HomeMy WebLinkAboutWQ0011448_Residual Annual Report 2020_20210224Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0011448
Applicant/Permittee Town of Snow Hill
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Washington
CO Reviewer
Admin Reviewer
Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * Drew Matthews
Email Address*
dniatthev4s@soilplus.net
Project Information
........ .................................................................................................................................................. .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
2528839301
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
WQ0011448
Has Current Existing permt number
Applicant/Permittee Address*
PO Box247 Snow Hill, NC 28580
Facility Name *
Town of Snow Hill RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form} Engineering Rans, Specifications, Calculations, Bc.)
2020 Snow Hill Annual Report.pdf 4.11MB
Upload only 1 FLFdocurrent (less than 250 fvB). Miltiple documents rust be combined into one RJFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
a�f4ri (M&A"
Submission Date 2/24/2021
TOWN OF SNOW HILL
2020 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0011448
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
February 23, 2021
SOIL PLUS
SOIL PLUS
February 23, 2021
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2020 LAND APPLICATION ANNUAL REPORT
Town of Snow Hill "Class B" Program
NC Permit No.: WQ0011448
Soil Plus Project No. 200804.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Snow Hill on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The Town of Snow Hill conducted application events on permitted fields in Greene
County during 2020. A total of 31.49 Dry Tons or 248,400 Gallons of permitted residual
biosolids were land applied to permitted fields.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Town of Snow Hill (252-939-5051) for further assistance.
Respectfully,
Drew Matthews, Soil Plus
John Bauer, Town of Snow Hill
Jason Smith, Granville Farms
P.O. Box 1396
Oxford, NC 27565
(252) 883-9301
dmatthewsgsoilplus.ne t
www.soilplus.net
Town of Snow Hill
2020 Annual Land
Application of
Residual Biosolids
Report
WQ0011448
Snow Hill, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Analytical Data
TCLP
FIELD LOADING
SUMMARY FORM
Town of Snow Hill Farm
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
Fecal Coliform Data
30-Day Bench Scale Test
SOIL SAMPLES
Town of Snow Hill Farm
Town of Snow Hill
2020 Class B Annual Report
WQ Permit# WQ0011448
Annual Certification Form
Source Summary
Field Loading Summary
ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0011448 Town of Snow Hill Granville Farms, Inc. Greene (252) 939-5051
Year: 2020
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Yes No
Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how � rol
the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 1
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 31.49
Total number of acres utilized for land application during the year: 11.4
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑d
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilitie
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Jow I du �N l l l(,
�typ p *Sinatureof Permittee D to
Per tee Name and Tie a or rint : aiy[...� 1/21/2021
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
* Preparer is defined in 46 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Source Summary Report
MILr'p VolumeApplied AN
Town of Snow Hill WWTP 248,400 31.49
Total 248,400 31.49
Site# SH
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
3 11.4 248,400 31.49 58.30 Common 196 29.7% Annual Ryegrass - 50
Bermudagrass Hay Hay
Total 248,400 31.49
Town of Snow Hill
2020 Class B Annual Report
WQ Permit# WQ0011448
Residual Sampling Summary Form
Field Loading Calculations
2020 Analytical
2020 TCLP
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0011448 Facility Name Town of Snow Hill Source Permit No. NC0020842 Source Name Town of Snow Hill W WTP
Laboratory 1 Meritech, Inc.
Laboratory 2
Sample or CompositeDate 7/29/2020
Parameter (mg/I(g) Class A Class B
Aluminum
N/A
N/A
8,130
Ammonia Nitrogen
N/A
N/A
3,120
Arsenic
41
75
1.64
Cadmium
39
85
1.28
Calcium
N/A
N/A
15,400
Copper
1,500
4,300
602
Lead
300
840
34.2
Magnesium
N/A
N/A
3,490
Mercury
17
57
288
Molybdenum
N/A
75
5.03
Nickel
420
420
24.2
Nitrate -Nitrite Nitrogen
N/A
N/A
329
Percent Solids
N/A
N/A
3.04
PH (no units)
N/A
N/A
6.80
Phosphorus
N/A
N/A
31,700
Potassium
N/A
N/A
5,900
PAN (Inj./Inc.)
