarter 3 0 / mg/L 0 / lbs/day 2020 2nd 6 Months (Avg) 0 / mg/L 0 / lbs/day 2020 2nd 6 ...(Max) 0 / mg/L 0 / lbs/day 2020 2nd 6 ...(Min) 0 / mg/L 0 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Sample Date SamplelD Result/Limit Mass/Limit TKN 07/14/2020 S Micross071420Se1f 08/27/2020 P Micross082720POTW Jul 2020 Week 2 Aug 2020 Week 4 Jul 2020 Average Aug 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 6.3 / mg/L 2.317 / lbs/day 7.88 / mg/L 5.454 / lbs/day 6.3 / mg/L 2.317 / lbs/day 7.88 / mg/L 5.454 / lbs/day 6.3 / mg/L 2.317 / lbs/day 7.88 / mg/L 5.454 / lbs/day 7.09 / mg/L 3.886 / lbs/day 7.09 / mg/L 3.886 / lbs/day 7.88 / mg/L 5.454 / lbs/day 6.3 / mg/L 2.317 / lbs/day 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Zinc 07/14/2020 S Micross071420Se1f 0.43 / mg/L 0.158144 / lbs/day Ju12020 Week 2 0.43 / mg/L 0.158144 / lbs/day Ju12020 Average 0.43 / mg/L 0.158144 / lbs/day 2020 Quarter 3 0.43 / mg/L 0.158144 / lbs/day 2020 2nd 6 Months (Avg) 0.43 / mg/L 0.158144 / lbs/day 2020 2nd 6 ...(Max) 0.43 / mg/L 0.158144 / lbs/day 2020 2nd 6 ...(Min) 0.43 / mg/L 0.158144 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Wednesday, February 24, 2021 10:32:OOPM * Indicates Violation ** Indicates TRC Violation Page 7 of 7 Novan, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 07/31/2020 S Novan0720F1ow 0.000141 / MGD 08/31/2020 S Novan0820F1ow 0.000117 / MGD 09/30/2020 S Novan0920F1ow 0.000126 / MGD 10/31/2020 S Novan1020F1ow 0.000137 / MGD 11/30/2020 S Novan1120Flow 0.000136 / MGD 12/31/2020 S Novan1220F1ow 0.0001 / MGD Jul 2020 Week 4 0.000141 / MGD Aug 2020 Week 4 0.000117 / MGD Sep 2020 Week 4 0.000126 / MGD Oct 2020 Week 4 0.000137 / MGD Nov 2020 Week 4 0.000136 / MGD Dec 2020 Week 4 0.0001 / MGD Ju12020 Average 0.000141 / MGD Aug 2020 Average 0.000117 / MGD Sep 2020 Average 0.000126 / MGD Oct 2020 Average 0.000137 / MGD Nov 2020 Average 0.000136 / MGD Dec 2020 Average 0.0001 / MGD 2020 Quarter 3 0.000128 / MGD 2020 Quarter 4 0.000124 / MGD 2020 2nd 6 Months (Avg) 0.000126 / MGD 2020 2nd 6 ...(Max) 0.000141 / MGD 2020 2nd 6 ...(Min) 0.0001 / MGD 2020 2nd 6 ...(Count) 6 / Sample Date SamplelD Result/Limit Mass/Limit COD 11/30/2020 P Novan113020POTW 991 / mg/L / Nov 2020 Week 4 991 / mg/L / Nov 2020 Average 991 / mg/L / 2020 Quarter 4 991 / mg/L / 2020 2nd 6 Months (Avg) 991 / mg/L / 2020 2nd 6 ...(Max) 991 / mg/L / 2020 2nd 6 ...(Min) 991 / mg/L / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Copper 11/30/2020 P Novan113020POTW 0.098 / mg/L / Nov 2020 Week 4 0.098 / mg/L / Nov 2020 Average 0.098 / mg/L / 2020 Quarter 4 0.098 / mg/L / Wednesday, February 24, 2021 10:29:44PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3 Novan, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Copper 2020 2nd 6 Months (Avg) 0.098 / mg/L 2020 2nd 6 ...(Max) 0.098 / mg/L 2020 2nd 6 ...(Min) 0.098 / mg/L 2020 2nd 6 ...(Count) 1 / Sample Date SamplelD Result / Limit Mass / Limit Mercury - LL 11/30/2020 P Novan113020POTWH 0.000033 / 0.000142 mg/L g Nov 2020 Week 4 0.000033 / mg/L Nov 2020 Average 0.000033 / mg/L 2020 Quarter 4 0.000033 / mg/L 2020 2nd 6 Months (Avg) 0.000033 / mg/L 2020 2nd 6 ...(Max) 0.000033 / mg/L 2020 2nd 6 ...(Min) 0.000033 / mg/L 2020 2nd 6 ...(Count) 1 / Sample Count : 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit pH 11/30/2020 P Novan113020POTW 6.5 / 6.0 - 10.0 SU / Nov 2020 Week 4 6.5 / SU / Nov 2020 Average 6.5 / SU / 2020 Quarter 4 6.5 / SU / 2020 2nd 6 Months (Avg) 6.5 / SU / 2020 2nd 6 ...(Max) 6.5 / SU / 2020 2nd 6 ...(Min) 6.5 / SU / 2020 2nd 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:29:44PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3 Novan, Inc. # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 0 0 0 0 0 0 1 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : Months Sampled : 0 0 0 0 1 Weeks Sampled : 1 # 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Temperature 11/30/2020 P Nov 2020 Nov 2020 2020 2020 2020 2020 2020 Novan113020POTW Week 4 Average Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 r1 0.00 # Over Mo Avg C : 0.00 # Over Mo Avg C TRC : 0.00 # Over Mo Avg M : 0.00 # Over Mo Avg M TRC : 0.00 0.00 20 / 66 20 / 20 / 20 / 20 / 20 / 20 / 1 / Months Sampled : 0 0 0 0 °C °C °C °C °C °C °C 1 0/0 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 1 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 11/30/2020 Nov 2020 Nov 2020 2020 2020 2020 2020 2020 P Novan113020POTW Week 4 Average Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 16.4 / 16.4 / 16.4 / 16.4 / 16.4 / 16.4 / 16.4 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:29:44PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3 Phononic SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month 07/31/2020 S Phononic0720F1ow 0.006297 / MGD 08/31/2020 S Phononic0820F1ow 0.006865 / MGD 09/30/2020 S Phononic0920F1ow 0.006251 / MGD 10/31/2020 S Phononic1020F1ow 0.006806 / MGD 11/30/2020 S Phononic1120Flow 0.007381 / MGD 12/31/2020 S Phononic1220F1ow 0.008029 / MGD Jul 2020 Week 4 0.006297 / MGD Aug 2020 Week 4 0.006865 / MGD Sep 2020 Week 4 0.006251 / MGD Oct 2020 Week 4 0.006806 / MGD Nov 2020 Week 4 0.007381 / MGD Dec 2020 Week 4 0.008029 / MGD Jul 2020 Average 0.006297 / 0.020 MGD Aug 2020 Average 0.006865 / 0.020 MGD Sep 2020 Average 0.006251 / 0.020 MGD Oct 2020 Average 0.006806 / 0.020 MGD Nov 2020 Average 0.007381 / 0.020 MGD Dec 2020 Average 0.008029 / 0.020 MGD 2020 Quarter 3 0.006471 / MGD 2020 Quarter 4 0.007405 / MGD 2020 2nd 6 Months (Avg) 0.006938 / MGD 2020 2nd 6 ...(Max) 0.008029 / MGD 2020 2nd 6 ...(Min) 0.006251 / MGD 2020 2nd 6 ...(Count) 6 / Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Bismuth 07/16/2020 P Phononic071620POT W 07/22/2020 S Phononic072220Se1f 08/07/2020 S Phononic080720Se1f 09/21/2020 S Phononic092120Se1f 10/20/2020 S Phononic102020Se1f 11/19/2020 S Phononic111920Self 0.324 / mg/L 0.079 / mg/L 0.049 / mg/L 0.102 / mg/L 0.015 / mg/L 0.165 / mg/L Wednesday, February 24, 2021 10:27:27PM * Indicates Violation ** Indicates TRC Violation Page 1 of 5 Phononic SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Bismuth 12/18/2020 S Phononic121820Se1f 0.21 / mg/L Jul 2020 Week 3 0.324 / mg/L Jul 2020 Week 4 0.079 / mg/L Aug 2020 Week 1 0.049 / mg/L Sep 2020 Week 3 0.102 / mg/L Oct 2020 Week 3 0.015 / mg/L Nov 2020 Week 3 0.165 / mg/L Dec 2020 Week 3 0.21 / mg/L Jul 2020 Average 0.202 / mg/L Aug 2020 Average 0.049 / mg/L Sep 2020 Average 0.102 / mg/L Oct 2020 Average 0.015 / mg/L Nov 2020 Average 0.165 / mg/L Dec 2020 Average 0.21 / mg/L 2020 Quarter 3 0.139 / mg/L 2020 Quarter 4 0.13 / mg/L 2020 2nd 6 Months (Avg) 0.135 / mg/L 2020 2nd 6 ...(Max) 0.324 / mg/L 2020 2nd 6 ...(Min) 0.015 / mg/L 2020 2nd 6 ...(Count) 7 / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 07/16/2020 P Phononic071620POT 0.000002 / 0.000142 mg/L / W 08/17/2020 S Phononic081720Se1fH 0.000002 / 0.000142 mg/L / g Jul 2020 Week 3 0.000002 / mg/L / Aug 2020 Week 3 0.000002 / mg/L / Jul 2020 Average 0.000002 / mg/L / Aug 2020 Average 0.000002 / mg/L / 2020 Quarter 3 0.000002 / mg/L / 2020 2nd 6 Months (Avg) 0.000002 / mg/L / 2020 2nd 6 ...(Max) 0.000002 / mg/L / 2020 2nd 6 ...(Min) 0.000002 / mg/L / 2020 2nd 6 ...(Count) 2 / / Wednesday, February 24, 2021 10:27:27PM * Indicates Violation ** Indicates TRC Violation Page 2 of 5 Phononic SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Molybdenum 07/16/2020 P Phononic071620POT < 0.001 / mg/L < / W 08/07/2020 S Phononic080720Se1f < 0.003 / mg/L < 0.0002 / lbs/day Jul 2020 Week 3 < 0.001 / mg/L < / Aug 2020 Week 1 < 0.003 / mg/L < 0.0002 / lbs/day Jul 2020 Average < 0.001 / mg/L < / Aug 2020 Average < 0.003 / mg/L < 0.0002 / lbs/day 2020 Quarter 3 < 0.002 / mg/L < 0.0002 / lbs/day 2020 2nd 6 Months (Avg) < 0.002 / mg/L < 0.0002 / lbs/day 2020 2nd 6 ...