HomeMy WebLinkAboutWQ0018352_Residual Annual Report 2020_20210223Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00018352
Applicant/Permittee Town of Boiling Springs
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Mooresville
CO Reviewer
Admin Reviewer
Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Michael F. Gibert
Email Address*
mike.gibert@boilingspringsnc.net
electronic subntttal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
17044342357
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00018352
Fbs Current Existing perrrit number
Applicant/Permittee Address* PO Box 1014 Boiling Springs NC 28017
Facility Name * Town of Boiling Springs RLAP
Please provide comments/notes on your current submittal below.
2020 Annual LA Residuals Report for the Town of Boiling Springs
The Permittee/Town Manager (Lucas Shires) is no longer employed by the Town. I am
signing this report with Signatory Authority.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Annual LA Residuals Report.pdf 5.97MB
Upload only 1 RCFdocurrent (less than 250 M3). ivL@iple documents nest be corrbined into one RDFfile unless file is larger than
upload lirrit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature`
rra�W1q' 4*x0te-
Submission Date 2/23/2021
THE TOWN OF
BOILING SPRINGS
NORTH CAROLINA
Date: 2/22/2021
To: The Information Processing Unit
NCDWR Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Land Application of Residuals
Town of Boiling Springs I NC
Permit # WQ0018352
To Whom it May Concern:
Please find enclosed the original report and all applicable forms and test results for the Annual
Residuals Land Application Report for the Town of Boiling Springs. An electronic copy of the 2020
Annual Land Application Report has also been submitted. Aerobic digested residuals continue to be
land applied to permitted fields for the beneficial reuse as a soil conditioner and fertilizer
supplement.
I will be signing this Annual Report with Signatory Authority. Please let me know if additional
information is needed at 704-434-2357.
Sincerely,
Mike Gibert
Public Works Director
Town of Boiling Springs
Enclosures:
Annual Land Application Report 2020
114 East College Avenue I PO Box 1014 1 28017 1 704 434 2357 1 www.boilingspringsnc.net
ANNUAL LAND APPLICATION
OF RESIDUALS
2020 ANNUAL REPORT
TOWN OF BOILING SPRINGS
Permit No. WQ0018352
THE TOWN OF
BOILING SPRINGS
-NC]RTH r;.
CERTIFICATION FORM
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit*: WQ0018352 County: Cleveland Year: 2020
Facility Name (as shown on permit): Town of Boiling Springs
Land Application Operator: Todd Humphries Phone: 704-300-8641
Land application of residuals as allowed by the permit occurred during the past calendar year?
r❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepermit]
3
Total number of fields utilized for land application during the yearl
1
Total amount of dry tons applied during the year for all application sites:
6.7
Total number of acres utilizes for land application during the year:
9.84
Part B - Annual Com iance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the pen -nit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations. "
Mike Gibert / Public Works Director
Permittee Name and Title (type or print)
Signature otPreparer*
Signature of
2-
Date Signature of Land Applier
Date
Z_zv-Zv z/
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 5039 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)
RESIDUALS SAMPLING FORMS
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ00183.52 Laboratory: 1)
Facility Name: Town of Boiling Springs 2)
Residual Source WQ # or NCO071943 3)
NPDES #: 4)
WWTP Name: Town of Boiling Springs WWTP 5)
Residual Analvsis Data
Pace Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)'
Sample or Composite Date
8/25/20
2111/20
Percent Solids W
NA
1.2
Arsenic
75
49.6
Cadmium
85
5
Copper
4,300
275
Chromium
NA
0
Lead
840
27.7
24.3
Mercury
57
2.2
Molybdenum
75
24.8
Nickel
420
24.8
Selenium
100
49.6
Zinc
7,500
712
Total Phosphorus
NA
15500
TKN
NA
31200
Ammonia -Nitrogen
NA
753
Nitrate and Nitrite
NA
5890
' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0018352 Laboratory: 1) Pace Analytical Services
Facility Name: Town of Boiling Springs 2)
Residual Source NCO071943 3)
NPDES # or WQ#: 4)
WWTP Name: Town of Boiling Springs WWTP 5)
Residual Analysis Data
Parameter
Sample or • p• Date
MMM
-
Magnesium
' 1 1
----_------
Potassium
M.-I
Percent Mositure
Reactive Cyanide----__-_---
Reactfive Sulfide
1
-_--_------
Flashpointdeg F1
1
-----------
-----------=
-----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
DENR FORM RSSF - B (1212006)
METALS FIELD LOADING SUMMARY
LAND APPLICATION FIELD SUMMARY
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Boiling Springs
Land Owner: James Petty
Operator: Todd Humphries
Crop 1 Name: Easture
WQ Permit #: WQ0018352 Field #: I Acres Utillzed: 9.84
Annual Dry Tons Applied: 6.7054 Site #: 3PI Acres Permitted: 22.41
Predominant Soil Series: Pacolet-Bethlehem Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 220 Crop 2 Name: Crop 2 Max. PAN:
`
y c
0 0
La
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
3'o
Solids
Volume
Applied r
pp per
Acre
(Dry TonslAc)
Residual Sources
(NPDF,S #, WQ#,
Fert., Animal
Waste, etc)
Soil
mod'
(Dry'
Moist)
Precip.
Past 24
Hrs.
inches
a
]v'
*
_X
fD w
°a
w "
* a'
*
TKN
mg*g
Z >
o 3
�'�•
mglkg
Nitrate
and
Nitrite
mglkg
PAN Applied
(Ibslacrel
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop i
Crap 2
6122/20
20000
1.2
0.102
NCO071943
dry
0
S
0.5
0.3
1 31200
753 1
5890
3.133
NA
pasture
6/23/20
12000
1.2
0.061
NCO071943
dry
0.05
S
0.5
0.3
31200
753
5890
1.880
NA
pasture
6124/20
20000
1.2
0.102
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
3.133
NA
pasture
6/25/20
10000
1.2
0.051
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
1566
NA
pasture
10/6120
14000
1.2
0.071
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
2.193
NA
pasture
i0n20
14000
1.2
0.071
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
2.193
NA
pasture
1018/20
24000
1.2
0.122
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
3.759
NA
pasture
I D/9120
20000
1.2
0.102
NCO071943
dry
0
S
0.5
0.3
31200
753
5890
3.133
N A
pasture
0.000
0.000
0.000
0.000
1
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF suph
to thi,, hn-m :
TOTALS:
0
t3aooa
As
Cd
Cu
Cr
Pb
I Ig
Mo
Ni
Se
Zn
p
20.989
0.000
Lime Applied
Annuallbslacre
0.061 0.006 0.336 0.000 0.034 0.003 0.030 0:030 0.061 0.870 18,941
1,486 0.10.1 3. 711 0.277 0.485 0.012 0.511 0.526 1.043 10.998
I.547 0.109 4.047 0.277 0.519 0.015 0,551 0.556 1.104 11.868
36 1 34 1 1338 1 n/a 1 267 1 15 nia 1 .174 89 1 2498
1 220
Date
lbs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including thy, possibility of fines and imprisonment for knowing violations."
Z-
zz-Z,-Z/
Signature of Land Applier
Date
*Application Method: S - Surface. IN - Injection, INC - Incorporation
**Volatiliw,ation Rate: Surface - 0.3. Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1. anaerobially digested -0.2.
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF i 1212006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Boiling Springs Total Dry Tons Applied (Annual):
Permit #: WQ0018352 Cation Exchange Capacity (non 503 only):
6,196
Operator: Todd Humphries Owner: James PettX Predominant Soil Series: Pacolet-Bethleher
Acres Used: 9.84 Acres Permitted: 22.41 Site #: 1 Field #: JP1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
8125/20
2
8/25/20
3
8/25/20
4
8/25/20
5
8/25/20
fi
8125/20
7'
8/25/20
8
8/25120
9
10
11
12
% Solids
1.2
1.2 1
1.2
1 1.2
1.2
1.2
1.2
1 1.2
Arsenic
49.6
49.6
49.6
49.6
49.6
49.6
49.6
49.6
Cadmium
5
5
5
5
5
5
5
5
Copper
275
275
275
275
275
275
275
275
Chromium
Lead
27.7
27.7
27.7
27.7
27.7
27.7
27.7
1 27.7
Mercury
2.2
2.2
2.2
2.2
T2
2.2
2.2
2.2
Molyb-
denum
24.8
24.8
24.8
24.8
24.8
24.8
24.8
24.8
Nickel
24.8
24.8
?4.8
24.8
24.8
24.8
24.8
24.8
Selenium
49.6
49.6
49.6
49.6
49.6
49.6
49.6
49.6
Zinc
712
712
712
712
712
712
712
712
Total
Phos-
horus
15500
15500
15500
15500
15500
15500
15500
15500
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7,
8
9
10
11
12
DT/Ac./
App.
v
Event
0.10
0.06
0.10
0.05
0.07
0.12
0.10
Arsenic
0.010
1 0.006
0.010
0.005
0.007
0.012
1 0.010
0,000
0.000
1 0.000
0.000
0.000
1 0.061
Cadmium
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.000
0,000
0.000
0.000
0.000
0.006
Copper
0.056
0,034
0,056
0.028
0.039
0.067
0.056
0.000
0,000
0.000
0.000
0.000
0.336
Chromium
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
Lead
0.006
0.003
0,006
0.003
0.004
0.007
0.006
0.000
0.000
0.000
0.000
0,000
0.034
Mercury
0.000
0.000
0.000
0.000
0.000
0,001
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.005
0.003
0.005
0.003
0,004
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.030
denum
Nickel
0.005
0.003
0.00.5
0.003
0.004
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.030
Selenium
0.010
0A06
0.010
0.005
0,007
0.012
0.010
0.000
0.000
0.000
0.000
0.000
0.061
Zinc
0.145
0.087
0.14.5
0,073
0.101
0.174
0.145
0,000
0.000
1 0.000
0.000
0.000
0.870
Total
Phos-
3.162
1.891
3.162
1.581
2.201
3.782
3.162
0.000
0.000
0.000
0.000
0,000
18.941
horus
"I certify. under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Z-ZZ- 7oz(
Date
DENR FORM MFLSF (12/2006)
RESIDUALS ANALYSIS LAB SHEETS
aceAnalytical
www P44:010sx0m
ANALYTICAL RESULTS
Project: Digester Sludge Samples
Pace Project No 92492276
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville, NC 28078
(7041875-9092
Sample: Digester Sludge Lab ID: 92492276001 Collected. 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311, 09/01/20 09:03 Initial pH: 7.68, Final pH: 4.92
Pace National - Mt. Juliet
2,4-5-TP (Silvex)
ND mg/L 0.00200 1 09/02/20 08:24 09/02/20 18:20
93-72-1
2,4-D
ND mglL 0.00200 1 09/02/20 08:24 09/02/20 18:20
94-75-7
Surrogates
2,4-DCAA (S)
58.8 % 14.0-158 1 09/02/20 08:24 09/02/20 18:20
19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 80818 Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311: 08/27/20 13:05
Initial
pH: ; Final pH:
5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
ND
mg1L
000050
1
09/02/20 22:23
09/03120 16:09
58-89-9
Chlordane (Technical)
ND
mg1L
0.0030
1
09/02/20 22:23
09/03/20 16:09
57-74-9
Endrin
ND
mg1L
0.00050
1
09/02/20 22 23
09f03120 16:09
72-20-8
Heptachlor
N❑
mg1L
0A0050
1
09/02120 2223
09/03/20 16 09
76-44-8
Heptachlor epoxide
ND
mglL
0.00050
1
09102/20 22:23
09/03/20 18:09
1024-57-3
Methoxychlor
ND
mglL
1.0
1
09/02/20 22:23
09/03/20 16:09
72-43-5
Toxaphene
ND
mg1L
0.0030
1
09102/2022:23
0910312016:09
8001-35-2
Surrogates
Decachlorobiphenyl (S)
157
%
10-154
1
09102120 22:23
09/03/20 16:09
2051-24-3 S3
Tetrachloro-m-xylene (S)
103
%
10-184
1
09/02/20 22:23
09/03/20 16:09
877-09-8
Metals (ICP) 6010D
Analytical Method: EPA 6010D Preparation
Method: 3015
Pace National
- Mt Juliet
Calcium
651000
ugiL
1000
1
09/02/2010:42
09102/2012:32
7440-70-2
Magnesium
42400
ug1L
1000
1
09/02/2010:42
09/0212012:32
7439-95-4
Sodium
41900
uglL
3000
1
0910212010:42
09/0212012:32
7440-23-5
6010 MET ICP
Analytical Method: EPA 6010D Preparation
Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum
18900
mglkg
496
1
08/3012015:31
08131/2012:13
7429-90-5
Arsenic
ND
mglkg
496
1
08/30120 15:31
08/31120 12:13
7440.38-2
Cadmium
ND
mglkg
5 0
1
08130/20 15:31
08131/20 12:13
7440-43-9
Calcium
51100
mglkg
496
1
08/3012015:31
08/311201213
7440-70-2
Copper
275
mglkg
24 8
1
08/30/20 15:31
08131/20 12:13
7440.50-8
Lead
27.7
mg/kg
24.8
1
08/30/20 15 31
08/31/20 12A3
7439-92-1
Magnesium
4070
mglkg
496
1
0813012015:31
0813112012:13
7439-95-4
Molybdenum
ND
mglkg
24-8
1
08130/2C 15:31
08/31/20 12 13
7439-98-7
Nickel
ND
mglkg
24.8
1
08130/2015:31
08131/20 12: 13
7440-02-0
Potassium
ND
mglkg
24800
1
0813012015:31
08/31/2012:13
7440.09-7
Selenium
ND
mg/kg
49.6
1
08/30/2015:31
08131/20 12:13
7782-49-2
Sodium
ND
mglkg
24800
1
08130/2015:31
0813112012:13
7440-23-5
Zinc
712
mglkg
49.6
1
08130/2015:31
0813112012:13
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 09/0412020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 35
aceAnalytrca(
i www.panlaEs.com
ANALYTICAL RESULTS
Project: Digester Sludge Samples
Pace Project No. 92492276
Pace Analytical Services, LLC
9800 Kincey Ave Suite l00
Hul NC 28078
(704)875-9092
Sample: Digester Sludge Lab lD: 92492276001 Collected: 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICR TCLP
Analytical Method EPA6010D Preparation Method EPA3010A
Leachate Method/Date: EPA 1311:08I30120 13 34 Initial pH:: Final pH:
2
Pace Analytical Services - Asheville
Arsenic
0.12 mglL 0.050 1 09101/2002:07
09101/2010:36
7440-38-2
Barium
ND mglL 0.25 1 09/01/2002:07
091011201036
7440-39-3
Cadmium
NO mg/L 0 0050 1 09/01/20 02:07
09/01/20 10:36
7440.43-9
Chromium
NO mglL 0 050 1 09/01/23 02:07
09/01/20 10 36
7440-47-3
Lead
NO mglL 0 025 1 09/01/20 02:07
09/01/20 1036
7439-92-1
Selenium
NO mglL 0.10 1 09101/2002:07
09101/2010.36
7762.49.2
Silver
ND l 0.025 1 09/01/20 02:07
09101/20 10,36
7440.22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA7470A
Leachate Method/Date: EPA 1311: 08/30/20 13:34 Initial pH Final pH:
2
Pace Analytical Services - Asheville
Mercury
NO mglL 0-00020 1 0910112011:14
09102/2014:53
7439-97-6
7471 Mercury
Mercury
8270E TCLP RVE
1.4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(l Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2.4.6-Trichlorophenol
Surrogates
Nitrobenzene-tl5 (S)
2-Fluorobiphenyl (S)
Terpher l-d14 (S)
Phenol-d6 (S)
2-Fluoraphenol (S)
2.4,6-Tribromophenol (S)
8260D MSV TCLP
Benzene
Analytical Method: EPA 7471 B Preparation Method. EPA 7471 B
Pace Analytical Services - Asheville
2.2 mglkg 0.15 1 08/2812013:10 08/28/2015:09 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311. 08/27120 13:05 Initial pH:. Final pH: 5
Pace Analytical Services - Charlotte
NO
mglL
0.050
1
09/02120 20:42
09/03/20 10:24
106-46-7
ND
mg1L
0.050
1
09/02/20 20:42
09/03/20 10:24
121-14-2
NO
mglL
0.050
1
09/02120 20:42
09/03/20 10:24
87-68-3
NO
mglL
0.050
1
09)02120 20A2
09/03/20 10 24
118-74-1
NO
mg1L
0.050
1
09/02/20 20:42
09/03/20 10:24
67-72-1
NO
mglL
0.050
1
09/02120 20 42
09/03/20 10:24
95-48-7
ND
mg1L
0.050
1
09/02120 20:42
09/03120 10:24
15831-10-4
NO
l
0.050
1
09/02120 20A2
D9103120 10:24
98-95-3
NO
mg1L
0.10
1
09/02/20 20:42
09/03/20 10:24
87-86-5
NO
mg1L
0.050
1
09/02/20 20A2
09/03120 10:24
110-86-1
NO
mg1L
0.050
1
D9102120 20:A2
09/03120 10:24
95-95-4
ND
ril lL
0.050
1
09/02/20 20:42
09/03/20 10:24
88-06-2
91
%
13-130
1
09/02120 20A2
09/03/20 10:24
4165-50-0
86
%
13-130
1
09/02/20 20:42
09/03120 10:24
321-60-8
125
%
25.130
1
09/02/20 20:42
09/03/20 1024
1718-51-0
51
%
10-130
1
09/02/20 20:42
09/03/20 10:24
13127-88-3
63
%
10-130
1
09/02120 20 42
09/03/20 10:24
367-12-4
93
%
10-137
1
09/02/20 20:42
09/03/20 10:24
118-79-6
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311. 08/2812D 10:57
Pace Analytical Services - Charlotte
ND mglL 0.10 20 08/30/20 2132 71-43-2
REPORT OF LABORATORY ANALYSIS
BC
Thts reperl shall not be reproduced. except in Full.
Date: 09/0412020 03:59 PM without the written consent of Pace Analytical Services. LLC Page 6 of 35
aceAnalytical
www.pacehbs.com
ANALYTICAL RESULTS
Project: Digester Sludge Samples
Pace Project No 92492276
Pace Analytical Services, LLC
9800 Kincey Ave- Suite 100
Funtersville, NC 28078
(704)875-9092
Sample: Digester Sludge Lab ID: 92492276001 Collected: 08/25/20 08:00 Received: 08/25/20 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Dmit DF Prepared Analyzed CAS No. Qual
8260D MSV TCLP
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1.4-Dichlorobenzene
1,2-Dichloroethane
1.1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
Calculated Results
Sodium Adsorption Ratio
1010 Flash poiri losed Cup
Flashpoint
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
Date: 09/04/2020 03:59 PM
Analytical Method: EPA 8260D Leachate Method/Date : EPA 1311: 08/28/20 10-57
Pace Analytical Services - Charlotte
ND
mglL
0.20
20
08/30/20 21:32
78-93-3
ND
mglL
0.10
20
08/30/20 21:32
56-23-5
ND
mglL
0,10
20
08/30/20 21732
108-90-7
ND
mg1L
0.10
20
08/30/20 21:32
67-66-3
ND
mg/L
0.10
20
08/30/20 21:32
106-46.7
ND
mglt
0.10
20
08/30/20 21:32
107-06-2
ND
mg/L
0.10
20
08/30/20 21:32
75-35-4
ND
mg/L
0-10
20
08/30/20 21:32
127-18.4
ND
mglL
0.10
20
08/30/20 21:32
79-01-6
ND
mg1L
0.10
20
08/30/20 21:32
75-01-4
104 %
70-130 20
105 %
67-135 20
101 %
70-130 20
Analytical Method: SM 254OG-2011
Pace Analytical Services - Charlotte
1.2 %
0-10 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
98.8 % 0.10 1
Analytical Method: Calculated Preparation Method: Cali
Pace National - Mt. Juliet
0.429 1
Analytical Method: EPA 1010A
Pace Analytical Services -Asheville
08/30/20 21:32 17060-07-0
08/30/20 21:32 2037-26-5
08/30/20 21:32 460-00.4
08/26/20 18:02
08/26120 17:46
0910212012:32 09/0212012:32 SAR
>200 deg F
70.0
1 09/02/20 16:03
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
8.5 Sid, Units
0-10
1 08/31/20 14:54 Q
Analytical Method: SM 271OB-2011
Pace Analytical Services -Asheville
15200 mg/kg
0.12
1 09103/2015:52 N2
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg
753
1 08/3012013:07 08131/2010:17 7664-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not oe reproduced, except in full,
without the written consent of Pace Analytical Services, L _G. Page 7 of 35
) 7
'i
aceAnalytrcal
www.pacelabs.com
ANALYTICAL RESULTS
Project: Digester Sludge Samples
Pace Project No.: 92492276
Pace Analytical Services, LLC
9800 Kineey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: Digester Sludge Lab ID: 92492276001 Colllected 08/25/20 08:00 Received 08/25/20 09 10 Matrix Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method. EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen Kjeldahl, Total
31200 mglkg 3540 1 08/28/20 22:19 08/29/20 06:16 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method- EPA 353-2 Rev 2.0 1993 Preparation Method. EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
5890 mglkg 1590 5 08/25/20 21:37 08/25/20 23:43
Nitrogen, Nitrate
5890 mglkg 1590 5 08/25/20 21:37 08/25/20 23:43 14797-55-8
Nitrogen, Nitrite
ND mglkg 318 1 08/25/20 21:37 08/25/20 22:50 14797-65-0
365.1 Phosphorus, Total
Analytical Method EPA 365 1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
15500 mg/kg 370 5 08/31/20 20:14 09/01/20 18:28 7723-14-0
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method SW-846 7 3.3.2
Pace Analytical Services - Greensburg
Cyanide. Reactive
ND mglkg 81.0 1 08/27120 16.51 08/27/20 20:23
734S Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mglkg 810 1 08/27/20 16:51 08127i20 17:07
Dale 09/04/2020 03 59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC.
i(MI)
J(M1)
Page 8 of 35
CHAIN -OF -CUSTODY Analytical Request Document
LAB USE WO # : 92492276 umber or to
�CeAnalytical
I
I
o
Chain -of -Custody is a LEGAL, DOCUMENT - Complete ail relevem fields
Coenparty: Town of i3ollin9 Springs
Billing information:
f 1 !
92492276
ar
kWr6W.' PD BOX 1024 Boiling Springs NC 28017
PO Box 1014 Boiling Springs NC 2801713
Container Preservative Type**
Lab Pra]ett Manager:
Report To: Mike filbert
Email To: mike. gibertpboilingspringsnc.ne!
" Preservative Types: (1) nittic acid, (2) sulfuric acid, (3) hydrochloric add, (4) sodium hydroxide, 15) zinc acetate,
Copy To: Todd.Humpfiriest_Dballingspringsnc.net
Site Collection Info/Address: Town of Boiling Springs WWTP
!6) methanol, (7) sodium bisulfate,13) sodium Mosuifate, (9) hexane, (A)
ascorbic add, W ammonium sulfate,
Rockford Read Shelby NC M52
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Analyses
Lab Profile/Une:
CttstomarProject Name/Numtler:
State: County/City: Time Zone Collected:
Lab Sande Receipt Checklist:
14c / 0evelarrr I )PT I IMT I ICT I %]ET
Custody 8cals PrasvntiIrtact . N
Phone: 704434-2357
Site/F'acllity 10 ti:
Compliance Monitoring?
Custody signatures Present � 'r
•C4
Email:
[X ] Yes [ ] No
CoLlector 51tinature Present N NA
Bottles Intact el ,, NA
Collected By (print):
PurChase Order#:
DW PWS 10 N:
Correct aottles %N NA
volema N NA
TODD HUMPHRIES
Quote
tf:
DW Location Code:
Buff iC: nt
Collected By (signature):
Turnaround Date Regtttred:
Immediately Packed on Ice:
>
Samples Received on Ice � N NA
[ ) Yes [ ]NO
0
USDA RegulateedoSoil9pta)ala y N
Sample Disposal:
Rush:
Reld Rltered (if applicable):
Samples in Holding 'rime C-Ai Aft
I Dispose as approprtatr, ( 1 Return
[ ] Same Day [ ] Next Day
[ ]Yes ( [ No
0)
(n
O
Residual Chlorine Present
l I Arthive:
[ ] Z Day [ [ 3 Day [ ] 4 Day [ ] 5 Day
LU
V
V
LL
❑
V
Cl stxiP3: _
Sample pf1 Acceptable ta0
[ )Hold:
(Ex���,gesApply)
Analysis:
V
L7
_.l
>
U)
� 0_
Q
F""
Z
�
IPK Strips:
Matrix Codes (Insert in Matrbt box bekm):
Drinking Water (DW), Ground Water (GW), Wastewater (WW),
j=
Q
m
a
fi
Sul fide Present Y u
Product (P), Soh/Solid (SL), Oil (OLL Wipe (WPI, Air W), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
L~L1
Q
W
Q
O
O
Lead Acetate &trips:
Como /
collected (or
Composite End
Res
A of
V
Q
x
Q
LAB 7,e 3yLy
Customer Sample ID
Matrbt •
Grab
Composite Start)
Cl
Ctns
-4
J
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F-
LU
Y
Lab Sanipie i i Ca <mter t s: I'
Oats
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Date
Time
H
f-
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ILL
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i
Digester Sludge
WW
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8/25/20
8:00
1
X
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Digester Sludge
WW
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8/25/20
8:001
1
X
i
Digester Sludge
WW
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8/25/20
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1
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WW
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8125/20
8:001
1
X
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WW
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8/25/20
8:001
1
X
I
Digester Sludge
WW
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8/25/20
8:001
1
X
Digester Sludge
WW
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8/25/20
8.001
1
X
Digester Sludge
WW
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8/25/20
8.00
1
X
Digester Sludge
WW
G
8/25/20
8:00
1
X
Digester Sludge
WW
G
8/25/20
8:00
1
X
Customer Remarks / Special Cortftorts/ Possiible Hazards:
TypeoliceUseck Blue Dry Norse
SHORT HOLDS PRESENT (S72 hours)! Y <2> N/A
LAB Sample Temperature info:
r
Packing Material Used:
8
Lab 4:
8
Temp aIaoB Re • /P �i
Therm Cooler1. I1 e)
Cooler Temp Upon Receipt;
�• /�Fj�y�,71.7rt-(�,L�'
/?
�
Samples received via:
Cooler 1 Teem Corr, Fact CC
I
1 Corrected Temp. r C
Radchem sample(s) screened 1<500 epm): Y N NA
FEDl7f llP5 Client Courier a Dotter
Cooler
Rellnqu y {Signature}
Date/Time:
Received d is lure)
Date/Time- !?p
MTfL iA13 USE ONLY
Zj zu
�'�
Table #:
Relinquished by/Company: (5 nature)
Dat /lime:
Received by/C Ignat re)
Date/nme:
ACctnum.-
Trip Blank Received: Y N NA
Template:
HCL McOH TSP Other
I—
Prelogin:
Relinquished /Company:{Signature)
Datef0me: (k);".
ivedj�co a Signature)
r1 sL
D /}Time:
PM,
Non Conformance(s):
page:
0
tJ
`�V�� yq
Ps -.YES
I NO
nf:
CHAIN -OF -CUSTODY Analytical Request Document
a
ceA/lalytical
Chain -of -Custody is a LEGAL DOCUMENT - Complete all rekvent fields
Company- Town of Boiling Springs Billing Information:
Address: PO Boar 1014 Bolling Springs NC M17 PO Box 103A Boiling Springs NC 29011
Report To: Mike Glbert
Copy To. Todd.Humphries@boiiingspringsnc.net
Customer Project Name/Number.
Phone:70"34-2357
ErnalL
Collected By (print):
TODD HUMPHRIES
Collected By )signature)",
ID If:
se Order # :
#:
ound date Require&
LAB USE ONLY- Affix Workorder/Login Label Here or List Pate Workorder Number or
MTJL Log -in plumber Here �
ALL SHADED AREAS are for LAB USE ONLY 9
Container Preservative Type " Lab Project Manager.
M To: mike.gibert@boilingspringsnc.net
"• Preservative Types: (2) nitric add, (2) sulfuric add, 01 hydrochloric acid, (4) sodium hydroxide, (S) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (6) ammonium sulfate.
Collection JnWAddresv Town of Bolling Springs WWTP
(Cj ammonium hydroxide, (0) TSP, (U) Unpreserved, (0) Other
kford Road Shetby NC 28152
Analyses
Lab ProflieAine:
e: County/City: Time Zone Collected:
Lab Sample 3s
NC / Cleveland PT MT CT x ET
[ ) [ l [ l l [
L
a?
�
_
N
ntteckliet:
Cust«fp5eals Fresenri;nCdct Y N
Present,
Custody; S_gnatures Prfsen:t N
Compliance Monitoring?
[ X ] Yes ( ]NO
p
7Jtt Collector Signature Present lHA
U
Z
Bottles Intact: ti HA
Correct eactles N NA
DW PWS ID q:
DW Location Code:
3
1
i'
TV
E
Q
C1J
Sufficient Volume v it KA
9ampir5 Ra_e.lued on Toe N Nei
Immediately Packed on Ice:
>
VOA _ Headapace Acceptable N
( lYes ]No
O.
P
USDA Reulat.00 5o4a
m
C%
(y1t.
Sample Disposal: flush: Field Filtered (if appllcablel: %J g ? ro samples in Y.old.ng Time tm
( ] Dispose as appropriate I I Return [ ] Same On [ ] Next Day ( 1 Yes ] ) No O m C Residua 1 Cn1,or.n� i'rasent '.' K
1 I►+ehi,ra [ 12 Day [ 3 nay [ ] 4 Day [ 15 Day c E — o c Strips:
1 am: ? (q N +- p Sample pH Rtcttptable Y
]HN
[ExWlteCliargesApply) Anat0s: it) E .` pH Stripe:
• Matrix Codes (Insert In Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), _ c E Q Z 5ulEida kxesent Y rt
3 m - Q C Lead Acetate Strips;
Product (P). Soll/3olid (SL), Oil (OL). Wipe (WP), Air {AR}, Tissue (TS), Bioassay (B), Yapor (y), Other JOT) E Lo C
Comp / CoFlected (ar Composite End Res # of c ` 2 e E o Lab USE ONLY,
A
Customer Sample ID MaMx' Grab CampostteStart) CI Ctns M 0 4a o E tab Sample ai I cQoa�]snt"s7:
Date Time DaEe Time a - U Z (L U) Q I
:DlaesterS[ucke WW I G 1 1 8/25/20 8:00 1-1 X001
Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: ]fdgti Blue Dry None
ALL results must be reported 10 MgJKfor SAR. We. #
Pdd ing Material Used:
do need the 5AR calculation.
—1 .ne '* . / [ ! , Jn
Radchem aample(s) screened 1c500 cprn): Y N NA
ul�
pang: (Signature)
n
IRT HOLDS PRESENT (c72 hours): Y
Tracking th
mples received via:
FEDEX UPS C€lent Courier !
Date/Tirrpe: MTJL
G r1. Table #:
N/A LAB Sample Temperature Info. Tome EID#. lied f
♦N
Therm SDjI:
Cooler 1 Temp upon Receipt:
Cooler 1 Therm Corr. factlac
Cooler 1 Corrected Tamp:l6
Trip Blank Received: Y N
HCL McOH TSP Other
Pretogin:
PM:
PEI:
)ate/Time:
ed / aturel
We��
Date/Time:
F0 rU7
Non Contorrn"s):
YES / fNOI�
Page'
o'i f: ��
!2'eAnalytical'
mparty: Totem of Boiling Springs
CHAIN -OF -CUSTODY Analytical Request Document I LABUSE ONLY- Afflu Workorder/Login Label Here or List Pace Workorder Number or
MTX Login Number Here
dress: PO Box 1014 Boiling Springs NC 28017
port To- Mike Gibert
py To: Todd.Humphries@bollingspringsnc.net
st rner Project Name/Number.
Is a LEGAL DOCUMENT • Complete all relevant fields
lilting Information: ALL SHADED AREAS are for LAB USE ON Y
10 Box 1014 Bailing Springs NC 28017 _
Container Preservative Type'* Lab Project managew'
:mall To: mike.gibert0bofNngsrpringsnc.rM
'• Preservative Types: (1) nitric add, (2) sulfuric acid, (3) hydrochloric and, (41 sodium hydroxide. {51 zinc acetate.
die Collection Info/Address: Town of Boiling Springs WWTP (51 methanol,17) sodium bisulfate, (9) sodium thiosutfate, (9) hexane, (AI ascorbic and, (B► ammonium sulfate,
toddord Road Shelby NC 28LS2 (Cf ammonium hydroxide, (DI TSP. IV) UnpreServed, 10) Other
Analyses Lab Profife/Llne:
'Mate: County/City: Time2oneCnlletYed: Lab Sample Receipt Checklist:
NC / Cleveland [ IPT [ )MT [ la XIE7
Dne: 704-434-M7
Site/Fati(lty ID N
Compliance Monitoring?
Custody Seats PrNaent/lritaat. t N
Custody Signatures Present Y !rw
sail:
[ X ) Yes [ ] No
Collector Signature Present N ltA
Bottles intact ti HA
Correct Battles N 3!A
Itected By (print):
PtadraseOrder 0:
DWPWSIDM;
DDHUMPHRIES
Quote A:
DW Location Code:
sufficient volume
Samples -Received on Ice
Itected By (signature):
Turnaround Date Required:
Immediately Packed on Ice:
I ] Yes [ ]NO
-
dA - tiesdspace, Acc ptablo Y N'
DR Regulated Soils ? N R
ripleDisposal:
Rush:
Field Flltered
(if appllcable):
mplos in Holdl:x$ Time(► H NA
Dispose as appropriate ( l Itelinn
[ J Same Day [ ] Next Day
( [ Yes [ )No
sidual Chlorine Prauent 7 ,00
Archive:
[ 12 Day [ 13 Day 1 14 Day [ ] 5 Day
Strips:
Hold:
(E■ped"Charges Apply)
Analysis:
0
f
le PH Acceptable Y N I
pH 5t:ips:
Sulfide Present Y x,t
4atrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
roduct (P), Soi1/Solld (SLI, Oil (OL), Wipe (WP), Air (AR), Time (TS), 81loassay (B), Vapor (V), Other (OT)
Lead Acetate Strips;
Comp /
Collected (or
Composite End
Res
d of
LRB GSF OULT Y:
torSampklD
me
Matrix'
Grab
Composltestart)
CE
Ctns
=,
lab B Cr�nmaeta:
Date I Time 1 Date I Time
gester5ludge WW G
,comer Remarks / Special Conditions / Posslbie Hazards: Type of Ice used:
ore is no "Digested Sludge HI(Y' sample due to lack of Packing Material
Gies and we were able to combine two samples in one
lection bottle. Reactluity report in mg/l, Corrosivity in
io�e
Slue Dry None
& Ignitabilty in deg/f �. Radchem samples) screened 1<5M cpm): Y N NA
i fished by/Com :{5ignature) Date me: Rec!, � a lgnature)
Yr 2.>
li(qulshed by/Company: (Si ture) I Date/Time: Received by ev: I anaturel
0 w
(Signature)
SHORT HOWN PRESENT (s72 hours) : Y UN/A
Lab Tracking p:
Samples received via:
FEDEX UPS Client Courier tfaceCoor
Date/71me: TJL LAB USE ONLY
rC1�il r� Table q:
LAB Sample Temperature Info:
Temp Blank R v 4 N )
Therm ID#:
Cooler 1 Temp Upon Receipt:
Cooler 1 Therm Carr. Factpnc
Cooler 1 Corrected Temp:ff
Ccmffi9nts:
ite/rime; Acctnurn: Trip Blank Received: Y N *
Template: HCL McOH TSP Other
Prelogiw
ite/Time: PM: Non Confer eels[ ipage-
� t PB: YES '/ N !of:
Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 08/25/2020
Reported: 08/27/2020
For: Town of Boiling Springs
Comments: Geometric Mean: 13.736 MPN/g
STATESVILLE
ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
200825-14-01
Fecal Coliforms
DS1
62500
MPN/g
SM92210E-2006
08/25/2020
MD
200825-14-01
Percent Solids
DS1
1.44
%
SM2WB-2011
08/25/2020
MD
200825-14-02
Fecal Coliforms
DS2
11806
MPNIg
SM92210E-2006
08/25/2020
MD
200825-14-02
Percent Solids
DS2
1.44
%
SM2WB-2011
08/25/2020
MD
200825-14-03
Fecal Coliforms
DS3
3449
MPN/g
SM92210E-2006
08/25/2020
MD
200825-14-03
Percent Solids
DS3
1 45
%
SM2WB-2011
08/25/2020
MD
200825-14-04
Fecal Coliforms
DS4
16783
MPN/g
SM92210E-2006
08/25/2020
MD
200825-14-04
Percent Solids
DS4
1.43
ado
SM254OB-2011
08/25/2020
MD
200825-14-05
Fecal Coliforms
DS5
20408
MPN/g
SM92210E-2006
08/25/2020
MD
200825-14-05
Percent Solids
DS5
1 47
%
SM2WB-2011
06/25/2020
MD
200825-14-06
Fecal Coliforms
DS6
9028
MPN/g
sM92210E-2006
08/25/2020
MD
200825-14-06
Percent Solids
OS6
1 44
%
SWWB-2011
08/25/2020
MD
200825-14-07
Fecal Coliforms
DS7
11724
MPN/g
sM9221cE-2006
08/25/2020
MD
200825-14-07
Percent Solids
DS7
1.45
%
SM25408-2011
08/25/2020
MD
Respectfully submitted,
�).Q WOL,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 ptagge 10 of 13
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CHAIN -OF -CUSTODY Analytical Request Document LM USE OHtY- AM. Wa40rdaJL0pm LAW Hen or List Pace Wolkankr Wv bn or
MTIL Loa -in Number Here
Cha1n-01-Cu90dr ,S a LFGAi DOCUMENT • Cgmpiale aA reft"M fields
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End
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itllM
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lltester Sludge #1
ligester Sludge Ill
WW
G
8/25/20
6:00
WW
G
8/25/20
6:15
%gester Sludge 03
WW
G
8/25/20
6:30
ligester Sludge 04
W W
G
8/25/20
6:45
)igester Sludge #5
WW
G
8125/20
7:00
„tester Sludge 06
WW
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8/25/20
7.15
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8/25/20
7.30
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Town of Boiling Springs
Land Application of Residual Solids
Tanker truck and spreader used (19ft. X 600ft. Approx) 11,780 gal acre or 3.8 foads acre
Year: Z
Weather Volume
soil i
�- LO Catio condition 1 condition gallons� �
�F?rstll�;i �®
PATHOGEN & VECTOR ATTRACTION
REDUCTION FORMS
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boiling Springs WQ Permit Number: WQ00183352
WWTP Name: Town of Boiling Springs WWTP NPDES Number: NCO071943
Monitoring Period: From 1/1/2020 To 12/31/2020
Pathoeen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑ T
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑ 1
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
Alternative I El I
Alternative 2 ❑
If applicable to alternative
performed (Class B
only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑ 1
Air Drying❑
Composting [I
Aerobic Digestion F]
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech
ni ue
Mininut
Geo. Mean
aximu
Units
Fecal Coliform
? x 10 to the
6th power
per gram of
total solids
MPN
3449
13736
62500
MPN/g
0
7/year
Grab
SM9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
All.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) J
Alt. 9 (Injection) ❑
AIt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ 4*1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Gibert / Public Works Director Todd Humphries / Wastewater Supervisor
Preparer Name and Title (type or print) Land Ap/pliier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)
Annual Pathogen and Vector Reduction Summary
Town of Boiling Springs permit # WQ0018352
2020
Fecal Coliform - Class B
There were seven (7) test results provided by Pace Analytical Services in Huntersville.
The calculated Geo Mean for the Fecal Coliform samples was 13736 MPNIg.
Vector Attraction Reduction
Option 4 - Sour test results are reported in the attached data showing seven (7)
test results at 1.23 mg Oxygenlglhr or less for Specific Oxygen Uptake Rate.
End temperature for each test result was under 30 Degrees Celsius and the percent
solids were under 2% for each result.
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
1)
4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin s,NC
W 00018352
8/25/20
26
8/25/20
Todd Humphries
/25/2020 r 6:00:00 A
Todd Humphries
300
1.44
26
24
0.1
5.1
1.0
milliliters
Yo Dry Solids
Degrees Celsius
Degrees Celsius
4.24 mg Oxygenlhr
0.98 mg Oxygenlg/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rater 0.77 mg Oxygenig;hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
M 2 3 4 5 6 7
Circle Test 4
PH
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
P
n S rin s,NC
018352
25/20
25
8/25120
Todd Humphries
8/25/2020 6:15
Todd Humphries
300
1.44
25
25
0.1
6.1
1.0
milliliters
Dry Solids
degrees Celsius
degrees Celsius
6.77 mg Oxygenlhr
1.57 mg Oxygen!glhr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.23 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 (2) 3 4 5 6 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature.
Sampling Date/Time
Sam pled By.
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/0
ki
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
P
rin s,NC
018352
5/20
27
8125/20
Todd Humphries
8/25/202016:30:00 AM
Todd Humphries
300
1.45
27
25
0.1
5.6
1.0
milliliters
Yo Dry Solids
jegrees Celsius
Degrees Celsius
3.83 mg Oxygen?hr
0.88 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.66 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 (3) 4 5 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name.
Biosolids Permit Number
Date
Digester Temperature.
Sampling DateJime.
Sampled By
Analysis DatelTime
Analyzed By
Sample Volume.
Total Solids
Beginning Temperature.
End Temperature
Dissolved Oxygen Level
(mg/1)
4.65
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin s,NC
W Q0018352
8/25/20
27
8/25/20
Todd Humphries
8/25/20 / 6:45 AM
Todd urn ries
300
.4
27
25.0
0.1
5.6
1.0
milliliters
Yo Dry Solids
legrees Celsius
Degrees Celsius
4.25 mg Oxygen/hr
0.99 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.74 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.
1 2 3 (4) 5 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name.
Biosoiids Permit Number
Date
Digester Temperature
Sampling DatelTime.
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling Sprin s,NC
W Q0018352
8/25/20
26
8/25/20
Todd Humphries
81 51 017:15AM
Todd Humphries
300
1.47
26
25.0
0.1
5.5
1.0
milliliters
Dry Solids
Degrees Celsius
Degrees Celsius
3.74 mg Oxygen/hr
0.85 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 (5) 6 7
Circle Test #
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time.
Analyzed By
Sample Volume
Total Solids.
Beginning Temperature
End Temperature
Dissolved Oxygen Level
5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Boiling S rin s,NC
W Q0018352
8/25/20
27
8/25120
Todd Humphries
8125/20 17:30 AM
Todd Humphries
300
1.44
27
26.0
0.1
5.6
1.0
n illiliters
Yo Dry Solids
legrees Celsius
legrees Celsius
3.31 mg Oxygenlhr
0.77 mg Oxygenlglhr
27 degrees Celsius
0.71068133
Temperature Corrected Specific Oxygen Uptake Rate:,, 0.54 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 (6) 7
Circle Test #
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number
Date.
Digester Temperature.
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
5.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
niters
)ry Solids
rees Celsius
rees Celsius
0.0
5.6
1.0
2.07 mg Oxygen/hr
0.48 mg Oxygen/g/hr
27 degrees Celsius
0.71068133
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr
lnstructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
1 2 3 4 5 G (7)
Circle Test #
SOIL ANALYSIS REPORT
Page 1 of 1
Report Number: 20-275-0557
Account Number: 11769
Send To: Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kincfey Ave
Huntersville NC 28078
•
Waypoint.
ANALYTICAL
"Every acre... Every year." -
SOIL ANALYSIS REPORT
Date Received: 10/01/2020 bate Ot Analysis: 10,'02,2020 Date Of Report: 10/26/2020
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Grower: Workorder: 92498087
Analytical Method(s): Mehhoi 3 SMP Buller pH Loss Qn 19nilion Water pH
HM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
%
Soil
Ibs1A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
PH
Index
meg11009
meg1100g
JP ft1 Field
21583
2.0
139
156 VH
160 VH
258 H
1169 M
15 VL
6.6
6.88
0.5
9.0
NC=130
NC-82
JP V Field
21584
1.8
126
259 VH
259 VH
265 VH
M
13 VL
6.8
6.91
0.2
8,3
NC=216
NC=132
11027
1
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO,N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
msr'cm Rate
JP #1 Field
4.6
23.9
64.9
0.7
5.6
16 M
10.3 VH
19 M
5.5 VH
10 M
NC = 33
NC = 257.5
NC = 119
NC = 275.0
JP #2 Field
8.0
26.6
61.9
0.7
2.4
16 M
10.3 VH
16 M
4.4 VH
0.7 M
1
1
1
NC = 33
NC = 257.5
NC = 100
NC w 220.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), 1. (Low). M (Medium)
H (High), VH (Very High). ENR . Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
o_
A
Explanation of symbols: Samples
% (percent), ppm (parts per million).1brJA This report applies to sarnplels) tested. Saes aye retained a
(pounds per acre), mslcm {milli -mhos per centimeter), meq+100g maximum of thirty days after tasting.
(milli -equivalent per 100 grams). Conversions: ppm x 2 - lbVA, Soluble Analysis pfepared by: Waypoint Analytical Virginia, Inc.
Salts msrcm x 640 = ppm.
by: 1f1( %QD w�I
Pauric Mc Groary Ph.DL, CPAg
i
-_ aceArralytrcal
Company: Town of Boiling Springs
CHAIN -OF -CUSTODY Analytical Request Document `p`a"3' W�� : g2498VS7 member°` �__.
0
N
N I
Address: PO Box 1014 Bolling Springs NC 28017
Report To: Mike Gibert
Copy To: Todd.Humphries@bollingspr(ngsnc.net
ier Project Name/Number:
70"34-2357 Site/Facility 1D N:
Is a LEGAL DOCUMENT - Complete all relevent fields 11111111111111111111111111Billing information: d
PO Box 1014 Boiling Springs NC 28017 92498087
COnuji.--
Email To: mike.gibert@boilingspringmc.net
" Preservative types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
Site Collection Info/Address: Tom of Bolling Springs WWTP (5) methanol, 171 sodium Bisulfate, (B) sodium thlosulfate, (9) hexane, (A) ascwhic acid, (B) ammonium sulfate,
Rockford Road Shelby NC 29152 (C) ammonium hydroxide, (0) TSP, JU) Unpreserved, (0) Other
Lab Profllei/1.4w.
State: Count /Ci Time Zone Collected: Ana#yses
y ty' Lab Sample Receipt: Checkli:;t,
NC / Cleveland I I PT MT CT I R I ET Custody Seals Present/Intact Y tith
Compliance Monitoring? I Custody Signatures Present cZ N NA
[ X ] Yes ( ] No Ce-liector Signature Present (T�t4 KA
Wlected (print):
81' (p )
Purchase Order# :
DW PWS ID #,
Bottleact N +act
Correct Ss�tilea CrNfan
Corr Correct
TODDHUMPHRIES
Quote#:
DW Location Code:
Suffirienc tiulume ODN vat
Samples Received on Ice tD N NA
Collede4 By (sib tur�
Turnaround Date Required:
Immediately Packed on Ice:
d
VoA - Headspace Acceptable Y N 1n
]Yes NO
USDA. Regulated Soils Y@2NA
$=plea in Holding Time (ESN NA
Stimple Disposal:
Rush:
Reid filtered (if applicable):
[ ] Dispose as appropriate I ] Return
[ j Same Day [ ] Next Day
[ J Yes ( I No
16-
Residual Chicrine Present Y H ep
[ 1 Archive;
[ ] 2 Day [ 13 Day [ ] 4 Day [ 1 5 Day
a
'"
0)
Cl Strips:
[ ]Hold:
[Expedite Charges A
Analysis:
++
CL
U
W
to
U
pH Acceptable Y N E
pH Strips:
Sulfide Present Y k
• Matrix Codes (Insert in Matrix box below): Drinking Water (DWI, Ground Water [GW), Wastewater (WW),
Product (P), Soil/Solid (SL), 011 (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
CL
in
o
E
N
LHad Acetate Strips:
w
t0
Cl
C
M
=
E
LAB 178E ONLY:
Comp /
Collected (or
Composite End
Res
# of
Customer Sample ID
Matrix'
Grab
Cam sfte Start
Cl
Ctns
;5
N
C)
�
0
in
p
Lab Sample ! Comments:
Date
Time
Date
Time
m
e0
S 7
LLJ
C)
2
2 cc
C3
d
cn
[�J�
JP #1 Field
WW
G
1
X
X
X
X
X
X
X
X
X
X
ti
JP #2 Field
WW
G
�9 2p
1
X
X
X
X
X
X
I X
I X
I x
X
W L
Customer Remarks / Special Conditions / Possible Hazards:
�• FC.!`:: �•+�
Type of Ice Used: lllg�7 Blue
Dry None
SHORT HOLDS PRESENT (02 hours)
: Y (!� N/A
LAB Sample Temperature Info:
Theerimp Blank Received: Y N
Therm IOM: 9127ftf
Cooler 1 Tenp Upon Receipt:.OA C
Cooler 1 Thera Corr, Fectoz4%e,?C
Cooler 1 Corrected Tenp: -14roc
Comments,
Packing Material Used:
8
LabTracking#
Radchem sample(s) screened (<500cpm): Y N NA
Samples rmiyedvia:
FEDEX UPS Client Courier r
R qujsh ompry: ((Signature)
u
Date/Time:
-3o ZJ
Receiv y/ : {Signature)
batetTme.,
MT1L LAB USE ONLY
Table #:
Rel(n u ompan (Slgnature)
DateMme:
/Company: ( nature)
•�` 9'~'� 1
Date/Time:
C(
' t�D
Aectnum:
Template:
Prelogin:
PM:
PB:
Trip Blank Received: Y N 40
HCL McOli T5P Other
Relinquished by/Company: (Signature)
Datejrime:
Received try/Company: (Signature)
Date/Time:
felon Conformance ls);
YES / NO
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