WQ0000543_Residual Annual Report 2020_20210223

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0000543
Applicant/Permittee City of Sanford
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide inforration on the person to be contacted by N B Staff
Name * Lysa Finnerty
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
14105376150
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00000543
Fbs Current Existing perrrit number
Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220
Facility Name * City of Sanford RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report for City of Sanford NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form} Engineering Fans, Specifications, Calculations, Bc.)
Sanford NC 2020 Annual Report FINAL.pdf 15.14MB
Upload only 1 FCFdocurrent (less than 250 fvB). Miltiple documents rust be contained into one F7Ffile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2021

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 23, 2021
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report for Permit No. WQ0000543
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Sanford, NC.
If you have any questions or need additional information, please do not hesitate to contact Scott
Siletzky at [phone] or Chris Wynne at [phone].
Sincerely,
W�1 01_ I t
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Chris Wynne, Synagro
Scott Siletzky, City of Sanford
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2020 ANNUAL REPORT

City of Sanford, NC
Residuals Land Application Program
2020 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00000543 County Lee Year 2020
Facility Name (as shown on permit) City of Sanford W WTP NPDES No. NCO024147
Land Application Operator Synaero Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Sumnin:
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 14
Total amount of dry tons applied during the year for all application sites: 953.75
Total number of acres utilized for land application during the year: 308.12
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality YES X NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
it. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." f / I ,
Hal Heewer, Public City Manager Z 2a2(
Permittee Name and Title type or print) Si e
It at
Signature of Preparer* Date Signa a of Land Apph Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ROY COOPER
r;
x,
MICHAEL S. REGAN
S. DANIEL SMITH
NORTH C,AROtLINA
£iirectce
Environmental Quality
Certified Mail #
7017 0190 0000 9562 6520
Return Receipt Requested
April 03, 2020
T Chet Mann
City of Sanford
PO Box 3729
Sanford, NC 27331
SUBJECT: NOTICE OF VIOLATION
Tracking Number: NOV-2020-PC-0192
Permit No. WQ0000543
City of Sanford RLAP
Lee County
Dear Permittee:
CITY OF SAt FUHL) LD
cis � n V i
A
2020
The North Carolina Division of Water Resources conducted an inspection of the City of Sanford RLAP on April 1,
2020. This inspection was conducted to verify that the facility is operating in compliance with the conditions and
limitations specified in Non -discharge Permit No. WQ0000543. A summary of the findings and comments noted
during the inspection are provided in the enclosed copy of the inspection report.
The Annual Report Review inspection was conducted by Division of Water Resources staff from the Raleigh
Regional Office. The following violation(s) were noted during the inspection:
Inspection Area Description of Violation
Sampling Condition IV.3 requires analysis be conducted on residuals from each source generating
facility at the frequency specified in Attachment A. During 2019, there were only two
samples of residuals when there were required to be four samples based on dry tons applied.
This was noted in the land application certification form submitted in the 2019 annual report.

Remedial actions should have already been taken to correct this problem and prevent further occurrences in the
future. The Division of Water Resources may pursue enforcement action for this and any additional violations of
State law.
An explanation of non-compliance was submitted with the annual report but further information is required. To
prevent further action, please respond in writing to this office within 30 days upon your receipt of this Notice
of Violation regarding your plans for additional training and checks and balances to ensure samples are taken,
delivered and reported in the correct timeframe.
If you should have any questions, please do not hesitate to contact Gary Kreiser with the Water Quality
Regional Operations Section in the Raleigh Regional Office at 919-791-4200.
Sincerely,
Scott Vinson, Regional Supervisor
Water Quality Regional Operations Section
Raleigh Regional Office
Division of Water Resources, NCDEQ
ATTACHMENTS
Cc: WQS Raleigh Regional Office - Enforcement File
NON -DISCHARGE Compliance/Enforcement Unit - Enforcement File

SYNAGRO
April 24, 2020
N.C. Department of Environmental Quality
Division of Water Resources
Water Quality Regional Operations Section, Division of Water Resources
3800 Barrett Dr.
Raleigh, NC 27609
ATTENTION: Mr. Scott Vinson
REFERENCE: NOTICE OF VIOLATION
NOV-2020-PC-0192
PERNHT NO. WQ0000543
CITY OF SANFORD RESIDUALS LAND APPLICATION
LEE COUNTY
Dear Mr. Vinson:
On behalf of the City of Sanford, Synagro is submitting this in response to the Notice
of Violation letter received April 14t', 2020. As requested, the below items are in reference to
the additional training conducted and plans on how to avoid such occurrences in the future.
As a corrective action, once an issue with sampling frequency was determined,
Synagro immediately began retraining of all staff responsible for biosolids sampling across
North Carolina. Special emphasis was placed on the relationship of dry tons land applied and
the required sampling frequency as set forth in all North Carolina RLAP permits.
Additionally, further training was implemented outlining how the required sampling
frequency applies to not only pathogen and VAR testing but nutrients and metals testing as
well. This training was conducted as a result of having all the required pathogen and VAR
data but lacking the appropriate number and nutrients and metals results in the 2019 annual
report of the above referenced permit.
Additionally, in an effort to avoid future sampling frequency issues, a sampling
checklist has been developed. The checklist documents when samples need to be taken and
when sample results are received and reviewed. This checklist not only tracks when samples
need to be taken but also will be updated to show when results are received and reviewed for
compliance. This checklist should alleviate any future issues with sample retrieval dates,
sample shipping and receiving interruptions, and possible lab -based issues. The current
sampling schedule for the above referenced permit is provided as an attachment.
If you require additional information or have further questions, please contact me at
[phone] or rrothksyna rg o.com.
Sincerely,
Robert "Nate" Roth
284 Boger Road, Mocksville, NC 27028 9 Phone: [phone] Fax: [phone]

City of Sanford
Water Reclamation Facility
P.O. Box 3729
Sanford, NC 27331
April 29, 2020
NC Department of Environmental Quality
Division of Water Resources
Water Quality Regional Operations Section
Division of Water Resources
3800 Barret Drive
Raleigh, NC 27609
Subject: Notice of Violation
Tracking Number: NOV-2020-PC-0192
Permit No.: WQ0000543
City of Sanford RLAP
Lee County
Dear Mr. Vinson:
As per your letter dated April 3rd, 2020, citing a NOV issued for missed sampling, the additional information is
being included in this letter. The City of Sanford has contracted with Synagro to manage a majority of the Land
Application program to include required sampling. I have reached out to Synagro upon receipt of the Notice of
Violation requesting the response to your letter. I have included their response. I have also reviewed it and will
implememt the changes Synagro has noted in their letter. I will also maintain better communications with my
contacts at Synagro to avoid further infractions. If you have any questions or comments please contact me.
Sincerely,
���' a 6"�.�
Scott A. Siletzky
City of Sanford
Water Reclamation Facility Administator
Phone: [phone]
Email: scott.siletzkyksanfordnc.net
Enc: Syangro Letter
Sampling Schedule Checklist

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2020 - 12/31/2020
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTH/YEAR
May 2020
June 2020
July 2020
November 2020
December 2020
TOTAL
AMOUNT UNIT
731,600.00 G
427,800.00 G
1,915,800.00 G
1,153,200.00 G
607,600.00 G
4,836,000.00 G
DRY TONS
UNIT
DRY METRIC TONS
165.35
D
149.97
96.69
D
87.70
363.49
D
329.69
214.96
D
194.96
113.26
D
102.72
953.75
D
865.05
Report Date: 2/5/2021 4:37:47 PM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WO Permit Number: WQ0000543 Laboratory:
Facility Name: SANFORD, NC PACE ANALYTICAL
Residual Source WO # or
NPDES#: NCO024147
WWTP Name: BUFFALO CREEK WWTP
Residual Analysis Data
Product Type
Sample or Composite Date
AEDLIQ
03/24/20
AEDLIQ
04/21/20
AEDLIQ
07/08/20
AEDLIQ
10/01/20
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
3.76
5.42
4.55
4.47
Arsenic
75
11
6.2
3.4
7.1
Cadmium
85
2.5
1.9
1.2
1.6
Copper
4300
450
390
240
440
Chromium
NA
84
78
52
95
Lead
840
30
25
16
28
Mercury
57
0.63
0.37
<0.42
0.47
Molybdenum
75
21
17
11
18
Nickel
420
49
43
26
46
Selenium
100
5.6
4.7
4
8.7
Zinc
7500
1000
850
510
1000
Total Phosphorus
NA
29000
24000
21000
31000
TKN
NA
84000
56000
33000
48000
Ammonia -Nitrogen
NA
17000
12000
7500
11000
Nitrate and Nitrite
NA
96.6
69.7
193
144
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
fie - A ' al ►t) al
Signature of Preparer" , Date
"Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (12/2006)
Printed: 2/5/2021 4:35:42 PM For: 2039 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0000543 Laboratory:
Facility Name: SANFORD, NC PACE ANALYTICAL
Residual Source
NPDES # or WQ#: NCO024147
WWTP Name: BUFFALO CREEK WWTP
Residual Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Sample or Composite Date
03/24/20
04/21/20
07/08/20
10/01/20
Parameters (mg/kg dry weight)
Aluminium
17000
14000
8200
17000
Calcium
18000
16000
8800
17000
Magnesium
6600
5600
3000
6700
pH (s.u.)
6.80
6.90
7.50
7.20
Potassium
11000
7700
4500
6400
Sodium
3300
2400
1200
2600
PAN
28697
19270
11593
16744
SAR (Ratio)
1.0333
0.9653
0.5992
0.9007
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of PreparerDate
"Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/5/2021 4:36:26 PM For : 2039 01 DENR FORM RSSF-B (12/2006)

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Sanford
Lot Number:VC25024
Date Completed:04/09/2020
NIM�� Mr�
04/10/2020 10:23 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VC25024
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure. The LOQs
have been changed to reflect the additional mass.
PCBs by GC
The following sample was diluted due to the nature of the sample matrix: VC25024-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received: 03/25/2020
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
03/25/2020 2220
SRB
48982
1 350.1
(Ammonia - N ) 350.1
25
03/26/2020 1321
SLC
48894
1
(Ignitability) 1010A
1
04/07/2020 1032
SLC
50227
1
(Nitrate - N ) 9056A
1
03/29/2020 1501
HKL
49410
1
(Nitrite - N ) 9056A
1
03/29/2020 1501
HKL
49786
1
(Phosphorus) 365.1
25
03/27/2020 1235
DMA
03/27/2020 0758 49065
1
(Reactive Cya) 7.3.3
1
03/27/2020 1610
KFE
03/26/2020 0910
1
(Reactive Sul) 7.3.4
1
03/29/2020 0909
HET
03/26/2020 0910
1
(Soil pH meas) 9045D
1
03/26/2020 1940
SRB
49111
1 351.4
(TKN) 351.2
2
03/31/2020 1411
DMA
03/30/2020 0822 49288
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.76
%
1
Ammonia - N (gas diffusion)
350.1
17000
660
350
mg/kg
1
Ignitability (Pensky-Martens Closed -Cup)
1010A
>140
140
0
o F
1
Nitrate - N (soluble)
9056A
90
13
0.65
mg/kg
1
Nitrite - N (soluble)
9056A
6.6
5.3
0.51
mg/kg
1
Phosphorus
7723-14-0
365.1
29000
3300
660
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
50
mg/kg
1
Soil pH measured in water @ 20.5 ° C
9045D
6.8
su
1
TKN
351.2
84000
1300
1300
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/5030B 8260D
10 04/09/2020 0242 JTH
50426
04/07/2020 1917
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Benzene
71-43-2
8260D
ND
0.050
0.0040
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
0.049 J
0.10
0.020
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.050
0.0040
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
0.0040
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
0.0040
mg/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.050
0.0040
mg/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.050
0.0040
mg/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.050
0.0040
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
0.0040
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
0.0040
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
103 70-130
1,2-Dichloroethane-d4
103 70-130
Toluene-d8
109 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/3520C
8270E 1 04/07/2020 1426 JCG
04/01/2020 1522 49681
03/26/2020 0255
2 1311/3520C
8270E 2 04/07/2020 1740 JCG
04/01/2020 1522 49681
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
0.0050
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
0.0050
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
0.0050
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
0.0050
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
0.010
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
0.010
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.98
0.080
0.030
mg/L
2
Nitrobenzene
98-95-3 8270E
ND
0.040
0.015
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
0.020
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
0.0050
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
0.0050
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
0.0050
mg/L
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
64 37-129 68
37-129
2-Fluorophenol
37 24-127 43
24-127
Nitrobenzene-d5
64 38-127 62
38-127
Phenol-d5
66 28-128 57
28-128
Terphenyl-d14
82 10-148 80
10-148
2,4,6-Tribromophenol
44 41-144 46
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/8151A
8151A 1 04/03/2020 1245 DAL1
04/01/2020 2347 49691
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
0.0050
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
0.0013
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
89 50-112
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 3665A 8082A 10 04/08/2020 1412 DAL1 04/06/2020 2220 50123
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016
12674-11-2
8082A
ND
7900
ug/kg
1
Aroclor 1221
11104-28-2
8082A
ND
7900
ug/kg
1
Aroclor 1232
11141-16-5
8082A
ND
7900
ug/kg
1
Aroclor 1242
53469-21-9
8082A
ND
7900
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
7900
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
7900
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
7900
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
87 41-132
Tetrachloro-m-xylene
87 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 04/02/2020 1712 DAL1 04/01/2020 1432 49666 03/26/2020 0255
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
gamma-BHC(Lindane)
58-89-9
8081B
ND
0.00040
0.00017
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
0.0015
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
0.00016
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
0.00021
mg/L
1
Toxaphene
8001-35-2
8081B
ND
0.0080
0.0030
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
77 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 03/26/2020 1435 KSH2
03/26/2020 0218
48980
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL Units Run
Mercury
7439-97-6 7471B
0.63 J
2.0 0.48 mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result < LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
Leachate Date
1 1311/3010A
6010D
1 03/27/2020 1909 LLL
03/27/2020 0423 49145
03/26/2020 0255
1 1311/7470A
7470A
1 03/27/2020 0857 KSH2
03/27/2020 0400 49150
03/26/2020 0255
2 1311/3010A
601OD
1 03/28/2020 1459 KSH2
03/27/2020 0423 49145
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Arsenic
7440-38-2 6010D
0.067 J 0.15
0.025
mg/L
1
Barium
7440-39-3 6010D
0.11 J 0.25
0.031
mg/L
1
Cadmium
7440-43-9 6010D
ND 0.050
0.0060
mg/L
2
Chromium
7440-47-3 6010D
ND 0.10
0.013
mg/L
1
Lead
7439-92-1 601OD
ND 0.10
0.047
mg/L
1
Mercury
7439-97-6 7470A
ND 0.0020
0.00091
mg/L
1
Selenium
7782-49-2 601OD
ND 0.20
0.085
mg/L
2
Silver
7440-22-4 6010D
ND 0.10
0.021
mg/L
1
ICP-AES
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst
6010D 1 03/27/2020 1819 LLL
6010D 1 03/28/2020 1543 KSH2
Prep Date Batch
03/26/2020 2331 49117
03/26/2020 2331 49117
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
17000
170
65
mg/kg
2
Arsenic
7440-38-2 6010D
11
6.5
2.2
mg/kg
1
Cadmium
7440-43-9 6010D
2.5
2.2
0.55
mg/kg
2
Calcium
7440-70-2 6010D
18000
2200
270
mg/kg
1
Chromium
7440-47-3 6010D
84
4.4
1.1
mg/kg
1
Copper
7440-50-8 6010D
450
4.4
2.0
mg/kg
1
Iron
7439-89-6 6010D
24000
44
20
mg/kg
2
Lead
7439-92-1 6010D
30
4.4
2.0
mg/kg
1
Magnesium
7439-95-4 6010D
6600
2200
270
mg/kg
2
Manganese
7439-96-5 6010D
2000
6.5
2.6
mg/kg
1
Molybdenum
7439-98-7 6010D
21
17
4.4
mg/kg
2
Nickel
7440-02-0 6010D
49
17
4.6
mg/kg
1
Potassium
7440-09-7 6010D
11000
2200
270
mg/kg
1
Selenium
7782-49-2 6010D
5.6 J
8.7
3.5
mg/kg
2
Sodium
7440-23-5 6010D
3300
2200
270
mg/kg
1
Zinc
7440-66-6 6010D
1000
22
5.5
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
2
�
� R
r.:
_ _ L
FT
A � "tt c '
00 { C
E ( i7
37O
all UH NM
aswa,o pup x3
=�11:J lul0�
(ua�ag
101eris.' egad C
Vj-j V a Beu+Q
8Cd
`� 4C I
C p ro
u
(b
r�ayy
1JJ
j
CL M
�
o
Va
T
9
z
a
r =
o
k t
"
n
' p
0
9Fiw
L 4
CL Q {l1
Q
a: 7
LM
7
z
I x
61c2 SP
4
m
n
J
a ca
fl Q
o
LL C
l—L =p
I=
1 E
F
—
Vdi
AM
0 L
T
0
1] C W
IE
EIC
c
6
1=1111111111M
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
ra IO'.
]]rcw�eltl `�'G?7�4Cr. r,�Eao18C-14 �'
h'unc��rve d+27:n I S
F sa nple Receipt C heek1st (SRC 13pkv'
C[icrit, Syna,gt'o _ Goolerlispectedhvfdafc:r-x:a r 01.Qt --o VC25024
llcans o: re cipt: ❑ ;1-3I : client 2 UPS ❑ FedF,x Other;
®Y Nta 1, W clv custadY saa is presettC ;)n the cooler?
J Yrs Nn NA12- If custody sm[s wore praseni: -e9-e they udu4i and unbrokrn?
IPH '�Iriip ID: NA Chlorine Stria ID, NA — Tnttd �A
by.
Original lem-jcrature upcirl rrrooipt f JD� r]+�_d I Cot'rec�rrl) tetnpelaUtr* upon receipt solid Snap�Cup la; 19 2313
.8 15-8 40 fqA !t'A ¢C NA iNA NA +TlA o�
1+letl>od: ©:'emperPdt� Blartk®AgainstBottles IRCiun 117: 5 IRGil uMwrcu6DnFacWr, 0 °C
1Uthod cfcool unt: R`et I" F-1 I— Rjoks ❑ Dry lcc � Mone. --
0 Yes ❑ TON
f tcmpt.rglurtl Df sny canlcr cxcek red 6A c Prtsjret 11aa14,e-r Notifi ed - —
_ PM was NQfiFtcd try: pE,o'.�c ? attiz.il ! (li-40-fact,'Circle ale)_
i� i'es No ❑ 14A 4- 1t t:,10P coramemial courier's picking slip atl�tched w tills form'
® `res � hlo 5- w'ere }rnpp�cus[�iv 7mrrdures{�eliotlaisJledlreceivt�d}fo][ov�+ud'd
Yew r fa 5, �Nca,c 3Ainh31« Ills 115jtW an the { O C',1
I j YC3 ❑ Na 1- Wem sample IDs listed an rill sample contaiticrs?
Yes ❑Teo S. Vddrtcnl[MtiQn r141�- R. time listed oil thar_OC?
❑ Yes 21 ]-0 9. Was wI1,� stior dax sim�a iisferl inr all sample _cintainers?
E Yes ❑ M1ir, 10- Diet H I I c•o-jteitj% label ui arrnaicn (ID, date, fait) agree witli 11,c OOC7 -
YE8 ❑ No' I [. creiw1l. to be FerformL-d Iisted ckn he k:OC?
yea i�To
12- Did all sarap[cs arrive irk W PJ%OPOT oontairers #or each Iq�i! andlor in goad catlditior.
Ol
(unbroken, lids on, etcrp,
m Yes NO
x
14- V'I�ro all sarrlp]cs MCeived IVithilt', tic hcilding lime or49 hours, %vhjc:.cver op,rtcs FRsc!
15r WCM all Sam les cgruttinei:s miss:npfexcL= (cimrenne:)lain 1e47klr�: listed n CO S
© YC3 ❑ No
15. For VOA ar-d RSK-175 snmpie�, here bubbles 1prr;4rnt >"pC s:ac" r 6:rttn
0 NA in diblxctcr)
in ktn+ oftlie VOA viaJs?
❑ YB0 No
VJ NA 17. Were all T)Rf�f111�A1;<!rll ITienL 581;1p165 !$Ctil'4d 1t fl pH of •: 2?
Yes ❑ iNu
A:A i8. k `ere a[I vvariids stmplcs reoeiy J at a jH > 12 and sulFide 5MP]a recelvW at a pi i > 9?
❑ Yts QNu
!9. V4`ere all spp rcable Nl I T1CNloya,ii ,i,c nollp j {{ Ins [,j samples tree oT residt_a1
cblorire?
❑ llcs Q Vo
O NA 20- Wert client rcn)arhs'fcqucsts 1:.8- request--cl dilutions. �1S1ASD elea=gnaiiprks, etc--_}
vormet]ytranwribed horn the COC Jryt dic totnmenrsection in LIMB?
Yes No
? I . VJ�s the quote nutiber Issted on Ibc cm[kl:LMX labs:? i Fyes, not #` NA
Sa�niple Fruservatica (,rYfuSt ba cvrrtpja, for a:3y s3r.jPle><8) inc3rreody p�.s:rue e or with hc_Hdspace.)
5arr'p[d45; 'vero Teceivee] 4�cr}rrectly prageuwW kmd v,ere �IdjuZt ! fucardingly
insampi: 7�=jyjjjg will. NA mL oCdrole talc InSO4, HNO3, I-TCI, N�OH tl3irt c £R it NA
ritrre of preservt�tion If more fhan one Presrrvativo is needed, p[case nom in the comme�its Wow.
Samp(g() NA
,Lvere reeaived wide bubbles >5 MIA in dialreter.
Satnglx4(s) ItiA raceiYt}d with TIC > U,5 ir.VL (rr#J 9 is ,zv) Hnd were
�ljk:sled acm-dillaa(y in sample r�pp1ritisgv%'irii sodiorn thiostllfate (MS _) w-'* S--3, My 1D: ---NA
i 1 LwtsWu labels dpp[ied
bv: -Kh _ Data: 4lg5?2020
Comments,
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Sanford VWVFP
Lot Number:VD23022
Date Completed:05/01/2020
NIM�� Mr�
05/04/2020 11:41 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VD23022
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids the sample was weighed out 3 times the normal amount. The LOQ has been
elevated to reflect the dilution.
Nitrate
The following sample was diluted due to the nature of the sample matrix: VD23022-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VD23022-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:04/21/2020 0905 % Solids: 5.42 04/23/2020 2207
Date Received: 04/23/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 04/23/2020 2207 HET
51982
1 350.1
(Ammonia - N ) 350.1
25 04/28/2020 1458 SLC
52271
2
(Nitrate - N ) 9056A
5 05/01/2020 0900 AMR
52669
1
(Nitrite - N ) 9056A
1 04/26/2020 0109 HKL
52211
1
(Phosphorus) 365.1
50 04/28/2020 1620 DMA
04/28/2020 1146
52263
1
(Soil pH meas) 9045D
1 04/23/2020 1924 SRB
51981
1 351.4
(TKN) 351.2
2 04/29/2020 1516 DMA
04/29/2020 0934
52375
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
5.42
%
1
Ammonia - N (gas diffusion)
350.1
12000
460
240
mg/kg
1
Nitrate - N (soluble)
9056A
60
46
2.3
mg/kg
2
Nitrite - N (soluble)
9056A
9.7
3.7
0.35
mg/kg
1
Phosphorus
7723-14-0 365.1
24000
4600
920
mg/kg
1
Soil pH measured in water @
18.4 ° C
9045D
6.9
su
1
TKN
351.2
56000
920
920
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 04/27/2020 2324 JMH
04/27/2020 0317
51971
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
0.37 J
1.4
0.34
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 04/27/2020 1952 LLL
04/25/2020 1414
51966
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
14000
120
45
mg/kg
1
Arsenic
7440-38-2 6010D
6.2
4.5
1.5
mg/kg
1
Cadmium
7440-43-9 6010D
1.9
1.5
0.38
mg/kg
1
Calcium
7440-70-2 6010D
16000
1500
190
mg/kg
1
Chromium
7440-47-3 6010D
78
3.0
0.76
mg/kg
1
Copper
7440-50-8 6010D
390
3.0
1.4
mg/kg
1
Iron
7439-89-6 6010D
20000
30
14
mg/kg
1
Lead
7439-92-1 6010D
25
3.0
1.4
mg/kg
1
Magnesium
7439-95-4 6010D
5600
1500
190
mg/kg
1
Manganese
7439-96-5 6010D
1600
4.5
1.8
mg/kg
1
Molybdenum
7439-98-7 6010D
17
12
3.0
mg/kg
1
Nickel
7440-02-0 6010D
43
12
3.2
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VD23022-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:04/21/2020 0905 % Solids: 5.42 04/23/2020 2207
Date Received:04/23/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 04/27/2020 1952 LLL
04/25/2020 1414
51966
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
7700
1500
190
mg/kg
1
Selenium
7782-49-2 6010D
4.7 J
6.1
2.5
mg/kg
1
Sodium
7440-23-5 6010D
2400
1500
190
mg/kg
1
Zinc
7440-66-6 6010D
850
15
3.8
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
4
I
ti
2
9
}
o
E I
m
W
4
u
U
m
r
_
m
F}{
r}
w
dl
F
f
£ W
L
—£., E
d
E
3 7
16
3
rn
0112a rare
z
m
7
d
R
C
o
&wale pue i0
x
FL ❑❑
� it
m
ICI
LJ
(Illr�
1:3e; ON
rij
c>a
#r �,
m
I y
-
r9�jhJ 3i6uurs
7 C i s id
3
{[
a
C�2!-
U} oo
4
J.:j
m
y m
a W
emirs
eppJ91eH I
ra To ca
I
aFl-' sad A-Izkk wk
s
3
SMJOU
..
�2 dS i 1fY
hvfs'
r
L
'AIM
w
f..UI
W
VV
N N
a
al
E
z
❑x
-
E
F
£
F
{IJ D
Fi a
a
fl
�
i
t U
1
0� u
=0
96
d[iI
4 ui
_
E
i
/�
fiCGGy}
�
Y
Lr�
g
C9 i
LJ
++,�..,,
I
I
F^r
C
C}I L
cu
fr z
�' is
'r {'7
CL r -'I '6
H
I
W
4
1
} m
y�y
�
�S
7
n1
,m3m
1
I
j F4
�'
O
}
I ,E
LS E
=i
a
r3
Q fl
X
•V
Ia.
9
N
UI
JPUJ
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
..IC3IY r=11 ti'Ir4.y1fIC'JI�y1�EF p'�e�+c�Ingl
DDI
Sample Receipt Checklist (SRC)
Client; 3ynag-0
Coo lei, Nspwted bvldaie: WtG ! 04 23?2020 LDL #; VD23022
MC-MR13fre.oeiplt_
�] SESI client 0 UPS ❑ lVed[3-x
Ycs
%Vej%e �-xslcdv stale presrr_t on the eoojteT7
fl W& L-F
N If ctiMdy sraals were ' C, were the ieJt&Cta0� 0ril r{11 n?
ph Strip ID: NA
Chlorine gtrip JD' NA Tested by; NA
_
DftI}imAll to perat}u�ret3p4receipt/Ih-rive�d--a
(CnC4l�ed) remipt pemium upon rece"ASO]id Snap-C-up ID'
5.8 J 5.6 Q�
A +fry,7�� i+L oC NA �iryA } iNA
. A
1 thad: ❑TLgrnpPratLue $]unto mA ain t 13axle iR Gun lD; _ G Ili Gu,1 (iirrHrtiorl Faowr; ('
4i�thOd Ofcaalant: ® Wet TW ❑fee Parks CI Du� I" ❑ None -
[�Yes El
®ZtiA3.lfte�nperatlln,ofar5ucuulErcaeceedadb,0°C,wasPr,?Icx4l+lr�far�ar�]�,fifierl?
Ph] was i�loffmd hy' pJfone II --mail r t.<ce-M-fwe (ci rcic: nnc).
_Yes ❑ No
❑ NA l d, Is die carrmcmial courier's packin8 �1 ip attache>310 Ibis fora —
6Q Yes ❑ No
5. v4'ere rop4r custody yncodki-es [rd inquishccrraceivc xd) followed?
❑ Yec No
G. Wcne sam pie IA Bred on the UUC?
6CJ Yl� ; ❑ ND
7. Wure sample IDs lisl:Pd on all sample uunLai ners?
® Yes ❑ iz
2, 4ia� collection date &. umc iistad IM the GOC'I'
9_ %V2,1 collection 4w & tinie lisl6�i an all s.4mple conffiirim9
i l0
L�] lla
lf]_ i}id aC cplBirlr babel inti rmarfgn (ID, dwbe, time) t with diet7C7
11_ Wtn- to rn be performed iislyd on the DOC;�
❑ .0
V1 veal ❑
YMI ® N
d Yas , ❑
U YM L-171:o
❑ Yrs ❑ 7 0
❑ Yes ❑ No
❑ Yet ❑ l*io
psi r'JQI
cNecRivc 7i1r 9.120111$
19-2043
9C
1-2, Did R.11 saniFlle; afivc in for each rep: and/or in good ovidition
(UJI bmken I I ids 011, &[L')?
_ 13. W:19 Adc, uate su'31 w It; VDlume 3VAiiabie. —
14. ",'= v[I sarrlplts reoeived W Rhin bolding bane ps 48 hours, whichcm colncs Fir,-t'f
15, Wem 8rly sale lei containers miwjnV'exl2esa (chore one) samplcs Not limed oil ccc?
16. For VOA rnd R -17S smiip[es, -were bubbles ptukni> pea-s[73e, (%"or 6;rjrrm in diametort)
` in an}• of the VOA vials°
NA 17, 1'!-= a ll DR(XMC#alslnuo'ierrl samples rout! ivt!tt at a f I Of < 2.2
NA 19. %Vm al, c}-an isle Emr ples rernived at !up.-H > 12 and sulfide s=n ]cs rc=lvad at a pH > 9?
Wl NA . ' Wem all applicable'`IH 1CN.i� rLrnirie,'p relio]! 4` O,51no'.,) samples ftc of mNi:la,ul
!A2
?U. Vk+ere cii >t remark ?roquests {i.t:. rcquesoed cl iutio s, M5, 45ll deli R#io1u, etc.
correCliy uwscrilled ft` rn Ire COG into the comment secliur, in Ll MS?
1. WFH the 91.101M number ]i�icH an the ContAiner lahu] i Ifves. 0 NA
n7]}I41'I'fiSrrvatirin (,Ytujjr b4 completed for an}' 52tttplc(a) ino&Tectly presarvod orMTh Th heaftace_)
mplc4S) i4A1 )ram MtG VW iF1OU wly preserved aiid were Oust j :.ra; cling[ ,
smnp:e ra,cu-ivutg with N.�_ _ml, Of circic onr' V4, HN D3. H CI, NaO H using SR A! NA
me of prescrratia7 NA IPmore than one prese,-vra!ive is r_eedorlplease nw6 in the cnmmznts belt. w,
NA
xrertt received wi(h bubbles >G mm ill diamr tc.,
nple*s) NA W-rc reoeivu-d with TRr } 0.5 n1VL (If#] 9 is no) and were
L1gCL +,L(*rair,&3y in sampleTCCdVins%y:l tAodium thiusulfate (Nai2 yO%)-twifJh She7Jy 1D, NA
barcDca k0els aM1ied trv. two
Commerim.
Date:' 1}4r7-3#2420
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVFP
Lot Number:VG09014
Date Completed:07/15/2020
NIM�� Mr�
07/16/2020 2:55 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VG09014
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids sample -001 was weighed out at 3 times the normal amount. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VG09014-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:07/08/2020 1030 % Solids: 4.55 07/10/2020 0022
Date Received: 07/09/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 07/10/2020 0022 MOM
59554
1 350.1
(Ammonia - N ) 350.1
10 07/13/2020 1300 DRD
59639
1
(Nitrate - N ) 9056A
1 07/11/2020 2000 AMR
59956
1
(Nitrite - N ) 9056A
1 07/11/2020 2000 AMR
59957
1
(Phosphorus) 365.1
25 07/10/2020 1312 DMA
07/10/2020 0837
59501
1
(Soil pH meas) 9045D
1 07/09/2020 1838 SRB
59537
1 351.4
(TKN) 351.2
1 07/15/2020 1330 DMA
07/15/2020 0905
60035
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.55
%
1
Ammonia - N (gas diffusion)
350.1
7500
220
110
mg/kg
1
Nitrate - N (soluble)
9056A
63
11
0.54
mg/kg
1
Nitrite - N (soluble)
9056A
130
4.4
0.42
mg/kg
1
Phosphorus
7723-14-0 365.1
21000
2700
550
mg/kg
1
Soil pH measured in water @
22.7 ° C
9045D
7.5
su
1
TKN
351.2
33000
550
550
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/14/2020 0827 JAB2
07/13/2020 1557
59552
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
1.7
0.42
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 07/11/2020 0349 KSH2
07/09/2020 1606
59484
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
8200
140
53
mg/kg
1
Arsenic
7440-38-2 6010D
3.4 J
5.3
1.8
mg/kg
1
Cadmium
7440-43-9 6010D
1.2 J
1.8
0.45
mg/kg
1
Calcium
7440-70-2 6010D
8800
1800
220
mg/kg
1
Chromium
7440-47-3 6010D
52
3.5
0.89
mg/kg
1
Copper
7440-50-8 6010D
240
3.5
1.6
mg/kg
1
Iron
7439-89-6 6010D
12000
35
16
mg/kg
1
Lead
7439-92-1 6010D
16
3.5
1.6
mg/kg
1
Magnesium
7439-95-4 6010D
3000
1800
220
mg/kg
1
Manganese
7439-96-5 6010D
830
5.3
2.1
mg/kg
1
Molybdenum
7439-98-7 6010D
11 J
14
3.5
mg/kg
1
Nickel
7440-02-0 6010D
26
14
3.7
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VG09014-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:07/08/2020 1030 % Solids: 4.55 07/10/2020 0022
Date Received:07/09/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 07/11/2020 0349 KSH2
07/09/2020 1606
59484
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
4500
1800
220
mg/kg
1
Selenium
7782-49-2 6010D
4.0 J
7.1
2.9
mg/kg
1
Sodium
7440-23-5 6010D
1200 J
1800
220
mg/kg
1
Zinc
7440-66-6 6010D
510
18
4.4
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
t
's
S
E
52
IM
F
'
f-:
F
'u
OWN M.Q
-2
X IL
KID
z
ON
51§ 1
;E E
H
E-
M
5
E
J;410
arN
V.2
CM ID L
x
E3
z
Lx
rL
1--
0
.r.w z
d
L
0
[q
Q
Mi
2
13
CL
nr —,T-
Li
E-
In In
Z
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Shwy Brvi-OrTrMUO 3Arirca, ;PC.
I'.�.yu 1 ud' 1
T]oramt Nu.nLcr M6??: 8C. I.;j [� hcl ivo zoo art ^0 6 i
Sample Receipt C'heukIust (SRC')
Tent: Cooler llls eG#edyldata'1 r Lot #�;{
hiasn&ofnceijjO [j SESI ❑ Client :PS TAecf�i Utliar: —
0 yC5 a I- Werc custackseals r mllt nn'the C001ca
LjjyNp A 2" If CU31od y seals wert resent, twere titcy intact and u311 ar can7_
Strip 1D: -- Ch krrine tdp ID; �'� 1 7esoed�b:�- -
t Ml lbemportumre upon mcript f Derived (Corrected) temperature upun recoipt 'U-alid Siiap pup In-,
;Zhod; ©TempCratUrO Pjank47TkA2L; st33attles IF, GUr to; 1 JR Gull Qkrcu6on Fart -ow 4 °C
I�Setlwrl of coolant; I -Wet lee ❑ lee Pwksl ❑ Ury loe ❑ Noue
❑ 3, ifte(ligltruture of any corder okceed+ed 6ff} C, was 11'roject Martagef7'lratifjQxl{
Yes []-No la'�-JA
Purl %l 4 d by it
Yrs
u�5. o#i ie . phone 1elnml ? fac to faces {oitcic ono
© Zti rr [INA 4, 19 tho camrrteMietl courier's }pocking slip attg bed to tibia fco l-0
❑ 7k n 5, Mere FOM cu5rLut P wzd*s (relh1gnishedhcceived) #ollowec?
-N o 6, Winre Bauap]e ILLS ]a!j[,d vn the CCC? -�
❑ 1N0 7- Wear owxple IDs liigod on all'saitf 1e V. Mlai,ners7
O Na & W4$ co]ltetion date & tuna listed on tha CbC7.
Was collaUlon date & time listed on all as la utltuoers7
QN0 IDid all rmtahwr label Wan atiar (ID} date, time) Um with the COC?
No ] 1- yf = tads to be perfarnted linked rm tho CQC?
No 12L bid 211 samples rffrlw 1n 12�e gaper VMk JnelS fca cash rest and1or hi gowd camdip on
(unbinkeA lids an, etc.)?
O 'Ye-d ©No
13. Was adegtlak� sawplc rolurnc:avallable
14_ WMV all saM&N reae[ved width % the holding tinie ur 49 botrs, whiclrever' Uwne.-q ti rs_t7
15. Were Mw Samples cattlairirrm missin cacaess (6-11t one] Sam
'IRA los Not IWcd on COC?
lfi, For V4A sold RSR-i7S satnples� Kara huhttlas present "pca-size" (War 6riwk in diaindcr)
in any ofibte VOA vials?
NIA 17, W&a a a] I DRfVnutal6r,k3irient sampics rcceivzd 83 a PH of <27
1$A IS- wrre Al cyan irk samples reoeivad at a PH > 12 and sulfide s® lea received at R PH > 97 .
NA l Were all applicable.MI1alI1C , e}a+Xidrlg enoL O.Smglt samples c (3r uatua
chlorine?
NA 20, Wcra client rCmaTWVques?s (ii.e, regllkated diNtiuns, lti+D:SIMSD desigrtati0ms. etc...
}
Urrccily tran-whed frani t11e CDC inin Ow con ucat scuion in DIMS?
Was the quota number listad On the eordainer libel? if yet. Quote # �A
Pms—!r Gon -(Must Ix mmpleled for aoy satrrplu(s) incorrectly pre%ervcd or with hcadspape)
_were received baorrmq pnscryW an w adjnsicd Wcording]y
in aampk IOCciving with s mL. of circle o," one, M, kiN 3, HC4 � AOA using SR #
'1�mo c f pres 3+at[�ors �. If mAxc fli m one preservative is nccded, please note in the comtni r is below.
5aaulbic[s) I _. w�sra reoefvcd wit# bubbles >6 mrn in &Rrnotcr,
atttrle�(s) lucre mceivcd with 7RC > 0.5 M6,1 Uf P I9 k 11o) and vt-rre
adjt151cd,accard[n91y in sample rcceiVing with sodium #hiosrxlfdw (NGL�%) Wilk Shea]+} IL?,
barcode labels iipplicd by: MA M 7— D=
C�ItIIa�Slts; ��
i
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVFP
Lot Number:VJ03015
Date Completed:10/12/2020
NIM�� Mr�
10/13/2020 3:59 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VJ03015
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids, the initial amount used for sample -001 deviated from the standard procedure. The
LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:VJ03015-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:10/01/2020 1130 % Solids: 4.47 10/05/2020 2313
Date Received:10/02/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
2
(% Solids) SM 2540G
1 10/05/2020 2313 MOM
68892
1 350.1
(Ammonia - N ) 350.1
25 10/09/2020 1542 DRD
69087
1
(Nitrate - N ) 9056A
1 10/10/2020 0216 AMR
69482
1
(Nitrite - N ) 9056A
1 10/10/2020 0216 AMR
69483
1
(Phosphorus) 365.1
50 10/08/2020 1622 DMA
10/07/2020 1133
69153
1
(Soil pH meas) 9045D
1 10/06/2020 2233 SRB
69036
1 351.4
(TKN) 351.2
2 10/07/2020 1045 DMA
10/06/2020 1406
68936
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
4.47
%
2
Ammonia - N (gas diffusion)
350.1
11000
560
290
mg/kg
1
Nitrate - N (soluble)
9056A
51
11
2.2
mg/kg
1
Nitrite - N (soluble)
9056A
93
4.5
2.2
mg/kg
1
Phosphorus
7723-14-0 365.1
31000
5600
1100
mg/kg
1
Soil pH measured in water @
20.4 ° C
9045D
7.2
su
1
TKN
351.2
48000
1100
1100
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/05/2020 1343 JAB2
10/05/2020 0938
68766
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
0.47 J
1.8
0.44
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/08/2020 1402 KSH2
10/07/2020 0847 68742
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
17000
150
55
mg/kg
1
Arsenic
7440-38-2 6010D
7.1
5.5
1.8
mg/kg
1
Cadmium
7440-43-9 6010D
1.6 J
1.8
0.46
mg/kg
1
Calcium
7440-70-2 6010D
17000
1800
230
mg/kg
1
Chromium
7440-47-3 6010D
95
3.7
0.91
mg/kg
1
Copper
7440-50-8 6010D
440
3.7
1.6
mg/kg
1
Iron
7439-89-6 6010D
22000
37
17
mg/kg
1
Lead
7439-92-1 6010D
28
3.7
1.6
mg/kg
1
Magnesium
7439-95-4 6010D
6700
1800
230
mg/kg
1
Manganese
7439-96-5 6010D
1600
5.5
2.2
mg/kg
1
Molybdenum
7439-98-7 6010D
18
15
3.7
mg/kg
1
Nickel
7440-02-0 6010D
46
15
3.8
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:VJ03015-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:10/01/2020 1130 % Solids: 4.47 10/05/2020 2313
Date Received:10/02/2020
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 1 10/08/2020 1402 KSH2
10/07/2020 0847 68742
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
6400
1800
230
mg/kg
1
Selenium
7782-49-2 6010D
8.7
7.3
3.0
mg/kg
1
Sodium
7440-23-5 6010D
2600
1800
230
mg/kg
1
Zinc
7440-66-6 6010D
1000
18
4.6
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
�
I
rtmm,
I
� 3D�
S7
s+IFet1 nYJ
c,x»rvv F� IIQ
r
�I.� 3Wsci
�oI-)las"'M
db 4
W
z
R^
413 ' x
L
L" ! LL c}2
s
�6,a 4
� a� � °S
as
LU rt
o
uo
m
V �
W
d
O
qy
y�
O
43,c
f 4
7p
°1 b
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7
I

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Chmliftt(SRCi 11AE001M1$1 R�vl;Pd-.9/29/2024
t�eAsa,'Fr .71 Issuing Iu,tharity: Pace _NV - WCOL Purge 1 of 1
Saiuplc Receipt Checklist (RQ
[liege: SYMSGRO Cooler lo. ecl.ol hyldate: KSL + 1U12r1V2A Tx3L
4ensofretc.R: t: ,I Paq�e Lslient ❑ k I [3S LJFOdE.x OthC:;
liven` cun4r seals • reseirr Dn the cn❑1cr?
Yarj Q No I WIAA 2, ifcustod seals %,Y= PMLWrLl,. were thew intsel rind unbroken?
Al Snip TT}- C!llo-[Tim drip ID: 11_A r - Tested by. n' I
Jriginal tarrtpCs'ature upsm mccipC Derived (Comcile,4) i mparrJum lip—J.) 3eceipt %Solid nap'C'T' ICY 2.0.zG5C}
3 ;F +2-0 or ?]A !NA o�C MA r 1 A CC NA INN CC.
—horl:Tern erature Blank 21k inst 6ottl;,s I Cain 10: 5 1R Gun Corrcctior Fader; a _`C
p
h7c;thod of Coolant; ❑,f Wet ice ff lec Punks ❑ Dr_y ice u None
Yes E]lfgn E]N " If tempeeattlre of any cooler me 6.OF C, --&, Fr(ject M31W Nulit1
Purl was Natifled by, p4rne i cmil,' faee-to-faao (,circle sue).
yes
No
d Wtl
4, is the omummiul cuuritv's packbig Flip auached m this farm? I
l Ycs
7 Ye'
No
No
15.
Were proper au5tody procedulys (ralirjqulshedlr eivrd) fall owed? 1
6. Vwre c sample IDS listed all 1.70 COG?
rL Yes
Ida
f- ViFels sarnpl IN- listed on all wmpluwriLa;ned's? M
Yes
Nsr
S. Was colieok in dflta & time IL-tcd on lho COC? I
❑ 1'ea
7T0`-
)Was, oa'lec4icxt date & t=rr lied ern all sample cflurtaincr9
i 4- Did all oontainer label nformation (ID, ;]ate, tiule) F19w. urilh the CPO
Yrs
7 ho
I
Ill. Were tests to be perfiormed listed on the COC?
1 12- Did all samplai arrive in the proprr cvutainevs for each test and/or it good evndilkln
0 Ynsi ❑ No �(unbirokci), lids on, arc .1 a --
❑ Yesj 0
No 13- Was adaguabe sample vu:umc rvailuble? _
Nb 14. Were aII garrpkn-mx;eiVed witbin r/x it holding firm or 4 hours, vihicnevor Corner tirst'
Ns 15. 14'ara awry, �am les con lainens 113LS;ingreXoess (oir-_o 0310 sam es 1331ad cul Coe?
] 6. For VOA and R SK-175 = MPICs, rfcro buablet present =pea size "I %"ar 6+:nm in diarritAerf
NO �1+iA in anv of t11= VOA vials? —
❑y ONO
El Yes © Coo
NA 17- Vk+erc 911 T)R€Vnetalse'nutrient aanl le$ i+�oaived at }T of <?'.' 1
N!t l R.'Nare all oyaolde S les received w pH > 12 and sttlfid� .som %W iea::acd at r1 pH >
[ENA11 lg. 9Vsre a KTrl,licr�l�l1Hy JcyanidrJplweno]ffi25,t?6IM$.3 { 0-Sn1+Lj Samples free a:
'residua; chlarinc? II
NA *2,20,17es
Were elicrlt rcmarks+requans (i.e- requested dilurians,-MWhISD rl#zPations,
'tlw Iran scribed from the COC iitto tLC Carom ME sect' on in LIMPI
die quote rumba I istod an [Ire container label? If yes, Quotc #,
5arnijk Preser-ation (M i ist he cnir plcrcd for any aanp Wr) incarTcctl.v pra%erved Dr with hem
Samples) ' w-re received inrtolrcc:ly pTi ywved and
ill =pie receiving'Mlh mL of cirole one=1-LS04, H-1401, I H-A, NaOH usiagt SR it rk �
Time Df preservation NA . LC more Iran 911e, prelervw1ve i s needed, please noly in the W
NA
qdjua&d
below,
were rcecivcd with b'abb* >G mm ir1 dixnneter-
s Nr4 rrC7C roc ivod �titlt TT{ p.5 rn�r1f (1l i; 17rr j and lust e
arcording3y insarnple rc1NCeivii1gwith sodi..rm thingllfam( atSYO,) wilhSheltly TD,
R bartode labelq applied b r: A]ID _ I)Atr.- 10.13q'020
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00066-0-0001- ACRES UTILIZED: 31.7
LANDOWNER: STINSON, JR HENRY ANNUAL DRY TONS APPLIED: 85.87 SITE #: NC CH 00066 ACRES PERMITTED: 31.7
OPERATOR: HENRY STINSON PREDOMINANT SOIL SERIES: NANFORD-BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: FESCUE PASTURE (FSP) CROP I MAX. PAN: 135 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons _(G) site Name of Crop Type
or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) % Residual t Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Source Moist Inches Method* Rate- Rate— mg/kg mg/kg mg/kg T, 2 Crop 1 Crop
Amount LIOM Solids DryTons/Ac i
_—
_7/15i2_02_0 _T8_6,000T0 (G) 1-113 9B_CAEDL ­®RY— "0 —0/2' SUR O�5 0.30 T3_,00_0._00 7,50-0.00 T93 0-0 :Z.804 FSP
7116/2020 198,400.00 (G) r, 4.550 1.187 SBCAEDL DRY 110-<112 )0.30 33,000.00 7,500.00 193.00 27.524 FSP
7/17/2020 68,200.00 (G) 4.550 0.408 SBCAEDL DRY .10-<1/2" SUR (0.5 0,30 33,000.00 7,500.00 19100 9.462 FSP
452,600.00 (G)
Total 2.708 Total 62.790 0.000
ASS®CD
Annual lb. .,a Applied 0.018 pp 0.007
FCumulall,e _Ibs/acre Appi Fed0. 118 0.039
1 1
Federal C.P.L.R. (lbs/acre)-- 36.6 34.8 267.9 15.0 375.0 89.0 1 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant al for bmitting false information, including the possibility of fines and impnisotneqf for knowing violations."
#DATE
NR = Not Reported or Not equ
VIG ired ATURE OF LAND APPLIER Mineralization Rates: Compost -0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
eau
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00066-0-0002- ACRES UTILIZED: 20.0
LAND OWNER: STINSON, JR. HENRY ANNUAL DRY TONS APPLIED: 70.58 SITE #: NC CH 00066 ACRES PERMITTED: 20.0
OPERATOR: HENRY STINSON PREDOMINANT SOIL SERIES: NANFORD-BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 180 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Site u _ Name of Crop Type
r or Cubic Yards (Y) Cond. Precip G Volati- F Mineral- 9 Ammonia Nitrate PAN Applied Receiving Residual €j
tl g
Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application
Month Amount UOM Solids Dry TonslAc Source Moist Inches Method Rate*' Rate*** mg/kg rnglkg mgikg Crop 1 Crop 2 Crop 1 Crop 2 i
7/21/2020 i 117,800.00 (G) 4.550 1.119 SBCAEDL 7 DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,500.00 193.00 25.937 FSH
i
7/22/2020 ? 148,800.00 (G) 4.550 1A13 SBCAEDL w DRY 110-<1/2" SUR 0.5 0.30 33,000.00 7,500.00 193.00 32.763 1 FSH i
712312020 105,400.00 (G) 4.550 1.001 SBCAEDL I DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,500.00 193.00 23,207 G FSH i
Jul-20 372,000.00 {G)
Total 3.533 Total 81.907 0.000
AS
p i Lime Applied
HG
Annual Ibs/acre Applied 0.024 0 008 1.696 3 96 67 01B3 0.003 0.078 0.1J84 0 028 3.603 148.369 Date i Lbs/Ac
Ibs/acre Applied
0.033
0.477 0.012 0.279 1.097
Permit PAN Limit (Ibs/acre) 1st Crop _ -
Federal C.P.L.R. (Ibs/acre)— 36.6 34.8 1,339.0 p 267.9 15.0 � 75.0 89.0� 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK W WTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are signific e s for ubmitting false information, including the possibility of fines and imprisonr9ent f kknnowing violations."
Z
SI NATURE OF LAND APPLIER D E
NR = Not Reported or No equired **' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 "** * See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00066-0-0003- ACRES UTILIZED: 16-9
LAND OWNER: STINSON, JR. HENRY ANNUAL DRY TONS APPLIED: 56.47 SITE #: NC CH 00066 ACRES PERMITTED: 16.9
OPERATOR: HENRY STINSON PREDOMINANT SOIL SERIES: NANFORD-BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP) CROP I MAX. PAN: 135 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
—
Gallons _(G)
,it Name of Crop Type
p
or Cubic Yards (Y) Cond. ::11 cip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) % Residual Dry, Wet i Past 24 Hrs, Application lization ization TKN Nitrogen i, and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate- mg/kg mg/kg mglkg Crop _1 -Z.—p2 Crop 1 —Crop 2
—7/-27—/262-0— 179,800.00_(G) 4.5_50 2-025 — _SBCAEDL DRY 0 —0/2' SUR _0.5 0.3_0 33_,00000 --7—,50000 193.0-0 746_.942 T_S_P
7/28/2020 55,800.00 (G) 4.550 0.628 SBCAEDL DRY 110-<1/2" SUR 0.5 0.30 33,000.00 7,500.00 193.00 14.568 FSP
7/31/2020 9 62,000.00 (G) 4.550 0.698 SBCAEDL DRY "0­1/2" SUR 0.5 030 33,000.00 7,500.00 193.00 16.187 FSP
Jul-20 297,600.001 (G)
Total 3.351 Total 77.697 0.000
Lime Applied
�A �HG �N T:7��Iiel
MO I
I Date
LbsfAc
-D B 0 _�074 7 0.027 3�.418
S 0
0 0.0�
[Annual lbs/acre Applied 023 �O008 I C6U 8 OC349 0 . 107 03 M
lbs/acre Applied
PAN Limit
0.035
0,496 0.012 1 0.299 1 1.145 1 0.100
135
Federal C.P.L.R. (lbs/acre)**** 36.6 34.8 1,339.0 _2_67_.9 1 15.0 375.0 89.0 1 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant p attles r submitting false information, including the possibility of fines and impris
,relyt for knowing violations."
I / 21
JIGNATURE OF LAND APPLIER DATE
NR = Not Reported or of
equired Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge -0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page: 1
FACILITY NAME: SANFORD, NC
WQ PERMIT #: WQ0000543
FIELD#: NC-CH-00066-0-0004-
ACRES UTILIZED: 25.5
LAND OWNER: STINSON, JR. HENRY
ANNUAL DRY TONS APPLIED: 70.58
SITE #: NC CH 00066
ACRES PERMITTED: 30.9
OPERATOR: HENRY STINSON
PREDOMINANT SOIL SERIES: NANFORD-BADIN
CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP)
CROP 1 MAX. PAN: 135
CROP 2 NAME:
CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
I Gallons (G) Site W� I
�
G
Name of Crop Type 4
q or Cubic Yards (Y) �
B Cond. �, Precip �
Volati-
� Mineral-
Ammonia
` Nitrate
PAN Applied Receiving Residual
Date or or Wet Tons (W) %
Residual Dry, Wet, Past 24 Hrs. Application
lization
ization TKN
Nitrogen
and Nitrite
(lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method*
Rate*
Rate*** mglkg
mg/kg
mg/kg
Crop 1 Crop 2 Crop 1 Grop 2
7/29/2 20 0 136,400.00) (G) 4.550
1.015 SBCAEDL 1 DRY "0-<1/2" SUR
0.5
0.30 33,000.00
7,500.00
193.00
23.531 FSP
7/30/2020 1 124,000.00� (G) 4.550
0.923 SBCAEDL DRY "0-<1/2" SUR
0.5
0.30 33,000.00
7,500.00
193.00
21.392 FSP
u
7/31/2020 111,600.001 (G) 4.550
0.830 SBCAEDL DRY "0-<1/2" SUR
0.5
0.30 33,000.00
7,500.00
193.00
19.253 FSP
Jul-20_ 372,000.001 (G)
L
Total
2.768
Total
64.176 0.000
CU R
Lime AppliedAS
Annual Ibs/acre Applied
-HG—
02
007C 1.329fi 0.288 0.—00
6
�Nl 0S-------------
0
Date Lbs/Ac
C.P.L.R.
36,6
6.369
1
267.9
0.009 1 0.227
375.0 1 89.0
10.895
SBCAEDL = SANFORD, NC BUFFALO CREEK W WTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant petialtiO for s4bmitting false information, including the possibility of fines and impriso e for knowing violations."
Z 2t
Cred
ATURE OF LAND APPLIER ATE
NR = Not Reported or Not ... Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation '*** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD#: NC-CH-00066-0-0006- ACRES UTILIZED: 21,7
LAND OWNER: CYNTHIAIANGELA ANNUAL DRY TONS APPLIED: 79.99 SITE #. NC CH 00066 ACRES PERMITTED: 21.7
CTr)QVfrAr)r-Q
OPERATOR: HENRY STINSON PREDOMINANT SOIL SERIES: CID CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: FESCUE HAY (FSH) CROP I MAX. PAN: 189 CROP 2 NAME: CROP 2 MAX, PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) --7
i Name of CrCropTyTypesite
I --T----
or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
I
Date or y or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month # Amount OM Solids Dry Tons/Ac Source Moist Inches Method* Rate- Rate— mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2
—DRY —"6--<112- SUR --6-3-0 33,000.00 —�— —T5-0000 193.00 18.871 --TS—H
—(G) 4.5 0 0.814 SBCAEDL
7/8/2020 93,000.00
719/2020 186,000.00(G) 4.550 1.628 SBCAEDL DRY 110-<J/2" SUR 0.5 0.30 33,000.00 7,500.00 193.00 37.742 FSH
193.00 18.871
7110/2020 142,600.001 (G) 4.550 1.248 SBCAEDL 0-<112" SUR 0.5 0.30 33,000.00 7,500.00 193.00 28,936 FSH
Jul-20 421,600.00, (G)
— ---------
Total 3.690 Total 85.549 0.000
H �G �M —0�� �NS F
0.0 0.f� -f—Lb;/-A—.j
1 0.1 0.0
AS R PB
Annual Ibs/acre Applied 025 00009 OC384 0.118 03 92 30
itive lbs/acre Applied
PAN Limit (lbs/acre)
36.6
7.783
267.9
0.286 1 1.045
89.0 � 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG, LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significantg false information, including the possibility of fines and imprisonoent f9f knowing violations."
21
-�= - _ Cl/Zl
q1GOATURE OF LAND APPLIER It D4rE
NR = Not Reported or Not RVuired Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 211/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00077-0-0004- ACRES UTILIZED: 53.9
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 115.57 SITE #: NC CH 00077 ACRES PERMITTED: 53.9
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: NANFORD BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP) CROP 1 MAX. PAN: 129 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
1 Gallons (G) a Name of Crop Type
or Cubic Yards (Y) p Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) $ % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite 4, (lbslacre) Application 1
o i
Month Amount ? UOM 1 Solids ? Dry TonslAc s Source Moist Inches Method* Rate- Rate*** � mg/kg mg/kg � mg/kg Crop 1 Crop 2 Crop 1 E Crop 2 r
11/412020 155,000.00 (G) 4.470 `s 0,536 i SBCAEDL DRY 0-<1/2" SUR 0,5 0.30 48,000.00 11,000.00 144.00 17.950 FSP
11/5/2020 124,000.00 (G) 4.470 0.429 SBCAEDL DRY "0-<1/2" SUR 0.6 r 0.30 48,000.00 11,000.00 144.00 14.360 FSP
i 11/6l2020 93,000.00 (G) 4.470 � 0.322 �' SBCAEDL DRY � 0-<1/2" I SUR 0.5 � 0.30 46,000.00 11,000.00 °' 144.00 10.770 FSP 1
r 11/9/2020 142,600.00 (G) 4,470 0.493 SBCAEDL DRY 0-<1/2" SUR 6 0.5 0.30 48,000.00 11,000.00 144.00 16.514 FSP
LN.v-20
020 i 105,400.00 (G) 4.470 0.365 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 12.206 FSP
I 620,000.00 (G) s 1
Total 2.145 Total 71,800 0.000
` AS CD CU CR PB HG MO NI SE 2N P� Lime Applied
Annuallbs/acre Applied 0.030 0.007 1.887 �g 0407 0.120 0.002 0.077 0.197 0.037 4.288 132.935 �D>ate. Lbs(Ac
0.030 1 0.007 1 1.887 ) 0,407 S 0.120
1st
0.197 1 0.037
29
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.6 1,339.0 a 267.9 15.0 375.0 89.0 ; 2,500.0 )
SBCAEDL = SANFORD, NC BUFFALO CREEK W WTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significa en tie f submitting false information, including the possibility of fines and imprisooeq
ffar knowing violations."
SI ATURE OF LAND APPLIER ATE
NR = Not Reported or of aired *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SU - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection(Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/112021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WO PERMIT #: WQ0000543 FIELD#: NC-CH-00077-0-0005- ACRES UTILIZED: 15.6
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 57.45 SITE #: NC CH 00077 ACRES PERMITTED: 15.6
OPERATOR PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID LIGNUM CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: CORN SILAGE (CSI) CROP I MAX. PAN: 224 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Site Name of Crop Type
or Cubic Yards (Y) I Cond. v Precip t Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
I
Date or or Wet Tons (W) i % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month
A
Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate- Rate— mg/kg # mg/kg mg/kg Crop I Crop 2 Crop I Crop 2
_;'_O-_�1/2- �;_U_R —6.-5 T3_0 16,00000 12.00-0.00 —69.70— 793 4-70
--61412020 DRY
1 6�y T CSI
T67—,400.00 (G) 5.420 2.425 SBCAEDL
6/512020 M86,800.00, (G) 5.420 1.258 TSBCAEDL DRY 110-<1/2" SUR 0.5 0.30 56,000.00 12,000.00 69.70 48.466 CS1
if
Jun-20 254,200.00' (G)
Total 3.683 Total 141.936 0.000
AS ED PB HG MO N1 SE ZN P Lime Applied
CLI CR L
—6,261 176.778 Date LbsJAc
0.046 0.01 T8_ 0.184 0.003 0.125 0.317
Annual lbs/acre Aoulied 73 0.57.5 0.035
lbs/acre
.080 0.214 1 0.658 1 0.062 1 11,281
Permit PAN Limit (lbstacre) 1st urop:
Federal C.P.L.R. (lbs/acre)-- 36.6 89.0 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant for stibrruttir12 false information, including the possibility of fines and imprisghmett for knowing violations."
?—/q / V
,"ATURE OF LAND APPLIER T—FTE
NR = Not Reported or Not Required ... Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DEN R FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00077-0-0007- ACRES UTILIZED: 17.1
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 72.87 SITE #: NC CH 00077 ACRES PERMITTED: 23.4
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID LIGNUM CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: CORN SILAGE (CSI) CROP I MAX. PAN: 224 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Name of Crop Type
Gallons (G) Site Name of Crop Type
or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount LIOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate— I mg/kg I mg/kg mg/kg Crop Crop 2 Crop I Crop 2
8/2-020 --14-8,800.6-0 (G) I_5.42_0_f 19-67 SBCAEDL 6_RY_ "0 _<112- --7SUR --0.5--0.30--56,6O-O.00---i27000-00 _69.70_,75_796 CSI
May-20 148,800.00 (G)
--r— 7-T, _
6/3/2020 173,600.00 (G) 5.420 2.217 SBCAEDL DRY 110-<112" SUR 0.5 0.30 56,000.00 12,000.00 1 _69-7-085431 CSI
Jun-20 173,600.001 (G)
Total 4.184 Total 161.227 0.000
AS I CD CU CR PB HG MO SE 039
0.142 0.36 _� 0.039
AS
CD CU R �HG �MO �_N_l 7­SE Lime Applied
0 00 0.0 0
0.052�O�016 3.263 OC653 ��O.P2'09 0.003 360 —Date Lbs/A.
Annual lbs/acre Applied
0.080
1.148 1 0.334 1 0.005 1 0217 ! 0,644
Permit PAN Limit (lbs/acre) 1 st Crop
Federal C.P.L.R. (lbs/acre)**- 36.6 89.0 2,500.0
tl
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significa en ties o submitting false information, including the possibility of fines and impriso 4 knowing violations."
f 91IGNATURE OF LAND APPLIER 7 DArE
NR = Not Reported or 4,/Required Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 211/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: W00000543 FIELD#: NC-CH-00077-0-0008- ACRES UTILIZED: 11.8
LANDOWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 61.66 SITE #: NC CH 00077 ACRES PERMTTED: 31.7
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: NANFORD BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: CORN SILAGE (CSI) CROP 1 MAX. PAN: 231 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Name of Crop Type
g' or Cubic Yards (Y) % Cond. Precip Volati- Mineral- p Ammonia Nitrate PAN Applied Receiving Residual
i ¢
I Date or or Wet Tans (W) 6 % i Residual Dry, Wet, � Past 24 Hrs. Application � lization 4 ization i TKN Nitrogen� and Nitrite " (Ibslacre) Application
Month Amount UOM Solids Dry TonslAc r Source Moist Inches Method Rate** Rate*" mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
5/14/2020 148,800.00 (G) 5.420 2.850 SBCAEDL DRY "0-<1/2" S R 0.5 0.30 56,000.00 12,000.00 69.70 109.840 CSI s
5/15/2020 124,000.00 (G) 5A20 2.375 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 56,000.00 12,000.00 69,70 91.533 CSI E k
May-20 272,800.00 (G)
Total 5.225 Total 201.373 0.000
AZN L�Applflie�dR�PB�O�HG SE S CCO
0004 83
06 Date
.0Annual ibs/acre Applied 6AM
Ibs/acre Applied 6.676 6.022 4.629� 0.952 0.289 0.004 0.200 0.513
PAN Limit
34.8
89.0
SBCAEDL = SANFORD, NC BUFFALO CREEK W WTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant lti fors mitting false information, including the possibility of fines and imprison �eent 4,r knowing violations."
Z a
S TURE OF LAND APPLIER I DATE
NR = Not Reported or Not R ired *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD#: NC-CH-00077-0-0011- ACRES UTILIZED: 29.1
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 73.96 SITE #.- NC CH 00077 ACRES PERMITTED: 29.1
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID SILT LOAM CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: FESCUE PASTURE (FSP) CROP 1 MAX. PAN: 134 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) — Site Name of Crop Type
or Cubic Yards (Y)
Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
N
Date Or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN # Nitrogen and Nitrite (lbs/acre) Application
Amount Solids Dry Tons/Ac Source Moist Inches Method* Rate- Rate— mg/kg mg/kg mg/kg Crop op I Crop 2
Month unt UOM crop I F cro,
---T8—,000.00 -- —T44 0-0 26,-599--"�F-
-f2—/10/2020 ---1-24,000.650---(-G—)--A70 0.794 T —SBCAEDL —DRY`— ---0-Z1-1Y— —SU R 0-5 —6-3-0 11,000.00 1 FSP
12/11/2020 148,800.00 (G) 4.470 0.953 SBCAEDL DRY 1'0-<112" SUR 0.5 0.30 48,000.00 11,000.00 144.00 31.919 4 FSP
12/12/2020 124,000.00 (G) 4.470 0.794 SBCAEDL DRY -<1/2" SUR 0.5 k 030 48,000.00 11,000.00 144.00 26.599 1 FSP
LD..-20 396,800.001 (G)
Total 2.541 Total 85.117 0.000
AS T—CD CU CR —P-§---T,—HG MONILime Applied
B IN
— — :]! --- ---T 1 0.234 OSOL 50L83 157!�,58
FA..u.1 lb./a.,. Applied 0.036 0.008 1 2.237 0,483Tf 0.1742 �O002 Date Lbs/Ac
lbs/acre
0.020 1 4.
0.005 l 0.190
10.634
Permit PAN Limit (lbs/acre) 1 st Crop,
36.6 34.8 1,339.0 15.0 375.0 89.0 2,500.0
Federal C.P.L.R. (lbs/acre)—* 267.9
-J
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significantan
information, including the possibility of fines d ninphison4ent knowing violations."
7 21 iq4; I
%--- SIG URE OF LAND AP LIER DfTE
NR = Not Reported or Not R ired Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD#: NC-CH-00077-0-0013- ACRES UTILIZED: 15.4
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 48.54 SITE #: NC CH 00077 ACRES PERMITTED: 15.4
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID SILT LOAM CATION EXCHANGE CAPACITY (NON-503):
CROP I NAME: FESCUE PASTURE (FSP) CROP I MAX. PAN: 134 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Site Name of Crop Type
or Cubic Yards (Y) Cond. Precip volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
I Date or or Wet Tons (W) % Residual DryWets Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
, , Past 24 Hi
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate— Rate— mg/kg mg/kg mg/kg Crop-1 Crop 2 Crop 1 Crop 2
DRY 0-1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 50261 FSP
/2012020 1 24,000.00 (G) 4.470 1 �501 SBCAEDL
/21 /2020 136,400.00 (G) 4A70 1.651 SBCAEDL DRY 110-<1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 55.287 FSP
0
EN2 260,400.00 (G)
Total 3.152 Total 105.548 0400
PB HG MO NI SE ZN P Lime Applied
JAnnua'I I I bs/acre Applied --0-04-5--T 0. 0 1 _0E 2.774 0.599 0.177 0.003 0.113 a 0290 0.055 6.304 195.414 Date Lbs/Ac
lbstacre Applied
0,010 1 2.
177 11 0.003
0.055 1 6.304
Permit PAN Limit (Ibs/acre) 1st Crop
Federal C.P.L.R. (lbs/acre)**— 36.6 34
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted- I am
aware that there are significant pe ies�mitting false information, including the possibility offines and impVent X : knowing violations."
717_ t
N-11 SIGtOTURE OF LAND APPLIER I DArrE
NR = Not Reported or Not Reiredl Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 211/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD* NC-CH-00077-0-0014- ACRES UTILIZED: 18.9
LANDOWNER: PAUL& LUCY PRICE ANNUAL DRY TONS APPLIED: 50.85 SITE ft: NC CH 00077 ACRES PERMITTED: 18.9
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID SILT LOAM CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP) CROP 1 MAX. PAN: 134 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): See list at bottom of report
Name of Crop Type
-d- (G—) —7 —,,T— _sit -
I
or Cubic Yards (Y) Cond. Precip Volatl q Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons (W) % gResidual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount LIOM Solids Dry Tons/Ac E Source Moist Inches Method* EI Rate** Rate- mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
--'— 0.5 0.30 78­—
11/24/202 99,200� (G) 4.470 0.978 SBCAEDL DRY 0-<112" SUR 000.00 11,000.00 144.00 32.763 FSP
11/25/2020 173,600.00 (G) 4.470 1.712 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 57.335 FSP
Nov-20 272,800.00 (G)
Total 2.690 Total 90.098 0.000
AS �16�D �EC RE PB HG MO NI SE Lime Applied
MO
0 11 �0.00�30�.097 Lbs/Ac
[A .5 E70151� Date
I lbl..,. Applied 0.009 �2.368�� 0.511 .151
Permit PAN Limit (Ibs/acre} 1st Crop' 134
Federal _C.PL.R, (lbs/acre_)—36.6 1 34.8 89.0 2,500.0
L_
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant P submitting false information, including the possibility of fines and impris9fimen /for
knowing violations."
Zi
NATURE OF LAND APPLIER PATE
NR = Not Reported or Not Uquired Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD* NC-CH-00077-0-0015- ACRES UTILIZED: 14.8
LANDOWNER: PAUL& LUCY PRICE ANNUAL DRY TONS APPLIED: 39.29 SITE #: NC CH 00077 ACRES PERMITTED: 14.8
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: NANFORD BADIN CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE PASTURE (FSP) CROP I MAX PAN: 135 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) (G) 7- Site Name of Crop Type
or Cubic Yards (Y) Cond Preelp volati Mineral- Ammonia Nitrate PAN Applied Receiving Residual
'
Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application , lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount - UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate- Rate*- mg/kg mg/kg mg/kg --dr—opl Crop 2 Crop 1 —Crop 2
--1273—/2020 --12-4,006-60- —(G) --4—.470 1.562 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 52.299 S FSP
12/4/2020 86,800,00 (G) 4A70 1.093 SBCAEDL C DRY 0-1/2" SUR 0.5 0.30 48,000.00 11,000.00 144.00 36.609 i FSP
Dec-20 210,800.00 (G) J
Total 2.655 Total 88.908 0.000
�HG�MO N I SE ZN P Lime Applied
10
I 0.096 0.2� 0.0 �310 �164P60,1
AS ::4::0:CD9", CU CR PB G 0.0 0.096
0.038 -T-- 0. �Lb./A.
0 2.336 0.504
Annual lbs/acre Applied 0.069 2.336 0.504 0 1�49 0.003 244 0,046 5Z
Applied
1st
0,504 t 0.
0.244 1 0.046
135
Federal C.P.L.R. (lbs(acre)**- 36.6 34.8 1,339.0 267.9 15.0 375.0 89A L2,501.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penal7l sub false information, including the possibility of fines and impris96 mer/ for knowing violations."
0
/ n
, A
SIGNA E OF LAND AP LIER IDATE
NR = Not Reported or Not Requi Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, InjectorVincorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2J1/2021 DENR FORM FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: I
FACILITY NAME: SANFORD, NC WQ PERMIT #: WQ0000543 FIELD#: NC-CH-00077-0-0016- ACRES UTILIZED: 15.2
LAND OWNER: PAUL & LUCY PRICE ANNUAL DRY TONS APPLIED: 70.06 SITE #: NC CH 00077 ACRES PERMITTED: 30.3
OPERATOR: PAUL & LUCY PRICE PREDOMINANT SOIL SERIES: CID LIGNUM CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: CORN SILAGE (CSI) CROP I MAX. PAN: 224 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Name of Crop Type
Gallons (G) Site Sit
S C C-nd Pre
W W
a _TDryet, FP
Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
or Cubic Yards (Y) Precip
I Application
Date or or Wet Tons (W) % Residual ast24Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre)
Month Amount UOM Solids a Dry Tons/Ac Source Moist Inches Method* i Rate— Rate— mg/kg mg/kg mglkg —E-ro—pl Crop 2 Crop 1— Crop 2
7R-12/2020— _1_48 80-0 (FO _(G) —5.4-20-1 22-13 SBCAEDL DRY "0-1/2" SUR —0.5 0-30 _56,006._00_12_,00000
5/13/2020 161,200.00 (G) 5,420 2.397 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 56,000.00 12,000.00 69,70 1 92.377 CS1
I
May-20 (G)
310,000.00
Total 4.610 Total 177.648 0.000
C' 1:: 1:! 1 1 2 SE ZN P Lime Applied
AS CID CU 1:l 018 3.595 0.7
EA..u.1 lb./..,e Applied _0057— O.018 q 909 n7 0.003 0.157 1 0.396 1 0.043_ 7.836 221.256 Date Lbs/Ac
224
Federal C.P.L.R. (lbslacre)—* 36.6 034.8 @ 1,339.0 267,9 1 15.0 375.0 � 89.0 2,500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant p nalt 17biruitti false information, including the possibility of fines and knowing violations."
-7A
2� "1=
` SIGNAT OF LAND AP LIER ATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R. : Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 See Site pH & Lime Application Records Section of Report
Printed: 2/1/2021 DENR FORM FSF (12/2006)

SECTION 4

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Sanford
Lot Number:VC25024
Date Completed:04/09/2020
NIM�� Mr�
04/10/2020 10:23 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VC25024
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure. The LOQs
have been changed to reflect the additional mass.
PCBs by GC
The following sample was diluted due to the nature of the sample matrix: VC25024-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received: 03/25/2020
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
03/25/2020 2220
SRB
48982
1 350.1
(Ammonia - N ) 350.1
25
03/26/2020 1321
SLC
48894
1
(Ignitability) 1010A
1
04/07/2020 1032
SLC
50227
1
(Nitrate - N ) 9056A
1
03/29/2020 1501
HKL
49410
1
(Nitrite - N ) 9056A
1
03/29/2020 1501
HKL
49786
1
(Phosphorus) 365.1
25
03/27/2020 1235
DMA
03/27/2020 0758 49065
1
(Reactive Cya) 7.3.3
1
03/27/2020 1610
KFE
03/26/2020 0910
1
(Reactive Sul) 7.3.4
1
03/29/2020 0909
HET
03/26/2020 0910
1
(Soil pH meas) 9045D
1
03/26/2020 1940
SRB
49111
1 351.4
(TKN) 351.2
2
03/31/2020 1411
DMA
03/30/2020 0822 49288
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
3.76
%
1
Ammonia - N (gas diffusion)
350.1
17000
660
350
mg/kg
1
Ignitability (Pensky-Martens Closed -Cup)
1010A
>140
140
0
o F
1
Nitrate - N (soluble)
9056A
90
13
0.65
mg/kg
1
Nitrite - N (soluble)
9056A
6.6
5.3
0.51
mg/kg
1
Phosphorus
7723-14-0
365.1
29000
3300
660
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
50
mg/kg
1
Soil pH measured in water @ 20.5 ° C
9045D
6.8
su
1
TKN
351.2
84000
1300
1300
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/5030B 8260D
10 04/09/2020 0242 JTH
50426
04/07/2020 1917
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Benzene
71-43-2
8260D
ND
0.050
0.0040
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
0.049 J
0.10
0.020
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.050
0.0040
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
0.0040
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
0.0040
mg/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.050
0.0040
mg/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.050
0.0040
mg/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.050
0.0040
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
0.0040
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
0.0040
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
103 70-130
1,2-Dichloroethane-d4
103 70-130
Toluene-d8
109 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/3520C
8270E 1 04/07/2020 1426 JCG
04/01/2020 1522 49681
03/26/2020 0255
2 1311/3520C
8270E 2 04/07/2020 1740 JCG
04/01/2020 1522 49681
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
0.0050
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
0.0050
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
0.0050
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
0.0050
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
0.010
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
0.010
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.98
0.080
0.030
mg/L
2
Nitrobenzene
98-95-3 8270E
ND
0.040
0.015
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
0.020
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
0.0050
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
0.0050
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
0.0050
mg/L
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
64 37-129 68
37-129
2-Fluorophenol
37 24-127 43
24-127
Nitrobenzene-d5
64 38-127 62
38-127
Phenol-d5
66 28-128 57
28-128
Terphenyl-d14
82 10-148 80
10-148
2,4,6-Tribromophenol
44 41-144 46
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
Leachate Date
1 1311/8151A
8151A 1 04/03/2020 1245 DAL1
04/01/2020 2347 49691
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
0.0050
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
0.0013
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
89 50-112
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 3665A 8082A 10 04/08/2020 1412 DAL1 04/06/2020 2220 50123
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016
12674-11-2
8082A
ND
7900
ug/kg
1
Aroclor 1221
11104-28-2
8082A
ND
7900
ug/kg
1
Aroclor 1232
11141-16-5
8082A
ND
7900
ug/kg
1
Aroclor 1242
53469-21-9
8082A
ND
7900
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
7900
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
7900
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
7900
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
87 41-132
Tetrachloro-m-xylene
87 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 04/02/2020 1712 DAL1 04/01/2020 1432 49666 03/26/2020 0255
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
gamma-BHC(Lindane)
58-89-9
8081B
ND
0.00040
0.00017
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
0.0015
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
0.00016
mg/L
1
Methoxychlor
72-43-5
8081B
ND
0.0016
0.00021
mg/L
1
Toxaphene
8001-35-2
8081B
ND
0.0080
0.0030
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
77 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 03/26/2020 1435 KSH2
03/26/2020 0218
48980
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL Units Run
Mercury
7439-97-6 7471B
0.63 J
2.0 0.48 mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL
= Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J =
Estimated result < LOQ and > DL
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client:Synagro Laboratory ID:VC25024-001
Description: Sanford WWTP Matrix: Solid
Date Sampled:03/24/2020 1030 % Solids: 3.76 03/25/2020 2220
Date Received:03/25/2020
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
Leachate Date
1 1311/3010A
6010D
1 03/27/2020 1909 LLL
03/27/2020 0423 49145
03/26/2020 0255
1 1311/7470A
7470A
1 03/27/2020 0857 KSH2
03/27/2020 0400 49150
03/26/2020 0255
2 1311/3010A
601OD
1 03/28/2020 1459 KSH2
03/27/2020 0423 49145
03/26/2020 0255
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Arsenic
7440-38-2 6010D
0.067 J 0.15
0.025
mg/L
1
Barium
7440-39-3 6010D
0.11 J 0.25
0.031
mg/L
1
Cadmium
7440-43-9 6010D
ND 0.050
0.0060
mg/L
2
Chromium
7440-47-3 6010D
ND 0.10
0.013
mg/L
1
Lead
7439-92-1 601OD
ND 0.10
0.047
mg/L
1
Mercury
7439-97-6 7470A
ND 0.0020
0.00091
mg/L
1
Selenium
7782-49-2 601OD
ND 0.20
0.085
mg/L
2
Silver
7440-22-4 6010D
ND 0.10
0.021
mg/L
1
ICP-AES
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst
6010D 1 03/27/2020 1819 LLL
6010D 1 03/28/2020 1543 KSH2
Prep Date Batch
03/26/2020 2331 49117
03/26/2020 2331 49117
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
17000
170
65
mg/kg
2
Arsenic
7440-38-2 6010D
11
6.5
2.2
mg/kg
1
Cadmium
7440-43-9 6010D
2.5
2.2
0.55
mg/kg
2
Calcium
7440-70-2 6010D
18000
2200
270
mg/kg
1
Chromium
7440-47-3 6010D
84
4.4
1.1
mg/kg
1
Copper
7440-50-8 6010D
450
4.4
2.0
mg/kg
1
Iron
7439-89-6 6010D
24000
44
20
mg/kg
2
Lead
7439-92-1 6010D
30
4.4
2.0
mg/kg
1
Magnesium
7439-95-4 6010D
6600
2200
270
mg/kg
2
Manganese
7439-96-5 6010D
2000
6.5
2.6
mg/kg
1
Molybdenum
7439-98-7 6010D
21
17
4.4
mg/kg
2
Nickel
7440-02-0 6010D
49
17
4.6
mg/kg
1
Potassium
7440-09-7 6010D
11000
2200
270
mg/kg
1
Selenium
7782-49-2 6010D
5.6 J
8.7
3.5
mg/kg
2
Sodium
7440-23-5 6010D
3300
2200
270
mg/kg
1
Zinc
7440-66-6 6010D
1000
22
5.5
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
2
�
� R
r.:
_ _ L
FT
A � "tt c '
00 { C
E ( i7
37O
all UH NM
aswa,o pup x3
=�11:J lul0�
(ua�ag
101eris.' egad C
Vj-j V a Beu+Q
8Cd
`� 4C I
C p ro
u
(b
r�ayy
1JJ
j
CL M
�
o
Va
T
9
z
a
r =
o
k t
"
n
' p
0
9Fiw
L 4
CL Q {l1
Q
a: 7
LM
7
z
I x
61c2 SP
4
m
n
J
a ca
fl Q
o
LL C
l—L =p
I=
1 E
F
—
Vdi
AM
0 L
T
0
1] C W
IE
EIC
c
6
1=1111111111M
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
ra IO'.
]]rcw�eltl `�'G?7�4Cr. r,�Eao18C-14 �'
h'unc��rve d+27:n I S
F sa nple Receipt C heek1st (SRC 13pkv'
C[icrit, Syna,gt'o _ Goolerlispectedhvfdafc:r-x:a r 01.Qt --o VC25024
llcans o: re cipt: ❑ ;1-3I : client 2 UPS ❑ FedF,x Other;
®Y Nta 1, W clv custadY saa is presettC ;)n the cooler?
J Yrs Nn NA12- If custody sm[s wore praseni: -e9-e they udu4i and unbrokrn?
IPH '�Iriip ID: NA Chlorine Stria ID, NA — Tnttd �A
by.
Original lem-jcrature upcirl rrrooipt f JD� r]+�_d I Cot'rec�rrl) tetnpelaUtr* upon receipt solid Snap�Cup la; 19 2313
.8 15-8 40 fqA !t'A ¢C NA iNA NA +TlA o�
1+letl>od: ©:'emperPdt� Blartk®AgainstBottles IRCiun 117: 5 IRGil uMwrcu6DnFacWr, 0 °C
1Uthod cfcool unt: R`et I" F-1 I— Rjoks ❑ Dry lcc � Mone. --
0 Yes ❑ TON
f tcmpt.rglurtl Df sny canlcr cxcek red 6A c Prtsjret 11aa14,e-r Notifi ed - —
_ PM was NQfiFtcd try: pE,o'.�c ? attiz.il ! (li-40-fact,'Circle ale)_
i� i'es No ❑ 14A 4- 1t t:,10P coramemial courier's picking slip atl�tched w tills form'
® `res � hlo 5- w'ere }rnpp�cus[�iv 7mrrdures{�eliotlaisJledlreceivt�d}fo][ov�+ud'd
Yew r fa 5, �Nca,c 3Ainh31« Ills 115jtW an the { O C',1
I j YC3 ❑ Na 1- Wem sample IDs listed an rill sample contaiticrs?
Yes ❑Teo S. Vddrtcnl[MtiQn r141�- R. time listed oil thar_OC?
❑ Yes 21 ]-0 9. Was wI1,� stior dax sim�a iisferl inr all sample _cintainers?
E Yes ❑ M1ir, 10- Diet H I I c•o-jteitj% label ui arrnaicn (ID, date, fait) agree witli 11,c OOC7 -
YE8 ❑ No' I [. creiw1l. to be FerformL-d Iisted ckn he k:OC?
yea i�To
12- Did all sarap[cs arrive irk W PJ%OPOT oontairers #or each Iq�i! andlor in goad catlditior.
Ol
(unbroken, lids on, etcrp,
m Yes NO
x
14- V'I�ro all sarrlp]cs MCeived IVithilt', tic hcilding lime or49 hours, %vhjc:.cver op,rtcs FRsc!
15r WCM all Sam les cgruttinei:s miss:npfexcL= (cimrenne:)lain 1e47klr�: listed n CO S
© YC3 ❑ No
15. For VOA ar-d RSK-175 snmpie�, here bubbles 1prr;4rnt >"pC s:ac" r 6:rttn
0 NA in diblxctcr)
in ktn+ oftlie VOA viaJs?
❑ YB0 No
VJ NA 17. Were all T)Rf�f111�A1;<!rll ITienL 581;1p165 !$Ctil'4d 1t fl pH of •: 2?
Yes ❑ iNu
A:A i8. k `ere a[I vvariids stmplcs reoeiy J at a jH > 12 and sulFide 5MP]a recelvW at a pi i > 9?
❑ Yts QNu
!9. V4`ere all spp rcable Nl I T1CNloya,ii ,i,c nollp j {{ Ins [,j samples tree oT residt_a1
cblorire?
❑ llcs Q Vo
O NA 20- Wert client rcn)arhs'fcqucsts 1:.8- request--cl dilutions. �1S1ASD elea=gnaiiprks, etc--_}
vormet]ytranwribed horn the COC Jryt dic totnmenrsection in LIMB?
Yes No
? I . VJ�s the quote nutiber Issted on Ibc cm[kl:LMX labs:? i Fyes, not #` NA
Sa�niple Fruservatica (,rYfuSt ba cvrrtpja, for a:3y s3r.jPle><8) inc3rreody p�.s:rue e or with hc_Hdspace.)
5arr'p[d45; 'vero Teceivee] 4�cr}rrectly prageuwW kmd v,ere �IdjuZt ! fucardingly
insampi: 7�=jyjjjg will. NA mL oCdrole talc InSO4, HNO3, I-TCI, N�OH tl3irt c £R it NA
ritrre of preservt�tion If more fhan one Presrrvativo is needed, p[case nom in the comme�its Wow.
Samp(g() NA
,Lvere reeaived wide bubbles >5 MIA in dialreter.
Satnglx4(s) ItiA raceiYt}d with TIC > U,5 ir.VL (rr#J 9 is ,zv) Hnd were
�ljk:sled acm-dillaa(y in sample r�pp1ritisgv%'irii sodiorn thiostllfate (MS _) w-'* S--3, My 1D: ---NA
i 1 LwtsWu labels dpp[ied
bv: -Kh _ Data: 4lg5?2020
Comments,
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name: l
Monitoring Period:
of Sanford WQ Permit Number: W00000543
Buffalo WWTP NPDES Number: NCO024147
From 01/01/20 To 03/31/20
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf .,....I:....hlo t....1+ar....f;— ,. r —A ll9oce A nr rJave Rl ommnlatn tha fnllawina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'
CFU
<12900
69300
<90400
CFU/g
0
Quarterly
Grab
SM9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (tye or print)
61J&L a. 11 a
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
F � Synagro +
Sanford WWTP fi�1�D le Information
Information
fit. Boyd 01109/20 �#
Analyses and Results
NC OE.NR 0854
NC PHHS 937799
US EPA#NCOM8
2001.079
Yes
K Siena 01JOW20
2001-079 1
;kmok Cr For. calif stne-s - 550500
cPkIg
"'Mk." OTtl .120 RL W2,20 - MF
2
<59700
CPWY
.svao
3
40100
CM4
40100
4
<40200
6
e13600
crwQ
1V�uxi
6
e90400
club
wuoo
7
02900
alliq
, wz
Geo;noon 69300
2001-079 1
_ IS A) 1.98%
01110120 RL 2640 G -7S
2
1.68%
nuR
3
2,490i4
4
2.49'%
6
0.734°/Q
0
6
s�
0.01
7
�y1,11%
0.776%
V Cl
Report Rg1tiQY1
i.rb blrr for _ Date
SanfnKd td(.' '17330 c4�r rarGa�nkrs,�t€ [in .e �ii

ndi
_
U-1
tj
4, F...
(
W
0ML
`v
y
at
IVS VOA
�!
I
009 ! ozs
ILIAV
y.
A, W z
xIiiuVq
CO
J..
O
N
dy
u
1
fi

CAMERON TESTING SERVICES
Sample Preservation Check -In Sheet
Projeot # zD Checked In By:
Date: Q l �] Zfj Temp 4.0 °C Time:
Rothe: CD CTS CTS USM Fcdex General UPS
Sampled Pickup Courier
Sample Analysis Matrix Comp! Container PI'egt;t3t1Ve
No Requested Grab
Nano HCL M804 HNO3 NaOH Thio Other
C I / G one HCL MSO4 HNO3 NaOH Thio Other
d
C J
P
G
❑
HCL
H2304
HNO3
NaOH
Thio
Other
3
C I
P
G
IICL
H2SO4
HNO3
NaOH
Thin
Olhor
C /
P
G
one
HCL
R2804
HNO3
NaOH
Thin
Other
C / G
P
G
HCL
H2SO4
HNO3
NaOH
Thi❑
Other
C G
P
/ G
HCL
HCL
H2804
H2SO4
I-IN03
HNO3
NaOH
NaOH
Thin
TWO
Other
Oilier
�' (}
I G
one
C / G
P / G
None
HCL
IM04
HNO3
NaOH
Thip
Other
C / G
p / G
None
PMCL
H2SO4
HNO3
MON
Thin
Other
C / G
PIG
Nanc
HCL
H2804
HNO3
1ga0H
Thin
Other
C / G
PIG
None
HCL
H2SO4
HNO3
Moll
Thlo
Other
C / G
P I G
None
HCL
H2SO4
HNO3
Na07i
Min
Other
C / G
P / G
Norio
HCL
H2804
HNO3
NaOH
Thlo
Other
C / G
P / G
None
HCL
H2804
BN03
MOH
Two
Olher
C / G
PIG
None
HCL
E2804
HNO3
Na0H
Thio
Other
C I G
P / G
Norio
HCL
HZSO4
LW03
NaOH
Thia
Other
C / G
PIG
None
IICL
H2804
I-IN03
NAOH
Thlo
Other
C l G
P l G
None
HCL
H2SO4
IIN03
NnOH
TUGOther
COMMENTS:

City of Sanford
Big Buffalo WWTP
Sludge Calculations
IN
VSR = 68.51371
W1
DISH
111.4005
W2
WET
211.3736
W3
DRY
112.9494
W4
ASH
111.7579
1.549317
PERCENT VOLITILE SOLIDS 0.769256
OUT
W1
DISH
112.1643
W2
WET
212.1990
W3
DRY
119.5975
W4
ASH
115.7908
PERCENT SOLIDS 7.430622
PERCENT VOLITILE SOLIDS 0.512121
PERCENT VOLITILE SOLIDS REDUCTION 68.51371
Is it above 38% Yes

VSR
Grab Date: 3- 1-2v Zo
Lab Tech's Initials:
RAS (IN) DIGESTER
Sample OUT
Volume
100 MIS.
Dish # (�
Crucible Weight
III , OvS
gm
Crucible & Liquid
2.11 .73 -) 3 (6
gm
Dried
l l 2 -WIA
gm
Burned
3-14
m
111.7S79
100 MIS.
n
112. 1643
Zt2_ IggO
115��7")08
Date/Time In: 3-3-2020/ 11,4 2 %-
Date/Time Out: 3-H-2olo/ 11,kI- Drying Oven p. 1py 1 C
Temp: °
Time ln: 3- f-Tos, 12' Zquffle Furnace '"
Time Out: 3-k-Zato IZ' W1 Temp: T T 0 °C
Were the samples well mixed before analyzing? Yes V No /
Was the temp of the drying oven in the proper operating range? Yes, No
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes V No
If not what were the corrective actions?
Samplers T (- ,, S 1`3

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
of Sanford WQ Permit Number: WQ0000543
Buffalo WWTP NPDES Number: NCO024147
From 04/01/20 To 06/30/20
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlieahle to alternative nerfnrmed (Class A or Class Rl emmnlete the fnllowinu monitnrinQ data!
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 611
CFU
17800
51800
125000
CFU/g
0
Quarterly
Grab
SM9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifolm
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (type or print)
11 ;l
Signature of Preparer* ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc- Laboratory Report
NC DENR M54
NC PHHS 937799
US EPA*NC01948
ClkmL-
Synagro
CT9 Pr0j.
004-148
Project:
Santord WWTP
R1uqulatory
Y'bs
Sample Information
SOMP106
G. Wynne Dote 04171/20
.v"d
C. Cameron
Do*
0401120
Analyses and Results
LablQ
S&MF34010 Ann"
R suit
C
J
20 E
�R�oirrlrpft
1
2004-148
-1 Fec. ColdorfrF-S
53200
utpu
17M
0W'm K
9MD -MF
-2
35600
a+a
17aw
-3
35600
CFuig
17BD8
-4
125000
Meg
1780@
-5
124000
cFkwo
178b4
-6
53400
M%w
178W
-7
17800
uwg
178M
Goar can
51800
2OD4-148 01
-1 TS M
5. 64 %
%
0.01
04/t 1 I2O RL
2540 G -T5
-2
5.6 %
%
a.a,
�3
5.62%
%
11.131
-4
5.61 %
um
-5
5 63%
0.o1
5-61 %
%
601
-7
5-62 %
'A
801
Ropoct
Rovlow
—
Lab DIroctor
onto
219 S. stwo a Su.
Sanford NC 37.13G
9i9-248.4.240
ChM d"WrOlF*UnML?. CMn

:.fir'
219 S. Sieele Sir.
Sanford, NC 27nO
Pharie: 919-2+]LB-424 D
Cameron Testing Services, Inc.
KC M)GVQ Ce't fi-,'5c N(, PH S Cert # 37799 US EPA NC41918
Chain of Custody
Page I & t
Cornparty:
Ciagf
Email;i.ksynagrocorn
CTS lab use only
Contact:
�„ `
4'1 S Y �i 4x �l �
kro�ie;
-
]'�,' �3�6'49'1r
Sample Temp Lab 1D
Address {City,
284 Boger Rd.
Fax-
109 (YIN)
State, Zlp}
N1oc€csvillly, NC
27028
N6tes:
Permit(YIN)
Project,
�Gk y
Rush {YEN} Due:
Collected:
Nriaw 445
t iL! -
Signateire:
Samp4 Information
Number of battles
Requested Analysis
°0
C7 a
Preservatives= (U)npreserved, H{cl€,
T b
Sample IQ
'
C5 T
ci D
H2(S)o4. H(Nd 03. (Nio)ThiO5urfate, Na(0)H.
ID
[J
0
T
m
Other (), Indicate
J
FC pF
Relin uiled:
ceived:
atelTime
1/2,ou 2:00 FM
Rush wofk }Trill require prror approval. Additional charges will apply

City of Sanford
Big Buffalo WWTP
Sludge Calculations
IN
VSR = 68.85148
W1
DISH
111.4027
W2
WET
211.4223
W3
DRY
111.8766
W4
ASH
111.5252
0.473807
PERCENT VOLITILE SOLIDS
0.741507
OUT
W1
DISH
112.1654
W2
WET
212.1412
W3
DRY
120.7063
W4
ASH
116.6760
PERCENT SOLIDS
8.542967
PERCENT VOLITILE SOLIDS
0.471882
PERCENT VOLITILE SOLIDS REDUCTION 68.85148
Is it above 38%

VSR
Grab Date: 4 2D 2�
Lab Tech's Initials:
RAS (IN) DIGESTER
Sample OUT
Volume 100 MIS.
Dish #1 A
Crucible Weight
Crucible & Liquid
Dried
Burned
ltl.'�n2'l
211. L4
ttt, �Y766
S2 �2
gm
gm
gm
gm
100 MIS.
D
Z!2- ►'�!2
! 20. 7o63
1! t'or 6 7 &o
3m
gm
gm
gm
Date/Time In: (0-202n/ q ,0 f
Drying Oven
Date/Time Out: 4-1-tozv/ 9 :D S- Temp: I04-1 °C
Time In: !y ; 0'9 ""*-
Muffle Furnace
Time Out: 1 i : o 'j 41 Temp: SSO °C
Were the samples well mixed before analyzing? Yes No
Was the temp of the drying oven in the proper operating range? Yes ✓ No
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes ✓ No
If not what were the corrective actions?
Samplers I L

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 07/01/20 To 09/30/20
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to alternative nerformed (Clnaa A nr rincc Rl eamnlete the fnllnwino mnnitarina dntn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61
CFU
<29000
<29300
<29500
CFU/g
0
Quarterly
Grab
SM9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (type or print)
Signature of Preparer* We
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc, Laboratory Report
NC DENRk&
NC PH HST r»
USE PA 9INC01me
Client:
Synagr CTS PrO.
200 059
Dw Ca „a77@
Project:
Sanford WWTP Regulatory
Yes
Sample Information
Sampled
C. Wynne
a m 07108J20 RuceNud
]
Cameron Dift
07108120
Analyses and Result
Lab
ampi IDƒ
? ? A ■!ate Wi n!
]
i /
f
i :
kd- Mothk,
2J@
xJ
Reference
<
2007-059
-01
-W_ , Fec c6U�a <29000
CPULV
ZWW
071DWO RL
g DMF
-
-02
<29100
cRxw
2,0o
-03
<29200
cFft
29M
-04
<29500
cFm
2e00
-05
429200
_N
»m,
-06
<29500
9m
&!k
-7
Q9500
@m
2500
Goorrva, <29300
-
-01
k r ! 345%
■-
07MWO RL
25400.TS
32
i %
0.01
_D3
343%
001
-04
3.39%
001
-05
3.42%
0r
-06
3.38%
cot
-7
3.68%
0-01
Repo 4Md
�
Lab Director
Date
95skxkc
SOMAn & NC 27 p
919.2(1154M
rhnAx mcru awl am

219 S- st"16 Str
Sanford. NC 27330
nkn - ell r r1Il_AIAA
Cameron Testing Services, Inc
NC 4 r.,VJ Cert #654 NC P H H S Gait # 37799 US EPA NG01918
Chain of Custody
Page of
' ^ = j 11 tD
Ertwil
` , , synagro am
CT lab use only
pIKM
Vf, 'I r9 fis 2-7
Sample Temp
el,y/�/� Lab ID
Address Pty, 284 Boger -Rd.
Fax:
Ice (YN)
SWA'zlP) Mocksvllle, ING 8
now:
Permit(YAY)
�}70
Project. Ort'"S I�*� I
R*sh(YtH)
DM.
camp in
Number of battles
Requested Analysis
C7 a
�
P[eservabves iU]npahserwed H(GY,
C� Lab
ID
Sample ID
6
� �
�
H2(S}04. H(NP3, tNa)Thiosulfate, Na(0)H,
r
Other (Y), Indicate
7 y
Rellrl i15f1 CI;
T4fr+�
Received:
Daterrime
i
Rush work will require prior approval Additional charges will apply

City of Sanford
Big Buffalo WWTP
Sludge Calculations
K
VSR = 53.51587
W1
DISH
1114033
W2
WET
2115184
W3
DRY
1117609
W4
ASH
1115009
0.357189
PERCENT VOLITILE SOLIDS 0.727069
OUT
W1
DISH
112.1667
W2
WET
2121518
W3
DRY
1175599
W4
ASH
1145762
PERCENT SOLIDS 5.394004
PERCENT VOLITILE SOLIDS 0.553234
PERCENT VOLITILE SOLIDS REDUCTION 63.61587
Is it above 38% �x a

V SR
Grab Date:
Lab Tech's Initials:
DIGESTER
Sample RAS (IN)
OUT
Volume 100 MIS.
100 MIS
Dish #1
1 D
Crucible Weight
Crucible & Liquid
Dried
Burned
N(233
211• �l�`i
I I I _7609
111, Soo9
gm
gm
gm
3m
Ji2.1 66�
212.1 S1�
11 7. TS9c)
11K_ 5762.
am
gm
3m
gm
Date/Time In: 7-74c*{ ! o t 3 7 Drying Oven
Date/Time Out. 7 L lczd ►p; 3 7 Temp /pdy. rC
Time In 12 = 2 Muffle Furnace
Time Out' j ; p 1- Temp' 3� V °C
Were the samples well mixed before analyzing? Yes No
Was the temp of the drying oven in the proper operating range? Yes V No
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes,/ No
If not what were the corrective actions?
Samplers D ,

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford
WWTP Name: Bia Buffalo WWTP
WQ Permit Number: WQ0000543
NPDES Number: NCO024147
Monitoring Period: From 10/01/20 To 12/31/20
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicable to alternative nerformed (Class A or Class Bl complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
CFU
<9680
<19300
<25000
CFU/g
0
Quarterly
Grab
SM9222D
Coliforin
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (type or print)
4u A- �j a n at
Signature of Preparer* ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
Client: Synagro CTS Proj.
Project: Sanford WWTP Regulatory
Sample Information
Sampled C. VWnne Date 1010112.0 Recelred
E
Analyses and Results
010-00
Yes
NC C E N R #654
NC PHHS #37(99
US EPA #NC01918
DW Cart 4 37799
M. Sims Date 10/011 0
Lab ID Sam le ID
p
x a _0
E 2
A nalyte
Result
c
a _
m
`—°
:: +:
�7
Std. Methods
+
cC
a
Reference
2 70-003 -.
iIt> qE Ge
rec. Colifarm, S
<22 00
cFwo
22200
1MI)20 RI
922,K - w.r
<211710r0
uwj
21700
-3
{ JVOV
CFueg
25000
�23000
CFurg
23000
F
< 19200
CFUN
19200
<9680
CF ig
9680
-7
<19100
Grwa
19100
Geoman
<19300
2010-003 -'I
TS (%)
4.51`Io
00,
10.101120 RL
2�40 G JS
-2
4_61%
0.01
-3
4.00%
0 0'
-4
4. 34 %
0.01
-5
5. 1 %
o.oi
-6
10.10%
o.01
-7
5.17%
0.01
Report
RevWw
Lab Nrector
219 S. Stmlc Slr. 919-208A24U
Sonford NC 27330 chriS came:rimtesling coin

�!19 S Steele Str.
Sanford PIC 27330
Phone [phone]
Cameron Testing Services, in
NC 4NW'GtiV Cen 9654 NC PHKS Cer# 5 37799 US EPA NCO1918
Chain of Custody
Pace _ of
Cam;ssny: Synagro
Erneli;
( � .K
CTS lab use only
Contact: , 1ij)d I - G � r, s W rt n
Winne-
Phone:
�: 7
Sample Temp r, Lab 1d
fC1
' �.
Address jCft. 284 Bogef Rd.
Fait;
3 So eiV-1 kld 7
Ice MN)
stale,zl- .Mocksviile, 70 8
FING t
f�ropec S 6 "U [y IN f
Rusn (YIN) 11ue
Cone bee: Nam. (%-
.;s SipPle`h1'°"
Sample Information
Number of bottles
Requested Ana"is
x
Z
a a _
I
Preserv�llvo6 (Ujnpre&erwd, H(C)E.
CTS Lab
I0
Sa mple l
m _ -
t ;. c
�I (S)04. H(Ny 03, (Na)Thiasultate, Na(0)H.
� j
'
m
OINer ( ), Ind.Katio
SL4 V7T;�oa1 a�,1-1
+t►rq
�{ �i ��- v
-7
of
045Ayy
L/
04,
C�
IRelin uished:
Received:
DaltmMine
++
F� GIS 1i n+tL to I12 020
Rush work will requ Pre prior approval. Additional charges will apply

VSR
Grab Date - 2,010
Lab Tech's Initials
RAS (IN) DIGESTER
Sample OUT
Volume 100 MIS 100 MIS
Dish #1 a 1 0
Crucible Weight
Crucible & Liquid
Dried
Burned
gm
3m
3m
3m
I t 1L. 16 ei
21Z -n,7Z
lZI1-7IS6
iIY,3o1,9
gm
gm
gm
am
Date/Time In ly y,Y'Zv / l l -, I j ,--
Drying Oven
Date/Time Out 1,a / (1- 1, 5 cr-- Temp 10 W °C
Time In 1 Z . Z ( Muffle Furnace
Time Out j : D cf Temp TY-0 °C
Is the Balance Level No
Were the samples well mixed before analyzing? Yes V"No
Was the temp of the drying oven in the proper operating range? Yes �No
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes V No
If not what were the corrective actions?
Samplers 1 C I S V

ta1o81a6
City of Sanford
Big Buffalo WWTP
Sludge Calculations
TiT
i
W1
DISH
1114021
W2
WET
2110532
W3
DRY
1118069
W4
ASH
1115291
0406217
PERCENT VOLITILE SOLIDS 0686265
O
W1
DISH
1121689
W2
WET
2121272
W3
DRY
1217156
W4
ASH
1183099
PERCENT SOLIDS 9 550683
PERCENT VOLITILE SOLIDS 0356741
PERCENT VOLITILE SOLIDS REDUCTION 7464645
`'
Is it above 38% les
7464645
0

SECTION 6

Agricultural Lime Application Log
Year: 2020
Project: Sanford WWTP
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-CH-77-4
6.2
0.0
0.0
NC-CH-77-5
6.7
0.0
0.0
NC-CH-77-7
6.3
0.0
0.0
NC-CH-77-8
6.6
0.0
0.0
NC-CH-77-11
6.2
0.0
0.0
NC-CH-77-13
6.1
0.0
0.0
NC-CH-77-14
6.2
0.0
0.0
NC-CH-77-15
6.3
0.0
0.0
NC-CH-77-16
6.2
0.0
0.0
NC-CH-66-1
5.3
1.3
0.0
NC-CH-66-2
6.1
0.0
0.0
NC-CH-66-3
5.4
1.1
0.0
NC-CH-66-4
5.8
0.5
0.0
NC-CH-66-6
5.9
0.3
0.0
*Permit does not require lime application

SECTION 7

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002596
Client:
Henry (Jr) Stinson
Advisor:
Chris Wynne
vo-
Predictive
904 Delphus Stinson Rd.
483 Bogar Road
Goldston, NC 27252
Mocksville, NC 27028
==�
Mehlich-3 Extraction
Soil Report
Sampled County: Chatham
Links to Helpful Information
Client ID: 130941
Advisor
ID: 509090
Sampled: 07/09/2020 Received: 08/19/2020 Completed: 08/26/2020
Farm: ch-66
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E 2.2
50-70 0
0
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
10
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.51 0.95
9.6 75 2.4 5.3 491 74
51 20
77
251
160 168
717
717
707
0.2 2
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E 1.1
50-70 0
30
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
70
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.60 0.98
9.7 86 1.4 6.1 205 34
68 16
53
1058 644 651
309
309
367
0.1 1
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E 1.9
50-70 0
0
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.76 0.92
8.5 75 2.1 5.4 244 93
53 16
65
621
382 390
637
637
531
0.1 1
North Carolina
r
Tobww Trust FwW C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY21-SL002596
Henry (Jr) Stinson
Page 2 of 3
Sample ID: 4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E 1.6
50-70 0
0
0
0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0
0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.46 1.02 9.7
82 1.8 5.8 335 79
56 21
65
661
406
414
616
616
608
0.1
1
Sample ID: 6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E 1.7
50-70 0
30
0
0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
70
0
0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.46 0.98 13.2
85 2.0 5.9 385 34
64 19
65
821
502
510
1072
1072
1027
0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002596
Henry (Jr) Stinson
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL011228
�5{i �141..tiL
Client: Paul Price
Advisor: Chris Wynne
Predictive
645 J. Cook Rd
Synagro LLC
;•
Goldston, NC 27252
284 Boger Road
+_ Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Chatham
Links to Helpful Information
Client ID: 435848
Advisor ID: 509090
Sampled: 10/27/2020 Received: 10/29/2020 Completed: 11/13/2020 Farm: ch-77
Sample ID: 4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.56 1.05 10.2 90 1.0 6.2 101 102 60 25
93 1107 678 410 410
394 0.1 1
Noah Carolina
i�
Futaw frum Fund Ciwn1nl55km
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL011228
Paul Price
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031965
Client: Paul Price
Advisor:
Chris Wynne
vo-
Predictive
645 J. Cook Rd
483 Bogar Road
Goldston, NC 27252
Mocksville, NC 27028
==�
Mehlich-3 Extraction
Soil Report
Sampled County: Chatham
Links to Helpful Information
Client ID: 435848
Advisor
ID: 509090
Sampled: 05/14/2020 Received: 06/09/2020 Completed: 06/16/2020 Farm: CH-77
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage 0.0 180-220 0
30 0 0
pH$
0
0
0
Note: 3 Note:
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.36 1.07
9.5 93 0.6 6.7 210 92 71 18
66
1556 940
441
441
682
0.2 2
Sample ID: 7
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage 0.0 180-220 0
50 0 0
0
0
0
0
Note: 3
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.41 1.06
9.3 90 1.0 6.3 170 76 70 16
44
1715 1041
385
385
588
0.1 1
Sample ID: 8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage 0.0 180-220 0
30 0 0
pH$
0
0
0
Note: 3 Note:
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.32 1.03
11.3 93 0.8 6.6 187 90 68 21
68
1284 778
441
441
524
0.2 2
North Carolina
r
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031965
Paul Price
Page 2 of 3
Sample ID: 16
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Corn, silage
0.0
180-220 0
20
0
0
0 0
0 0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS -I NO3-N
0.36 1.04 10.5
88 1.2 6.2
221 107
60 23 74
919
565
744 744
641 0.2 2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SLO31965
Paul Price
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm

Page 1 of 1
Report No: 20-364-0526
Account No: 46789
Advisor: Synagro Central LLC/ Dunn
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint'(D
ANALYTICAL
Client: Paul Price
645 J Cook Rd
Goldston NC 27252
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: CH-77
Date Received: 12/29/2020
Date of Report: 12/30/2020
Lab No Field ID Sample ID
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
09090 11
MIN 6.2
0.8
59
35
29
675
419 419 235 235 150 6.7 88 59 26 1.0 0.1
Crop Recommendations:
Rec Uom Lime (Vacre)
N
P205
K20
S
Mn
Zn Cu B Mg Last Crop
1- Lawn
Ib/1000 sf 0.0
4.0
0
3.0
0.48
0
0 0 0 0
2-Adjust pH to 6.0
lb/acre 0.0
0
0
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 20-330-0576
Account No: 46431
Advisor: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Waypoint'(D
ANALYTICAL
Client: Paul Price
645 J Cook Rd
Goldston NC 27252
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: CH-77
Date Received: 11/25/2020
Date of Report: 11 /30/2020
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
CEC BS%
Ca%
Mg%
ESP
Na
I18056
13
MIN
6.1
1.2
63
94
29
1106
679
679
238
238
315
8.6 86
63
17
1.1
0.1
Crop Recommendations:
Rec Uom
Lime (Vacre)
N
P205
K20
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Fescue Hay
lb/acre
0.0
150
10
0
20
0
0
0
0
0
2-Adjust pH to 6.0
lb/acre
0.0
0
0
18057
14
MIN
6.2
1.1
51
98
27
1050
644
644
293
293
270
9.1 87
63
18
1.5
0.1
Crop Recommendations:
Rec Uom
Lime (Vacre)
N
P205
K20
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Fescue Hay
lb/acre
0.0
150
23
0
20
0
0
0
0
0
2-Adjust pH to 6.0
lb/acre
0.0
0
0
18059
15
MIN
6.3
0.9
63
65
25
506
316
316
335
335
300
8.6 89
69
16
1.0
0.1
Crop Recommendations:
Rec Uom
Lime (Vacre)
N
P205
K20
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Fescue Hay
lb/acre
0.0
150
10
20
20
0
0
0
0
0
2-Adjust pH to 6.0
lb/acre
0.0
0
0
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.