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HomeMy WebLinkAboutWQ0018352_Residual Annual Report 2020_20210223Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* W00018352 Applicant/Permittee Town of Boiling Springs Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Mooresville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * Michael F. Gibert Email Address* mike.gibert@boilingspringsnc.net electronic subntttal, confirmation of receipt, and other correspondence. Project Information ........ ......... ................................................................................................................... . Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 17044342357 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00018352 Fbs Current Existing perrrit number Applicant/Permittee Address* PO Box 1014 Boiling Springs NC 28017 Facility Name * Town of Boiling Springs RLAP Please provide comments/notes on your current submittal below. 2020 Annual LA Residuals Report for the Town of Boiling Springs The Permittee/Town Manager (Lucas Shires) is no longer employed by the Town. I am signing this report with Signatory Authority. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) 2020 Annual LA Residuals Report.pdf 5.97MB Upload only 1 RCFdocurrent (less than 250 M3). ivL@iple documents nest be corrbined into one RDFfile unless file is larger than upload lirrit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature` rra�W1q' 4*x0te- Submission Date 2/23/2021 THE TOWN OF BOILING SPRINGS NORTH CAROLINA Date: 2/22/2021 To: The Information Processing Unit NCDWR Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2020 Annual Land Application of Residuals Town of Boiling Springs I NC Permit # WQ0018352 To Whom it May Concern: Please find enclosed the original report and all applicable forms and test results for the Annual Residuals Land Application Report for the Town of Boiling Springs. An electronic copy of the 2020 Annual Land Application Report has also been submitted. Aerobic digested residuals continue to be land applied to permitted fields for the beneficial reuse as a soil conditioner and fertilizer supplement. I will be signing this Annual Report with Signatory Authority. Please let me know if additional information is needed at 704-434-2357. Sincerely, Mike Gibert Public Works Director Town of Boiling Springs Enclosures: Annual Land Application Report 2020 114 East College Avenue I PO Box 1014 1 28017 1 704 434 2357 1 www.boilingspringsnc.net ANNUAL LAND APPLICATION OF RESIDUALS 2020 ANNUAL REPORT TOWN OF BOILING SPRINGS Permit No. WQ0018352 THE TOWN OF BOILING SPRINGS -NC]RTH r;. CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit*: WQ0018352 County: Cleveland Year: 2020 Facility Name (as shown on permit): Town of Boiling Springs Land Application Operator: Todd Humphries Phone: 704-300-8641 Land application of residuals as allowed by the permit occurred during the past calendar year? r❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summarv: Total number of application fields in thepermit] 3 Total number of fields utilized for land application during the yearl 1 Total amount of dry tons applied during the year for all application sites: 6.7 Total number of acres utilizes for land application during the year: 9.84 Part B - Annual Com iance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the pen -nit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. " Mike Gibert / Public Works Director Permittee Name and Title (type or print) Signature otPreparer* Signature of 2- Date Signature of Land Applier Date Z_zv-Zv z/ Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 5039 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RESIDUALS SAMPLING FORMS ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ00183.52 Laboratory: 1) Facility Name: Town of Boiling Springs 2) Residual Source WQ # or NCO071943 3) NPDES #: 4) WWTP Name: Town of Boiling Springs WWTP 5) Residual Analvsis Data Pace Analytical Parameter (mg/kg) Conc. Limit (mg/kg)' Sample or Composite Date 8/25/20 2111/20 Percent Solids W NA 1.2 Arsenic 75 49.6 Cadmium 85 5 Copper 4,300 275 Chromium NA 0 Lead 840 27.7 24.3 Mercury 57 2.2 Molybdenum 75 24.8 Nickel 420 24.8 Selenium 100 49.6 Zinc 7,500 712 Total Phosphorus NA 15500 TKN NA 31200 Ammonia -Nitrogen NA 753 Nitrate and Nitrite NA 5890 ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0018352 Laboratory: 1) Pace Analytical Services Facility Name: Town of Boiling Springs 2) Residual Source NCO071943 3) NPDES # or WQ#: 4) WWTP Name: Town of Boiling Springs WWTP 5) Residual Analysis Data Parameter Sample or • p• Date MMM - Magnesium ' 1 1 ----_------ Potassium M.-I Percent Mositure Reactive Cyanide----__-_--- Reactfive Sulfide 1 -_--_------ Flashpointdeg F1 1 ----------- -----------= ----------- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date DENR FORM RSSF - B (1212006) METALS FIELD LOADING SUMMARY LAND APPLICATION FIELD SUMMARY ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Boiling Springs Land Owner: James Petty Operator: Todd Humphries Crop 1 Name: Easture WQ Permit #: WQ0018352 Field #: I Acres Utillzed: 9.84 Annual Dry Tons Applied: 6.7054 Site #: 3PI Acres Permitted: 22.41 Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 220 Crop 2 Name: Crop 2 Max. PAN: ` y c 0 0 La Volume applied (enter one) Solids/ Liquid 9 Cu. Yds Gallons 3'o Solids Volume Applied r pp per Acre (Dry TonslAc) Residual Sources (NPDF,S #, WQ#, Fert., Animal Waste, etc) Soil mod' (Dry' Moist) Precip. Past 24 Hrs. inches a ]v' * _X fD w °a w " * a' * TKN mg*g Z > o 3 �'�• mglkg Nitrate and Nitrite mglkg PAN Applied (Ibslacrel Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop i Crap 2 6122/20 20000 1.2 0.102 NCO071943 dry 0 S 0.5 0.3 1 31200 753 1 5890 3.133 NA pasture 6/23/20 12000 1.2 0.061 NCO071943 dry 0.05 S 0.5 0.3 31200 753 5890 1.880 NA pasture 6124/20 20000 1.2 0.102 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 3.133 NA pasture 6/25/20 10000 1.2 0.051 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 1566 NA pasture 10/6120 14000 1.2 0.071 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 2.193 NA pasture i0n20 14000 1.2 0.071 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 2.193 NA pasture 1018/20 24000 1.2 0.122 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 3.759 NA pasture I D/9120 20000 1.2 0.102 NCO071943 dry 0 S 0.5 0.3 31200 753 5890 3.133 N A pasture 0.000 0.000 0.000 0.000 1 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF suph to thi,, hn-m : TOTALS: 0 t3aooa As Cd Cu Cr Pb I Ig Mo Ni Se Zn p 20.989 0.000 Lime Applied Annuallbslacre 0.061 0.006 0.336 0.000 0.034 0.003 0.030 0:030 0.061 0.870 18,941 1,486 0.10.1 3. 711 0.277 0.485 0.012 0.511 0.526 1.043 10.998 I.547 0.109 4.047 0.277 0.519 0.015 0,551 0.556 1.104 11.868 36 1 34 1 1338 1 n/a 1 267 1 15 nia 1 .174 89 1 2498 1 220 Date lbs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including thy, possibility of fines and imprisonment for knowing violations." Z- zz-Z,-Z/ Signature of Land Applier Date *Application Method: S - Surface. IN - Injection, INC - Incorporation **Volatiliw,ation Rate: Surface - 0.3. Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1. anaerobially digested -0.2. aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF i 1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual): Permit #: WQ0018352 Cation Exchange Capacity (non 503 only): 6,196 Operator: Todd Humphries Owner: James PettX Predominant Soil Series: Pacolet-Bethleher Acres Used: 9.84 Acres Permitted: 22.41 Site #: 1 Field #: JP1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 8125/20 2 8/25/20 3 8/25/20 4 8/25/20 5 8/25/20 fi 8125/20 7' 8/25/20 8 8/25120 9 10 11 12 % Solids 1.2 1.2 1 1.2 1 1.2 1.2 1.2 1.2 1 1.2 Arsenic 49.6 49.6 49.6 49.6 49.6 49.6 49.6 49.6 Cadmium 5 5 5 5 5 5 5 5 Copper 275 275 275 275 275 275 275 275 Chromium Lead 27.7 27.7 27.7 27.7 27.7 27.7 27.7 1 27.7 Mercury 2.2 2.2 2.2 2.2 T2 2.2 2.2 2.2 Molyb- denum 24.8 24.8 24.8 24.8 24.8 24.8 24.8 24.8 Nickel 24.8 24.8 ?4.8 24.8 24.8 24.8 24.8 24.8 Selenium 49.6 49.6 49.6 49.6 49.6 49.6 49.6 49.6 Zinc 712 712 712 712 712 712 712 712 Total Phos- horus 15500 15500 15500 15500 15500 15500 15500 15500 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7, 8 9 10 11 12 DT/Ac./ App. v Event 0.10 0.06 0.10 0.05 0.07 0.12 0.10 Arsenic 0.010 1 0.006 0.010 0.005 0.007 0.012 1 0.010 0,000 0.000 1 0.000 0.000 0.000 1 0.061 Cadmium 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.000 0,000 0.000 0.000 0.000 0.006 Copper 0.056 0,034 0,056 0.028 0.039 0.067 0.056 0.000 0,000 0.000 0.000 0.000 0.336 Chromium 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 Lead 0.006 0.003 0,006 0.003 0.004 0.007 0.006 0.000 0.000 0.000 0.000 0,000 0.034 Mercury 0.000 0.000 0.000 0.000 0.000 0,001 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.005 0.003 0.005 0.003 0,004 0.006 0.005 0.000 0.000 0.000 0.000 0.000 0.030 denum Nickel 0.005 0.003 0.00.5 0.003 0.004 0.006 0.005 0.000 0.000 0.000 0.000 0.000 0.030 Selenium 0.010 0A06 0.010 0.005 0,007 0.012 0.010 0.000 0.000 0.000 0.000 0.000 0.061 Zinc 0.145 0.087 0.14.5 0,073 0.101 0.174 0.145 0,000 0.000 1 0.000 0.000 0.000 0.870 Total Phos- 3.162 1.891 3.162 1.581 2.201 3.782 3.162 0.000 0.000 0.000 0.000 0,000 18.941 horus "I certify. under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Z-ZZ- 7oz( Date DENR FORM MFLSF (12/2006) RESIDUALS ANALYSIS LAB SHEETS aceAnalytical www P44:010sx0m ANALYTICAL RESULTS Project: Digester Sludge Samples Pace Project No 92492276 Pace Analytical Services, LLC 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (7041875-9092 Sample: Digester Sludge Lab ID: 92492276001 Collected. 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A Leachate Method/Date: 1311, 09/01/20 09:03 Initial pH: 7.68, Final pH: 4.92 Pace National - Mt. Juliet 2,4-5-TP (Silvex) ND mg/L 0.00200 1 09/02/20 08:24 09/02/20 18:20 93-72-1 2,4-D ND mglL 0.00200 1 09/02/20 08:24 09/02/20 18:20 94-75-7 Surrogates 2,4-DCAA (S) 58.8 % 14.0-158 1 09/02/20 08:24 09/02/20 18:20 19719-28-9 8081 TCLP Pesticides RVE Analytical Method: EPA 80818 Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311: 08/27/20 13:05 Initial pH: ; Final pH: 5 Pace Analytical Services - Charlotte gamma-BHC (Lindane) ND mg1L 000050 1 09/02/20 22:23 09/03120 16:09 58-89-9 Chlordane (Technical) ND mg1L 0.0030 1 09/02/20 22:23 09/03/20 16:09 57-74-9 Endrin ND mg1L 0.00050 1 09/02/20 22 23 09f03120 16:09 72-20-8 Heptachlor N❑ mg1L 0A0050 1 09/02120 2223 09/03/20 16 09 76-44-8 Heptachlor epoxide ND mglL 0.00050 1 09102/20 22:23 09/03/20 18:09 1024-57-3 Methoxychlor ND mglL 1.0 1 09/02/20 22:23 09/03/20 16:09 72-43-5 Toxaphene ND mg1L 0.0030 1 09102/2022:23 0910312016:09 8001-35-2 Surrogates Decachlorobiphenyl (S) 157 % 10-154 1 09102120 22:23 09/03/20 16:09 2051-24-3 S3 Tetrachloro-m-xylene (S) 103 % 10-184 1 09/02/20 22:23 09/03/20 16:09 877-09-8 Metals (ICP) 6010D Analytical Method: EPA 6010D Preparation Method: 