WQ0011431_Residual Annual Report 2020_20210223

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0011431
Applicant/Permittee Town of Cleveland
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd
.......................................................... ronc su_ -
Name * Rob Willcox
Email Address*
[e-mail]
Project Information
........ .....................................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363399128
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0011431
Fbs Current Existing perm number
Applicant/Permittee Address* Post Office Box429; Cleveland, N.C. 27013
Facility Name * Town of Cleveland RLAP
Please provide comments/notes on your current submittal below.
2020 Annual Report Submittal on behalf of BioGreen for Town of Cleveland
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Town of Cleveland-2020 NCDEQ Annual Report-
9.22MB
WQ0011431.pdf
Upload only 1 PCF docurrent (less than 250 M3). Miltiple docurrents must be combined into one PDF file unless file is larger than
upload linit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
� wl�
Submission Date 2/23/2021

2020 ANNUAL REPORT
LAND APPLICATION PROGRAM
TOWN OF CLEVELAND
PERMIT #WQ0011431
Compiled by:
Bio-Green Services, Inc.
383 Potts Road
Advance, NC 27006
January 2021

February 1, 2021
NCDEQ- DWR
91' Floor, Office # 942W
512 N Salisbury Street
Raleigh, NC 27604 1170
Attention: Non -Discharge Branch
Reference: 2020 LAND APPLICATION ANNUAL REPORT
TOWN OF CLEVELAND
Permit No. WQ0011431
Non -Discharge Branch:
Bio-Green Services, Inc.is submitting all monitoring and reporting requirements as
specified in the above referenced permit. Bio-Green compiled this report using data
gathered during the compliance year by Bio-Green and The Town of Cleveland. This
data includes:
]-Annual Land Application Certification Form
II - Annual Residual Sampling Summary Form
III- Annual Land Application Field Summary Form
IV - Lab Sheets
V - Annual Pathogen and Vector Reduction Forms
VI - Soil Analysis
If there is any further information required or questions regardingthis annual report
please do not hesitateto contact Bio-Green forfurther assistance.
Sincerely,
V
Ray Gambill

Town of Cleveland
PO Box 429
Cleveland, NC 27013
704-278-4777
NC PERMIT# NC 0049867
Patrick Phifer-Mayor Town of Cleveland
PO Box 429
Cleveland, NC 27013
704-278-4777
LAND APPLIER:
Bio-Green Services, Inc.
383 Potts Road
Advance, NC 27006
Total DryTons - 10.17
Total Metric DryTons - 9.22

TABLE OF CONTENTS
SECTION NO.
I
II
III
IV
V
VI
TITLE
Annual Land Application Cc
Form ACF
Annual Residual Sampling S
Form RSSF
Annual Land Application Fi4
Form FSF
Lab Sheets (Analytical Data)
Annual Pathogen and Vector
Soil Analysis
kation Form
mary Form
Summary Form
Forms

ANNUAL LAND APPLICATION CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0011431 County:
Facility Name (as shown on permit):
Land Application Operator:
Rowan
Bio-Green Services, Inc.
Year: 2020
Town of Cleveland
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the ermit:
1
Total number of fields utilized for land application during the year:
I
Total amount of dry tons applied during the year for all application sites:
10.17
Total number of acres utilizes for land application during the year:
10
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
S) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations." "') , X //A
f�y�,��l�/lZF�i2 /yj,��d►� 02 /71Zoz1
Permittee Name and Title (type or print) Signature of Per ittee Date
E:L
Signature of Preparer* VU Date Sig re of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)
Date
DENR FORM ACF (12/2008)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your hermit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0011431 Laboratory:
Facility Name: Town of Cleveland
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analvsis Data
NCO049867
Cleveland WWTP
1) Statesville Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Cone.
Limit
Sample or Composite Date
2/26/20
Percent Solids (%)
NA
1.29
Arsenic
75
1.45
Cadmium
85
0.527
Copper
4,300
366
Chromium
NA
na
Lead
840
2.143
Mercury
57
0.766
Molybdenum
75
4.26
Nickel
420
8.22
Selenium
100
5.04
Zinc
7,500
721
Total Phosphorus
NA
3411
TKN
NA
43498
Ammonia -Nitrogen
NA
260.465
Nitrate and Nitrite
NA
7279.07
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under Penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false i0ormation, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0011431
Facility Name: Town of Cleveland
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
NCO049867
Cleveland WWTP
Laboratory: I) Statesville Analytical
2)
3)
4)
5)
Parameter
CompositeSample or Date
Potassium'
1
-----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * UV
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
ate
DENR FORM RSSF - B (12/2006)

ANNUAL LAND APPLICATION SUMMARY FORM

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Cleveland WQ Permit #: WQ0011431 Field #: 1 Acres Utilized: 10
Land Owner: Town of Cleveland Annual Dry Tons Applied: 10.1669 Site #: NC-RA-01 Acres Permitted: 10
Operator: Same Predominant Soil Series: Enon Cation Exchange Capacity (non 503): _
Crop I Name: Fescue Crop 1 Max. PAN: 188 Crop 2 Name: Fescue Crop 2 Max. PAN:
y
�? p
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
u
/u
Solids
Volume
Applied per
pp ' p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES # WQ#
'
Fert., Animal
Waste etc)
Soil
Cond.
(Dry,
Wet,
Moist
Precip.
Past 24
Hrs.
inches
Y
7
cD 'S
a w
0
°
o
=
*
o'
TKN
mg/kg
Z a
El
o
g
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop ]
Crop 2
0.000
0.000
0.000
0.000
March
67500
1.29
0.363
TOC
Dry
0
S
0.5
0.3
43497.7
260.465
7279.07
I4.800
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Sept
54000
1.29
0.290
TOC
Dry
0
S
0.5
0.3
43497.7
260.465
7279.07
11.940
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
Dec
67500
1.29
0.363
TOC
Dry
0
S
U
0.3
43497.7
260.465
7279.07
14.800
NA
Fescue
Residuals Applications totals on FORM
FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
189000
::::,::::::]"
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
41.441
0.000
Lime Applied
Annuallbs/acre
0.003
0.015
0.018
36
0.001
5.49
5,491
34
0.744
21.406
22.150
1338
#######
0.055
#######
na 1
0.004
0.019
0.023
267
0.002
0.024
0.026
15
0.009
0.516
0.525
na 1
0.017
0.589
0.606
374 1
0.010
0.001
0.011
89
1.465
50.198
51.663
2498
6.931 =:
=::
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified ,personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
ignature of Land Applier Date aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
._..res Used:
Town of Cleveland
WQ0011431
Bio-Green Services, Inc. Owner:
10 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Town of Cleveland Predominant Soil Series:
10
Site #: NC-RA-01 Field #:
10.16
Enon
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kz % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2
3
2/26/20
4
5
_BJ
2/26/20io
11
12
2/26/20
% Solids
1.29
1.29
1.29
Arsenic
1.45
1.45
1.45
Cadmium
0.527
0.527
0.527
Copper
366
366
366
Chromium
na
na
na
Lead
2.143
2.143 1
2.143
Mercury
0.766
0.766
0.766
Molyb-
denum
4.26
4.26
4.26
Nickel
8.22
8.22
8.22
Selenium
5.04
5.04
5.04
Zinc
721
721
721
Total
Phos-
horus
3411
3411
3411
Annual Heavy lvletal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
Loi
iLi
12
`/Ac./
_2J
c
App.
rt
Event
0.363
0.290
0.363
y
Arsenic
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.001
0.000
0.000
0.001
0.003
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.000
0.000
0.266
0.000
0.000
0.000
0.000
0.000
0.212
0.000
0.000
0.266
0.744
Chromium
0.000
0.000
######
0.000
0.000
0.000
0.000
0.000
######
0.000
0.000
######
######
Lead
0.000
0.000
0.002
0.000
0.000
0.000
0.000
0.000
0.001
0.000
0.000
0.002
0.004
Mercury
0.000
0.000
0.001 7
0. 000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
0.002
Molyb
denum
0.000
0.000
0.003
0.000
0.000
0.000
0.000
0.000
0.002
0.000
0.000
0.003
0.009
Nickel
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.005
0.000
0.000
0.006
0.017
Selenium
0.000
0.000
0.004
0.000
0.000
0.000
0.000
0.000
0.003
0.000
0.000
0.004
0.010
Zinc
0.000
0.000
0.523
0.000
0.000
0.000
0.000
0.000
0.418
0.000
0.000
0.523
1.465
Total
Phos-
0.000
0.000
2.476
0.000
0.000
0.000
0.000
0.000
1.978
0.000
0.000
2.476
6.931
horus
1 certiry, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
C� .natur Lan Applier
Date
DENR FORM MFLSF (12/2006)

