WQ0041666_Modification_20210225

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0041666
Applicant/Permittee EMA Resources, Inc
Applicant/Permittee Address 755 Yadkinville Rd, Mocksville, NC 27028
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Organization
Facility Name EMA Resources DCAR
County Davie
Fee Category Minor
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $245
Complete App Date 02/25/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Kendall
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
c Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363993646
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
WQ0041666
Fbs Current Existing permt number
Applicant/Permittee *
EMA Resources, Inc.
Applicant/Permittee Address*
755 Yadkinville Rd, Mocksville, NC 27028
Facility Name *
EMA Resources DCAR
Please provide comments/notes
on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spec'rfications, Calculations, Rc.)
EMA Resources Permit Modification - WQ0041666.pdf 4.33MB
Upload only 1 RCFdocurrent (less than 250 M3). Ma@iple documents nest be combined into one RDFfile unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date
ff &Oaw
2/19/2021

g
Inc.
Permit Modification
For
EMA Resources Inc. - WQOO41666
Distribution of Residual Solids
(503 Exempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
February 19, 2021
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

February 19, 2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Modification — WQ0041666
To Whom it May Concern:
EMA Resources is submitting the included permit modification for the EMA Resources
Inc. — DCAR Permit WQ0041666. We are asking to have the Piedmont Water Facility
added as a source to our distribution permit. They are currently a source on Synagro
Inc.'s permit. We do not have a copy of their permit. A check for $245.00 is being mailed
along with a hard copy of this modification.
If you have any questions concerning this modification, please contact Brent Collins —
Director of Technical Services
Respectfully,
Brent Collins
Director of Technical Services
brent.collins(cr�,emaresourcesinc.com
[phone]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

Current Permit

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. DANI£L SMITH
Director
ERIK BLANKENSHIP — PRESIDENT
EMA RESOURCES, INC.
755 YADKINVILLE ROAD
MOCKSVILLE, NORTH CAROLINA 27028
Dear Mr. Blankenship:
NORTH CAROLINA
Environmental Quality
July 16, 2020
Subject: Permit No. WQ0041666
EMA Resources DCAR
Distribution of Class A
Residuals
Davie County
In accordance with your permit application request received May 5, 2020, we are forwarding
herewith Permit No. WQ0041666 dated July 16, 2020, to EMA Resources, Inc. for the operation of the
subject residuals management program.
This permit shall be effective from the date of issuance through January 31, 2027, and shall be
subject to the conditions and limitations as specified therein. The Permittee shall submit a renewal
application no later than August 4, 2026.
Please pay particular attention to the monitoring requirements listed in Attachment A. Failure to
establish an adequate system for collecting and maintaining the required operational information shall result
in future compliance problems.
If any parts, requirements, or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Erick Saunders at (919)
707-3659 or erickson.saunders&ncdenr.gov.
Sincerely,
S. Daniel Smith, Director
Division of Water Resources
cc: Duplin County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Roy Whitaker — EMA Resources, Inc. (Electronic Copy)
N11H fH (:A�i(1!.INA �
D E Q North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617
0­O'torenwm­talQ"I 919,707.9000

Mr. Erik Blankenship
July 16, 2020
Page 2 of 2
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
ENIA Resources, Inc.
Davie County
FOR THE
operation of a residuals management program for EMA Resources, Inc. and consisting of the distribution
of Class A residuals generated by the approved facility listed in Attachment A, with no discharge of wastes
to surface waters, pursuant to the application received May 5, 2020, and in conformity with other supporting
data subsequently filed and approved by the Department of Environmental Quality and considered a part
of this permit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503.
This permit does not exempt the Permittee from complying with Federal Regulation 40 CFR Part 503.
This permit shall be effective from the date of issuance through January 31, 2027, and shall be subject to
the following conditions and limitations:
L SCHEDULES
1. The Permittee shall request renewal of this permit on Division -approved forms no later than August 4,
2026. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
The Permittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distributing residuals, take immediate corrective actions, and contact the Winston-Salem Regional
Office supervisor. [15A NCAC 02T .0108(b)(1)(A)]
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)]
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [15A NCAC 02T .1101]
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4. Pollutant concentrations in distributed residuals shall not exceed the following Ceiling Concentrations
or Monthly Average Concentrations, on a dry weight basis:
Parameter
Ceiling Concentration
Monthly Average
Concentration
img/w
(mg1kg)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
N/A
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T .1105(a), 02T .1105(c)]
5. Class A biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T
.1106(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1106(a), 02T .1106(d)]
6. Class A biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T .1107(c)]
7. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class A land application sites are as follows (all distances in feet):
Liquid Cake
Residuals Residuals'
I. Each private or public water supply source:
100
100
ii. Surface waters such as intermittent and perennial streams, perennial
100
25
waterbodies, and wetlands:
iii. Surface water diversions such as ephemeral streams, waterways, and
25
0
ditches:
iv. Groundwater lowering ditches where the bottom of the ditch
25
0
intersects the SHWT:
v. Each well with exception of monitoring wells:
100
100
vi. Bedrock outcrops:
25
0
' Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported
and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast
spreader or other equipment designed for handling solid materials) without leaving any
significant liquid fraction behind.
[15A NCAC 02T .1108(b)]
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8. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soll.ncsu.edl /yields/index.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group -Guidance
Document: Chapter 1
(http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
In. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T . I 109(a)(1)(K)]
9. Prior to distributing Class A residuals that have a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. The Permittee
shall notify third -party entities of the effects of a high SAR content residuals on their receiving sites.
[I5A NCAC 02T .0 1 08(b)(1)(A)]
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III. OPERATION AND MAINTENANCE REQUIREMENTS
1. The Permittee shall operate and maintain the residuals management program as anon -discharge system.
[15A NCAC 02T .1100]
2. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by whom the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
I. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
e. Detailed inspection procedures:
I. Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f Detailed sampling and monitoring procedures:
I. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[15A NCAC 02T .I I I0(a)]
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .0204]
4. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying bulk Class A residuals. [15A NCAC 02T .1110(b)]
5. The Permittee shall ensure that spill control provisions are available when transporting or land applying
bulk Class A residuals. [15A NCAC 02T .1110(a)(4)]
6. Class A residuals may be staged at the land application site for up to 30 days for biological residuals
and 60 days for non -biological residuals. Class A residuals shall be stored or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [15A NCAC 02T .1110(c), 02T .1110(d)]
7. Adequate measures shall be taken to prevent wind erosion and runoff from the bulk Class A residual
land application sites. [15A NCAC 02T .0108(b)(1)(A)]
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8. Bulk Class A residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
f During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot;
k. If the application exceeds agronomic rates; or
1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B .0212
or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .0215, and .0216.
[15A NCAC 02T. I 109(a)(1), 02T. I 109(b)]
9. The Permittee shall notify all third -party entities receiving bulk Class A residuals that land application
activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T
.1108(b) and 02T .1109(a)(1) (i.e., Conditions IL7.a. and III.8., respectively). [15A NCAC 02T
.1103(a)(4), 02T .1103(a)(5)]
10. Bagged or other container Class A residuals shall have an affixed label or an information sheet provided
to the person receiving the Class A residuals. The label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[15A NCAC 02T. I 109(c)]
11. The Permittee shall not distribute bulk Class A residuals to any person or entity known to be applying
residuals contrary to the conditions of this permit. The Permittee shall report to the Winston-Salem
Regional Office any person or entity known to be applying residuals contrary to the conditions of this
permit. [15A NCAC 02T .0108(b)(1)(A)]
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IV. MONITORING AND REPORTING REQUIREMENTS
The Permittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [15A NCAC 02T .0108(c)]
2. The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be
performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Heptachlor (and its epoxide)
(0.008)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlorobutadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
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3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T .1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class A pathogen reduction
requirements in 15A NCAC 02T .1106(a), and one vector attraction reduction requirement in 15A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106(a), 02T .1107(a), 02T .1111(c)]
5. Representative samples of residuals that are prepared for distribution shall be collected and analyzed.
[15A NCAC 02T .1I I I(a)]
6. The Permittee shall maintain records for all bulk Class A residual distribution events. These records
shall include the following:
a. Residuals source (as listed in Attachment A);
b. Date of distribution;
c. Name and address of residuals recipient;
d. Volume of residuals distributed to each recipient; and
e. Intended use of residuals.
[15A NCAC 02T .010g(c)]
7. One hard copy and one electronic copy of an annual report shall be submitted on or before March 1st
The annual report shall meet the requirements described in the Instructions for Residuals Application
Annual Reporting Forms. Instructions for reporting and annual report forms are available at
httD:Hdea .nc. eov/about/divisions/water-resources/water-resources-hermits/wastewater-branch/non-
discharge-permitting-unit/reportin -fg orms, or can be obtained by contacting the Non -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .I I I1(d)]
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8. Noncompliance Notification
The Permittee shall report to the Winston-Salem Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Distribution of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Winston-Salem Regional Office within
five days of first knowledge of the occurrence, and this report shall outline the actions proposed or
taken to ensure the problem does not recur. [15A NCAC 02T .0108(b)(1)(A)]
V. INSPECTIONS
1. The Permittee shall perform inspections and maintenance to ensure proper operation of the Permittee's
storage and distribution facilities. [15A NCAC 02T .1110(f)]
2. The Permittee shall inspect the Permittee's residuals processing, storage, and transport facilities to
prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes
to the environment, threats to human health, or public nuisances. The Permittee shall maintain an
inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[15A NCAC 02T .0108(b)(1)(A), 02T .1110(f)]
3. Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the distribution sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
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VL GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.613, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215.1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T .0105(n)]
4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15A NCAC 02T .0105(c)(6)]
If the permitted residuals program change ownership, or the Permittee changes their name, the
Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terms and conditions of this permit until the permit is transferred to the successor -
owner. [G.S.143-215.1(d3)]
6. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter
02T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials:
I. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii. to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[15A NCAC 02T .0110]
WQ0041666 Version 1.0 Shell Version 200201 Page 9 of 10

7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S. 143-215.6B, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or
exhausted.
b. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Permittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual
fee.
[15A NCAC 02T .0120(b), 02T .0120(d)]
8. This permit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee.
[15A NCAC 02T .0120(c)]
Permit issued this the 16'h day of July 2020
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Daniel Smith, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0041666
WQ0041666 Version 1.0 Shell Version 200201 Page 10 of 10

ATTACHMENT A — APPROVED RESIDUAL SOURCES
EMA Resources, Inc.
Certification Date: July 16, 2020
Permit Number: WQ0041666 Version: 1.0
Monitoring
Monitoring
Monitoring
Permit
Biological
Maximum
Frequency for
Frequency for
Frequency for
Approved
Owner
Facility Name
County
Number
Residuals
Dry Tons
Non -hazardous
Metals and
Pathogen &
Mineralization
per Year'
Characteristics z
Nutrients
Vector Attraction
Rate
Reductions 4, s, 6
Lear Corporation
Lear Corporation WWTP
Duplin
NC0002305
Yes
318
Annually
Annually
Annually
0.3
Total
318
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen reductions as stipulated under permit Condition IVA.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Applied
Monitoring Frequency
Dry Tons Applied (metric tons)
(short tons per year)
(40 CFR 503 and 15A NCAC 02T
.1111 c
< 290
< 319
Once per year (Annually)
> 290 to < 1,500
> 319 to < 1,650
Once per quarter (4 x Year)
> 1,500 to < 15,000
> 1,650 to < 16,500
Once per 60 days (6 x Year)
> 15,000
> 16,500
Once per month (12 x Year)
6. Residuals are generated during the biological treatment of industrial wastewater with an estimated 1% domestic waste stream contribution, and meet the definition of "Biological Residuals" as
defined in 15A NCAC 02T .1102(6). However, it was demonstrated that the residuals are pathogen free and are not required to monitor for Vector Attraction Reduction in accordance with 15A
NCAC 02T . 1107(c) provided that no significant odor complaints or problems with vector attraction are encountered at the land application site and Fecal Coliform Concentrations remain less than
1,000 MPN per dry gram of residuals.
If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is
required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to United States Environmental
Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information.
WQ0041666 Version 1.0 Attachment A Page 1 of 1

DCAR Form

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
L APPLICANT INFORMATION:
1. Applicant's name: EMA Resources Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership E:1 Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Erik Blankenship Title: President
Applicant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] Email Address: erik.blankenshipa emaresourcesinc.com
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip: -
Telephone number: (_) _- Email Address:
3. Fee submitted: $245.00 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00041666
Date of most -recently issued permit: 07/16/2020
Date of most -recently certified Attachment A (if different than the permit): 07/16/2020
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Piedmont Triad Regional Water Authority_
City: Randleman State: NC Zip: 27317-_
Coordinates: Latitude: 35' 51' 52" Longitude: 79. 49' 15"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
County where facility is located: Randolph
2. Facility contact (person familiar with residuals preparation):
Name: Greg Flory Title: Superintendent
Mailing address: PO Box 1326
City: Randleman State: NC Zip: 27317-
Telephone number: [phone] E-mail address: gfloryLc/ptrwa.org
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; p No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: days (Note: the Division requires minimum 30 days storage in units that are
separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); land applied at agronomic rates
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 1035 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 1035 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): 90 days
6. Does the facility have a stormwater management plan? ® Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: There is a drain in
each section of the storage area that flows to a lift station which then pumps it back to the thickener.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
0
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
L , attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Sea], Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ® No, Explain; Ka
I, Erik Blankenship - President
[Signature Authority's Name— PLEASE PRfNT) (Title)
attest that this application for
EMA Resources i
(Facility Name)
has been reviewed by me and is accurate and complete to the hest of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
TSignature: Date:
FORM: DCAR 06-16 Page 3 of 3

RSC Form

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: EMA Resources Inc.
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
N
Synagro
Piedmont Water
Randolph
1035
1035
'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Piedmont Triad Regional Water Authority_
2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ® Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: _).
3. Facility contact person and title: Greg Flory
Complete mailing address: PO Box 1326
City: Randleman State: NC Zip: 27317-
Telephone number: [phone] E-mail address: gflory&ptrwa.or
4. Facility physical address: 7297 Adams Fard Rd
City: Randleman State: NC Zip: 27317-
Coordinates: Latitude: 35' 51' 52" Longitude: 79. 49' 14"
Datum: NAD83 Level of accuracy: nearest second
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 14.7 MGD and facility average daily flow: 11.1 MGD
8. Average amount of residuals being generated at this facility 1035 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 875,00 gallon equalization basin, 450,000 decant basin, 450,000 sludge thickener
Type and volume of residuals storage (i.e., outside of residuals treatment units): 9600 square feet uncovered sludge storage
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Eaton Analytical and Date of analysis: 12/8/2020
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: >179 OF (> 140°F)
Passed reactivity test: W yes Eno. HCN: Ph"' mg/kg (<250) & H2S: ' ' mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mg/1)
Arsenic
5.0
<0.03
Hexachlorobenzene
0.13
<0.0025
Barium
100.0
0.23
Hexachloro-1,3-Butadiene
0.5
<0.01
Benzene
0.5
<1
Hexachloroethane
3.0
<0.025
Cadmium
1.0
<0.005
Lead
5.0
<0.015
Carbon Tetrachloride
0.5
<1
Lindane
0.4
<0.0005
Chlordane
0.03
<0.0025
Mercury
0.2
<0.2
Chlorobenzene
100.0
<1
Methoxychlor
10.0
<0.0005
Chloroform
6.0
<1
Methyl Ethyl Ketone
200.0
<10
Chromium
5.0
0.0044
Nitrobenzene
2.0
<0.01
m-Cresol
200.0
Pentachlorophenol
100.0
<0.025
o-Cresol
200.0
<0.01
Pyridine
5.0
<0.025
p-Cresol
200.0
<0.01
Selenium
1.0
<0.05
Cresol
200.0
<0.01
Silver
5.0
<0.01
2,4-D
10.0
Tetrachloroethylene
0.7
<1
1,4-Dichlorobenzene
7.5
<0.01
Toxaphene
0.5
<0.015
1,2-Dichloroethane
0.5
<1
Trichloroethylene
0.5
<1
1,1-Dichloroethylene
0.7
<1
2,4,5-Trichlorophenol
400.0
<0.01
2,4-Dinitrotoluene
0.13
<0.01
2,4,6-Trichlorophenol
2.0
<0.01
Endrin
0.02
<0.00010
2,4,5-TP (Silvex)
1.0
<0.005
Heptachlor and its Hydroxide
0.008
<0.000050
Vinyl Chloride
0.2
<1
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 01/21/2021
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
14.6
Cadmium
85
39
15.8
Copper
4,300
1,500
74.3
Lead
840
300
12.5
Mercury
57
17
0.0416
Molybdenum
75
n/a
25.2
Nickel
420
420
9.1
Selenium
100
100
10.3
Zinc
7,500
2,800
12.6
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 24.5 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 01/21/2021
Parameter
Result
(mg1kg)
Aluminum
9800
Ammonia -Nitrogen
976
Calcium
2490
Magnesium
588
Nitrate -Nitrite Nitrogen
<17.6
pH (Standard Unit)
4.9
Phosphorus
1480
Potassium
245
Sodium
394
Total Kjeldahl Nitrogen
6040
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.91
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
2531
3746
Injection/Incorporation
3019
4234
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, 9 air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of

Vicinity Map

Pr 00, a.-
OUALL 1 " = 660'
DATE 02-18-21
DRAWN BY: BC1
gritin-M
to -
A'
jk"
A,
riijgggitui be, Ge Eje, Property Boundary
"-M
Randleman Regional Reservoir FIGURE NO.
1!FMA Piedmont Triad Regional Water Authority 2
esources, Inc. I

Process Flow

JFK Water Treatment Plant Process Flow Schematic

Quantitative Justification

Quantitative Justification for Residuals Production Rate
Facility:
Piedmont Water
Requested Permitted Rate:
1135 dry tons/year
Justification:
We are estimating 1135 dry tons of water plant residuals
Calculations:
(5,500 cubic yard) x (24.5% solids) x (16.85 weight of water/cubic yard) = 1135 dt/yr

Analytical Information

Waypointo
ANALYTICAL
2/1 /2021
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 21-022-0131
Client Project Description: PTRWA
Randleman, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/22/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
06/30/2021
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program
- NELAP
LA037
12/31/2021
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2021
Page 1 of 1 00001/21-022-0131
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 21-022-0131
Client Project Description: PTRWA
Randleman, NC
Lab No Client Sample ID
88717 PTRWA WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected
Solids 01/21/202110:00
Date Received
O1/22/2021
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: PTRWA
Lab Report Number: 21-022-0131
Date: 1 /29/2021
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Analyte: Calcium
QC Batch No: L533538
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L533538
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L533538
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 21-022-0131
Lab No : 88717
Sample ID : PTRWA WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project PTRWA
Information : Randleman, NC
REPORT OFANALYSIS
Report Date : 02/01/2021
Received : 01/22/2021
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/21/2021 10:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
75.5
%
0.010
1
01/25/21 16:34
FMM
SW-DRYWT
Ammonia Nitrogen
976
mg/Kg -
dry
102
102
1
01/29/21 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<17.6
mg/Kg -
dry
17.6
17.6
1
01/27/21 15:46
ZBD
4500NO3F-2011
Organic N
5065
mg/Kg -
dry
249.4
502.0
1
01/28/21 15:36
CALCULATION
pH
4.9
S.U.
1
01/28/2114:50
CxC
9045D
Total Solids
24.5
%
0.010
0.010
1
01/25/21 16:34
FMM
2540G-2011
Total Volatile Solids
33.4
%
0.010
0.010
1
01/25/21 16:34
FMM
2540G-2011
Total Kjeldahl Nitrogen
6040
mg/Kg -
dry
502
1
01/28/21 15:36
CLP
4500NORGD-2011
Phosphorus
1480
mg/Kg -
dry
11.3
20.4
1
01/28/21 01:56
TJS
6010D
Aluminum
9800
mg/Kg -
dry
18.9
20.4
1
01/28/21 01:56
TJS
6010D
Arsenic
14.6
mg/Kg -
dry
0.979
2.04
1
01/28/21 01:56
TJS
6010D
Cadmium
15.8
mg/Kg -
dry
0.0816
0.408
1
01/28/21 01:56
TJS
6010D
Calcium
2490
mg/Kg -
dry
158
204
1
01/28/21 01:56
TJS
6010D
Chromium
3.37
mg/Kg -
dry
0.963
1.02
1
01/28/21 21:37
TJS
6010D
Copper
74.3
mg/Kg -
dry
1.27
2.04
1
01/28/21 01:56
TJS
6010D
Iron
465000
mg/Kg -
dry
694
816
20
01/28/21 21:47
TJS
6010D
Lead
12.5
mg/Kg -
dry
0.734
1.22
1
01/28/21 01:56
TJS
6010D
Magnesium
588
mg/Kg -
dry
10.5
20.4
1
01/28/21 01:56
TJS
6010D
Manganese
2190
mg/Kg -
dry
6.65
10.2
5
01/28/21 21:42
TJS
6010D
Mercury
0.04163
mg/Kg -
dry
0.0131
0.0592
1
01/28/21 13:29
DDB
7471A
Molybdenum
25.2
mg/Kg -
dry
0.551
1.02
1
01/28/21 01:56
TJS
6010D
Nickel
9.10
mg/Kg -
dry
0.489
1.02
1
01/28/21 01:56
TJS
6010D
Potassium
245
mg/Kg -
dry
25.2
40.8
1
01/28/21 01:56
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 21-022-0131
Lab No : 88717
Sample ID : PTRWA WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project PTRWA
Information : Randleman, NC
REPORT OFANALYSIS
Report Date : 02/01/2021
Received : 01/22/2021
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/21/2021 10:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
10.3
mg/Kg - dry
1.31
2.04
1
01/28/21 21:37
TJS
6010D
Sodium
394
mg/Kg - dry
53.1
102
1
01/28/21 01:56
TJS
6010D
Zinc
12.6
mg/Kg - dry
3.31
5.10
1
01/28/21 01:56
TJS
6010D
Sulfur
4730
mg/Kg - dry
21.1
40.8
1
01/28/21 01:56
TJS
6010D
Sodium Absorption Ratio
0.91
Ratio
0.01
0.01
1
01/28/21 01:56
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 21-022-0131
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#100
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ory Phillips Date & Time: 01/22/2021 15:03:31
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
EMA Resources Inc
Brent Collins
Account #46�45
For Laboratory Use Only
755 Yadkinville Rd
Mocksvilie, NC 27028
Project Description
Projeet/slte Location (City/State)
�R'USH'-AddlV.naI char es a I of Shi!s PP Y pment
cial Detection limit{s] Fed fx
NiW -Key
P'17'�tDate
Results Needed
❑upS ❑L15PS
Courier ❑Client Drop Off
1n1W -Wastewater GW -Groundwater
DW-Drinking Water S-Soil/50d D-Oil
t�!
{
P-Product M-Mist
Other
Project Number
Project Manager Phonefl
Project Manager Email
Purchase Order Number
Site/FaciliIV ID A
336-399-3646
[e-mail]
M z
fn
A Cool c 10r Na25203 (Micro ❑niq)
aypoi nt.
C
« CJ C U
�
Coal ra 6C
ANALYTICAL
Y
❑
� � �
E tQ E
O
C H2504 pHci
D Nome Required
2790 Wbitteu Road
u y
v E D
e Naorlpwta
Memphis. TN 38133
c
Unless noted, all containers �
Q
� C4 Z to
a
F HNQ3pHs2
G HCt pHr2
[phone]
per Table If of 40 CFR Part M
r`�
a
H HBP04 pH<2
136. y
Z
f —
1 Cool K= GC NAZZ03
Date Time
Identification z
Requ ed Anal sis /Preservative
Commentr dates
IAA drQ9
}Sa�m]ple
Q
[.CJ► f l�'i �I
Meials:Af,As,Ca,Cd,Cr,Cu,Fe,Pb
M n, Mg, Mo, Hg, Ni, Se,Na, P,S, K,Zn
IIII I IIIII Ilil Ilf�l �IIII�IIIIII II I �II I III ���II III I� 46245
I
EMA Resourcas Ine
021
15:02'47
P Rv\fA
For Laboratory Use Only Sa Ivy (ma e - Print)
Client RemarkslCommants
Ice Custody
Seals
! Y%N
Rah Comments
o�
T
Sludge Samples -
Report Dry Weight
C-•
Y
Relirt
e Tirrle Received by: [SIGNATURE] Date Time
Blank oolerTe
Rel na,, d by: (SIGNATURE)
batd Time Receive V. [SI A
HE] pate Time
aL 1�
Relinquished by: (SIGNATURE]
Date Time Re d [SFG
REf pa 'i'i e
f
'' 7
•
(L

ti% eurofins
Eaton Analytical
LABORATORY REPORT
If you have any questions concerning this report, please do not hesitate to call us at
[phone] or [phone].
This report may not be reproduced, except in full, without written approval from EEA.
Page 1 of 31

ti% eurofins
Eaton Analytical
STATE CERTIFICATION LIST
State
Certification
State
Certification
Alabama
40700
Missouri
880
Alaska
IN00035
Montana
CERT0026
Arizona
AZ0432
Nebraska
NE-OS-05-04
Arkansas
IN00035
Nevada
IN00035
California
2920
New HampshirE
2124
Colorado
IN00035
New Jersey*
IN598
Colorado Radiochemistry
IN00035
New Mexico
IN00035
Connecticut
PH-0132
New York'
1398
Delaware
IN035
North Carolina
18700
Florida(Primary AB)*
E87775
North Dakota
R-035
Georgia
929
Ohio
87775
Hawaii
IN035
Oklahoma
D9508
Idaho
IN00035
Oregon*
4156
ilinois*
200001
Dcnnexihianiay
FR-nnaar
Illinois Microbiology
17767
Puerto Rico
IN00035
Illinois Radiochemistry
IN00035
Rhode Island
LA000343
Indiana Chemist
C-71-01
South Carolina
95005
Indiana Microbiology
M-76-07
South Dakota
IN00035
Iowa
098
Tennessee
TN02973
Kansas'
Texas*
T104704187
Kentucky
90056
Texas/TCEQ
TX207
Louisiana*
A014
Utah*
IN00035
Maine
IN00035
Vermont
VT-8775
Maryland
209
Virginia*
460275
Massachusetts
M-IN035
Washington
C837
Michigan
9926
West Virginia
9927 C
Minnesot,
018-999-338
Wisconsin
999766900
Mississippi
IN035
Wyoming
IN035
EPA
IN00035
*NELAP/TNI Recognized Accreditation Bodies
Revision date: 09/29/2020
Page 2 of 31

ti% eurofins
Eaton Analytical
LABORATORY CASE NARRATIVE
Client: Piedmont Triad Regional Water Authority Report #: 506164CN
All method QC was within acceptance limits.
Note: Method TCLP analysis was performed by Eurofins Lancaster Laboratories
Environmental, Lancaster, PA.
Note: This report may not be reproduced, except in full, without written approval from
EEA.
12/23/2020
Authorized Signature Title Date
Page 1 of 1
Page 3 of 31

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins Lancaster Laboratories Env, LLC
2425 New Holland Pike
Lancaster, PA 17601
Tel: [phone]
Laboratory Job ID: 410-23421-1
Client Project/Site: PTRWA - NC
For:
Eurofins Eaton Analytical
110 S Hill Street
South Bend, Indiana 46617
Attn: South Bend Reports
Authorized for release by:
1212312020 9:27.51 AM
Barbara Weyandt, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Page 4 of 31
12
13
74

Client: Eurofins Eaton Analytical Laboratory Job ID: 410-23421-1
Project/Site: PTRWA - NC
Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD,
and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note
exceptions. Noncompliant quality control (QC) is further explained in narrative comments.
QC results that exceed the upper limits and are associated with non -detect samples are qualified but further
narration is not required since the bias is high and does not change a non -detect result. Further narration is
also not required with QC blank detection when the associated sample concentration is non -detect or more
than ten times the level in the blank.
Matrix QC may not be reported if insufficient sample or site -specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise
specified in the method.
Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are
confirmed unless attributed to a dilution or otherwise noted in the narrative.
Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency
requirements/permits.
Measurement uncertainty values, as applicable, are available upon request.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of
the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper
techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity,
however, unless sampling has been performed by a member of our staff. Times are local to the area of activity.
Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not
performed within 15 minutes of collection.
This report shall not be reproduced except in full, without the written approval of the laboratory. 0 VA
WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results
for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other
warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or
implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall
Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental
damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence
(either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins
Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no
legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no
purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental
which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster
Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order
submitted by client.
Barbara Weyandt
Project Manager
1212312020 9:27:51 AM
Page 2 of 28 FP2 2L3232

Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Laboratory Job ID: 410-23421-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
Surrogate Summary .......................................
9
QC Sample Results ........................................
11
QC Association Summary ...................................
18
Lab Chronicle ............................................
21
Certification Summary ......................................
22
Method Summary .........................................
23
Sample Summary .........................................
24
Chain of Custody ..........................................
25
Receipt Checklists .........................................
28
12
13
74
Page 3 of 28
Eurofins Lancaster Laboratories Env, LLC
12PIWO20 32

Definitions/Glossary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greaterthan or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Qualifier Description
^5- Linear Range Check (LRC) is outside acceptance limits, low biased.
^5+ Linear Range Check (LRC) is outside acceptance limits, high biased.
B Compound was found in the blank and sample.
J Result is less than the RL but greaterthan or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
1C Result is from the primary column on a dual -column method.
2C Result is from the confirmation column on a dual -column method.
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA
Minimum Detectable Activity (Radiochemistry)
MDC
Minimum Detectable Concentration (Radiochemistry)
MDL
Method Detection Limit
ML
Minimum Level (Dioxin)
MPN
Most Probable Number
MQL
Method Quantitation Limit
NC
Not Calculated
ND
Not Detected at the reporting limit (or MDL or EDL if shown)
NEG
Negative / Absent
POS
Positive / Present
PQL
Practical Quantitation Limit
PRIES
Presumptive
QC
Quality Control
RER
Relative Error Ratio (Radiochemistry)
RL
Reporting Limit or Requested Limit (Radiochemistry)
RPD
Relative Percent Difference, a measure of the relative difference between two points
TEF
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
TNTC
Too Numerous To Count
Job ID: 410-23421-1
12
13
74
75
Eurofins Lancaster Laboratories Env, LLC
Page 4 of 28 FP2&3720232

Case Narrative
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Narrative
Job Narrative
410-23421-1
Job ID: 410-23421-1
Receipt
The sample was received on 12/9/2020 11:59 AM; the sample arrived in good condition, and, where required, properly preserved and on
ice. The temperature of the cooler at receipt time was 2.5°C
Receipt Exceptions
The Chain -of -Custody (COC) was incomplete as received and/or improperly completed. Analyses were not listed on COC. Entered
analyses based on attached bottle order.
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC/MS Semi VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page
F47
Herbicides M
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. MPesticides
Method 8081 B: The following sample was diluted due to the nature of the sample matrix: Sludge (410-23421-1). Elevated reporting limits
(RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
Method 1010A: The Pensky Martens closed cup apparatus is designed to determine the flash point of a liquid sample. The sample
submitted could not be mixed well enough to obtain uniform heating. The temperature being measured was that of the material near the
top of the cup. The material at the bottom of the cup could have a higher temperature. The temperature reported may not be accurate.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins Lancaster Laboratories Env LLC
Page 5 of 28 FWRW 6212

Detection Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Client Sample ID: Sludge Lab Sample ID: 410-23421-1
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac D
Method
Prep Type
Chloroform
39
20
4.0
ug/L
20
8260D
TCLP
Barium
0.23 B
0.0050
0.0010
mg/L
1
601OD
TCLP
Chromium
0.0044 J
0.015
0.0016
mg/L
1
601OD
TCLP
Flashpoint
>179
50.0
50.0
Degrees F
1
1010A
Total/NA
Paint Filter
No
No Unit
1
9095B
Total/NA
pH
5.7
0.01
0.01
S.U.
1
9045D
Soluble
This Detection Summary does not include radiochemical test results.
12
13
74
75
Eurofins Lancaster Laboratories Env, LLC
Page 6 of 28 FP2 ai3232

Client Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Client Sample ID: Sludge Lab Sample ID: 410-23421-1
Date Collected: 12/08/20 13:50 Matrix: Sludge
Date Received: 12/09/20 11:59
Method: 8260D -Volatile Organic Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Benzene
ND
20
4.0
ug/L
12/16/20 18:39
20
Carbon tetrachloride
ND
20
4.0
ug/L
12/16/20 18:39
20
Chlorobenzene
ND
20
4.0
ug/L
12/16/20 18:39
20
Chloroform
39
20
4.0
ug/L
12/16/20 18:39
20
1,1-Dichloroethene
ND
20
4.0
ug/L
12/16/20 18:39
20
1,2-Dichloroethane
ND
20
6.0
ug/L
12/16/20 18:39
20
2-Butanone
ND
200
6.0
ug/L
12/16/20 18:39
20
Tetrachloroethene
ND
20
4.0
ug/L
12/16/20 18:39 20
Trichloroethene
ND
20
4.0
ug/L
12/16/20 18:39 20
Vinyl chloride
ND
20
4.0
ug/L
12/16/20 18:39 20
Surrogate
%.Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
100
80- 120
12116120 18:39
20
4-Bromofluorobenzene (Surr)
95
80 - 120
12116120 18:39
20
Dibromofluoromethane (Surr)
97
80 - 120
12116120 18:39
20
Toluene-d8 (Surr)
100
80 - 120
12116120 18:39
20
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
2,4,5-Trichlorophenol
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
2,4,6-Trichlorophenol
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
2,4-Dinitrotoluene
ND
0.025
0.0050
mg/L
12/15/2010:00
12/16/20 14:08
1
2-Methylphenol
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
4-Methylphenol
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
Hexachlorobenzene
ND
0.0025
0.00050
mg/L
12/15/2010:00
12/16/20 14:08
1
Hexachlorobutadiene
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
Hexachloroethane
ND
0.025
0.0050
mg/L
12/15/2010:00
12/16/20 14:08
1
Nitrobenzene
ND
0.010
0.0025
mg/L
12/15/2010:00
12/16/20 14:08
1
Pentachlorophenol
ND
0.025
0.0050
mg/L
12/15/2010:00
12/16/20 14:08
1
Pyridine
ND
0.025
0.010
mg/L
12/15/2010:00
12/16/20 14:08
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Sum)
74
10- 150
12115120 10:00
12116120 14:08
1
2-Fluorobiphenyl (Surr)
76
44 - 102
12115120 10:00
12116120 14:08
1
2-Fluorophenol (Sum)
32
10 - 84
12115120 10:00
12116120 14:08
1
--------------------------------------------------------------------------------------------------------------------------------------------
Nitrobenzene-d5 (Surr)
75
23 - 128
12115120 10:00
12116120 14:08
1
p-Terphenyl-d14 (Surr)
80
31 - 113
12115120 10:00
12116120 14:08
1
PhenoW5 (Surr)
22
10 - 67
12115120 10:00
12116120 14:08
1
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Endrin (1C)
ND
0.0010
0.00040
mg/L
12/19/20 05:24
12/21/20 07:57
10
gamma-BHC (Lindane) (1C)
ND
0.00050
0.00010
mg/L
12/19/20 05:24
12/21/20 07:57
10
Heptachlor (1C)
ND
0.00050
0.00020
mg/L
12/19/20 05:24
12/21/20 07:57
10
-------------------------------------------------------------------------------------------------------------------------------------
Heptachlor epoxide (1C)
ND
0.00050
0.00012
mg/L
12/19/20 05:24
12/21/20 07:57
10
Methoxychlor (1 C)
ND
0.0050
0.0015
mg/L
12/19/20 05:24
12/21/20 07:57
10
Toxaphene (1C)
ND
0.15
0.050
mg/L
12/19/20 05:24
12/21/20 07:57
10
----------------------------------------------------------------------------------------------------------------------------------------
Chlordane (n.o.s.) (1C)
ND
0.025
0.0080
mg/L
12/19/20 05:24
12/21/20 07:57
10
Eurofins Lancaster Laboratories Env, LLC
Page 7 of 28 FP2&31BQ202

Client Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Client Sample ID: Sludge Lab Sample ID: 410-23421-1
Date Collected: 12/08/20 13:50 Matrix: Sludge
Date Received: 12/09/20 11:59
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl (Surr) (1C)
78
DCB Decachlorobiphenyl (Surr) (2C)
72
Tetrachloro-m-xylene (Surr) (1C)
94
Tetrachloro-m-xylene (Surr) (2C)
87
Method: 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
Silvex (2,4,5-TP) (1C)
ND
2,4-D (1C)
ND
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacetic acid (Surr)
76
(1 C)
2,4-Dichlorophenylacetic acid (Surr)
82
(2C)
Method: 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
Arsenic
ND
Barium
0.23 B
Cadmium
ND
Chromium
0.0044 J
Lead
ND
Selenium
ND ^5+
Silver
ND ^5-
Method: 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
Mercury
ND
General Chemistry
Analyte
Result Qualifier
Flashpoint
>179
Paint Filter
No
Percent Moisture
75.8
Percent Solids
24.2
General Chemistry - Soluble
Analyte
Result Qualifier
pH
5.7
Limits
Prepared
Analyzed
Dil Fac
10 - 164
12119120 05:24
12121120 07:57
10
10 - 164
12119120 05:24
12121120 07:57
10
39 - 139
12119120 05:24
12121120 07:57
10
39 - 139
12119120 05:24
12121120 07:57
10
RL
MDL Unit
D Prepared
Analyzed
oil Fac
0.0050
0.0010 mg/L
12/20/20 20:12
12/22/20 09:13
1
0.050
0.016 mg/L
12/20/20 20:12
12/22/20 09:13
1
Limits
Prepared
Analyzed
Dil Fac
26 - 136
12120120 20:12
12122120 09:13
1
26 - 136
12120120 20:12
12122120 09:13
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
0.030
0.016
mg/L
12/14/2014:28
12/18/2013:00
1 IE
0.0050
0.0010
mg/L
12/14/2014:28
12/15/2017:38
1
0.0050
0.0010
mg/L
12/14/2014:28
12/15/2017:38
1
M
0.015
0.0016
mg/L
12/14/2014:28
12/15/2017:38
1
0.015
0.0071
mg/L
12/14/2014:28
12/18/2013:00
1
0.050
0.016
mg/L
12/14/2014:28
12/18/2013:00
1
0.010
0.0050
mg/L
12/14/2014:28
12/18/2013:00
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
0.20
0.079
ug/L
12/14/20 14:21
12/15/20 21:10
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
50.0
50.0
Degrees F
12/11/20 08:48
1
No Unit
12/18/20 17:27
1
1.0
1.0
%
12/11/20 01:06
1
1.0
1.0
%
12/11/20 01:06
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
0.01
0.01
S.U.
12/14/2019:37
1
Eurofins Lancaster Laboratories Env, LLC
Page 8 of 28 FP2&312Q2O2

Surrogate Summary
Client: Eurofins Eaton Analytical
Job ID: 410-23421-1
Project/Site: PTRWA - NC
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Sludge
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCA
BFB
DBFM
TOL
Lab Sample ID Client Sample ID (80-120)
(80-120)
(80-120)
(80-120)
410-23421-1 Sludge 100
95
97
100
Surrogate Legend
DCA= 1,2-Dichloroethane-d4 (Surr)
43
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCA
BFB
DBFM
TOL
Lab Sample ID Client Sample ID (80-120)
(80-120)
(80-120)
(80-120)
LCS 410-77394/5 Lab Control Sample 99
95
97
101
MB 410-77394/7 Method Blank 101
95
98
100
Is
Surrogate Legend
DCA= 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
M
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Sludge
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
NBZ TPHd14 PHL
Lab Sample ID Client Sample ID (10-150)
(44-102)
(10-84)
(23-128) (31-113) (10-67)
410-23421-1 Sludge 74
76
32
75 80 22
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
TPHd14 = p-Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
NBZ
TPHd14
PHL
Lab Sample ID Client Sample ID
(10-150)
(44-102)
(10-84)
(23-128)
(31-113)
(10-67)
LCS 410-76811/2-A Lab Control Sample
87
78
48
81
90
36
LCSD 410-76811/3-A Lab Control Sample Dup
96
78
48
77
85
36
MB 410-76811/1-A Method Blank
90
75
39
73
92
29
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
Page 9 of 28
Eurofins Lancaster Laboratories Env, LLC
FP2&312Q202

Surrogate Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
NBZ = Nitrobenzene-d5 (Surr)
TPHd14 = p-Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
Job ID: 410-23421-1
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Sludge Prep Type: TCLP
Lab Sample ID Client Sample ID
410-23421-1 Sludge
Surrogate Legend
DCB = DCB Decachlorobiphenyl (Surr)
TCX = Tetrachloro-m-xylene (Surr)
Percent Surrogate Recovery (Acceptance Limits)
DCBI DC132 TCx1 TCX2
(10-164) (10-164) (39-139) (39-139)
78 72 94 87
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate
Recovery (Acceptance Limits)
DC131
DC132
TCX1
TCX2
Lab Sample ID Client Sample ID (10-164)
(10-164)
(39.139)
(39.139)
LCS 410-78343/2-A Lab Control Sample 90
88
71
74
LCSD 410-78343/3-A Lab Control Sample Dup 98
102
82
86
MB 410-78343/1-A Method Blank 85
93
81
83
Surrogate Legend
DCB = DCB Decachlorobiphenyl (Surr)
TCX = Tetrachloro-m-xylene (Surr)
Method: 8151A - Herbicides (GC)
Matrix: Sludqe Prep TVDe: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCPAAI DCPAA2
Lab Sample ID Client Sample ID (26-136) (26.136)
410-23421-1 Sludge 76 82
Surrogate Legend
DCPAA = 2,4-Dichlorophenylacetic acid (Surr)
Method: 8151A - Herbicides (GC)
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAAI
DCPAA2
Lab Sample ID Client Sample ID
(26-136)
(26-136)
LCS 410-78628/2-A Lab Control Sample
65
71
LCSD 410-78628/3-A Lab Control Sample Dup
61
67
MB 410-78628/1-A Method Blank
71
83
Surrogate Legend
DCPAA = 2,4-Dichlorophenylacetic acid (Surr)
12
13
74
Page 10 of 28
Eurofins Lancaster Laboratories Env, LLC
FP2&3120202

QC Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Method: 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: MB 410-77394/7
Matrix: Solid
Analysis Batch: 77394
MB MB
Analyte
Result Qualifier
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
2-Butanone
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
MB MB
Job ID: 410-23421-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
MDL
Unit
D Prepared Analyzed
oil Fac
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
•
1.0
0.30
ug/L
12/16/20 10:29
1
10
0.30
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
1.0
0.20
ug/L
12/16/20 10:29
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 80 - 120
4-Bromofluorobenzene (Surr) 95 80 - 120
Dibromofluoromethane (Surr) 98 80 - 120
Toluene-d8 (Surr) 100 80 - 120
Lab Sample ID: LCS 410-77394/5
Matrix: Solid
Analysis Batch: 77394
Analyte
Benzene
1,1-Dichloroethene
1,2-Dichloroethane
2-Butanone
Trichloroethene
Vinyl chloride
Surrogate
1,2-Dichloroethane-d4 (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
Toluene-d8 (Surr)
Prepared Analyzed Dil Fac
12116120 10:29 1
12116120 10:29 1
12116120 10:29 1
12116120 10:29 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
20.0
21.3
ug/L
107
80 - 120
20.0
22.7
ug/L
113
80 - 131
20.0
19.9
ug/L
99
73 - 124
150
168
ug/L
112
59-135
20.0
20.8
ug/L
104
80 - 120
20.0
21.4
ug/L
107
56 - 120
LCS LCS
%Recovery Qualifier
Limits
99
80 - 120
95
80 - 120
97
80 - 120
101
80 - 120
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 410-76811/1-A
Matrix: Solid
Analysis Batch: 77341
Analyte
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
2-Methylphenol
4-Methylphenol
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 76811
MB MB
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed oil Fac
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
ND
0.025
0.0050
mg/L
12/15/20 10:00
12/16/20 08:33 1
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
Eurofins Lancaster Laboratories Env, LLC
Page 11 of 28 FP2&3I2Q202

QC Sample Results
Client: Eurofins Eaton Analytical
Job ID: 410-23421-1
Project/Site: PTRWA - NC
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) (Continued)
Lab Sample ID: MB 410-76811/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77341
Prep Batch: 76811
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed oil Fac
Hexachlorobenzene
ND
0.0025
0.00050
mg/L
12/15/20 10:00
12/16/20 08:33 1
Hexachlorobutadiene
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
Hexachloroethane
ND
0.025
0.0050
mg/L
12/15/20 10:00
12/16/20 08:33 1
Nitrobenzene
ND
0.010
0.0025
mg/L
12/15/20 10:00
12/16/20 08:33 1
Pentachlorophenol
ND
0.025
0.0050
mg/L
12/15/20 10:00
12/16/20 08:33 1
Pyridine
ND
0.025
0.010
mg/L
12/15/20 10:00
12/16/20 08:33 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
90
10 - 150
12115120 10:00
12116120 08:33
1
2-Fluorobiphenyl (Surr)
75
44 - 102
12115120 10:00
12116120 08:33
1
2-Fluorophenol (Surr)
39
10 - 84
12115120 10:00
12116120 08:33
1
Nitrobenzene-d5 (Surr)
73
23 - 128
12115120 10:00
12116120 08:33
1
p-Terphenyl-d14 (Surr)
92
31 - 113
12115120 10:00
12116120 08:33
1
Phenol-d5 (Surr)
29
10 - 67
12115120 10:00
12116120 08:33
1
Lab Sample ID: LCS 410-76811/2-A
Matrix: Solid
Analysis Batch: 77341
Analyte
Spike
Added
LCS
Result
LCS
Qualifier
Unit
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 76811
%Rec.
D %Rec Limits
1,4-Dichlorobenzene
0.250
0.177
mg/L
71
41 -86
2,4,5-Trichlorophenol
0.250
0.225
mg/L
90
59 - 126
2,4,6-Trichlorophenol
0.250
0.214
mg/L
85
59 - 129
2,4-Dinitrotoluene
0.250
0.226
mg/L
90
52 - 128
2-Methylphenol
0.250
0.195
mg/L
78
41 - 113
4-Methylphenol
0.250
0.173
mg/L
69
41 - 109
Hexachlorobenzene
0.250
0.246
mg/L
98
55 - 123
Hexachlorobutadiene
0.250
0.194
mg/L
78
20 - 108
Hexachloroethane
0.250
0.160
mg/L
64
22 - 88
Nitrobenzene
0.250
0.217
mg/L
87
52 - 119
Pentachlorophenol
0.500
0.343
mg/L
69
54 - 131
Pyridine
0.500
0.197
mg/L
39
23 - 64
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
87
10 - 150
2-Fluorobiphenyl (Surr)
78
44 - 102
2-Fluorophenol (Surr)
48
10 - 84
Nitrobenzene-d5 (Surr)
81
23 - 128
p-Terphenyl-d14 (Surr)
90
31 - 113
Phenol-d5 (Surr)
36
10 - 67
Lab Sample ID: LCSD 410-76811/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77341
Prep Batch: 76811
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
1,4-Dichlorobenzene
0.250
0.173
mg/L
69
41 -86 3 30
2,4,5-Trichlorophenol
0.250
0.244
mg/L
98
59 - 126 8 30
Eurofins Lancaster Laboratories Env, LLC
Page 12 of 28 FP2&312Q202

QC Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Job ID: 410-23421-1
Lab Sample ID: LCSD 410-76811/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77341
Prep Batch: 76811
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
2,4,6-Trichlorophenol
0.250
0.240
mg/L 96 59 - 129 12 30
2,4-Dinitrotoluene
0.250
0.224
mg/L 90 52 - 128 1 30
2-Methylphenol
0.250
0.195
mg/L 78 41 - 113 0 30
4-Methylphenol
0.250
0.173
mg/L
69
41 - 109 0 30
HexachIorobenzene
0.250
0.236
mg/L
94
55 - 123 4 30
Hexachlorobutadiene
0.250
0.188
mg/L
75
20 - 108 3 30
Hexachloroethane
0.250
0.157
mg/L
63
22-88 2 30
Nitrobenzene
0.250
0.204
mg/L
81
52 - 119 6 30
Pentachlorophenol
0.500
0.462
mg/L
92
54 - 131 30 30
Pyridine
0.500
0.181
mg/L
36
23-64 9 30
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
2,4,6-Tribromophenol (Sum)
96
10- 150
Is
2-Fluorobiphenyl (Surr)
78
44 - 102
2-Fluorophenol (Sum)
48
10 - 84
Nitrobenzene-d5 (Surr)
77
23 - 128
p-Terphenyl-d14 (Surr)
85
31 - 113
Phenol-d5 (Surr)
36
10 - 67
M
Method: 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MB 410-78343/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 78655
Prep Batch: 78343
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Endrin (1C)
ND
0.00010
0.000040
mg/L
12/19/20 05:24
12/21/20 07:25 1
gamma-BHC (Lindane) (1C)
ND
0.000050
0.000010
mg/L
12/19/20 05:24
12/21/20 07:25 1
Heptachlor (1C)
ND
0.000050
0.000020
mg/L
12/19/20 05:24
12/21/20 07:25 1
Heptachlor epoxide (1C)
ND
0.000050
0.000012
mg/L
12/19/20 05:24
12/21/20 07:25 1
Methoxychlor (1 C)
ND
0.00050
0.00015
mg/L
12/19/20 05:24
12/21/20 07:25 1
Toxaphene (1C)
ND
0.015
0.0050
mg/L
12/19/20 05:24
12/21/20 07:25 1
Chlordane (n.o.s.) (1C)
ND
0.0025
0.00080
mg/L
12/19/20 05:24
12/21/20 07:25 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr) (1C)
85
10 - 164
12119120 05:24
12121120 07:25
1
DCB Decachlorobiphenyl (Surr) (2C)
93
10 - 164
12119120 05:24
12121120 07:25
1
Tetrachloro-m-xylene (Surr) (IC)
81
39 - 139
12119120 05:24
12121120 07:25
1
--------------------------------------------------------------------------------------------------------------------------------------------
Tetrachloro-m-xylene (Surr) (2C)
83
39 - 139
12119120 05:24
12121120 07:25
1
Lab Sample ID: LCS 410-78343/2-A
Matrix: Solid
Analysis Batch: 78655
Spike
LCS LCS
Analyte
Added
Result Qualifier
Unit
Endrin (1C)
0.000125
0.000110
mg/L
gamma-BHC (Lindane) (2C)
0.000250
0.000208
mg/L
Heptachlor (2C)
0.000250
0.000211
mg/L
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 78343
%Rec.
D %Rec Limits
88 60 - 151
83 51 - 132
84 38 - 135
Eurofins Lancaster Laboratories Env, LLC
Page 13 of 28 FP2&31BQ202

QC Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 410-78343/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78655 Prep Batch: 78343
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Heptachlor epoxide (2C) 0.000375 0.000317 mg/L 85 56 - 132
Methoxychlor (2C) 0.00100 0.000925 mg/L 92 58 - 165
LCS LCS
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl (Surr)
90
(1 C)
DCB Decachlorobiphenyl (Surr)
88
(2C)
Tetrachloro-m-xylene (Surr)
71
(1 C)
Tetrachloro-m-xylene (Surr)
74
(2C)
Lab Sample ID: LCSD 410-78343/3-A
Matrix: Solid
Analysis Batch: 78655
Analyte
Endrin (1C)
gamma-BHC (Lindane) (2C)
Heptachlor (2C)
Heptachlor epoxide (2C)
Methoxychlor (2C)
LCSD LCSD
Surrogate
%Recovery Qualifier
DCB Decachlorobiphenyl (Surr)
98
(1 C)
DCB Decachlorobiphenyl (Surr)
102
(2C)
Tetrachloro-m-xylene (Surr)
82
(1 C)
Tetrachloro-m-xylene (Surr)
86
(2C)
Method: 8151A - Herbicides
(GC)
Limits
10 - 164
10 - 164
39 - 139
39 - 139
Spike
Added
0.000125
0.000250
0.000250
0.000375
0.00100
Limits
10 - 164
10 - 164
39 - 139
39 - 139
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 78343
LCSD LCSD
%Rec. RPD
Result Qualifier
Unit
D %Rec
Limits RPD Limit
0.000129
mg/L
104
60 - 151 16 30
0.000234
mg/L
94
51 - 132 12 30
0.000243
mg/L
97
38 - 135 14 30
0.000360
mg/L
96
56 - 132 13 30
0.00108
mg/L
108
58 - 165 16 30
Lab Sample ID: MB 410-78628/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 79065
Prep Batch: 78628
MB MB
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed oil Fac
Silvex (2,4,5-TP) (1C)
ND
0.0050 0.0010 mg/L
12/20/20 20:12
12/22/20 07:33 1
2,4-D (1C)
ND
0.050 0.016 mg/L
12/20/20 20:12
12/22/20 07:33 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4-Dichlorophenylacetic acid (Surr)
71
26 - 136
12120120 20:12
12122120 07:33 1
(1 C)
2,4-Dichlorophenylacetic acid (Surr)
83
26 - 136
12120120 20:12
12122120 07:33 1
(2C)
0
Page 14 of 28
Eurofins Lancaster Laboratories Env, LLC
FP2&312Q2O2

QC Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 410-78628/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 79065 Prep Batch: 78628
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Silvex (2,4,5-TP) (2C) 0.0250 0.0185 mg/L 74 58 - 148
2,4-D (2C) 0.0250 0.0178 J mg/L 71 42 - 147
LCS LCS
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacetic acid 65
(Surr) (1 C)
2,4-Dichlorophenylacetic acid 71
(Surr) (2C)
Lab Sample ID: LCSD 410-78628/3-A
Matrix: Solid
Analysis Batch: 79065
Analyte
Silvex (2,4,5-TP) (2C)
2,4-D (2C)
Limits
26 - 136
26 - 136
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 78628
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.0250 0.0180 mg/L 72 58 - 148 3 30
0.0250 0.0176 J mg/L 71 42 - 147 1 30
LCSD LCSD
Surrogate %Recovery Qualifier Limits
2,4-Dichlorophenylacetic acid 61 26 - 136
(Surr) (1 C)
2,4-Dichlorophenylacetic acid 67 26 - 136
(Surr) (2C)
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 410-76490/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77261
Prep Batch: 76490
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed oil Fac
Barium
ND
0.0050
0.0010
mg/L
12/14/2014:28
12/15/2016:42 1
Cadmium
ND
0.0050
0.0010
mg/L
12/14/2014:28
12/15/2016:42 1
Chromium
ND
0.015
0.0016
mg/L
12/14/2014:28
12/15/2016:42 1
Lab Sample ID: MB 410-76490/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 78193
Prep Batch: 76490
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed oil Fac
Arsenic
ND
0.030
0.016
mg/L
12/14/2014:28
12/18/2011:57 1
Barium
0.00100
J
0.0050
0.0010
mg/L
12/14/2014:28
12/18/2011:57 1
Cadmium
ND
0.0050
0.0010
mg/L
12/14/2014:28
12/18/2011:57 1
Chromium
ND
0.015
0.0016
mg/L
12/14/2014:28
12/18/2011:57 1
Lead
ND
0.015
0.0071
mg/L
12/14/2014:28
12/18/2011:57 1
Selenium
ND
^5+
0.050
0.016
mg/L
12/14/2014:28
12/18/2011:57 1
Silver
ND
^5-
0.010
0.0050
mg/L
12/14/2014:28
12/18/2011:57 1
0
Page 15 of 28
Eurofins Lancaster Laboratories Env, LLC
FP2&31BQ202

QC Sample Results
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: LCS 410-76490/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77261
Prep Batch: 76490
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
Barium
0.0100
0.0106
mg/L
106 80 - 120
Cadmium
0.0100
0.0106
mg/L
106 80 - 120
Chromium
0.0300
0.0320
mg/L
107 80 - 120
Lab Sample ID: LCS 410-76490/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 78193
Prep Batch: 76490
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
Arsenic
0.0600
0.0704
mg/L
117 80 - 120
Barium
0.0100
0.0108
mg/L
108 80 - 120
Cadmium
0.0100
0.00984
mg/L
98 80 - 120
Chromium
0.0300
0.0308
mg/L
103 80 - 120
Lead
0.0300
0.0268
mg/L
89 80 - 120
Is
Selenium
0.100
0.119 ^5+
mg/L
119 80 - 120
Silver
0.0200
0.0230 ^5-
m9 /L
115 80 - 120
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 410-76488/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77240
Prep Batch: 76488
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Mercury ND
0.20 0.079 ug/L
12/14/20 14:21 12/15/20 20:46 1
Lab Sample ID: LCS 410-76488/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 77240
Prep Batch: 76488
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Mercury
1.00
1.04
ug/L 104 80 - 118
Method: 1010A - Ignitability, Pensky-Martens Closed -Cup Method
Lab Sample ID: LCS 410-75746/1
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 75746
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Flashpoint
81.0
82.00
Degrees F 101 96.9 - 103.
1
Lab Sample ID: LCSD 410-75746/2
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 75746
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Flashpoint
81.0
82.00
Degrees F 101 96.9 - 103. 0 4
1
Eurofins Lancaster Laboratories Env, LLC
Page
16 of 28
FP2&3120202

QC Sample Results
Client: Eurofins Eaton Analytical
Job ID: 410-23421-1
Project/Site: PTRWA - NC
Method: 9045D - pH
Lab Sample ID: LCS 410-76595/1-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 76627
Spike
LCS
LCS %Rec.
Analyte
Added
Result
Qualifier Unit D %Rec Limits
pH
7.00
7.3
S.U. 104 95 _ 105
Lab Sample ID: LCSD 410-76595/2-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 76627
Spike
LCSD
LCSD %Rec. RPD
Analyte
Added
Result
Qualifier Unit D %Rec Limits RPD Limit
pH
7.00
7.3
S.U. 104 95 _ 105 0 4
Method: 9095B - Paint Filter
Lab Sample ID: MB 410-78272/1
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 78272
MB MB
Analyte
Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Paint Filter
No
No Unit 12/18/20 17:27 1
Eurofins Lancaster Laboratories Env, LLC
Page 17 of 28 FP2 BO202

QC Association Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
GUMS VOA
Leach Batch: 76055
Job ID: 410-23421-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
410-23421-1
Sludge
TCLP
Sludge
1311
Analysis Batch: 77394
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
410-23421-1
Sludge
TCLP
Sludge
8260D 76055
MB 410-77394/7
Method Blank
Total/NA
Solid
8260D
LCS 410-77394/5
Lab Control Sample
Total/NA
Solid
8260D
GUMS Semi VOA
Leach Batch: 76078
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
1311
Prep Batch: 76811
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
3510C
76078
MB 410-76811/1-A
Method Blank
Total/NA
Solid
3510C
LCS 410-76811/2-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 410-76811/3-A
Lab Control Sample Du
P P
Total/NA
Solid
3510C
Analysis Batch: 77341
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
8270E
76811
MB 410-76811/1-A
Method Blank
Total/NA
Solid
8270E
76811
LCS 410-76811/2-A
Lab Control Sample
Total/NA
Solid
8270E
76811
LCSD 410-76811/3-A
Lab Control Sample Dup
Total/NA
Solid
8270E
76811
GC Semi VOA
Leach Batch: 76078
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
1311
Prep Batch: 78343
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
3510C
76078
MB 410-78343/1-A
Method Blank
Total/NA
Solid
3510C
LCS 410-78343/2-A
Lab Control Sample
Total/NA
Solid
3510C
�LCSD 410-78343/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 78628
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
8151A
76078
MB 410-78628/1-A
Method Blank
Total/NA
Solid
8151A
LCS 410-78628/2-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 410-78628/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Analysis Batch: 78655
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
8081B
78343
MB 410-78343/1-A
Method Blank
Total/NA
Solid
8081B
78343
r
12
13
74
Eurofins Lancaster Laboratories Env, LLC
Page 18 of 28 FP2 20202

QC Association Summary
Client: Eurofins Eaton Analytical
Job ID: 410-23421-1
Project/Site: PTRWA - NC
GC Semi VOA (Continued)
Analysis Batch: 78655 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCS 410-78343/2-A
Lab Control Sample
Total/NA
Solid
8081B
78343
LCSD 410-78343/3-A
Lab Control Sample Dup
Total/NA
Solid
8081 B
78343
Analysis Batch: 79065
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
8151A
78628
MB 410-78628/1-A
Method Blank
Total/NA
Solid
8151A
78628
LCS 410-78628/2-A
Lab Control Sample
Total/NA
Solid
8151A
78628
�LCSD 410-78628/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
78628
Metals
Leach Batch: 76078
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
1311
Prep Batch: 76488
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
7470A
76078
MB 410-76488/1-A
Method Blank
Total/NA
Solid
7470A
LCS 410-76488/2-A
Lab Control Sample
Total/NA
Solid
7470A
Prep Batch: 76490
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
3010A
76078
MB 410-76490/1-A
Method Blank
Total/NA
Solid
3010A
LCS 410-76490/2-A
Lab Control Sample
Total/NA
Solid
3010A
Analysis Batch: 77240
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
7470A
76488
MB 410-76488/1-A
Method Blank
Total/NA
Solid
7470A
76488
LCS 410-76488/2-A
Lab Control Sample
Total/NA
Solid
7470A
76488
Analysis Batch: 77261
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
6010D
76490
MB 410-76490/1-A
Method Blank
Total/NA
Solid
6010D
76490
LCS 410-76490/2-A
Lab Control Sample
Total/NA
Solid
6010D
76490
Analysis Batch: 78193
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
TCLP
Sludge
6010D
76490
MB 410-76490/1-A
Method Blank
Total/NA
Solid
6010D
76490
LCS 410-76490/2-A
Lab Control Sample
Total/NA
Solid
6010D
76490
General Chemistry
Analysis Batch: 75636
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
410-23421-1
Sludge
Total/NA
Sludge
Moisture
Eurofins Lancaster Laboratories Env, LLC
Page 19 of 28
FP2&MG202

QC Association Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
General Chemistry
Analysis Batch: 75746
Lab Sample ID
Client Sample ID
410-23421-1
Sludge
LCS 410-75746/1
Lab Control Sample
LCSD 410-75746/2
Lab Control Sample Dup
Leach Batch: 76595
Lab Sample ID
Client Sample ID
410-23421-1
Sludge
LCS 410-76595/1-A
Lab Control Sample
LCSD 410-76595/2-A
Lab Control Sample Dup
Analysis Batch: 76627
Lab Sample ID
Client Sample ID
410-23421-1
Sludge
LCS 410-76595/1-A
Lab Control Sample
LCSD 410-76595/2-A
Lab Control Sample Dup
Analysis Batch: 78272
Lab Sample ID
Client Sample ID
410-23421-1
Sludge
MB 410-78272/1
Method Blank
Job ID: 410-23421-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Sludge
1010A
Total/NA
Solid
1010A
Total/NA
Solid
1010A
Prep Type
Matrix
Method
Prep Batch
Soluble
Sludge
DI Leach
Soluble
Solid
DI Leach
Soluble
Solid
DI Leach
•
Prep Type
Matrix
Method
Prep Batch
Soluble
Sludge
9045D
76595
Soluble
Solid
9045D
76595
Soluble
Solid
9045D
76595
Prep Type
Matrix
Method
■ii
Prep Batch
Total/NA
Sludge
9095B
Total/NA
Solid
9095B
Eurofins Lancaster Laboratories Env, LLC
Page 20 of 28 FP261MG202

Lab Chronicle
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Job ID: 410-23421-1
Client Sample ID: Sludge Lab Sample ID: 410-23421-1
Date Collected: 12/08/20 13:50 Matrix: Sludge
Date Received: 12/09/20 11:59
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
TCLP
Leach
1311
76055
12/12/20 07:05
CZ7N
ELLE
TCLP
Analysis
8260D
20
77394
12/16/2018:39
TQ4J
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
3510C
76811
12/15/2010:00
R9CT
ELLE
TCLP
Analysis
8270E
1
77341
12/16/2014:08
W6XI
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
3510C
78343
12/19/20 05:24
UKQ8
ELLE
TCLP
Analysis
8081B
10
78655
12/21/2007:57
UAMZ
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
8151A
78628
12/20/20 20:12
UKL2
ELLE
TCLP
Analysis
8151A
1
79065
12/22/20 09:13
UAMZ
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
3010A
76490
12/14/2014:28
UJLA
ELLE
TCLP
Analysis
6010D
1
77261
12/15/2017:38
ULJC
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
3010A
76490
12/14/2014:28
UJLA
ELLE
TCLP
Analysis
6010D
1
78193
12/18/2013:00
UCIG
ELLE
TCLP
Leach
1311
76078
12/12/20 08:18
CZ7N
ELLE
TCLP
Prep
7470A
76488
12/14/2014:21
UJLA
ELLE
TCLP
Analysis
7470A
1
77240
12/15/20 21:10
UEFS
ELLE
Total/NA
Analysis
1010A
1
75746
12/11/20 08:48
USAE
ELLE
Soluble
Leach
DI Leach
76595
12/14/20 18:15
JB
ELLE
Soluble
Analysis
9045D
1
76627
12/14/2019:37
JB
ELLE
Total/NA
Analysis
9095B
1
78272
12/18/2017:27
JB
ELLE
Total/NA
Analysis
Moisture
1
75636
12/11/20 01:06
PTG7
ELLE
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
in
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Page 21 of 28
Eurofins Lancaster Laboratories Env, LLC
FP2&MG202

Accreditation/Certification Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority
North Carolina (WV/SW)
Program
State
Identification Number Expiration Date
521 12-31-20
Job ID: 410-23421-1
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
1010A Sludge Flashpoint
Moisture Sludge Percent Moisture
Moisture Sludge Percent Solids
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Eurofins Lancaster Laboratories Env, LLC
Page 22 of 28 FP2 20202

Method Summary
Client: Eurofins Eaton Analytical
Job ID: 410-23421-1
Project/Site: PTRWA - NC
Method Method Description
Protocol
Laboratory
8260D Volatile Organic Compounds by GC/MS
SW846
ELLE
8270E Semivolatile Organic Compounds (GC/MS)
SW846
ELLE
8081B Organochlorine Pesticides (GC)
SW846
ELLE
8151A Herbicides (GC)
SW846
ELLE
6010D Metals (ICP)
SW846
ELLE
7470A Mercury (CVAA)
SW846
ELLE
1010A Ignitability, Pensky-Martens Closed -Cup Method
SW846
ELLE
9045D pH
SW846
ELLE
9095B Paint Filter
SW846
ELLE
Moisture Percent Moisture
EPA
ELLE
1311 TCLP Extraction
SW846
ELLE
3010A Preparation, Total Metals
SW846
ELLE
3510C Liquid -Liquid Extraction (Separatory Funnel)
SW846
ELLE
5030C Purge and Trap
SW846
ELLE
7470A Preparation, Mercury
SW846
ELLE
8151A Extraction (Herbicides)
SW846
ELLE
DI Leach Deionized Water Leaching Procedure
ASTM
ELLE
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
M
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
Page 23 of 28 FP2 (2Cb2

Sample Summary
Client: Eurofins Eaton Analytical
Project/Site: PTRWA - NC
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
410-23421-1 Sludge Sludge 12/08/2013:50 12/09/2011:59
Job ID: 410-23421-1
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Eurofins Lancaster Laboratories Env, LLC
Page 24 of 28 FP2w 2Q202

v
m
N
00
0
w
N
tiff eurofins
Lancaster Laboratories Acct. #
Environmental
of Custody
1111111111111111111111111111111111
ital use only
COC#615180
Client Information
�
a
0
c
1 °—
Analysis
Requested
For Lab Use Only
�FSC:
lient: W i J y Nc
(�) 11
Acct. #:
q
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� 17)
LU
ca 0
Z
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ITS
3
L
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Preservation and
Filtration Codes
SCR#: I Aq go
reject Name/#:
PWSID #:
Preservation Codes
H=HCI T=Thiosulfate
N=HNO3 B=NaOH
S=H2SO4 P=H3PO4
F=Field Filtered O=Other
ro�ec7tM�ager:
f �Qj
i
P..0O..#+: jam% �J/'�
1 120Sv�/
amp
�� �10 '_CL
Quote #:
Remarks
tale where samples were collected:
C
For Compliance:
Yes ❑ No
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a
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Sample Identification
Collected
Date
Time
��� L1<-# 2
!2 t3 Zo
i3'4
I
61LL t!�
135-0
51 del
12-g 20
13q 8
Turna me (TAT) Requested (please circle)
�Standard Rush
(Rush TATts� aboratory approval and surcharge.)
Requested TAT in business days:
E-mail address: �' ee r t e
Relinquished by
Dat
�
23 Z
Time
[ go
Received y
Date
Time
I�.ZC�
Relinqui d by
Date
i�lsl�o
Time
ISoB
Received by
Date
Time
Relinquished by
Date
Time
Received by
Date
lume
Relinquished by
Date
Time
Received by
Date
Time
Data Package Options (circle if required)
Type I (EPA Level 3
Type VI (Raw Data Only)
Equivalent/non-CLP)
Type III (Reduced non-CLP) NJ DKQP TX TRRP-13
NYSDEC Category A or B MA MCP CT RCP
Relinquished by
Date
Time
Received by
�
Date
J
Ti1np✓`
'11J��//J
EDD Required? Yes No
If yes, format:
Relinquished by Comm c I Carrier.
UPS FedEx Other
Site -Specific QC (MS/MSD/Dup)? Yes No
(If yes, indicate QC sample and submit triplicate sample volume.)
Temperature upon receipt '.S _°C
Eurofins Lancaster Laboratories Environmental, LLC • 2425 New Holland Pike, Lancaster, PA 17601 •717-656-2300 • FOR HELP COMPLETING FORM CHECK OUT https://www.eurofinsus.com/coc
The white copy should accompany samples to Eurofins Lancaster Laboratories Environmental. The yellow copy should be retained by the client. 7044 0919
Page 25 of 28
12/23/2020

. 4:: eurofins Sample Container Record
I nnnratories
E
Client: 11411 _410-23421-oz Chain
Euroor custody
fins Eaton A
Cape Fear, NC Public Utility
Bill to client's Fed -Ex A# 696 949 018
Group: 1
Ship To:
PTRWA-NC
7297 Adams Farm Road
Randleman, NC 27317
336-498-5510
Attn: Thomas Hedrick
Number of Sample Locations: 1
Dne complete set of bottles listed below must be filled for each of the 1 sample location(s).
*264903*
Order Number: 264903
Order Date: 11/22/2020
Page 1 of 2
Standard Frm#: 311103
Count Code Description Preservative Analysis Name Hold Time
1 20 500 ml wide mouth glass None Flash Point 30 days
Paint Filter Liquids Test NA
pH 0 immediate
Group: 2
Number of Sample Locations: 1
One complete set of bottles listed below must be filled for each of the 1 sample location(s).
Count Code Description Preservative Analysis Name Hold Time
1 21 1000 ml wide mouth glass None TCLP Metals 28 days
TCLP Pest/Herb 14 days
TCLP SVOCs 14 days
Group: 3
Number of Sample Locations: 1
One complete set of bottles listed below must be filled for each of the 1 sample location(s).
Count Code Description Preservative Analysis Name Hold Time
1 76 60 ml wide mouth glass VOA None TCLP VOCs 14 days
If you have any questions, please contact your Client Service Representative, Barbara Weyandt, at [phone] x7264
Date Needed: Pack By: Shipping Method: This order is:
1112412020 1 11112312020 jFedEx Standard Per your Request
Version 2.2.6
Page 26 of 28 FP2&MG202
[L4

eurofins
Sample Container Record
*264903*
Lancaster Laboratories
U,virorimpHnI
Client: 11411
Eurofins Eaton Analytical, In
Cape Fear, NC Public Utility Authority
Bill to client's Fed -Ex A# 696 949 018
Ship To:
PTRWA-NC
7297 Adams Farm Road
Randleman, NC 27317
336-498-5510
Attn: Thomas Hedrick
Sample Acceptance Policy
Order Number: 264903
Order Date: 11/22/2020
Page 2 of 2
Standard Frm#: 311103
Samples must be submitted in a manner that meets the criteria listed below. Clients will be contacted for direction on how to proceed for any
non -regulatory samples that do not meet the criteria specified below. Regulatory samples that were not processed properly in the field
regarding any required preservation, filtration, and/or packaging on ice in accordance with the EPA methodology must be rejected by the
laboratory.
• Regulatory samples (SDWA, NPDES, etc.) must be identified on the sample submission paperwork to ensure proper sample handling and reporting.
• Documentation must be complete and include: sample identification, the location, date and time of collection, collector's name or initials,
preservation type, sample type, and any special remarks concerning the sample.
• Proper sample labeling must include unique identification on a durable (water resistant) label using indelible ink.
• Sufficient sample volume (including required Matrix QC) must be collected in appropriate containers with proper field preservation processes (i.e.
chemical, filtration) completed as dictated in the methods or regulations at the time of collection. The laboratory will provide appropriate bottleware
and preservative.
• Samples must be shipped promptly to meet specified holding times with adequate packing materials to prevent damage during shipment and
sufficient wet ice to meet method temperature requirements (0-6C, not frozen).
• Trip blank vials are provided when sample vials for volatile analyses are requested. The trip blank vials must be kept with your sample bottles at all
times and returned to the laboratory with your shipment in order to ensure the integrity of your volatile samples.
• Safe Drinking Water Act (SDWA) compliance samples from PENNSYLVANIA will be rejected upon sample receipt if the method required trip /field
blanks are not submitted with the samples per PADEP.
If you have any questions, please contact your Client Service Representative, Barbara Weyandt, at [phone] x7264
Date Needed: Pack By: Shipping Method: This order Is:
11/24/2020 11/23/2020 JFedEx Standard I 1Per your Request
Version 2.2 6
Page 27 of 28 FP2 9(202
13
14

Login Sample Receipt Checklist
Client: Eurofins Eaton Analytical
Login Number: 23421
List Number: 1
Creator: Cyms, Carolyn M
Question Answer
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable (</=6C, not frozen).
True
Cooler Temperature is recorded.
True
VW: Container Temperature is acceptable (</=6C, not frozen).
N/A
VW: Container Temperature is recorded.
N/A
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
There is sufficient vol. for all requested analyses.
True
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
N/A
Is the Field Sampler's name present on COC?
True
Sample Preservation Verified.
N/A
Residual Chlorine Checked.
N/A
Sample custody seals are intact.
N/A
Job Number: 410-23421-1
List Source: Eurofins Lancaster Laboratories Env
Comment
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Page 28 of 28 FP2 M202