N/A
N/A
12,113
PAN (Surface)
N/A
N/A
10,553
Selenium
!00
100
1.67
Sodium
N/A
N/A
7,400
SAR
N/A
N/A
226
TKN
N/A
N/A
32 000
Zinc
2,800
7,500
852
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
&,,AGMAN FIELD LOADING ESTIMATES
Facility Town of Snow Hill VP P
Sampling Date 7/29/2020
Solids 3.04
Mineralization Rate 0.3
Gallons per DT 7,888.43
pH 6.8
Sodium Absorpotion 2.26 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 32,000 lbs./1,000 gal 8.11
Ammonia Nitrogen (mg/Kg) 3,120.00 lbs./1,000 gal 0.79
Nitrate -Nitrite (mg/Kg) 329.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 10,553 lbs./1,000 gal 2.68
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 12,113 lbs./1,000 gal 3.07
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.50
Phosphorus lbs./1,000 gal 8.04
Calcium lbs./1,000 gal 3.90
Magnesium lbs./1,000 gal 1.39
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
1.64
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.28
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
602.00
Copper lbs./1,000 gal
0.15
Lead (mg/Kg)
34.20
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
2.88
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
24.20
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
1.67
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
852.00
Zinc lbs./1,000 gal
0.22
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
32,000
10,553 21.11
21,447
32,000
12,113 24.23
19,887
21,447
3,217 6.43
18,230
19,887
2,983 5.97
16,904
18,230
1,367 2.73
16,863
16,904
1,268 2.54
15,636
16,863
632 1.26
16,230
15,636
586 1.17
15,050
16,230
304 0.61
15,926
15,050
282 0.56
14,768
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 16,074 32.15
Total 17,232 34.46
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Drew Matthews
CIient: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Report Date:
Project:
Date Sample Rcvd:
8/14/2020
Snow Hill
7/29/2020
Meritech Work Order # 072920102 Sample: SH072920 Grab
7/29/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.04 %
7/30/20
0-100 %
SM 2540B
Ammonia, Nitrogen
3,120 mg/kg
8/7/20
10 mg/kg
EPA 350.1
TKN
32,000 mg/kg
8/5/20
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<329 mg/kg
8/4/20
329 mg/kg
EPA 353.2
Aluminum, total
8,130 mg/kg
8/13/20
2.50 mg/kg
EPA 200.7
Arsenic, total
<1.64 mg/kg
8/13/20
1.64 mg/kg
EPA 200.7
Cadmium, total
1.28 mg/kg
8/13/20
0.200 mg/kg
EPA 200.7
Calcium, total
15,400 mg/kg
8/13/20
10.0 mg/kg
EPA 200.7
Copper, total
602 mg/kg
8/13/20
1.00 mg/kg
EPA 200.7
Lead, total
34.2 mg/kg
8/13/20
0.500 mg/kg
EPA 200.7
Magnesium, total
5,490 mg/kg
8/13/20
10.0 mg/kg
EPA 200.7
Mercury, total
2.88 mg/kg
8/4/20
0.02 mg/kg
EPA 245.1
Molybdenum, total
5.03 mg/kg
8/13/20
0.500 mg/kg
EPA 200.7
Nickel, total
24.2 mg/kg
8/13/20
2.0 mg/kg
EPA 200.7
Phosphorus, total
31,700 mg/kg
8/13/20
2.00 mg/kg
EPA 200.7
Potassium, total
5,900 mg/kg
8/13/20
20.0 mg/kg
EPA 200.7
Selenium, total
<1.67 mg/kg
8/13/20
1.67 mg/kg
EPA 200.7
Sodium, total
7,400 mg/kg
8/13/20
20.0 mg/kg
EPA 200.7
Zinc, total
852 mg/kg
8/13/20
0.500 mg/kg
EPA 200.7
pH
6.8 S.U.
7/30/20
1.0 -14.0 S.U.
SM 4500-HB
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Chain of Custody Record (COC)
NPDES#:
Client: SOII Plus Phone: 252-883-9301
MERITECH, INC.
PO Box 1396 919-690-1157
Address: Fax:
ENVIRONMENTAL LABORATORIES
Oxford, NC 27565 Email: samples@soilplus.net
°
642 Tamco Rd. Phone: 336-342-4748
Project: Town of Snow Hill
Reidsville NC 27320 Fax: 336-342-1522
P.O.#:
Email: info@meritech-labs,com
Turn Around Time*
Attention:
*RUSH wank needs prior approval.
How would you like your report sent?
0
www.meritech-labs.com
�a4
Circle all that apply: Email(preferred), Fax, Mail std(1Ddays) =[:!�f
X
Sampling Dates & Times
Person Taking Sample (Sign/Print);Drew Matthews
Lab Use Only
Sample Location
and/or ID #
5tart
End
°mp?
� °f
Test(s) Required
_On Ice?
Yes / Na
pH OK?
Date
Time
Date
Time
Grab.
Cont.
�
Cl OK?
SH 072920
7/29/20
41:1�0 ABM
G
3
VV
Residual Analysis (Al, Ammonia-N, As, Cd, Ca, Cu, Pb,
Mg, Hg, Mb, Ni, Nitrate -Nitrite N, %TS, pH, P, K, Se,
Na, TKN, Zn)
Temperature Upon
f l 11 Receipt:
*** t
Method of
** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Shipment:
Comments: please report Residual Analysis results in mg/kg
Compositor #
[] UPS
Please email results to samples@soiIplus, net Jug #
Q Fed Ex
Are these results for regulatory purposes? Yes 14
1�! 1
No ❑'. Report results in: mg/L t_a mg/kg I ug/L i,J
Hand Delivery
Relinquished by: Date: 1 Tlme:
N '1�L�1�2r1
Re ved ti Date: Time: 1
iZ:_,r. _ �•-d �:�'r°
Other
Re' quis d by: ate: / Tlme:
Received by: Date: Time:
Relinquished by: Date: Time:
Received h Lab: AA �3� te: Time: (�
Y .l } j 1C
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Drew Matthews
Report Date:
8/19/2020
Client: Soil Plus
P.O. Box 1396
Project:
Snow Hill
Oxford, NC 27565
Date Sample Revd:
7/29/2020
Meritech Work Order # 072920103 Sample: SH 072920 Grab
7/29/2020
1311-
TCLP Metals
Parameter
Results
Analysis Date
Det. Limit
Reg. Limit
Method
Arsenic
<0.100 mg/L
8/13/2020
0.100
5.0
EPA 200.7
Barium
0.349 mg/L
8/13/2020
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/13/2020
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/13/2020
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/13/2020
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/4/2020
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/13/2020
0.100
1.0
EPA 200.7
Silver
<0.050 mg/L
8/13/2020
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
Reporting Limit
Method
Volatiles 8260
Attached
7/31/2020
-
8260
Semi Vol. 8270
Attached
8/10/2020
-
8270
Other Tests
Parameter
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.49 %
8/10/2020
0-100 %
SM 2540B
Cyanide, total
<0.500 mg/kg
8/4/2020
0.500 mg/kg
EPA 335.4
Sulfide
2.05 mg/kg
8/3/2020
1.00 mg/kg
SM4500S2D
[gnitability
132.0 OF
8/6/2020
-
EPA 1030
Corrositivity (pH)
6.3 S.U.
8/10/2020
1.0 - 14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
i-*0 Laboratory Certification No.165
Page 2
Contact: Drew Matthews Report Date: 8/19/2020
Client: Soil Plus
P.O. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/29/2020
Meritech Work Order # 072920103 Sample: SH 072920 Grab 7/29/2020
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. -Limit Dilution Factor
Endrin
Attached - - -
Chlordane
Attached - - -
Toxaphene
Attached - - -
Methoxychlor
Attached - - -
Heptachlor
Attached - - -
Lindane
Attached - - -
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Attached
Attached
I hereby certify that I have reviewed and approve these data.
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
MERITECH, INC.
�- Environmental Laboratories
Laboratory Certificate #165
Client:
Project.
Client Sample ID:
Sample Collection:
Meritech Sample ID:
Soil Plus
Town of Snow Hill
SH 072920
07/29/20
072920103
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 07/31/20
Extraction:
07/30/20
Analyst: VWV
Report Date:
08/05/20
Parameter
Result
Units
Det. Limit
Re6. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/l,
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 08/10/20
Extraction:
07/30/20
Analyst: PM
Report Date:
08/12/20
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
]0
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentaeblorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2.4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. � t'CA//,-,///
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
(336) 342-4748 * info@meritechiabs.com
7
RESEARCh & ANALYTICAL � b .... •"
Fib 'W4'.
LABORATORIES, INC. ?KC#34 i
Analytical/Process Consultations 'a'16A °?rc �,h4
Toxicity Characteristic Leachate Procedure (TCLP) Analysis for Meritech, Inc., collected 29 July 2020)
072920103
EPA HW Quantitation Results Characteristic
Number Contaminant Limit(mg/L) (mg/L) Level(mg/L) EPA Method Analyst
I. TCLP PESTICIDESIHERBICIDES
D-020
Chlordane
D-016
2,4-D
D-012
Endrin
D-031
Heptachlor
D-013
Undane
D-014
Methoxychlor
D-015
Toxaphene
D-017
2,4,5-TP(Silvex)
Sample Number
Sample Date
Sample Time (hrs)
Sample Matrix
Date Analyzed
0.003
BQL
0.030
8081
MG
1.000
BQL
10.0
8151
MG- f
0.002
BQL
0.020
8081
Ma`
0.0008
BQL
0.008
8081
M
0.040
BQL
0.400
8081
1.000
BQL
10.0
8081
G
0.05
BQL
0.500
8081
MG
0.100
BQL
1.00
8151
MG
85357-01
07/29/20
1015
Sludge
08/05-08/I 1/2020
mglkg = milligams per kilogram = parts per million (ppm) BQL = Bolow Qwwtitation Limits
380.2013
Chain of Custody Record (COC)
NPDES#:
Client: Soil Plus Phone: 252-883-9301
Address: PO Box 1396 Fax: 919-690-1157
Oxford, NC 27565 Email: samples@soilplus.net
Project: Town of Snow Hill
P•O.#:
Attention: Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
$td (10 days) 3-5 Da s 74 - 4R Hrs
Circle all that apply: Email(preferrea), Fax, Mail � , F—=.
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: 336-342-4748
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs.com
� www.meritec ` G�y s.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print):Drew Matthews 9'�J V10-4
Lab Use Only
Start
End
Comp, .
Grab?
Hof
Cont.
Test(s)
Required
on Ice?
i�s / No
K?
pH O
Cl OK?
Date
Time
Date
Time
SH 072920
7/29/20
I,'-):i'5Art
G
3
Full TCLP (Ignitability, Corrositivity, Reactivity)
Temperature Upon
r Receipt:
Method of
Shipment:
*** Dechlorination (<O.S ppm) of Ammonia, Cyanide, Phenal
and TKN samples must be done in the field prior to preservation. ***(
Comments: please report TCLP results in mg/L
Please email results to samples@soilplus.net
Compositor#
Jug #
[] UPS
Fed Ex
Are these results for regula ory purposes?. Yes W
No O;
Report results in: mg/L mg/kg D ug/L Q
Hand Delivery
Relinquished by. Date; .�lU� j,�Time:
JJ rr
I .� 3t� ��
Wive y: / -" F a Time:
Q: Other
Re ipqu a by Date: Timer
�,( !�J el
Received by: Date: Time:
Relinquished by: Date: Tlme;
Received by Lab: % M L _gr�pate: Time: ) 2 0
Town of Snow Hill
2020 Class B Annual Report
WQ Permit# WQ0011448
Land Application Field Summary Form
PernutNumber WQ0011448
Facility Name Town of Snow Hill
LandOwner Town of Snow Hill
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# SH County Greene Crop 1 Common Bermudagrass Hay
Field Name 3 SoilSeries Autryville Crop 1 Pan 196
Acres Permited 11.40 Soil Abbrevation: AuB Crop 2 Annual Ryegrass - Hay
Crop 2 Pan 50
Volume
Acres Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied
% Solids Used DT/Ac. Tons Source
Condition Precip
Method
P Volatilization Mineralization
TKN Ammonia -Nitrite PAN
PAN Crop
03/30/2020 Gallons 130,000
3.04 11.40 1.45 16.48 Town of Snow Hill WWTP
Moist < 0.5"
Surface
91.65 0.50 0.3
32,000 3,120.00 329.00 30.51
Crop 1
07/29/2020 Gallons 118,400
3.04 11.40 1.32 15.01 Town of Snow Hill WWTP
Dry < 0.5"
Surface
83.47 0.50 0.3
32,000 3,120.00 329.00 27.79
Crop 1
Total Volume Applied
248,400
Total Dry Tons 31.49
Sum Total P 175.12
Total 58.30
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.009
0.007
3.326
0.189
0.016
0.028
0.134
0.009
4.707
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.177
0.076
30.120 2.335
1.836
0.145
0.263
1.256
0.227
36.810
Cumulative Total
0.186
0.083
33.446
2.025
0.161
0.291
1.390
0.236
41.517
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
Jinx S�4L **Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
1-21-2021 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date
Town of Snow Hill
2020 Class B Annual Report
WQ Permit# WQ0011448
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Geometric Mean
30-Day Bench Scale Test
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Snow Hill WQ Permit Number: WQ0011448
WWTP Name: Town of Snow Hill WWTP NPEDS Number: NCO020842
Monitoring Period: 01/01/2020 to 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 300 672 2,093 0 Annually Grab Samples
Weight)
Analytical Technique SM 9222 D
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
I requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
h
'l Jason Smith Vl'
ca C
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer*
1 /21 /2021
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Drew Matthews Report Date: 8/3/2020
Client: Soil Plus
P.O. Box 1396 Project: Town of Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/29/2020
Meritech Work Order # 07292095 Sample: SH 072920 (001) Grab 7/29/20
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 3.02 % 7/30/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,505 col/g dry wt 7/29/20 130 col/g dry wt SM 9222D B7
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
07292096 Sample: SH 072920 (002) Grab
Results Analysis Date Reporting Limit
3.03 % 7/30/20 0-100 %
300 col/g dry wt 7/29/20 130 col/g dry wt
7/29/20
Method
SM 2540B
SM 9222D
Qualifier
B7
Meritech Work Order #
07292097 Sample: SH 072920 (003) Grab
7/29/20
Parameters
Results Analysis Date Reporting Limit
Method
Qualifler
% Total Solids
3.01 % 7/30/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
604 col/g dry wt 7/29/20 130 col/g dry wt
SM 9222D
B7
Meritech Work Order #
07292098 Sample: SH 072920 (004) Grab
7/29/20
Parameters
Results Analysis Date Reporting Limit
Method
Qualifier
%Total Solids
3.02 % 7/30/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
602 col/g dry wt 7/29/20 130 col/g dry wt
SM 9222D
B7
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
07,
�10
Page 2
Contact: Drew Matthews Report Date: 8/3/2020
Client: Soil Plus
P.O. Box 1396 Project: Town of Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/29/2020
Meritech Work Order # 07292099
Parameters
Results
Sample: SH 072920 (005) Grab 7/29/20
Analysis Date Reporting Limit Method Qualifler
% Total Solids 3.03 % 7/30/20 0-100 % SM 2540B
Fecal Coliform. (Sludge) <300 col/g dry wt 7/29/20 300 col/g dry wt SM 9222D B7
Meritech Work Order # 072920100 Sample: SH 072920 (006) Grab 7/29/20
Parameters Results Analysis Date Reporting Limit Method Qualifier
% Total Solids 3.03 % 7/30/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 600 col/g dry wt 7/29/20 130 col/g dry wt SM 9222D B7
Meritech Work Order # 072920101 Sample: SH 072920 (007) Grab 7/29/20
Parameters
% Total Solids
Fecal Coliform (Sludge)
Results Analysis Date Reporting Limit Method Qualifier
304 % 7/30/20 0-100 % SM 2540E
2,093 col/g dry wt 7/29/20 130 col/g dry wt SM 9222D B7
B7 Many non-coliform colonies or interfering non-coliform growth present. in this competitive situation, the
reported coliform value may under -represent actual coliform density.
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
3.zo.zo3 Chain of Custody Record (COC)
NPDES#:
Client: Soil Plus Phone: 252-883-9301
Address: PO Box 1396 Fax: 919-690-1157
Oxford, NC 27565 Email: samples@soilplus.net
Project: Town of Snow Hill
P•O•#:
Attention: Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email (preFerred], Fax, Mail Std(s) 3-s Days 14-4AHrs
MERITECH, INC.
a - ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: 336-342-4748
Reidsville NC 27320 Fax: 336-342-1522
Email: info@meritech-labs.com
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): Drew MatthewsA-�:2L�Lab
Use Only
Start
End
pomp?
Grab?
Hof
Cont,
Tests
Required
Re `�
on Ice?
�
�"$ / No
pH OK?
Cl OK?
Date
Time
Date
Time
SH 072920 (00 ])
7/29/20
q'S-o AM
G
1
Fecal Coiiform / % Total Solids
SH 072920 (002)
7/29/20
tj':32 flex
G
1
Fecal Coliform / % Total Solids
SH 072920 (003)
7/29/20
��'. js�,�
G
1
Fecal Coliform / % Total Solids
SH 072920 (004)
7/29/20
'. n,M
G
1
Fecal Coliform I % Total Solids
SH 072920 (005)
7/29/20
Cf. Llo W,1
G
1
Fecal Coliform 1 % Total Solids C
SH 072920 (006)
7/29/20
r}'.ij3.Ap,-t
G
1
Fecal Coliform / % Total Solids I"
SH 072920 (007)
7/29/20
4M
G
1
Fecal Coliform ! % Total Solids
Temperature Upon
C Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Comments;
Please email results to samples@soilplus.net
Compositor #
Jug #
UPS
Q_ Fed Ex
Are these results for regulatory purposes? Yes 1Z No
Report results In: mg/L Q• mg/kg M, ug/L Q
Q Hand Delivery
Relinquished by: Date: 1 ' Time: f •7
'7 29 2�
Removed i Date: Time!
/ t 3
Other
R . u e qd by pate: Time
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab:k V) te: Time: I 1
J �N `ti -.
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Drew Matthews Report Date: 8/28/2020
Client: Soil Plus
P.Q. Box 1396 Project: Snow Hill
Oxford, NC 27565 Date Sample Rcvd: 7/29/2020
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 072920104 Sample: SH 072920 Grab 7/29/20
Total Solids Volatile Solids % Volatile Solids
Week 1 0.980 0.720 0.734
Week 2 1.01 0.750 0.739
Week 3 0.870 0.650 0.747
Week 4 1.12 0.790 0.700
Week S 0.880 0.640 0.726
Mass Balance Equation =1.03% Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
I hereby certify thatl have reviewed and approve these data. -Amndo' NoUC00A,
Laborato Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342-4748 fax.(336)342-1522
3.zo.zo��
Chain of Custody Record (COC)
NPDFS#:
Client: Soil Plus Phone: 252-883-9301
Address: PO Box 1396 Fax: 919-690-1157
Oxford, NC 27565 Email: samples@soilplus.net
Project: Town of Snow Hill
P.O.#:
Attention: Turn Around rime*
Now would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email(prererredj, Fax, Mail Std(10days) 3-5 o74�s
X
MERITECH, INC,
ENVIRONMENTAL LABORATORIES
i
-"'. 0 W
642 Tamco Rd, Phone: 336-342-4748
Reidsville NC 27320 Fax; 336-342-1522
Email: info@meritech-Iabs.com
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Drew Matthews V/ Q
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test(s) Required
on Ice?
Yis / No
pH OK?
Cl OK?
Date
Time
Date
Time
SH 072920
7/29/20
jQ-oD rkl-,,
G
1
30 Day Bench Scale Test
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
a —
Comments:
Please email results to samples@sollplus.net
Compositor #
[� UPS
jug #
Q Fed Ex
Are these results for regulat; ry purposes? Yes f�J
No CJ.
Report results in: mg/L 0 mg/kg Q' ug/L El
Hand Delivery
Relinquished by:
Date; n Tlme: , J
7)<'L•�7v Z• > �r�
R €ve ' y: +, Date: Time:
�•.. ��6''
Other
Rainq i' ed byf Da e: 1 Time:
•G� f� - f C/ �-) •'
Received by: Date: Time:
Relinquisher) by: Date: Tlrne:
Received by Lab: jn Time:
j l �,
Town of Snow Hill
2020 Class B Annual Report
WQ Permit# WQ0011448
Soil Samples
Page 1 of 1
Report No: 20-316-0581
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms Inc
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax 252-206-9973
www.waypointanalytical.com
Farm: Snow Hill
Date Received: 11/11/2020
Date of Report: 11/13/2020
Lab No Field ID Sample ID
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
107753 3
MIN 0.1 4.7
3.0
294
31
27
56
70 0 410 410 365 4.7 37 27 6 0.7 0
Crop Recommendations:
Rec Uom Lime (Vacre)
N
P205
K20
S
Mn
Zn Cu B Mg Last Crop
1- Bermudagrass Hay
lb/acre 2.1
200
0
159
0
0
0 0 0
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.