ML. Transportation/Application Log
For Liquid Biosolids
Name: 1 ci Y� Project:_] ] eV Date:
Vehicle No: Quantity: ik5.
ao Hub Meter -Start: Hub Meter -Stop:
Alkaline Stabilization: Yes ❑ No
Temperature:
Site Conditions:
Rainfall:
>90 70-90
Dry Moist
<V27 rainfall
32-70—
Wet
<32 Miles to Field
>'1:` rainfall
Time At
Field
Field
No.
AA
Me;t�
(SI
=��W
EMMMMM
MMMIMM
===FMM
MMMAMM
M=rM==
Comments: l *Application method: S=Surface; SR=Surface with Incorporation; I=Injection
❑Certified Operator
Inspected Signature rcense o. p rator s Signature
White —Office / Yellow —Client / Pink Trucker

01,
Transportation/Application Log
For Liquid Biosolids
Name: /� k �L� wr�r'> �o Project: f o'e-�w a f C %gtlT -- Z— 2Z
Vehicle No: l D � Quantity: _ mod C/ Herb Meter -Start: Hub Meter -Stop:
Alkaline Stabilization: Yes C7 No Q
Temperature: >90 0-9 32-70 <32 Miles to Field
Site Conditions: Dry Moist Wet
Rainfall: <`/" rainfall >'/2 rainfall
Time At
Field
Emma
MethodM:
===mom
MMMMEM
MMMMM
==
m9m
WMMMMNN�
MMMMFM����WMMMM
i
MMMMM
MMMMEM
MMMMM
mmmm
MMMMM
MMMMM
MMMMM
==W==
MMMMM
MMMMM
MMMMM
Comments:
`Application method: S=Surface; S/I=Surface with Incorporation; 1=Injection
❑Certified Operator
Inspected Signature WeraSignature
White -Office / Yellow -Client / Pink -Trucker

Transportation/Application Log
,UL For Liquid Biosolids
Name: Al t ev-" Project: C / e"�, l/ f-srz ' Date:
Vehicle No: /0 Quantity: "/ <9Q Hub Meter -Start: Hub Meter -Stop:
Alkaline Stabilization: Yes ❑ No Q"
Temperature:
Site Conditions:
Rainfall:
>90 70-90
Dry Dist
<V2" rainfa
<32 Miles to Field
>'/Z' rainfall
Load
No.
WWTP
Time
Out
Time At
Field
Gallons
Landowner
Site No.
Field
No.%
Acres
Crop
Appi
Method
(S/SI/I)
f
3
4
5
6
7
9
10
It
12
13
14
15
16
17
18
19
20
Comments: *Application method: S-Surface; S/I=Surface with Incorporation; I=Injection
❑Certified Operator
Inspected Signature Eicense No. p to s Signature
White —office / Yellow -Client / Pink —Trucker

Transportation/Application Log
For Liquid Biosolids
Name:_ LEE Project: Cf egy104-v Date: 7 T/1�
-z�
Vehicle No: . Q F, Quantity: ZI5-00 Hub Meter -Start: Hub Meter -Stop:
Alkaline Stabilization: Yes CI No
Temperature: >90 70-90 2370 <32 Miles to Field
Site Conditions: Dry oist Wet
Rainfall: <V2" rainfall >%' rainfall
own
Appl E
MMMFMM
c Comments: / � ��- � :%- 6/ &'71P((1 Application method: S=Surface; S/I=Surface with Incorporation; I=Injection
Certified Operator
Inspected Signature ►cense o. Operator's mature
White -office I Yellow -Client / Pink -Trucker

LAB SHEETS

CLEVELAND WWTP
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 26, 2020
Date Reported: June 23, 2020
January 26, 2021
Cleveland WWTP Permit No. WQ0011431
Mineralization Rate 0.3 1.29 % Solids
0MY ptl
Parameter
%
Mg/Kg Dry Weight
(% x 10,00(
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
4.350
43,497.700
86.995
Phosphorus
0.341
3,411.000
6.822
Potassium
0.254
2,540.000
5.080
PAN (injected)*
2.051
20,510.706
41.021
PAN (surface)*
2.038
20,380.473
40.761
Ammonia Nitrogen
0.026
260.465
0.521
Calcium
2.470
24,700.000
49A00
Calcium Carbonate Eq.
---
---
---
Magnesium
---
1,620.000
3.240
Sodium
---
11,860.500
23.721
Sulfur
---
---
Nitrate N /Nitrite N
---
7,279.070
14.558
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
16,700.00
33.400
Arsenic
---
1.450
---
Cadmium
---
0.527
0.001
Chromium
---
---
---
Copper
---
366.00
0.732
Lead
- -
2.143
0.004
Mercury
---
0.766
---
Molybdenum
---
4.260
---
Nickel
---
8.22
0.016
Selenium
---
5.040
---
Zinc
---
721.00
1.442
Statesville Analytical 200226-21-01
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
2.24
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Analytical Results
Bio Green Services
383 Potts Road
Advance, NC 27006
Receive Date: 02/26/2020
Reported: 01 /26/2021
For: Cleveland Digester Sludge
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200226-21-01
Aluminum
CDigester
16700
mg/kg
EPA 200.7rev4.41994
02/27/2020
MD
200226-21-01
Ammonia Nitrogen
CDigester
260.465
mg/kg
SM4500NH3BE-1997
03/03/2020
WE
200226-21-01
Arsenic
CDigester
1.45
mg/kg
EPA200.8
03/05/2020
MT
200226-21-01
Cadmium ICP
CDigester
0.527
mg/kg
EPA200.7
02/27/2020
MD
200226-21-01
Calcium
CDigester
24700
Mg/kg
EPA200.7
02/27/2020
MD
200226-21-01
Copper
CDigester
366
mg/kg
EPA200.7
02127/2020
MD
200226-21-01
Lead -Solid
CDigester
2.143
mg/kg
SM3113B
03/06/2020
MD
200226-21-01
Mercury Solid
CDigester
0.766
mg/kg
SM3112&2011
03/03/2020
MD
200226-21-01
Molybdenum
CDigester
4.26
mg/kg
EPA200.7
02/27/2020
MD
200226-21-01
Nickel
CDigester
8.22
mg/kg
EPA200.7
02/27/2020
MD
200226-21-01
Nitrate/Nitrite -
CDigester
7279.07
mg/kg
SM4500FIA
03/02/2020
CL
Solids
200226-21-01
PAN
CDigester
207.1
mg/L
calculation
03/16/2020
CL
200226-21-01
Percent Solids
CDigester
1.29
%
SM254OB-2011
02/26/2020
MD
200226-21-01
pH
CDigester
6.09
Std. Units
$M4500HB-011
02/26/2020
CL
200226-21-01
Potassium - Solid
CDigester
2540
mg/kg
EPA200.7
03/06/2020
MT
200226-21-01
SAR
CDigester
2.24
%
calculation
03/16/2020
CL
200226-21-01
Selenium
CDigester
5.04
mg/kg
EPA200.8
03/05/2020
MT
Subcontracted
200226-21-01
Sodium - Solid
CDigester
11860.5
mg/kg
SM 3111 B
02/2712020
MD
200226-21-01
T. Phosphorus Solid CDigester
3411
mg/kg
SM4500PE-2011
02/28/2020
CL
200226-21-01
TCLP
CDigester
See Attached
as Noted
02/27/2020
PACE
200226-21-01
TKN
CDigester
43497.7
mg/kg
SM4500NorgB-2011
02/28/2020
CL
200226-21-01
Zinc
CDigester
721
mglkg
EPA200.7
02/27/2020
MD
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 1 of 34

Sample Number Parameter
200226-21-01 Magnesium
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Sample ID Result
CDigester 1620
Unit Method
Analyzed Analyst
mglkg EPA200.7 02/27/2020 MD
PO Box 228 • Statesville, NC 28687. 704/872/4697
Page 2 of 34

Condition of Receipt
Sample Number 200226-21-01 Temp on Arrival: 2.8
PH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Copper
Nitric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Sodium
Nitric Acid Chemicals in containers, lab
Received on Ice
pH on Arrival: <2 Parameter Schedule: Sodium - Solid
Nitric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Potassium
Nitric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Potassium - Solid
Nitric Acid Chemicals in containers, lab
Received on Ice
PH on Arrival: <2 Parameter Schedule:
Nitric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule:
Received on Ice
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 3 of 34

PH on Arrival: <2 Parameter Schedule:
PH on Arrival: <2 Parameter Schedule:
PH on Arrival: <2 Parameter Schedule:
Chemicals in containers, lab
Received on lee
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
Parameter Schedule: Percent Solids
Received on Ice
Chemicals in containers, lab
Parameter Schedule: pH
Received on Ice
Chemicals in containers, lab
Parameter Schedule: TCLP
Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: TKN
Sulfuric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen
Sulfuric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite
Sulfuric Acid Chemicals in containers, lab
Received on Ice
pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite - Solids
Sulfuric Acid Received on Ice
Chemicals in containers, lab
PH on Arrival: <2 Parameter Schedule: Phosphate, Total as P
Sulfuric Acid Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 24

Parameter Schedule:
Parameter Schedule:
Received on Ice
Chemicals in containers, lab
Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 34

Client:
,
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; Il?.C'uunsvilleSNU P.t9W 38
Slulesvillc. NC =ltifil;7
Address: � � j]
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(704) 872.46W
Chain of
Custody Record
Contact Person: Qry��•I Phone f(3-3 D t 3 pt)l 3 FAXII
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P b
PO N Requisitioned by, (Time Dale)
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Sam le to#
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Relinquished by:
Time 40
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am, pm Date ;�2f4f20 Transported by:
Relinquished by;
Time
am, pm Date /�/ Holding times met: ✓
Received by:
Time
am, pm Date 1_!_—
-
Com osite Sam I #1:
Compliance work:
Time begin am,
pm Date _J_I_
Non-compliance work:
Time end_ am,
pm Date hl
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Composite $Ampllnra 92:
� Lai Comments:
Samples Transported On Ice:
Time begin am, pm Date _I___,J_
Time end am, pm Date _/__!_.__
Initials:
n
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PaceAnalytical
www.pacalabs.com
March 17, 2020
Crystal Little
Statesville Analytical, Inc.
122 Court Street
PO Box 228
Statesville, NC 28687
RE: Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800 Kincey Ave. Suile loll
Hunlersville, NC 28078
[phone]
Dear Crystal Little:
Enclosed are the analytical results for sample(s) received by the laboratory on February 27, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, excepl in full,
fie` �1 without the writlen consent of Pace Analytical Services. 41-C
BQRr N
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Flo
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CERTIFICATIONS
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
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REPORT OF LABORATORY ANALYSIS
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PO Box 228 • Statesville, NC 28687 • 704/872/4697
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rj Pace Analytical Services, LLC
-Pacegnarl/ ical . 9800 Kincey Ave. Suite 100
/'irr yc [' Hunlersville, NC 26078
www.pacilabs.com [phone]
Project: CLEVELAND DIGESTOR
Pace Piojecl No.: 92467118
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REPORT OF LABORATORY ANALYSIS
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PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 9 of 34

►r
RaceAnalXical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800 K}ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab Ili Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92467118D01 200226.21
CPA8151A
LEL
3
PAN
EPA8081B
SEM
9
PASkG
EPA 8082A
SEM
8
PASI-C
EPA 6010D
SH1
7
PASI-A
EPA 7470A
Soo
1
PASI-A
EPA 8270E
PKS
18
PASI-C
EPA 8260D
SAS
14
PASI-C
ASTM 02974-87
KDF
1
PASI-C
EPA 1010A
SMK
1
PASI-A
EPA 9045D
SMK
1
PASI-A
EPA 9095E
SMK
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM 4500S2F-2011
PAS
1
PASI-PA
92467118002 200226.21 PC8
EPA8082A
SEM
8
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 28
PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 10 of 34

PaceAnalytical
wwwr.patelabs.com
ANALYTICAL RESULTS
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville, NC 28078
[phone]
Sample: 200226.21 Lab ID; 92467118001 Collecled: 02126/20 07:30 Received: 02127120 09:40 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachale Method/Date:
1311;
03/05120 12:43
2,4,5-TP (Silvex)
ND
mg1L
0.00200 1
03f09120 06:54 03111/20 10:04 93-72-1
2,4-❑
ND
mg7L
0.00200 1
03/09120 05:54 03111/20 10:04 94-75-7
Surrogates
2,4-DCAA (S)
61.6
%
14.0-158 1
03/09/20 06:54 03111/20 10:04 19719.28-9
8081 TCLP Pesticides RVE
Analytical Method:
EPA 8081 B Preparalion Method: EPA 3510C
Leachate MelhodlDate:
EPA 1311:
03103120 13731 Initial
pH: 4.97; Final pH: 5
gamma-BHC (Lindane)
ND
ug1L
0.50 1
03/04/20 15:43 03106120 20:17 58-89-9
Chlordane (Technical)
ND
ugfL
3.0 1
03104/2015A3 03106120 20:17 57-74-9
Endrin
ND
ug1L
0.50 1
03/04/20 15:43 03/06120 20;17 72-20-8
Heptachlor
ND
ug1L
0.50 1
03104/2015:43 03106120 20; 17 76-44-8
Heptachlor epoxide
ND
ug1L
0.50 1
03104/20 15:43 03/06120 20:17 1024-57-3
Methoxychlor
ND
ug1L
1000 1
03104)20 15:43 03/06120 20:17 72.43-5
Toxaphene
ND
ugfL
3.0 1
03/04/20 15:43 03106120 20:17 8001.35.2
Surrogates
Decachlorobiphenyl (S)
91
%
10-138 1
03104)20 15:43 03/06/20 20:17 2051.24.3
Tetrachloro-m-xylene (3)
86
%
10-110 1
03104/20 15:43 03/06/20 20:17 877-09-B
8082 TCLP PCBs RVE
Analytical Method: EPA 8062A
Preparation Method: EPA 3510C
Leachale Method/Date:
EPA 1311:
03103120 13:31 Initial
pH: 4.97; Final pH: 5
PCB-1016 (Aroclor 1016)
ND
ugfL
1000 1
03/10120 15:07 03/11120 18:13 12674.11-2
PCB-1221 (Aroclor 1221)
ND
ug1L
1000 1
03110120 15:07 0311112018:13 11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug1L
1000 1
03110120 15:07 03111/20 18:13 11141-16-5
PCB-1242 (Aroclor 1242)
ND
ugfL
1000 1
03110120 15:07 0311V20 18:13 53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug1L
1000 1
03110120 15:07 03111/20 18:13 12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug1L
1000 1
03110120 15:07 03/11120 18:13 11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug1L
1000 1
03/10120 15:07 0311V20 18:13 11096-82-5
Surrogates
Decachlorobiphenyl (S)
96
%
10-132 1
03/10120 15:07 03111/20 18:13 2051-24-3
6010 MET ICP, TCLP
Analytical Method: EPA 60100
Preparation Method: EPA 3010A
Leachale MelhodlDate: EPA 1311;
03/04/20 13:25 initial
pH: 5.91, Final pH: 4.5
Arsenic
ND
mg1L
0.050 1
03/05/20 08:20 03105/20 23:12 7440-38-2
Barium
ND
mg1L
0.25 1
03105/20 0820 03105120 23:12 7440.39-3
Cadmium
ND
mg1L
0.0050 1
03/05/20 08:20 03105120 23:12 7440.43-9
Chromium
ND
mg1L
0.050 1
03105120 08:20 03f05120 23:12 7440-47-3
Lead
ND
mg1L
0,025 1
03105/20 08:20 03/05120 23:12 7439-92-1
Selenium
ND
mg1L
0.10 1
03105/20 08:20 03/05120 23:12 7782.49-2
Silver
ND
mg1L
0.025 1
03105120 08:20 03/0512023:12 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A
Preparation Method: EPA 7470A
Leachate MelhodlDate- EPA 1311; 03104120 13:25 Initial
pH: 5.91; Final pH: 4.5
Mercury
ND
mg1L
0.00020 1
031M2011:30 0310512015:40 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 0311712020 04:44 PM wilhoul the written consent of Pace Analytical Services, LLC.
Page 5 of 28
PO Box 228 • Statesville, NC 28687 • 704/972/4697
Page 11 of 34

I�
PaceAnalytical"
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28D78
(709)675-91192
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Sample: 200226.21
Lab ID: 92467118001 Col[ecled:
02/26120 07:30
Received: 0212712D 09:40 Matrix: Solid
Resuffs reported on a 'dry weight"
basis and are adjusted for percent moisture, sample size and any ditutions.
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CAS No.
Qual
8270E TCLP RVE
Analytical Method:
EPA 8270E Preparation
Method: EPA 3510C
1,4-Dichlarobenzene
ND
ug1L
50.0
1
03/05/20 12:25 03105/20 22:29 106-46-7
2,4-Dinilrotoluene
ND
ug1L
50.0
1
03105120 12:28 03/05/20 22:29 121-14-2
Hexachtoro-1.3-butadiene
ND
uglL
50.0
1
03/05120 12:28 03105120 22:29 87-68-3
Hexachlorobenzene
ND
ug1L
50.0
1
03105/20 12:28 03/05/20 22:29 118.74-1
Hexachloroethane
ND
ug1L
50.0
1
03fO5120 12:28 03105120 22:29 67-72-1
2-Methylphenol(o-Cresol)
NO
ug1L
50.0
1
03/05120 12:28 03105/20 22:29 95A8-7
384-Melhylphenol(m&p Cresol)
ND
ug1L
50.0
1
03JO5120 12:28 03105/20 22:29 15831-10-4
Nitrobenzene
ND
ug1L
50.0
1
03/05120 12:28 03105120 2229 98-95-3
Pentachlcrophenal
ND
ug1L
too
1
03/05120 12:28 03105120 22:29 67-86-5
Pyridine
ND
ug1L
50.0
1
03/05120 12:28 03105120 22:29 110-86-1
2.4,5-Trichlorophenal
ND
ug1L
50.0
1
03/05120 12:28 03105120 22:29 95-954
2.4,6-Trichlorophenol
ND
ug1L
50.0
1
03/05120 12t28 0310512D 22:29 88-06-2
Surrogates
Nitrobenzene-d5 (S)
54
%
12-102
1
03/05120 12:28 03105/20 22:29 4165-60-0
2-Fluorobiphenyl (S)
48
%
13-107
1
03/05/20 1218 03105120 22:29 321-60.8
TerphenyL414 (S)
103
%
21-132
1
U31051201218 03105120 22:29 1718-51.0
Phenol-d6 (S)
51
%
10-110
1
DY05120 12:28 03105/20 2229 13127-88-3
2-Fluorophenol (S)
56
%
10-110
1
03/05/20 12:28 03105120 22:29 367-12-4
2,4,6-Tribromophenol (S)
57
%
27-108
1
03105/20 12:28 03105120 22:29 118-79-6
8260D MSV TCLP
Analytical Method-
EPA 82600
Benzene
ND
ug1L
100
20
0311112011,37 7143-2
2-Butanone (MEK)
ND
uglL
200
20
03/11/20 11:37 78-93.3
Carbon lelrachloride
ND
ug1L
100
20
03/11120 11:37 56-23.5
M1
Chlorobenzene
N❑
uglL
100
20
0311112011:37 108-90-7
Chloroform
ND
uglL
100
20
03/1112U 11:37 67-66-3
1,4-Dichlorobenzene
ND
ug1L
100
20
03111/2011:37 106-46-7
1,2-Dichloroelhane
ND
uglL
100
20
031ll/2011:37 107-06-2
1.1-Dichloroethene
ND
uglL
ion
20
0311112011:37 75.35-4
L1,M0
Tetrachloroethene
ND
uglL
100
20
0311112011:37 127.18-4
Trichloraelhene
ND
ug1L
100
20
0311112011:37 79-01-6
Vinyl chloride
ND
ug1L
100
20
03/11/20 11:37 75.01-4
L1
Surrogates
1,2-Dichloroelhane-d4 (S)
105
%
70-130
20
03111120 11:37 17060-07-0
Toluene-d8 (S)
98
%
67-135
20
03/11120 11:37 2037-26-5
4-Bromofluorobenzene (S)
101
%
70-130
20
03111/20 11:37 460.004
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.8
%
0.10
1
02/27/20 17;27
1D10 Flash point,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200
deg F
70.0
1
03111120 10:31
9D45 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
18
Std. Units
0.10
1
03109120 18:36
H3
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced. except
in full.
Date: 0311712020 04:44 PM
without
the whiten consent of Race Analytical Services. LLC.
Page 6 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 12 of 34

PaceAnalxical
wwx.p�celabs.rom
ANALYTICAL RESULTS
Project: CLEVELAND ❑IGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvifle, NC 28078
[phone]
Sample: 200226.21 Lab ID: 92467118001 Collected: 02/26120 07:30 Received: 02/27120 09:40 Matrix: So9d
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
9095 Paint Filter Liquid Test
Analytical Method: EPA 9D95B
Free Liquids
Fail 1.0 1 03110120 14:45
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
NO mglkg B3.1 1 03102/20 14:11 03102120 14:59
7348 Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Sulfide. Reactive
NO mg/kg 831 1 03102/20 14A1 03/02120 14:14
Sample: 200226.21 PCB
Lab IDc 92467118002 Collected: 02/26120 07:30 Received: 02127/20 09:40 Matrix: Water
Parameters
Results units Report Limit DF Prepared Analyzed CAS No. Dual
B062 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C
PCB-1016 (Aroclor 1016)
NO
uglL
5.0
1
03111/20 1101 03/16/20 1629 12674-11-2
PCB-1221(Aroclor1221)
NO
uglL
5.0
1
0311112015:01 0311612016:29 11104-28.2
PC8-123Z (Aroclor1232)
NO
uglL
5.0
1
03111/20 15:01 03/16/20 16:29 11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug1L
5.0
1
03111/20 15:01 03/16/20 16:29 53469-21-9
PC13-1248 (Aroclor 1248)
NO
ug1L
5.0
1
03111120 15:01 03116/20 16:29 12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug1L
5.0
1
03111/20 15:01 03/16/20 16:29 11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug1L
5.0
1
03111/20 15:01 03116/20 16:29 11096-82-5
Surrogates
Oecachlorobiphenyl (S)
77
%
1D•130
1
03/11120 15:01 03116/20 16:29 2051-24-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 0311712020 04;44 PM wilhout the written consent of Pace Analytical Services, I.I.C.
Page 7 of 28
PO Box 228 • Statesville, NC 28687 •704/872/4697
Page 13 of 34

PaceAnaljdical
www.pacelabs.com
QUALITY CONTROL DATA
Project: CLEVELAND ❑IGESTOR
Pace Project No.: 92467118
QC Batch: 1439420 Analysis Method: EPA8151A
QC Balch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151A
Associated Lab Samples: 92467118001
METHOD BLANK: R3507336-1 Matrix: Solid
Associated Lab Samples: 92467118001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
2,4-D mg1L ND 0.00200 0311012013AS
2,4,5-TP (Silvex) mg1L ND 0.00200 03110120 13:45
2,4-DCAA (S) % 63.6 14.0-158 03110120 13:45
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
(7041875-9092
LABORATORY CONTROL SAMPLE:
R3507336-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
2,4•D
mglL
0.0500
0.0375
75.0 50.0-120
2,4,5-TP (Silvex)
mglL
0-0500
0.0340
66.0 50.0-125
2,4-DCAA (S)
%
66.6 14.0-158
Results preserNetl on this page are in the units rnrhealed by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03117/2020 04:44 PM without the written consent of Pace Analytical Services. LLC.
Page 8 of 28
PO Box 228 • Statesville, NC 28687 • 704/372/4697
Page 14 of 34

�aceAnalytical
www.pacelabs.com
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Batch: 526656
OC Batch Method: EPA 7470A
Associated Lab Samples: 92467118001
METHOD BLANK: 2822383
Associated Lab Samples; 92467118001
Parameter
Mercury
QUALITY CONTROL DATA
Analysis Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Matrix: Water
Blank Reporting
Units Result Limit Analyzed
mg1L ND 0.00020 031OW2015:29
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave, suite 100
Hunlersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2323597
Spike LCS LCS °% Rec
Parameter Units Conic_ Result % Rec Limits Qualifiers
Mercury mg1L 0.0025 0.0024 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2823598 2823599
MS MSD
92467118001 Spike Spike MS MSD Ms MSD % Rec
Parameter Unils Result Conc. Conc. Result Result % Rec e% Rec Limits RPD Qual
Mercury mg1L ND 0.0025 0.0025 0.0025 0.0024 99 96 75-125 2
Results presented on this page are In the units indicated by the "Units" coiumn except where an alternate unit is presented re the right nil the osult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date- 0311712020 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 28
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 15 of 34

t
_-PaceAnapical
www.pacolabs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Batch: 528653 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92467118001
METHOD BLANK: 2822383
Associated Lab Samples: 92467118001
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Matrix: Water
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
mgfL
ND
0.050
03/05/20 23:00
mglL
NO
0.25
03/05/20 23:00
mglL
NO
0.0050
03/05/20 23700
mgfL
NO
0.050
03105120 23:00
mg1L
ND
0.025
03/05120 2100
mg1L
ND
0.10
03105120 23:00
mg1L
ND
0.025
03105/20 23:00
METHOD BLANK: 2822623
Matrix: Water
Associated Lab Samples: 92467118001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg1L
ND
0.050
03/05120 23:06
Barium
mg1L
NO
0.25
03/05120 23:06
Cadmium
mglL
NO
0.0050
03105120 23:06
Chromium
mg1L
NO
0,050
03/05120 23:06
Lead
mg1L
NO
0,025
03f05120 23:06
Selenium
mg1L
ND
GAD
03/05120 23:06
Silver
mg1L
ND
0.025
03/05120 23:06
Pace Analytical Services, LLC
9800 Kincey Ave. Suite100
Hunlersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2623587
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Arsenic
mg1L
2.5
2.2 89
80-120
Barium
mg1L
2.5
2.3 90
80-120
Cadmium
mglL
2.5
2.3 91
80-120
Chromium
mg1L
2.5
2.2 89
BO-120
Lead
mg1L
2.5
2.3 90
80-120
Selenium
mglL
2.5
2.5 98
80.120
Silver
mglL
1.2
1.2 92
80-120
LABORATORY CONTROL SAMPLE:
2823588
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Arsenic
mg1L
2.5
2.2 90
80-120
Barium
mg1L
2.5
2.3 91
80-120
Results presented on this
page are in the units Indicated by the "Units" column
axeepL where an alternate unit
is presented to nto right or the resutL.
REPORT OF LABORATORY ANALYSIS
This report shall nol be reproduced, except in full.
Dale: 03117/2020 04:44 PM
without the wrilten consent or Pace
Analytical Services. LLC.
Page 10 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 16 of 34

r
.PaceAnalytical
wtvw.pacelabs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Hunlersville. NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2823588
Spike
LCS
LCS
e/ Rec
Parameter
Units
Canc.
Result
% Rec
Limits Oualifiers
Cadmium
mg1L
2.5
2.3
92
80-120
Chromium
mg1L
2.5
2.2
89
80-120
Lead
mg1L
2-5
2.3
92
80-120
Selenium
mg1L
2.5
2.5
100
80-120
Silver
mg1L
1.2
1.1
90
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2623589
2623590
MS
MSD
92467118001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Canc.
Result
Result
% Rec
% Ree
Limits
RPD Qual
Arsenic
mg1L
ND
25
2.5
2.3
2.3
90
91
75-125
1
Barium
mg1L
ND
2.5
2.5
2.3
2.4
89
90
75-125
1
Cadmium
mglL
ND
2.5
2.5
2.2
2,3
90
92
75-125
2
Chromium
mg1L
ND
2.5
2.5
2.2
2.3
89
91
75-125
2
Lead
mg1L
ND
2.5
2.5
2.2
2.3
89
91
75-125
2
Selenium
mg1L
N❑
2.5
2.5
2.4
2.4
98
98
75-125
0
Silver
mg1L
ND
1.2
1.2
1.2
1.2
92
94
75-125
2
Results presented on this page are In the units indicated by the Vnits" column except whore an alternate ..if is pmaanled to the right at the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale' 03/17/2020 04A4 PM without the written consent at Pace Analytical Services, L-C.
Page 11 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 17 of 34

I,
-PaceAnalj cal
is".pacelabs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Balch: 529737 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV TCLP
Associated Lab Samples: 92467118001
METHOD BLANK: 2829325
Associated Lab Samples: 92467118001
Parameter
1,1-Dichloroethene
1.2-Dichtoroethane
1,4-Dichtorobenzene
2-Butanone (MEK)
Benzene
Carbon tetrachloride
Chlarobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
1,2-Dichloroelhane-d4 (8)
4-BromoBuorobenzene (S)
Toluene-d8 (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed
ug7L
NO
5.0
031111201120
ug7L
ND
5.0
0311112011:20
ug7L
ND
5.0
0311112011:20
ug7L
ND
10.0
0311112011:20
ug1L
ND
5.0
0311112011720
ug7L
ND
5.0
03111/2011:20
ug7L
46.4
5.0
03f11/2011:20
ug7L
NO
5.0
03111/2011:20
ug7L
NO
5.0
03/11/2011:20
ug1L
NO
5.0
03111/2011:20
ug7L
NO
5.0
0311112011:20
%
104
70-130
031111201120
%
101
70-130
03/11/20 11:20
%
101
67-135
0311112011:20
Qualifiers
Pace Analytical services, LLC
9800 kincey Ave. Suite 100
Hunlersville. NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2829324
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug7L
50
68.9
138
70-130 L1
1,2-Dichloroelhane
ug7L
5D
58.0
116
70-130
1,4-Dichlorobenzene
u911-
50
5T3
115
70.130
2-Bulanone {MEK)
ug1L
100
121
121
64-135
Benzene
ug7L
50
62.0
124
70-130
Carbon tetrachloride
ug7L
50
65.1
130
70.130
Chlarobenzene
ug7L
50
57.9
116
70-130
Chloroform
ug7L
50
59.4
119
70-130
Tetrachloroelhene
ug7L
50
59.2
118
69-130
Trichloroethene
ug7L
50
62.2
124
70-130
Vinyl chloride
ug7L
50
69.2
138
70-131 L1
1,2-Dichloroelhane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
e/
100
70-130
Toluene-d8 (S)
%
102
67-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2829326 2829327
MS MSD
92467118001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
1,1-Dichloroethene ug1L ND 400 400 643 636 161 159 70-154 1 MO
Results presented on this page are In the units Indicated by the -Unite- column except where an alternate unit is preserved to the eight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 03/1712020 04:44 PM without the written consent of Pace Analytical Services. LLC. Page 12 of 26
PO Box 228 • Statesville, NC 28687 - 704/872/4697
Page 18 of 34

/�
RaceAnalytical
www.pacelabs.cnm
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project Nmi 92467118
Pace Analytical Services, LLC
9800 Kincey Ave. Suite lno
Huntersvitle, NC 28078
(704JB75-9092
MATRIX SPIKE t£ MATRIX SPIKE DUPLICATE: 2829326
MS
92467118001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2829327
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
t,2-Dichlaraethane
ug1L
ND
400
400
533
538
133
134
70-137
1
1,4-Dichlorobenzene
uglL
ND
400
400
485
498
121
124
70-133
3
2-Butanone(MEK)
uglL
ND
B00
800
1030
1050
128
131
60-139
2
Benzene
uglL
ND
400
400
551
554
138
138
70-151
0
Carbon tetrachloride
uglL
ND
400
400
579
5B7
145
147
70-143
1 M1
Chlorobenzene
ug/L
ND
400
400
509
520
127
130
70-138
2
Chforolorm
ug1L
ND
400
400
556
545
139
135
70-139
2
Telrachloroethene
ug1L
ND
400
400
529
528
132
132
59-143
0
Trichioroethene
uglL
ND
400
400
545
545
136
136
70.147
0
Vinyl chloride
ug1L
ND
400
400
619
609
155
152
70-156
2
1,2-Dichloroelhane-d4 (S)
%
100
99
70-130
4-Bromofluorobenzene(S)
%
100
101
70-130
Toluene-d8 (S)
%
100
99
67-135
Re5eh5 presented on this page are In the units indfcaled by the "Units" column eacupt where an ahemme unit Is presented to the rrght of the resu4.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 03117/2020 04:44 PM without the written consent of Pace Analytical Services. LLC_
Page 13 of 28
PO Box 228 - Statesville, NC 28687 • 704/872/4697
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PaceArralytica!
www.parelahe.com
Project: CLEVELAND DIGESTOR
Pace Projec[ No.: 92467118
QC Balch: 528498
QC Batch Melhod: EPA 3510C
Associated Lab Samples: 92467118001
METHOD BLANK: 2821559
Associated Lab Samples: 92467118001
Parameter
Units
Chlordane (Technical)
ug1L
Endrin
uglL
gamma-BHC (Lindane)
uglL
Heptachlor
uglL
Heptachlor epoxide
uglL
Methoxychlor
uglL
Toxaphene
uglL
Decachlarobiphenyl (S)
e/
Tetrachloro-m-xylene (S)
%
QUAL[TY CONTROL DATA
Analysis Method: EPA8081B
Analysis Description: 8081 TCLP Pesticides RV
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
3.0
03/06/20 22:14
ND
0.50
03106/20 22:14
ND
0.50
03106f20 22:14
ND
0.50
03106/20 22:14
ND
0.50
03/06/20 22A4
ND
1000
03/06120 22:14
ND
3.0
03106120 22:14
B7
10-138
03106/20 22:14
61
10-110
031D6120 22:14
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Hunlersville. NC 26078
[phone]
LABORATORY CONTROL SAMPLE:
282281E
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Endrin
ug1L
1.2
1.3
101
20-134
gamma-BHC (Lindane)
ug1L
1.2
1.2
96
20.118
Heptachlor
ug1L
1.2
0.71
57
20.142
Heptachlor epoxide
ug1L
1.2
1.0
82
22-133
Melhoxychlor
ug1L
3.8
3.8J
102
44-150
Decachlombiphenyl (S)
%
115
10-138
Tetrachloro-m-xylene (S)
%
78
10-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2822819
2822820
MS
MSD
92467509001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Endrin
uglL
ND
1.2
1.2
1.0
1.3
60
102
21-133
25
gamma-BHC (Lindane)
ug1L
ND
1.2
1.2
1.1
1.2
87
96
24-119
10
Heptachlor
uglL
ND
1.2
1.2
0.64
0.94
51
75
16-128
38 R1
Heptachlor epoxide
uglL
No
1.2
1.2
0.87
1.2
70
93
50-150
28
Methoxychlor
uglL
ND
3.8
3.8
2.9.1
3.7J
77
100
50-150
Decachlorobiphenyt (S)
%
76
83
10.138
Tetrachlora-m-xylene (S)
%
124
99
10-110
SO
Results presented on this page arc in the units Indicaled by the -Units" column except where an alternate unit Is presented to the right of the resull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/17/2020 04:44 PM without the written consent of Pace Analylical Services. LLC.
Page 14 of 28
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 20 of 34

r�
PaceAnalj4ical
www.panlabs.rom
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Batch: 529863 Analysis Method: EPA 80B2A
OC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB
Associated Lab Samples: 9246711131302
METHOD BLANK: 2829865
Associated Lab Samples: 92467118002
Parameter
PCB-1016 (Aroclor 1016)
PC13-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 {Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Decachlorobiphenyl (S)
Matrix: Water
Blank
Reporting
Units
Result
Limit
Analyzed Qualifiers
ugI
ND
0.50
0311612016:58
ug1L
ND
0.50
0311612016:58
ug1L
ND
0.50
0311612016:58
ug1L
ND
0-50
03/1612016:58
uglL
ND
0-50
0311612016:58
ug1L
ND
0.50
0311612016:58
ug1L
ND
0.50
031t612016:58
172
10-130
03116/2016:58 53
Pace Analytical Services, LLC
9800 Nincey Ave. Suite 100
Hunlersvitle. NC 28078
1704)875.9092
LABORATORY CONTROL SAMPLE: 2829866
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016) uglL 5 5-0 101 41-130
PCB-1260 (Aroclor 1260) ug1L 5 5.9 118 42-130
Decachlorobiphenyl (S) % 148 10-130 50
Results preserved on this page are In the units indicated by Iho "Units" column except where an allemale unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced. except in full,
Date: 03/17/2020 04:44 PM without the written consent or Pace Analytical Services. LLC.
Page 15 of 28
PO Box 228 • Statesville, NC 28687 it, 704/872/4697
Page 21 of 34

.FaceAnalytical
www.pece)abs.coln
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28075
[phone]
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
OC Batch: 529437
Analysis Method: EPA B082A
QC Balch Method: EPA 3510C
Analysis Description: 8082 TCLP PCB RV
Associated Lab Samples: 92467118001
METHOD BLANK: 2627697
Matrix: Water
Associated Lab Samples: 92467118001
Blank Reporling
Parameter
Units
Result Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
ND 1000
03/11/20 20:10
PCB-1221 (Aroctor 1221)
ug1L
NO 1000
03111120 20:10
PCB-1232 (Aroclor 1232)
ug1L
ND 1000
03/11/20 20:10
PCB-1242 (Aroclor 1242)
uglL
NO 10DO
03/11120 20:10
PCB-1248 (Aroclor 1248)
ug1L
NO 1000
D3111120 20:10
PCB-1254 (Aroclor 1254)
ug1L
NO 1000
03/11120 20:10
PCB-1260 (Aroctar 1260)
ug1L
NO 1000
03/11120 20:10
Decachlorobiphenyl(S)
%
108 10-132
03/11120 20:10
LABORATORY CONTROL SAMPLE: 2827696
Spike LCS
LCS % Rec
Parameter
units
Conc. Result % Rec Limits qualifiers
PCBA016 (Aroclor 1016)
ug1L
25 NO
102 38-113
PCB-1260 (Aroclor 1260)
ug1L
25 NO
99 35-120
Decachlorobipbenyl (S)
%
98 10-132
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2827699 2827700
MS MSD
92467118001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua[
PCB-1016 (Aroclor 1016) ug1L
NO
25 25 ND
ND 96 109
19-142
PCB-1260 (Aroclor 1260) ug1L
NO
25 25 NO
ND 101 106
19-142
Decachiorobiphenyl(S) %
106 115
10-132
Results presented an this page are in the units indicated by the "Units' column except where an allemale unkt is presented to the right of the resPlL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in gulf.
Date: 03/1712020 04:44 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 2a
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 22 of 34

..PaceAnalXical R,
www.pacelebs.com
QUALITY CONTROL DATA
Project: CLEVELAND DI(3ESTOR
Pace Project No.: 92467118
OC Batch: 528685 Analysis Method: EPA 8270E
OC Batch Method: EPA 3510C Analysis Description: 8270E TCLP MSSV
Associated Lab Samples: 92467118001
METHOD BLANK: 2820943
Associated Lab Samples: 92467118001
Parameter
Units
Matrix: Wafer
Blank Reporting
Result Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
uglL
ND
50.0
03/0512016:32
2,45-Trichlorophenol
ugfL
ND
50.0
0310512016:32
2,4,6-Trichlorophenol
ugfL
ND
50.0
03f0512016:32
2,4-Dinilrotofuene
ugfL
ND
50.0
03f0512016:32
2-Methylphenol(0-Cresol)
uglL
ND
50.0
03/0512016:32
3&4-Met1iylphen01(m&p Cres0l)
ugfL
N❑
50.0
03/05120 16:32
Hexachloro-1.3-butadiene
ug1L
ND
50.0
03/0512016:32
Hexachlorobenzene
ugfL
ND
50.0
0310512016-32
Hexachloroethane
ugfL
ND
50.0
03105f2016-32
Nitrobenzene
ugfL
ND
50.0
031051201&32
Pentachlornphenol
ugfL
ND
100
03105/2016:32
Pyridine
ugfL
ND
50.0
0310512016:32
2,4,6-Tribromophenol (S)
%
106
27.108
03/05/20 16:32
2-Fluorobiphenyl(S)
%
81
13-107
03105/20 16:32
2-Fluorophenol(S)
%
84
10-110
03/05/20 16:32
Nitrobenzene-d5 (S)
%
91
12-102
03105f2O 16:32
Phenol-d6 (S)
%
65
10-110
03105/20 16:32
Terphenyl-d14 (S)
%
120
21-132
03/05/20 16t32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville. NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2823688
Spike
LCS
LCS
% Rec
Parameter
Units
Conc-
Result
% Rec
Limits Oualifiers
1,4-Dichlorobenzene
ugfL
500
269
54
30-130
2,4,5-T4chlorophenol
ugfL
500
456
91
40-130
2,4,6-Trichlorophenol
ugfL
500
453
91
40-130
2,4-Dinitrotoluene
ugfL
500
516
103
49-130
2-Melhylphenol(o-Cresol)
ugfL
500
437
87
30-130
3&4-Methylphenol(m&p Cresol)
ug1L
Soo
430
86
20-130
Hexachloro-1,3-buladiene
ugfL
500
219
44
10-130
Hexachlorobenzene
ugfL
500
471
94
30-130
Hexachloroethane
ugfL
500
241
48
10.130
Nitrobenzene
ugfL
500
392
78
20-130
Pentachlorophenol
ug1L
1000
1180
118
10-140
Pyridine
ugfL
500
286
57
10-130
2,4,6-Tribromophenol(S)
%
121
27-108 SO
2-Fluorobiphenyl(S)
%
82
13-107
2-Fluorophenol(S)
%
84
10-110
Nitrobenzene-d5(S)
%
91
12-102
Phenol-d6 (S)
%
66
10-110
Terphenyl-d14(S)
%
116
21-132
Resulls presented on this page are in the units Indlcated by the ^Units- column except where an alternate unit is preserved to tha right or The result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/1712020 04:44 PM wilhoul the written consent of Pace Analytical Services, I.I.C. Page 17 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 23 of 34

FaceAnalytical
www.pacclabs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704}875-9092
MATRIX SPIKE & MATRIX SPIKE DUPLICAT& 2823689
MS
2629235001 Spike
Parameter Units Result Cone-
MSD
Spike
Conc.
2823690
MS
Result
MS❑
Result
MS
% Rec
MS❑
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
500
500
289
272
56
54
30-130
6
2,4.5-Trichlorophenol
uglL
ND
500
500
486
421
97
84
40-130
14
2,4,6-Trichlorophenol
ugJL
ND
500
500
479
406
96
81
40-130
16
2,4-Dinilrotoluene
ug/L
ND
500
500
537
538
107
108
49-130
0
2-Methylphenol(o-Cresol)
ug/L
ND
Soo
500
48i
416
96
83
30-130
15
3&4-Methylphenol(m8p
uglL
ND
500
500
482
412
96
82
20-130
16
Cresol)
Hexachloro-1.3-buladiene
ug1L
ND
500
500
226
210
45
42
10-130
7
Hexachlorobenzene
ug/L
ND
500
500
498
457
100
91
30-130
9
Hexachloroethane
ug/L
ND
500
500
257
246
51
49
10-130
4
Nitrobenzene
uglL
NO
500
500
420
364
84
73
20-130
14
Pentachlorophenal
uglL
ND
1000
1000
1220
1180
122
118
10-140
3
Pyridine
ug1L
NO
Soo
500
322
242
64
48
10.130
29
2,4,6-Tribromophenal (S)
%
124
115
27-108
S0
2-Fluorobiphenyl (S)
%
85
71
13-107
2-Fluorophenol (S)
%
102
78
10-110
Nitrobenzene-dS(S)
%
93
61
12-102
Phenol-d6 (S)
%
90
60
10-110
Terphenyl-dl4 (8)
a1
112
102
21-132
Results presented an this page are in the units indicated by the "Units" column excupi where an allemate unit is pre —Wed to the right a1 the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03M712020 04:44 PM without the written consent of Pace Analytical Services. LLC.
Page 18 ❑123
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 24 of 34

FaceAnalyticaln
www.pace)ahs.com
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
OC Balch: 527562
QC Balch Method; ASTM D2974-87
Associated Lab Samples: 92467118001
SAMPLE DUPLICATE: 2818743
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2818744
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry WeightlPerceril Moisture
92467131001 Dup
Units Result Result RPD Qualifiers
14.4 13A 9
92467118001 Dup
Units Result Result RPD Qualifiers
% 98.8 98.8 0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1OU
Hunlersville, NC 28078
[phone]
Results presented on this page am In the units indicated By the "Units" column except where an anemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in ruii.
Date: 0311712020 04:44 PM wllhnul the written consent of Pace Analytical Services, LLC. Page 19 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 25 of 34

PaceAnalytical
www.p2celaLs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Batch: 529708 Analysis Method: EPA 1010A
QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Paint, Closed Cup
Associated Lab Samples: 92467118001
SAMPLE DUPLICATE: 2829222
92467118001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Pace Analytical Services, LLC
9800 Kincey Ave. Suile 100
Hunteisville. NC 28978
[phone]
Results presonted on %his page are In the unite Indicated by the "Units" column except where an arreroate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
❑ate'. 0311712020 04:44 PM without the written consent of Pace Analytical Services, LLC, Page 20 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 26 of 34

r.
Face Analytical
www.pacolabs.com
QUALITY CONTROL DATA
Project: CLEVELAND DIGESTOR
Pace Project Nv.: 92467116
OC Batch: 529162 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92467116001
SAMPLE DUPLICATE: 2826379
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2826380
Parameter
pH at 25 Degrees C
92466542001 Dup
Unils Result Result RPD Qualifiers
Std. Units 6.8 6.9 0 H3
92467299001 Cup
Units Result Result RPD Qualifiers
Std. Units 4.2 4.2 1 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite IN
Hunlersville. NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an ahumate ..it is presented to the right al the result
REPORTOF LABORATORY ANALYSIS
This report shall not he reproduced, except In full,
Date: 03/1712020 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28
PO Box 228 o Statesville, NC 28687 0 704/872/4697
Page 27 of 34