3015 Pace National - Mt Juliet Calcium 651000 ugiL 1000 1 09/02/2010:42 09102/2012:32 7440-70-2 Magnesium 42400 ug1L 1000 1 09/02/2010:42 09/0212012:32 7439-95-4 Sodium 41900 uglL 3000 1 0910212010:42 09/0212012:32 7440-23-5 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Pace Analytical Services - Asheville Aluminum 18900 mglkg 496 1 08/3012015:31 08131/2012:13 7429-90-5 Arsenic ND mglkg 496 1 08/30120 15:31 08/31120 12:13 7440.38-2 Cadmium ND mglkg 5 0 1 08130/20 15:31 08131/20 12:13 7440-43-9 Calcium 51100 mglkg 496 1 08/3012015:31 08/311201213 7440-70-2 Copper 275 mglkg 24 8 1 08/30/20 15:31 08131/20 12:13 7440.50-8 Lead 27.7 mg/kg 24.8 1 08/30/20 15 31 08/31/20 12A3 7439-92-1 Magnesium 4070 mglkg 496 1 0813012015:31 0813112012:13 7439-95-4 Molybdenum ND mglkg 24-8 1 08130/2C 15:31 08/31/20 12 13 7439-98-7 Nickel ND mglkg 24.8 1 08130/2015:31 08131/20 12: 13 7440-02-0 Potassium ND mglkg 24800 1 0813012015:31 08/31/2012:13 7440.09-7 Selenium ND mg/kg 49.6 1 08/30/2015:31 08131/20 12:13 7782-49-2 Sodium ND mglkg 24800 1 08130/2015:31 0813112012:13 7440-23-5 Zinc 712 mglkg 49.6 1 08130/2015:31 0813112012:13 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 09/0412020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 35 aceAnalytrca( i www.panlaEs.com ANALYTICAL RESULTS Project: Digester Sludge Samples Pace Project No. 92492276 Pace Analytical Services, LLC 9800 Kincey Ave Suite l00 Hul NC 28078 (704)875-9092 Sample: Digester Sludge Lab lD: 92492276001 Collected: 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6010 MET ICR TCLP Analytical Method EPA6010D Preparation Method EPA3010A Leachate Method/Date: EPA 1311:08I30120 13 34 Initial pH:: Final pH: 2 Pace Analytical Services - Asheville Arsenic 0.12 mglL 0.050 1 09101/2002:07 09101/2010:36 7440-38-2 Barium ND mglL 0.25 1 09/01/2002:07 091011201036 7440-39-3 Cadmium NO mg/L 0 0050 1 09/01/20 02:07 09/01/20 10:36 7440.43-9 Chromium NO mglL 0 050 1 09/01/23 02:07 09/01/20 10 36 7440-47-3 Lead NO mglL 0 025 1 09/01/20 02:07 09/01/20 1036 7439-92-1 Selenium NO mglL 0.10 1 09101/2002:07 09101/2010.36 7762.49.2 Silver ND l 0.025 1 09/01/20 02:07 09101/20 10,36 7440.22-4 7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA7470A Leachate Method/Date: EPA 1311: 08/30/20 13:34 Initial pH Final pH: 2 Pace Analytical Services - Asheville Mercury NO mglL 0-00020 1 0910112011:14 09102/2014:53 7439-97-6 7471 Mercury Mercury 8270E TCLP RVE 1.4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methylphenol(l Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol 2.4.6-Trichlorophenol Surrogates Nitrobenzene-tl5 (S) 2-Fluorobiphenyl (S) Terpher l-d14 (S) Phenol-d6 (S) 2-Fluoraphenol (S) 2.4,6-Tribromophenol (S) 8260D MSV TCLP Benzene Analytical Method: EPA 7471 B Preparation Method. EPA 7471 B Pace Analytical Services - Asheville 2.2 mglkg 0.15 1 08/2812013:10 08/28/2015:09 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311. 08/27120 13:05 Initial pH:. Final pH: 5 Pace Analytical Services - Charlotte NO mglL 0.050 1 09/02120 20:42 09/03/20 10:24 106-46-7 ND mg1L 0.050 1 09/02/20 20:42 09/03/20 10:24 121-14-2 NO mglL 0.050 1 09/02120 20:42 09/03/20 10:24 87-68-3 NO mglL 0.050 1 09)02120 20A2 09/03/20 10 24 118-74-1 NO mg1L 0.050 1 09/02/20 20:42 09/03/20 10:24 67-72-1 NO mglL 0.050 1 09/02120 20 42 09/03/20 10:24 95-48-7 ND mg1L 0.050 1 09/02120 20:42 09/03120 10:24 15831-10-4 NO l 0.050 1 09/02120 20A2 D9103120 10:24 98-95-3 NO mg1L 0.10 1 09/02/20 20:42 09/03/20 10:24 87-86-5 NO mg1L 0.050 1 09/02/20 20A2 09/03120 10:24 110-86-1 NO mg1L 0.050 1 D9102120 20:A2 09/03120 10:24 95-95-4 ND ril lL 0.050 1 09/02/20 20:42 09/03/20 10:24 88-06-2 91 % 13-130 1 09/02120 20A2 09/03/20 10:24 4165-50-0 86 % 13-130 1 09/02/20 20:42 09/03120 10:24 321-60-8 125 % 25.130 1 09/02/20 20:42 09/03/20 1024 1718-51-0 51 % 10-130 1 09/02/20 20:42 09/03/20 10:24 13127-88-3 63 % 10-130 1 09/02120 20 42 09/03/20 10:24 367-12-4 93 % 10-137 1 09/02/20 20:42 09/03/20 10:24 118-79-6 Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311. 08/2812D 10:57 Pace Analytical Services - Charlotte ND mglL 0.10 20 08/30/20 2132 71-43-2 REPORT OF LABORATORY ANALYSIS BC Thts reperl shall not be reproduced. except in Full. Date: 09/0412020 03:59 PM without the written consent of Pace Analytical Services. LLC Page 6 of 35 aceAnalytical www.pacehbs.com ANALYTICAL RESULTS Project: Digester Sludge Samples Pace Project No 92492276 Pace Analytical Services, LLC 9800 Kincey Ave- Suite 100 Funtersville, NC 28078 (704)875-9092 Sample: Digester Sludge Lab ID: 92492276001 Collected: 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Dmit DF Prepared Analyzed CAS No. Qual 8260D MSV TCLP 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1.4-Dichlorobenzene 1,2-Dichloroethane 1.1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture Calculated Results Sodium Adsorption Ratio 1010 Flash poiri losed Cup Flashpoint 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen 350.1 Ammonia Nitrogen, Ammonia Date: 09/04/2020 03:59 PM Analytical Method: EPA 8260D Leachate Method/Date : EPA 1311: 08/28/20 10-57 Pace Analytical Services - Charlotte ND mglL 0.20 20 08/30/20 21:32 78-93-3 ND mglL 0.10 20 08/30/20 21:32 56-23-5 ND mglL 0,10 20 08/30/20 21732 108-90-7 ND mg1L 0.10 20 08/30/20 21:32 67-66-3 ND mg/L 0.10 20 08/30/20 21:32 106-46.7 ND mglt 0.10 20 08/30/20 21:32 107-06-2 ND mg/L 0.10 20 08/30/20 21:32 75-35-4 ND mg/L 0-10 20 08/30/20 21:32 127-18.4 ND mglL 0.10 20 08/30/20 21:32 79-01-6 ND mg1L 0.10 20 08/30/20 21:32 75-01-4 104 % 70-130 20 105 % 67-135 20 101 % 70-130 20 Analytical Method: SM 254OG-2011 Pace Analytical Services - Charlotte 1.2 % 0-10 1 Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte 98.8 % 0.10 1 Analytical Method: Calculated Preparation Method: Cali Pace National - Mt. Juliet 0.429 1 Analytical Method: EPA 1010A Pace Analytical Services -Asheville 08/30/20 21:32 17060-07-0 08/30/20 21:32 2037-26-5 08/30/20 21:32 460-00.4 08/26/20 18:02 08/26120 17:46 0910212012:32 09/0212012:32 SAR >200 deg F 70.0 1 09/02/20 16:03 Analytical Method: EPA 9045D Pace Analytical Services -Asheville 8.5 Sid, Units 0-10 1 08/31/20 14:54 Q Analytical Method: SM 271OB-2011 Pace Analytical Services -Asheville 15200 mg/kg 0.12 1 09103/2015:52 N2 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Pace Analytical Services - Asheville ND mg/kg 753 1 08/3012013:07 08131/2010:17 7664-41-7 REPORT OF LABORATORY ANALYSIS This report shall not oe reproduced, except in full, without the written consent of Pace Analytical Services, L _G. Page 7 of 35 ) 7 'i aceAnalytrcal www.pacelabs.com ANALYTICAL RESULTS Project: Digester Sludge Samples Pace Project No.: 92492276 Pace Analytical Services, LLC 9800 Kineey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Digester Sludge Lab ID: 92492276001 Colllected 08/25/20 08:00 Received 08/25/20 09 10 Matrix Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method. EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen Kjeldahl, Total 31200 mglkg 3540 1 08/28/20 22:19 08/29/20 06:16 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method- EPA 353-2 Rev 2.0 1993 Preparation Method. EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 5890 mglkg 1590 5 08/25/20 21:37 08/25/20 23:43 Nitrogen, Nitrate 5890 mglkg 1590 5 08/25/20 21:37 08/25/20 23:43 14797-55-8 Nitrogen, Nitrite ND mglkg 318 1 08/25/20 21:37 08/25/20 22:50 14797-65-0 365.1 Phosphorus, Total Analytical Method EPA 365 1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 15500 mg/kg 370 5 08/31/20 20:14 09/01/20 18:28 7723-14-0 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method SW-846 7 3.3.2 Pace Analytical Services - Greensburg Cyanide. Reactive ND mglkg 81.0 1 08/27120 16.51 08/27/20 20:23 734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2 Pace Analytical Services - Greensburg Sulfide, Reactive ND mglkg 810 1 08/27/20 16:51 08127i20 17:07 Dale 09/04/2020 03 59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. i(MI) J(M1) Page 8 of 35 CHAIN -OF -CUSTODY Analytical Request Document LAB USE WO # : 92492276 umber or to �CeAnalytical I I o Chain -of -Custody is a LEGAL, DOCUMENT - Complete ail relevem fields Coenparty: Town of i3ollin9 Springs Billing information: f 1 ! 92492276 ar kWr6W.' PD BOX 1024 Boiling Springs NC 28017 PO Box 1014 Boiling Springs NC 2801713 Container Preservative Type** Lab Pra]ett Manager: Report To: Mike filbert Email To: mike. gibertpboilingspringsnc.ne! " Preservative Types: (1) nittic acid, (2) sulfuric acid, (3) hydrochloric add, (4) sodium hydroxide, 15) zinc acetate, Copy To: Todd.Humpfiriest_Dballingspringsnc.net Site Collection Info/Address: Town of Boiling Springs WWTP !6) methanol, (7) sodium bisulfate,13) sodium Mosuifate, (9) hexane, (A) ascorbic add, W ammonium sulfate, Rockford Read Shelby NC M52 (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other Analyses Lab Profile/Une: CttstomarProject Name/Numtler: State: County/City: Time Zone Collected: Lab Sande Receipt Checklist: 14c / 0evelarrr I )PT I IMT I ICT I %]ET Custody 8cals PrasvntiIrtact . N Phone: 704434-2357 Site/F'acllity 10 ti: Compliance Monitoring? Custody signatures Present � 'r •C4 Email: [X ] Yes [ ] No CoLlector 51tinature Present N NA Bottles Intact el ,, NA Collected By (print): PurChase Order#: DW PWS 10 N: Correct aottles %N NA volema N NA TODD HUMPHRIES Quote tf: DW Location Code: Buff iC: nt Collected By (signature): Turnaround Date Regtttred: Immediately Packed on Ice: > Samples Received on Ice � N NA [ ) Yes [ ]NO 0 USDA RegulateedoSoil9pta)ala y N Sample Disposal: Rush: Reld Rltered (if applicable): Samples in Holding 'rime C-Ai Aft I Dispose as approprtatr, ( 1 Return [ ] Same Day [ ] Next Day [ ]Yes ( [ No 0) (n O Residual Chlorine Present l I Arthive: [ ] Z Day [ [ 3 Day [ ] 4 Day [ ] 5 Day LU V V LL ❑ V Cl stxiP3: _ Sample pf1 Acceptable ta0 [ )Hold: (Ex���,gesApply) Analysis: V L7 _.l > U) � 0_ Q F"" Z � IPK Strips: Matrix Codes (Insert in Matrbt box bekm): Drinking Water (DW), Ground Water (GW), Wastewater (WW), j= Q m a fi Sul fide Present Y u Product (P), Soh/Solid (SL), Oil (OLL Wipe (WPI, Air W), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) L~L1 Q W Q O O Lead Acetate &trips: Como / collected (or Composite End Res A of V Q x Q LAB 7,e 3yLy Customer Sample ID Matrbt • Grab Composite Start) Cl Ctns -4 J � F- LU Y Lab Sanipie i i Ca <mter t s: I' Oats T me Date Time H f- I Q ILL iL i Digester Sludge WW G 8/25/20 8:00 1 X ] Digester Sludge WW G 8/25/20 8:001 1 X i Digester Sludge WW G 8/25/20 &001 1 X Digester Sludge WW G 8125/20 8:001 1 X Digester Sludge WW G 8/25/20 8:001 1 X I Digester Sludge WW G 8/25/20 8:001 1 X Digester Sludge WW G 8/25/20 8.001 1 X Digester Sludge WW G 8/25/20 8.00 1 X Digester Sludge WW G 8/25/20 8:00 1 X Digester Sludge WW G 8/25/20 8:00 1 X Customer Remarks / Special Cortftorts/ Possiible Hazards: TypeoliceUseck Blue Dry Norse SHORT HOLDS PRESENT (S72 hours)! Y <2> N/A LAB Sample Temperature info: r Packing Material Used: 8 Lab 4: 8 Temp aIaoB Re • /P �i Therm Cooler1. I1 e) Cooler Temp Upon Receipt; �• /�Fj�y�,71.7rt-(�,L�' /? � Samples received via: Cooler 1 Teem Corr, Fact CC I 1 Corrected Temp. r C Radchem sample(s) screened 1<500 epm): Y N NA FEDl7f llP5 Client Courier a Dotter Cooler Rellnqu y {Signature} Date/Time: Received d is lure) Date/Time- !?p MTfL iA13 USE ONLY Zj zu �'� Table #: Relinquished by/Company: (5 nature) Dat /lime: Received by/C Ignat re) Date/nme: ACctnum.- Trip Blank Received: Y N NA Template: HCL McOH TSP Other I— Prelogin: Relinquished /Company:{Signature) Datef0me: (k);". ivedj�co a Signature) r1 sL D /}Time: PM, Non Conformance(s): page: 0 tJ `�V�� yq Ps -.YES I NO nf: CHAIN -OF -CUSTODY Analytical Request Document a ceA/lalytical Chain -of -Custody is a LEGAL DOCUMENT - Complete all rekvent fields Company- Town of Boiling Springs Billing Information: Address: PO Boar 1014 Bolling Springs NC M17 PO Box 103A Boiling Springs NC 29011 Report To: Mike Glbert Copy To. Todd.Humphries@boiiingspringsnc.net Customer Project Name/Number. Phone:70"34-2357 ErnalL Collected By (print): TODD HUMPHRIES Collected By )signature)", ID If: se Order # : #: ound date Require& LAB USE ONLY- Affix Workorder/Login Label Here or List Pate Workorder Number or MTJL Log -in plumber Here � ALL SHADED AREAS are for LAB USE ONLY 9 Container Preservative Type " Lab Project Manager. M To: mike.gibert@boilingspringsnc.net "• Preservative Types: (2) nitric add, (2) sulfuric add, 01 hydrochloric acid, (4) sodium hydroxide, (S) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (6) ammonium sulfate. Collection JnWAddresv Town of Bolling Springs WWTP (Cj ammonium hydroxide, (0) TSP, (U) Unpreserved, (0) Other kford Road Shetby NC 28152 Analyses Lab ProflieAine: e: County/City: Time Zone Collected: Lab Sample 3s NC / Cleveland PT MT CT x ET [ ) [ l [ l l [ L a? � _ N ntteckliet: Cust«fp5eals Fresenri;nCdct Y N Present, Custody; S_gnatures Prfsen:t N Compliance Monitoring? [ X ] Yes ( ]NO p 7Jtt Collector Signature Present lHA U Z Bottles Intact: ti HA Correct eactles N NA DW PWS ID q: DW Location Code: 3 1 i' TV E Q C1J Sufficient Volume v it KA 9ampir5 Ra_e.lued on Toe N Nei Immediately Packed on Ice: > VOA _ Headapace Acceptable N ( lYes ]No O. P USDA Reulat.00 5o4a m C% (y1t. Sample Disposal: flush: Field Filtered (if appllcablel: %J g ? ro samples in Y.old.ng Time tm ( ] Dispose as appropriate I I Return [ ] Same On [ ] Next Day ( 1 Yes ] ) No O m C Residua 1 Cn1,or.n� i'rasent '.' K 1 I►+ehi,ra [ 12 Day [ 3 nay [ ] 4 Day [ 15 Day c E — o c Strips: 1 am: ? (q N +- p Sample pH Rtcttptable Y ]HN [ExWlteCliargesApply) Anat0s: it) E .` pH Stripe: • Matrix Codes (Insert In Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), _ c E Q Z 5ulEida kxesent Y rt 3 m - Q C Lead Acetate Strips; Product (P). Soll/3olid (SL), Oil (OL). Wipe (WP), Air {AR}, Tissue (TS), Bioassay (B), Yapor (y), Other JOT) E Lo C Comp / CoFlected (ar Composite End Res # of c ` 2 e E o Lab USE ONLY, A Customer Sample ID MaMx' Grab CampostteStart) CI Ctns M 0 4a o E tab Sample ai I cQoa�]snt"s7: Date Time DaEe Time a - U Z (L U) Q I :DlaesterS[ucke WW I G 1 1 8/25/20 8:00 1-1 X001 Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: ]fdgti Blue Dry None ALL results must be reported 10 MgJKfor SAR. We. # Pdd ing Material Used: do need the 5AR calculation. —1 .ne '* . / [ ! , Jn Radchem aample(s) screened 1c500 cprn): Y N NA ul� pang: (Signature) n IRT HOLDS PRESENT (c72 hours): Y Tracking th mples received via: FEDEX UPS C€lent Courier ! Date/Tirrpe: MTJL G r1. Table #: N/A LAB Sample Temperature Info. Tome EID#. lied f ♦N Therm SDjI: Cooler 1 Temp upon Receipt: Cooler 1 Therm Corr. factlac Cooler 1 Corrected Tamp:l6 Trip Blank Received: Y N HCL McOH TSP Other Pretogin: PM: PEI: )ate/Time: ed / aturel We�� Date/Time: F0 rU7 Non Contorrn"s): YES / fNOI� Page' o'i f: �� !2'eAnalytical' mparty: Totem of Boiling Springs CHAIN -OF -CUSTODY Analytical Request Document I LABUSE ONLY- Afflu Workorder/Login Label Here or List Pace Workorder Number or MTX Login Number Here dress: PO Box 1014 Boiling Springs NC 28017 port To- Mike Gibert py To: Todd.Humphries@bollingspringsnc.net st rner Project Name/Number. Is a LEGAL DOCUMENT • Complete all relevant fields lilting Information: ALL SHADED AREAS are for LAB USE ON Y 10 Box 1014 Bailing Springs NC 28017 _ Container Preservative Type'* Lab Project managew' :mall To: mike.gibert0bofNngsrpringsnc.rM '• Preservative Types: (1) nitric add, (2) sulfuric acid, (3) hydrochloric and, (41 sodium hydroxide. {51 zinc acetate. die Collection Info/Address: Town of Boiling Springs WWTP (51 methanol,17) sodium bisulfate, (9) sodium thiosutfate, (9) hexane, (AI ascorbic and, (B► ammonium sulfate, toddord Road Shelby NC 28LS2 (Cf ammonium hydroxide, (DI TSP. IV) UnpreServed, 10) Other Analyses Lab Profife/Llne: 'Mate: County/City: Time2oneCnlletYed: Lab Sample Receipt Checklist: NC / Cleveland [ IPT [ )MT [ la XIE7 Dne: 704-434-M7 Site/Fati(lty ID N Compliance Monitoring? Custody Seats PrNaent/lritaat. t N Custody Signatures Present Y !rw sail: [ X ) Yes [ ] No Collector Signature Present N ltA Bottles intact ti HA Correct Battles N 3!A Itected By (print): PtadraseOrder 0: DWPWSIDM; DDHUMPHRIES Quote A: DW Location Code: sufficient volume Samples -Received on Ice Itected By (signature): Turnaround Date Required: Immediately Packed on Ice: I ] Yes [ ]NO - dA - tiesdspace, Acc ptablo Y N' DR Regulated Soils ? N R ripleDisposal: Rush: Field Flltered (if appllcable): mplos in Holdl:x$ Time(► H NA Dispose as appropriate ( l Itelinn [ J Same Day [ ] Next Day ( [ Yes [ )No sidual Chlorine Prauent 7 ,00 Archive: [ 12 Day [ 13 Day 1 14 Day [ ] 5 Day Strips: Hold: (E■ped"Charges Apply) Analysis: 0 f le PH Acceptable Y N I pH 5t:ips: Sulfide Present Y x,t 4atrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), roduct (P), Soi1/Solld (SLI, Oil (OL), Wipe (WP), Air (AR), Time (TS), 81loassay (B), Vapor (V), Other (OT) Lead Acetate Strips; Comp / Collected (or Composite End Res d of LRB GSF OULT Y: torSampklD me Matrix' Grab Composltestart) CE Ctns =, lab B Cr�nmaeta: Date I Time 1 Date I Time gester5ludge WW G ,comer Remarks / Special Conditions / Posslbie Hazards: Type of Ice used: ore is no "Digested Sludge HI(Y' sample due to lack of Packing Material Gies and we were able to combine two samples in one lection bottle. Reactluity report in mg/l, Corrosivity in io�e Slue Dry None & Ignitabilty in deg/f �. Radchem samples) screened 1<5M cpm): Y N NA i fished by/Com :{5ignature) Date me: Rec!, � a lgnature) Yr 2.> li(qulshed by/Company: (Si ture) I Date/Time: Received by ev: I anaturel 0 w (Signature) SHORT HOWN PRESENT (s72 hours) : Y UN/A Lab Tracking p: Samples received via: FEDEX UPS Client Courier tfaceCoor Date/71me: TJL LAB USE ONLY rC1�il r� Table q: LAB Sample Temperature Info: Temp Blank R v 4 N ) Therm ID#: Cooler 1 Temp Upon Receipt: Cooler 1 Therm Carr. Factpnc Cooler 1 Corrected Temp:ff Ccmffi9nts: ite/rime; Acctnurn: Trip Blank Received: Y N * Template: HCL McOH TSP Other Prelogiw ite/Time: PM: Non Confer eels[ ipage- � t PB: YES '/ N !of: Analytical Results Pace Analytical 9800 Kincey Suite 100 Huntersville, NC 28078 Receive Date: 08/25/2020 Reported: 08/27/2020 For: Town of Boiling Springs Comments: Geometric Mean: 13.736 MPN/g STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200825-14-01 Fecal Coliforms DS1 62500 MPN/g SM92210E-2006 08/25/2020 MD 200825-14-01 Percent Solids DS1 1.44 % SM2WB-2011 08/25/2020 MD 200825-14-02 Fecal Coliforms DS2 11806 MPNIg SM92210E-2006 08/25/2020 MD 200825-14-02 Percent Solids DS2 1.44 % SM2WB-2011 08/25/2020 MD 200825-14-03 Fecal Coliforms DS3 3449 MPN/g SM92210E-2006 08/25/2020 MD 200825-14-03 Percent Solids DS3 1 45 % SM2WB-2011 08/25/2020 MD 200825-14-04 Fecal Coliforms DS4 16783 MPN/g SM92210E-2006 08/25/2020 MD 200825-14-04 Percent Solids DS4 1.43 ado SM254OB-2011 08/25/2020 MD 200825-14-05 Fecal Coliforms DS5 20408 MPN/g SM92210E-2006 08/25/2020 MD 200825-14-05 Percent Solids DS5 1 47 % SM2WB-2011 06/25/2020 MD 200825-14-06 Fecal Coliforms DS6 9028 MPN/g sM92210E-2006 08/25/2020 MD 200825-14-06 Percent Solids OS6 1 44 % SWWB-2011 08/25/2020 MD 200825-14-07 Fecal Coliforms DS7 11724 MPN/g sM9221cE-2006 08/25/2020 MD 200825-14-07 Percent Solids DS7 1.45 % SM25408-2011 08/25/2020 MD Respectfully submitted, �).Q WOL, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 ptagge 10 of 13 O m D x N N Oa Let Cu v N C tD Z r7 N 00 Ql 00 V r T J v 00 V m � is3A p, to � w � 0 V Rice ialyfral CHAIN -OF -CUSTODY Analytical Request Document LM USE OHtY- AM. Wa40rdaJL0pm LAW Hen or List Pace Wolkankr Wv bn or MTIL Loa -in Number Here Cha1n-01-Cu90dr ,S a LFGAi DOCUMENT • Cgmpiale aA reft"M fields ®dine Mf."Mk t ALL SHADED AREAS are for LAB USE ONLY PD era Im MMh- fmen"? L. ro �.e wxr MfICrK fPrtrlP qC s.ox TaMlg6Mr! - - Xi iow4orlpgboi%npprsnasnc.net wr Protect NameiNurnlwr Caret raw Prewvavve T LAIr Waled Manerar. r TWWAMafban9barleMir►ipitamM " heler•aea. Tww I ll sow odd. l:l +uarwk rpm of hrMedlierk no& 141 "r hrbv..or isi der wme CrreCtlan inlolh ddrecs fasws pf N�s1� iFrM�a F ; Iaermal M wd% m bft,0M. (=1 ' k W ft0idr. M Terre W pre he aud. fal rdw ern rMle. ITirr/ Mad Shelby NC ir1S1 Ki aasasraam hraraa�de, IMT101 {ul Urlpas!"wo. (010drw r. CowtriCly Tlewiarscambew: NC I ae"u d I wr Compliance Marina**? I x I Yes I I No DW Pws LD e_ D'rr Lamm Code. Immediately Packed an lee Yea No WOW 040-w; I LT"M rs rpnrwou I I Rel.n I a'emw I m w: Roil; I I S"w DaY ( l Next Day 1 12 Dot 1 13 DaY ( 14 Day 1 15 Dar fe.p.rae Dow AMllp P*W Filtered I# 1 1 Yes ! I NO AnahRtr Maox Codes (him kl Mob* pa bduwl:D iekirg Water (OWI. Ground Water (GW I. Wntemt Pr IWWi, pmdw Im. SaA/Sard OU. Or pU Wipe (WPI, Air CAN), Tlswe Trs1, Rloete 1V (111, vaPIK M. other ICM onow$w4ftA MNm' Canty I Gob CdIrtA011rrcam End Date itllM oats Tine lltester Sludge #1 ligester Sludge Ill WW G 8/25/20 6:00 WW G 8/25/20 6:15 %gester Sludge 03 WW G 8/25/20 6:30 ligester Sludge 04 W W G 8/25/20 6:45 )igester Sludge #5 WW G 8125/20 7:00 „tester Sludge 06 WW G 8/25/20 7.15 Mestef Sludge #7 WIN G 8/25/20 7.30 Crammer R"wittt I Spa" Conditions I Possible -16. Ol al wa thw: that fto &V Mow ry IMarrrlel Ute� Item tartlplaitl soerned E40R cpnY Y N NIL o tiro �� tX110 ItOlDS I+RESFrrt 1�72 Muvsl' t N PI/A tAb Ttsddr� M: SOMA" Iraeired vUL FLIDE7t UPS Ownt Coww Paw COLWW FlalA/17rne: !� ` UTIL Ua 215E BM TwnOM. CurLody aeada rraeit-t 11.1"t Y r 80L Ole[ady Aig"t,ra rsssAnt T M dA Col Leetpe ilgnat=v Yr'errmr. Y r ft Fottlea IRteCt Y O ril Cares& flbttlea Y N nA Sortie wt Yo1ar t x KA Racet+eo are xoe T F tq =iea vuA - BeadePeos AaespeaCte Y O TOL USDA alpgnlAlted SCUA Y IL KA $a glee In ilotdtsq Ties T r M PrsldYrl `tiler the IYeMmL t IS KA CS Srr Lpai sampl■ PH Aceeptsble T >+ %A PLL 6t4l9el SUIIt** Prtlaent T M WI ..aa A. -.tat. ft rlra� Lai 110E OpLYr Ltl raeple a _.�te: L' Bieck Va it.d; Y e IOL IGe= r I Trp Upon AecAipti oC r 1 rh» Carr. r&,tCrL oC r 1 Carfamea T.ey: ,oC TAp�liFOelfleI r N MA Na "" TSP Duier vs I No or _ ._ Town of Boiling Springs Land Application of Residual Solids Tanker truck and spreader used (19ft. X 600ft. Approx) 11,780 gal acre or 3.8 foads acre Year: Z Weather Volume soil i �- LO Catio condition 1 condition gallons� � �F?rstll�;i �® PATHOGEN & VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Town of Boiling Springs WQ Permit Number: WQ00183352 WWTP Name: Town of Boiling Springs WWTP NPDES Number: NCO071943 Monitoring Period: From 1/1/2020 To 12/31/2020 Pathoeen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ T Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ 1 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alternative I El I Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ 1 Air Drying❑ Composting [I Aerobic Digestion F] Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o dences Frequency of Analysis Sample Type Analytical Tech ni ue Mininut Geo. Mean aximu Units Fecal Coliform ? x 10 to the 6th power per gram of total solids MPN 3449 13736 62500 MPN/g 0 7/year Grab SM9221 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: All.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) J Alt. 9 (Injection) ❑ AIt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ 4*1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Gibert / Public Works Director Todd Humphries / Wastewater Supervisor Preparer Name and Title (type or print) Land Ap/pliier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) Annual Pathogen and Vector Reduction Summary Town of Boiling Springs permit # WQ0018352 2020 Fecal Coliform - Class B There were seven (7) test results provided by Pace Analytical Services in Huntersville. The calculated Geo Mean for the Fecal Coliform samples was 13736 MPNIg. Vector Attraction Reduction Option 4 - Sour test results are reported in the attached data showing seven (7) test results at 1.23 mg Oxygenlglhr or less for Specific Oxygen Uptake Rate. End temperature for each test result was under 30 Degrees Celsius and the percent solids were under 2% for each result. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level 1) 4 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boiling Sprin s,NC W 00018352 8/25/20 26 8/25/20 Todd Humphries /25/2020 r 6:00:00 A Todd Humphries 300 1.44 26 24 0.1 5.1 1.0 milliliters Yo Dry Solids Degrees Celsius Degrees Celsius 4.24 mg Oxygenlhr 0.98 mg Oxygenlg/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rater 0.77 mg Oxygenig;hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. M 2 3 4 5 6 7 Circle Test 4 PH Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level Slope: I ntercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: P n S rin s,NC 018352 25/20 25 8/25120 Todd Humphries 8/25/2020 6:15 Todd Humphries 300 1.44 25 25 0.1 6.1 1.0 milliliters Dry Solids degrees Celsius degrees Celsius 6.77 mg Oxygenlhr 1.57 mg Oxygen!glhr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.23 mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 (2) 3 4 5 6 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature. Sampling Date/Time Sam pled By. Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level (mg/0 ki Slope: I ntercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: P rin s,NC 018352 5/20 27 8125/20 Todd Humphries 8/25/202016:30:00 AM Todd Humphries 300 1.45 27 25 0.1 5.6 1.0 milliliters Yo Dry Solids jegrees Celsius Degrees Celsius 3.83 mg Oxygen?hr 0.88 mg Oxygen/g/hr 26 degrees Celsius 0.746215397 Temperature Corrected Specific Oxygen Uptake Rate: 0.66 mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 (3) 4 5 6 7 Circle Test # Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name. Biosolids Permit Number Date Digester Temperature. Sampling DateJime. Sampled By Analysis DatelTime Analyzed By Sample Volume. Total Solids Beginning Temperature. End Temperature Dissolved Oxygen Level (mg/1) 4.65 Slope: I ntercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boiling Sprin s,NC W Q0018352 8/25/20 27 8/25/20 Todd Humphries 8/25/20 / 6:45 AM Todd urn ries 300 .4 27 25.0 0.1 5.6 1.0 milliliters Yo Dry Solids legrees Celsius Degrees Celsius 4.25 mg Oxygen/hr 0.99 mg Oxygen/g/hr 26 degrees Celsius 0.746215397 Temperature Corrected Specific Oxygen Uptake Rate: 0.74 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. 1 2 3 (4) 5 6 7 Circle Test # Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name. Biosoiids Permit Number Date Digester Temperature Sampling DatelTime. Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boiling Sprin s,NC W Q0018352 8/25/20 26 8/25/20 Todd Humphries 81 51 017:15AM Todd Humphries 300 1.47 26 25.0 0.1 5.5 1.0 milliliters Dry Solids Degrees Celsius Degrees Celsius 3.74 mg Oxygen/hr 0.85 mg Oxygen/g/hr 26 degrees Celsius 0.746215397 Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 (5) 6 7 Circle Test # Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time. Analyzed By Sample Volume Total Solids. Beginning Temperature End Temperature Dissolved Oxygen Level 5 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Town of Boiling S rin s,NC W Q0018352 8/25/20 27 8/25120 Todd Humphries 8125/20 17:30 AM Todd Humphries 300 1.44 27 26.0 0.1 5.6 1.0 n illiliters Yo Dry Solids legrees Celsius legrees Celsius 3.31 mg Oxygenlhr 0.77 mg Oxygenlglhr 27 degrees Celsius 0.71068133 Temperature Corrected Specific Oxygen Uptake Rate:,, 0.54 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 5 (6) 7 Circle Test # Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number Date. Digester Temperature. Sampling Date/Time Sampled By. Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level 5. Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: niters )ry Solids rees Celsius rees Celsius 0.0 5.6 1.0 2.07 mg Oxygen/hr 0.48 mg Oxygen/g/hr 27 degrees Celsius 0.71068133 Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr lnstructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 5 G (7) Circle Test # SOIL ANALYSIS REPORT Page 1 of 1 Report Number: 20-275-0557 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kincfey Ave Huntersville NC 28078 • Waypoint. ANALYTICAL "Every acre... Every year." - SOIL ANALYSIS REPORT Date Received: 10/01/2020 bate Ot Analysis: 10,'02,2020 Date Of Report: 10/26/2020 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Workorder: 92498087 Analytical Method(s): Mehhoi 3 SMP Buller pH Loss Qn 19nilion Water pH HM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil Ibs1A M3 K Mg Ca Na Soil Buffer H Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg11009 meg1100g JP ft1 Field 21583 2.0 139 156 VH 160 VH 258 H 1169 M 15 VL 6.6 6.88 0.5 9.0 NC=130 NC-82 JP V Field 21584 1.8 126 259 VH 259 VH 265 VH M 13 VL 6.8 6.91 0.2 8,3 NC=216 NC=132 11027 1 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K Mg Ca Na H NO,N S Zn Mn Fe Cu B SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate msr'cm Rate JP #1 Field 4.6 23.9 64.9 0.7 5.6 16 M 10.3 VH 19 M 5.5 VH 10 M NC = 33 NC = 257.5 NC = 119 NC = 275.0 JP #2 Field 8.0 26.6 61.9 0.7 2.4 16 M 10.3 VH 16 M 4.4 VH 0.7 M 1 1 1 NC = 33 NC = 257.5 NC = 100 NC w 220.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), 1. (Low). M (Medium) H (High), VH (Very High). ENR . Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. o_ A Explanation of symbols: Samples % (percent), ppm (parts per million).1brJA This report applies to sarnplels) tested. Saes aye retained a (pounds per acre), mslcm {milli -mhos per centimeter), meq+100g maximum of thirty days after tasting. (milli -equivalent per 100 grams). Conversions: ppm x 2 - lbVA, Soluble Analysis pfepared by: Waypoint Analytical Virginia, Inc. Salts msrcm x 640 = ppm. by: 1f1( %QD w�I Pauric Mc Groary Ph.DL, CPAg i -_ aceArralytrcal Company: Town of Boiling Springs CHAIN -OF -CUSTODY Analytical Request Document `p`a"3' W�� : g2498VS7 member°` �__. 0 N N I Address: PO Box 1014 Bolling Springs NC 28017 Report To: Mike Gibert Copy To: Todd.Humphries@bollingspr(ngsnc.net ier Project Name/Number: 70"34-2357 Site/Facility 1D N: Is a LEGAL DOCUMENT - Complete all relevent fields 11111111111111111111111111Billing information: d PO Box 1014 Boiling Springs NC 28017 92498087 COnuji.-- Email To: mike.gibert@boilingspringmc.net " Preservative types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, Site Collection Info/Address: Tom of Bolling Springs WWTP (5) methanol, 171 sodium Bisulfate, (B) sodium thlosulfate, (9) hexane, (A) ascwhic acid, (B) ammonium sulfate, Rockford Road Shelby NC 29152 (C) ammonium hydroxide, (0) TSP, JU) Unpreserved, (0) Other Lab Profllei/1.4w. State: Count /Ci Time Zone Collected: Ana#yses y ty' Lab Sample Receipt: Checkli:;t, NC / Cleveland I I PT MT CT I R I ET Custody Seals Present/Intact Y tith Compliance Monitoring? I Custody Signatures Present cZ N NA [ X ] Yes ( ] No Ce-liector Signature Present (T�t4 KA Wlected (print): 81' (p ) Purchase Order# : DW PWS ID #, Bottleact N +act Correct Ss�tilea CrNfan Corr Correct TODDHUMPHRIES Quote#: DW Location Code: Suffirienc tiulume ODN vat Samples Received on Ice tD N NA Collede4 By (sib tur� Turnaround Date Required: Immediately Packed on Ice: d VoA - Headspace Acceptable Y N 1n ]Yes NO USDA. Regulated Soils Y@2NA $=plea in Holding Time (ESN NA Stimple Disposal: Rush: Reid filtered (if applicable): [ ] Dispose as appropriate I ] Return [ j Same Day [ ] Next Day [ J Yes ( I No 16- Residual Chicrine Present Y H ep [ 1 Archive; [ ] 2 Day [ 13 Day [ ] 4 Day [ 1 5 Day a '" 0) Cl Strips: [ ]Hold: [Expedite Charges A Analysis: ++ CL U W to U pH Acceptable Y N E pH Strips: Sulfide Present Y k • Matrix Codes (Insert in Matrix box below): Drinking Water (DWI, Ground Water [GW), Wastewater (WW), Product (P), Soil/Solid (SL), 011 (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) CL in o E N LHad Acetate Strips: w t0 Cl C M = E LAB 178E ONLY: Comp / Collected (or Composite End Res # of Customer Sample ID Matrix' Grab Cam sfte Start Cl Ctns ;5 N C) � 0 in p Lab Sample ! Comments: Date Time Date Time m e0 S 7 LLJ C) 2 2 cc C3 d cn [�J� JP #1 Field WW G 1 X X X X X X X X X X ti JP #2 Field WW G �9 2p 1 X X X X X X I X I X I x X W L Customer Remarks / Special Conditions / Possible Hazards: �• FC.!`:: �•+� Type of Ice Used: lllg�7 Blue Dry None SHORT HOLDS PRESENT (02 hours) : Y (!� N/A LAB Sample Temperature Info: Theerimp Blank Received: Y N Therm IOM: 9127ftf Cooler 1 Tenp Upon Receipt:.OA C Cooler 1 Thera Corr, Fectoz4%e,?C Cooler 1 Corrected Tenp: -14roc Comments, Packing Material Used: 8 LabTracking# Radchem sample(s) screened (<500cpm): Y N NA Samples rmiyedvia: FEDEX UPS Client Courier r R qujsh ompry: ((Signature) u Date/Time: -3o ZJ Receiv y/ : {Signature) batetTme., MT1L LAB USE ONLY Table #: Rel(n u ompan (Slgnature) DateMme: /Company: ( nature) •�` 9'~'� 1 Date/Time: C( ' t�D Aectnum: Template: Prelogin: PM: PB: Trip Blank Received: Y N 40 HCL McOli T5P Other Relinquished by/Company: (Signature) Datejrime: Received try/Company: (Signature) Date/Time: felon Conformance ls); YES / NO Page: of: