WQ0003919_Residual Annual Report 2020_20210223

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0003919
Applicant/Permittee City of Kinston
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide inforration on the person to be contacted by N B Staff
Name * Lysa Finnerty
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
14105376150
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0003919
Fbs Current Existing perrrit number
Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220
Facility Name * City of Kinston RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report for City of Kinston NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Forr} Engineering Fans, Specifications, Calculations, Bc.)
Kinston NC 2020 Annual Report FINAL.pdf 5.54MB
Upload only 1 FFdocurrent (less than 250 fvB). Miltiple documents rust be contained into one FJFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2021

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 23, 2021
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report for Permit No. WQ0003919
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Kinston, NC.
If you have any questions or comments, please contact Kenneth Stevens at [phone] or
Chris Wynne at [phone].
Sincerely,
oe"i& Shuuc" ,es
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Kenneth Stevens, City of Kinston
Chris Wynne, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF KINSTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003919
2020 ANNUAL REPORT

City of Kinston, NC
Residuals Land Application Program
2020 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WQ0003919 County Lenoir Year 2020
Facility Name (as shown on permit) Kinston Regional WRF NPDES No. NCO024236
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. if NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 38
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 254.31
Total number of acres utilized for land application during the year: 52.80
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
IL Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Kenneth Stevens, WRF Superintendent
Permittee Name and Title (type or print) Signature of PCtt Date
Signature ofPreparer* Date Signa e Appli r Date
(if different from Permittee) (if different fro ermittee and Pr arer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
KINSTON, NC
KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
MONTH/YEAR
July 2020
IEel /_1I
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
1,525.00 Y 254.31 D 230.66
1,525.00 Y 254.31 D 230.66
Report Date: 2/2/2021 3:59:47 PM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0003919 Laboratory:
Facility Name: KINSTON, NC PACE ANALYTICAL
Residual Source WQ # or
NPDES#: NCO024236
WWTP Name: KINSTON REGIONAL WRF
Residual Analysis Data
Product Type
Sample or Composite Date
AEDCAK
04/28/20
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
19.80
Arsenic
75
5.7
Cadmium
85
2.1
Copper
4300
390
Chromium
NA
30
Lead
840
27
Mercury
57
<0.89
Molybdenum
75
9.9
Nickel
420
20
Selenium
100
10
Zinc
7500
1400
Total Phosphorus
NA
32000
TKN
NA
50000
Ammonia -Nitrogen
NA
4500
Nitrate and Nitrite
NA
6.99
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 1?5.9kprand 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/2/2021 5:04:33 PM For: 2060 02

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0003919
Facility Name:
KINSTON, NC
Residual Source
NPDES # or WQ#:
NCO024236
WWTP Name:
KINSTON REGIONAL WRF
Residual Analysis Data
Product Type
AEDCAK
Sample or Composite Date
04/28/20
Parameters (mg/kg dry weight)
Aluminium
26000
Calcium
24000
Magnesium
5400
pH (s.u.)
6.80
Potassium
4800
Sodium
2400
PAN
15907
SAR (Ratio)
1.6165
Laboratory:
PACE ANALYTICAL
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
L�
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/2/2021 5:04:02 PM For: 2060 02 DENR FORM RSSF-B (1212006)

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Kinston
Lot Number:VD29008
Date Completed:05/07/2020
NIM�� Mr�
05/08/2020 9:58 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q PCCRBp��
AAW
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ANSI NdmlAccre00- Board
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A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VD29008
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure amount per.
The LOQ has been adjusted accordingly.
Mercury
The following sample was diluted due to the nature of the sample matrix: VD29008-001. This sample was
foamy so to protect the integrity of the instrument it was diluted 10 fold The LOQ has been elevated to
reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VD29008-001
Description: Kinston WWTP Matrix: Solid
Date Sampled:04/28/2020 0930 % Solids: 19.8 04/29/2020 2359
Date Received: 04/29/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 04/29/2020 2359 HET
52469
1 350.1
(Ammonia - N ) 350.1
25 05/01/2020 1327 DRD
52545
1
(Nitrate - N ) 9056A
1 05/01/2020 1659 AMR
52733
1
(Nitrite - N ) 9056A
1 05/01/2020 1659 AMR
52734
1
(Phosphorus) 365.1
250 05/04/2020 1426 DMA
05/04/2020 0914
52789
1
(Soil pH meas) 9045D
1 04/30/2020 2024 SRB
52590
1 351.4
(TKN) 351.2
10 05/06/2020 1544 DMA
05/06/2020 0951
52983
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
19.8
%
1
Ammonia - N (gas diffusion)
350.1
4500
130
66
mg/kg
1
Nitrate - N (soluble)
9056A
6.4
2.5
0.12
mg/kg
1
Nitrite - N (soluble)
9056A
0.59 J
1.0
0.097
mg/kg
1
Phosphorus
7723-14-0 365.1
32000
6300
1300
mg/kg
1
Soil pH measured in water @
19.7 ° C
9045D
6.8
su
1
TKN
351.2
50000
1300
1300
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
10 05/05/2020 0152 JMH
05/04/2020 0550
52456
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
3.7
0.89
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 05/01/2020 1613 LLL
04/30/2020 2257
52446
2 3050B
601 OD
1 05/02/2020 1354 LLL
04/30/2020 2257
52446
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
26000
31
12
mg/kg
1
Arsenic
7440-38-2 6010D
5.7
1.2
0.39
mg/kg
1
Cadmium
7440-43-9 6010D
2.1
0.39
0.098
mg/kg
1
Calcium
7440-70-2 6010D
24000
390
49
mg/kg
1
Chromium
7440-47-3 6010D
30
0.78
0.19
mg/kg
1
Copper
7440-50-8 6010D
390
0.78
0.35
mg/kg
1
Iron
7439-89-6 6010D
13000
7.8
3.5
mg/kg
1
Lead
7439-92-1 6010D
27
0.78
0.35
mg/kg
1
Magnesium
7439-95-4 6010D
5400
390
49
mg/kg
1
Manganese
7439-96-5 6010D
190
1.2
0.46
mg/kg
1
Molybdenum
7439-98-7 6010D
9.9
3.1
0.78
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VD29008-001
Description: Kinston WWTP Matrix: Solid
Date Sampled:04/28/2020 0930 % Solids: 19.8 04/29/2020 2359
Date Received:04/29/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 05/01/2020 1613 LLL
04/30/2020 2257 52446
2 3050B
6010D 1 05/02/2020 1354 LLL
04/30/2020 2257 52446
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
20 3.1
0.82
mg/kg
1
Potassium
7440-09-7 6010D
4800 390
49
mg/kg
2
Selenium
7782-49-2 6010D
10 1.6
0.63
mg/kg
1
Sodium
7440-23-5 6010D
2400 390
49
mg/kg
2
Zinc
7440-66-6 6010D
1400 3.9
0.97
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

FACILITY NAME: KINSTON, NC
LANDOWNER: W B HARGETT
OPERATOR: DEXTER EDWARDS
CROP 1NAME: BERMUDAGRASS,COASTAL -
OACTI IA /Rr`M
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02944-0-0001-
ANNUAL DRY TONS APPLIED: 20.85 SITE #: NC JO 02944
PREDOMINANT SOIL SERIES: LEON
CROP 1 MAX. PAN: 99 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 7.5
ACRES PERMITTED: 7.7
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati- Mineral-
Ammonia
Nitrate
PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual Dry, Wet,
Past 24 Hrs.
Application
lization ization
TKN
Nitrogen
and Nitrite
(Ibs/acre) Application
Month
Solids
Dry Tons/Ac
Source Moist
Inches
Method*
Rate** Rate***
mg/kg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2 Crop 1 Crop 2
7/13/2020
125.00
(Y)
19.800
2.779
KIKRAEDC DRY
110-<1/2"
SUR
0.5 0.30
50,000.00
4,500.00
6.99
88.422
d BCP
Jul-20
125.00
(Y)
Annual Ibs/acre Applied
Cumulative Ibs/acre Applied
Permit PAN Limit (Ibs/acre)
1st Crop
Total 2.779
AS CD CU I CR PB HG
0.032 0.012 2.168 10.167 0.150 1 0.005
0.326 0,177 21.430 2.643 2.613 0.052
Total 88.422 0.000
MO NI SE ZN P L
0 0.055 0.111 .056 7.782 177.877 Date
89.0 1 2,500.0
99
Lbs/Ac
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant Pena ' ors fitting false information, including the possibility of fines and impriso en for knowing violations."
SI A URE OF LAND APPLIER i 05ATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation **' C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ****' See Site pH & Lime Application Records Section of Report
Printed: 2/112021 DENR FORM FSF (12/2006)

FACILITY NAME: KINSTON, NC
LANDOWNER: W B HARGETT
OPERATOR: DEXTER EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
PACTI IR 1pro\
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02944-0-0002-
ANNUAL DRY TONS APPLIED: 25.01 SITE #: NC JO 02944
PREDOMINANT SOIL SERIES: LEON
CROP 1 MAX. PAN: 99 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 8.6
ACRES PERMITTED: 8.6
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond. Precip
Volati- Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet, Past 24 Hrs.
Application
lization ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist Inches
Method*
Rate** Rate"**
mg/kg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1 Crop 2
7/13/2020
150.00
(Y)
19.800
2.909
KIKRAEDC
DRY 0-<1/2"
SUR
0.5 0.30
50,000.00
4,500.00
6.99
92.534
BCP
Jul-20
150.00
(Y)
Total 2.909 Total 92.534 u.uuu
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.033 0.012 1 2.269 0.175 0.157 0.005 0.058 0.116 0.058 8.144 1 186.151 Date Lbs1Ac
Cumulative Ibs/acre Applied 0.254 0.117 16.244 2.118 1.760 0.032 I 0.485 I 1A30 I 0.270 9 51.823 I I ! B
Permit PAN Limit (Ibs/acre) 1st Crop 1 I I I I ! 99 I 9
Federal C.P.L.R. (Ibs/acre)-- 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this do ument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalt s r s b tting false information, including the possibility of fines and imprison �rzl
�r knowing violations."
G �
SIGN RE OF LAND APPLIER ATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-p.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 **** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: KINSTON, NC
LANDOWNER: W B HARGETT
OPERATOR: DEXTER EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
DACTI IA M(`M
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02945-0-0002-
ANNUAL DRY TONS APPLIED: 20.85 SITE #: NC JO 02945
PREDOMINANT SOIL SERIES: AUTRYVILLE
CROP 1 MAX. PAN: 203 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 5.2
ACRES PERMITTED: 5.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati- Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization ization
TKN Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate** Rate***
mg/kg mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
7/15/2020
125.00
(Y)
19.800
4.009
KIKRAEDC
DRY
110-<1/2"
SUR
0.5 0.30
50,000.00 4,500.00
6.99
127.531
BCP
I
Jul-20
126.00
(Y)
Total 4.009 total 1zi.Wi u.uuu
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.046 0.017 3.127 0.241 0.216 0.007 0.079 0.160 0.080 11.224 256.554 Date Lbs/Ac
Cumulative Ibs/acre Applied 0,073 0.033 4.767 0.460 0.427 0.012 0.128 0.282 0.104 16.141
Permit PAN Limit (Ibs/acre) 1st Crop 203
Federal C.P.L.R. (Ibs/acre)**** 36.6 ( 34.8 I 1,339.0 267.9 1 15.0 375.0 1 89.0 1 2,500.0
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penatt f ub n' ' g false information, including the possibility of fines and imprisonme t 7Z-i
wing violations."
Z `�
SIGNA E OF LAND APPLIER DA E
NR = Not Reported or Not Requir d *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: KINSTON, NC
1►1 aIU►PP►1 � �rl�ll : I�l'�e3 � W I
OPERATOR: DEXTER EDWARDS
CROPINAME:BERMUDAGRASS,COASTAL-
DACTI IA /Rr`D\
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02945-0-0003-
ANNUAL DRY TONS APPLIED: 75.04 SITE #: NC JO 02945
PREDOMINANT SOIL SERIES: BLANTON
CROP 1 MAX. PAN: 203 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 12.5
ACRES PERMITTED: 14.8
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati- Mineral-
Ammonia
Nitrate
PAN Applied Receiving Residual
Date or
or Wet Tons (W)
%
Residual Dry, Wet,
Past 24 Hrs.
Application
lization ization
TKN Nitrogen
and Nitrite
(Ibs/acre) Application
Month
Solids
Dry Tons/Ac
Source Moist
Inches
Method*
Rate** Rate—
mg/kg mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2 Crop 1
Crop 2
7/15/2020
450.00
(Y)
19.800
6.003
KIKRAEDC DRY
"0-<1/2"
SUR
0.5 0.30
50,000,00 4,500.00
6.99
190.991
BCP
Jul-20
450.00
(Y)
Annual Ibs/acre Applied
Cumulative Ibs/acre Applied
1st
Total 6.003
AS CD CU CR PE HG MO NI SE
0.068 0.025 4.683 0.360 0.324 0.011 0.119 0.240 0.120
0.341 0.132 20.522 3.264 2.081 0.066 0.557 1.640 0.335
Total 190.991 0.000
ZN P Lime Applied
i.809 384.215 Date Lbs/Ac
67.793
203
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 1 15.0 ' 375.0 1 89.0 1 2,500.0
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document w prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties s m'tti g false information, including the possibility of fines and impriso nt r knowing violations."
CT L +j
SIGNA E OF LAND APPLIER D TE
NR = Not Reported or Not Requi *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **' C.P.L.R.: Cumulative Pollutant Loading Rate
" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 **'** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: KINSTON, NC
R_\91exelAiN11:4 ATiYl l:/ 0CIMa1
OPERATOR: DEXTER EDWARDS
CROP 1NAME: BERMUDAGRASS,COASTAL -
DdQTi ID Mr`M
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02945-0-0005-
ANNUAL DRY TONS APPLIED: 54.20 SITE M NC JO 02945
PREDOMINANT SOIL SERIES: BLANTON
CROP 1 MAX. PAN: 203 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 9.0
ACRES PERMITTED: 9.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati- Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past24 Hrs.
Application lization ization
TKN Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids Dry Tons/Ac
Source
Moist
Inches
Method* Rate** Rate***
mg/kg mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1 Crop 2
7116/2020
325.00
(Y)
19.800 6.022
KIKRAEDC
DRY
"0-<112"
SUR 0.5 0.30
50,000.00 4,500.00
6.99
191.580
BCP
Jul-20
325.00
(Y)
Total 6.022 Total 191.580 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.069 0.025 4.697 0.361 0.325 0.011 0.119 0.241 0.120 16.861 385.401 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.136 0.051 7.641 0.794 0.624 0.016 0.209 0.494 0.185 1 26.679
Permit PAN Limit (Ibs/acre) 1st Cropl 203
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1,339.0 267.9 15.0 375.0 89.0 1 2,500.0
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a s stem esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties r bmi g false information, including the possibility of fines and impriso cot f lowing violations."
SIGNAT OF LAND APPLIER DATE
NR = Not Reported or Not RequireR *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
" Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
*` Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * *** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

FACILITY NAME: KINSTON, NC
>ITPIZil'n1�L1:A�i�l3:lJ��I�i1
OPERATOR: DEXTER EDWARDS
CROP 1NAME: BERMUDAGRASS,COASTAL -
DA TI IA !Dr`D%
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003919 FIELD#: NC-JO-02945-0-0006-
ANNUAL DRY TONS APPLIED: 58.37 SITE #: NC JO 02945
PREDOMINANT SOIL SERIES: BLANTON
CROP 1 MAX. PAN: 203 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 10.0
ACRES PERMITTED: 18.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(lbs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate—
mg/kg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
7/16/2020
350.00
(Y)
19.800
5.837
KIKRAEDC
DRY
110-<1/2"
SUR
0.5
0.30
50,000.00
4,500.00
6.99
185.685
BCP
Jul-20
350.00
(Y)
Total 6.837 Iotai iaa.oaa V.VVV
AS CD CU CR PB HG Mfl NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.067 0.025 4.553 0.350 0.315 0.010 0.116 0.233 0.117 16.342 1 373.542 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.145 0.055 8.256 0.831 0.703 0.016 i 0.220 ( 0.520 ! 0.192 I 28.810 I I t
Permit PAN Limit (Ibslacre) 1st Crop I i I 8 203 I
Federal C.P.L.R. (Ibslacre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties fo ub a ' g also information, including the possibility of fines and imprison gent r knowing violations."
Z1
SIGNRTU E F LAND APPLIER D TE
NR = Not Reported or Not Required **" Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation `*'* C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

SECTION 4

SUMM111 Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOL0C4r;S,INC Cuyahoga Falls, Ohio44223
Arraly0ca1 Laboralorfas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
May 06, 2020
Chris Wynne
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Kinston
Dear Chris Wynne: Order No.: 20041278
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/24/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Califomia 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-011-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada 011009232020-1, New
Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon 01I200001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah 011009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 32

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 20041278
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 5/6/2020
CLIENT: Synagro
Project: Kinston
WorkOrder Narrative:
20041278: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20041278-OOIA TCLP-SVOC_8270E: Surrogate outside recovery limits. Minimum method criterion of
one surrogate within established recovery limits was met.
Analytical Sequence QC Notes:
CCV 40ppm 36593 SVOC-MSTR S(8270): Surrogate outside recovery limits. Minimum method
criterion of one surrogate within established recovery limits was met.
PEST ccv 250PPB SVOC-CPEST_NPW(8081): Ending CCV exhibits outlying recoveries for several
analytes. Matrix influence possibly affected instrument calibration. Sample is ND
Original
Page 2 of 32

MMIT
summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� Wo#: 20041278
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co Date: 5/6/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 32

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHHOLOGNUS, INC. Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Kinston
Lab SampleID Client Sample ID
20041278-001 Kinston WWTP
Tag No Date Collected
4/22/2020 11:00:00 AM
Workorder
Sample Summary
WO#: 20041278
06 May-20
Date Received Matrix
4/24/2020 10:10:00 AM Sludge
Page 4 of 32

SUMM'
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHN❑ L0G1E5, IHC
Cuyahoga Falls, Ohio 44223
WO#: 20041278
ArWyft cal taboralonag
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
06 May-20
Client:
Synagro
Project:
Kinston
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
20041278-OOIA Kinston WWTP 4/22/2020 11:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
5/1/2020 3:00:00 PM
Percent Solids by SM2540Mod
4/28/2020 4:25:00 PM
pH (SW9045D)
4/30/2020 10:06:00 AM
Reactive Cyanide (9014/7.3.3.2)-Solid
4/27/2020 9:09:00 AM
Reactive Sulfide (9034)/7.3.4.2
4/27/2020 9:09:00 AM
TCLP Herbicides by EPA 8321B
4/29/2020 2:00:00 PM 5/2/2020 5:35:00 AM
TCLP Mercury Analysis (SW1311/7474/29/2020 2:00:00 PM
5/1/2020 9:55:00 AM 5/1/2020 1:05:00 PM
TCLP Metals Analysis (SW1311/60104/29/2020 2:00:00 PM
4/30/2020 8:00:00 AM 5/1/2020 1:00:58 PM
TCLP Metals Analysis (SW1311/60104/29/2020 2:00:00 PM
4/30/2020 8:00:00 AM 5/1/2020 12:04:29 PM
TCLP Pesticides Analysis (SW1311/8(4/29/2020 2:00:00 PM
4/30/2020 1:00:00 PM 5/4/2020 7:01:00 PM
TCLP Semi-Volatiles Analysis 4/29/2020 2:00:00 PM
4/30/2020 1:00:00 PM 5/4/2020 4:45:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
4/29/2020 2:00:00 PM 4/30/2020 12:39:00 PM
Original
Page 5 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20041278
Date Reported: 5/6/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/22/2020 11:00:00 AM
Lab ID: 20041278-OOIA
Project: Kinston
Client Sample ID Kinston WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: MJM
1 5/1/2020 1:05:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
5/1/2020 12:04:29 PM
TCLP Badum(Ba)
ND
5.00
mg/L
1
5/1/2020 12:04:29 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
5/1/2020 12:04:29 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
5/1/2020 12:04:29 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
5/1/2020 12:04:29 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
5/1/2020 12:04:29 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
5/1/2020 1:00:58 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.500
mg/L
5
5/4/2020 4:45:00 PM
2,4,5-Trichlorophenol
ND
1.25
mg/L
5
5/4/2020 4:45:00 PM
2,4,6-Trichlorophenol
ND
1.25
mg/L
5
5/4/2020 4:45:00 PM
2,4-Dinitrotoluene
ND
0.0500
mg/L
5
5/4/2020 4:45:00 PM
Cresols, Total
ND
25.0
mg/L
5
5/4/2020 4:45:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
5
5/4/2020 4:45:00 PM
Hexachlorobenzene
ND
0.0100
mg/L
5
5/4/2020 4:45:00 PM
Hexachloroethane
ND
0.500
mg/L
5
5/4/2020 4:45:00 PM
Nitrobenzene
ND
0.500
mg/L
5
5/4/2020 4:45:00 PM
Pentachlorophenol
ND
1.25
mg/L
5
5/4/2020 4:45:00 PM
Pyridine
ND
1.25
mg/L
5
5/4/2020 4:45:00 PM
Surr: 2-Fluorophenol
95.3
10 - 109
%Rec
5
5/4/2020 4:45:00 PM
Surr: Phenol-d6
91.8
10 - 109
%Rec
5
5/4/2020 4:45:00 PM
Surr: Nitrobenzene-d5
73.7
19 - 120
%Rec
5
5/4/2020 4:45:00 PM
Surr: 2,4,6-Tribromophenol
120
10 - 120
%Rec
5
5/4/2020 4:45:00 PM
Surr: 2-Fluorobiphenyl
90.5
22 - 117
%Rec
5
5/4/2020 4:45:00 PM
Surr: p-Terphenyl-d14
125
34 - 116
S %Rec
5
5/4/2020 4:45:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation
exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 6 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://n,n-m,.settek.coin
Analytical Report
(base report)
WO#: 20041278
Date Reported: 5/6/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 4/22/2020 11:00:00 AM
Lab ID: 20041278-OOIA
Project: Kinston
Client Sample ID Kinston WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
17.6
Surr: DCB
19.3
TCLP HERBICIDES BY EPA 8321 B
2,4-D ND
2,4,5-TP ND
Surr: 2,4-Dichlorophenylacetic aci 105
SW8081 SW351OC Analyst: MES
0.125
mg/L
5
5/4/2020 7:01:00 PM
0.250
mg/L
5
5/4/2020 7:01:00 PM
0.0125
mg/L
5
5/4/2020 7:01:00 PM
0.0125
mg/L
5
5/4/2020 7:01:00 PM
0.0125
mg/L
5
5/4/2020 7:01:00 PM
0.0125
mg/L
5
5/4/2020 7:01:00 PM
0.0125
d mg/L
5
5/4/2020 7:01:00 PM
10 - 119
%Rec
5
5/4/2020 7:01:00 PM
10 - 119
%Rec
5
5/4/2020 7:01:00 PM
SW8321A SW1311M Analyst: BJH
0.500 mg/L 50 5/2/2020 5:35:00 AM
0.500 mg/L 50 5/2/2020 5:35:00 AM
70 - 130 %Rec 50 5/2/2020 5:35:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260 SW1311M Analyst: RMT
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
1,2-Dichloroethane
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
MEK
ND
5.00
mg/L 50 4/30/2020 12:39:00 PM
Benzene
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
Carbon tetrachloride
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
Chlorobenzene
ND
2.50
mg/L 50 4/30/2020 12:39:00 PM
Chloroform
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
Tetrachloroethene
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
Trichloroethene
ND
0.250
mg/L 50 4/30/2020 12:39:00 PM
Vinyl chloride
ND
0.100
mg/L 50 4/30/2020 12:39:00 PM
Surr: 4-Bromofluorobenzene
91.5
70 - 130
%Rec 50 4/30/2020 12:39:00 PM
Surr: Di brom ofl uorom ethane
100
70 - 130
%Rec 50 4/30/2020 12:39:00 PM
Surr: Toluene-d8
99.3
70 - 130
%Rec 50 4/30/2020 12:39:00 PM
Qualifiers: B Analyte detected in the associated
Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 7 of 32

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arralyt9cal Laboralories TEL: [phone] FAX. [phone] WO#: 20041278
Website: http://www.settek.com Date Reported: 5/6/2020
CLIENT: Synagro
Matrix: SLUDGE
Lab ID: 20041278-OOIA
Project: Kinston
Client Sample ID Kinston WWTP
Tag Number:
Collection Date:
4/22/2020 11:00:00 AM
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCISOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495 mg/Kg
1
4/27/2020 9:09:00 AM
RCISOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
mm/sec
1
5/1/2020 3:00:00 PM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: MAH
Percent Solids
17.8
%
1
4/28/2020 4:25:00 PM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH
7.1
s.u.@20.7C
1
4/30/2020 10:06:00 AM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
4/27/2020 9:09:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
PL
Permit Limit
RL
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 8 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
frSU
MM'EF 3310 Win St.
Anal�7n tes Report
ENOROMMEWAL IrECHNOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20041278
Wehsite: http://www.settek.com
06-May-20
Client: Synagro
State: NW
Project: Kinston
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20041278-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
N
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
N
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Key
Key
NC WW SCM A Accredited
NC WW SCM N Not Accredited
Version #2
Page 9 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Anal�7n tes Report
EMOROMMEWAL IrECHHOL.OG{r,S,
INC, Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
20041278
Wehsite: http://www.settek.com
06-May-20
Client: Synagro
State: NW
Project: Kinston
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
20041278-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited
Version #2
Page 10 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: 43196
Sample ID: MB-43196
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/29/2020
RunNo: 112443
Client ID: PBS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 5/1/2020
SegNo: 2759079
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Silver(Ag) ND 0.500
Sample ID: LCS-43196
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/29/2020
RunNo: 112443
Client ID: LCSS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 5/1/2020
SegNo: 2759080
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Silver(Ag)
2.18 0.500 2.000 0 109 80 120
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 11 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43196
WO#: 20041278
06-May-20
Sample ID: TCLP BLANK 4-30-2
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/30/2020
RunNo: 112438
lient ID: PBS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 5/1/2020
SegNo: 2758451
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 12 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 20041278
06-May-20
Client: Synagro
Project: Kinston BatchID: 43196
Sample ID: MB-43196
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/29/2020
RunNo: 112326
Client ID: PBS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 4/29/2020
SegNo: 2755399
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-43196
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/29/2020
RunNo: 112326
Client ID: LCSS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 4/29/2020
SegNo: 2755400
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.96
0.500
2.000
0
98.1
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
101
80
120
TCLP Cadmium(Cd)
1.97
0.100
2.000
0
98.5
80
120
TCLP Chromium(Cr)
2.00
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
2.07
0.500
2.000
0
104
80
120
TCLP Selenium(Se)
1.99
0.0500
2.000
0
99.5
80
120
TCLP Silver(Ag)
2.05
0.500
2.000
0
102
80
120
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43196
WO#: 20041278
06-May-20
Sample ID: TCLP BLANK 4-29-2
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/29/2020
RunNo: 112326
lient ID: PBS
Batch ID: 43196
TestNo: SW6010D SW3010A
Analysis Date: 4/29/2020
SegNo: 2755401
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43209
WO#: 20041278
06-May-20
Sample ID: MB-43209
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 4/29/2020
RunNo: 112431
lient ID: PBS
Batch ID: 43209
TestNo: SW8260 SW1311M
Analysis Date: 4/30/2020
SegNo: 2758003
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
M-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.100
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
48.6
Surr: Dibromofluoromethane
50.1
Surr: Toluene-d8
50.2
50.00 97.2 70 130
50.00 100 70 130
50.00 100 70 130
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43218
WO#: 20041278
06-May-20
Sample ID: MB-43218
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
lient ID: PBS
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2758485
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.783
Surr: Phenol-d6
0.756
Surr: Nitrobenzene-d5
0.678
Surr: 2,4,6-Tribromophenol
1.07
Surr: 2-Fluorobiphenyl
0.779
Surr: p-Terphenyl-d14
1.13
1.000
78.3
10
109
1.000
75.6
10
109
1.000
67.8
19
120
1.000
107
10
120
1.000
77.9
22
117
1.000
113
34
116
QC+
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43218
WO#: 20041278
06-May-20
Sample ID: LCS-43218
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
lient ID: LCSS
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2758486
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.426
0.100
0.8000
0
53.2
36.4
130
2,4,5-Trichlorophenol
0.809
0.250
0.8000
0
101
31.7
132
2,4,6-Trichlorophenol
0.796
0.250
0.8000
0
99.4
31.1
133
2,4-Dinitrotoluene
0.818
0.0500
0.8000
0
102
43.3
130
o-Cresol
0.637
0.250
0.8000
0
79.6
32.9
130
Cresols, Total
ND
5.00
1.600
0
79.8
31.7
130
Hexachloro-1,3-butadiene
0.427
0.0200
0.8000
0
53.4
31.4
130
Hexachlorobenzene
0.769
0.0500
0.8000
0
96.2
43.1
130
Hexachloroethane
0.393
0.100
0.8000
0
49.1
36.5
130
Nitrobenzene
0.584
0.100
0.8000
0
73.0
39.5
130
Pentachlorophenol
0.834
0.250
0.8000
0
104
34
130
Pyridine
0.428
0.250
0.8000
0
53.6
10
130
Surr: 2-Fluorophenol
0.851
1.000
85.1
17.1
130
Surr: Phenol-d6
0.836
1.000
83.6
10
130
Surr: Nitrobenzene-d5
0.686
1.000
68.6
32.6
130
Surr:2,4,6-Tribromophenol
1.20
1.000
120
4.43
130
Surr:2-Fluorobiphenyl
0.813
1.000
81.3
41.8
130
Surr: p-Terphenyl-d14
1.18
1.000
118
36.4
130
QC+
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43218
WO#: 20041278
06-May-20
Sample ID: 20041350-002AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
lient ID: BatchQC
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2760532
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.558
0.200
0.8000
0
69.7
33.8
126
2,4,5-Trichlorophenol
0.900
0.500
0.8000
0
113
28.7
144
2,4,6-Trichlorophenol
0.921
0.500
0.8000
0
115
12.8
153 mQC+
2,4-Dinitrotoluene
0.914
0.100
0.8000
0
114
20.4
155
o-Cresol
0.755
0.500
0.8000
0
94.4
10
148
Cresols, Total
ND
10.0
1.600
0
93.0
10
148
Hexachloro-1,3-butadiene
0.528
0.0400
0.8000
0
66.0
29
126
Hexachlorobenzene
0.913
0.100
0.8000
0
114
33.7
134
Hexachloroethane
0.540
0.200
0.8000
0
67.5
32.8
132
Nitrobenzene
0.676
0.200
0.8000
0
84.6
20
158
Pentachlorophenol
0.871
0.500
0.8000
0
109
10
176
Pyridine
ND
0.500
0.8000
0
61.8
10
130
Surr:2-Fluorophenol
0.930
1.000
93.0
3.39
130
Surr: Phenol-d6
0.946
1.000
94.6
5
130
Surr: Nitrobenzene-d5
0.797
1.000
79.7
14.5
154
Surr: 2,4,6-Tribromophenol
1.34
1.000
134
19.5
130 S
Surr:2-Fluorobiphenyl
0.938
1.000
93.8
34.4
130
Surr: p-Terphenyl-d14
1.28
1.000
128
8.86
156
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 18 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Kinston BatchID: 43218
WO#: 20041278
06-May-20
Sample ID: 20041350-002AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/30/2020
RunNo: 112439
Dient ID: Batch=
Batch ID: 43218
TestNo: SW8270 SW3510C
Analysis Date: 5/1/2020
SegNo: 2760533
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.476
0.200
0.8000
0
59.4
33.8
126
0.5576
15.9
30
2,4,5-Trichlorophenol
0.807
0.500
0.8000
0
101
28.7
144
0.9004
11.0
30
2,4,6-Trichlorophenol
0.799
0.500
0.8000
0
99.9
12.8
153
0.9208
14.1
30 mQC+
2,4-Dinitrotoluene
0.855
0.100
0.8000
0
107
20.4
155
0.9140
6.65
30
o-Cresol
0.672
0.500
0.8000
0
84.0
10
148
0.7548
11.6
30
Cresols, Total
ND
10.0
1.600
0
83.0
10
148
0
0
30
Hexachloro-1,3-butadiene
0.492
0.0400
0.8000
0
61.5
29
126
0.5280
7.06
30
Hexachlorobenzene
0.834
0.100
0.8000
0
104
33.7
134
0.9128
8.97
30
Hexachloroethane
0.478
0.200
0.8000
0
59.8
32.8
132
0.5400
12.1
30
Nitrobenzene
0.644
0.200
0.8000
0
80.6
20
158
0.6764
4.85
30
Pentachlorophenol
0.783
0.500
0.8000
0
97.9
10
176
0.8708
10.6
30
Pyridine
ND
0.500
0.8000
0
48.0
10
130
0
0
30 m
Surr: 2-Fluorophenol
0.871
1.000
87.1
3.39
130
0
Surr: Phenol-d6
0.881
1.000
88.1
10
130
0
Surr: Nitrobenzene-d5
0.742
1.000
74.2
14.5
154
0
Surr: 2,4,6-Tribromophenol
1.25
1.000
125
19.5
130
0
Surr:2-Fluorobiphenyl
0.846
1.000
84.6
34.4
130
0
Surr: p-Terphenyl-d14
1.18
1.000
118
8.86
156
0
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 19 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INC
Cuyahoga Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: 43232
TCLP Mercury ND 0.00200
TCLP Mercury 0.00396 0.00200 0.00400 0 99.0 80 120
TCLP Mercury ND 0.00200
Sample ID: 20041350-004AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: Batch=
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2758994
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00514 0.00200
0.00400 0 128 75
125
S
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 20 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: 43232
TCLP Mercury 0.00515 0.00200 0.00400 0 129 75 125 0.00514 0.194 20 S
TCLP Mercury ND 0.00200
Sample ID: TCLP BLANK 2 5-1-
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: PBS
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2759005
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 21 of 32

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 20041278
06-May-20
Client: Synagro
Project: Kinston BatchID: 43232
Sample ID: M1132-43232
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/1/2020
RunNo: 112445
Client ID: PBS
Batch ID: 43232
TestNo: SW7470A SW7470A
Analysis Date: 5/1/2020
SegNo: 2759012
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
ND 0.00200
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: R112323
Cyanide, Reactive ND 0.485
Cyanide, Reactive 9.44 0.495 10.00 0 94.4 85 115
Cyanide, Reactive ND 0.500 0.5000 0 81.0 65 135
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754434
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
8.98 0.485
10.00 0 89.8 75
125
Qualifies: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 23 of 32

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20041278
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 06-May-20
Client: Synagro
Project: Kinston BatchID: R112323
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754434
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20041299-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 112323
Client ID: Batch=
Batch ID: R112323
TestNo: SW9014
Analysis Date: 4/27/2020
SegNo: 2754435
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.35 0.490 10.00 0 93.5 75 125 8.984 3.97 10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 24 of 32

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20041278
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 06-May-20
Client: Synagro
Project: Kinston BatchID: R112336
Sample ID: MB-R112336
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 112336
Client ID: PBS
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755023
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R112336
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 112336
Client ID: LCSS
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755024
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
3120 25.0 3280 0 95.1 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 25 of 32

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20041278
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 06-May-20
Client: Synagro
Project: Kinston BatchID: R112336
Sample ID: 20041299-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 112336
Client ID: Batch=
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755029
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3080 25.0 3280 0 93.9 75 125
Sample ID: 20041299-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 112336
Client ID: Batch=
Batch ID: R112336
TestNo: SW9034
Analysis Date: 4/27/2020
SegNo: 2755030
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3180 25.0 3280 0 97.0 75 125 3080 3.19 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 26 of 32

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 20041278
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 06-May-20
Client: Synagro
Project: Kinston BatchID: R112363
Sample ID: MB-R112363
SampType: MBLK
TestCode: PctSolid_S(2 Units: %
Prep Date:
RunNo: 112363
Client ID: PBS
Batch ID: R112363
TestNo: A2540B
Analysis Date: 4/28/2020
SegNo: 2755968
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Percent Solids ND 0 0
Sample ID: 20041364-007ADUP
SampType: DUP
TestCode: PctSolid_S(2 Units: %
Prep Date:
RunNo: 112363
Client ID: Batch=
Batch ID: R112363
TestNo: A2540B
Analysis Date: 4/28/2020
SegNo: 2755970
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Percent Solids 20.5 0 0 20.77 1.43 5
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 27 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: R112377
pH 7.0 7.0 0 99.6 98.6 101.4
pH 7.8 7.8 0.4 5
Sample ID: PH 7 CHECK
SampType: LCS
TestCode: PH_DW(4500 Units: s.u.@21.9C
Prep Date:
RunNo: 112377
Client ID: LCSW
Batch ID: R112377
TestNo: SW9045D
Analysis Date: 4/30/2020
SegNo: 2756616
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 28 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,_3, INCCuyahoga
Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX. [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: R112457
Ignitability 7.96 7.240 0 110 70 130
Ignitability non-flammable 0 0 20
Ignitability >2.2 0 0 20
Sample ID: 20041479-005ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 112457
Client ID: Batch=
Batch ID: R112457
TestNo: SW1030
Analysis Date: 5/1/2020
SegNo: 2759310
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability >2.2 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 32

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ Lggir,_3, INC
Cuyahoga Falls, Ohio 44223
WO#: 20041278
Arrafyt�cal iaboralorfas
TEL: [phone] FAX. [phone]
Website: http://www.settek.com
06-May-20
Client:
Synagro
Project:
Kinston
BatchID: R112457
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Sample ID: 20041282-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 112457
Client ID: Batch=
Batch ID: R112457
TestNo: SW1030
Analysis Date: 5/1/2020
SegNo: 2759316
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifies: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 30 of 32

DBPix Ev n Summit I'naironmeaital 7kchnolo ies, Inc,
�3M Win Slrecl
Cuv.lhgni Falls. Uhis>' •4•3_'?3 el: 3.10,2;3•821 I F-w 331}.2i?.44X
Analysis Request/Chain of Custody
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�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTALTECHNOLOGiES.lftC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafyacal Laboralnrlas TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 20041278 RcptNo: 1
Logged by: Jacqueline Rasile 4/24/2020 10:10:00 AM
Completed By: Jacqueline Rasile 4/24/2020 2:29:13 PM
Reviewed By: Sara E. Kidd 4/24/2020 3:45:50 PM
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes d❑ No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes V No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
V
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
V
No ❑
g. Are samples (except VOA and ONG) properly preserved?
Yes
V
No ❑
10. Was preservative added to bottles?
Yes
❑
No V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No V
13. Does paperwork match bottle labels?
Yes
V
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
V
No ❑
15. Is it clear what analyses were requested?
Yes
0
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
15.4
Goodl
Not Present
Page 32 of 32

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Kinston WQ Permit Number: WQ0003919
WWTP Name: Kinston Regional WRF NPDES Number: NCO024236
Monitoring Period: From 01/01/20 To 12/31/20
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahle to alternative nerfnrmed (Glace A nr Clacc Rl emmnlete the fnllnwinu mnnitnrinu data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 h
MPN
MPN/g
Coliform
power per gram
of total solids
<4710
20100
245000
CFU/g
0
Annually
Grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Kenneth Stevens, Wastewater Superintendent
Preparer Name and Title ( prj t or type) Land Applier Name and Title (if applicable) (type or print)
Signature of Prep Date Signature of Land Applier (if applicable)
*Preparer is de 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Cameron Testing Services, InC. Laboratory Report
Client: Synagro CTSPro.
Project- Kinston WWTP Regulatory
Sample Information
Sampled C. Wynne DO* 04rM0 RacPMW
Analyses and Results
NC DENR 9654
NC FHHS 937799
US EPA ##CCU 191$
004-160
var,
S_ Puckett Dab 04P22120
Lab 10 n* to
Anah la
R0501t
O
O
e
r
Ro4`4roflCo
2004-Y 60 -1
, . ,f
Fac_ CoWbwo -S
<7410
crura
7410
p4rMU
RL Q22D - Mf
-2
<4710
cram
4710
0
27900
mro
6970
-4
11600
mog
5800
-5
88701)
CrLvg
4930
-6
2450M
Cnro
6140
-7
c5450
c
54M
Gaomeao
20100
-1
CO
TSM
13.58%
av+
041MM
Rt 2%0G-76
-2
2 11 ,2 I4
4.41
0
14,4%
001
-4
17.2%
a.m
-5
20.3%
cot
-6
16-3%
a.o1
-7
18.4%
001
Rwwt
RWA Mr
Pr*NA Moog" Datf
219 S. Surtic Str 919 2L612Q
; wmfixd ,VL` 17330 dffMr11 A OMkm

14 S SAaelft su.
SantFd. NC 773M
Ph,nnr. e11ci-POR 47db
Cameron Testing Services, Inc.
NC WWiGVV Cert. #fi54 NC PHHS OM # 377" US EPA NG01919
Chain of Custody
Page of
cornvanY--- f1 1 O
Email;
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as a
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v0 4 - 5
Address [City, 284 13oCge Fed.
Fax;
be (YIN)
State.Yigl Mocksville, NC 77028
Notes
perrm(Y"
Project; 4:�i4tI�� . r-t I
Rush(YAI) Due:
,i
C W Now ow C rr s _OI
-;; 4%_
s'`iQrrshu�:
Sample Information
Numbor of bottles
Requested Analysis
w W
OL-0 sc
Z
Ep
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PMservatives: 1,u)r1preservej f+,.Ckl
CT Lab
Sample ID
M E
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Received:
DaFeMme
ti
Rosh work till require prior eppmval Add9ion ll charges wrlI apply

Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 7:54am
Sampled By: SF
Analysis Date/Time: 6/30/20 7:57am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 20.3 degrees Celsius
End Temperature: 23.5 degrees Celsius
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
8.96
1
5.52
2
3.9
3
2.53
4
1.36
5
0.78
6
0.48
7
0.32
8
0.26
9
0.24
10
0.22
11
0.2
12
0.18
13
0.17
14
0.16
15
0.15
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
21.85 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate:1 0.04 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1

10
aM
E
c
a�
a�
x 4
O
a�
0
cn
cn
-2
Oxygen Uptake Rate Chart
y
-0.4055
+ 5.03
8
1
2
3
4
5
6
7
8
9
10
11
12
1
14
15
16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 8:34am
Sampled By: SF
Analysis Date/Time: 6/30/20 8:38am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 21.3 degrees Celsius
End Temperature: 23.7 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.26
1
6.05
2
5.61
3
5.21
4
4.78
5
4.33
6
3.87
7
3.46
8
3.13
9
2.87
10
2.65
11
2.43
12
2.24
13
2.04
14
1.85
15
1.64
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
22.5 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
oil

H.,
7
0
a� 5
E
le
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 9:21am
Sampled By: SF
Analysis Date/Time: 6/30/20 9:25am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 21.7 degrees Celsius
End Temperature: 24.3 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
8.38
1
6.22
2
5.94
3
5.72
4
5.53
5
5.42
6
5.27
7
5.17
8
5.1
9
5.01
10
4.95
11
4.85
12
4.74
13
4.59
14
4.54
15
4.43
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
3

9
H.,
7
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 9:50am
Sampled By: SF
Analysis Date/Time: 6/30/20 9:53am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 21.6 degrees Celsius
End Temperature: 24.3 degrees Celsius
Dissolved Oxygen Level
(mg/1)
8.15
6.91
6.62
6.41
5.7
760
5.4
5.�
5.1
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
22.95 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
4

9
H.,
7
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 10:30am
Sampled By: SF
Analysis Date/Time: 6/30/20 10:33am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 22.3 degrees Celsius
End Temperature: 24.6 degrees Celsius
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
7.9
1
7.4
2
7.21
3
7.07
4
6.88
5
6.72
6
6.59
7
6.48
8
6.38
9
6.29
10
6.23
11
6.14
12
6.05
13
5.96
14
5.86
15
5.77
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
23.45 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.20 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
5

9
E:3
7
am
E
m
5
x
O
m
4
0
cn
cn
0 3
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: KRWRF
Biosolids Permit Number: WQ0003919
Date: 6/30/2020
Digester Temperature: 24
Sampling Date/Time: 6/30/20 10:55am
Sampled By: SF
Analysis Date/Time: 6/30/20 10:58am
Analyzed By: SF
Sample Volume: 300 milliliters
Total Solids: 2 % Dry Solids
Beginning Temperature: 23.2 degrees Celsius
End Temperature: 24.7 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.79
1
6.78
2
6.34
3
5.88
4
5.42
5
4.92
6
4.46
7
3.96
8
3.43
9
2.92
10
2.39
11
1.91
12
1.45
13
1.1
14
0.83
15
0.65
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
mg Oxygen/hr
mg Oxygen/g/hr
23.95 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate:1 0.86 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

9
E:3
7
am
E
m
5
x
O
m
4
0
cn
cn
0 3
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

SECTION 6

Agricultural Lime Application Log
2020
Project: Kinston Regional WRF
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(tons/acre)
Tons/Acre
Applied
Date Applied
NC-JO-2944-1
5.4
0.8 0.0
NC-JO-2944-2 =1
5.1 11
1.3 0.0
NC-JO-2945-2
4.9
1 1.2 0.0
NC-JO-2945-3
5.9
1 0.0 0.0
NC-JO-2945-5
5.4
1 0.9 0.0
NC-JO-2945-6
5.0
1 1.4 0.0 *
Lime will be spread in Spring 2021 *

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031966
Client:
Patricia Edwards
Advisor:
Chris Wynne
vo-
Predictive
Edward Land & Cattle
483 Bogar Road
209 Willard Edwards Rd
Mocksville, NC 27028
:...$'
Soil Report Mehlich-3 Extraction
Beulaville, NC 28518
'
- -
Links to Helpful Information
Sampled County: Jones
Client ID: 366610
Advisor
ID: 509090
Sampled: 05/21/2020 Received: 06/09/2020 Completed: 06/16/2020 Farm: JO-2944
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., E 0.8 60-80 0
80
25 0 0
0
0
0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.97 1.33
5.4 70 1.6 5.4 589 31 59 8
50
73
61 609
609
414
0.1 2
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 1.3 60-80 0
110
0 0 0
0
0
0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
1.74 1.30
6.2 65 2.2 5.1 243 16 53 10
26
61
54 1052
1052
360
0.1 2
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., E 1.5 60-80 0
110
0 25 0
0
0
0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
2.15 1.34
6.2 62 2.3 4.9 82 15 53 8
24
40
41 333
333
156
0.1 2
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SLO31966
Patricia Edwards
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL002601
Client: Patricia Edwards Advisor: Chris Wynne
vo- Predictive
Edward Land & Cattle 483 Bogar Road
209 Willard Edwards Rd Mocksville, NC 27028
:...$' Soil Report Mehlich-3 Extraction
Beulaville, NC 28518
Links to Helpful Information
Sampled County: Jones
Client ID: 366610 Advisor ID: 509090
Sampled: 07/10/2020 Received: 08/19/2020 Completed: 08/26/2020 Farm: jo-2945
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be
detrimental to crop production. The C and Z symbols are printed on your report for soil test
Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with
zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids
and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce
potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for
copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field.
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., E 1.2 60-80 0
120 25 0 0 0 0 0
Note: 12
2 - Bermuda hay/past., M 0.0 180-220 0
210 $ 0 0 0 0 0
Note: 12 Note:
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
1.14 1.32 4.3 57 1.8 4.9 181 13 46 9
41 95 74 74 345 345 163 0.1 2
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Bermuda hay/past., E 0.0 60-80 0
80 0 0 0 Z 0 0
Note: 12 Note:
2- Bermuda hay/past., M 0.0 180-220 0
160 0 0 0 Z 0 0
Note: 12 Note:
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.46 1.28 9.4 83 1.6 5.9 692 29 69 12
64 135 98 98 2278 2278 505 0.1 1
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL002601
Patricia Edwards
Page 2 of 3
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 0.9
60-80 0
80
0
0
0
0
0
0
Note: 12
2- Bermuda hay/past., M 0.0
180-220 0
170
0
0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.51 1.30 7.7
76 1.8 5.4 635 28
65 9
65
114
85
85
1816
1816
438
0.1
1
Sample ID: 6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., E 1.4
60-80 0
100
0
0
0
Z
0
0
Note: 12 Note: $
2- Bermuda hay/past., M 0.0
180-220 0
180
0
0
0
Z
0
0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.60 1.29 5.4
59 2.2 5.0 369 22
48 9
46
130
95
95
2352
2352
428
0.0

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002601
Patricia Edwards
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm