NC0003174_Response Multiple Notices_20210217

Diamond Shoal Seafood Inc. -PO Box 610, Oriental -NC 28571.
252-249-0123 Phone, 252-249-2337 Fax
02/17/2021
NC Department of Environmental Quality
943 WASHINGTON ST.
Washington, NC 27889
20/
To whom it may concern:
This is in response to the Certified letters we received for Diamon Shoal Seafood Inc. Permit #0007609
We hold 2 permits:
Diamond Shoal Seafood Inc. Permit # 0007609
Fulcher's Point Pride Seafood Inc. Permit # 0003174
I have enclosed copies of Envirochem for our,water samples, for both locations, for the moths of :
July 2020 for Diamond Shoal Seafood.
August for Diamond Shoal Seafood and Fulcher's Point Pride.
September for Diamond shoal Seafood and Fulcher's Point Pride.
No Flow for neither Company for October.
November for Diamond Shoal Seafood and Fulcher's Point Pride.
No Flow for Dec. 2020 and Jan. 2021 for neither Company.
No Flow so far for February 2020 for Fulcher's Point Pride Seafood, and sample will be taken for
Diamond shoal Seafood. Early next week.
If you will notice the report for August 2020 for Fulcher's Point Pride Seafood was submitted, the data
for Diamond Shoal Seafood was submitted under this report by error.
Didn't know how to correct it.
I allowed this to get away from me, until I tried to make sense of it and it was to confusing, at this point I
am not sure I am entering the information correctly.
I know I need to get this situation handled, and I really need your help to do it.
Could someone please call me and walk me through this or could I make an appointment and come to
Washington and have someone help me?
I appreciate your help in this matter.

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Pamlico
ORC CERT NUMBER: 995491
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
Composite Sample Time
Total Composite Time
Operator Arrival Time
Operator Time On Site
0
u cg
c
No Reporting Reason""
50050
00010
00400
50060
C0530
00300
C0600
C0665
00556
Monthly
Monthly
Monthly
Monthly
Quarterly
Monthly
Quarterly
Quarterly
Monthly
Estimate
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
TEMP-C
pH
CHLORINE
TSS - Conc
DO
TOTAL N -
TOTAL P - Cone
OIL-GRSE
2400 clock
Hrs
2400 dock
Hrs
YARN
mgd
deg c
su
ug/I
mg/1
mg/I
mg/1
mg/I
mg/1
1
2
3
4
5
6
7
8
9
10
1
12
13
14
15
16
17
10
19
20
21
22
23
24
25
26
27
28
2600
29.1
7.82
-10
-2.5
7.59
1
0.08
5
29
30
31
Mon hly Average Limit:
15
Monthly Average:
2600
29.1
-10
-2.5
7.59
1
0.08
5
Daily Maximum:
2600
29.1
7.82
-10
-2.5
7.59
1
0.08
5
Daily Minimum:
2600
29.1
7.82
-10
-2.5
7.59
1
0.08
5
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pd0

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Composite Sample Time
Total Composite Time
Operator Arrival Time
Operator Time On Site
0
V
a
0
No Reporting Reasonetr•
2400 clock
Hes
2400 clock
Hrs
YAWN
I
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Mon hly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: YES
2
Composite Sample Time
Total Composite Time
Operator Arrival Time
Operator Time On Site
p
U
0
O
It
1.
X
Z
50050
00010
00400
50060
QD530
00300
C0600
C0665
00556
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Quarterly
Quarterly
Monthly
Estimate
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
TEMP-C
pH
CHLORINE
TSS - Qty Daily
DO
TOTAL N N.
TOTAL P - Cone
OIL -CASE
2400 clock
H.
2400 clock
Hrs
YARN
mgd
deg c
su
ug/
Ibs/day
mg/I
mg/I
mg/I
Ibs/day
t
2
3
4
5
6
7
8
9
10
1
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Mon hly Average Limit
33
0.9
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: YES (Continue)
r
q
Composite Sample Time
EB.
F
Operator Arrival Time
0;
—
i
O
ORC On Site?*•
2400 clock
Hrs
2400 clock
Hrs
Y/B/N
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
1€
19
20
21
22
23
24
25
26
27
28
29
30
31
Monthly Average Limit:
Monthly Avenge:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 003 NO DISCHARGE*: YES
E
F
fi
g
e
Total Composite Time
Operator Arrival Time
Operator Time On Site
+
1
p`
0
G
=
s
_
;
50050
00010
00400
50060
QD530
00300
C0600
C0665
00556
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Quarterly
Quarterly
Monthly
Estimate
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
TEMP-C
p11
CHLORINE
TSS - Qty Daily
DO
TOTAL N -
TOTAL P - Cone
OIL-GRSE
2400 clock
H.
2400 clock
Hrs
YARN
mgd
deg c
.,u
ug/l
lbs/day
mg/I
mg/1
mg/1
lbs/day
3
4
7
11
II
12
13
14
15
16
17
19
20
21
22
23
24
25
2G
27
28
29
30
31
Monthly Avenge Limit:
57
I0
Monthly Avenge:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 003 NO DISCHARGE*: YES (Continue)
C
E
i-
E
U
F E
-
E
U
o
F
E
4
_
a
u
O
Operator Time On Site
ORC On Site^*•
No Reporting Reason....
2400 clock
Ws
2400 clock
Hrs
Y/B/N
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Mon hly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NFDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: YES
Composite Sample Time
Total Composite Time
Operator Arrival Time
Operator Time On Site
el
ci
Y
re
No Reporting Reason•••"
50050
00010
00400
50060
QD530
00300
C0600
C0665
00556
Monthly
Monthly
Monthly
Monthly
Monthly
Monthly
Quarterly
Quarterly
Monthly
Estimate
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
TEMP-C
pH
CHLORINE
TSS - Qty Daily
DO
TOTAL N -
TOTAL P - Cone
OIL-GRSE
2400 clock
Hrs
2400 dock
Hrs
Y/B/N
mgd
deg c
su
ug/1
Ibs/day
mg/I
mg/I
mg/I
lbs/day
3
4
5
6
7
8
9
10
1
12
13
14
15
16
17
I8
19
20
21
22
23
24
25
26
27
28
29
30
31
Monthly Average Limit:
10
1.4
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycic; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174 PERMIT VERSION: 5.0 PERMIT STATUS: Active
FACILITY NAME: Fulcher's Point Pride Seafood CLASS: PCNC COUNTY: Pamlico
OWNER NAME: Fulcher's Point Pride Seafood ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2020 (August 2020) VERSION: 1.0
STATUS: Submitted
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: YES (Continue)
Composite Sample Time
Total Composite Time
Operator Arrival Time
o
E
F
O
-
O
V
O
4
4
4
2400 clock
H.
2400 clock
Hrs
Y/B/N
3
4
5
6
7
8
9
10
1
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
20
29
30
31
Monthly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

NPDES PERMIT NO.: NC0003174
FACILITY NAME: Fulcher's Point Pride Seafood
OWNER NAME: Fulcher's Point Pride Seafood
GRADE: PCNC
eDMR PERIOD: 08-2020 (August 2020)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 5.0 PERMIT STATUS: Active
CLASS: PCNC COUNTY: Pamlico
ORC: Not Required ORC CERT NUMBER: 995491
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Submitted
CONTACT PHONE #: [phone]
Electronically Certified by Elsa Barrera Schmidt on 2020-09-24 14:26:02.505
SUBMISSION DATE: 09/24/2020
ORC/Certifier Signature:Elsa Barrera Schmidt
I certify that this report is accurate and complete to the best of my knowledge.
Phone #:[phone] Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances. The written submission shall be made as required by part II.E.6 of the
NPDES permit.
Electronically Signed by Elsa Barrera Schmidt on 2020-09-24 14:26:48.799
Permittee/Submitter Signature: ***Elsa Barrera Schmidt
Permittee Address: 101 S Ave Oriental NC 28571 Permit Expiration Date: 06/30/2022
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Envirochem
CERTIFIED LAB #: 20-37205
PERSON(s) COLLECTING SAMPLES: Eric McHorney
CERTIFIED LABORATORIES
PARAMETER CODES
eilz.qh,
Phone #:[phone] Date
Parameter Code assistance may be obtained by visiting https://deq.nc.gov/about/divisions/water-resources/edmr/user-documentation.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: YES indicates that No Flow/Discharge occurred and, as a result, no data is reported for any parameter on the DMR for the
entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).
Discharge Monitoring Report - Copy Of Record(COR_NC0003174_Ver_1.0_8_2020.pdf)

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Diamond Shoal Seafood
4146 Orchard Creek Road
Oriental, NC 28571
Attention: Elsa Schmidt
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 09, 2020
Customer PO #:
Customer ID: 19060033
Report #: 2020-14604
Project ID: NC0007609 - Qrtly / Mthly
Lab ID
20-37207
Test
Sample ID:
Site: Effluent - Grab
Method
Collect DatelTime
8/27/2020 12:25 PM
Matrix
Water
Results
Sampled by
Eric McHorney
Date Analyzed
Residual Chlorine
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
Total Phosphorus
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
Nitrate+Nitrite-Nitrogen
Total Nitrogen
10041 ULR
EPA 1664
SM2540D
SM 2540 F
SM 2550 B
SM 4500 H B
SM 4500 0 G
SM 4500 P F
EPA 351.2
EPA 353.2
Total Nitrogen
<10 pg/L
<5.0 mg/L
<2.5 mg/L
<0.1 mg/L
29.1 C
7.82 units
7.59 mg/L
0.08 mg/L
0.5 mg/L
0.46 mg/L
1.0 mg/L
08/27/2020
09/03/2020
08/28/2020
08/28/2020
08/27/2020
08/27/2020
08/27/2020
09/03/2020
09/03/2020
09/01/2020
09/07/2020
Comment:
Reviewed by:
Report# 2020-14604
Page 1 of 1

Date: $4164
tnalyst: C- Ma-J401r064-'
Certification # 94
Facility Name: bI .4A ,..41 IA
Permit #:
pH
Reference+B -
IBC b6- x,c9c)
Calibration Time
Cal Butler 4 0 s u
Cal Buller 10 0 s u
- ..
Check Buffer 7 0 s u
�., ......, ... 1-pn-004
Comments t
1,- -cif) A•••
4..., 1
(4)
(.z. . o c-
(d)
1 .,es.4.
( ')
S(e rt .-
q -2.1 drew
e
4 su buffer Lod,/ Ricca 2901791 EXD 1220 7 su buffer Lodi/
Ricca 2808744 Exo 7/20
10 su hutTer Lod/ Ricca 2905A94 Exo 10 20
Sample location
td
Sample Collection
Time •
Sample Analysis
Time•
pH Result
s u
►Post -analysis Buffer
Check value s u
Comments/Data Qualifiers
ral.... t.,4•-
1)-' 7-v-p—
‘It ).--1 1'—
i .8)-
I.
► P b tT h
k
ost an y sis u er c ec as required when perform rig analyses at multiple sampling locations and must he within ± 0 1 units of the buffer's true value
VI pH salues in pH units (t e . s u ) Recod ail data to he nearest 0 01 s u. and report to the nearest 0 1 s u
Total Residual Chlorine (TRC)
Reference \1ethod Sh14500 CI-G201 I Hach 8167 IiR Please circle I bl t1
Dail Check
Y
Standard Result
ug L or mg/L
Post -analysts
Check Std
("lion analyzing
at multiple sites)
Time check
Standard
Analyzed
,Eleli4a.,+
Sample
Location
Sample
Collection
Time
a i
Sample
Analysis
Time
tea e , co,w instrument
CRC Result
ugn- or mgiL
it/ tLtit.I-C I-002
Comments/Data Qualifiers
•oQr� tG
4:6r�
13 11-t'—
Il: )-Ill—r
8U� /L
ray nod., i.-rt
c., a .a . -a..
f) _i 4
_ L-'• 1
A
Check standards must recoser within *I O'Io of the check Stan s true %alue
Mutual Calibration Cur%c Verification Date' I
ee N1'JL ur g'L
Reagent Blank Value _ _(When applicable. Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
- Reference Method SM a500 O G -201 I I
Calibration/
\ enficanon
I ime
taubrationtanable
\leterreadmg
or °o efficiency
after calibration
•Post-analysscaibrauan
s entication (when necessary)
nstrumont ID r 1. SIG Ilk/NJ-MU
omments
rmperamro
Barometric
Pressure
Theoretical
Value mg/L
Calculated
Value mg/L
Vo. J.aA...
Xel • b
7k 4/. f,
7.45'=/oo %
1 ,c this tort when performing a teritieutiun inttt•.td of
tdhbration
Sample Location
Sample Collection
Time
-Sample Analysis
Time
DO reading
ing/L
Comments/Data Qualifiers
E (..4 4....+--
11-' a r P —
iv al.--i P—
• 7 . s \
.
I I I
• tt hen rt I
pc ormmg aria ses a[ mu rip a txanons, the meter must be h
recahhrated at eacsite before aria lt sis or a post-analy sis calibration terificat:on must be performed
' II :aiorle is nica,ured Jirt•eth m the ,t err .tnd u.i .m4it: aril•, t me trial rid auuld be ; _..oiticd t• rii i -0I: •t i;-v. ,,r,..i ,n -WO or , , •,:•.nntel.
Temperature
Rrf'.rnnr,. Vrrhnd C,A �c:n
Sample Location
Sample
Collection
r me
' Sam pte
\nalysis
Iune
Temperature
'C
ivtrument iu r.l 1tt31-pit-004
I ommrnts,DataQualifiers
r 4 Ike,;-
11:a-t-r--1
I: 3-1 P
a41 . i
t..,^,tit.•,. r.,. .,a,...• i
i.r...,. ... .
........ ...
. .
Annual Verification Date 12020
Field Personnel Note:
Rev 07 2019
rt�.J to ru!_ i•,u tiic•..:r crasti:.l in ..t.i rr tin tut , ��•
DOC.Q 1.001

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client C iW lO Y., Sf1C:X.4 Date: .-Z-i"*"tw Report Number —1460-
Receipt of sample: Delivered 4 UPS • FedEx ■ Other ■
• YES
• NO
N/A
1. Were custody seals present on the cooler?
• YES
• NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 3 • L °C Cor cted temperature upon receipt °C
How temperature taken: • Temperature Blank
Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
• YES
• NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
0 NO
4. Were proper custody procedures (relinquished/received) followed?
YES
• NO
5. Were sample ID's listed on the COC?
YES
• NO
6. Were samples ID's listed on sample containers?
YES
• NO
7. Were collection date and time listed on the COC?
YES
• NO
8. Were tests to be performed listed on the COC?
YES
• NO
9. Did samples arrive in proper containers for each test?
YES
• NO
10. Did samples arrive in good condition for each test?
YES
■ NO
11. Was adequate sample volume available?'
YES
• NO
12. Were samples received within proper holding time for requested tests?
AYES
• NO
13. Were acid preserved samples received at a pH of <2? *
• YES
• NO
14. Were cyanide samples received at a pH >12?
• YES
• NO
15. Were sulfide samples received at a pH >9?
YES
• NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
• YES
• NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
• YES
• NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Diamond Shoal Seafood, Inc.
PROJECT NAME: NC 007609
REPORT NO: a-o— /,-1 4 a y
Address: 4146 Orchard Creek Road
CONTACT NAME: Elsa Schmidt
PO NO:
Pamlico, NC 28571
REPORT TO:
PHONE/FAX: [phone]
COPY TO:
email: [e-mail]
..--
ampled By: S[. •• .
I nT111Rlrr F F=ttlunnt W = Woll CT - Ct.e.�..• Cn - C..:1 QI-
•• •--••., - �....-....., -. -- .. v.., v. - vw va..., VV - VVI, VL - .71uuav, Vu1C,.
Sample Identification
Colliction
m
E a
W :-
�'
B
a o
E 0
0
Container
"0 (P or G)
o a�
t E
o w
m m
g m
z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
W
Z
=
0
x
"
s,
o
_
o.
_`
o
W
o
Effluent (1/month)
C
31.L1-1
X
TSS, SS
g%,/).
)?,;ly,4
G
G
(field): 1. $3
C
P
X
iiipH
Oil andnd Grease
ase
G
G
Temperature: a-'g • 4 8c.
C
P
G
G
D.O. (field): 1- 9
C
P
'6)
X
p ek. 1
Total N/P (quarterly)
G
G
i
LL Chlorine: l�� /
C
P
V)
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Delivered By:
Comments:
Accepted: Rejected: Resample JRequpsted:
Received By:
Date: 7 �7 Time: i
TURNAROUND:

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Fulcher's Point Pride Seafood
101 South Avenue
Oriental NC 28571
Attention: Elsa Schmidt
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 09, 2020
Customer PO #:
Customer ID: 19060034
Report #: 2020-14603
Project ID: Monthly Monitoring.
Lab ID
20-37205
Test
Sample ID:
Site: 001 Effluent - Grab
Method
Collect Date/Time
8/27/2020 11:45 AM
Matrix
Water
Results
Sampled by
Eric McHorney
Date Analyzed
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
EPA 1864
SM 2540 D
SM 2540 F
SM 2550 B
SM 4500 H B
SM 4500 0 G
<5.0 mg/L
<2.5 mg/L
<0.1 ml/L
22.4 C
7.2 units
4.76 mg/L
09/02/2020
08/28/2020
08/28/2020
08/27/2020
08/27/2020
08/27/2020
Lab ID
20-37206
Test
Sample ID:
Site: 002 Effluent - Grab
Method
Collect Date/Time Matrix Sampled by
8/27/2020 11:55 AM Water Eric McHorney
Results Date Analyzed
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
EPA 1864
SM 2540 D
SM 2540 F
SM 2550 8
SM 4500 H B
SM 4500 0 G
<5.0 mg/L
<2.5 mg/L
<0.1 ml/L
28.2 C
7.3 units
3.85 mg/L
09/02/2020
08/28/2020
08/28/2020
08/27/2020
08/27/2020
08/27/2020
Comment:
Reviewed by:
cakoPL
Report #:: 2020-14603
Page 1 of 1

' Date: 5$ _ .144
nalyst: .- 11'4,6-14.1'44'i
L - Ce catlon q 94
Facility Name: CC"- C ttCI $ o 4
Permit *: PeA cat t llt�
pH
Reference Method SM4500 H+B -201 1
Instrument ID
ECHEN1-
Calibration Time
Cal ButTer 4 0 s u
Cal ButTer 10 0 s u
Check Buffer 7 0 s u
Comments
'1-SIDA-.
4.J l
(d)
10..os
('1)
1.0�{
('4)
..
S{o�,�� q-i.; -e
'pH check butTer must ead within ± 0 I pH units of the buffer's true value
4 su buffer Lot*/ Ricca 2901791 Exo 12,20 7 su buffer Lot#.
Ricca 2808744 Ern 7/20
10 su butTer Lot* Ricca 2905A94 E.io It) 20
1
Samplelocation
Sample Collection
Time•
Sample Anat sis
Time•
pH Result
, u
"'Post -analysis Buffer
Check value s u
Comments/Data Qualities
ei,. r• I (Lfib (
(1 ' 14 °- 4- •
(l : 4 714,-+
'71 S'
0w1&11L -.
((:5f,4—.-
1t 'S7A—'
7.Ae
► Post analysis butTer check is required when perform ng analyses at multiple sampling locations and must be within = 0 1 units of the butTer's true value
\II pH values in pH units ti e . s u ) Recoil all data to he nearest 0 01 s u and report to the nearest 0 1 s u
Total Residual Chlorine (TRC)
Reference Method SM 4500 CI-G2011 Hach 8167 HR Please circle a licable Method
Instru
Post -analysts
Daily Check I
Check Std
Standard Result I
"it or mg L when analyzing
at multiple sues)
Time check
Standard
\nalvzed
Sample
Location
Sample
Collection
Time
Sample
\nalysts
Time
(RC Result
,igi1 or m i.
Comments Data Qualifiers
yQ' o.+111.
4a1d
PT Pk
i
RC Daily Check Standard true value V• (i"1 mg/L or g/L acceptance range a pg/L u mgiL
heck standards must recover within±1000 of the check t 's true value
\nnual Calibration Curse Verification Date: I -tOZQ
!t:aeent Blank Value When applicable.Anal}ze and document a reagent blank when standards. sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
Reference Method SM 4500 0 G; 201 I
Instrument ID
EC I I E Mt-DO-o02
ebratioN
\ enlicanon
1 me
v ulibrauon variable
Steer reading
or °o efficiency
atter calibration
• Post -analysis calibration
verification
verification [when necessary)
Temperature
Barometric
Pressure
Theoretical
Value mg/L
Calculated
Value mg/L
1/0: 344..,
Pt • 6
Ii /.6
'Ur =1oo'/a
-
1 .c this row when pertitrniing a verification instead of
calibration
sample
le Location
Sample Collection
Time
Sample Analysis
_ r me
DO reading
mg/L
Comments/Data Qualifiers
a,,-IC.,...tl oo!
I :YSA--
I1:../1/h.
41I.
of a._ t 10 o l--
1 ! : t-s4,_
it 6-7,,....-
3' P c
,
• When performing anal ses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be pertormed
;•'c :m_a unJ .i: r: �ti. r. t., me ,i!,al, v, th i •tit: .1 mnr, u,: ncu,m.d ui ,r.0 i•� unnteJidlch
Temperature
Reverence tethod SM 2550 B-20I(1 i tstrument ID FC HEI-pH-(IW
•ample Location
;ample
Collection
r me
' Sample
\nalssis
Inc.
Temperature
'C I Comments Data Qualifiers
el..l 4r-ci 1 Oc> +
I I "4
I !' -174-•
,11. Y I
0. -4 ((0.-
11: ccAp.
t 1.. S 7.4 --
i
D-.' -
I
;Ir.%, naidoii,. ,n,
\nnual Verification Date I 2I)2U
Held Personnel Note:
Rev 07 2019 -
[AI ;� __ __',l "I 1 �I�l_ :I`Il !'I'J` JC ;Sub A In ti:!LI .11 IIII'I �LI!JI•
IDOC .Q 1.001

11
Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client:H/1A cineArs ot�' Date: � w Report Number: '7�o'1 03
Receipt of sample: Delivered UPS • FedEx • Other ■
• YES
• NO
N/A 1. Were custody seals present on the cooler?
49
• YES
0 NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 3•Z °C Cor cted temperature upon receipt °C
How temperature taken: ■ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
• YES
• NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
• NO
4. Were proper custody procedures (relinquished/received) followed?
YES
• NO
5. Were sample ID's listed on the COC?
YES
• NO
6. Were samples ID's listed on sample containers?
YES
• NO
7. Were collection date and time listed on the COC?
YES
• NO
8. Were tests to be performed listed on the COC?
YES
• NO
9. Did samples arrive in proper containers for each test?
YES
0 NO
10. Did samples arrive in good condition for each test?
YES
• NO
11. Was adequate sample volume available?'
YES
• NO
12. Were samples received within proper holding time for requested tests?
i`( YES
• NO
13. Were acid preserved samples received at a pH of <2? *
• YES
• NO
14. Were cyanide samples received at a pH >12?
• YES
• NO
15. Were sulfide samples received at a pH >9?
AYES
• NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
• YES
• NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
• YES
• NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@environmentalchem ists.com
Client: Fulcher's Point Pride Seafood
PROJECT NAME: Monthly Monitoring
REPORT NO: - f`-/6o3
ADDRESS: 101 South Avenue
CONTACT NAME:
PO NO:
Oriental, NC 28571
REPORT TO: Elsa Schmidt
PHONE/FAX: [phone]
COPY TO:
email: [e-mail]
samples E3y:1�.,/lilt.„rf,,.-y�r�
SAMPLE TYPE: 1 = Influent E = Effluent- W = ST =Stream SO —Soil SL — SI d O h
Sample Identification
[�
collection
Gm
eq F
Composite
or
Grab
Container
(P or G)
:-`
o E'
" E
0 W
m E
3 z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
z
1
0
_
0
z
0
z
o
-
W
o
Outfall 001
C
P
37�J
X
p����
Oil/Grease (2/year)
3f/l��Z o
1 /'�t,4-.
G
G
pH/temp:'7•J-Y.g)-4.41
C
P
TSS, SS (1/year)
G
G
DO(field): L/• -7lv
C
P
<r(X
UPS pH/temp:
G
G
Outfall 002
C
P
oG,
X
X
��
�
OIJGrease,TSS,SS(monthly)
p ���
Total N/P (quarterly)
$�t'7/p
II!! 5-y—,d,.
G
G%Z
pH/temp: )' i' �-
C
P
G
4`'` r
X
G
DO(field): -?. gc
C
P
G
G
Outfall 003
C
P
X
X
TSS,SS,Oi1/Grease (monthly)
G
G
pH/temp: DO(field);
C
P
X
Total NIP (quarterly)
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Tom new��. ....._.I_ ._. �......:.,....1.
l • _ -
Delivered By:
Comments:
Rejected: Resample Re uest d:
� Received By:�( e�
Date: 0/7 ) Time:
TURNAROUND:

i

ANALYTICAL & CONSULTING CHEMISTS
(0-v
E . . .e. :,a I e mists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223Lab • 910.392.4424 Fax
710 Bowsertown Road; Manteo, NC 27954 ° 252 473.5702 Lab/Fax
' 255-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax
info*it environmentalchemists.com
Fulcher's Point Pride Seafood
101 South Avenue
Oriental NC 28571
Attention:
Date of Report: Dec 14, 2020
Customer PO #:
19060034
2020-20140
Customer ID:
Report #:
Project ID: Monthly Monitoring.
Lab ID
20-51326
Test
Sample ID:
Site: Outfall 001
Method
Collect Date/Time
Matrix
11/25/2020 12:35 PM Water
Results
Sampled by
Connie Branch
Date Analyzed
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
EPA 1664
SM 2540 D
SM 2540 F
SM 2550 B
SM 4500 H B
SM 4500 0 G
<5.0 mg/L
<2.5 mg/L
<0.1 ml/L
17.8C
7.7 units
7.73 mg/L
11/30/2020
11/25/2020
11/27/2020
11/25/2020
11/25/2020
11/25/2020
Lab ID
20-51327
Test
Sample ID:
Site: Outfall 002
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
Total Phosphorus
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
Nitrate+Nitrite-Nitrogen
Total Nitrogen
Method
EPA 1664
SM 2540 D
SM 2540 F
SM 2550 B
SM 4500 H B
SM45000G
SM 4500 P F
EPA 351.2
EPA 353.2
Total Nitrogen
Collect Date/Time Matrix Sampled by
11/25/2020 12:45 PM Water Connie Branch
Results Date Analyzed
<5.0 mg/L
<2.5 mg/L
0.1 ml/L
17.8 C
7.5 units
4.28 mg/L
0.22 mg/L
0.8 mg/L
< 0.02 mg/L
0.8 mg/L
11/30/2020
11/25/2020
11/27/2020
11/25/2020
11/25/2020
11/25/2020
12/09/2020
12/09/2020
12/07/2020
12/11/2020
Comment:
Reviewed by:
Report #: 2020-20140 Page 1 of 1

Calibration Time,
e.) 3 t)
Cal Buffer 4.0 s u
1/, 0
('' )
Cetliification # 94
Facility Name: FL1 nc r .
PH
Reference Method SM4500 H- B -2011 , .'Instrument ID
Cal Buffer 100 s u
'pH check buffer must read within ± 0 1 pH units of the buffer's true value
4 su buffer Lot#/: Ricca 2001 B20 Exp 1/2022 7 su buffer Lot;/: Ricca 2008993 Exp. 72022
Permit H: t aC I/1 C(I 1)....C)
Check,Buffer 7.0 s.0 iComments
Sample location
10 su buffer Lot'. Ricca 1001791 72021
Sample Collection
Time.)
/ a Lf
Sample Analysis
Time
pH Result
s. u
7.94
1- sr /
► Post analysis buffer check is required when performing analyses at multiple sampling
All pH values in pH units (i.e , s u) Record all data to the nearest 0 01 s u and report to
Daily Check
a rd
pg'L1or
Result
Reference Met
Post -
Check Std
met_ (when analyzing
at multiple sites)
Total Residual
SM 4500 CI-0201 l .'Hach 8167 HR
Time check
Standard
Analyzed
Sample
Location
fD
TRC Daily Check Standard true value Z
Sample
Collection
Time
Post-anatysis Buffer
Check value s.0
Comments/Data Qualifiers
locations and must be w ithin = 0 1 units of the buffer's true value
the nearest 0 1 s u
Chlorine (TRC)
Please circle applicable Method Instrument ID 1 b o f V o 0 TJ
Sample
Analysis
Time
b
SRC Result
pg L)or me'L
or mg/L acceptance range 150.53t)
Check standards must recover within f 10% of the c eck standard's true value
Annual Calibration Curve Verification Date: t - ZD ? Q LOT li ZOO I i i I
Reagent Blank Value. (When applicable. Analyze and document a reagent blank when standards. sample dilutions or
Dissolved Oxygen (DO)
Reference Method SM 4500 0 G.-2011 Instrument ID
CommentsData Qualifiers
Calibration
Verification
Time
5) S'r
Calibration sanable
Temperature
11. 3 o c
pg/1
Meter reading
or °A efficiency
after calibration
Ntr
pe/L;or mg/L
e Post -analysis calibration
verification (when necessary)
Exp. Date: 2-
PT Samples are prepared)
P l Ono 7 9
Comments
Use this row when performing a verification instead of
• -, r 1, ,
Sample Location
Sample Collection
Time
*Sample Analysis
Time
DO reading
m•rL
CommentsData Qualifiers
146.\ r
132 o
13 3 0
9 .s 7-
s When performing analyses at muluple locations, the meter must be recal'brated at each site before analysis or a post -analysis calibration verification must be performed
* If sample is measured directly in the stream and/or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediately
Temperature
Reference Method SM 2550 B-�010 Instrument ID
Sample Location
Sample
Collection
Time
'Sample
Analysis
Time
Temperature
°C
-
Comments'Data Qualifiers
it sample is measured directly in the stream and or on site, only time analyzed would be recorded, with a note that they are measured in situ or immediately
Annual Verification Date
Field Personnel Note;
QA.001
Rev 9-2020

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: F- uL Pot NT-
6602 Windmill Way
Wilmtggton, NC 28405
' 910.392.0223
Date: t i Z7 c b Report Number: 0 Q v 1
Receipt of sample:
❑ YES I❑ NO 104
N/A
O YES 0 NO 62 N/A j2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt q °C Corrected temperature upon receipt
How temperature taken: 0 Temperature Blank t' Against Bottles
ECHEM Pickup Client Delivery 0 (UPS 0 FedEx 0 Other 0
1. Were custody seals present on the cooler?
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
0 YES I❑ NO
64 YES J ❑ NO
YES J❑ NO
IBC YES ❑ NO
1g YES I❑ NO
vi YES I❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
YES ❑,. , NO 9. Did samples arrive in proper containers for each test?
IX YES 0 NO 10. Did samples arrive in good condition for each test?
YES J❑ NO
YES
0 NO
YES I❑
0 YES I❑
0 YES I ❑
YES I❑
YES I❑
❑ YES
11. Was adequate sample volume available?'
12. Were samples received within proper holding time for requested tests?
NO 13. Were acid preserved samples received at a pH of <2? *
NO 14. Were cyanide samples received at a pH >12?
NO 15. Were sulfide samples received at a pH >9?
NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°C

Analytical & Consulting Chemists
ENVIRON aIEN Vl AL CHE STS
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Fulcher's Point Pride Seafood
' vv .
PROJECT NAME: Monthly Monitoring
REPORT NO: 'L0 - 'Z 1" \'
ADDRESS: 101 South Avenue
CONTACT NAME:
PO NO:
Oriental, NC 28571
REPORT TO: Elsa Schmidt
PHONE/FAX: [phone]
-; 2 1
COPY TO:
email: [e-mail]
Sampled By:
SAMPLE TYPE: I = Influent_ E = Effluent W = ST =Stream SO =Soil SL - Slud a Oth r•
.,.
Sample Identification
Co7Tection
v
�'
Composite
or
Grab
Container
(P or G)
Chlorine
mg(L
LAB ID
NUMBER
PRESERVATION
- g e
ANALYSIS REQUESTED
ate
Time
Temp
Z
0
=
o
_
0
_
00
_`
If,
o
Outfall 001
l%�:1 �j
i� 3;�
7 $o `
r(�Zb
>
X
Oil/Grease (2/year)
G
G
pH/temp:. .�.
! (� �,�y:,
13�
`
1 7
G
X
TSS, SS (1/year)
G
DO(field):' ? [^.�f
7es,
tI 1'll��
J
Psi
a c
17
C
P1
G
G
C
P
G
G
Outfall 002
j
ij 1'P °
I'l, - s-'
y 7, c c
C.
P
5 r ST1
X
TSS, SS(monthly)
G
G
p p�
pH/temp: .7 j
.,1 '41
)1. 9c `�
C
P
X4(
2
Oil/Grease (monthly)
G
G
DO(field):it:" �zlU„S u
i q'i S
) ... c''�
C
P
L
�'z
X
Total N/P (quarterly)
G
G
%
G
G
Outfall 003'1-�)•1 k- ..
`If
C
P
X
TSS, SS(monthly)
G
G
pH/temp:
p P .,_-----
P
X
Oil/Grease (monthly)
G
G
DO(field):
C
P
X
Total N/P (quarterly)
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
(AA-UK.,//ltl�
Sl = L.) 'Z2.
ii
f)
the .
•
ccepted:
Rejected: Resample Requested:
Received By: Date: Time:
Temperature •e d °C (, A
Delivered 8 „_j • ,
Comments: TURNAROUND:

/\/pv
ANALYTICAL & CONSULTING CHEMISTS
Diamond Shoal Seafood
4146 Orchard Creek Road
Oriental, NC 28571
Attention:
1 e. ' fists, Mica
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
sF10 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28510 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 14, 2020
Customer PO #:
Customer ID: 19060033
Report #: 2020-20142
Project ID: NC0007609 - Monthly
Lab ID
20-51329
Test
Sample ID:
Site: Effluent - Grab
Method
Collect Date/Time Matrix Sampled by
11/25/2020 1:30 PM Water Connie Branch
Results Date Analyzed
Residual Chlorine
Oil & Grease (O&G)
Residue Suspended (TSS)
Residue Settleable (SS)
Temperature
pH
Dissolved Oxygen
Total Phosphorus
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
Nitrate+Nitrite-Nitrogen
Total Nitrogen
10041 ULR
EPA 1864
SM2540D
SM 2540 F
SM 2550 B
SM 4500 H B
SM 4500 0 G
SM 4500 P F
EPA 351.2
EPA 353.2
Total Nitrogen
< 10 pg/L
<5.0 mg/L
<2.5 mg/L
0.1 mg/L
18.6C
7.79 units
4.57 mg/L
0.37 mg/L
< 0.5 mg/L
0.84 mg/L
0.8 mg/L
11/25/2020
11/30/2020
11 /25/2020
11/27/2020
11 /25/2020
11/25/2020
11 /25/2020
12/09/2020
12/09/2020
12/07/2020
12/11/2020
Comment:
Reviewed by:
Report #:: 2020.20142 Page 1 of 1

'Date: it�� Q Z? a.
A nalyst:` (At `1
Facility Name: L i
Permit If:j
Certlf atject 9d
MVC:, AICY
4'
PH
Calibration Time
Cal Buffer 4 0 S.U.
-
Cal Buffer 10.0 s u
- --- - - -- -- _ --•
Check Buffer 7.0 5 u
• .......,...,t.,.. -0 d ...?,.. -
Comments
®? 3 0
If- 0 0 `J'
(o- d 7- (J)
7.. 3 0(4)
rue value
4 su buffer Lot#/: Ricca 2001 B20 Exp 1/2022 7 su buffer Lot#/: Ricca 2008993 Exp. 7/2022
10 su buffer Lodi: Ricca 1001791 7/2021
Sample location
Sample Collection
Time*
Sample Analysis
Time♦
pH Result
s.0
Post-analysis►Buffer
Check value s.u.
Comments/Data Qualifiers
110_s d g: tb
1d
(33
q-°1
D Post analysis buffer check is required when perform ng analyses at multiple sampling locations and must be within * 0.1 units of the buffer's true value
All pH values in pH units (i.e , s u) Record all data to he nearest 0 01 s u and report to the nearest 0 I s u
Total Residual Chlorine (TRC)
Reference Metho M 4500 CI-G20 I l: Hach 8167 HR (Please circle a plicablc
Daily Check
and Result
µg L or mg L
Post-ant}c
Check Std
(µ'hen analyzing
at multiple sites)
Time check
Standard
Analyzed
Sample
Location
Sample Sample
Collection Analysis Result
Time Time I µgl_ or mg'L
t
Comments'Daa Qualifiers
-
6g38Nvrti
b, i c
I3 C)
1.1? k)WeA ICOA vJ
TRC Dady Check Standard true •atuc l
eterence Melhoa
Calibration
Verification
Time
Calibration x anable
Meter reading
or%efficiency
after calibration
sPosl-analysis calibration
verification (when necessary)
Comments
Temperature
Barometric
pressure
Theoretical
Value mg/L.
Calculated
Value mg/L
061
to-i -u C
Ff 2 g
cis -1 % 1,
-
=
Use this row when performing a verification instead of
calibration
Sample Location
Sample Collection
Time
'Sample Analysis
Time
DO reading
mg/L
CommentsData Qualifiers
00 fr i.k.:b
03
0
/ 1 3 cl
9-'
W
♦ hen performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed
• If sample is measured directly in the stream and/or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediately
Temperature
Reference Method SM 2550 B-�010 lnstnunent ID
Sample Location
Sample
Collection
Time
'Sample
Analysis
Time
Temperature
°C
Comments/Data Qualifiers
• If I
d
camp a is measure directly Inthe stream anu.or on site, only time analyzed would be recorded, with a note that they are measured in situ or immediately
Annual Verification Date ! - ZO 20
Field Personnel Note:
QA.001
Rev 9-2020

Environmental Chemist, Inc., Wilmington, NC Lab #94
((C Sample Receipt Checklist
Client: IVs.v1/ Oy"1C:+ 1.1\04)-13 Date:
6602 Windmill
Wilmington, NC 28
910.392.0.
Report Number: i_J — Z-O 1
Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other CI
I❑ NO
❑ NON/A 11. Were custody seals present on the cooler?
: N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt g . °C Corrected temperature upon receipt
0 Temperature Blank [ Against Bottles
❑ YES
❑ YES
How temperature taken:
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
0 YES I❑
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
YES 0 NO 5. Were sample ID's listed on the COC?
YES I❑ NO
YES I❑ NO
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
YES I ❑ NO
YES I❑ NO
YES I ❑ NO
YES I❑ NO
YES I ❑
8. Were tests tp be performed listed on ,the COC?
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
NO 112. Were samples received within proper holding time for requested tests?
YES I❑ NO
❑ YES 0 NO
❑ YES ❑ NO
YES I❑ NO
❑ YES I❑ NO
O YES I❑ NO
13. Were acid preserved samples received at a pH of <2? *
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
NO 13. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
(Must be completed for any sampfe(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2S0. HNO: HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly prese.ryed samples. Obtain a new sample or
notify the state lab if dire`ted to analyzed by the customer. Who was notified, date and time.
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Ccich•:�n,; ,; plc.. (cl e_:
Analytical & Consulting Chemists
ENVI
®LAMENT
L CHEMISTS, NC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Diamond Shoal Seafood, inc.
PROJECT NAME: NC 007609
REPORT NO: c2-4)(* 4;---
Address:=,4146 Orchard Creek Road
CONTACT NAME: Elsa Schmidt
PO NO:
Pamlico, NC 28571
REPORT TO:
PHONE/FAX: [phone]
rI) '( fl
COPY TO:
email: [e-mail]
Sampled By —
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
v
Sample Identification
Collection
a a,
E›,
rn ~
Composite
or
Grab
Container
(P or G)
C =
o rn
cLi E
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
w
Zo
z
u
'o
,,
zz
a
z
o
F
w
==-
o
Effluent (1/month)
C
P
519
X
TSS, SS
G
G
7
pH (field): � Li
T
}y:2-i-6i-,
0
)�5.�`c
C
P
X
OH and Grease
G
G
jciLL
Temperat re: 1 ' L
}
G
G(
*.>-.1 1 .'••• -I (iti&Z
D.O. (eld):
1);-'2ci-Kt,
.)
J U
) •49°`-
C
P
r-�
X
Total N/P (quarterly)
G
G
LL Chlorine:
Ill,Iz �)�
r_3
o `,
C
P
G
G
L9 0v1 09 e os, v �
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
DatelTime
egeived By:
Date/Time
1.
{
�� �A
jl/2s /
0 6
2. �/� ;l i'
! �t
/ ,/'�
J
—l1
Temperature
Delivered B Comments
ed °C - Accepted: ✓ f' Rejected: Resample Requested:
Received By:---.,' , G" I L �i__, Date: Time: ) C. , _2,
TURNAROUND: