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WQ0034468_Residual Annual Report 2020_20210223
Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* W00034468 Applicant/Permittee Brunswick County Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Wilmington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * Rob Willcox Email Address* rob@Wllcomabesoil.com Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363399128 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 IT Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0034468 Fbs Current Existing perm number Applicant/Permittee Address* Post Office Box249; Bolivia, N.C. 28422 Facility Name * Brunswick County DCAR Please provide comments/notes on your current submittal below. 2020 Annual Report for Brunswick County Distribution of Class A Residuals At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form} Engineering Rans, Specifications, Calculations, Bc.) 2020 CLASS A ANNUAL REPORT-WQ0034468-Brunswick 20.31 MB County.pdf Upload only 1 PCF docurrent (less than 250 M3). Miltiple docurrents must be combined into one R7F file unless file is larger than upload linit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature � wl� Submission Date 2/23/2021 2020 ANNUAL REPORT BRUNSWICK COUNTY PUBLIC UTILITIES DISTRIBUTION OF CLASS A RESIDUALS NON -DISCHARGE PERMIT NO. WQ0034468 Prepared For: Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231 B Summerfield Road Summerfield, North Carolina 27358 February 2021 willcox&mabe SOIL SOLUTIONS February 23, 2021 N.C. Department of Environmental Quality Division of Water Resources — Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Information Processing Unit Reference: 2020 ANNUAL REPORT Brunswick County Public Utilities Non -Discharge Permit No. WQ0034468 WMSS Project No. 15-04, Phase: 12 Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit for Brunswick County on behalf of Brunswick County. WMSS compiled this report using data provided by Brunswick County and BioGreen Services, Inc. This data includes: 1) Class A Annual Distribution and Marketing / Surface Disposal Certification and Summary Form, 2) Annual Residual Sampling Summary Form, 3) Annual Pathogen and Vector Attraction Reduction Form (503), and 4) Analytical Data. Brunswick County distributed a total of 1,044.11 Dry Tons of Biosolids under Permit No. WQ0034468 during the 2020 calendar year (West Brunswick Regional W WTP — 664.62 Dry Tons, and Northeast Brunswick WWTP — 379.49 Dry Tons). If there is any further information required or questions regarding this distribution program please do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations with Brunswick County Public Utilities at (910) 253-2485 or Rob Willcox with Willcox & Mabe Soil Solutions, PLLC at (336) 339-9128 for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC --� 1114z� Rob Willcox, L.S.S. Partner / Soil Scientist EnclOsure(S) cc: Brunswick County Public Utilities Shared\WMSS Projects12015\15-04 Brunswick County\Phase 12 - 2020 Annual Report\Class A12020 CLASS A ANNUAL REPORT- Brunswick County.doc Willcox & Mabe Soil Solutions, PLLC /7231 B Summerfield Road/ Summerfield, NC 27358 / Rob336.339.9128 or Martin 336.312.1396 /www.vwillcoxmabesoil.com Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 NC DISTRIBUTION OF CLASS A RESIDUALS PERMIT NO. WQ0034468 WEST BRUNSWICK REGIONAL WWTP PERMIT NO. WQ0023693 NORTHEAST BRUNSWICK REGIONAL WWTP NPDES PERMIT NO. NCO086819 Mr. Donald Dixon, Deputy Director of Wastewater Operations Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 (910) 253-2485 2020 West Brunswick Regional WWTP Dry Tons - 664.62 2020 Northeast Brunswick Regional WWTP Dry Tons - 379.49 Total Dry Tons 1,044.11 2020 West Brunswick Regional WWTP Dry Metric Tons 602.81 2020 Northeast Brunswick Regional WWTP Dry Metric Tons 344.20 Total Dry Metric Tons 947.01 TABLE OF CONTENTS SECTION NO. TITLE Class A Distribution and Marketing 1 Surface Disposal Certification Summary Form Form DMSDF II Annual Residual Sampling Summary Form Form RSSF III Annual pathogen and Vector Attraction Reduction Form (503 Rules) Form PVRF 503 1V Lab Sheets Analytical Data Class A Distribution and Marketing 1 Surface Disposal Certification Summary Form FORM DMSDF CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT # . WQ0034468 FACILITY NAME: West Brunswick Regional NVWTP PHONE: 9I0-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb - Wastewater Superintendent FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) 0 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes El No ❑ —► If No skip parts A, B, C and certify form below Part A*: �. Month I Sources(s) (include NPDES # if f applicable) January February March A ril Nlav June July August Sc tember October November WQ0023693 WQ0023693 Part B . Volume (dry tons) Recipient Information Residual In Product Out Name(s) Volume (dry tons) Intended use(s) 58.07 Albert Hughes 1 58-07 1 Fertilizer WQ0023693 12.45 Albert Hughes 12.45 Fertilizer WQ0023693 21.34 Harvey Bell 21.34 Fertilizer WQ0023693 41.79 T. Malsby 41,79 Fertilizer WQ0023693 74.38 Pearly Vereen 74.38 Fertilizer WQ0023693 17.66 D. Walters 17.66 Fertilizer WQ0023693 13.02 D. Watters 13.02 Fertilizer WQ0023693 22.09 C. Bullard 22.09 Fertilizer WQ0023693 15.02 Harvey 13e11 15.02 Fertilizer llecemuer I WQ0023693 7.95 C. Bullard 7.95 Fertilizer Total from FORA DMSDF (sup) 0 0 380.85 380.85 Totals: Annual (dry tons): 0 0 1 664.62 664.62 Amendment(s) used: 1 1 Bulking A =cnt(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total ?number of Form DMSDF (Supp)l 1 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well, "I certify, tinder penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imawing violations." Signature of Perrnittee Date Signature of Preparer"* Date (if different from Pcrmittcc) "Prepares is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26) DENR FORM DMSDF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0034468 FACILITY NAME: West Brunswick Regional WWTP PHONE: 9I0-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) F1 Distribution and Marketing (complete Parts A. and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January WQ0023693 1 23.45 Pearly Vereen 23.45 Fertilizer January WQ0023693 48.02 Clyde Galloway 48.02 Fertilizer April WQ0023693 19.56 Pearly Vereen 19.56 Fertilizer April WQ0023693 6.22 Harvey Bell 6.22 Fertilizer May WQ0023693 1.78 J. Tennant 1.78 Fertilizer May WQ0023693 9.78 Pearly Vereen 9.78 Fertilizer May WQ0023693 15.11 A. Vereen 15.11 Fertilizer May WQ0023693 14.22 E. Robinson 14.22 Fertilizer June WQ0023693 17.78 C. Sellers 17.78 Fertilizer June WQ0023693 28.45 D. Clemmons 28.45 Fertilizer July WQ0023693 50.20 Harvey Bell 50.20 Fertilizer July September WQ0023693 WQ0023693 13.02 26.03 T. Malsby A. Vereen 13.02 26.03 Fertilizer Fertilizer September WQ0023693 41.84 C. Hill 41.84 Fertilizer October October October November December WQ0023693 WQ0023693 WQ0023693 WQ0023693 WQ0023693 10.60 7.07 15.91 15.91 12.37 A. Hughes N. Applewhite Harvey Bell D. Little N. Applewhite 10.60 7.07 15.91 15.91 12.37 Fertilizer Fertilizer Fertilizer Fertilizer Fertilizer December WQ0023693 3.53 D. Little 3.53 Fertilizer Totals: Annual (dry tons): 0 0 380.85 380.85 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 DEN FORM DMSDF (Supp) (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0034468 FACILITY NAME: Northeast Brunswick Regional W WTP PI10N E: 910-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb - Wastewater Superintendent FACILITY TYPE: (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and fart C) H Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes El No ❑ —► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if AmcndAmendment/Volume (dry tons) Recipient Information applicable) Residual In Product Out Names) Volume (dry tons) Intended usc(s) Bulking; Aeent January NC0086819 4.00 Hany Hart 4.00 Fertilizer February NCO086819 15.00 J. Tcncnt 15.00 Fertilizer 11arch NCO096819 16.00 K. Knox 16.00 Fertilizer April NCO086819 25.61 IlarveyBell 25.61 Fertilizer May NCO086819 Fertilizer .lone NCO086819 10.25 A. Ciemmons 10.25 Fertilizer July NCO086819 7.83 T. Maultsby 7,83 Fertilizer August NCO086819 10.44 D. Watters 10.44 Fertilizer September NCO086819 1.74 C. Hill 1.74 FCrtlli7.er October NC0086819 8.42 R. Clemntons 8.42 Fertilizer November NCO086819 Fertilizer December NCO086819 16.85 C. Bullard 16.85 Fertilizer Total from FORM DMSDF (sup) 0 0 263.35 263.35 Totals: Annual (dry tons):1 0 0 379.49 379.49 Amendment(s) used: Bulkiiij, Aizent(s) used: * If more space is required. attach additional inibrmalion sheets (FORM DMSDF (supp)): Part C: Total Number of Form DMSDF (Stipp)j 1 Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items I-3 below) issued by the Division of Water Resources: ❑ No —a If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copiers of certified laboratory results are attached. 2. Ail operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received lion the Division of Water Resources. 3. No contravention ot'Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of lair, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Pennittee C Bate Signature of Prcparer** Date (if difforent from Permiltee) **Prcparcr is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'.I 102 (26) DENR FORM DMSDF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0034468 FACILITY NAME: Northeast Brunswick Regional WWTP PHONE: 9I0-253-2479 COUNTY: Brunswick OPERATOR: Tim Webb FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) F71 Distribution and Marketing (complete Parts A. and Bl Part A*• Part B*• Volume (dry tons) Recipient Information Sources(s) (include NPDES # if Amendment/ Name(s) Volume (dry Intended use(s) Month applicable) Bulking Agent Residual in Product Out tons) January NCO086819 45.01 Sonny Hart 45.01 Fertilizer January NCO086819 38.01 D. Little 38.01 Fertilizer Februay NCO086819 14.00 C. Sellers 14.00 Fertilizer February NCO086819 14.00 K. Knox 14.00 Fertilizer March NCO086819 15.00 J. Tenent 15.00 Fertilizer June NCO086819 6.15 A. Vereen 6.15 Fertilizer June NCO086819 20.49 T. Maultsby 20.49 Fertilizer July NCO086819 1138 R. Clemmons 11.38 Fertilizer July NCO086819 6.09 Pearly Vereen 6.09 Fertilizer September NCO086819 6.09 D. Watters 6.09 Fertilizer September NCO086819 18.34 R. Clemmons 18.34 Fertilizer October NCO086819 29.48 C. Bullard 29.48 Fertilizer December NCO086819 39.31 N. Applewhite 39.31 Fertilizer Totals: Annual (dry tons): 0 0 263.35 263.35 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l I DENR FORM DMSDF (Supp) (12/2006) Annual Residual Sampling Summary Form FORM RSSF ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0034468 Laboratory: 1) Environmental Chemists, Inc. Facility Name: Brunswick County 2) Residual Source WQ # or 3) NPDES ##: WQ0023693 4) WWTP Name: West Brunswick Regional WWTP 5) Residual Analysis Data Cone. Sample or Composite Date Parameter Limit (mg/kg) (nia/ka)' 03/11/20 04/22/20 07/08/20 10/07/20 Percent Solids (%) NA 4.12 3,28 3.43 3.26 Arsenic 75 10.2 14.5 18.9 16.0 Cadmium 85 6.04 14.5 9.83 14.5 Chromium NA 38.4 32.9 56.0 70.6 Copper 4,300 544 485 481 546 Lead 840 20.2 18.7 19.0 22.1 Mercury 57 I.5 0.97 0.659 0.675 Molybdenum 75 12.9 14.5 9.65 14.5 Nickel 420 23.5 2I.1 21.0 22.3 Selenium 100 6.04 14.5 9.65 14.5 Zinc 7,500 1,640 2,130 6,650 4,510 Total Phosphorus NA 72,500 52,100 4I,800 49,900 TKN NA 65,200 88,000 80,400 77,700 Ammonia -Nitrogen NA 36,700 50,900 37,700 44,300 Nitrate and Nitrite NA 108 160 151 160 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. 9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 3-tea f ignature ofPreparer * _ Date i�eliprer is deed-iii 40 CFR Pa�� 5a3.9(rj acid-15A NCAC' 2T . ] ] 02 (2f) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0034468 Laboratory: 1) Facility Name: Brunswick County 2) Residual Source IVQ0023693 3) NPDES # or WQ#: 4) WWTP Name: West Brunswick Regional 1ArWTP S) Residual Analvsis Data Environmental Chemists, Inc. Parameter (mg/kg) Aluminum Calcium Sample or Composite Date 03/11/20 04/22/20 07/08/20 10/07/20 35,200 25,500 17,300 31,200 24,300 24,600 1 23,500 30,600 Magnesium 4,270 4,700 3,990 5,060 p1l 8.00 8.67 8.47 8.60 Potassium 4,930 7,130 5,280 5,150 Sodium 2,180 2,230 1,950 5,090 SAR 0.69 0.62 0.57 1.28 " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date DEN FORM RSSF - B f 12/2006) *Pre parcr is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPD) S B: WWTP Name: Residual Analvsis Data WQ0034468 Brunswick County NCO0868I 9 Northeast Brunswick Regional WWTP Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. Parameter Conc. L,imi( Sample or Composite Date (mg/kg) (ing/kg)' 01/08/20 04/21/20 07/07/20 10/08/20 Percent Solids (%) NA 3.69 3.78 3.21 5.18 Arsenic 75 10.5 12.0 16-8 9.19 Cadmium 85 6.67 12.0 10.5 9.19 Chromium NA 70.5 39.4 38.0 25.7 Copper 4,300 358 202 211 181 Lead 840 19.9 12.0 10.5 10.1 Mercury 57 1.1 1.27 0.536 0.347 Molybdenum 75 14.7 I2.0 10.5 9.19 Nickel 420 44.2 23-3 23.1 15.6 Selenium 100 8.08 12.0 10.5 0.476 Zinc 7,500 1,840 1,340 1,360 1,040 Total Phosphorus NA 2,030 55,000 971 34,900 TKN NA 112,000 105,000 125,000 86,500 Anintania-Nitrogen 1 NA 57,900 75,100 73,500 46,400 Nitrate and Nittite NA 18.6 329 17.9 107 I . 1...4u..,.-F-L 40W1111Ua uiU LU11111K uuucUlluuuun 11inns usica to uns iorin al-e not applicable. KeWrence the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer r r Date e r *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102(26.) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in DORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analvsis Data WQ0034468 Brunswick County NCO086819 Northeast Brunswick Regional VAVTP Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. Parameter (ing/kg) Sample or Composite Date 01/08/20 04/21/20 07/07/20 10/08/20 Aluminum 11,000 6,030 6,980 5,540 Calcium 33,900 i9,500 21,400 18,900 Magnesium 9,020 6,240 5,890 6,220 pH 7.56 7.48 7.64 9.04 Potassium 32,100 18,800 16,900 10,700 Sodium 3,770 2,020 2,210 1,020 SAIL 0.90 0.62 0.62 0.59 9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ram, Signature ofPreparer * Date *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) Annual Pathogen and Vector Attraction Reduction Form - (503 Rules) FORM PVRF 503 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693 11'lonitoring Period: From 1/1/2020 To 3/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: f Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 I] Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic El Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B:-7 Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Number of Frequency Sample Analytical in Sludge Minit-nuir Geo. Mean Maxim Units Excee- of Analysis dences Type Tech-nique 2 x 10 to the MPhf 61h power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 40 41 43 MPN! 0 Quarterly Grab weight) Gram SM92210E i Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliforrn) weight) Vector Attraction Reduction (40 CFR 503-33) - Please Alt -I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilizmtion ❑ Alt. 9 (injection) ❑ Alt. 10 (incotpotation) ❑ MUMILe uprion performeu: Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) Aft 7 (Drying -Stable) ❑Alt. 8 (Drying - Unstable) No vector attraction reduction alternatives were nerformed CERTIFICATION STATEMENT (please check the appropriate statement) 1] "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." u "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check statement attach an explanation why you have not met one or both of the requirementc_1 "This determination has been made under my direction and supervision in accordance with the system designe! to ensure that qualified personnel properly gather and evaluate the information used to determine that the 25 pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." � Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Land plier a e and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number; WWTP Name: West Brunswick Regional WWTP NPDES Number: Monitoring Period: From 4/l /2020 To 6/30/2020 WQ0034468 WQ0023693 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ 1Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 EI Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic El Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: AIternative 1 ❑ Alternative 2 ❑ It applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density umber o Parameter g t3' Frequency Sample Analytical in Sludge Minima Geo. Mean Maximu Units Excee- of Analysis dences Type Teel, -pique 2 x 10 to the I MPN 6th power per gram of Fecal Coliform total solids CFiT 1000 mpn per gram of total solid (dry 50 53 S5 MPN/ 0 Quarterly Grab SM92210E weight) Cram. Salmone lEa bacteria 3 MPN per 4 grams (in lieu of Fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503,33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) El JAIt. 4 (Spec. Q, uptake) El Alt. 5 (I4-Day Aerobic) ❑ Alt. 6 (Aik. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an ex lanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent 06 0 f U Y1 Preparer Name and Title (type or print) Land A lier ame and Title (if applicable)(type or print) Signature of Preparer* Date Agnature Wof Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12120061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693 Monitoring Period: From 7/112020 To 9/30/2020 Pathogen Reduction (40 CFR 503,32) - Please indicate level achieved and alternative performed: ' Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 El Alternative 4 ❑ Alternative 5 El Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic El Seta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Signi Lime Stabilization ❑ Air Drying❑ Compost Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the Parameter Allowable Level Pathogen Density in Sludge Minimum Geo. Mcan Maximum Units 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFI 1000 mpn per gram of total solid (dry 52 54 56 MPN/ weight) Gram ntly Reduce Pathogens": ❑ Aerobic Digestion ❑ i i owing monitoring data: Limoumber o e- Frequency Sample Analvtical deuces of Analysis 'Type Tech -nique 0 I Quarterlyl Grab I SM9221'CE Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.] (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 0 Alt. 4 (Spec. OZ uptake) 0 Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt, S (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were nerformed ri CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach, an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including line and imprisonment." Tim Webb - Wastewater Superintendent f Q ir�t S Preparer Name and Title (type or print) Land pier ame and Title (if applicable)(typc or print) Si a - . lg�-I Signature of Preparcr* Date Si attire of Land A Iter if applicable) � pp (� pp ) Date' *Preparer is defined in 40 CFR fart 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQU034468 WWTP Name: West Brunswick Regional WWTI' NPI?ES Number: WQ0023693 Monitoring Period: From 10/1/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: tEAlternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ 1 Heat Drying ❑ I Heat Treatment ❑ Therniophilic Cl Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: I Alternative 1 If applicable to alternative pi Lime Stabilization ❑ Anaerobic Digestion ❑ If applicable to alternative Parameter Fecal CoIiform Allowable Level in Sludge 2 x 10 to the MPN 6th power per pram of total solids CFU W I Alternative 2 ❑ I Class 13 only) indicate "Process to Signific Air Drying❑ I Compostin€ A (Class A or Class B) complete the fo Pathogen Density nimuH Gco. Mean Maximo Units ntly Reduce Pathogens"% ElAerobic Digestion El owing monitoring data: amber of Exece- Frequency SampleiTech-ni4ue Anal ytic"I denccs of AnaIysis Type 1000 mpn per grain MPN/ of total solid (dry 528 557 595 I weight) Grand U Quarterly Grab SM92210E Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 0 Alt. 4 (Spec. O, uptake) El Alt. 5 (14-Day Aerobic) ❑ Alt. 6 {Ark, Stabilization ❑ Alt 7 (Drying -Stable) ❑Alt. $ (Drying -Unstable) El Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check thlls statement attach an explanation why you have not mct one or both of the requirements.) j "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent 1 K p � {S� � rt �1 Preparer Name and Title (type or print) Land A p}i r in and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date! *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: Monitoring Period: From 1/1/2020 To 3/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative perforn Cla A• Al ss temattve I ❑ Alternative 2 ❑ I Alternative 3 Alternative 4 0-1. Alternative 5 E I Alternative 6 WQ0034469 j NCO086819 to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": ❑I Heat Drying ❑ Heat Treatment ❑ Thermophilie El ❑ I Gamma Ray ❑ Pasteurization ❑ Class B: I AIternative I If applicable to alternative pt Lime Stabilization ❑ Anaerobic Digestion ❑ If applicable to alternative Parameter Fecal Coliform Allowable Level in Sludge 2 x 10 to the WIN 6th power per gram of total solids CFU 1000 mpn per gam of total solid (dry 1J I Alternative 2 ❑ Class B only) indicate "Process to Significantly Reduce Pathogens": Air Drying❑ I Composting ❑ Aerobic Digestion ❑ ,d (Class A or Class B) complete the following monitoring data: Pathogen Density Number a Excce- I Frequency Sample Ana inimunj Gco. Mean jMaxiniuUnits dences I ofAnalysisl Type ITCCII 483 I 502 I 518 I AMPN/ I 0 Gram Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate Grab I SM9221 Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) Cj Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying -Unstable) Alt. 9 (Injection) ❑ 1Alt. 10 (Incorporation) ET No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) C1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) i "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb-- Wastewater Superintendent 1 Preparer Name and Title (type or print) Land A 'er N to r►d Title (if applicable)(type or print) 01 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined is 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Dame: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: NCO086819 Monitoring Period: From 4/l/2020 To 6/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alterrative 2 ❑ Alternative 3 Alternative 4 ❑ Alternative 5 0 I Alternative 6 ❑❑ It applicable to alternative performed (Class A Compost ❑ Heat Drying ❑ Beta Ray ❑ Gamma Ray ❑ Class B: Alternative 1 ❑ If applicable to alternative performed (Class B Lime Stabilization ❑ ;estion ❑ to alternative nerfo Parameter Allowable Level in Sludge 2 x I0 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of Fecal total solid (dry Vector Attraction Reduction Alt.] (VS reduction) ❑ Alt. 5 (]4-Day Aerobic) ❑ Alt. 9 (Injection) ❑ 40 Air indicate "Process to Further Reduce Heat Treatment ❑ Pasteurization ❑ T- Alternative 2 indicate "Process to (Class A or rlace R) rmmntnto th.. Pathogen Density Minimu Geo. Mean Maximo Units 329 338 353 'MPN/ Gram 2FR 503.33) - Please indicate option aerl ilic El ntly Reduce Pathogens": ❑ lAcrobic Digestion ❑ owing monitoring data: Umber o Excee- Frequency Sampie denceti lufAnalysisl Type IT 0 ! Quarterly I Grab I SM9221 CE Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) El JAIt. 4 (Spec. O, uptake) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) Alt. 10 (Incorporation} ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am, aware that there are significant penalties for false certification including fine and imprisonment." Titre Webb - Wastewater Superintendent n ( oe�6 C. n S Preparer Name and Title (type or print) Land Ap ier Name and Title (if applicable)(type or print) Signature of Prepares* Date Signature of Land Applier (if applicable) Date *Prepares is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1 102 (26) ❑ENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: NCO086819 Monitoring Period: From 7/1f2020 To 9/30/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ ThermophiIic El Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: I Alternative 1 It applicable to alternative performed (Class 13 Lime Stabilization ❑ Air DrAnaerobic Digestion ❑ IL If applicable to alternative Derformed (C'la. Parameter Fecal Coliform Allowable Level in Sludge 2 x 10 to the MPN 6th power per gram of total solids Chit 1000 mpn par grant of total solid (dry Alternative 2 ❑ only) indicate "Process to Significantly Reduce Pathogens": mg❑ Composting ❑ jAerobic Digestion ❑ i i s A or Class B) complete the following monitoring data: Pathogen Density N er of Excee- Frequency Sample Analytical Geo. Mean Maximo Units dences of Analysis Type Tech-niquE 43 45 47 1 MPN/ 0 Quarterly Grab I S1,49221 CC Gram Salmonella bacteria 3 MPN per 4 gams (in lieu of fecal total solid (dry colifonn) weight) Vector Attraction Reduction (40 CFR 503.33) - Please Alt. I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt. 9 (Injection) ❑ Alt. 10 (hicorporation) ❑ Indicate option performed: Alt. 3 (30-day bench) El I Alt. 4 (Spec. O, uptake) ❑ Alt 7 (Drying - Stable) ❑ IAIL 8 (Drying - Unstable) ❑ No vector attraction reduction alternatives were perforated ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and impri onment." Tim Webb - Wastewater Superintendent Preparer Name and Title (type or print) Land Applier Nameand Title (if applicable)(type or print) Signature of Preparcr Date Si nature g of Land Applier (tf applicable} Date . *Preparer is defined in 40 CFR Part 503.9(r) and 1 5A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: NCO086819 Monitoring Period: From 10/I/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 El Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 i] Alternative 6 ❑ If applicable to alternative performed (Class A Compost ❑ Heat Drying ❑ Beta Ray ❑ Gamma Ray ❑ Class B: Alternative 1 ❑ If applicable to alternative performed (Class 13 Lime Stabilization ❑ I Air Dry applicable to alternative Parameter Fecal Coliform Allowable Level in Sludge 2 x 10 to the MPN 6th power per gram of total solids CFU 1000 mpn per gram of total solid (dry Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry eoliform) weight) indicate "Process to Further Reduce P Heat Treatment ❑ I Tl Pasteurization ❑ Alternative 2 indicate "Process to Class A or Class B) cox Pathogen Density lung Geo. Mean Maxima 325 I 336 I 353 tte the Units MPN/ Gram ntly Reduce Pathogens": ❑I Aerobic Digestion ❑ omber nwing monitoring data: u Excee- Frequency Sample A dences of Analysis Type T Grab I SM92210E I Vector Attraction Reduction (40 CFR 503,33) - Please indicate option performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) E] IAIt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ A1t 7 (DtyinQ - Stable) ❑ I Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system design to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." N. Tim Webb - Wastewater Superintendent �:Ln Preparer Name and Title (type or print) Lan lien a e and Title (if applicable)(type or print) Signature of Preparer* Date Signature oFLand Applier (if applicable) Date *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) Lab Sheets ANALYTICAL DATA BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 11, 2020 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 4.12 % Solids 8.00 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 6.520 65,200.000 130A00 Phosphorus 7.250 72,500.000 t45MO Potassium 0.493 4,930.000 9.860 PAN (injected)* 4.536 45,358.000 90.716 PAN (surface)* 2.701 27,008.000 54.016 Ammonia Nitrogen 3.670 36,700.000 73.400 Calcium 2.430 24,300.000 48.600 Calcium Carbonate Eq. --- --- --- Magnesium --- 4,270.000 8.540 Sodium --- 2,180.000 4.360 Sulfur --- ___ Nitrate N / Nitrite N --- 108.000 0.216 Barium --- --- --- SAR 0.69 Chloride --- ___ Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 35,200.00 70.400 Arsenic --- 10.20 0.020 75 Cadmium --- 6.04 0.012 85 Chromium --- 38.40 0.077 --- Copper --- 544.00 E088 4,300 Lead --- 20.20 0.040 840 Mercury --- 1.500 0.003 57 Molybdenum --- 12.90 0.026 75 Nickel --- 23.50 0.047 420 Selenium --- 6.04 0.0 t2 100 Zinc --- 1,640M 3.280 7,500 Envirochem: 2020-04194 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits for calculation purposes. West Brunswick WWTP WQ0034468 Class A -1st Quarter 2020 . x. mil....... 03/11/20 43 1.6335 03/11/20 41 1.6128 03/11/20 40 1.6021 03/11/20 42 1.6232 03/11/20 41 1.6128 03/11/20 41 1.6128 03/11/20 40 1.6021 Total 1 11.2992 Average 1 1.6142 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. eni v�rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way' Wilmington, NC 28405 a 910.392,0223 Lab a 910 392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252,473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax info, env ironmentalchen-dsts.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10318 Site: Sludge 3/11/2020 12:10 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Chlordane (TCLP) SW 646 Method 8081813510 <0.02 mg/L 03/19/2020 Endrin (TCLP) SW 846 Method 80BIB13510 <0.0005mg/L 03/19/2020 Heptachlor (TCLP) SW 846 Method 8081B13510 <0.0005mg/L 03/19/2020 Heptachlor epoxide (TCLP) SW 646 Method 8081 B135 10 <0.0005 mg/L 03/19/2020 Lindane (TCLP) SW 846 Method 8081 B135 10 <0.0005 mg/L 03/19/2020 Methoxychlor (TCLP) SW 546 Method 8081B13510 <0.0005 mg/L 03119/2020 Toxaphene (TCLP) SW 846 Method 8081 B1351 0 <0.05 mg/L 03/19/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,5-Trichlorophenol (TCLP) SW B46 method 827013510 <0.050 mg/L 03/20/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4-Dinitrotoluene (TCLP) SW 845 method 8270/3510 <0.050 mg/L 03/20/2020 Cresol (TCLP) SW 846 method 8270/3510 <0,050 mg/L 03/20/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2D20 Hexachloroethane (TCLP) SW 845 method 8270/3510 <0.050 mg/L 03/20/2020 m } p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Pentachlorophenol (TCLP) SW B46 method 8270/3510 <0,250 mg/L 03/20/2020 Pyridine (TCLP) SW 846 method 627013510 <0.050 mg/L 03/20/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0,003 mg/L 03/20/2020 2,4-D (TCLP) SW646 Method 8151A <0.003 mg/L 03/20/2020 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 1,2-Dichloroethane (TCLP) SW846 Method8260/5030 <0.01 mg/L 03/25/2020 Benzene (TCLP) SW846 Methcd 82601503E <0.01 mg/L 03/25/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Report #:. 2020�04194 Page 1 of 4 3- S ,?l eriviroc i . r ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 e 9:10.392,0223 Lab a 910.392.4424 Fax 710 Dowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 2.55-A Wilmington Highway, J7cksonville, NC 28540 a 9'10.347.5843 Lab/Fax info a;environnientaIchemists.con1 Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 03/25/2020 Tetrachloroethylene (TCLP) SW846 Method 826015030 <0.01 mg/L 03/25/2020 Trichloroethylene (TCLP) SVV846Method B26015030 <0.01 mg/L 03/25/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 RCI Cyanide EPA 335A 0.202 mg/kg 03/18/2020 Sulfide SM 4500 S p 2.50 mg/kg 03/31 /2020 Ignitability SW 846 method 1010 >180 °F 03/27/2020 Sludge Residuals Aluminum EPA200.7 35200mglkg 03/16/2020 Arsenic EPA 200.7 10.2 mg/kg 03/12/2020 Cadmium EPA 200.7 <6.04 mg/kg 03/12/2020 Calcium EPA 2007 24300 mg/kg 03/12/2020 Chromium EPA 200.7 38Amg/kg 03/12/2020 Copper EPA 200 7 544 mg/kg 03/12/2020 Lead EPA2001 20.2 mg/kg 03/12/2020 Magnesium EPA 200.7 4270 mg/kg 03/12/2020 Molybdenum EPA 200.7 12.9 mg/kg 03/12/2020 Nickel EPA 200.7 23.5 mglkg 03/12/2020 Potassium EPA 200.7 4930 mg/kg 03/12/2020 Selenium EPA 200.7 <6.04 mg/kg 03/12/2020 Sodium EPA 200.7 2180 mg/kg 03/12/2020 Zinc EPA 200.7 1640 mg/kg 03/12/2020 Nitrate+Nitrite-Nitrogen EPA353.2 108mg/kg 03/23/2020 Total Solids (%) SM 2540 B 4.12 % 03/12/2020 pH SM 4500 H 8 8.00 units 04/02/2020 Ammonia Nitrogen SM 4500 NH3 C 36700 mg/kg 03/15/2020 Total Kjeldahl Nitrogen (TKN) SM 45DO Erg B 65200 mg/kg 03/15/2020 Report #:; 2020.04194 Page 2 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392. 442-4 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252,473.5702 Lab/Fax 255-A Mh-nington Hi htvay, Jacksonville, NC 28540 + 9'10.347.584; Lab/Fax in fo([lvcnvit-onn1c[ILL ICl7eIII ists-coIII Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Total Phosphorus SM 460a P F 72500 mg/kg 03/27/2020 Mercury SW84674718 1.50mg/kg 03/13/2020 TCLP Metals Arsenic EPA 2007 <1.0 mg/L 03/19/2020 Barium EPA 200.7 <1.0 mg/L 03/19/2020 Cadmium EPA200.7 <1.0mg/L 03/19/2020 Chromium EPA200.7 <1.0mg/L 03/19/2020 Lead EPA 200.7 <1.0 mg/L 03/19/2020 Selenium EPA 200.7 <1.0 mg/L 03/19/2020 Silver EPA 200.7 <1.0 mg/L 03/19/2020 Mercury EPA 245.1 <0.0002 mg/L 03/19/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10319 Site: 1 3/11/2020 12:01 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids {%) SM 2540 D 4.20 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <43 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10321 Site: 2 3/11/2020 12:02 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.46 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10322 Site: 3 3/11/2020 12:03 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4 52 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPN/g 03/11/2020 Report #:. 2020-04194 Page 3 of 4 Environmental Chemists, Inc, 6602 Windmill Way, Wilmington, NC 28405 O 910.392.0223 Lab e 910.392.4421 Fax 710 Bows,rtoivn Road, klanteo, NC 27954 c 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonvilie, NC 28540 • 91.0.347.5843 Lab/Fax inib iCL�cnvironmenEitichemists.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO ##• Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10323 Site: 4 3/11/2020 12:04 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.31 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <42 MPN/g 03/11 /2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10324 Site: 5 3/11/2020 12:05 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.44 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10325 Site: 6 3/11/2020 12:06 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids SM 2540 B 4.49 % 03/12/2020 Fecal Density SM92210E=MPN 24hr503 <41 MPN/g 03/11/2020 Lab 1D Sample ID: Collect Date/Time Matrix Sampled by 20-10326 Site: 7 3/11/2020 12:07 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 254o a 4,53 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPN/g 03/11/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: Report #:: 202o-04194 Page 4 of 4 6nvironrinental Chemist, Inc., Wiirnington, 1NC Lab #94 5602 Windmill Way ,'Vilmington, %C 28405 ? 10-392,02Z3 5ample Receipt Checklist Client: C Plh Date::. 0 Report•Number: C`- Receipt of sample; Defrvered O YES ❑ NO y/A UPS ❑ fedEx ❑ Other ❑ 0 YES Cl No 1• Were custody seals present on the cooler? N/A 2. if custody seals were present, were they intact/ Original temperature upon receipt —l'C unbroken? How temperature taken; Corrected temperature upon receipt 1R Gun ID: Thomas Traceable S/O192S11557ture Blank against Battles 14 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6'C RIGun `was Project M 0 YES ❑ NO 4. Were proper custody 1 8 /C1A notified? I YES dY procedures (relinquished/received] followed? ❑ NO 5. `Were sample ID's Ilsted on the COC7 YES Cl NO 6. 'Nere samples ID's listed on sample containers? ! YES ❑ NO 7, Were collection date and time l11�isted an the COC? �? YES ❑ NO 8. Were tests to be rformed listed on the CC)C? YES: ❑ NO 9. Ed samples arrive en proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? SZ YES ❑ NQ 11. Was adequate sample volume available?` 6Q YES ❑ NQ 1Z, Were samples received within proper holding time for requested tests? ❑ YES ❑ No 13. Were acid preserved samples received at a pH of <27 • sts. ❑ YES 0 v0 14. Were p 0 YESyanide sam Ies received at a pH >12? Cl❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/T1cN/Phenol received at a chlorine residual of <0.5 rn L? - ❑ YES ❑ NCl 17. Were Sulfide/Cyanrde received at a chlorine re i / • s dual of ' TOC/Volatiles are QH checked at time of anafvsis and recorded on the benchsheet. 9acteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet Sample Preservation: ,;lrfust be completed for any samples) incorrect) Samples) Y preserved or with headspace) ,vere received incorrectly preserved and were adjusted accordingly by adding (circle one): H'so E Time of preservation: a NO' ICI NaOH f more than one preservative is needed, notate n comments below Note: Nonfy customer service ;mmediatel for ir, Y Carrectiv oreserved samp,es. Obtain a new 5amol --)m otlfv the state lab if directed to analvred by the customer Who was n of f#ed. care and time e or Volatiles Sample(s) •vere received with headspace .�.,C..�n.iitjL ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Sample Collection and Chain of Custody Wilmington, NC 28405 Phone: (9I0) 392-0223 Fax (910) 392.4424 Client: Brunswick Co Public Utilities WEST BRUNSWICK REGIONAL Collected By: Brian Blanton Report No: - Ll (`t`f Sample Type: I = Influent, E = Effluent, W =Well, ST=Stre_am, SO =Soil, SL= Slud2e Other: a PRESERVATION Collection Sample Identification ANALYSIS REQUESTED .a z DATE Cn TIME TEMP v t = w L 0 WBR WBR WBR WBR WBR WBR WBR WBR TRIANNUALS t031 9 SL SL SL SL x x x C C G CE L C G SL SL Y SL SL C C� x x x CJ C G rP —c P C EL C G P G C G P G G Transfer Relinquished By: Date/Time Received By: 2. 7LE. Temperature when Received: L4 _ Accepted: Rejected; Resample Requested: Delivere B.. _ Received By:fe,C Date: c, ()L— Time: : -?a �-- TCLP, Nutrients, metals, RCi FECAL DENSITY FECAL DENSITY FECAL DENSITY FECAL DENSITY FECAL DENSITY FECAL DENSITY FECAL DENSITY Date/Time tt- Cl � I 1 Brunswick County public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab a 910392.4424 Fax 710 Bowsertown Road, Manteo, NC 27994 a 252.473.5702 Lab/Fax 235-.A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax infold environrnentalchernists.com Date of Report: Mar 16, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10319 Site: 1 3/11/2020 12:01 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Fecal Density SM 9221C E MPN 24 hr 503 <43 MPNIg 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10321 Site: 2 3/11/2020 12:02 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Fecal density SM 9221C E MPN 24 hr 503 <41 MPN1g 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10322 Site: 3 3/11/2020 12:03 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Fecal Density SM 9221C E MPN 24 hr 503 <40 MPNIg 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10323 Site: 4 3/11/2020 12:04 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Fecal Density SM 9221C E MPN 24 hr 503 e42 MPN/g 03/11/2020 Lab ID 20-10324 Test Sample ID: Site: 5 Collect DatelTime 3/11/2020 12:05 PM Method Matrix Sampled by Solid/Sludge Brian Blanton Results Date Analyzed Fecal Density SM 9221 G E MPN 24 hr 503 <41 MPN/g 03111 /2020 Lab ID 20-10325 Test Sample ID: Site: 6 Collect Date/Time 3/1112020 12:06 PM Method Matrix Sampled by Solid/Sludge Brian Blanton Results Date Analyzed Fecal Density u :�9221C E MPNI2 , �' h502 <ta nenkii n"J4 AInnnn �y t Mr-Imrg v'Jr 1 ircv,cu Report*:: 2020-04194 Page 1 of 2 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Lab ID Sample ID: 20-10326 Site:7 Test Fecal Density Comment: Reviewed by, Environmental Chemists, Inc. 6602 Windmill V1ray, Wilmington, NC 28405 e 910.392.0223 Lab a 91.0.392,442.4 Fax 710 Bowsertown Road, Manteo, NC'_7954 m 292.473.5702 Lab/Fax 25:5-A Wilmington Highway, Jacksonville, NC 285,40 e 910.347.58 43 Lab/Fax in fL)(q,?environmenialelierni,;ts, corn Date of Report: Mar 16, 2020 Customer PO M. Customer ID: 08100011 Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Collect DatelTime Matrix Sampled by 3/11/2020 12.07 PM Solid/Sludge Brian Blanton Method Results Date Analyzed SM 9221C E MP 24 hr 503 <40MPN/g 03111/2020 Report #:: 2020-04194 Page 2 of 2 ENVIRONMENTAL, CHEMISTS, INC 6602 Windmill Way qi w Sample Collection and Chain of Custody Wilmington, NC 28405 1'lione: (910) 392-0223 Fax (910) 392.4424 Client: Brunswick Co Public Utilities WEST BRUNSWICK REGIONAL Collected B Brian Blanton Re ort No: Sample Tyne: I = Influent _E_ = Effluent, W =Well, ST =Stream, SO =Soil, S.L-- Sludge Other: a ... PRESERVATION w Collection Sample Identification r o = Q o w o ANALYSIS REQUESTED o o Li ° P Z DATE TIME TEMP U U -- �' y w T W.13R �031 g SL' ' X TCLP, Nutrients, metals, RCI 3-11-'2a G_ WBR {031 g SL C X FECAL DENSITY �-�t.7,o �;�} G WBR SL C .P X FECAL DENSITY G WIM SL C ' X FECAL DENSITY WBR SL C X FECAL DENSITY G WBR SL C X FECAL DENSITY WBR Lo SL C P FECAL DENSITY WBR SL C —��P—T x FECAL DENSITY G C P G G C P G G TRIANNUALS Transfer Relinquished By: Date/Time Received By: Date/Tithe I.Lx�,.� 2. Temperature when Received: 4-t> Accepted: Rejected: Resample Requested: By: Received By. Deiivere Date: 31t, 1,P— Tizne: - i? County of Brunswick Public Utilities �A,,,�AAotia! West Brunswick Regional Facility Laboratory A'onh Carolina Liboraim y Cerlificalion Number: NCO0903 Anna JeRoux, Lab Supervisor 110 Box 249 235 Grey Water Road Tclephonc: 910-253-2896 anna.leroux brunswickcoun nc. ov Bolivia, NC 28422 Supply, NC 28462 Fax: 910-755-7927 Report Date: 29-Apr-2020 SampleT ` Satnwle Date Test & Me HOW West _ Brunswick Thirty Day Bench Beginning: 3/11/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 4/13/2020 as Required to Meet Option 3 4,19% WWTP EPA [503.33(b)(3)] PASS Certified by: End of Report) �it .< Anna IeRoux, Laboratory Supervisor BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 22, 2020 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.28 % Solids 8.67 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry To (Mg/Kg x 0.002) Nitrogen (TKN) 8.800 88,000.000 176.000 Phosphorus 5.210 52,100.000 104.200 Potassium 0.713 7,130.000 14.260 PAN (injected)* 6.219 62,190.000 124.380 PAN (surface)* 3.674 36,740,000 73.480 Ammonia Nitrogen 5.090 50,900.000 101.800 Calcium 2.460 24,600.000 49.200 Calcium Carbonate Eq. --- ___ --- Magnesium --- 4,700.000 9.400 Sodium --- 2,230.000 4.460 Sulfur --- --- Nitrate N / Nitrite N --- t60.000 0.320 Barium --- --- --- SAR 0.62 Chloride --- _ _ Iron --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 25,500.00 51.000 Arsenic --- 14.50 0.029 75 Cadmium --- 14.50 0.029 85 Chromium --- 32.90 0.066 --- Copper --- 485.00 0.970 4,300 Lead --- 18.70 0.037 840 Mercury --- 0.970 0,002 57 Molybdenum --- 14.50 0.029 75 Nickel --- 21.10 0.042 420 Selenium --- 14.50 0.029 100 Zinc --- 2,130.00 4.260 7,500 Envirochem: 2020-06687 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. West Brunswick WWTP WQ0034468 Class A - 2nd Quarter 2020 PM-:.:...:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.::. 04/22/20 54 1.7324 04/22/20 55 1.7404 04/22/20 51 1.7076 04/22/20 53 1.7243 04/22/20 50 1.6990 04/22/20 52 1.7160 04/22/20 54 1.7324 Total 1 12.0520 Average 1.7217 Geometric Mean €€.5.€...`. Fecal Coliform MPN 1 gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. ANALYTICAL & CONSULTING CHEMISTS : nvironmen.tal Chemists, Inc. 6602 Windmill Wav, 1Nilalingtnn, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bo vsertown Read, Manteo, NC 77954 % 252 473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28,940 0 9L0.347.5843 Lab/Fax info@environiuentrilchemisls.cum Brunswick County Public Utilities Date of Report: May 07, 2020 Post Office Box 249 Customer PO ##: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-06687 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16477 Site: Sludge 4/22/2020 10:26 AM Solid/Sludge Client Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 25500mglkg 05/04/2020 Arsenic EPA200-7 <14.5mg/kg 04/30/2020 Cadmium EPA 200.7 <14.5 mg/kg 04/30/2020 Calcium EPA 200.7 24600 mg/kg 05/04/2020 Chromium EPA 200.7 32.9mg/kg 04/30/2020 Copper EPA 200.7 485 mglkg 0413012020 Lead EPA 200.7 18.7 mg/kg 04/30/2020 Magnesium EPA 200.7 4700mg/kg 04/30/2020 Molybdenum EPA 200.7 <14.5 mg/kg 04/30/2020 Nickel EPA 200.7 21.1 mglkg 04/30/2020 Potassium EPA 200.7 7130 mg/kg 04/30/2020 Selenium EPA 200.7 <14.5 mg/kg 04/30/2020 Sodium EPA 200.7 2230mg/kg 05104/2020 Zinc EPA 200.7 2130 mg/kg 04/30/2020 Nitrate+Nitrite-Nitrogen EPA353.2 160mg/kg 04/2712020 Total Solids SM 2540 B 3.28 % 04/23/2020 PH SM 4500 H B 8.67 units 04/29/2020 Ammonia Nitrogen SM 4500 NH3 C 50900 mg/kg 04/24/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 88000 mg/kg 04/24/2020 Total Phosphorus SM 4500 P F 52100 mg/kg 04/2912020 Mercury SW646 7471 B 0.9700 mg/kg 04/29/2020 Report V 2020-o6667 Page 1 of 3 1 ` -Environmental .armlets, Inca 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab 6 910.392.4424 Fax sM; 710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax 255-A Wslminaton Flighwav, Jacksonville, NC 28540 ' 910.347.5843 Lah/Fax ANALYTICAL & CONSULTING CHEMISTS info(c'tcn� ironmLnt �.lcl�emisfs.com Brunswick County Public Utilities Date of Report: May 07, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-06687 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-16478 Site: #1 4/22/2020 10:27 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%} SM 2540 B 3.36 % 04/23/2020 Fecal Density SM 9221C E MPN 24 hr 503 <54 MPNIg 04/22/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16480 Site: #2 4/22/2020 10:28 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (°to} SM 2540 a 3.29 % 04/23/2020 Fecal Density SM 9221C E MPN 24 hr 503 <55 MPN/g 04/22/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16481 Site: #3 4/22/2020 10:29 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.54 % 04/23/2020 Fecal Density SM92210EMPN 24hr503 <51 MPN/g 04/22/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16482 Site: #4 4/22/2020 10:30 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) Fecal Density Lab ID Sample ID: 20-16483 Site: #5 Test Total Solids (%) Fecal Density SM 2540 s 3.46 % 04/23/2020 SM 9221C E MPN 24 itr 503 <53 MPNIg 04/22/2020 Collect Date/Time Matrix Sampled by 4/22/2020 10:31 AM Solid/Sludge Client Method Results Date Analyzed SM 2540 6 SM 9221 C E MPN 24 hr 503 3.61 % 04/23/2020 <50 MPNIg 04/22/2020 Report #:: 2020-06687 Page 2 of 3 Environmental Chemists, Inc. 40®r,5 6602 Windmill WaNI, Wilmington, NC: 2S405 a 910.392.0223 Lab a 9111.392,=4424 Fax 710 Sowsertown road, Mznteo, NC 2795�4 a 252.�473.5702 Lab/Faux ;11 255-AL17ilmington Highway, Jacksonville, NC 285-10 e 910.347,5843Lab/Fax ANALYTICAL_ & CONSULTING CHEMISTS info(ir cnvirollmentalellcmists.com Brunswick County Public Utilities Date of Report: May 07, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-06687 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16484 Site: #6 4/22/2020 10:32 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.50 % 04/23/2020 Fecal Density SM 9221C E MAN 24 hr 503 <52 MPN/g 04/22/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-16485 Site: #7 4/22/2020 10:33 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 254o B 3.38 % 04/23/2020 Fecal Density SM 9221C E MPN 24 hr 503 <54 MPN/g 04/22/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: Report #:: 2020-06687 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392 0223 � � Sample Receipt Checklist Client',j' �EC A. _ Dated a /�() Re o p rt Number. Receipt of sample. Deiivere ❑ YES ❑ NO UPS ❑ FedEx ❑ Other ❑ N/A 1• Were custody ❑ seals present on the Cooler? YES ❑ NO N/A 2. 0 custody seals were present, were they intact/unbroken?Original temperature upon receipt p How temperature Laken: C Corrected temperature upon receipt QC ❑ Temperature Blank IR Gun ID: Thomas 'traceable S/N 192521657 Against Bottles ❑ YES ❑ NO IR Gun Correction Factor -C: 0.0 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custod YES ❑ NO 5p11 y procedures (relinQuished/received] followed? S. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COL? YES ❑ NO B. Were tests to be performed listed o11 n111 the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume availaole?' ® YES C] NO 12. Were samples received within proper holding time far requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of c2?' © 'ES 0 NO 14. Were cyanide samples received at a pH a12? Cl�10❑ YES ❑ NO 15. Were sulfide samples received at a pH a9? 3=Y YES ❑ NO 16. Were NH3/'TKN/phenol received at a chlorine residual of cp.5 m/L? •• ES ❑ NO 117. Were Sulfide/Cyanide recewed at a Chlorine residual of <0.5 m/L? TOC/volatlies are pH checked at time of artaNsis and recorded on the benchsheet. " Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample preservation: (Must be completed for any sample(s) incorrect! Sample(s) V preserved or with hsadspace) were received incorrectly preserved and were adjusted accordingly by adding (circle one): HzSO' HfV03 HCI NaOH Time of preservation: if more than one preservative is needed, notate in Comm Note: i"Oufv customer service Immediately for inCorrec h Preserved ents below samples. Obtain a new sample ar notify the state lab if directed toanaly=ed by the customer. Wha was notified, date and time: Volatiles 5ample(s) were received with headspace COMMENTS: --------------------------------------------------------------------------------------------------------------------- r•r1P n w nn� ENVIRONMENTAL CHEMISTS, .INC 6602 Windmill Way t Sample Collection and Chain of Custody Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4424 Client: Brunswick Co Public Utilities WEST BRUNSWICK REGIONAL Collected BY: Brian Blanton Re ort No: )--'3� r. Sample Type:_ I.= Influent, E _ Effluent, W =Well, ST =Stream,, SO =Soil, SL= Sludge x W CollectionCL - PRESERVATION Sample Identification J. 1. E c" e C, o p � p w ANALYSIS REQUESTED .a 4 DATE TIME TEMP U U a U x x z H o WBR .� 10.�� { SL SL SI, C X X � Nuts Tents, metals, FECALDGNSITY FECAL DEiVSITY ,--z2-u' �� �-'1- C WI3R -- WBR t�� J6 q � c� C G f' G WBR WBR 1 j 1 `�'2 i u2� SL SL C X X FECAL DENSITY FECAL DENSITY -t-L CJ -3� C G %i. .z C c WBR ff t � t�-31 SL SL C X FECALDEN51'rY FECAL DENSITY ��i Z- C G WBR f (AT, LR- �Z-zr G WBR 5- k03 3 NV SL C C12. FECAL DENSITY dp C G P G C G P� G G a .1at'a1 � 1 ■ V M l..rf] Transfer Relinquished By: Date/Time Rece' ;ed By. 1 Date/'Time t�`�� 2. Temperature when Received: 5 . it-, Accepted: I� , '` I Rejected: kesanive 'T Requested: Delivered,By: - - Received By: WKC,�,� County of Brunswick Public Utilities yQ CAR West Brunswick Regional Facility Laboratory North Carolina Laboratory Certification Number: NCO0903 Anna IeRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone: 910-253-2896 aleroux(@,brunsco.net Bolivia, NC 28422 Supply, NC 28462 Fax: 910-755-7927 Report Date: 5/22/2020 �[ ample Tyne Test -& Method Results West Brunswick Thirty Day Bench Beginning: 4/22/2020 Reduction of Vector Attraction (c15% is considered passing) Regional Digestor Scale Test Ending: 5/21/2020 as Required to Meet Option 3 2.08% WWTP EPA [503.33(b)(3)] PASS (End of Report) Certified by: Brian Blanton BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled. July 8, 2020 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.43 % Solids 8.47 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 8.040 80,400.000 160.800 Phosphorus 4.180 41,800.000 83.600 Potassium 0.528 5,280.000 10.560 PAN (injected)* 5.066 50,661.000 101.322 PAN (surface)* 3,181 31,811.000 63.622 Ammonia Nitrogen 3.770 37,700.000 75.400 Calcium 2.350 23,500.000 47.000 Calcium Carbonate Eq. --- --- --- Magnesium --- 3,990.000 7.980 Sodium --- 1,950.000 3.900 Sulfur ___ ___ Nitrate N / Nitrite N --- 151.000 0.302 Barium Chloride .-- Iron --- --- Aluminum --- 17,300.00 34.600 Arsenic --- 18.90 0.038 Cadmium --- 9.83 0.020 Chromium --- 56.00 0.112 Copper --- 481.00 0.962 Lead -- 19.00 0.038 Mercury --- 0.659 0.001 Molybdenum --- 9.65 0.019 Nickel --- 21.00 0.042 Selenium --- 9.65 0.019 Zinc --- 6,650.00 13.300 Envirochem: 2020-11217 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application; (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 0.57 Ceiling Coneen. (Mg/Kg) 75 85 4,300 840 57 75 420 100 7,500 West Brunswick WWTP WQ0034468 Class A - 3rd Quarter 2020 07/08/20 55 1.7404 07/08/20 54 1.7324 07/08/20 56 1.7482 07/08/20 53 1.7243 07/08/20 52 1.7160 07/08/20 53 1.7243 07/08/20 55 1.7404 Total 1 12.1259 Average 1 1.7323 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Eenvirocu]he]m ANALYTICAL &, CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Glenn Walker Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 iiowsertown ]load, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info;r environmentalchemists.com Date of Report: Jul 23, 2020 Customer PO #: Customer ID: 08100011 Report M 2020-11217 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28216 Site: ATAD Tank #4 7/8/2020 11:00 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) 5M 2540 6 3.29 % 07/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <55 MPN/g 07/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-28217 Site: ATAD Tank #4 7/8/2020 11:01 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.39 % 07/0812020 Fecal Density SM 0221C EMPN 24 hr 503 <54 MPN/g 07/0812020 Lab 1D Sample ID: Collect DatelTime Matrix Sampled by 20-28218 Site: ATAD Tank #4 7/8/2020 11:02 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.24 % 07/08/2020 Fecal Density SM 9221 C E MPN 24 hr 503 <56 MPNIg 07/0812020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28219 Site: ATAD Tank #4 7/8/2020 11.03 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) 5M 2540 B 3.40 % 07/08/2020 Fecal density 5M 9221C E MPN 24 hr 503 <53 MPNIg 07/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-28220 Site: ATAD Tank #4 7/8/2020 11:04 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.50 % 07/08/2020 Fecal Density SM 0221 C E MPN 24 hr 503 <52 MPNIg 07/08/2020 Report k* 2020-11217 Page 1 or 3 [envirochern ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Sox 249 Bolivia NC 28422 Attention: Glenn Walker Environmental Chemists, Inc. 5602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Date of Report: Jul 23, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-11217 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Daterrime Matrix Sampled by 20-28221 Site: ATAl3 Tank #4 7/8/2020 11:05 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.42 % 07/08/2020 Fecal Density SM0221C E MPN 24 hr503 <53 MPN1g 07/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-28222 Site: ATAD Tank #>!4 7/8/2020 11:06 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.31 % 07/08/2020 Fecal Density SM 0221C E MPN 24 hr 503 <55 MPNIg 07/08/2020 Report Ja': 2020-11217 Page 2 of F""W, It Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab + 910.392.4424 Fax - 710 Bowsertown RDad, Mantea, NC 27954 a 252.473.5702 Lab/fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention; Glenn Walker Date of Report: Jul 23, 2020 Customer PO #: Customer ID: 08100011 Report #• 2020-11217 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-28223 Site: ATAD Tank #4 7/8/2020 10:50 AM Solid/Sludge Kyle Price Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 17300mglkg 07/14/2020 Arsenic EPA 200.7 18.9 mglkg 07/14/2020 Cadmium EPA200.7 <9.83mg/kg 07/14/2020 Calcium EPA 200.7 23500 mg/kg 07/14/2020 Chromium EPA 2007 56.0mg/kg 07/14/2020 Copper EPA 200 7 481 mg/kg 07/14/2020 Lead EPA 200.7 19.0 mg/kg 07/14/2020 Magnesium EPA200,7 3990mg/kg 07/14/2020 Molybdenum EPA 200.7 9.65 mg/kg 07/14/2020 Nickel EPA 200.7 21.0 mglkg 07/14/2020 Potassium EPA 200.7 5280 mg/kg 07/16/2020 Selenium EPA 20a.7 <9.65 mg/kg 07/14/2020 Sodium EPA 200.7 1950mg/kg 07/14/2020 Zinc EPA 200.7 6650 mg/kg 07/1412020 Nitrate+Nitrite-Nitrogen EPA353.2 151 mg/kg 07/20/2020 Total Solids (%) 5M 2540 9 3.43 % 07/08/2020 pH SM 4500 H 8 8.47 units 07/13/2020 Ammonia Nitrogen SM 4500 NH3 C 37700 mg/kg 07/11 /2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Org 8 80400 mg/kg 07/11/2020 Total Phosphorus SM 4500 P F 41800 mglkg 07/15/2020 Mercury SW645 74718 0.6590 mg/kg 07/1412020 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: ! iJu Report #:: 2020-11217 Page 3 of 3 Environmental Chemist, inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Recei t Checklist Client:Fzw Ls icr_ tiW_ Date: a Report Number: - 1 `7 Receipt of sample: Delivere UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? 12. ❑ YES 113 NO N/A If custody seals were present, were they intact/unbroken? Ori final temperature upon receipt YJ 'C Corrected temperature upon receipt 'C How temperature taken; ❑ Temperature Blank V Against Bottles tR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project M r./—QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the CDC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES 13 NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO IT Did samples arrive in proper containers for each test? YES ❑ NO 110. Did samples arrive in good condition for each test? YES ❑ NO il. Was adequate sample volume available?' tV YES ❑ NO 12. Were samples received within proper holding time for requested tests? 13 YES ❑ NO 13. Were acid preserved samples received at a pH of 42? • CJ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES 13 NO 15. Were sulfide samples received at a pH >9? Cl YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? " ❑ YES 11 NO 17. Were Sulfide/Cyanide received at a chlorine residual of e0.5 m/L? E3 YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet, '• Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Samplels] were received incorrectly preserved and were adjusted accordingly by adding (circle one): HzSO. HNO3 HCl NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab it directed to analyzed by the customer. who was notihed, date and time, Volatiles Sample(s) were received with headspace COMMENTS: DOC, e% .002 COUNTY OF BRUNSWICK West Brunswick Regional Laboratory Public Utilities Department 235 Grey Water Road Wastewater Treatment Division Supply, NC 28462 Phone: 910-755-7921 Fax: 910.755-7927 Sample Collection and Chain of Custody Collected By: Kyle Price Report No.: 1 ?i'n — Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other, Sample IdenUfleaflon ATAD 4 WSR ATAD 4 WBR Collection 71anwo 1100 63'C Vai'2020 11:01 631C Sample Type SL SL Composite a Grab Container {ptasUc or Glass} P G C7 P ATAD 4 WBR ATAD 4 WBR ATAD 4 WBR ATAD4 WBR ATAD 4 WBR 63-C 63-C 63'C 63'C 63'C 631G 1 SL SL SL SL SL SL P 7IM020 11:02 r7 P 71W2020 11:03 G P P 7/8/2020 11:04 G P P 71M020 11:05 G — VM020 11;06 G _ ATAD4 WBR 71WO20 10:50 G Chlorine LAB ID m9& NUMBEI 0 0 �r111g 0 +� 0 ANALYSIS PRESERVATION REQUESTED t NONE HCI Ha50a HNO, TRIO OTHER X i Fetal Density % Fecal Density X Fecal Density % I Fecal [ten X Fecal Density X Fecal DenaLay % Feral Densr! X Nu(,irn�yMp}�ay % ~olds ATTENTION: Samples submitted for analysis for Ammonia, TKN, Cyanide, Phenol and all Bacleriologicals must be dechlodnaied to :5 0.2 ppm at lima of collection. Transfer Relinquished By: Date/Time Received By: DatefTime 1 O?* `2( 110DLo iIOa 2 3n��114-v —r Temperature when Received: L f • ( Accepted- jJ Rejected Required: 0quirtM; Delivered By, TZ;R Comments: "K�County of Brunswick Public Utilities y��TNCAN O; West Brunswick Regional Facility Laboratory North Carolina Laboratory Certification Number. NCO0903 Anna leRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone; 910-253-2896 anna.leroux(a7brunSWlckcountync.00y Bolivia, NC 28422 Supply, NC 28462 Fax: 910-755-7927 E Sample Tvne West Brunswick Thirty Day Bench Regional Digestor Scale Test WWTP Beginning: 8/13/2020 Reduction of Vector Attraction Ending: 9/12/2020 as Required to Meet Option 3 EPA [503.33(b)(3)] (End of Report) Certified by: ,'" Anna leRoux, Laboratory Supervisor Report Date: 15-Sep-2020 (<15% is considered passing) 5.37% PASS BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 7, 2020 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.26 % Solids 8.6 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 7.770 77,700A00 155.400 Phosphorus 4.990 49,900.000 99.800 Potassium 0.515 5,150.000 10.300 PAN (injected)* 5,448 54,480.000 108.960 PAN (surface)* 3.233 32,330.000 64.660 Ammonia Nitrogen 4.430 44,300.000 88.600 Calcium 3.060 30,600.000 61.200 Calcium Carbonate Eq. --- --- Magnesium --- 5,060.000 10.120 Sodium --- 5,090.000 10.180 Sulfur --- --- Nitrate N / Nitrite N --- 160.000 0.320 Barium --- --- --- SAR 1.28 Chloride --- --- --- Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 31,200.00 62.400 Arsenic --- 16.00 0.032 75 Cadmium --- 14.50 0.029 85 Chromium --- 70.60 0.141 --- Copper --- 546.00 1.092 4,300 Lead --- 22.10 0.044 840 Mercury --- 0.675 0.001 57 Molybdenum --- 14.50 0.029 75 Nickel --- 22.30 0.045 420 Selenium --- 14.50 0.029 100 Zinc* Re -Test --- 4,510.00 9.020 7,500 Envirochem: 2020-1713 5 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. West Brunswick WWTP WQ0034468 Class A - 4th Quarter 2020 11/04/20 595 2.7745 11/04/20 528 2.7226 11/04/20 554 2.7435 11/04/20 561 2.7490 11/04/20 548 2.7388 11/04/20 558 2.7466 11/04/20 554 2.7435 Envirochem: 2020-18 83 9 Total 1 19.21$5 Average 2.7455 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Environmental Chemists, Inc. 5602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCaenvironmentalchemists.com Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Donald Dixon Date of Report: Nov 02, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-17135 Project ID. WSR WWTP Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-43781 Site: Sludge 10/7/2020 10:43 AM Solid/Sludge Joshua Cavenaugh Test Method Results Date Analyzed Total Solids SM 2540 8 3.26 % 10/07/2020 Sludge Residuals Aluminum EPA 200.7 31200 mglkg 10/12/2020 Arsenic EPA 200.7 16.0mglkg 10/12/2020 Cadmium EPA200.7 <14.5mg/kg 10/12/2020 Calcium EPA 200.7 30600 mglkg 10/12/2020 Chromium EPA 200.7 70.6mg/kg 10/12/2020 Copper EPA 200.7 546 mg/kg 10/12/2020 Lead EPA 200.7 22.1 mglkg 10/12/2020 Magnesium EPA 200.7 5060mglkg 10/12/2020 Molybdenum EPA 200.7 <14,5 mg/kg 10/12/2020 Nickel EPA 200.7 22.3mglkg 10/12/2020 Potassium EPA 200.7 5150mglkg 10/12/2020 Selenium EPA 200.7 <14.5 mglkg 10/12/2020 Sodium EPA 200.7 5090mglkg 10/16/2020 Zinc EPA 200.7 r6s-T 8530 mglkg 10/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 41516 160 mg/kg 10/09/2020 pH SM 4500 H B 8.60 units 10/13/2020 Ammonia Nitrogen SM 4500 NH3 C 44300 mg/kg 10/08/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 77700 mglkg 10/13/2020 Total Phosphorus SM 4500 P F 49900 mglkg 10/13/2020 Mercury SW8467471B 0.6750mglkg 10/30/2020 Report N.: 2020.17135 Page I of 3 Environmental Chemist, Inc., Wilmington, NC Late #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, INC 28405 910.392.0223 Client: IA.nSu0I CLCU k o Date: I L Z(D Report Number: Zc— i —� 6s Receipt of sample: EgHEM Pickup Client Delivery ❑ UPS ❑ Fed Ex ❑ Other ❑ ❑ YES I0 NO 10 N/A 11. Were custody seals present on the cooler? ❑ YES 10 NO PT N/A r 12, If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Cor ected temperature upon receipt °C How temperature taken: _ ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Cnrr;rtinn Pat-mr. °r . n n ❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? ❑ NO 6. Were samples Us listed on sample containers? LYE ❑ ❑ NO NO 7. Were collection date and time listed on the COC? S. Were tests to be performed listed on the COC? YES YES ❑ ❑ ❑ NO NO NO 9. Did samples arrive in proper containers for each test? 10. Did samples arrive in good condition for,each test? 11. Was adequate sample volume available?' ❑ YES YES ❑ ❑ NO NO 12. Were samples received within proper holding time for requested tests? 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ ❑ ❑ YES YES YES ❑ ❑ ❑ NO NO NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Vofatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 ENVIRONMENTAL CHEMISTS, INC 4= Sample Collection and Chain of Custody Client: �� w� ��C Cam. Collected B 651 C_ vex ,7 v • , 7 77 v- - kamnip Tvne! I = Inflvient- R = F.fflnent- W =Wp L CT=CtriPgm_ QdI =finil_ Ai = C1as (lihnr• 6602 windmill way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4424 .(ter .. PRESERVATION a Collection a Mo 9 v Sample Identificatiou zS o e a A. ? Wz o 0 O ANALYSIS REQUESTED d o DATE TIME T1 MP 3 v c W 5ua�-r,}Jl� 43 St- C Z) laSvl;�i ,��S�a� ris 10 Lr� G i4 (13 -7 5 L C x FC- 7v n s L45 0 G t� 5 L c t) k 13 4 (0 G [S 43 C k 4�-213 G Is LI 3 7 S L C X } c=. "�- v o ZI G s u3iglo C [I� k ��.-�� aft (11dG << 41 $'7 C G 4ti Li318$' S C V�.`�-20 Ids i UG G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. j U/7/2-r>2P 2. i emperature when Receive `i. Accepted:V— Rejected-.— ResMnple Requested: Delivered By:- Received By: e� _ Date: iv Time: 7-10p -- Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax ' 710 Bowsertown Road, Manteo, NC 27954 0 252,473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Brunswick County Public Utilities Date of Report: Nov 06, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-18852 Project ID: Lab ID Sample ID: BCPU Collect DatelTime Matrix Sampled by 20.47982 Site: ATAD #3 WBR 11/4/2020 10:05 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 7300 mg/kg 11/05/2020 Total Solids (%) SM 2540 a 3.22 % 11/05/2020 Lab ID Sample ID: BCPU Collect DatelTime Matrix Sampled by 20-47988 Site: SNDR Nke - �ST� 11/4/2020 10:00 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 4510 mg/kg 11/05/2020 Total Solids (%) SM 2540 B 1.72 % 11/05/2020 Lab ID Sample 1D: BCPU Collect DatelTime Matrix Sampled by 20-47989 Site: GBT Belt 11/4/2020 1:20 PM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 5210 mg/kg 11/05/2020 Total Solids (%) SM 2540 B 5.07 % 11/05/2020 Lab ID Sample ID: BCPU Collect DatelTime Matrix Sampled by 20-47990 Site: GBT SupernMe 11/4/2020 1:21 PM Water Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 552 ttg/L 11/05/2020 Lab ID Sample 1D: BCPU Collect DatelTime Matrix Sampled by 20-47991 Site: CS Inf 11/4/2020 10:20 AM Water Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 150pg/L 11/05/2020 Report.:: 2020-18e52 ���-6Page 1 of 2 r- Environmental Chemists Inc. 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL& CONSULTING CHEMISTS info@environmentalchemists.com Brunswick County Public Utilities Date of Report: Nov 06, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-18852 Project ID: Lab ID Sample ID: BCPU Collect Date/Time Matrix Sampled by 2047992 Site: OIB fnf 11/4/2020 10:21 AM Water Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 106 pg1L 11/05/2020 Lab ID Sample ID: BCPU Collect Datefrime Matrix Sampled by 20-47993 Site: WBR Inf 11/4/2020 10:22 AM Water Michael Garrity Test Method Results Date Analyzed Zinc EPA 2007 332 pg/L 11/05/2020 Lab ID Sample ID: BCPU Collect DatefTime Matrix Sampled by 2047994 Site: Oak Island PS Inf 11/4/2020 10:23 AM Water Michael Garrity Test Method Results Date Analyzed Zinc EPA 200.7 299 pg/L 11/05/2020 Comment: Reviewed by: Reparl ft,: 2020-10652 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392,0223 Sample Receipt Checklist Client:Su Date: Report Number: Receipt of sample: ECHEM Pickup Client Delivery -©---UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO 0 N/A 11. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 12, If custody seals were present, were they intact/unbroken? Original temperature upon receipt . S °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank tZ Against Bottles iR Gun ID: Thomas Traceable SIN 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. if temperature of cooler exceeded 6°C, was Project Mgr_/QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? OZ YES ❑ NO 5. Were sample 1D's listed on the CDC? CX YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ ND 7. Were collection date and time listed on the COU YES ❑ NO 8. Were tests to be performed listed on the COU JR YES I0 NO 1 9. Did samples arrive in proper containers for each test? YES JE1 NO 110. Did samples arrive in good condition for each test? YES ❑ NO Ill. Was adequate sample volume availableT YES 13 NO j 12. Were samples received within proper holding time for requested tests? YES ❑ NO 113. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 114. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 115. Were sulfide samples received at a pH >9? ❑ YES 113 NO 116, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residua! of <0.5 m/L? ❑ YES 10 NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace} Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO, HCI NaOH ime of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or rictify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA,002 Rev 1 �- ; . 33YI�j�F �;!['!SiY3R4i{ni7`In�Y",�. (_;oiiectea isV: mi w ow -❑urri R9irinTp Tvnp• T = Tnfbipnt_ R = ENVIRONMENTAL CHEMISTS, INC Sample Collection and Chain of Custody_ W =Wp11_ CT=,Rtream_ Gn =Rail_ ql.= Rhad rp. Other! 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4424 PRESERVATION w Collection = .N A nth 5 Sample Identification o `o o c o o" ANALYSIS REQUESTED DATE TIME TEMP V" u z KM *3 wrw 7-+nC. L j� 131� Iti- -2o �ao5 S(a SL X Totoa ins 21* rush 1 G 5WOZ Zcnc, -741 p F ir�i-2o (doa 5L C X Tofc�1 �.ir,c, 2 ►� rush G Z 6c,1t S Gam$ "! �i %fie L C Ao'ka ihe- Tqf r rwl ' G GUT" CM0-*e. 47 01% It-14-20 012-1 oihcr }� Zghr eWh (D G CS jnfiutnt 1 759E tl-44-2a toZo Z X _ l040�hc 2'�hr vuah Ct G CAF) 1rl tu�cr� L('ig 1+-4-to 14 z1 { x 04!rw 2�{fir vu,,h G WBR e IY1+tu,n# Lfgi 9 3 1 -�-zA taz�. `tow -641 246- rt,A G G ocir-Istr,L� PS Ih�tuc t-f?g `f t+-►�- xp ao� 3 6 Tod•# Pik' Zghi- KA4, G G C P G G C P G G Transfer Relinquished By: Date/Time Receive By: Date/Time 715 it Svc) 2. Temperature when Received: 5r, S— Accepted:_ Rejected: Resample Requested• ]Circe: Delivered By:,!!5— ... -;� Received By;�� �. 7„G, Date: '-��p ra-- Z% [ ; ST" ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 26422 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalcliemists.com Date of Report: Nov 11, 2020 Customer PO M. Customer ID: 08100011 Report M 2020-18839 Project ID: WBR WWTP Sludge Lab ID Sample ID: WBR ATAD Collect DatelTime Matrix Sampled by 20-47927 Site: ATAD #3 - 1 11/4/2020 10:20 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.03 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <595 MPN/g 11/04/2020 Lab ID Sample ID: WBR ATAD Collect DatelTime Matrix Sampled by 20-47928 Site: ATAD #3 - 2 11/4/2020 10:21 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.41 % 11/06/2020 Fecal Density 9M 9221C E MPN 24 hr 503 <528 MPNIg 11/04/2020 Lab ID Sample ID: WBR ATAD Collect DatelTime Matrix Sampled by 20-47929 Site: ATAD #3 - 3 11/4/2020 101-22 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.26 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <554 MPN/g 11/04/2020 Lab ID Sample ID: WBR ATAD Collect DatelTime Matrix Sampled by 20-47930 Site: ATAD #3 - 4 11/4/2020 10:23 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.21 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <561 MPNIg 11/04/2020 Lab ID Sample ID: WBR ATAD Collect DatelTime Matrix Sampled by 20-47931 Site: ATAD 93 - 5 11/4/2020 10:24 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 329 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <548 MPNIg 11/04/2020 Report #:: 2020-1 Bam Page 1 of 2 F770' Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax "9 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Brunswick County Public Utilities Date of Report: Nov 11, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-18839 Project ID: WBR WWTP Sludge Lab ID Sample ID: WBR ATAD Collect Date/Time Matrix Sampled by 20-47932 Site: ATAD 43 - 6 11/4/2020 10:25 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (°/a) SM 2640 B 3.23 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <558 MPN/g 11/04/2020 Lab ID Sample ID: WBR ATAD Collect Date/Time Matrix Sampled by 20-47933 Site: ATAD #3 - 7 11/4/2020 10:26 AM Solid/Sludge Michael Garrity Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.25 % 11/05/2020 Fecal Density SM 9221C E MPN 24 hr 503 <554 MPN/g 11/04/2020 Comment: Results reported on a dry weight basis. Reviewed by: ,CG Report #' 2020-1BB39 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: Date: 1 I /b Report Number: c2 Q g Receipt of sample: ECHEM Pickup X, Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑ ❑ YES JE1 NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt "C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6`C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples iD's listed on sample containers? YES I0 NO 7. Were collection date and time listed on the COU YES ❑ NO 8. Were tests to be performed listed on the COC? YE5 ❑ NO 9. Did samples arrive in proper containers for each test? YES 10 NO 10. Did samples arrive in good condition for each test? YES I ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 114. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 115. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 116. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? t] YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatifes are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: Sample(s) by adding (circle one): (Must be completed for any sample(s) incorrectly preserved or with headspace) were received incorrectly preserved and were adjusted accordingly HISO' HNO, HCI NaOH 'Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 'C — 7 Enviroche— ENVIRONMENTAL CHEMIST'S, INC Sam le Collection and Chain of Custody 6602 Windmill Way Wilmington, NC 28445 Phone: (910) 392-0223 Fax (910) 392.4424 Client: 5 PL. Collected B ha-eA i+ Report -No: f PP 3 Samnle Tvne: I = Influent. E = EfTfuent. W =Well. ST =Stream. SO =Soil. SL= SludYYe Other: ... PRESERVATION r 0 A Collection 2„ 1i s e Sample Identification �� o .9 c v c a � ANALYSIS REQUESTED A DATE TIME TEMP U° �► U z Cq m z c Mr`i-zo I bozo 5U SL C X �re.ccl Dftdzt Y TS° f1TAD [3 V.tiBR �9�-� Y►-'i-20 [�� l 5� sL C X Y.Ur'A DG'J't- YTS°( G AT A D 'Y 3 wl3 R Y 7 5 11-4- 20 tioz z 5Le SL G X 1't,cr.,l Q�r•a� 7sq a G jr- �('7� �a 1w-4- 7A loz 3 5� sL C % Ftce.,1 'bey,,; TS°1a G l Aa �431 [�-y-ao Ioz'I SL C T) �c c�+S Dcw;+ lTzS% G Alwi AS INO R 4!7 i ? 10 2 5 S-te SL K F�� c� Dgna.f ITS°I G Av;A�'� WU D Y7�'� it- 'A-20 lotto 5lo SL C f crA DWI L s l G C P G G C P G G C P T1G G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: Y r Accepted: Rejected:—�;-- Resample Reques ed• Delivered By: - _ Received By:_�. �_ / Date: Z� Time: ,Y: 3 o e— "`c County of Brunswick Public Utilities >r I cnaWest Brunswick Regional Facility Laboratory g`�'Qrh o`��`t North Carolina Laboratory Certification Number: NCO0903 Anna leRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone: 910-253-2896 anna.leroux brunsWckcoun nc. ov Bolivia, NC 28422 Supply, NC 28462 Fax; 910-755-7927 Report Date: I Q Nov-2020 Sample Tvne Sample Date Test & Method Results West Brunswick Thirty Day Bench Beginning: 10/5/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 111412020 as Required to Meet Option 3 5.49% WWTP EPA [503.33(b)(3)] PASS Certified by: (End of Report) z g-rInvla /e �' ejfv v Anna IeRoux, Laboratory Supervisor BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 8, 2020 NE Brunswick Re Tonal WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.69 % Solids 7.56 pH Parameter % �MgIKg Dry Weight (% x 10,000) Pounds/Dry Toss (Mg/Kg x 0.002) Nitrogen (TKN) 11.200 112,000,000 224,000 Phosphorus 0.203 2,030.000 4.060 Potassium 3.210 32,100.000 64.200 PAN (injected)* 7.415 74,148.600 148.297 PAN (surface)* 4.520 45,198.600 90.397 Ammonia Nitrogen 5.790 57,900.000 115.800 Calcium 3.390 33,900,000 67.800 Calcium Carbonate Eq. --- ___ Magnesium --- 9,020.000 18.040 Sodium --- 3,770.000 7.540 Sulfur --. __- Nitrate N / Nitrite N --- 18.600 0.037 Barium --- ___ --- Chloride --- _._ --- Iron --- --- Aluminum --- 11,000.00 22.000 Arsenic --- 10.50 0.021 Cadmium --- 6.67 0.013 Chromium --- 70.50 0.141 Copper --- 358.00 0.716 Lead --- I9.90 0.040 Mercury --- 1.100 0.002 Molybdenum --- 14.70 0.029 Nickel --- 44.20 0.098 Selenium --- 8.08 0.016 Zinc --- I,840.00 3.680 Envirochem: 2020-0043 8 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or c detection limits are listed as detection limits for calculation purposes. 5AR 0.90 Ceiling Cancen. (Mg/Kg) 75 85 4,300 840 57 75 420 100 7,500 NE Brunswick WWTP WQ0034468 Class A - I st Quarter 2020 3aFa1Coii` P.:. 02/24/20 515 2.7118 02/24/20 483 2.6839 02/24/20 518 2.7143 02/24/20 512 2.7093 02/24/20 494 2.6937 02/24/20 494 2.6937 02/24/20 499 2.6981 Total 1 18.9049 Average 2.7007 Geometric Mean 110. 0= Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 6 910. � Y g 39_.0223 Lab 91p.39_7 .44�4 Fax 4100 'dP 710 Bawsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax ANALYTICAL 8, CONSULTING CHEMISTS info@en,,irornlicntaicttemists.cam Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-00438 Project ID: NEBR Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01044 Site: Sludge 1/8/2020 9:00 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 808181351a <0.02 mg/L 01/22/2020 Endrin (TCLP) SW 846 Method aae1B/3510 <0.0005 mg/L 01/22/2020 Heptachlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/22/202D Heptachlor epoxide (TCLP) SW 846 Method 80B1B13510 <0.0005 mg/L 01/22/2020 Lindane (TCLP) SW 846 Method 8081 B13510 <0.0005 mg/L 01122/2020 Methoxychlor (TCLP) SW 846 Method 8o81B/3510 <0.0005 mg/L 01/22/2020 Toxaphene (TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 01/22/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 2,4,5-Trichlorophenol (TCLP) SW 845 method 827013510 <0.050 mg/L 01/22/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270t351a <0.050 mg/L 01/22/2020 2,4-Dinitrotoiuene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Hexachloro benzene (TCLP) SW 846 method 6270/3510 <0.050 mg/L 01/22/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 m + p-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/2212020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Pentachlorophenol (TCLP) SW 846 method 827o/3510 <0.250 mg/L 01/22/2020 Pyridine (TCLP) SW 846 method 827013510 <0.050mg/L 01/22/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.0003 mg/L 01/23/2020 2,4-D (TCLP) SW846 Method 8151A <0.0003 mg/L 01/23/2020 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Benzene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Carbon Tetrachloride (TCLP) SW846 Method 826016030 <0.04 mg/L 01/15/2020 Report a:: 2020-00438 Pam 1 of 4 Environmental Chemists, Inc. 6602 Win dmill Wa Wilming ton, NC 2 5 � � � , Fax $40- 9 y 10.39_.i}2_3 Lab 910.39 � .�,4424 F as 710 Bowsertown load, Manteo, NC 27954 • 252.473.5702 I,ab/Pax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(cr)environtnenta.Ichemists.com Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-00438 Project ID: NPBR Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Chloroform (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 024 mg/L 01/15/2020 Tetrachloroethylene (TCLP) SW845 Method 8260/5030 <0.04 mg/L 01/15/2020 Trichloroethylene (TCLP) SW846 Method B26015030 <0.04 mg/L 01/15/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 RCI Cyanide EPA 335.4 0.234 mg/kg 01/13/2020 Sulfide SM 4500 S D 1.75 mg/kg 01 /22/2020 Ignitability SW 846 method 1010 >205 'F 01/23/2020 pH SW 846 Method 9045D 7.56 units 01/20/2020 Sludge Residuals Aluminum EPA20o.7 11000mg/kg 01/13/2020 Arsenic EPA 200.7 10.5 mg/kg 01/13/2020 Cadmium EPA 200.7 <6.67mg/kg 01/13/2020 Calcium EPA 200.7 33900 mg/kg 01/13/2020 Chromium EPA 200.7 70.5 mg/kg 01/13/2020 Copper EPA 200.7 358mg/kg 01/13/2020 Lead EPA 20o.7 19.9 mg/kg 01/13/2020 Magnesium EPA 2001 9020 mg/kg 01/13/2020 Molybdenum EPA 200.7 14.7 mg/kg 01/13/2020 Nickel EPA200.7 44.2mg/kg 01/13/2020 Potassium EPA 200.7 32100 mg/kg 01/13/2020 Selenium EPA 200.7 8.08mglkg 01/13/2020 Sodium EPA 200.7 3770 mg/kg 01/13/2020 Zinc EPA 200.7 1840 mg/kg 01113/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 18.6 mg/kg 01/16/2020 Total Solids (%) SM 254a B 3.69 % 01/10/2020 Ammonia Nitrogen SM 4500 NH3 C 57900 mglkg 01/10/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 112000 mglkg 01/10/2020 Report 9:: 2020-00438 Page 2 of 4 Environmental Chemists, Inc. 6602'Kindmill Waj; Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax sM, 710 Bowsertown Road, Mantes, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalclieniists.com Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #; 2020-00438 Project ID: NEBR Total Phosphorus SM 4500 P F 2030 mg/kg 01/23/2020 Mercury Sw846 7471B 1.10 mg/kg 01/17/2020 TCLP Metals Arsenic EPA 200.7 <1.0mg/L 01/22/2020 Barium EPA 200.7 <1.0 mg/L 01/22/2020 Cadmium EPA 200.7 <1.0mg/L 01/22/2020 Chromium EPA 2007 <1.0 mg/L 01/22/2020 Lead EPA 200.7 <1.0 mg/L 01/22/2020 Selenium EPA 200.7 <1.0 mg/L 01/22/2020 Silver EPA 2001 <1.0 mg/L 01/22/2020 Mercury EPA245.1 <0.0002mg/L 01/24/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-01045 Site: #1 1/8/2020 9:01 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM254oB Fecal density SM 9221C E MPN 24 hr503 Lab ID Sample ID: Collect Date/Time 20-01055 Site: #2 1/8/2020 9:02 AM Test Method Total Solids (%) SM 2541) t4 Fecal Density SM 9221 C E MPN 24 hr503 Lab ID Sample ID: Collect Date/Time 20-01058 Site: #3 1/8/2020 9:03 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 3.50 % 01/10/2020 <515 MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.73 % 01/10/2020 <483 MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.48 % 01/10/2020 <518 MPN/g 01/08/2020 Report #:. 2020-00438 Pace 3 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilm ington, tan �^ NC 28405 910.'i92. � � 02�� Lab 91 . 0 39_.4424 Fax 71.0 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347 5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inforenvironnientalchvmists.conl Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-00438 Project 1D: NEBR Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-01057 Site: #4 1/8/2020 9:04 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B Fecal Density SM 9221C E MP 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-01058 Site: #5 1/8/2020 9:05 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MP 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-01059 Site: #6 1/8/2020 9:06 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-01060 Site: #7 1/8/2020 9:07 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MP 24 hr 503 Comment: Sludge residuals reported on a dry weight basis. Reviewed by: r 3.52 % 01/10/2020 <512 MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.65 % 01/10/2020 <494 MPNIg 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.65 % 01/10/2020 <494 MPNIg 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3,61 % 01/10/2020 <499 MPN/g 01/08/2020 Report #;. 2020-00438 Pane 4 nr a COUNTY OF BRUNSWICK West Brunswick Regional Laboratory Public Utilities Department ,�SYnCRCpU4 235 Grey Water Road Wastewater Treatment Division Supply, NC 28462 �pRrHCA" O Phone: 910-755-7921 Fax: 910-755-7927 Sample Collection and Chain of Custody Collected By: Matthew Henry Report No.: 10-41 Sample Type: 1 = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other: Sample Collection Sample Composite Container Chlorine LAB I❑ PRESERVATION ANALYSIS REQUESTED Identification Type or Grab (Plastic or Glass) mg/L NUMBER NONE I HC! H2SO4 HNO, THIO OTHER G P NEBR 1/8/2020 9:00 17.8'C SL �u �, f _1 TCLP/RCUnutrient X /metalstresiduals G P NEBR 1/8/2020 9:01 17.8'C SL j X fecal density G P NEBR 1/8/2020 9:02 17.8'C SL X fecal density G P NEBR 1/8/2020 9:03 17.8`C SL _ V z X fecal density G P NEBR 1/8/2020 9:04 17,81C SL X fecal density G P NEBR 1/8/2020 9:05 17.8'C SL ��-cY >s X fecal density G P NEBR 1/8/2020 9:06 17.8'C SL X fecal density G P NEBR 1/8/2020 9:07 17,8•C SL X I Ifecal density Transfer Relinquished By: DatelTime /11 ecei�ed. By: �/ DatelTime Temperature when Received. ; f�i Accepted: Rejected: Resample Required: Delivered By: L-- - Comments: b�J� W K Gyt County of Brunswick Public Utilities y�'9lN CIINo�,tT West Brunswick Regional Facility Laboratory North Carolina Laboratory Cerfrficalion Number: NCO0903 Anna leRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone: 910-253-2896 alerouxna brunsco.net Bolivia, NC 28422 Supply, NC 28462 Fax: 910-755-7927 Report Date: 7-Feb-2020 t sample Tyne Test & Method Results North Brunswick Thirty Day Bench Beginning: 1/7/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 2/7/2020 as Required to Meet Option 3 10.60% WWTP EPA [503.33(b)(3)] PASS Certified by: (End of Report) Anna leRoux, Laboratory Supervisor BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 21, 2020 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.78 % Solids 7.48 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 10.500 105,000.000 210.000 Phosphorus 5.500 55,000.000 110.000 Potassium 1.880 I8,800.000 37.600 PAN (injected)* 8.440 84,399.000 168.798 PAN (surface)* 4.685 46,849.000 93.698 Ammonia Nitrogen 7.510 75,100.000 150.200 Calcium 1.950 19,500.000 39.000 Calcium Carbonate Eq. -.- --- --- Magnesium --- 6,240.000 12.480 Sodium --- 2,020.000 4.040 Sulfur Nitrate N / Nitrite N --- 329.000 0.658 Barium --- --- --- SAR 0.62 Chloride --- --- --- Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum .._ 6,030.00 12.060 Arsenic --- 12.00 0.024 75 Cadmium --- 12.00 0.024 85 Chromium --- 39.40 0.079 --- Copper --- 202.00 0.404 4,300 Lead --- 12.00 0.024 840 Mercury --- 1.270 0.003 57 Molybdenum --- 1200 0.024 75 Nickel --- 23.30 0.047 420 Selenium --- 12.00 0.024 100 Zinc --- 1,340.00 2.680 7,500 Envirochem: 2020-05 867 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. NE Brunswick WWTP WQ0034468 Class A - 2nd Quarter 2020 9g: 04/21/20 334 2.5237 04/21/20 329 2.5172 04/21/20 353 2.5478 04/21/20 342 2.5340 04/21/20 340 2.5315 04/21/20 332 2.5211 04/21/20 338 2.5289 Total 1 17.7043 Average 1 2.5292 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. { *770 te X1I1'�+chenx� ANALYTICAL & CONSULTING CHEMISTS Elnvironmental Chemists, Inc. 6602 Windmill Way, Wilniill-Lon, IBC 23405 p 910,392.0223 Lab v 911).392.4424 Fax 71.0 Bowsertown Road, Mantel,, PVC 27954 • 252.473.5702 Labjax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infpiiii nvironnimtalchemists.caal Brunswick County Public Utilities Date of Report. Apr 21, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-05867 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID; Collect DatelTime Matrix Sampled by 20-14399 Site: Sludge 4/8/2020 10:00 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 6030mglkg 04117/2020 Arsenic EPA 200.7 <12.0 mg/kg 04/15/2020 Cadmium EPA200.7 <12.0mg/kg 04/15/2020 Calcium EPA 200.7 19500 mg/kg 04/15/2020 Chromium EPA 200.7 39.4mglkg 04/15/2020 Copper EPA 200.7 202 mg/kg 04/15/2020 Lead EPA 200.7 <12.0 mg/kg 04/15/2020 Magnesium EPA20a.7 6240mg/kg 04/15/2020 Molybdenum EPA200.7 <12.0mg/kg 04/15/2020 Nickel EPA 200.7 23.3 mg/kg 04/15/2020 Potassium EPA 200.7 18800 mg/kg 04115/2020 Selenium EPA 200.7 <12.0 mglkg 04/15/2020 Sodium EPA 200.7 2020 mg/kg 04/15/2020 Zinc EPA 200.7 1340mg/kg 04/15/2020 Nitrate+Nitrite-Nitrogen EPA353.2 329mglkg 04/17/2020 Total Solids (%) SM 2540 e 3.78 % 04/08/2020 pH SM 4500 H B 7.48 units 04/20/2020 Ammonia Nitrogen SM 4500 NH3 C 75100 mg/kg 04/09/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org s 105000 mg/kg 04109/2020 Total Phosphorus SM 4500 P F 55000 mglkg 04116/2020 Mercury SW646 7471E 1.27 mg/kg 04/16/2020 Report #:: 2020-05767 page 1 of 3 Finvlronmental Chemists, Inc. 6602 Windmill VJay, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 B(iwsertown Road, Wlanteu, ylC 27954 - 252.473.5702 Lab/Fax 255-A Wilminnton Highway, Jacksonville, NC 28540 E 910 347.5843 Lab/Fax [llEO([�011V1 C671177L'nl alC1lCRil5E5.�On1 Brunswick County Public Utilities Date of Report: Apr 21. 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-05867 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-14400 Site. 1 4/8/2020 10:01 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 5.40 % 04/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <334 MPN/g 04/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-14401 Site: 2 4/8/2020 10:02 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 5.48 % 04/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <329 MPN/g 04108/202D Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-14402 Site: 3 4/8/2020 10:03 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 5.10 % 04/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <353 MPN/g 04/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-14403 Site: 4 4/8/2020 10:04 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) Fecal Density Lab ID Sample ID: 20-14404 Site:5 SM 2540 B SM 9221 C E MPN 24 hr 503 5.27 % 04/08/2020 <342 MPN/g 04/08/2020 Collect Date/Time Matrix Sampled by 4/8/2020 10:05 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) Fecal Density SM 2540 B SM 9221C E MPN 24 hr 503 5.30 % 04/08/2020 <340 MPNIg 04/08/2020 Report #'_ 2020-05867 Pau- 2 of 3 4 ,R Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab • 910.391.4424 Fax �� I01i) 710 Bowsertown Road, Manteo, NC Z 954 a 252.473.5702 Lab/Fax ?_55-A Wilmington Highway, JackScmvjile, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info+ii;erlvironmentalchenrists.com Brunswick County Public Utilities Date of Report: Apr 21, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-05867 Project ID: NE Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-14405 Site: 6 4/8/2020 10:06 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (°1°) SM 2540 B 5.43 % 04/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <332 MPN/g 04/08/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-14406 Site: 7 4/8/2020 10:07 AM SolidlSludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 254a B 5.34 % 04/08/2020 Fecal Density SM 9221C E MP 24 hr 503 <338 MPN/g 04/08/2020 Comment Sludge residuals, except pH, reported on a dry weight basisl pH reported on an as received basis. Reviewed by: ' Report 4: 2020-05867 Pgne 3 nr S Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: Fl"IQ"Ir nc\ DateV—*J�oa5 % Report Number: b` Receipt of sample: ❑ YES ❑ NO Delivered UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A N/A 1. Were custody seals present on the cooler? Original temperature upon 2. if custody seals were present, were they intact/unbroken? receipt �C Now temperature taken: ❑ Temperature Blank Corrected temperature upon receipt IR Gun ID: Thomas Traceable 5/N 192511657 ® against Bottles ❑ -YES ❑ NO IR Gun Correction Factor'C: 0.0 3. If temperature of cooler 02 YES ❑ NO exceeded 6'C, was Project M r. 4. Were proper custodya /QA notified? YES ❑ NO procedures {relinquished/received) followed? 5. Were sample ID's listed on p ❑ ❑ NO the COC7 6. Were samples ID's listed on sample containers? ❑ NO 7. Were collection date and time listed on the COC? ❑ NO NO S. Were tests to be performed listed on the COC? YES❑ NO 9. Did samples arrive in proper containers for each test? ❑ 10. Did samples arrive in good condition for each test? RS13 ❑ NO 11. Was adequate sample volume availableT YES❑ No NO 12. Were samples received within proper holding time for requested tests? 13, Were acid preserved 0 NO samples received at a pH of <2? 14. Were cyanide samples ❑ NO received at a pH >127 15. Were sulfide samples received at a >9? ❑ NO NO pH 16, Were NH3/TKN/Phenol received at a chlorine residual of <05 rrii 17. Were Sulfide/Cyanide received at a chlorine residual of c0.5 m/L? " TOC/Volatiles are PH checked at time of analysis and recorded an the benchsheet. *R Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any samples) incarrectl Sample(s) Y Preserved or with headspace) were received incorrectly preserved and were a by adding (circle one): H2504 HNO Time of preservation: ; HCl NaOH djusted accordingly If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or lotify the state lab if directed to analyzed by the customef. who was notified, date and time: Voiatiles Sample(s) were received with headsoace COMMENTS: QC ENVIRONMENTAL CHEMISTS, .INC 6602 Windmill Way r` Wilmington, NC 28405 Sample Collection and Chain of Custody Phone: (910) 392-0223 Fax (910) 392.4424 Client: Brunswick County Public Utilities -Northeast Brunswick Re Tonal WWTP Collected By: Matthew Henry Report No: 0 -6526 Sample T e: I = Influent E = Effluent W =Well ST =Stream SO =Soil SL= Sludize Other: a a L PRESERVATION Collection Sample Identification a o o c o an w p w ANALYSIS REQIIESTE, D z DATE rE E; U U TIME TEMP U U - U o O NEBR SLUDGE l�3 SL PX418/20 (; l�Tutrient / me.tal /residuals NEBRSLUDGE a30.2*C P 4/8/20 2*c SL G X Fecal Density NEBR SLUDGE P 01 4/8/20 10:02 3o•2 c SL C X Fecal Density NEBR SLUDGE P O Z 4/8/20 30.z*c SL 1D.03 G X Fecal Density NEBR SLUDGE P trJ3 4/8/20 3o.2*c SL 10:04 G !C Fecal Density NEBR SLUDGE P � 1 4/8/20 30.2*c SL 1p•OS G XFecal Density NEBR SLUDGE SL P o 4/8120 30.z*c 10:06 C X Fecal Density NEBR SLUDGE SL P 4/8/20 . 302{C 10:07 G X Fecal Density ----------------------------- NOTE: COPPER, ZINC; AND NICKEL ARE TQ BE.ANALYZED DOWN TO.00;t ug/L Transfer Relinquished By: Date/Tune Received By: Date/Time f 2. Temperature when Received: e.r Accepted: y,,` Rejected: Resample Requested: Delivered By: Received By: Date: Time: ' County of Brunswick Public Utilities ~may, , `; West Brunswick Regional Facility Laboratory North Carolina Laboratory Cert yratiox NMnher: NCO0903 Anna IeRoux, Lab Supervisor PO Box 249 235 Grey Water Road 'Telephone: 910-253-2896 arena. leroux(aDbrunswickcountVnc.gov Bolivia, NC 28422 Supply, NC 28,162 Fax: 910-755-7927 Rcporl Date: I I-May-2020 EaKiliSamnle Tvne S Dle Date Test & " esult Northeast Brunswick Thirty Day Bench Beginning: 4/8/2020 Reduction of Vector Attraction (<15% is considered passing) Regional ❑igestor Scale Test Ending: 5/8/2020 as Required to Meet Option 3 2.01% WWTP EPA [503.33(b)(3)] PASS (End of Report) Certified by: e - Ae AT Anna IeRoux, Laboratory Supervisor BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: July 7, 2020 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0,30 3.21 % Solids 7.64 pH Parameter F- % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 12.500 125,000.000 250.000 Phosphorus 0.097 971.000 1.942 Potassium 1.690 16,900.000 33.800 PAN (injected)* 8.897 88,967.900 177.936 PAN (surface)* 5.222 52,2I7.900 104.436 Ammonia Nitrogen 7.350 73,500.000 147.000 Calcium 2.140 21,400.000 42.800 Calcium Carbonate Eq. --- --- Magnesium --- 5,890,000 11.780 Sodium --- 2,210.000 4.420 Sulfur --_ --- --- Nitrate N / Nitrite N --- 17.900 0.036 Barium --- --- --- SAR 0.62 Chloride --- --- --- Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 6,980M 13.960 Arsenic --- 16.80 0.034 75 Cadmium --- 10.50 0.021 85 Chromium --- 38.00 0.076 --- Copper --- 211.00 0.422 4,300 Lead --- 10.50 0.021 840 Mercury --- 0.536 0.001 57 Molybdenum --- 10.50 0.021 75 Nickel --- 23.10 0.046 420 Selenium --- 10.50 0.021 100 Zinc -- 1,360.00 2.720 7,500 Envirochem: 2020-11016 *Determination of Plant Available Nitrogen (PAN): Injected Application; (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits for calculation purposes. NE Brunswick WWTP WQ0034468 Class A - 3rd Quarter 2020 07/07/20 46 1.6628 07/07/20 46 1.6628 07/07/20 45 1.6532 07/07/20 43 1.6335 07/07/20 46 1.6628 07/07/20 44 1.6435 07/07/20 47 1.6721 Total 11.5905 Average I.6558 Geometric Mean} MI Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. [envil-rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 232.473.5702 Lab/Fax 255-A Wilmington �Iighway, Jacksonville, NC 28540 ■ 910.347,5943 Lab/Fax info r@,t environmentalchemists.com Brunswick County Public Utilities Date of Report: Jut 23, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: OB100011 Attention: Matthew Henry Report #: 2020-11016 Project ID: NEBR Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-27706 Site: Sludge 7/712020 10.00 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 69BO mg/kg 07/14/2020 Arsenic EPA 200.7 16.8mglkg 07/14/2020 Cadmium EPA 200.7 <10.5 mg/kg 07/1412020 Calcium EPA 200.7 21400 mg/kg 07114/2020 Chromium EPA2oo.7 38.0mg/kg 07/14/2020 Copper EPA 200 7 211 mg/kg 07/14/2020 Lead EPA 200,7 <10.5 mg/kg 07/14/2020 Magnesium EPA 200.7 5890mglkg 07/14/2020 Molybdenum EPA 200.7 <10.5 mg/kg 07/14/2020 Nickel EPA 20o.7 23.1 mg/kg 0711412020 Potassium EPA200.7 16900mglkg 07/16/2020 Selenium EPA 200.7 <10.5mg1kg 07/14/2020 Sodium EPA2Do.7 2210mglkg 07/14/2020 Zinc EPA 200.7 1360 mg/kg 07114/2020 Nitrate+Nitrite-Nitrogen EPA353.2 17.9mg/kg 07/1512020 Total Solids (%) 5M 2540 B 3.21 % 07/08/2020 pH SM 4500 H B 7.64 units 07/16/2020 Ammonia Nitrogen SM 4500 NH3 C 73500 mg/kg 07/08/2020 Total Kieldahl Nitrogen (TKN) 5M 4500 org a 125000 mg/kg 07108/2020 Total Phosphorus SM4500 P F 971 mg/kg 07/10/2020 Mercury SW8467471B <0.536mg/kg 07/14/2020 Report # : 2020-11018 Page 1 at 3 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax pw 71013owsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax �3" 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmcntalcltemists.com Brunswick County Public Utilities Date of Report: Jul 23, 2020 Past Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-11016 Project ID: NEBR Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-27707 Site: Sludge #1 717/2020 10:01 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids SM 2540 B 3.95 % 0710812020 Fecal Density SM 0221 C E MPN 24 hr 503 <46 MPN/g 07/07/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-27708 Site: Sludge #2 7/7/2020 10:02 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.94 % 07/06/2020 Fecal Density SM 4221 C E MPN 24 hr 503 <46 M PN/g 07/07/2020 Lab iD Sample ID: Collect DatelTime Matrix Sampled by 20-27709 Site: Sludge #3 7/7/2020 10:03 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.05 % 07/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <45 M PNIg 07/07/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-27710 Site: Sludge #4 7/7/2020 10:04 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.22 % 07/0812020 Fecal Density SM 13221C E MPN 24 hr 503 <43 MPN/g 07/0712020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-27711 Slte: Sludge #5 7/7/2020 10:05 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids °/a) 5M 2540 B 3.94 % 07108/2020 Fecal Density SM 0221C E MPN 24 hr 503 <46 MPNIg 07/07/2020 Report #;; 2020.11018 Page 2 of 3 Lenvirioe-hem ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matthew Henry Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 26405 ■ 910.392-0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infogenvironmentalchemists.com Date of Report: Jul 23, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-11016 Project ID: NEBR Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-27712 Site: Sludge #6 7/7/2020 10.06 AM SolldlSludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2S4o B 4.11 % 07/08/2020 Fecal Density SM 9221C EMPN 24 hr503 <44 MPN/g 07/07/2020 Lab ID Sample ID: Collect Dateliime Matrix Sampled by 20-27713 Site: Sludge #7 717/2020 10:07 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) Fecal Density SM 2540 B SM 9221C E MPN 24 hr 503 3.90 % <47 MPNIg Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: 0 so , 014, 07/06/2020 07/07/2020 Report # : 2020-11018 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910,392.0223 Sample Recei t Checklist Client: N5 Date:'-7 /.7 0 Report Number: -- Receipt of sample: DeliveredO UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A II. Were custody seals present on the cooler? ❑ YES 113 NO N/A 12. If custody seals were present, were they intact/unbroken? Ori inal temperature upon receipt 221, y C Corrected temperature upon receipt How temperature taken: _ ❑ Temperature Blank Against Bottles iR Gun ID: Thomas Traceable S/N 19251 1 557 IR Gun Correction Factor'C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded FC, was Project M r./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO S. Were sample ID's listed on the CDC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ ftf0 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of a27. " ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? '• ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 11P Q YES ❑ NO Were orthophosphate samples filtered in the field within 15 minutes? ' TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. " Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. irnple Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) imple(s) were received incorrectly preserved and were adjusted accordingly r adding (circle one): H2SO, HNO3 HCl NaOH me of preservation; If more than one preservative is needed, notate in comments below Ete: Notify customer service immediately for incorrectly preserved samples. Obtam a new sample or tify the state lab if directed to analyzed by the customer. Who was notified, date and Ume 7latiles Sample(s) were received with headsoacp COMMENTS: DOC. 4A 002 'C COUNTY OF BRUNSWICKux a� West Brunswick Regional Laboratory Public Utilities Department 235 Grey Water Road Wastewater Treatment Division Supply, NC 28462 CaF4��� Phone: 910-755-7921 Pax: 910-755-7927 Sample Collection and Chain of Custody Collected By: Matthew Henry Report No.: C20 - 110 � Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other. Sample Identification Collection Sample Type Composite or Grab Container (Plastic or Glass) Chlorine mg1L LAB ID NUMBER PRESERVATION ANALYSIS REQUESTED —R6WETHCI H250A HNO3 THIO OTHER NEBR 75.6'C SL G P �� X residuals nutrienUmetals! 7f712020 10;00 NEBR 75.6'C SL G P T7u� X fecal density 7f72020 10:01 NEBR 75.6'C SL G P () 4a X fecal dsnsity 7/712020 10:02 NEBR 75.61C SL G P 01 X fecal density 71712020 10:03 NEBR 75 6'C SL G P X feral density 71712020 10:04 NEBR 75 WC SL G P r i X fecal density 7172020 10;05 NEBR 75.6'C SL G P 12 X fecal densil r 71712020 10;06 NEBR 75 6'C SL G P 13 X fecal density 7f72020 10:07 Transfer Relinquished By: DatelTime��// Received By: Date/Time UK �7 I �f_7 2 Temperature when Received; a I - q- Accepted; lJ Rejected: Resample Required: Delivered By: Comments: County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory Xorlh Carolina Laboralwy Certification r lumber: NC00903 Anna IeRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone: 910-253-2896 anna.I_eroux(o)brunswickcountync.gov Bolivia, NC 28422 Supply, NC29462 Fax: 910-755-7927 Report Dale: 1 1-Aug-2020 Facilijy Sample --Type Sample Date Test & Method Resultu Northeast Brunswick Thirty Day Bench Beginning: 7/7/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 8/6/2020 as Required to Meet Option 3 2.37% WWTP EPA [503.33(b)(3)] PASS Certified by: (End of Report) t r a Anna IeRoux, laboratory Supervisor BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 8, 2020 NE Brunswick RelZional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 5.18 % Solids 8.04 pH Parameter I Ma/Ka I]ry Waiaht IVnrinr�clTlry T.,� (% x 10,000) (Mg(Kg x 0.002) Nitrogen (TKN) 8.650 86,500.000 173.000 Phosphorus 3.490 34,900.000 69.800 Potassium 1.070 I0,700.000 21.400 PAN (injected)* 5.854 58,537.000 117.074 PAN (surface)* 3.534 35,337.000 70.674 Ammonia Nitrogen 4.640 46,400.000 92.800 Calcium 1.890 18,900.000 37.800 Calcium Carbonate Eq. --- --_ Magnesium --- 6,220.000 12.440 Sodium --- 1,620.000 3.240 Sulfur ___ --- --- Nitrate N / Nitrite N --- 107.000 0.214 Barium --- ___ -_- Chloride --- ___ --- Iron Aluminum --- 5,540.00 11.080 Arsenic --- 9.19 0.018 Cadmium --- 9.19 0.018 Chromium --- 25.70 0.051 Copper --- 181.00 0.362 Lead --- 10.10 0.020 Mercury --- 0.347 0.001 Molybdenum --- 9.19 0.018 Mickel --- 15.60 0.031 Selenium --- 0.476 0.001 Zinc --- 1,040.00 2.080 Envirocliem: 2020-17256 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 0.59 Ceiling Concen. (Mg/Kg) 75 85 4,300 840 57 75 420 100 7,500 NE Brunswick WWTP WQ0034468 Class A - 4th Quarter 2020 10/08/20 331 2.5198 10/08/20 345 2.5378 10/08/20 337 '7 2.52,6 10/08/20 325 2.5119 10/08/20 327 2.5145 10/08/20 333 2.5224 [10/08/20 353 2.5478 Total 1 17. Average 1 2.5260 1 Geometric Mean I Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matt Heyer Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910-392.0223 Lab • 910.392.4424 Fax 710 13owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 02, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-17256 Project ID: North East Brunswick Lab ID Sample ID: 20-44104 Site: Sludge Test Collect DatelTime 10/8/2020 10:45 AM Method Matrix Sampled by Solid/Sludge Matt Henry Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 5540mg/kg 10/12/2020 Arsenic EPA 200-7 <9.19 mg/kg 10/12/2020 Cadmium EPA 200.7 <9.19 mg/kg 10/12/2020 Calcium EPA 200.7 18900 mglkg 10/12/2020 Chromium EPA 200.7 25.7mg/kg 10/12/2020 Copper EPA200.7 181 mg/kg 10/12/2020 Lead EPA 200.7 10.1 mglkg 1011212020 Magnesium EPA 200.7 6220 mglkg 10/12/2020 Molybdenum EPA 200.7 <9.19 mg/kg 10/12/2020 Nickel EPA 200.7 15.6 mglkg 10/12/2020 Potassium EPA 200.7 10700 mg/kg 10/13/2020 Selenium EPA 200.7 <0.476 mg/kg 10/12/2020 Sodium EPA 200.7 1620 mglkg 10/20/2020 Zinc EPA 200.7 1040 mg/kg 10/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 107 mg/kg 10/12/2020 Total Solids (%) 5M 2540 B 5,18 % 1011212020 PH SM 45ao H a 8.04 units 10/13/2020 Ammonia Nitrogen SM 4500 NH3 C 46400 mg/kg 10/12/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 86500 mglkg 10/13/2020 Total Phosphorus SM 4500 P F 34900 mg/kg 10/13/2020 Mercury 5W846 7474E 0.3470 mg/kg 10/30/2020 Report #:: 2020-17256 Page 1 of 4 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matt Heyer Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab O 910.392.4424 Fax 71013owsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 02, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-17256 Project ID: North East Brunswick Lab ID Sample ID: Collect DatelTime Matrix Sampled by 2044105 Site: Sludge #1 10/8/2020 10:46 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids {%) SM 2540 B 5.45 % 10/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <331 MPNIg 10/08/2020 Lab ID Sample Id: Collect DatelTime Matrix Sampled by 20A4108 Site: Sludge #2 10/8/2020 10A7 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 a 5.23 % 10/08/2020 Fecal Density SM 9221 C E MPN 24 hr 503 <345MPN/g 10/08/2020 Lab ID Sample ID; Collect DatelTime Matrix Sampled by 20-44109 Site: Sludge #3 10/8/2020 10:48 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids {%) SM 2540 B 5.35 % 10/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <337 MPNIg 10/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-44110 Site: Sludge #4 10/8/2020 10:49 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 5.54 % 10/08/2020 Fecal Density SM 9221C E MPN 24 hr 503 <325 MPNIg 10/08/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-44111 Site: Sludge #5 10/812020 10:50 AM Solid/Sludge Matt Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 5.51 % 10108/2020 Fecal Density SM 9221C E MPN 24 hr $03 <327 MPNIg 10/08/2020 Report 9.: 2020.17256 Page 2 of 4 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matt Heyer Lab ID Sample ID: 20-44112 Site: Sludge #6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-44113 Site: Sludge #7 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Date of Report: Nov 02, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-17256 Project ID: North East Brunswick Collect Date/Time Matrix Sampled by 10/8/2020 10:51 AM Solid/Sludge Matt Henry Method Results Date Analyzed SM 2540 B 5.42 % 10/08/2020 SM 9221C E MPN 24 hf 603 <333 MPN/g 10/08/2020 Collect Daterrime Matrix Sampled by 10/8/2020 10:52 AM Solid/Sludge Matt Henry Method Results Date Analyzed Total Solids (%) SM 2540 a 5.10 % IW0812020 Fecal Density SM 9221C E MP 24 hr 503 <353 MPN/g 10/08/2020 Reperl ft:: 2020.17256 Page 3 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matt Heyer Lab ID Sample ID: 20-44116 Site: Aeration Basin Test Method Cyanide EPA 335 4 Reporting limit elevated due to matrix interference. Sludge Residuals info@environmentalchemists.com Date of Report: Nov 02, 2020 Customer PO #: Customer ID: 08100011 Report #t: 2020-17256 Project ID: North East Brunswick Collect Date/Time Matrix Sampled by 10/8/2020 11:45 AM Solid/Sludge Matt Henry Results <0.05 mg/kg Date Analyzed 1011212020 Aluminum EPA 200.7 4430 mg/kg 10/1212020 Arsenic EPA 2007 <173mg/kg 10/12/2020 Cadmium EPA 2007 <173 mg/kg 10/1212020 Calcium EPA 200 7 20200 mg/kg 10/1212020 Chromium EPA 2007 <173mglkg 10/12/2020 Copper EPA 2007 <173 mg/kg 10/12/2020 Lead EPA 2007 <173 mg/kg 10/12/2020 Magnesium EPA 200 7 <8679 mg/kg 10/12/2020 Molybdenum EPA 200.7 <173 mg/kg 10/12/2020 Nickel EPA 200 7 <173 mg/kg 10/12/2020 Potassium EPA 200.7 12000 mg/kg 10/12/2020 Selenium EPA 2007 <173 mglkg 10/12/2020 Sodium EPA 200 7 19500 mg/kg 10M6/2020 Zinc EPA 200 -7 786 mg/kg 10/12/2020 Total Solids SM 2540 B 0.28 % 10/08/2020 Ammonia Nitrogen sM 4500 NK3 c <35.7 mg/kg 10/1212020 Mercury SW84874718 <5.71 mg/kg 10/30/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ' Report x:. 2020-17258 Page 4 or 4 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: 1 n � ( C:L P Date: 1 _2u Report Number: 2-D— I TaLJ �o Receipt of sample: ECHEM Picku Client Delivery UPS ❑ FeclEx ❑ Other ❑ ❑ YES I0 N0 ❑ N/A 11. Were custody seals present on the cooler? ❑ YES IM NO I0 N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt .O "C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank IX Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8, Were tests to be performed listed on the COV YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 111. Was adequate sample volume available?` YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES I ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/l.? ❑ YES I0 NO 117, Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/I_? —Were ❑ YES 10 NO 118. orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded an the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation. (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): HZSOI HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 "C ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way "_. Wilmington, NC 28405 Sample Collection and Chain of Custody Phone: (91.0) 392-0223 Client: Brunswick CountyTo Public Utilities -Northeast Brunswick Re nal WWTF Fax (910) 392.4424 Collected By: Matthew HenryReport No: c;)-(D - (7 ,D-S Sam le Tyne: I = Influent E = Effluent W =Well ST =Stream SO =Soil SL= Sludge Other: Sample Identification a m as X z DATE Collection TIME TEMP - a GO -� g o = 0 o s z U U U z NEBR SLUDGE NEBR SLUDGE NEBR SLUDGE NEBR SLUDGE NEBR SLUDGE � NEBR SLUDGE 1�� NEBR SLUDGE 4L� � Oq g4(05 u �� D9 Lk LA 0 � [ ` '� ® �41 y I l 67.8*C 67.8*C 67.s*c 67s*c 67.8*C 67.8*c 67.8ic SZ, SL SL SL SL SL SL P X G p G p G P G p G P G P 10/B/ZO 10:45 I0/8/20 I0:46 to/s/20 Io:47 Io/8/20 I0-.48 10/8/20 10.49 ] 018120 10:50 10/8/Z0 10:51 NEBR SLUDGE 4 4 1, ,i �3 67.s*c SL G p IO/sn0 1a:52 NEBR Aeration Basin �-''� 1 y r I ` t `i 25.7* C SL G P G X 10/8/20 1 I:45 Aeration Basin Sample was taken in two half gallon jugs Transfer i Relinquished By: Date/Time Rec 2. Tom t h PRESERVATION .a 6 6 O_ w ANALYSIS REQUESTED U z x o Nutrient / metal / residuals X Fecal Density X Fecal Density X Fecal Density X Fecal Density X Fecal Density X Fecal Density X Fecal Density EF-717 %SOLIDS/METALSINH3 /CN- eived By: Date/Time pera ure w en Received• w Accepted: 2 Reject Resample Requested: Delivered By:_ Received By: Date: 10 19 Time• �- County of Brunswick Public Utilities Sp�TH CAHU�'�4 West Brunswick Regional Facility Laboratory North Carolina Laboratory Certification Number: NCO0903 Anna teRoux, Lab Supervisor PO Box 249 235 Grey Water Road Telephone: 910.253-2896 anna.leroux(o)brunsyAckeountVne.goy Bolivia, NC 28422 Supply, NC 28462 Fax: 910-755-7927 Report Date: 10-Nov-2020 SRMI)le Tvne amn[e Date Test & Method Results Northeast Regional Thirty Day Bench Beginning: 10/6/2020 Reduction of Vector Attraction (<15% is considered passing) WWTP Digestor Scale Test Ending: 11/5/2020 as Required to Meet Option 3 2.20% EPA [503.33(b)(3)] PASS (End of Report) Certified by: rrta ' Anna IeRoux, Laboratory Supervisor