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HomeMy WebLinkAboutWQ0034513_Residual Annual Report 2020_20210223Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0034513 Applicant/Permittee Brunswick County Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Wilmington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd .......................................................... ronc su_ - Name * Rob Willcox Email Address* rob@Wllcomabesoil.com Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363399128 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 IT Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00034513 Fbs Current Existing perm number Applicant/Permittee Address* Post Office Box249; Bolivia, N.C. 28422 Facility Name * Brunswick County RLAP Please provide comments/notes on your current submittal below. 2020 Annual Report for Brunswick County Class B Residuals At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form} Engineering Rans, Specifications, Calculations, Bc.) 2020 CLASS B ANNUAL REPORT-WQ0034513 - 9.31 MB Brunswick County.pdf Upload only 1 PCF document (less than 250 M3). NURiple docurrents must be combined into one PDF file unless file is larger than upload linit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature � wl� Submission Date 2/23/2021 2020 ANNUAL REPORT BRUNSWICK COUNTY PUBLIC UTILITIES RESIDUALS LAND APPLICATION PROGRAM NON -DISCHARGE PERMIT #W00034513 Prepared For: Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North. Carolina 27358 February 2021 February 23, 2021 N.C. Department of Environmental Quality Division of Water Resources — Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Information Processing Unit Reference: 2020 LAND APPLICATION ANNUAL REPORT Brunswick County Public Utilities Non -Discharge Permit No. WQ0034513 WMSS Project No. 15-04 Phase: 12 Non -Discharge Branch: willcox&mate SOIL SOLUTIONS Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Brunswick County Public Utilities (Brunswick County). WMSS compiled this report using data gathered during the compliance year by Brunswick County and BioGreen Services, Inc. This data includes: 1) land application certification forms, 2) annual residual sampling summary forms, 3) annual pathogen and vector attraction reduction forms, 4) annual field summary forms and metals field loading summary forms, 5) lab sheets, and 6) soil analysis reports. Brunswick County land applied a total of 74.73 dry tons of biosolids under Permit No. WQ0034513 during the 2020 calendar year (West Brunswick Regional WWTP-60.90 dry tons and Ocean Isle Beach WWTP-13.83 dry tons. If there is any further information required or questions regarding this annual report please do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations with Brunswick County at (910) 253-2485 or Rob Willcox with WMSS for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabc )O� Agronomist/Partner Enclosures ._� 4110_1c� Rob Willcox, L.S.S. Soil Scientist/Partner SharedlWMSS Projecls12015115-04 Bnanswick Counly\Phase 12 - 2020 Annual ReportUass 812020 CLASS B ANNUAL REPORT - Brunswick County.doc Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Madin 336.312.1396 /www.willcoxmabesoil.com TABLE OF CONTENTS SECTION NO. TITLE Annual Land Application Certification Forms (Form ACF) II Annual Residual Sampling Summary Forms (Form RSSF) III Annual Pathogen and Vector Attraction Reduction Forms (503 Rules) (Form PVRF 503) IV Annual Land Application Field Summary Forms and Annual Metals Field Loading Summary Forms (Form FSF and MFLSF) V Lab Sheets VI Soil Analysis Reports Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 RESIDUALS LAND APPLICATION PROGRAM CLASS B RESIDUALS PERMIT NO. WQ0034513 OCEAN ISLE BEACH WWTP PERMIT NO. WQ0006085 WEST BRUNSWICK REGIONAL WWTP PERMIT NO. WQ0023693 Mr. Donald Dixon, Deputy Director of Wastewater Operations Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 (910) 253-2485 2020 Ocean Isle Beach WWTP Dry Tons - 13.83 2020 West Brunswick Regional WWTP Dry Tons - 60.90 Total Dry Tons - 74.73 2020 Ocean Isle Beach WWTP Dry Metric Tons - 12.54 2020 West Brunswick Regional WWTP Dry Metric Tons - 55.24 Total Dry Metric Tons - 67.78 Brunswick County 2020 Summary (Class B - Permit No. WQ0034513) West - B Ocean Isle - B January 45,500 February March 156,000 April 153,000 May 201,000 June July August September October November December Total Gallons 354,500 201,000 Total DT 60.90 13.83 SECTION I ANNUAL LAND APPLICATION CERTIFICATION FORMS (Form ACF) ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 Facility Name (as sh Counh Brunswick Year: 2020 own on permit). Brunswick County Land Application Operator: Bio-Green Services, Inc, Phone: 336-9404544 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes13 No -if No, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. ........oul-1-dr- West BrunswickRegional WWTP Total number of application fields in the penuit: 13 Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: 60.90 Total number of acres utilizes for land application during the year,-1 48.0 Part B - Annual Com iance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. ® yes 11 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was perfonned and three (3) copies of certified laboratory results are attached, 5) All other monitoring was performed in accordance with the pemyit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . I I05(a) or the Pollutant Loading Rates in I5A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. w 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: i "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Donald B, Dixon - Deputy Director � Permittee Name and Title (type or print) Sig ratur f Pern]ittee ` Date Signatur reparcr* West Brunswick WWTP Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) DENR FORM ACF (12/2006) ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034513 County: Facility Name (as shown on permit): Land Application Operator: Brunswick Year: 2020 Brunswick County Bio-Green Services, Inc. Phone: 336-9404544 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Ocean isle Beach WWTP Total number of a lication fields in the permit: 23 Total number of fields utilized for land application during the year:1 1 Total amount of dry tons applied during the year for all application sites: 13.53 Total number of acres utilizes for land application during the year: 16.5 Part B - Annual Coin lance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-I3 below) issued by the Division of Water Resources. M Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. ) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and Iime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached, 4) AnnuaI TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in I5A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1 I05(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I I I 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements iii the permit were complied with or, in the case of a deviation, prior authorization was received fi•om the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations arc attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Donald B. Dixon - Deputy Director �� 1 i Permit#ce Name and Title (type or print) Sib tat of P is V pate i oa/ Signature reparer" Ocean Isle Beach WWTP Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T . 1102 (26) OENR FORM ACF (I2/2005) SECTION II ANNUAL RESIDUAL SAMPLING SUMMARY FORMS (Form RSSF) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORINI RSSF - B WQ Permit Number: WQ0034513 Laboratory: 1) Envirorunental Chemists, Inc. Facility Name: Brunswick County 2) Residual Source WQ # or 3) NPDFS #: WQ0006085 4) WWTP Name: Ocean Isle Beach WWTP 5) Residual Analysis Data Conc. Sample or Composite Date Parameter Limit (mg/kg) , �m k ): 01 /08/20 Percent Solids (°f°) NA 1.65 Arsenic 75 14.60 Cadmium 85 14.60 Chromium NA 14-60 Copper 4,300 269 Dead 840 14.60 Mercury 57 1.84 Molybdenuin 75 14.60 Nickel 420 14.60 Selenium 100 14.60 Zinc 7,500 655 Total Phosphorus NA 15,500 TKN NA 38,100 Anunonia-Nitrogen NA 1,230 Nitrate and Nitrite NA 25.60 " For surf ice disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." OF -3-? Signature of purer * Date reparcr is defined in AO CFR. Pair 503.i(i.) -gild 1 SA NCAC 2T .1 COz (2G) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM •- B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year, Use additional forms as needed. WQ Permit Number: WQ0034513 Facility Name: Brunswick County Residual Source NPDES # or WQ#: WWTP Name: WQ0006085 Ocean Isle Beach WWTP Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." r Signature Date *Preparer is defined in 40 Cl-R Pa it 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0034513 Laboratory: 1) Facility Name: Brunswick County Z) Residual Source WQ # or WQ0023693 3) NPDES #: 4) WWTP Name: West Bnmswick Regional WWTP 5) Residual Analysis Data Conc. Sample or Composite Date Parameter Limit (mg/kg) (mg/kg)a 03/11/20 Enviromnental Chemists, .Inc. Percent Solids (%) NA 4.12 Arsenic 75 10.2 Cadmium 85 6.04 Chromium NA 38.4 Copper 4,300 544 Lead 840 20.2 Mercury 57 1.5 Molybdenum 75 12.9 Nickel 420 23.5 Selenium 100 6.04 Zinc 71500 1,640 Total Phosphorus NA 72.500 TKN NA 65,200 Ammonia -Nitrogen NA 36,700 Nitrate and Nitrite NA 108 ' For surface disposal facilities the ceiling concentration limits listed in this form arc not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittin -false information, including the possibility of fines and imprisonment for knowing violations." Sienature of 1 risrer * Dale - - -- .-.... s --_ ....---------- --- t-----._.�_. _ ---- - -- - --_-------- -_- —.I--,------- - . --- ... _ .. -.-. - . - --- *I'rcl�arer is defined in 40 CFR Part503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM _ B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0034513 Laboratory: ]) Environmental Chemists, Inc. Facility Name: Brunswick County 2) Residual Source 3) NPDES # or WQ#: WQ0023693 4) WWTP Name: West Brunswick Regional VL'WTP S) Residual Analysis Data Sample or Composite Date Parameter (mg/kg) 03/11/20 Alurninum 35,200 Calcium 24,300 Magncsiurn 4,270 PH 8.00 Potassium 4,930 Sodium 2,180 SAR 0.69 "t certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted:. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." Signature of Warel. * Date *Prepares is defined in 40 CkR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) SECTION III ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS (503 RULES) (Form PVRF 503) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WWTP Name: Ocean Isle WWTP NPDES Number: Monitoring Period: From l/1/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: WQ0034513 WQ0006085 Class A: Alternative 1 E d Alternative 2 Ei Alternative 3 D Alternative 4 .A Alternative 5 i Alternative 6 0' If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 11 Heat Drying 0 1 Heat Treatment D Thermophilic E] Beta Ray El Gamma Ray C! Pasteurization: E. Class B: Alternative 1 El Alternative 2 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 1 Air Drying]-J Composting 0 lAerobic Digestion Iwo Anaerobic Digestion C s If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number of Excee- deuces Frequency of Analysis Sample Type Analytical Tech -pique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) F1 Alt. 2 (40-day bench) 0 Alt. 3 (30-day bench) f_f ,4 Alt.(Spec. 0, uptake) s Alt. 5 (14-Day Aerobic) =, Alt. 6 (Alk. Stabilization y� Alt 7 (Drying - Stable) ILJ I Alt. 8 (Drying - Unstable) Alt. 9 (Injection) Alt. 10 (Incorporation)j No vector attraction reduction alternatives were performed l CERTIFICATION STATEMENT (please -,check the appropriate statement) "I certify, under penalty of law,�that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Ray Gambill - President (BioGreen) Preparer Name and Title (type or print) Signatur f Preparer* Date Land AppIier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WWTP Name: West Brunswick Regional WWTP NPDES Number: Monitoring Period: From 1/1/2020 To 12/31/2020 Pathogen Reducti 40 CFR 50 a on { 332) -Please indicate level achieved and alternative performed.: Class A: Alternative I ❑ Alternative 2 ❑ Alternative 3 Alternative 4 ❑ Alternative 5 ❑ Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 El Altemative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens' Lime Stabilization ❑ Air Drying[] Composting lAcrobic Dine: Nstion ❑ to alternative oerfc Parameter Allowable Level in Sludge 2 x 10 to the FcFu 6th power per gram of Fecal Coliform total solids 1000 mpn per gram of total solid (dry Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction Alt.l (VS reduction) ❑ Al Alt. 5 04-Day Aerobic) ❑ Al Alt. 9 (Injection) AI s A or Class B) complete the Pathogen Density Geo. MeanjMaximunA Units 40 I 41 43 indicate option perfa WQ0034468 . WQ0023693 I ■ ■ tion El monitoring data: Frequency I Sample Ana Sxccc- denees lofAiialysisType Tech 0 1 Quarterly) Grab ❑ Alt. 3 (30-day bench) ❑ JAIt. 4 (Spec. Oz uptake) [] ❑ A10(Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) E] ❑ No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tim Webb - Wastewater Superintendent Ray Gambill - BioGreen Preparer Name and Title (type or print) Sand Ap ' r N me d. Title (if applicable)(type or print) Signature of Preparer* Date Si,, attire of Land Ap"Iier (ir applicable) Date ) CFR 503.33) - PI 2 (40-day bench) 6 (Alk. Stabilization 10 (Incorporation) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Brunswick County WQ Permit Number: WQ0034468 WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693 Monitoring Period: From 1/1/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 0 Alternative 2 E_) Alternative 3 lJ Alternative 4 0 Alternative 5 1:1 Altei native 6 �� If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying L1 Heat Treatment EJ Tbermophilic !I Beta Ray CE Gamma Ray 01 Pasteurization D Class B: Alternative 1 i -1 Alternative 2 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization E I Air DryingE, Composting i 3 jAcrobic Digestion D Anaerobic Digestion i s If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g ry Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech-nique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per grain of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal conform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.I (VS reduction) 0 Alt. 2 (40-day bench) iL! Alt. 3 (30-day bench) EI jAlt. 4 (Spec. 0, uptake) Alt. 5 (14-Day Aerobic) � 7 Alt. 6 (Alk. Stabilization L;�] Alt 7 (Drying - Stable) Q I Alt. 8 (Drying - Unstable) Alt. 9 (Injection) i..j Alt. 10 (Incorporation) Ej No vector attraction reduction alternatives were performed �1 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you cheek this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Ray Garnbill, President - BioGreen Prepare ame and Title (type or print) Signatu of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) SECTION N ANNUAL LAND APPLICATON FIELD SUMMARY FORMS ANNUAL METALS LOADING SUMMARY FORMS (Form FSF and MFLSF) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied: 48.16 Owner: Guy A. Hughes Etals Operator: Site #: NC-BR-AH Field #: 1 Al Hughes Acres Utilized: 16.50 Predominant Soil Series: Lynchburg-Ly Acres Permitted: 16.50 r y 0 Q Specify Totals r Acre % Solids Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Diy, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- all- zation Rate TKN Amino - ❑ia- Ni- tro en g Ni-trate and Nitrite PAN I PAN 2 Must Select Crop I Cro p or p Z E� Gal. L- CuNd. Report Totals in Gal. Crop 1 Crop 2 0 0.0000 0.000 0.000 1 0 0.0000 0.000 0.000 1 2 Mar-20 52,000 3,152 4.12 0.5414 West Brvnmick WWTP Dry <0.5" Inc. 1.00 0.30 65,200 36,700 108 49.118 ####### Soybeans 3 Apr-20 153,000 9,273 4.12 1.5931 Wesl Brunswick WWTP Dry <0.5 S 0.50 0.30 65,200 36,700 108 86.052 ####### Soybeans 4 May-20 201,000 12,182 1.65 0.8382 ocomIsle Beach WWTP Dry <05' S 0.50 0.30 38,100 1,230 25.60 19.616 ####### Soybeans 5 0 0.0000 0.000 0.000 6 0 0.0000 0.000 0.000 7 0 0.0000 0.000 0.000 8 0 0.0000 0.000 0.000 9 0 0.0000 0.000 0.000 10 0 0.0000 0.000 0.000 11 0 0.0000 0.000 0.000 12 TOTALS: 24,606 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.0669 0.0496 0.1843 2.7145 0.1085 0.0093 0.0782 0.1223 0.0496 7.9221 327.657 154,786 0.000 Date lbs/ac Current Cumulative lbs/ac 0.3409 0.2896 8.2743 3.0135 0.5595 0.0893 0.3892 0.5653 0.394G 29.2191 0.2740 1 0.2400 8.0900 0.2990 0.4510 0.0800 0.3110 1 0.4430 0.3450 21.2970 36 34 1 1,338 267 15 374 89 2,498 F 178 Prior Years Cumulative lbslac Permitted C. P. L. R_*** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significa enalties for submi ing false information, including the ossibility of fines and imprisonment for knowin(11 g violations." 06�16'lte� (YA - / �,-/ *Application Method: S - Surface, IN - Injection, INC Incorporation Signature o La Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loadina Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Dorm. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. nLRla rnonn rcr: fC/�nn21 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name. Brunswick County Total Dry Tons Applied (Annual): 48.16 Permit #: WQ0034513 Predominant Soil Series: Lynchburg-Ly Operator: Al Hughes Owner: Guy A. Hughes Etals Acres Used: 16.50 Acres Permitted: 16.50 Site #: NC-BR-AH Field #: I Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Corn- posite Date 3/11/20 3/11/20 5.i 1/8/20 61 7. 8.; 9.. 1fl..1 11_I 12: % Solids 4.12 4.12 1.65 Arsenic 10.2 10.2 14.60 Cadmium 6.04 6.04 14.60 ChronliLIM 38.4 38.4 14.60 Copper 544 544 269 Lead 20.2 20.2 14.60 Mercury 1.5 1.5 1.84 Molyb- denum 12.9 12.9 14.60 Nickel 23.5 23.5 14.60 Selenium 6.04 6.04 14.60 Zinc 1,640 1,640 655 Total Phos- hones 72,500 72,500 15,500 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 4-€ -.5.; ._6. 7' ._$.. .-P- 10.1 11 E 12 71 O a a v rD w_ 0' 0.5414 1.5391 0.8382 Arsenic 0 0 0.0110 0.0314 0.0245 0 0 0 0 0 0 0 0.0669 Cadmium 0 0 0.0065 0.0186 0.0245 0 0 0 0 0 0 0 0.0496 hromiun 0 0 0.0416 0.1182 0.0245 0 0 0 0 0 0 0 0.1943 Copper 0 0 0.5890 1.6745 0.4510 0 0 0 0 0 0 0 2.7145 Lead 0 0 0.0219 0.0622 0.0245 0 0 0 0 1 0 0 0 0.1085 Mercury 0 0 0.0016 0.0046 0.0031 0 0 0 0 0 0 0 0.0093 Molyb- denum 0 0 0.0140 0.0397 0.0245 0 0 0 0 0 0 0 0.0782 Nickel 0 0 0.0254 0.0723 0.0245 0 0 0 0 0 0 0 0.1223 Selenium 0 0 0.0065 0.0186 0.0245 0 0 0 0 0 0 0 0.0496 Zinc 0 0 1.7758 5.0482 1.0980 0 0 0 0 0 0 0 7.9221 Total Phos- 0 0 79.503 223.170 25.984 0 0 0 0 0 0 0 327.657 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information su mitted. 1 am aware that there are significant penalties for submitting false information, includi re ossi rty of fines and imprisonment for knowing violations" ignature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: Owner: PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied: 17.87 Guy A. Hughes Etals Site #: NC-BR-AH Field #: Operator: 2 Al Hughes Predominant Soil Series: Lynchburg-Ly Acres Utilized: 19.20 Acres Permitted: 19.20 o o Q S eci Totals Per Acre o /o Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. , Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od * Vola- tili- zation Rate** Miner- ali- zation Rate TKN Arxrrxro- nia- Ni- trogen Ni-trate and Nitrite PAN 1 PAN 2 Must Select Crop or CI Crop 2 Gal. rz Cu_Yd. Report Totals in Gal. Crop 1 Crop 2 0 0.0000 0.000 0.000 1 0 0.0000 0.000 0.000 2 Mar-20 104,000 5,417 4.12 0.9306 West Brunswick WWTF Dry <0.5" Inc. I.0 0.3 65,200 36,700 108 84.42I ####### Corn 3 0 0.0000 0.000 0.000 4 0 0.0000 0.000 0.000 5 0 0.0000 0.000 0,000 6 0 0.0000 0.000 0.000 7 0 0.0000 0.000 0.000 8 0 0.0000 0.000 0.000 9 0 0.0000 0.000 0.000 10 0 0.0000 0.000 0.000 11 0 0.0000 0.000 0.000 121 TOTALS: 15,417 As Cd Cr Cu Pb Hg I Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.0190 0.0112 0.0715 1.0125 0.0376 0.0028 0.0240 0.0437 0.0112 3.0524 134.937 84.421 0.000 Date I lbs/ac Current Cumulative lbs/ac 0.3410 0.2992 11.2145 1.3745 0.5486 0.0148 0.3930 0.5987 0.9602 131.0124 0.3220 0.2880 1 I.1430 0.3620 0.5110 0.0120 0.3590 0.5550 09490 27.9600 36 34 1,338 267 15 374 89 1 2,498 1 135 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significan p naities for submitt' b false information, including the possibility of fines and imprisonment for knowing violations." C % *Application Method: S -Surface, IN -Injection, INC -Incorporation Signature of and pplier Date **Volatilization Rate: Surface - 0.5, Infection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant LoadinLy Rate **A* The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1. nrhlq CnRhA CCG ICMnn21 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 17.87 Permit #: WQ0034513 Predominant Soil Series: Lynchburg-Ly Operator: Al Hughes Owner: Guy A. Hughes Etals Acres Used: 19.20 Acres Permitted: 19.20 Site #: NC-BR-AH Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 11 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 4,1 ...5,.1 s ..7 8 _91 Vi 1iI 121 "O rD -- w o' 0.9306 Arsenic 0.0000 0.0000 0.0190 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0190 Cadmium 0.0000 0.0000 0.0112 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0112 1lromiun 0.0000 0.0000 0.0715 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0715 Copper 0.0000 0.0000 1.0125 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 1.0125 Lead 0,0000 0.0000 0.0376 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0376 Mercury 0.0000 0.0000 0.0028 0.0000 0.0000 0.0000 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0.0028 Molyb- denum 0.0000 0.0000 0.0240 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0240 Nickel 0.0000 0.0000 0.0437 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0437 Selenium 0.0000 1 0.0000 0.0112 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0112 Zinc 0.0000 0.0000 3.0524 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 3.0524 Total Phos- 0.000 0.000 134,937 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 134.937 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includ ng the poss}bility o es and imprisonment for knowing violations" (( 6-2- 9 -2 Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF form and the mathematically linked FSF Form DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Brunswick County Permit #: WQ0034513 Annual Dry Tons Applied: 7.82 Owner: Harry Hart Operator: Harry Hart Predominant Soil Series: Rains-Ra Site #: NC-CO-HH Field #. 6 Acres Utilized: 12.30 Acres Permitted: 12.30 Specify ite o� Gal. Totals % Residuai Cond. Inches Appli- Vola- Miner- Arnrno- Must Select ,u Cu.Yd. Dry Tons Per Per Solid Sources Dry, Precip. cation tili- ali- Ni-trate nia- Crop 1 or Crop p Q Re port Acre s Acre (Summarize) TKN Past 24 Meth- zation zation and PAN 1 Ni- PAN 2 2 Totals in Gal. Wet, Moist Hrs. od* Rate** Rate Nitrite trogen CropTicrop 2 Jan-20 45,500 3,699 4.12 0.6355 West Brunwick WWTP M <0.5" Inc. 1.0 0.3 65,200 36,700 10$ 57.653 ####### Pines 0 D.D004 0.000 0.000 2 0 0.0000 0.000 0.000 3 0 0.0000 0.000 0.000 4 0 0.0000 0.000 0.000 5 0 0.0000 0.000 0.000 6 0 0.0000 0.000 0.000 7 0 0.0000 0.000 0.000 8 0 0.0000 0.000 0.000 9 0 0.0o0o 0.000 0.000 10 0 0.0000 0.000 0.000 11 0 0.0000 0.000 0.000 12 TOTALS: 3,699 As CdV.6914 Cu Pb Htr Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.0130 0.00850 0.0257 0.0019 0.0164 0.0299 0.0077 2.0844 92.148 57.653 0.000 Date lbs/ac Current Cumulative lbs/ac 0.0153 0.00850.7396 0.0383 0.0020 0.020 0.0340 0.0104 2.2417 Prior Years Cumulative Ibs/ac 0.0023 0.00090.0481 0.0126 0.0001 0.003 0.0042 0.0027 0.1572 Permitted C. P. L. R.*** 36 341,338 267 15 374 89 2,498 Permit PAN Limit Ist/2nd Crop 70 "I certify under nannity of Inw that th;Q A.,.....,, 4-, ,. - --.-_ .� -- --- .. 7 ____ _ ____.. �......,..., - - F& „Nun a. UIIuVL 111y U11 r%AJU11 ul su}lervision in accordance wltn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are 7 significan p nalties for submitti g false information, including the possibility of fines and imprisonment for knowing violations." -c:;2/? ) r 0-2'/*Application Method: S -Surface, IN - Injection, INC -Incorporation Signature of nd Applier Date **Volatilization Rate: Surface - 0.5, In i ection/I ncorp oration - 1..0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # L npNm GnRnn Gcr Ir/wwa1 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Brunswick County Total Dry Tons Applied (Annual): 7,82 Permit #: WQ0034513 Predominant Soil Series: Rains-Ra Operator: Harry Hart Owner: Harry Hart Acres Used: 12.30 Acres Permitted: 12.30 Site #: NC-CO-HH Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): .,7_ 2.f 3., 4' 51 .. a" 0.6355 Arsenic 0.0130 0.0000 0.0000 0.0000 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0130 Cadmium 0.0077 0,0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0,00001 0.0077 hMniul 0.0499 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0488 Capper 0.6914 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.00001 0.0000 0,0000 0.6914 Lead 0.0257 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0257 Mercury 0.0019 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0,0000 0.0019 Molyb- 0.0164 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0,0000 0.0164 denum Nickel 0.0299 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0,0000 0.0000 0.0000 0.0000 0.0000 0.0299 Selenium 0.0077 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 1 0.0000 0.0000 0.0000 0.0077 Zinc 2.4844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0,0000 0.0000 2.0844 Total Phos- 92.1475 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 92.1475 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the inform. 'on submitted. I am aware that there are significant penalties for submitting false information, including he possib ility o f' es and imprisonment for knowing violations" Si nahrre of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM FSF (5/2003) SECTION V LAB SHEETS BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 8, 2020 Ocean Isle Beach WWTP Permit No. WQ0034513 Mineralization Rate 0.30 1.65 % Solids 6.79 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (MgIKg x 0.002) Nitrogen (TKN) 3.810 38,100.000 76.200 Phosphorus 1.550 15,500.000 31.000 Potassium 0.903 9,030.000 18.060 PAN (injected)* 1.232 12,316.600 24.633 PAN (surface)* 1.170 11,701.600 23.403 Ammonia Nitrogen 0.123 1,230.000 2.460 Calcium 1.430 14,300.000 28.600 Calcium Carbonate Eq. --- --- --- Magnesium --- 6,050.000 12.100 Sodium --- 9,880.000 19.760 Sulfur --- --- Nitrate N / Nitrite N -- 25.600 0.051 Barium --- --- --- SAR 2.23 Chloride --- --- --- Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 3,310.00 6.620 Arsenic --- 14.60 0.029 75 Cadmium --- 14.60 0.029 85 Chromium --- 14.60 0.029 --- Copper --- 269.00 0.538 4,300 Lead --- 14.60 0.029 840 Mercury --- 1.840 0.004 57 Molybdenum --- 14.60 0.029 75 Nickel --- 14.60 0.029 420 Selenium --- 14.60 0.029 100 Zinc --- 655.00 1.310 7,500 Envirochem: 2020-00439 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. b ! 6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab ' 910.392.4424 Fax sn 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 r 910.347.5843 Lab/Par Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Scott Leonard Report #: 2020-00439 Project ID: Ocean Isle Beach Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01061 Site: DIB IIWINTP 1/8/2020 9:55 AM Solid/Sludge Scott Leonard Test Method Results Date Analyzed Chlordane (TCLP) SW 646 Method 80B1B13510 <0.02 mg/L 01/22/2020 Endrin (TCLP) SW 846 Method w81B13510 <0.0005 mg/L 01/22/2020 Heptachlor (TCLP) SW 846 Method 8081 B13510 <0.0005 mg/L 01/22/2020 Heptachlor epoxide (TCLP) SW 846 Method 80816/3510 <0.0005 mg/L 01/22/2020 Lindane (TCLP) SW 846 Method 80811313510 <0.0005 mg/L 01/22/2020 Methoxychlor (TCLP) SW 846 Method 8081B1351a <0.0005 mg/L 01/22/2020 Toxaphene (TCLP) SW 846 Method 8081 B13510 <0.05 mg/L 01/22/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050mg/L 01/22/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 0270/3510 <0.050 mg/L 01/22/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 827o13510 <0.050 mg/L 01/22/2020 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 Hexachloro-1 ,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0,050 mg/L 01/22/2020 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Pentachiorophenol (TCLP) 5W 846 method 827013510 <0.250 mg/L 01/22/2020 Pyridine (TCLP) SW 846 method 827013510 <0.050 mg/L 01/22/2020 2,4,5-TP (TCLP) SVV846 Method 8151A <0.0003 mg/L 01/23/2020 2,4-D (TCLP) SW646 Method 8151A <0.0003 mg/L 01/23/2020 1,1-Dichloroethylene (TCLP) SW846 Method 826015030 <0.01 mg/L 01/15/2020 1,2-Dichloroethane (TCLP) SW846 Method 826015030 <0.01 mg/L 01/15/2020 Benzene (TCLP) SW846 Method8260/5030 <0.01 mg/L 01/15/2020 Carbon Tetrachloride (TCLP) SW846 Method 6260/5030 <0.01 mg/L 01/15/2020 Report #:: 2020-00439 Page 1 of 3 IV Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392-0223 Lab ° 910.392.4424 Fax 710 Bowserlown Road, Manteo, NC 27954 • 252.473.3702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28340 ` 910.347.5843 Lab/Fax < ih . Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Scott Leonard Report #: 2020-00439 Project ID: Ocean Isle Beach Chlorobenzene (TCLP) SW846 Method 826o15o90 <0.01 mg/L 01/15/2020 Chloroform (TCLP) SW846 Method826015030 <0.01 mg/L 01/15/2020 Methyl ethyl ketone (TCLP) SW646 Method 826015o30 <0.05 mg/L 01/15/2020 Tetrachloroethylene (TCLP) SW846 Method 62601503D <0.01 mg/L 01/15/2020 Trichloroethylene (TCLP) SW846 Method 6260/5030 <0.01 mg/L 01/15/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/15/2020 RCI Cyanide EPA335.4 <0.125mg/kg 01/13/2020 Sulfide SM 4500 S D 0.60 mg/kg 01/22/2020 Ignitability SW 846 method loto >210'F 01/13/2020 pH SW 846 Method 9045D 6.79 units 01/20/2020 Sludge Residuals Aluminum EPA 200.7 3310 mg/kg 01113/2020 Arsenic EPA200.7 <14.6mg/kg 01/13/2020 Cadmium EPA 200.7 <14.6mg/kg 01/13/2020 Calcium EPA200.7 14300mglkg 01/13/2020 Chromium EPA200,7 <14.6mg/kg 01/13/2020 Copper EPA 200.7 269 mg/kg 01/13/2020 Lead EPA 200.7 <14.6 mg/kg 01/13/2020 Magnesium EPA 2003 6050 mg/kg 01/13/2020 Molybdenum EPA 2003 <14-6 mg/kg 01/13/2020 Nickel EPA 200.7 <14.6mg/kg 01/13/2020 Potassium EPA 200.7 9030 mglkg 01/13/2020 Selenium EPA200.7 <14.6 mg/kg 01/13/2020 Sodium EPA 200.7 9880 mg/kg 01/13/2020 Zinc EPA 200.7 655 mg/kg 01/13/2020 Nitrate+Nitrite-Nitrogen EPA353.2 25.6mglkg 01/16/2020 Total Solids (%) SM 2540 8 1,65 % 01/10/2020 Ammonia Nitrogen SM 450o NH3 C 1230 mg/kg 01/10/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 38100 mg/kg 01/10/2020 Report M; 2020.W439 Page 2 of 3 Environmental. Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 " 910,392.0223 Lab ` 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax lSlRi 255-A Wilmington Highway, Jacksonville, INC 28540 ' 910.347.5843 Lab/Fax 1111 Mweilvtioi3men t Menem iss.com Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Scott Leonard Report #: 2020-00439 Project ID: Ocean Isle Beach Total Phosphorus SM 4500 P F 15500 mg/kg 01/16/2020 Mercury SWB46 74716 <1.84 mg/kg 01/17/2020 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 01/22/2020 Barium EPA 200.7 <1.0 mg/L 01/22/2020 Cadmium EPA 200.7 <1.0mg/L 01/22/2020 Chromium EPA 200.7 <1.0mg/L 01/22/2020 Lead EPA 200.7 <1.0mg/L 01/22/2020 Selenium EPA 200.7 <1.0 mg/L 01/22/2020 Silver EPA 200.7 <1.0 mg/L 01/22/2020 Mercury EPA 245.1 <0.0002 mg/L 01 /24/2020 Comment: Sludge residuals reported on a dry weight basis. Reviewed by; Report C 2020-00439 Paoe 9 of 3 ENVIRONMENTAL CHEMISTS INC 6602 Windmill Way C � Wilmington, NC 28405 Sample Collection and Chain of Custody Phone: (910) 392-0223 aio�� �" `�-i Fax (916) 392.4424 iient• L - i WAMP r c�lfected Report No: '� 3 axn le T e: I = ILxfluent E = Effluent W =Well ST =Stream S4 =Soil SL= Slud a Other: PRESERVATION Collection a ample Identification a sEaF E �U` e ° ' EC' p 4 C ANALYSIS ItEQiJESTiII HATE TIME TEMP U U U !Z x 0 Lj T 1m� 1 1. uf� Ta ��r C� C P Gi C P C P i --- _ G C P G C P G ja aid C P G G C P G G C P G G C P G I G I I I_ PH - : I � 7 C rransfer Relinquished By: Date/Time Received By: Date/Thne 011 CJ c !mperatu •e when Received:_ Accepted: Rejected: R�sample Reque ted: slivered y: — (�-c� Received By: �=. ;Gc�.: f Date: ! Time: 3 a �-- ShArMVIck County Lime StabllWP ,on Ph Test Resuft Knftr.- G&iNkag, Mc. 11"W10- "ty rm Tav re"ermm CarwWPh --- 12,7 I ]ROW 1% Tat rm* Temp 'emV Canvcted 1% 24 Hour Ph Test ��vl I rmle bqzz; I 0�1 IZ7 raw P-el 0 0 C). 6'. (10 45. BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 11, 2020 West Brunswick Regional WWTP Permit No. WQ0034513 Mineralization Rate 0.30 4.12 % Solids Class B 8.00 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 6.520 65,200.000 130.400 Phosphorus 7.250 72,500.000 t45.000 Potassium 0.493 4,930.000 9.860 PAN (injected)* 4.536 45,358000 90.716 PAN (surface)* 2.701 27,008.000 54.016 Ammonia Nitrogen 3.670 36,700.000 73.400 Calcium 2.430 24,300.000 48.600 Calcium Carbonate Eq. --- --- _-- Magnesium --- 4,270.000 8.540 Sodium --- 2,180.000 4.360 Sulfur --- --- Nitrate N / Nitrite N --- 108,000 0.216 Barium --- --- --- SAR 0.69 Chloride --- ___ Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 35,200.00 70.400 Arsenic --- 10.20 0.020 75 Cadmium -- 6.04 0.012 85 Chromium --- 38.40 0.077 --- Copper --- 544.00 1.088 4,300 Lead --- 20.20 0.040 840 Mercury --- 1.500 0.003 57 Molybdenum - - 12.90 0.026 75 Nickel --- 23.50 0.047 420 Selenium --- 6.04 0.012 100 Zinc --- 1,640.00 3.280 7,500 Env irochem: 2020-04194 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Ra:te)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection Iimits for calculation purposes. West Brunswick Regional WWTP Non -Discharge Permit No. WQ0034513 Class B - 2020 Sample Date Fecal Coliform MPN per gram Log 03/11/20 43 1.6335 03/11/20 41 1.6128 03/11/20 40 1.6021 03/11/20 42 I.6232 03/11/20 41 1.6128 03/11/20 41 1.6128 03/11/20 40 1.6021 Envirochem: 2020-04194 Total 1 11.2992 Average 1 1.6142 Geometric Mean 41 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 mets Class B -Alternative l Pathogen Reduction Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910-392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 o 252,473.5702 Lab/Fax 255-A Wilmi.ngton Highway, Jackson vi ile, NC 28540 a 910.347.5843 Lab/Fax info(irenviroumentalcheniists.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample 1D: Collect Date/Time Matrix Sampled by 20-10318 Site: Sludge 3/11/2020 12:10 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8081B13510 <0.02 mg/L 03/19/2020 Endrin (TCLP) SW 846 Method 8081813510 <0.0005 mg/L 03/19/2020 Heptachlor (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 03/19/2020 Heptachlor epoxide (TCLP) SW 846 Method 8081 B13510 <0.0005 mg/L 03/19/2020 Undane (TCLP) SW 846 Method 60818/3510 <0.0005 mg/L 03/1912020 Methoxychlor (TCLP) SW 846 Method $081B13510 <0.0005 mg/L 03/19/2020 Toxaphene (TCLP) SW 646 Method 8081B1351a <0.05 mg/L 03/19/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 027013510 <0.050 mg/L 03/20/2020 Cresol (TCLP) SW 646 method 8270/3510 <0,050 mg/L 03/20/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachlorobenzene (TCLP) SW 646 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachloroethane (TCLP) SW 645 method 8270/3510 <0.050 mg/L 03/20/2020 m + p-Cresol (TCLP) SW 845 method 8270/3510 <0.050 mg/L 03/20/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 o-Cresol (TCLP) SW 646 method 8270/3510 <0.050 mg/L 03120/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 03/20/2020 Pyridine (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 03/20/2020 2,4-D (TCLP) SWB46 Method 8151A <0.003 mg/L 03/20/2020 1,1-Dichloroethylene (TCLP) SW848 Method 8260/5030 <0.01 mg/L 03/25/2020 1,2-D4chloroethane (TCLP) SW846 Method 826015030 <0.01 mg/L 03/25/2020 Benzene (TCLP) SW846 Method 826015030 <0.01 mg/L 03/25/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <Q.01 mg/L 0312512020 ReportM: 2020-04194 Page i of 4 •Y'�� �' zY LT. {/ _ ,yi-• w { ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Irks 6602 Windmill Way, WiLrlington, NC 25405 a 910.392.0223 Lab a 910-392.4424 Fax 710 Bawsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax infoCgelivi ronmen taicltemist s.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Chiorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Chloroform (TCLP) SW846 Melhod 8260/5030 <0.01 mg/L 03/25/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 03/25/2020 Tetrachloroethylene (TCLP) SW846 method 8260/5030 <0.01 mg/L 03/25/2020 Trichloroethylene (TCLP) SW846 Method826015030 <0,01 mg/L 03/25/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 RCI Cyanide EPA 335.4 0.202 mg/kg 03/18/2020 Sulfide SM 4500 S D 2.50 mglkg 03/31/2020 Ignitability SW 046 method 101a >180 °F 03/27/2020 Sludge Residuals Aluminum EPA 200.7 35200mg/kg 03/16/2020 Arsenic EPA 200.7 10.2 mg/kg 03/12/2020 Cadmium EPA 200.7 <6.04 mg/kg 03/12/2020 Calcium EPA 200.7 24300 mg/kg 03/12/2020 Chromium EPA200.7 38.4 mg/kg 03/12/2020 Copper EPA 200.7 544 mg/kg 03/12/2020 Lead EPA 20o.7 20.2 mg/kg 03/12/2020 Magnesium EPA 2oo.7 4270 mg/kg 03/12/2020 Molybdenum EPA 200.7 12.9 mg/kg 03/12/2020 Nickel EPA 200.7 23.5mg/kg 03/12/2020 Potassium EPA 200.7 4930 mg/kg 03/12/2020 Selenium EPA 200.7 <6.04 mg/kg 03/12/2020 Sodium EPA 200.7 2180 mg/kg 03/12/2020 Zinc EPA 200.7 1640 mg/kg 03/12/2020 Nitrate+Nitrite-Nitrogen EPA353.2 108mglkg 03/23/2020 Total Solids (%) SM 2540 B 4.12 % 03/12/2020 pH SM 4500 H B S.00units 04102/2020 Ammonia Nitrogen SM 4500 NH3 C 36700 mg/kg 03/15/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 65200 mg/kg 03/15/2020 Report #:. 2020.04194 Page 2 of 4 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910-392,0723 Lab 9 910392,4424 Fax 710 liowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info i6onvironmcntalchcinists.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Total Phosphorus SM 4500 P F 72500 mg/kg 03/27/2020 Mercury SW046 7471B 1.50 mg/kg 03/13/2020 TCLP Metals Arsenic EPA 2007 <1,0 mg/L 03/19/2020 Barium EPA200.7 <1,Omg/L 03/19/2020 Cadmium EPA200.7 <1,0mg/L 03/19/2020 Chromium EPA 200.7 <1.0 mg/L 03/19/2020 Lead EPA 200.7 <1.0 mg/L 03/19/2020 Selenium EPA200.7 <1.0mg/L 03/19/2020 Silver EPA 2001 <1.0 mg/L 03119/2020 Mercury EPA245,1 <0,0002mg/L 03/19/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10319 Site: 1 3/11/2020 12:01 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids SM 2540 B 4.20 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <43 MPNIg 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10321 Site: 2 3/11/2020 12:02 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.46 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPNIg 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10322 Site: 3 3/11/2020 12:03 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 254o B 4.52 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPNIg 03/11/2020 Report #:: 2020.04194 Page 3 of 4 n Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab • 910.392.4424 Fax ' 710 Bocvsertown load, Manteo, NC 27954 8 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info a;environmcntalcnenlists.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10323 Site:4 3/11/2020 12:04 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.31 % 03/12/2020 Fecal Density SM 0221C E MPN 24 hr503 <42 MPN/g 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10324 Site: 5 3/11/2020 12:05 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.44 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10325 Site: 6 3/11/2020 12:06 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (°1°) SM 2540 B 4.49 % 03/12/2020 Fecal Density SM92210EMPN 24hr503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-10326 Site: 7 3/11/2020 12:07 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%] SM 2540 B 4.53 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPN/g 03/11/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: kgj�'du' Report ff:: 2020.04194 Page 4 of 4 Environmental Chemist, Inc., Wilmington, NC Lab 494 5602 Windmill Way Wilmington. NC 28405 310.392.0223 Sample Receipt Checklist Client: 01 }�� Date:.3.. D..... QEGaft Number: (� -- Receipt of sample: Delivered ❑ YES ❑ NO N/A 11 uP5 ❑ FedEx ❑ Other p C3 YES ❑ YO 1. Were custody seals present on the cooler? Original N/A 2. if custody seals were present. were the ghat temperature upon receipt -a ?r y intact/unbroken? How temperature taken: ❑ Tem corrected temperature upon receipt ,C IR Gun ID: Thomas Traceable 5/N 19251i657ture Blank Against Bottles ❑ YES ❑ NO 3. If temperature of cooler 'excceeded 6'C,un lwas Project M YES ❑ NO 4. Were proper Custody6 /OA notified? YES ❑ NO p procedures {relinquished/received) followed? 5• Were sam le 10 s listed on the COG? YE5 ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. 'Were collectio111 n date and time listed on st the COC? !�D YES ❑ NO 8, Were tests to be ed on the YES ❑ wO 9. Did samples arrive en Proper rformed eonta containers foreachtest? ES [�' VO W. Did samples arrive in good condition for each test? rES ❑ NO 11. Was adequate sample volume ava,Iable?' YES ❑ NO 12. Were samples received within proper holding time for re ues ❑ YES ❑ NO 13. Were acid preserved samples received at a Q red tests? l ❑ YE5 0 . NO NO 1q, WpH of aZ? YES ere cyanide samples received at a PH'12 i ❑ 15. 'Were sulfide samples received at a pH >9? 1 ❑ YES ❑ NO 16. were NH3/TKN/Phenol received at a chlorine residual of <O,g • ❑ YES ❑ V0 17. Were Sulfide/Cyanide received at a chlorine residual of cp rn /L? ITOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. " 8acterla samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: I, Must be completed for any samples) incorrectly preserved or with h Sample(s) vere received incorrect) eadspace) by adding (circle one): { SDa `1N0 y Preserved and were adjusted accordingly Time of oreservation: �l[I `la0H f more than one preservative �s needed, n Note: Notify customer service ;mm notate in ediamy for incorrectly preserved samples. Obtain a new sample or ammen[5 below nOtlfy the Rate lab d directed to anaivzed by the custom Volatifes 5ample(s) ec .vho was �ot�fied, care and time. .,were received with headsoace CC]MMEiVTS: ENVIRONMENTAL CHEMISTS, INC 4W Sample Collection and Chain of Custody Client: Brunswick Co Public Utilities WEST BRUNSWICK REGIONAL Collected Bv: Brian Blanton Sample Type: I = Influent E = Effluent W =Well ST =Stream, SO =Soil, SL= Sludge v rua. Sample Identification WBR WBR WBR WBR WBR WBR WBR WBR TRIANNUA LS -�� W Q .a DATE Collecti TIME 3 - h - z� 10719 -„• Zo a =� �oIZ 3-1� to :L v 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (914) 392.4424 Dort No: ] - G((9H y PRESERVAT.ION o ANALYSIS REQUESTED U TERIP a SL X TCLP, Nutrients, mets Is, aCI SL C FECAL DENSITY G SL C tXV FECAL DENSITY G SL C FECAL DENSITY c SL C FECAL DENSITY X G SLC FECAL DENSITY X SL C P x FECAL DENSITY c SL C P) _ FECAL DENSITY c X C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Tinge 2. �.� Temperature when Received: Accepted: Rejected: Resample Requested: Delivere B Received By:.� Date: <, �%- Tim.e:�T.a ?--- - BrUnswick County Lime Stabilization Ph Too Remits Fkwkra B1"REEN .%rv(wZ, inc. Mudge SrsmRe: -a.Zg5__T ,,J_ —,eWWTp Permit Approximate Gallons., inifial Ph Test. Date Time 13 : 15 Opr ._ Ph _ - I ), - Z�— T , 5-a4 rempm wre Cor ftW P , 2 Hour Rh Test /s_ J3 , Operaor Hemp COt'.C6d Ph 24 Hour Ph Test ! ate Time 13 _---�IZ OpmataF _Gli r; 5 Ga�,D�.ftiu�v IMP corrected Ph a g v 3oa _ , r-_ ._ aa7 d ���� � �j �f i f`1,k�5�er �[� 5� PH TemPcrafure Correction Factors at Varying Temperatures froln Standard (25°C) f cinp�c I Caffedion FaoiOr 40 Pitts fi 45 3n Plus 0.42 39 Pius 0.39 37 Plusfl_36 36 Pfus 0.33 35 Pius f7.30 34 Pius 027 33 Plus 0.24 32 Plus02€ 31 Plus fi.i8 30 Pitts m,15 29 Pittsfi.i2 28 Plus 0.09 27 phis 0.06 26 PIus0.43 25 0.00 24 Minus .03 23 Minus 0.06 22 1:11nus 0.09 21 Minus 0.12 20 Minus 0.15 14 eXV=3:0.18 is Minusf}21 17 Mims 024 16 Mina5027 I5 Minus 0.30 14 Minns 0,33 13 MhIw 0.36 12 Minus o39 1€ 9W us0.42 10 Mittus 0.45 SECTION VI SOIL ANALYSIS REPORTS Page 1 of 4 Report Dumber: 21-015-0934 Account Number:46646 Send To: BID -GREEN SERVICES INC 383 PCITi-S RD ADVANCE NC 27006 0 Waypoint- ANALYTICAL "Every acre---Everyyear. ",. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Brunswick Co SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss An Ignition Water pH Date Received: 01/15/2021 Date Of Analysis: 01/1812021 Date Of Report: 01/18/2021 NC = Nnrth Carnlinn Fertilifv lnrlav vali is OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab o �0 Soil IblA s M3 K Mg Ca Na Soil Buffer H Field ID Number Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meg1100g 8GAH1 22336 2.4 90 125 VH 47 VL 111 H 611 M 28 L 5.6 6.80 1.3 5.5 MIN L NC = 104 NC = 24 BGAH2 22337 2.1 85 88 H 40 VL 106 H 544 M 22 VL 5.6 6.81 1.2 5.0 MINJ L NC = 73 NC = 20 BGAH3 22338 2-4 90 88 H 44 VL 109 H 577 M 26 VL 5A 6.77 1.6 5.6 L MIN NC = 73 NC = 23 1 BGPV1 22339 0.9 67 18 L 5 VL 15 H 75 L 17 H 5.4 6.91 0.2 0.8 VL MIN NC = 15 NC = 3 BGPV2 22341 0.4 57 20 L 5 VL 12 M 64 L -[-14 H 5.3 6.91 0.2 0.7 VLH NC = 17 NC = 3 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B Field ID SS % ado % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate mslcm Rate BGAH1 2.2 16.8 55.5 2.2 23.6 27 H 5.3 H 3 VL 347 VH 1.5 M 0.5 L NC=56 NC=132.5 NC=19 NC=75.0 BGAH2 2.1 17.7 1 54.4 1.9 1 24.0 28 H 3.7 H 2 VL 315 VH 1.1 M 0.5 L NC=58 NC=92.5 NC=13 NC=55.0 BGAH3 2.0 16.2 1 51.5 2.0 28-6 26 H 4.0 H 2 VL 329 VH 1.1 M 0.5 L NC=54 NC=100.0 NC=13 NC=55.0 BGPV1 1.6 15.6 46.9 9.2 25.0 19 M 0.5 VL 1 VL 43 H 0.2 VL 0.1 VL NC=40 NC=12.5 I NC=6 NC=10.0 BGPV2 1.8 14.3 45.7 8.7 28.6 1 20 M 0.6 VL 1 VLJ 32 H 0.2 VL 0.1 VL NC=42 NC=15.0 NC=6 NC=10.0 ,aVUJ k cN,=ac,n u�c pidrn dvdudme nuumnLs in me expiananan or symooiS: /a (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Baling after each value: VL {Very Low), L (Lowy, M {Medium), (pounds per acre), mslcm (milli -mhos per centimeter), meg1100g maximum of thirty days after testing. pp H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: 1iuvrc Mr &19wX' C.E.C. - Cation Exchange Capacity. Salts mslcm x $40 = ppm. .Analysis prepared by: waypointAnalytical Mrginle, Inc. Pauric Mc Groary Ph.D-, CPAg Page 2 of 4 Report Number: 21-015-0934 Account Number:46646 Send To: 310-GREEN SERVICES INC 383 POTTS RD ADVANCE NC 27006 Date Received: 01/15/2021 Date Of Report: 01/18/2021 o Waypoint.0 ANALYTICAL Every acre... Every year."rM SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Brunswick Co Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Field ID Intended Crop bu Tons1A N P205 K20 Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A IbIA Ib/A Ib1A IbIA IWA Ib/A BGAH1 Soybeans 45 0.8 15 0 105 0 0 1.4 4 0 0 0.5 BGAH2 Soybeans 45 0.8 15 30 108 0 0 2.2 4 0 0 0.5 BGAH3 Soybeans 45 1.3 15 30 106 0 0 2.0 4 0 0 0.5 BGPV1 Pasture 3 0.8 50 71 120 25 9 3.0 4 0 0.9 0.5 BGPV2 Pasture 3 0.8 50 67 120 25 8 3.0 4 0 0.9 0.5 I�.vmmen15: 22339 The sodium rating is high on this sample rather than optimum. Sample(s) : BGPVI,BGPV2 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made," Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �,uv,c �t Grow/ work,the results, or the company in any advertising, news release, or other public anounrements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg Page 3 of 4 Report Number: 21-015-0934 Account Number:46646 Send To: 610-GREEN SERVICES INC 383 POTTS RD ADVANCE NC 27006 Waypointo ANALYTICAL Every acre -Every year. "TM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Brunswick Co SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP BufferpH Loss pn Ignition Water pH Date Received: 01/15/2021 Date Of Analysis: 01/18/2021 Date Of Report: 01/18/2021 NC = North Carolina Fertilitv Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class lbs1A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H megN00g meq/10og SGH131 22342 1.7 78 688 VH 18 VL 32 L 363 L 17 VL 4.8 6.74 1.9 4.1 MIN L NC = 573 NC = 9 BGHH6 22343 0.6 61 I 23 L 5 VL 14 M 71 L 15 H 52 6.90 0.3 0.8 MIN VL NC = 19 NC = 3 1 BGCGS 22344 2.0 88 49 M 4 VL 17 L 80 VL 16 M 4.5 6.84 0.9 1.5 MIN L NC=41 NC=2 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K Mg Ca Na H NO,N S Zn Mn Fe Cu B. SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate BGHB1 1.1 6.5 44.3 1.8 46.3 18 M 23.6 VH 7 L 263 VH 4.1 VH 0.4 L NC = 37 NC = 590.0 NC = 44 NC = 205.0 BGHH6 1.6 14.6 44.4 8.2 37.5 19 M 0.7 VL 1 VL 44 H 0.2 VL 0.1 VL NC=40 NC=17.5 NC=6 NC=10.0 BGCG5 0.7 9.4 1 26.7 1 4.6 60.0 41 VH 0.4 VL 1 VL 17 H 0.2 VL 0.1 VL NC=85 NC=10.0 NC=6 NC=10.0 values an utis report represent the piani availame nulnems in me txplanation of syrnWis: % (percent), ppm (parts per million), Ibs/A This report apprise to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), megt100g maximum oithirty days after testing. rJ H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs1A, Soluble by: q"., Mir (rroug/ C.E.C. - Cation Exchange Capacity. Salts mslem x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. u Pauric Mc Groary Ph.D., CPAg Page 4 of 4 Report Number: 21-015-0934 Account Number:46646 Send To: BIO-GREEN SERVICES INC 383 POTTS R❑ ADVANCE NC 27006 Date Received: 01/15/2021 Date Of Report: 01/18/2021 s Waypoint.. ANALYTICAL Every acre... Everyyear. ",N SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 304-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: Brunswick Co Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons1A Ib1A Ib1A Ib1A Ib1A Ib1A Ib1A Ib1A Ib1A Ib/A Ib1A BGHB1 Pasture 3 1.5 50 0 120 19 10 0 3-F 0 0 0 13GHH6 Pines 3 0.8 50 61 120 25 9 T73-0 4 0 0.9 0.5 BGCG5 Pasture 3 1.0 50 40 120 25 0 3.0 4 0 0.9 0.5 [:omments: Samples): BGCG6,BGCG5 Crop: Pasture For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer. For soils low in sulfur, apply 20-40 Ibs of sulfur as a sulfate in the spring with the nitrogen. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �RWic jot (r/owcf/ Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the oD work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric Mc Groary Ph.D., CPAg