(Max) < 0.003 / mg/L < 0.0002 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Nickel 07/16/2020 P Phononic071620POT 0.097 / mg/L / 0.02 W 07/22/2020 S Phononic072220Se1f 0.112 / mg/L 0.00905 / 0.02 lbs/day 08/07/2020 S Phononic080720Se1f 0.126 / mg/L 0.01183 / 0.02 lbs/day 09/21/2020 S Phononic092120Se1f 0.062 / mg/L 0.005659 / 0.02 lbs/day 10/20/2020 S Phononic102020Se1f 0.094 / mg/L 0.01049 / 0.02 lbs/day 11/19/2020 S Phononic111920Self 0.155 / mg/L 0.009256 / 0.02 lbs/day 12/18/2020 S Phononic121820Se1f 0.175 / mg/L 0.010006 / 0.02 lbs/day Jul 2020 Week 3 0.097 / mg/L / Ju12020 Week 4 0.112 / mg/L 0.00905 / lbs/day Aug 2020 Week 1 0.126 / mg/L 0.01183 / lbs/day Sep 2020 Week 3 0.062 / mg/L 0.005659 / lbs/day Oct 2020 Week 3 0.094 / mg/L 0.01049 / lbs/day Nov 2020 Week 3 0.155 / mg/L 0.009256 / lbs/day Dec 2020 Week 3 0.175 / mg/L 0.010006 / lbs/day Ju12020 Average 0.1045 / mg/L 0.00905 / lbs/day Aug 2020 Average 0.126 / mg/L 0.01183 / lbs/day Sep 2020 Average 0.062 / mg/L 0.005659 / lbs/day Oct 2020 Average 0.094 / mg/L 0.01049 / lbs/day Nov 2020 Average 0.155 / mg/L 0.009256 / lbs/day Wednesday, February 24, 2021 10:27:27PM * Indicates Violation ** Indicates TRC Violation Page 3 of 5 Phononic SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nickel Dec 2020 Average 0.175 / mg/L 2020 Quarter 3 0.0993 / mg/L 2020 Quarter 4 0.1413 / mg/L 2020 2nd 6 Months (Avg) 0.1173 / mg/L 2020 2nd 6 ...(Max) 0.175 / mg/L 2020 2nd 6 ...(Min) 0.062 / mg/L 2020 2nd 6 ...(Count) 7 / 0.010006 / lbs/day 0.008847 / lbs/day 0.009917 / lbs/day 0.009382 / lbs/day 0.011830 / lbs/day 6 / Sample Count : I 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit pH 07/16/2020 P Phononic071620POT 6.9 / 5.5 - 10 SU W 08/17/2020 S Phononic081720Se1fH 6.5 / 5.5 - 10 SU g Jul 2020 Week 3 6.9 / SU Aug 2020 Week 3 6.5 / SU Jul 2020 Average 6.9 / SU Aug 2020 Average 6.5 / SU 2020 Quarter 3 6.7 / SU 2020 2nd 6 Months (Avg) 6.7 / SU 2020 2nd 6 ...(Max) 6.9 / SU 2020 2nd 6 ...(Min) 6.5 / SU 2020 2nd 6 ...(Count) 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Tellurium Wednesday, February 24, 2021 10:27:27PM * Indicates Violation ** Indicates TRC Violation Page 4 of 5 Phononic SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Tellurium 07/16/2020 P Phononic071620POT 0.372 / mg/L W 07/22/2020 S Phononic072220Se1f 0.316 / mg/L 08/07/2020 S Phononic080720Se1f 0.697 / mg/L 09/21/2020 S Phononic092120Se1f 0.158 / mg/L 10/20/2020 S Phononic102020Se1f 0.311 / mg/L 11/19/2020 S Phononic111920Self 0.578 / mg/L 12/18/2020 S Phononic121820Self 0.686 / mg/L Ju12020 Week 3 0.372 / mg/L Ju12020 Week 4 0.316 / mg/L Aug 2020 Week 1 0.697 / mg/L Sep 2020 Week 3 0.158 / mg/L Oct 2020 Week 3 0.311 / mg/L Nov 2020 Week 3 0.578 / mg/L Dec 2020 Week 3 0.686 / mg/L Jul 2020 Average 0.344 / mg/L Aug 2020 Average 0.697 / mg/L Sep 2020 Average 0.158 / mg/L Oct 2020 Average 0.311 / mg/L Nov 2020 Average 0.578 / mg/L Dec 2020 Average 0.686 / mg/L 2020 Quarter 3 0.386 / mg/L 2020 Quarter 4 0.525 / mg/L 2020 2nd 6 Months (Avg) 0.445 / mg/L 2020 2nd 6 ...(Max) 0.697 / mg/L 2020 2nd 6 ...(Min) 0.158 / mg/L 2020 2nd 6 ...(Count) 7 / Sample Date SamplelD Result/Limit Mass/Limit Temperature 07/16/2020 P Phononic071620POT 24 / °C / W Ju12020 Week 3 24 / °C / Jul 2020 Average 24 / °C / 2020 Quarter 3 24 / °C / 2020 2nd 6 Months (Avg) 24 / °C / 2020 2nd 6 ...(Max) 24 / °C / 2020 2nd 6 ...(Min) 24 / °C / 2020 2nd 6 ...(Count) 1 / / Wednesday, February 24, 2021 10:27:27PM * Indicates Violation ** Indicates TRC Violation Page 5 of 5 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Aluminum 07/29/2020 P PowerSecure072920P 11.5 / mg/L OTW 11/11/2020 S PowerSecure111120Sel 4.6 / mg/L f 11/18/2020 S PowerSecure1118220S 5.93 / mg/L elf Ju12020 Week 4 11.5 / mg/L Nov 2020 Week 2 4.6 / mg/L Nov 2020 Week 3 5.93 / mg/L Jul 2020 Average 11.5 / mg/L Nov 2020 Average 5.265 / mg/L 2020 Quarter 3 11.5 / mg/L 2020 Quarter 4 5.265 / mg/L 2020 2nd 6 Months (Avg) 7.343 / mg/L 2020 2nd 6 ...(Max) 11.5 / mg/L 2020 2nd 6 ...(Min) 4.6 / mg/L 2020 2nd 6 ...(Count) 3 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/31/2020 S PowerSecure0720Flow 0.000656 / MGD / 08/31/2020 S PowerSecure0830Flow 0.000811 / MGD / 09/30/2020 S PowerSecure0920Flow 0.005148 / MGD / 10/31/2020 S PowerSecure1020Flow 0.0007 / MGD / 11/30/2020 S PowerSecure1120Flow 0.001483 / MGD / Jul 2020 Week 4 0.000656 / MGD / Aug 2020 Week 4 0.000811 / MGD / Sep 2020 Week 4 0.005148 / MGD / Oct 2020 Week 4 0.0007 / MGD / Nov 2020 Week 4 0.001483 / MGD / Jul 2020 Average 0.000656 / 0.006 MGD / Aug 2020 Average 0.000811 / 0.006 MGD / Sep 2020 Average 0.005148 / 0.006 MGD / Oct 2020 Average 0.0007 / 0.006 MGD / Nov 2020 Average 0.001483 / 0.006 MGD / 2020 Quarter 3 0.002205 / MGD / 2020 Quarter 4 0.001092 / MGD / 2020 2nd 6 Months (Avg) 0.001760 / MGD / 2020 2nd 6 ...(Max) 0.005148 / MGD / 2020 2nd 6 ...(Min) 0.000656 / MGD / 2020 2nd 6 ...(Count) 5 / / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 5 Months Sampled : 5 Weeks Sampled : 5 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cadmium 07/29/2020 P PowerSecure072920P < 0.00008 / 0.11 mg/L < / OTW 11/11/2020 S PowerSecure111120Sel 0.006 / 0.11 mg/L / f 11/18/2020 S PowerSecure1118220S 0.0012 / 0.11 mg/L / elf Jul 2020 Week 4 < 0.00008 / mg/L < / Nov 2020 Week 2 0.006 / mg/L / Nov 2020 Week 3 0.0012 / mg/L / Jul 2020 Average < 0.00008 / 0.07 mg/L < / Nov 2020 Average 0.0036 / 0.07 mg/L / 2020 Quarter 3 < 0.00008 / mg/L < / 2020 Quarter 4 0.0036 / mg/L / 2020 2nd 6 Months (Avg) < 0.00243 / mg/L < / 2020 2nd 6 ...(Max) 0.006 / mg/L / 2020 2nd 6 ...(Min) < 0.00008 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Chromium 07/29/2020 P PowerSecure072920P < 0.001 / 2.77 mg/L < / OTW 11/11/2020 S PowerSecure111120Sel < 0.003 / 2.77 mg/L < / f 11/18/2020 S PowerSecure1118220S < 0.003 / 2.77 mg/L < / elf Jul 2020 Week 4 < 0.001 / mg/L < / Nov 2020 Week 2 < 0.003 / mg/L < / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chromium Nov 2020 Week 3 < 0.003 / mg/L < / Ju12020 Average < 0.001 / 1.71 mg/L < / Nov 2020 Average < 0.003 / 1.71 mg/L < / 2020 Quarter 3 < 0.001 / mg/L < / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.002 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Copper 07/29/2020 P PowerSecure072920P 0.22 / 3.38 mg/L / OTW 11/11/2020 S PowerSecure111120Sel 0.754 / 3.38 mg/L / f 11/18/2020 S PowerSecure1118220S 0.382 / 3.38 mg/L / elf Jul 2020 Week 4 0.22 / mg/L / Nov 2020 Week 2 0.754 / mg/L / Nov 2020 Week 3 0.382 / mg/L / Jul 2020 Average 0.22 / 2.07 mg/L / Nov 2020 Average 0.568 / 2.07 mg/L / 2020 Quarter 3 0.22 / mg/L / 2020 Quarter 4 0.568 / mg/L / 2020 2nd 6 Months (Avg) 0.452 / mg/L / 2020 2nd 6 ...(Max) 0.754 / mg/L / 2020 2nd 6 ...(Min) 0.22 / mg/L / 2020 2nd 6 ...(Count) 3 / / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 3 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cyanide 07/29/2020 P PowerSecure072920P < 0.003 / 0.60 mg/L < / OTW 11/11/2020 S PowerSecure111120Sel < 0.003 / 0.60 mg/L < / f 11/18/2020 S PowerSecure1118220S < 0.003 / 0.60 mg/L < / elf Jul 2020 Week 4 < 0.003 / mg/L < / Nov 2020 Week 2 < 0.003 / mg/L < / Nov 2020 Week 3 < 0.003 / mg/L < / Jul 2020 Average < 0.003 / 0.50 mg/L < / Nov 2020 Average < 0.003 / 0.50 mg/L < / 2020 Quarter 3 < 0.003 / mg/L < / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) < 0.003 / mg/L < / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Lead 07/29/2020 P PowerSecure072920P < 0.0003 / 0.69 mg/L OTW 11/11/2020 S PowerSecure111120Sel 0.0056 / 0.69 mg/L f 11/18/2020 S PowerSecure1118220S < 0.0025 / 0.69 mg/L elf Jul 2020 Week 4 < 0.0003 / mg/L Nov 2020 Week 2 0.0056 / mg/L Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Lead Nov 2020 Week 3 < 0.0025 / mg/L < / Jul 2020 Average < 0.0003 / 0.43 mg/L < / Nov 2020 Average < 0.0041 / 0.43 mg/L < / 2020 Quarter 3 < 0.0003 / mg/L < / 2020 Quarter 4 < 0.0041 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0028 / mg/L < / 2020 2nd 6 ...(Max) 0.0056 / mg/L / 2020 2nd 6 ...(Min) < 0.0003 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Mercury 11/11/2020 S PowerSecure111120Sel < 0 / 0.000142 mg/L < / f 11/18/2020 S PowerSecure1118220S < 0 / 0.000142 mg/L < / elf Nov 2020 Week 2 < 0 / mg/L < / Nov 2020 Week 3 < 0 / mg/L < / Nov 2020 Average < 0 / mg/L < / 2020 Quarter 4 < 0 / mg/L < / 2020 2nd 6 Months (Avg) < 0.00000 / mg/L < / 2020 2nd 6 ...(Max) < 0.00000 / mg/L < / 2020 2nd 6 ...(Min) < 0.00000 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 11/19/2020 P PowerSecure111920P < 0.000001 / mg/L < / OTWHg Nov 2020 Week 3 < 0.000001 / mg/L < / Nov 2020 Average < 0.000001 / mg/L < / 2020 Quarter 4 < 0.000001 / mg/L < / 2020 2nd 6 Months (Avg) < 0.000001 / mg/L < / 2020 2nd 6 ...(Max) < 0.000001 / mg/L < / 2020 2nd 6 ...(Min) < 0.000001 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 07/29/2020 P PowerSecure072920P 0.003 / mg/L / OTW 11/11/2020 S PowerSecure111120Sel < 0.003 / mg/L < / f 11/18/2020 S PowerSecure1118220S < 0.003 / mg/L < / elf Jul 2020 Week 4 0.003 / mg/L / Nov 2020 Week 2 < 0.003 / mg/L < / Nov 2020 Week 3 < 0.003 / mg/L < / Jul 2020 Average 0.003 / mg/L / Nov 2020 Average < 0.003 / mg/L < / 2020 Quarter 3 0.003 / mg/L / 2020 Quarter 4 < 0.003 / mg/L < / 2020 2nd 6 Months (Avg) < 0.003 / mg/L < / 2020 2nd 6 ...(Max) 0.003 / mg/L / 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Date SamplelD Result/Limit Mass /Limit Nickel 07/29/2020 P PowerSecure072920P 0.019 / 1.30 mg/L / OTW 11/11/2020 S PowerSecure111120Sel 0.0336 / 1.30 mg/L / f 11/18/2020 S PowerSecure1118220S 0.058 / 1.30 mg/L / elf Jul 2020 Week 4 0.019 / mg/L / Nov 2020 Week 2 0.0336 / mg/L / Nov 2020 Week 3 0.058 / mg/L / Ju12020 Average 0.019 / 1.00 mg/L / Nov 2020 Average 0.0458 / 1.00 mg/L / 2020 Quarter 3 0.019 / mg/L / 2020 Quarter 4 0.0458 / mg/L / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nickel 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 3 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.0369 / mg/L 0.058 / mg/L 0.019 / mg/L 3 / Months Sampled : 2 Weeks Sampled : 3 # % # 0 0.00 # Over Wk Avg C : 0 0.00 0 0.00 # Over Wk Avg C TRC : 0 0.00 0 0.00 # Over Wk Avg M : 0 0.00 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtAvg C: # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result/Limit Mass / Limit pH 07/29/2020 P PowerSecure072920P OTW 11/18/2020 S PowerSecure1118220S elf 12/11/2020 S PowerSecure121120Se if Jul 2020 Week 4 Nov 2020 Dec 2020 Jul 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 2020 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: Week 3 Week 2 Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 8.5 /6.0-10.0 SU 9 /6.0-10.0 SU 9.2 /6.0-10.0 SU 8.5 / SU 9 / SU 9.2 / SU 8.5 / SU 9 / SU 9.2 / SU 8.5 / SU 9.1 / SU 8.9 / SU 9.2 / SU 8.5 / SU 3 / 3 Months Sampled : 3 #0/0 0.00 # Over Mo Avg C : 0 0.00 0.00 # Over Mo Avg C TRC : 0 0.00 0.00 # Over Mo Avg M : 0 0.00 0.00 # Over Mo Avg M TRC : 0 0.00 0.00 0.00 # Over Wk Avg C : # Over Wk Avg C TRC : # Over Wk Avg M : # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 3 0/0 0.00 # Over Qt Avg C : 0.00 # Over Qt Avg C TRC : 0.00 # Over Qtr Avg M : 0.00 # Over Qtr Avg M TRC : Quarters Sampled : 0 0 0 0 2 0.00 0.00 0.00 0.00 Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Silver 07/29/2020 P PowerSecure072920P < 0.0003 / 0.43 mg/L < / OTW 11/11/2020 S PowerSecure111120Sel < 0.0025 / 0.43 mg/L < / f 11/18/2020 S PowerSecure1118220S < 0.0025 / 0.43 mg/L < / elf Jul 2020 Week 4 < 0.0003 / mg/L < / Nov 2020 Week 2 < 0.0025 / mg/L < / Nov 2020 Week 3 < 0.0025 / mg/L < / Jul 2020 Average < 0.0003 / 0.24 mg/L < / Nov 2020 Average < 0.0025 / 0.24 mg/L < / 2020 Quarter 3 < 0.0003 / mg/L < / 2020 Quarter 4 < 0.0025 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0018 / mg/L < / 2020 2nd 6 ...(Max) < 0.0025 / mg/L < / 2020 2nd 6 ...(Min) < 0.0003 / mg/L < / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Temperature 07/29/2020 P PowerSecure072920P 28 / 66 °C / OTW 11/18/2020 S PowerSecure1118220S 20.9 / 66 °C / elf 12/11/2020 S PowerSecure121120Se 22.1 / 66 °C / if Jul 2020 Week 4 28 / °C / Nov 2020 Week 3 20.9 / °C / Dec 2020 Week 2 22.1 / °C / Jul 2020 Average 28 / °C / Nov 2020 Average 20.9 / °C / Dec 2020 Average 22.1 / °C / 2020 Quarter3 28 / °C / 2020 Quarter 4 21.5 / °C / 2020 2nd 6 Months (Avg) 23.7 / °C / 2020 2nd 6 ...(Max) 28 / °C / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Temperature 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 20.9 / °C 3 / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 04 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit TTO 11/11/2020 S PowerSecure111120Sel < 0.0025 / 2.13 mg/L < / f 11/18/2020 S PowerSecure1118220S < 0.0025 / 2.13 mg/L < / elf Nov 2020 Week 2 < 0.0025 / mg/L < / Nov 2020 Week 3 < 0.0025 / mg/L < / Nov 2020 Average < 0.0025 / mg/L < / 2020 Quarter 4 < 0.0025 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0025 / mg/L < / 2020 2nd 6 ...(Max) < 0.0025 / mg/L < / 2020 2nd 6 ...(Min) < 0.0025 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass/Limit Zinc 07/29/2020 P PowerSecure072920P OTW 11/11/2020 S PowerSecure111120Sel f 11/18/2020 S PowerSecure 111 8220S elf Ju12020 Week 4 0.135 / 2.61 mg/L / 0.205 / 2.61 mg/L / 0.305 / 2.61 mg/L / 0.135 / mg/L / Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 PowerSecure SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc Nov 2020 Week 2 0.205 / mg/L Nov 2020 Week 3 0.305 / mg/L Ju12020 Average 0.135 / 1.48 mg/L Nov 2020 Average 0.255 / 1.48 mg/L 2020 Quarter 3 0.135 / mg/L 2020 Quarter 4 0.255 / mg/L 2020 2nd 6 Months (Avg) 0.215 / mg/L 2020 2nd 6 ...(Max) 0.305 / mg/L 2020 2nd 6 ...(Min) 0.135 / mg/L 2020 2nd 6 ...(Count) 3 / Sample Count : 3 Months Sampled : 2 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:22:48PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ammonia 08/14/2020 S SCM081420Se1f 09/24/2020 P SCM092420POTW Aug 2020 Week 2 Sep 2020 Week 4 Aug 2020 Average Sep 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 2.3 / mg/L 4.9 / mg/L 2.3 / mg/L 4.9 / mg/L 2.3 / mg/L 4.9 / mg/L 3.6 / mg/L 3.6 / mg/L 4.9 / mg/L 2.3 / mg/L 2 / 0.5917 / lbs/day 0.4496 / lbs/day 0.5917 / lbs/day 0.4496 / lbs/day 0.5917 / lbs/day 0.4496 / lbs/day 0.5207 / lbs/day 0.5207 / lbs/day 0.5917 / lbs/day 0.4496 / lbs/day 2 / Sample Date SamplelD Result / Limit Mass/Limit Average Flow for Month 07/31/2020 S SCM0720F1ow 0.009849 / 0.080 MGD / 08/31/2020 S SCM0820F1ow 0.010856 / 0.080 MGD / 09/30/2020 S SCM0920F1ow 0.011499 / 0.080 MGD / 10/31/2020 S SCM1020F1ow 0.011811 / 0.080 MGD / 11/30/2020 S SCM1120F1ow 0.009397 / 0.080 MGD / 12/31/2020 S SCM1220F1ow 0.005631 / 0.080 MGD / Jul 2020 Week 4 0.009849 / MGD / Aug 2020 Week 4 0.010856 / MGD / Sep 2020 Week 4 0.011499 / MGD / Oct 2020 Week 4 0.011811 / MGD / Nov 2020 Week 4 0.009397 / MGD / Dec 2020 Week 4 0.005631 / MGD / Jul 2020 Average 0.009849 / 0.050 MGD / Aug 2020 Average 0.010856 / 0.050 MGD / Sep 2020 Average 0.011499 / 0.050 MGD / Oct 2020 Average 0.011811 / 0.050 MGD / Nov 2020 Average 0.009397 / 0.050 MGD / Dec 2020 Average 0.005631 / 0.050 MGD / 2020 Quarter 3 0.010735 / MGD / 2020 Quarter 4 0.008946 / MGD / 2020 2nd 6 Months (Avg) 0.009841 / MGD / 2020 2nd 6 ...(Max) 0.011811 / MGD / 2020 2nd 6 ...(Min) 0.005631 / MGD / 2020 2nd 6 ...(Count) 6 / / Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cadmium 08/14/2020 S SCM081420Se1f < 0.0005 / mg/L < 0.000129 / lbs/day 09/24/2020 P SCM092420POTW < 0.00008 / mg/L < 0.000007 / lbs/day Aug 2020 Week 2 < 0.0005 / mg/L < 0.000129 / lbs/day Sep 2020 Week 4 < 0.00008 / mg/L < 0.000007 / lbs/day Aug 2020 Average < 0.0005 / mg/L < 0.000129 / lbs/day Sep 2020 Average < 0.00008 / mg/L < 0.000007 / lbs/day 2020 Quarter 3 < 0.00029 / mg/L < 0.000068 / lbs/day 2020 2nd 6 Months (Avg) < 0.00029 / mg/L < 0.000068 / lbs/day 2020 2nd 6 ...(Max) < 0.0005 / mg/L < 0.000129 / lbs/day 2020 2nd 6 ...(Min) < 0.00008 / mg/L < 0.000007 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result / Limit Mass/Limit Chloride 08/14/2020 S SCM081420Se1f 12 / mg/L 3.0872 / lbs/day 09/24/2020 P SCM092420POTW 17.5 / mg/L 1.6057 / lbs/day Aug 2020 Week 2 12 / mg/L 3.0872 / lbs/day Sep 2020 Week 4 17.5 / mg/L 1.6057 / lbs/day Aug 2020 Average 12 / mg/L 3.0872 / lbs/day Sep 2020 Average 17.5 / mg/L 1.6057 / lbs/day 2020 Quarter 3 14.75 / mg/L 2.3465 / lbs/day 2020 2nd 6 Months (Avg) 14.75 / mg/L 2.3465 / lbs/day 2020 2nd 6 ...(Max) 17.5 / mg/L 3.0872 / lbs/day 2020 2nd 6 ...(Min) 12 / mg/L 1.6057 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Copper 08/14/2020 S SCM081420Se1f 09/24/2020 P SCM092420POTW 11/06/2020 S SCM110620Se1f Aug 2020 Week 2 Sep 2020 Week 4 Nov 2020 Week 1 0.091 / 0.75 mg/L 0.023437 / lbs/day 0.116 / 0.75 mg/L 0.010644 / lbs/day 0.181 / 0.75 mg/L 0.04595 / lbs/day 0.091 / mg/L 0.023437 / lbs/day 0.116 / mg/L 0.010644 / lbs/day 0.181 / mg/L 0.04595 / lbs/day Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Copper Aug 2020 Average 0.091 / 0.50 mg/L 0.023437 / lbs/day Sep 2020 Average 0.116 / 0.50 mg/L 0.010644 / lbs/day Nov 2020 Average 0.181 / 0.50 mg/L 0.04595 / lbs/day 2020 Quarter 3 0.104 / mg/L 0.01704 / lbs/day 2020 Quarter 4 0.181 / mg/L 0.04595 / lbs/day 2020 2nd 6 Months (Avg) 0.129 / mg/L 0.026677 / lbs/day 2020 2nd 6 ...(Max) 0.181 / mg/L 0.045950 / lbs/day 2020 2nd 6 ...(Min) 0.091 / mg/L 0.010644 / lbs/day 2020 2nd 6 ...(Count) 3 / 3 / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Cyanide 08/14/2020 S SCM081420Se1f 0.012 / 0.04 mg/L 0.003087 / lbs/day 09/24/2020 P SCM092420POTW < 0.003 / 0.04 mg/L < 0.000229 / lbs/day Aug 2020 Week 2 0.012 / mg/L 0.003087 / lbs/day Sep 2020 Week 4 < 0.003 / mg/L < 0.000229 / lbs/day Aug 2020 Average 0.012 / 0.03 mg/L 0.003087 / lbs/day Sep 2020 Average < 0.003 / 0.03 mg/L < 0.000229 / lbs/day 2020 Quarter 3 < 0.007 / mg/L < 0.001658 / lbs/day 2020 2nd 6 Months (Avg) < 0.007 / mg/L < 0.001658 / lbs/day 2020 2nd 6 ...(Max) 0.012 / mg/L 0.003087 / lbs/day 2020 2nd 6 ...(Min) < 0.003 / mg/L < 0.000229 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 3 of I0 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Fluoride 08/14/2020 S SCM081420Se1f 0.12 / mg/L 0.0309 / lbs/day 09/24/2020 P SCM092420POTW < 0.05 / mg/L < 0.0046 / lbs/day Aug 2020 Week 2 0.12 / mg/L 0.0309 / lbs/day Sep 2020 Week 4 < 0.05 / mg/L < 0.0046 / lbs/day Aug 2020 Average 0.12 / mg/L 0.0309 / lbs/day Sep 2020 Average < 0.05 / mg/L < 0.0046 / lbs/day 2020 Quarter 3 < 0.09 / mg/L < 0.0177 / lbs/day 2020 2nd 6 Months (Avg) < 0.09 / mg/L < 0.0177 / lbs/day 2020 2nd 6 ...(Max) 0.12 / mg/L 0.0309 / lbs/day 2020 2nd 6 ...(Min) < 0.05 / mg/L < 0.0046 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass/Limit Lead 08/14/2020 S SCM081420Se1f < 0.0025 / 0.20 mg/L < 0.000643 / lbs/day 09/24/2020 P SCM092420POTW < 0.0003 / 0.20 mg/L < 0.000023 / lbs/day 11/06/2020 S SCM110620Se1f < 0.0025 / 0.20 mg/L < 0.000635 / lbs/day Aug 2020 Week 2 < 0.0025 / mg/L < 0.000643 / lbs/day Sep 2020 Week 4 < 0.0003 / mg/L < 0.000023 / lbs/day Nov 2020 Week 1 < 0.0025 / mg/L < 0.000635 / lbs/day Aug 2020 Average < 0.0025 / 0.10 mg/L < 0.000643 / lbs/day Sep 2020 Average < 0.0003 / 0.10 mg/L < 0.000023 / lbs/day Nov 2020 Average < 0.0025 / 0.10 mg/L < 0.000635 / lbs/day 2020 Quarter 3 < 0.0014 / mg/L < 0.000333 / lbs/day 2020 Quarter 4 < 0.0025 / mg/L < 0.000635 / lbs/day 2020 2nd 6 Months (Avg) < 0.0018 / mg/L < 0.000434 / lbs/day 2020 2nd 6 ...(Max) < 0.0025 / mg/L < 0.000643 / lbs/day 2020 2nd 6 ...(Min) < 0.0003 / mg/L < 0.000023 / lbs/day 2020 2nd 6 ...(Count) 3 / 3 / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass /Limit Mercury - LL 08/14/2020 S SCM081420Se1f < 0.000001 / 0.000142 mg/L < / 11/23/2020 P SCM112320POTWHg 0.000005 / 0.000142 mg/L / Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL Aug 2020 Week 2 < 0.000001 / mg/L < / Nov 2020 Week 4 0.000005 / mg/L / Aug 2020 Average < 0.000001 / mg/L < / Nov 2020 Average 0.000005 / mg/L / 2020 Quarter 3 < 0.000001 / mg/L < / 2020 Quarter 4 0.000005 / mg/L / 2020 2nd 6 Months (Avg) < 0.000003 / mg/L < / 2020 2nd 6 ...(Max) 0.000005 / mg/L / 2020 2nd 6 ...(Min) < 0.000001 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 08/14/2020 S SCM081420Se1f < 0.003 / mg/L < 0.0006 / lbs/day 09/24/2020 P SCM092420POTW < 0.001 / mg/L < 0.0001 / lbs/day Aug 2020 Week 2 < 0.003 / mg/L < 0.0006 / lbs/day Sep 2020 Week 4 < 0.001 / mg/L < 0.0001 / lbs/day Aug 2020 Average < 0.003 / mg/L < 0.0006 / lbs/day Sep 2020 Average < 0.001 / mg/L < 0.0001 / lbs/day 2020 Quarter 3 < 0.002 / mg/L < 0.0004 / lbs/day 2020 2nd 6 Months (Avg) < 0.002 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Max) < 0.003 / mg/L < 0.0006 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < 0.0001 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result/Limit Mass /Limit Nickel 08/14/2020 S SCM081420Se1f < 0.0025 / mg/L < 0.000643 / lbs/day 09/24/2020 P SCM092420POTW 0.001 / mg/L 0.000092 / lbs/day Aug 2020 Week 2 < 0.0025 / mg/L < 0.000643 / lbs/day Sep 2020 Week 4 0.001 / mg/L 0.000092 / lbs/day Aug 2020 Average < 0.0025 / mg/L < 0.000643 / lbs/day Sep 2020 Average 0.001 / mg/L 0.000092 / lbs/day 2020 Quarter 3 < 0.0018 / mg/L < 0.000367 / lbs/day Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nickel 2020 2020 2020 2020 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) • 0.0018 / • 0.0025 / 0.001 / 2 / mg/L mg/L mg/L • 0.000367 / • 0.000643 / 0.000092 / 2 / lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass / Limit Nitrate -Nitrite 08/14/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S SCM081420Se1f P SCM092420POTW Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 0.1 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.028 / 0.012 / 0.028 / 0.012 / 0.028 / 0.012 / 0.02 / 0.020 / 0.028 / 0.012 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 08/14/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S SCM081420Se1f P SCM092420POTW Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 23.1 / 6.94 / 23.1 / 6.94 / 23.1 / 6.94 / 15.02 / 15.02 / 23.1 / 6.94 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 5.943 / 0.637 / 5.943 / 0.637 / 5.943 / 0.637 / 3.29 / 3.290 / 5.943 / 0.637 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result / Limit Mass /Limit Oil & Grease, Total 08/14/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 S SCM081420Se1f P SCM092420POTW Week 2 Week 4 Average Average 10.1 / 200 2.5 / 200 10.1 / 2.5 / 10.1 / 2.5 / mg/L mg/L mg/L mg/L mg/L mg/L Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 2020 Quarter 3 < 6.3 / mg/L < / 2020 2nd 6 Months (Avg) < 6.3 / mg/L < / 2020 2nd 6 ...(Max) 10.1 / mg/L / 2020 2nd 6 ...(Min) < 2.5 / mg/L < / 2020 2nd 6 ...(Count) 2 / / 1 Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass / Limit pH 08/14/2020 S SCM081420Se1f 09/24/2020 P SCM092420POTW 11/06/2020 S SCM110620Se1f Aug 2020 Week 2 Sep 2020 Week 4 Nov 2020 Week 1 Aug 2020 Average Sep 2020 Average Nov 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 7 /6.0-10.5 SU / 8 /6.0-10.5 SU / 7.3 /6.0-10.5 SU / 7 / SU / 8 / SU / 7.3 / SU / 7 / SU / 8 / SU / 7.3 / SU / 7.5 / SU / 7.3 / SU / 7.43 / SU / 8 / SU / 7 / SU / 3 / / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Selenium 08/14/2020 S SCM081420Se1f < 0.005 / mg/L < 0.001286 / lbs/day 09/24/2020 P SCM092420POTW < 0.0005 / mg/L < 0.000046 / lbs/day Aug 2020 Week 2 < 0.005 / mg/L < 0.001286 / lbs/day Sep 2020 Week 4 < 0.0005 / mg/L < 0.000046 / lbs/day Aug 2020 Average < 0.005 / mg/L < 0.001286 / lbs/day Sep 2020 Average < 0.0005 / mg/L < 0.000046 / lbs/day 2020 Quarter 3 < 0.0028 / mg/L < 0.000666 / lbs/day 2020 2nd 6 Months (Avg) < 0.0028 / mg/L < 0.000666 / lbs/day 2020 2nd 6 ...(Max) < 0.005 / mg/L < 0.001286 / lbs/day 2020 2nd 6 ...(Min) < 0.0005 / mg/L < 0.000046 / lbs/day 2020 2nd 6 ...(Count) 2 / 2 / Sample Date SamplelD Result / Limit Mass/Limit Temperature 08/14/2020 S SCM081420Se1f 27.4 / 66 °C / 09/24/2020 P SCM092420POTW 22 / 66 °C / 11/06/2020 S SCM110620Se1f 19 / 66 °C / Aug 2020 Week 2 27.4 / °C / Sep 2020 Week 4 22 / °C / Nov 2020 Week 1 19 / °C / Aug 2020 Average 27.4 / °C / Sep 2020 Average 22 / °C / Nov 2020 Average 19 / °C / 2020 Quarter 3 24.7 / °C / 2020 Quarter 4 19 / °C / 2020 2nd 6 Months (Avg) 22.8 / °C / 2020 2nd 6 ...(Max) 27.4 / °C / 2020 2nd 6 ...(Min) 19 / °C / 2020 2nd 6 ...(Count) 3 / / Sample Count : 3 Months Sampled : 3 Weeks Sampled : 3 Quarters Sampled : 2 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result / Limit Mass /Limit TKN 08/14/2020 S SCM081420Se1f 09/24/2020 P SCM092420POTW 23 / 6.81 / mg/L mg/L 5.917 / 0.625 / lbs/day lbs/day Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 23 / 6.81 / 23 / 6.81 / 14.91 / 14.91 / 23 / 6.81 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 5.917 / 0.625 / 5.917 / 0.625 / 3.271 / 3.271 / 5.917 / 0.625 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 08/14/2020 09/24/2020 Aug 2020 Sep 2020 Aug 2020 Sep 2020 2020 2020 2020 2020 2020 S SCM081420Se1f P SCM092420POTW Week 2 Week 4 Average Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.81 / 1.04 / 0.81 / 1.04 / 0.81 / 1.04 / 0.925 / 0.925 / 1.04 / 0.81 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.2084 / 0.0954 / 0.2084 / 0.0954 / 0.2084 / 0.0954 / 0.1519 / 0.1519 / 0.2084 / 0.0954 / 2 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result /Limit Mass /Limit VOC 08/14/2020 Aug 2020 Aug 2020 2020 2020 2020 2020 2020 S SCM081420Se1f Week 2 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.021 / 0.021 / 0.021 / 0.021 / 0.021 / 0.021 / 0.021 / 1 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L Sample Date SamplelD Result /Limit Mass /Limit Zinc 08/14/2020 09/24/2020 Aug 2020 Sep 2020 S SCM081420Se1f P SCM092420POTW Week 2 Week 4 0.253 / 0.39 / 0.253 / 0.39 / mg/L mg/L mg/L mg/L 0.065088 / 0.035785 / 0.065088 / 0.035785 / lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 SCM Metal Products, Inc. SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Zinc Aug 2020 Average 0.253 / mg/L Sep 2020 Average 0.39 / mg/L 2020 Quarter 3 0.322 / mg/L 2020 2nd 6 Months (Avg) 0.322 / mg/L 2020 2nd 6 ...(Max) 0.39 / mg/L 2020 2nd 6 ...(Min) 0.253 / mg/L 2020 2nd 6 ...(Count) 2 / 0.065088 / lbs/day 0.035785 / lbs/day 0.050436 / lbs/day 0.050436 / lbs/day 0.065088 / lbs/day 0.035785 / lbs/day 2 / Wednesday, February 24, 2021 10:21:42PM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Acetone 11/11/2020 S TriPharm111120Self 0.091 / 5.44 mg/L 12/15/2020 P TriPharm121520POT < 0.25 / 5.44 mg/L < W Nov 2020 Week 2 0.091 / mg/L Dec 2020 Week 3 < 0.25 / mg/L < Nov 2020 Average 0.091 / 2.15 mg/L Dec 2020 Average < 0.25 / 2.15 mg/L < 2020 Quarter 4 < 0.171 / mg/L < 2020 2nd 6 Months (Avg) < 0.171 / mg/L < 2020 2nd 6 ...(Max) < 0.25 / mg/L < 2020 2nd 6 ...(Min) 0.091 / mg/L 2020 2nd 6 ...(Count) 2 / 0.0041 / 0.0041 / 0.0041 / 0.0041 / 0.0041 / 0.0041 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Ammonia 11/11/2020 S TriPharm111120Self 0.4 / mg/L / 12/15/2020 P TriPharm121520POT 0.3 / mg/L 0.0049 / lbs/day W Nov 2020 Week 2 0.4 / mg/L / Dec 2020 Week 3 0.3 / mg/L 0.0049 / lbs/day Nov 2020 Average 0.4 / mg/L / Dec 2020 Average 0.3 / mg/L 0.0049 / lbs/day 2020 Quarter 4 0.35 / mg/L 0.0049 / lbs/day 2020 2nd 6 Months (Avg) 0.35 / mg/L 0.0049 / lbs/day 2020 2nd 6 ...(Max) 0.4 / mg/L 0.0049 / lbs/day 2020 2nd 6 ...(Min) 0.3 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 10/31/2020 S TriPharm1020F1ow 0.002926 / MGD / 11/30/2020 S TriPharm1120Flow 0.001974 / MGD / 12/31/2020 S TriPharm1220F1ow 0.001882 / MGD / Oct 2020 Week 4 0.002926 / MGD / Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 1 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Average Flow for Month Nov 2020 Week 4 0.001974 / MGD Dec 2020 Week 4 0.001882 / MGD Oct 2020 Average 0.002926 / MGD Nov 2020 Average 0.001974 / MGD Dec 2020 Average 0.001882 / MGD 2020 Quarter 4 0.002261 / MGD 2020 2nd 6 Months (Avg) 0.002261 / MGD 2020 2nd 6 ...(Max) 0.002926 / MGD 2020 2nd 6 ...(Min) 0.001882 / MGD 2020 2nd 6 ...(Count) 3 / Sample Date SamplelD Result/Limit Mass/Limit BOD 11/11/2020 S TriPharm111120Self < 1 / mg/L < / 12/15/2020 P TriPharm121520POT 16.5 / mg/L 0.27 / lbs/day W Nov 2020 Week 2 < 1 / mg/L < / Dec 2020 Week 3 16.5 / mg/L 0.27 / lbs/day Nov 2020 Average < 1 / mg/L < / Dec 2020 Average 16.5 / mg/L 0.27 / lbs/day 2020 Quarter 4 < 8.8 / mg/L < 0.27 / lbs/day 2020 2nd 6 Months (Avg) < 8.8 / mg/L < 0.270 / lbs/day 2020 2nd 6 ...(Max) 16.5 / mg/L 0.270 / lbs/day 2020 2nd 6 ...(Min) < 1 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Cadmium 11/11/2020 S TriPharm111120Self < 0.001 / mg/L < / 12/15/2020 P TriPharm121520POT < 0.00008 / mg/L < 0.000001 / lbs/day W Nov 2020 Week 2 < 0.001 / mg/L < / Dec 2020 Week 3 < 0.00008 / mg/L < 0.000001 / lbs/day Nov 2020 Average < 0.001 / mg/L < / Dec 2020 Average < 0.00008 / mg/L < 0.000001 / lbs/day 2020 Quarter 4 < 0.00054 / mg/L < 0.000001 / lbs/day 2020 2nd 6 Months (Avg) < 0.00054 / mg/L < 0.000001 / lbs/day 2020 2nd 6 ...(Max) < 0.001 / mg/L < 0.000001 / lbs/day 2020 2nd 6 ...(Min) < 0.00008 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 2 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Chloride 11/11/2020 S TriPharm111120Self 1000 / mg/L 12/15/2020 P TriPharm121520POT 17.5 / mg/L W Nov 2020 Week 2 1000 / mg/L Dec 2020 Week 3 17.5 / mg/L Nov 2020 Average 1000 / mg/L Dec 2020 Average 17.5 / mg/L 2020 Quarter 4 508.75 / mg/L 2020 2nd 6 Months (Avg) 508.75 / mg/L 2020 2nd 6 ...(Max) 1000 / mg/L 2020 2nd 6 ...(Min) 17.5 / mg/L 2020 2nd 6 ...(Count) 2 / 0.2861 / lbs/day 0.2861 / lbs/day 0.2861 / lbs/day 0.2861 / lbs/day 0.2861 / lbs/day 0.2861 / lbs/day Sample Date SamplelD Result/Limit Mass/Limit COD 11/11/2020 S TriPharm111120Self 12/15/2020 P TriPharm121520POT W Nov 2020 Week 2 Dec 2020 Week 3 Nov 2020 Average Dec 2020 Average 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 38 / mg/L / 23 / mg/L 0.38 / lbs/day 38 / mg/L / 23 / mg/L 0.38 / lbs/day 38 / mg/L / 23 / mg/L 0.38 / lbs/day 30.5 / mg/L 0.38 / lbs/day 30.5 / mg/L 0.38 / lbs/day 38 / mg/L 0.38 / lbs/day 23 / mg/L / 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Cyanide 12/15/2020 P TriPharm121520POT < 0.003 / mg/L < 0.000041 / lbs/day W Dec 2020 Week 3 < 0.003 / mg/L < 0.000041 / lbs/day Dec 2020 Average < 0.003 / mg/L < 0.000041 / lbs/day 2020 Quarter 4 < 0.003 / mg/L < 0.000041 / lbs/day 2020 2nd 6 Months (Avg) < 0.003 / mg/L < 0.000041 / lbs/day 2020 2nd 6 ...(Max) < 0.003 / mg/L < 0.000041 / lbs/day 2020 2nd 6 ...(Min) < 0.003 / mg/L < 0.000041 / lbs/day 2020 2nd 6 ...(Count) 1 / 1 / Sample Date SamplelD Result / Limit Mass/Limit Ethyl acetate Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 3 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate 11/11/2020 S TriPharm111120Self < 0.001 / 5.44 mg/L < / 12/15/2020 P TriPharm121520POT < 0.025 / 5.44 mg/L < 0.0004 / lbs/day W Nov 2020 Week 2 < 0.001 / mg/L < / Dec 2020 Week 3 < 0.025 / mg/L < 0.0004 / lbs/day Nov 2020 Average < 0.001 / 2.15 mg/L < / Dec 2020 Average < 0.025 / 2.15 mg/L < 0.0004 / lbs/day 2020 Quarter 4 < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 Months (Avg) < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Max) < 0.025 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Fluoride 11/11/2020 S TriPharm111120Self < 0.05 / mg/L < / 12/15/2020 P TriPharm121520POT 0.37 / mg/L 0.006 / lbs/day W Nov 2020 Week 2 < 0.05 / mg/L < / Dec 2020 Week 3 0.37 / mg/L 0.006 / lbs/day Nov 2020 Average < 0.05 / mg/L < / Dec 2020 Average 0.37 / mg/L 0.006 / lbs/day 2020 Quarter 4 < 0.21 / mg/L < 0.006 / lbs/day 2020 2nd 6 Months (Avg) < 0.21 / mg/L < 0.0060 / lbs/day 2020 2nd 6 ...(Max) 0.37 / mg/L 0.0060 / lbs/day 2020 2nd 6 ...(Min) < 0.05 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Isopropyl acetate 11/11/2020 S TriPharm111120Self < 0.001 / 5.44 12/15/2020 P TriPharm121520POT < 0.025 / 5.44 W Nov 2020 Week 2 < 0.001 / Dec 2020 Week 3 < 0.025 / mg/L mg/L mg/L mg/L 0.0004 / 0.0004 / lbs/day lbs/day Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 4 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Isopropyl acetate Nov 2020 Average < 0.001 / 2.15 mg/L < / Dec 2020 Average < 0.025 / 2.15 mg/L < 0.0004 / lbs/day 2020 Quarter 4 < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 Months (Avg) < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Max) < 0.025 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Count : I 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 11/11/2020 S TriPharm111120Self < 0.000001 / 0.000142 mg/L < / 12/15/2020 P TriPharm121520POT < 0.000001 / 0.000142 mg/L < / WHg Nov 2020 Week 2 < 0.000001 / mg/L < / Dec 2020 Week 3 < 0.000001 / mg/L < / Nov 2020 Average < 0.000001 / mg/L < / Dec 2020 Average < 0.000001 / mg/L < / 2020 Quarter 4 < 0.000001 / mg/L < / 2020 2nd 6 Months (Avg) < 0.000001 / mg/L < / 2020 2nd 6 ...(Max) < 0.000001 / mg/L < / 2020 2nd 6 ...(Min) < 0.000001 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit Methylene Chloride 11/11/2020 S TriPharm111120Self < 0.003 / 0.78 mg/L Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 5 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Methylene Chloride 12/15/2020 P TriPharm121520POT < 0.025 / 0.78 mg/L < 0.000409 / lbs/day W Nov 2020 Week 2 < 0.003 / mg/L < / Dec 2020 Week 3 < 0.025 / mg/L < 0.000409 / lbs/day Nov 2020 Average < 0.003 / 0.18 mg/L < / Dec 2020 Average < 0.025 / 0.18 mg/L < 0.000409 / lbs/day 2020 Quarter 4 < 0.014 / mg/L < 0.000409 / lbs/day 2020 2nd 6 Months (Avg) < 0.014 / mg/L < 0.000409 / lbs/day 2020 2nd 6 ...(Max) < 0.025 / mg/L < 0.000409 / lbs/day 2020 2nd 6 ...(Min) < 0.003 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Count : 2 Months Sampled : 2 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Molybdenum 11/11/2020 S TriPharm111120Self < 0.003 / mg/L < / 12/15/2020 P TriPharm121520POT < 0.001 / mg/L < 0 / lbs/day W Nov 2020 Week 2 < 0.003 / mg/L < / Dec 2020 Week 3 < 0.001 / mg/L < 0 / lbs/day Nov 2020 Average < 0.003 / mg/L < / Dec 2020 Average < 0.001 / mg/L < 0 / lbs/day 2020 Quarter 4 < 0.002 / mg/L < 0 / lbs/day 2020 2nd 6 Months (Avg) < 0.002 / mg/L < 0.0000 / lbs/day 2020 2nd 6 ...(Max) < 0.003 / mg/L < 0.0000 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit n-Amyl acetate 11/11/2020 S TriPharm111120Self < 0.001 / 5.44 12/15/2020 P TriPharm121520POT < 0.025 / 5.44 W Nov 2020 Week 2 < 0.001 / Dec 2020 Week 3 < 0.025 / Nov 2020 Average < 0.001 / 2.15 mg/L mg/L mg/L mg/L mg/L 0.0004 / 0.0004 / lbs/day lbs/day Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 6 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit n-Amyl acetate Dec 2020 Average < 0.025 / 2.15 mg/L < 0.0004 / lbs/day 2020 Quarter 4 < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 Months (Avg) < 0.013 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Max) < 0.025 / mg/L < 0.0004 / lbs/day 2020 2nd 6 ...(Min) < 0.001 / mg/L < / 2020 2nd 6 ...(Count) 2 / Sample Count : I 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # 0/0 # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 1 / Sample Date SamplelD Result/Limit Mass/Limit Nitrate -Nitrite 11/11/2020 S TriPharm111120Self 0.4 / mg/L / 12/15/2020 P TriPharm121520POT 1 / mg/L 0.017 / lbs/day W Nov 2020 Week 2 0.4 / mg/L / Dec 2020 Week 3 1 / mg/L 0.017 / lbs/day Nov 2020 Average 0.4 / mg/L / Dec 2020 Average 1 / mg/L 0.017 / lbs/day 2020 Quarter 4 0.7 / mg/L 0.017 / lbs/day 2020 2nd 6 Months (Avg) 0.7 / mg/L 0.017 / lbs/day 2020 2nd 6 ...(Max) 1.0 / mg/L 0.017 / lbs/day 2020 2nd 6 ...(Min) 0.4 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit Nitrogen, Total 11/11/2020 S TriPharm111120Self 1.2 / mg/L / 12/15/2020 P TriPharm121520POT 1.6 / mg/L 0.026 / lbs/day W Nov 2020 Week 2 1.2 / mg/L / Dec 2020 Week 3 1.6 / mg/L 0.026 / lbs/day Nov 2020 Average 1.2 / mg/L / Dec 2020 Average 1.6 / mg/L 0.026 / lbs/day 2020 Quarter 4 1.4 / mg/L 0.026 / lbs/day 2020 2nd 6 Months (Avg) 1.4 / mg/L 0.026 / lbs/day 2020 2nd 6 ...(Max) 1.6 / mg/L 0.026 / lbs/day Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 7 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 1.2 / mg/L 2 / Sample Date SamplelD Result /Limit Mass /Limit pH 11/11/2020 S TriPharm111120Self 7.8 / 5.5 - 10.5 SU / 12/15/2020 P TriPharm121520POT 8 / 5.5 - 10.5 SU / W Nov 2020 Week 2 7.8 / SU / Dec 2020 Week 3 8 / SU / Nov 2020 Average 7.8 / SU / Dec 2020 Average 8 / SU / 2020 Quarter 4 7.9 / SU / 2020 2nd 6 Months (Avg) 7.9 / SU / 2020 2nd 6 ...(Max) 8 / SU / 2020 2nd 6 ...(Min) 7.8 / SU / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Temperature 11/11/2020 S TriPharm111120Self 12/15/2020 P TriPharm121520POT W Nov 2020 Week 2 Dec 2020 Week 3 Nov 2020 Average Dec 2020 Average 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 32 / 66 °C / 32 / 66 °C / 32 / °C / 32 / °C / 32 / °C / 32 / °C / 32 / °C / 32 / °C / 32 / °C / 32 / °C / 2 / / Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 8 of 10 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over MoAvg C: # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : Months Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 # Over WkAvg C: # Over Wk Avg C TRC : # Over WkAvg M: # Over Wk Avg M TRC : Weeks Sampled : # 0 0 0 0 2 Quarters Sampled : 1 # 0.00 # Over Qt Avg C : 0 0.00 0.00 # Over Qt Avg C TRC : 0 0.00 0.00 # Over Qtr Avg M : 0 0.00 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result /Limit Mass /Limit TKN 11/11/2020 12/15/2020 Nov 2020 Dec 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 S TriPharm111120Self P TriPharm121520POT W Week 2 Week 3 Average Average Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.79 / 0.58 / 0.79 / 0.58 / 0.79 / 0.58 / 0.69 / 0.69 / 0.79 / 0.58 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.009 / 0.009 / 0.009 / 0.009 / 0.009 / 0.009 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result/Limit Mass /Limit Total Phosphorus 11/11/2020 12/15/2020 Nov 2020 Dec 2020 Nov 2020 Dec 2020 2020 2020 2020 2020 2020 S TriPharm111120Self P TriPharm121520POT W Week 2 Week 3 Average Average Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.499 / 0.452 / 0.499 / 0.452 / 0.499 / 0.452 / 0.476 / 0.476 / 0.499 / 0.452 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.0074 / 0.0074 / 0.0074 / 0.0074 / 0.0074 / 0.0074 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample Date SamplelD Result/Limit Mass /Limit TSS 11/11/2020 S TriPharm111120Self 12/15/2020 P TriPharm121520POT W Nov 2020 Week 2 Dec 2020 Week 3 2.4 / 1.3 / 2.4 / 1.3 / mg/L mg/L mg/L mg/L • 0.020433 / < / • 0.020433 / lbs/day lbs/day Thursday, February 25,2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 9 of 10 TriPharm Services, Inc. dba Alcami Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TSS Nov 2020 Average < 2.4 / mg/L < / Dec 2020 Average < 1.3 / mg/L < 0.020433 / lbs/day 2020 Quarter 4 < 1.8 / mg/L < 0.020433 / lbs/day 2020 2nd 6 Months (Avg) < 1.8 / mg/L < 0.020433 / lbs/day 2020 2nd 6 ...(Max) < 2.4 / mg/L < 0.020433 / lbs/day 2020 2nd 6 ...(Min) < 1.3 / mg/L < / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit VOC 11/11/2020 S TriPharm111120Self 0.005 / mg/L / 12/15/2020 P TriPharm121520POT < 0.025 / mg/L < / W Nov 2020 Week 2 0.005 / mg/L / Dec 2020 Week 3 < 0.025 / mg/L < / Nov 2020 Average 0.005 / mg/L / Dec 2020 Average < 0.025 / mg/L < / 2020 Quarter 4 < 0.015 / mg/L < / 2020 2nd 6 Months (Avg) < 0.015 / mg/L < / 2020 2nd 6 ...(Max) < 0.025 / mg/L < / 2020 2nd 6 ...(Min) 0.005 / mg/L / 2020 2nd 6 ...(Count) 2 / / Sample Date SamplelD Result/Limit Mass/Limit Zinc 11/11/2020 S TriPharm111120Self 0.516 / mg/L / 12/15/2020 P TriPharm121520POT 0.205 / mg/L 0.003351 / lbs/day W Nov 2020 Week 2 0.516 / mg/L / Dec 2020 Week 3 0.205 / mg/L 0.003351 / lbs/day Nov 2020 Average 0.516 / mg/L / Dec 2020 Average 0.205 / mg/L 0.003351 / lbs/day 2020 Quarter 4 0.361 / mg/L 0.003351 / lbs/day 2020 2nd 6 Months (Avg) 0.361 / mg/L 0.003351 / lbs/day 2020 2nd 6 ...(Max) 0.516 / mg/L 0.003351 / lbs/day 2020 2nd 6 ...(Min) 0.205 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Thursday, February 25, 2021 9:00:56AM * Indicates Violation ** Indicates TRC Violation Page 10 of 10 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Ammonia 07/01/2020 S UTP1070120Se1f 07/23/2020 P UTP1072320POTW Jul 2020 Week 1 Ju12020 Week 4 Jul 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 1.1 / mg/L 1.6 / mg/L 1.1 / mg/L 1.6 / mg/L 1.35 / mg/L 1.35 / mg/L 1.35 / mg/L 1.6 / mg/L 1.1 / mg/L 2 / 0.5061 / lbs/day 0.5061 / lbs/day 0.5061 / lbs/day 0.5061 / lbs/day 0.5061 / lbs/day 0.5061 / lbs/day Sample Date SamplelD Result/Limit Mass/Limit Average Flow for Month 07/31/2020 S UTP10720F1ow 08/31/2020 S UTP10820F1ow 09/30/2020 S UTP10920F1ow 10/31/2020 S UTP11020F1ow 11/30/2020 S UTP11120F1ow 12/31/2020 S UTP11220F1ow Ju12020 Week 4 Aug 2020 Week 4 Sep 2020 Week 4 Oct 2020 Week 4 Nov 2020 Week 4 Dec 2020 Week 4 Jul 2020 Average Aug 2020 Average Sep 2020 Average Oct 2020 Average Nov 2020 Average Dec 2020 Average 2020 Quarter 3 2020 Quarter 4 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.035806 / MGD 0.030156 / MGD 0.030156 / MGD 0.031514 / MGD 0.038165 / MGD 0.034257 / MGD 0.035806 / MGD 0.030156 / MGD 0.030156 / MGD 0.031514 / MGD 0.038165 / MGD 0.034257 / MGD 0.035806 / MGD 0.030156 / MGD 0.030156 / MGD 0.031514 / MGD 0.038165 / MGD 0.034257 / MGD 0.032039 / MGD 0.034645 / MGD 0.033342 / MGD 0.038165 / MGD 0.030156 / MGD 6 / Sample Date SamplelD Result/Limit Mass/Limit BOD 07/01/2020 S UTP1070120Se1f 07/23/2020 P UTP1072320POTW 63.6 / 25 / mg/L mg/L 7.908 / lbs/day Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 1 of 7 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit BOD Jul 2020 Week 1 63.6 / mg/L Jul 2020 Week 4 25 / mg/L Ju12020 Average 44.3 / mg/L 2020 Quarter 3 44.3 / mg/L 2020 2nd 6 Months (Avg) 44.3 / mg/L 2020 2nd 6 ...(Max) 63.6 / mg/L 2020 2nd 6 ...(Min) 25 / mg/L 2020 2nd 6 ...(Count) 2 / 7.908 / lbs/day 7.908 / lbs/day 7.908 / lbs/day 7.908 / lbs/day 7.908 / lbs/day 1 / Sample Date SamplelD Result/Limit Mass/Limit Cadmium 07/01/2020 S UTP1070120Se1f < 0.0005 / mg/L < / Jul 2020 Week 1 < 0.0005 / mg/L < / Jul 2020 Average < 0.0005 / mg/L < / 2020 Quarter 3 < 0.0005 / mg/L < / 2020 2nd 6 Months (Avg) < 0.0005 / mg/L < / 2020 2nd 6 ...(Max) < 0.0005 / mg/L < / 2020 2nd 6 ...(Min) < 0.0005 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass /Limit Chloride 07/01/2020 S UTP1070120Se1f 18.5 / mg/L / 07/23/2020 P UTP1072320POTW 300 / mg/L 94.9009 / lbs/day Ju12020 Week 1 18.5 / mg/L / Jul 2020 Week 4 300 / mg/L 94.9009 / lbs/day Ju12020 Average 159.25 / mg/L 94.9009 / lbs/day 2020 Quarter 3 159.25 / mg/L 94.9009 / lbs/day 2020 2nd 6 Months (Avg) 159.25 / mg/L 94.9009 / lbs/day 2020 2nd 6 ...(Max) 300 / mg/L 94.9009 / lbs/day 2020 2nd 6 ...(Min) 18.5 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit COD 07/01/2020 S UTP1070120Se1f 07/23/2020 P UTP1072320POTW Jul 2020 Week 1 Ju12020 Week 4 Jul 2020 Average 2020 Quarter 3 136 / mg/L / 67 / mg/L 21.19 / lbs/day 136 / mg/L / 67 / mg/L 21.19 / lbs/day 101.5 / mg/L 21.19 / lbs/day 101.5 / mg/L 21.19 / lbs/day Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 2 of 7 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit COD 2020 2nd 6 Months (Avg) 101.5 / mg/L 2020 2nd 6 ...(Max) 136 / mg/L 2020 2nd 6 ...(Min) 67 / mg/L 2020 2nd 6 ...(Count) 2 / 21.19 / lbs/day 21.19 / lbs/day Sample .Date SamplelD Result / Limit Mass / Limit Cyanide 07/01/2020 S UTP1070120Se1f < 0.004 / mg/L < / Ju12020 Week 1 < 0.004 / mg/L < / Ju12020 Average < 0.004 / mg/L < / 2020 Quarter 3 < 0.004 / mg/L < / 2020 2nd 6 Months (Avg) < 0.004 / mg/L < / 2020 2nd 6 ...(Max) < 0.004 / mg/L < / 2020 2nd 6 ...(Min) < 0.004 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result / Limit Mass/Limit Fluoride 07/01/2020 S UTP1070120Se1f < 0.05 / mg/L < / Jul 2020 Week 1 < 0.05 / mg/L < / Jul 2020 Average < 0.05 / mg/L < / 2020 Quarter 3 < 0.05 / mg/L < / 2020 2nd 6 Months (Avg) < 0.05 / mg/L < / 2020 2nd 6 ...(Max) < 0.05 / mg/L < / 2020 2nd 6 ...(Min) < 0.05 / mg/L < / 2020 2nd 6 ...(Count) 1 / / Sample Date SamplelD Result/Limit Mass/Limit Mercury - LL 07/01/2020 S UTP1070120Se1f < 0.000001 / 0.000142 mg/L < / 07/23/2020 P UTP1072320POTWHg 0.000003 / 0.000142 mg/L / 11/23/2020 P UTP1112320POTWHg 0.000002 / 0.000142 mg/L / 12/11/2020 P UTP1121120POTWHg 0.000006 / 0.000142 mg/L / Jul 2020 Week 1 < 0.000001 / mg/L < / Jul 2020 Week 4 0.000003 / mg/L / Nov 2020 Week 4 0.000002 / mg/L / Dec 2020 Week 2 0.000006 / mg/L / Jul 2020 Average < 0.000002 / mg/L < / Nov 2020 Average 0.000002 / mg/L / Dec 2020 Average 0.000006 / mg/L / 2020 Quarter 3 < 0.000002 / mg/L < / Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 3 of 7 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Mercury - LL 2020 2020 2020 2020 2020 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 1 Sample Count : 0 0 0 0 0 0 4 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 0.000004 / 0.000003 / 0.000006 / 0.000001 / 4 / Months Sampled : 3 0 0 0 0 mg/L mg/L mg/L mg/L 0.00 # Over Wk Avg C : 0.00 # Over Wk Avg C TRC : 0.00 # Over Wk Avg M : 0.00 # Over Wk Avg M TRC : Weeks Sampled : 0 0 0 0 4 Quarters Sampled : 2 #0/0 0.00 # Over Qt Avg C : 0 0.00 0.00 # Over Qt Avg C TRC : 0 0.00 0.00 # Over Qtr Avg M : 0 0.00 0.00 # Over Qtr Avg M TRC : 0 0.00 Sample Date SamplelD Result / Limit Mass / Limit Molybdenum 07/01/2020 S UTP1070120Se1f Jul 2020 Week 1 Jul 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) < 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 0.003 / 0.003 / 0.003 / 0.003 / 0.003 / 0.003 / 0.003 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L < Sample Date SamplelD Result /Limit Mass /Limit Nitrate -Nitrite 07/01/2020 07/23/2020 Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 2020 2020 S UTP1070120Se1f P UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.7 / 1.8 / 0.7 / 1.8 / 1.2 / 1.2 / 1.2 / 1.8 / 0.7 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.554 / 0.554 / 0.554 / 0.554 / 0.554 / 0.554 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample .Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 07/01/2020 S UTP1070120Se1f 5.9 / mg/L Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 4 of 7 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit Nitrogen, Total 07/23/2020 Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 2020 2020 P UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 11 / 5.9 / 11 / 8.45 / 8.45 / 8.45 / 11 / 5.9 / 2 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 3.48 3.48 3.48 3.48 3.480 3.480 lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Sample .Date SamplelD Result /Limit Mass /Limit Oil & Grease, Total 07/01/2020 S 07/23/2020 P Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 2020 2020 UTP 1070120Se1f UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 12.9 2.5 12.9 2.5 7.7 7.7 7.7 12.9 2.5 2 / 200 / 200 Months Sampled : # 0 0 0 0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 Weeks Sampled : 2 # 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result/Limit Mass /Limit pH 07/01/2020 07/23/2020 Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 2020 S UTP1070120Se1f P UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 7.7 /5.5-10.0 SU 7.2 /5.5-10.0 SU 7.7 / SU 7.2 / SU 7.45 / SU 7.45 / SU 7.45 / SU 7.7 / SU 7.2 / SU Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 5 of 7 # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit pH 2020 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 2 / Months Sampled : 0 0 0 0 1 Weeks Sampled : 2 #0/0 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Temperature 07/01/2020 07/23/2020 Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 2020 2020 S UTP1070120Se1f P UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample Count : 0 0 0 0 0 0 2 0.00 0.00 0.00 0.00 0.00 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 25.1 / 66 28 / 66 25.1 / 28 / 26.6 / 26.6 / 26.6 / 28 / 25.1 / 2 / Months Sampled : 0 0 0 0 °C °C °C °C °C oC °C °c °C 1 Weeks Sampled : 2 # 0.00 # Over Wk Avg C : 0 0.00 0.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qt Avg C : # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 1 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit TKN 07/01/2020 07/23/2020 Jul 2020 Jul 2020 Jul 2020 2020 2020 2020 S UTP1070120Se1f P UTP1072320POTW Week 1 Week 4 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 5.2 / 9.21 / 5.2 / 9.21 / 7.21 / 7.21 / 7.21 / 9.21 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 2.913 / 2.913 / 2.913 / 2.913 / 2.913 / 2.913 / lbs/day lbs/day lbs/day lbs/day lbs/day lbs/day Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 6 of 7 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 001 Sample Date SamplelD Result /Limit Mass /Limit TKN 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 5.2 / mg/L 2 / Sample Date SamplelD Result /Limit Mass /Limit Total Phosphorus 07/01/2020 S UTP1070120Se1f 0.89 / mg/L / 07/23/2020 P UTP1072320POTW 1.69 / mg/L 0.5346 / lbs/day Ju12020 Week 1 0.89 / mg/L / Ju12020 Week 4 1.69 / mg/L 0.5346 / lbs/day Ju12020 Average 1.29 / mg/L 0.5346 / lbs/day 2020 Quarter 3 1.29 / mg/L 0.5346 / lbs/day 2020 2nd 6 Months (Avg) 1.29 / mg/L 0.5346 / lbs/day 2020 2nd 6 ...(Max) 1.69 / mg/L 0.5346 / lbs/day 2020 2nd 6 ...(Min) 0.89 / mg/L / 2020 2nd 6 ...(Count) 2 / 1 / Sample Date SamplelD Result/Limit Mass/Limit TSS 07/01/2020 S UTP1070120Se1f 07/23/2020 P UTP1072320POTW Jul 2020 Week 1 Ju12020 Week 4 Jul 2020 Average 2020 Quarter 3 2020 2nd 6 Months (Avg) 2020 2nd 6 ...(Max) 2020 2nd 6 ...(Min) 2020 2nd 6 ...(Count) 55 / mg/L / 27 / mg/L 8.541077 / lbs/day 55 / mg/L / 27 / mg/L 8.541077 / lbs/day 41 / mg/L 8.541077 / lbs/day 41 / mg/L 8.541077 / lbs/day 41 / mg/L 8.54108 / lbs/day 55 / mg/L 8.541077 / lbs/day 27 / mg/L / 2 / 1 / Sample Date SamplelD Result/Limit Mass /Limit Zinc 07/01/2020 Jul 2020 Jul 2020 2020 2020 2020 2020 2020 S UTP1070120Se1f Week 1 Average Quarter 3 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) 0.16 / 0.16 / 0.16 / 0.16 / 0.16 / 0.16 / 0.16 / mg/L mg/L mg/L mg/L mg/L mg/L mg/L 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Ou fall: 002 Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 7 of 7 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit Acetone 07/10/2020 07/30/2020 09/01/2020 09/18/2020 09/22/2020 10/27/2020 10/29/2020 11/12/2020 11/13/2020 11/23/2020 Jul 2020 Jul 2020 Sep 2020 Sep 2020 Sep 2020 Oct 2020 Nov 2020 Nov 2020 Jul 2020 Sep 2020 Oct 2020 Nov 2020 2020 2020 2020 2020 2020 2020 S UTP2071020Se1f P UTP2073020POTW S UTP2090120Se1f S UTP2091820Se1f S UTP2092220Se1f S UTP2102720Se1f S UTP2102920Se1f S UTP2111220Se1f S UTP2111320Se1f S UTP2112320Se1f Week 2 Week 4 Week 1 Week 3 Week 4 Week 4 Week 2 Week 4 Average Average Average Average Quarter 3 Quarter 4 2nd 6 Months (Avg) 2nd 6 ...(Max) 2nd 6 ...(Min) 2nd 6 ...(Count) Sample # Over Daily C : # Over Daily C TRC: # Over Daily M : # Over Daily M TRC : # Under Daily : # Under Daily TRC: Count : 10 0/0 2 20.00 2 20.00 0 0.00 0 0.00 0 0.00 0 0.00 # Over Mo Avg C : # Over Mo Avg C TRC : # Over Mo Avg M : # Over Mo Avg M TRC : 25.8 6.4 9.1 26 11.5 4.73 10.1 1.09 1.28 2.29 25.8 6.4 9.1 26 11.5 7.415 1.185 2.29 16.1 15.533 7.415 1.553 15.76 3.898 9.829 26 1.09 10 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 20.7 / 8.2 / 8.2 / 8.2 / 8.2 Months Sampled : 4 2 2 0 0 mg/L * mg/L mg/L mg/L * mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L * mg/L * mg/L mg/L mg/L mg/L mg/L mg/L mg/L * * * * Weeks Sampled : 8 #0/0 50.00 # Over Wk Avg C : 0 0.00 50.00 # Over Wk Avg C TRC : 0 0.00 0.00 # Over Wk Avg M : 0 0.00 0.00 # Over Wk Avg M TRC : 0 0.00 # Over QtAvg C: # Over Qt Avg C TRC : # Over Qtr Avg M : # Over Qtr Avg M TRC : Quarters Sampled : # 0 0 0 0 2 0.00 0.00 0.00 0.00 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate 07/10/2020 07/30/2020 Jul 2020 S UTP2071020Self P UTP2073020POTW Week 2 0.1 / 20.7 0.005 / 20.7 0.1 / mg/L mg/L mg/L Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 1 of 3 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit Ethyl acetate Jul 2020 Week 4 < 0.005 / mg/L < / Jul 2020 Average < 0.053 / 8.2 mg/L < / 2020 Quarter 3 < 0.053 / mg/L < / 2020 2nd 6 Months (Avg) < 0.053 / mg/L < / 2020 2nd 6 ...(Max) < 0.1 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : I 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit Isopropyl acetate 07/10/2020 S UTP2071020Se1f < 0.1 / 20.7 mg/L < / 07/30/2020 P UTP2073020POTW < 0.005 / 20.7 mg/L < / Jul 2020 Week 2 < 0.1 / mg/L < / Jul 2020 Week 4 < 0.005 / mg/L < / Jul 2020 Average < 0.053 / 8.2 mg/L < / 2020 Quarter 3 < 0.053 / mg/L < / 2020 2nd 6 Months (Avg) < 0.053 / mg/L < / 2020 2nd 6 ...(Max) < 0.1 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # cyo # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass /Limit Methylene Chloride 07/10/2020 S UTP2071020Se1f < 0.002 / 3.0 mg/L < / 07/30/2020 P UTP2073020POTW < 0.005 / 3.0 mg/L < / Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 2 of 3 United Therapeutics Corporation SAMPLE OVERVIEW 7/1/2020 To 12/31/2020 Sample Type: Effluent Wastewater Outfall: 002 Sample Date SamplelD Result /Limit Mass /Limit Methylene Chloride Jul 2020 Week 2 < 0.002 / mg/L < / Jul 2020 Week 4 < 0.005 / mg/L < / Jul 2020 Average < 0.004 / 0.7 mg/L < / 2020 Quarter 3 < 0.004 / mg/L < / 2020 2nd 6 Months (Avg) < 0.004 / mg/L < / 2020 2nd 6 ...(Max) < 0.005 / mg/L < / 2020 2nd 6 ...(Min) < 0.002 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Sample Date SamplelD Result/Limit Mass/Limit n-Amyl acetate 07/10/2020 S UTP2071020Se1f < 0.05 / 20.7 mg/L < / 07/30/2020 P UTP2073020POTW < 0.005 / 20.7 mg/L < / Jul 2020 Week 2 < 0.05 / mg/L < / Jul 2020 Week 4 < 0.005 / mg/L < / Jul 2020 Average < 0.028 / 8.2 mg/L < / 2020 Quarter 3 < 0.028 / mg/L < / 2020 2nd 6 Months (Avg) < 0.028 / mg/L < / 2020 2nd 6 ...(Max) < 0.05 / mg/L < / 2020 2nd 6 ...(Min) < 0.005 / mg/L < / 2020 2nd 6 ...(Count) 2 / / Sample Count : 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1 # % # % # % # % # Over Daily C : 0 0.00 # Over Mo Avg C : 0 0.00 # Over Wk Avg C : 0 0.00 # Over Qt Avg C : 0 0.00 # Over Daily C TRC: 0 0.00 # Over Mo Avg C TRC : 0 0.00 # Over Wk Avg C TRC : 0 0.00 # Over Qt Avg C TRC : 0 0.00 # Over Daily M : 0 0.00 # Over Mo Avg M : 0 0.00 # Over Wk Avg M : 0 0.00 # Over Qtr Avg M : 0 0.00 # Over Daily M TRC : 0 0.00 # Over Mo Avg M TRC : 0 0.00 # Over Wk Avg M TRC : 0 0.00 # Over Qtr Avg M TRC : 0 0.00 # Under Daily : 0 0.00 # Under Daily TRC: 0 0.00 Wednesday, February 24, 2021 8:53:56PM * Indicates Violation ** Indicates TRC Violation Page 3 of 3