FaceAnalytical'
www.pacelabs.com
Project: CLEVELAND DIGESTOR
Pace Project No.- 92467118
QC Batch: 529164
QC Balch Method: EPA 9095E
Associated Lab Samples: 92467118D01
SAMPLE DUPLICATE: 2826382
Parameter Units
Free Liquids
QUALITY CONTROL DATA
Analysis Method. EPA 909513
Analysis Description. 9095 PAINT FILTER LIQUID TEST
92467118001 pup
Result Result RPD Qualifiers
Fail Fail
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HUntetsvl}le, NC 28078
{704J575-0092
Results presented an this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 03117/2020 04:44 PM without the written consent of Pace Analytical Services. LLC.
Page 22 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 28 of 34

'PaoAnalytical
www.pacallbs.com
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
QC Batch: 386044
QC Batch Method: SW-846 7.3.3.2
Associated Lab Samples: 92467118001
METHOD BLANK: 1870222
Associated Lab Samples: 92467118001
Parameter Units
Cyanide, Reactive mg/kg
LABORATORY CONTROL SAMPLE: 1870223
Parameter Units
Cyanide, Reactive mgfkg
SAMPLE DUPLICATE: 1870224
Parameter
Cyanide, Reactive
Pace Analytical Services, LLG
9800 KinceyAve. Suite lo0
Huntersville. NC 79078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9014
Analysis Description: 733C Reactive Cyanide
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0,99 0310212014:55
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
99.7 ND 0 0-8
30352225001 Dup
Units Result Result
mgfkg ND N❑
RPD Qualifiers
Results presented on this page are In the units indicated by thu "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproddced. except in full,
Date: 03/17/2020 04:44 PM without the written consent of Pace Analytical Services. LLC. Page 23 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 29 of 34

r
PaceAnalyfical
www.pacetabs.civa
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
(704WS-9092
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
OC Batch: 386041
Analysis Method:
SM 450OS2F-2011
QC Batch Method: SW-846 7.3.4.2
Analysis Description:
734S Reactive Sulfide
Associated Lab Samples: 92467118001
METHOD BLANK: 1870219
Matrix: Solid
Associated Lab Samples: 92467118001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfide, Reactive
mg/kg
ND
9.9 03102/20 14:14
LABORATORY CONTROL SAMPLE: 1670220
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Sulfide, Reactive
mg/kg
199 39.8
20 0-52
SAMPLE DUPLICATE: 1870221
30352225001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Sulfide, Reactive
mg/kg
ND
ND
Results presented on this page are In the units indicated by the -Units" column except where an alternate unh is presantad to thu right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 03117/2020 04:44 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 30 of 34

Pace Analytical services, LLC
0600 / Kincey Ave. Suite 100
,.PaCeAna♦(XicaJ ' Huntersville. NC 28078
www.pacalabs.com
[phone]
QUALIFIERS
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitalion Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1.2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(0) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylnnitrile by EPA
Method 8260.
N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anaiyle is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAN
Pace Analytical National
PAST -A
Pace Analytical Services - Asheville
PAST-C
Pace Analytical Services - Charlotte
PASI-PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding lime.
L1 Analyle recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QG limits. Batch accepted based an laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
5o Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyle presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 0311712020 04:44 PM without the writlen consent of Pace Analytical Services, I.I.C. Page 25 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 31 of 34

Pace Analytical r
www.pacelabs.ron
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CLEVELAND DIGESTOR
Pace Project No.: 92467118
Pace Analytical Services, LLC
9800Kincey Ave. Suileto0
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92467118001
200226.21
8151A
1439420
EPA 8151A
1439420
92467118001
200226.21
EPA 3510C
528498
EPA 8081B
528985
92467118002
200226.21 PCB
EPA 3510C
529863
EPA 8082A
530383
92467118001
200225.21
EPA 3510C
529437
EPA 8082A
529573
92467118001
200226.21
EPA 3010A
528653
EPA 6010D
528672
92467118001
200226.21
EPA 7470A
528656
EPA 7470A
528736
92467118001
200226,21
EPA 3510C
528685
EPA 6270E
528814
92467118001
200226.21
EPA 6260D
529737
92467119001
200226.21
ASTM D2974-87
527562
92467118001
200225.21
EPA 101DA
52970E
92467118001
200226.21
EPA 9045D
529162
92467118001
200226.21
EPA 9095E
529164
92467118001
200226.21
S W-846 7.3.3.2
386044
EPA 9014
386111
92467118001
200226,21
SW-846 7.3.4.2
386041
SM 4500S2F-2011
386108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in 1ult,
Hale: 03/1712020 04:44 PM without the written consent of Pace analytical Services. LLC. Page 26 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 32 of 34

�r f CHAIN-OF-CU5TODYAnalytical Request Document LAB USE or• be7�
FaceAnavtical WO# : 92467118
Chain-ohfe, clotly is a LEGAL DOCUMENT -Complete all refevent rrelds
Billing information: _ 1111111111111111111111
Stales ill Analytical- Inc.
container 192467118
f 3'? 'T�]�r� Street
h ]3o\ 228 EmailTo��s,�+yt�t,d�', hrj �^---'—=1��--`—>—I—r +
o-J s.A•s s`'y`.t7 [r�`^ •� ETA 1',( C Prercr.ali.e Typrs: Ill nimr aud. 121 wlrurrc aced. III hymachlorlr aud. IQ spaium hydrpwide, 551+. r acrtaic,
Slalesv l le. NC 7 S60 ! 5ile Collection Into/Atldress. r L FC Y I melhana3, 171 spd um Guulfate, 191 sodium lhwsulfale, 191 hexane. Inl asmrole acid, 187 ammonium ulfote,
IQ am I.—ni hydro•edc. JDI T5P, IUJ Uppre,er.cd. (Dl olhcr
Anal ses Lab Prollle/Une:
Cuslo�1,r�rojett Jam /N mb c ,[.�,� 5la County/City: Time Zone Collected: bPr 5nt'Lln ttec•-ipt ch, :kl let:
Cal ei/ QS u f V` � I I PT I I MT I )CT [ JET
Phone: site/Facliity lO It: Compliance Monitoring 7 Custody Seals Pl-e$e+lt, tnr-act Y HtNA1
Lmail: cy:w
Cu Dr1)r SLgna Cures Pr! •G nt { TTI
_ I I Yes I INo Collector Signature Pr.:;enc Nh
CoIIce1+A 6+r.ipnntl: Purghasc Order It: DW PWSIp u; tlorre BoeCla "r�N liA
J6�C� GuoleIt: DW Location Code: suEfici•:nI, vnlvre W NA
Couectf)�.�y�,jignature : Turnaround Date Required. ImmePacked diately on ice: Sampd«H kecelvcd on t � N NA Voh - ,.•.ahspacc lccags ibla }' Ir �Jy
]Yes I ]No USDA Regulated Sotlu V JN
amyl •en in Itoldinn Yfn p `'l+ NA
Sample Disposal: Ru Sh: Ficld rirtered of applicable)'
I I Despose as appropnat I I nelurn I ]Same Day I ] Nexl Day I I Yes I INo r:c<! d,w 1 ChlUrtnc Yre: -a I. Y u Z9
I IArch.ve 2Da 3Da A Cl strips:
I I Y I I Y I I Day I I S Day sample pit Acc_p -a Y tJ N J
E IHold,_ IE.pedae Cha Analyses: ✓
fscr Apply) pll SL'r EPy:
Sulfide Prcr!•-:•t •r IJ Nr%
Matrix Codes (Insert n Matrix box below): Drinking Water {DWI, Ground Water (GW), Wastewater IW WI, Lend v,attor:c 5tri per:
Product (P), Soil/Sall (SLI. Oil (OL), Wipe IWP). Air (AR), Tissue ITS), Bioassay (B), Vapor IV), Other (OTI r 1
Comp / CDICCIed (br Res p of LFB USE CNLY:
Customer
/Sfafm]p�l/e�ID Matrix• Grab Composite Start) Composite End CI Ctns —y 4iL .",amply G ! bmmcn e:
7t1414L Z �J 72f� 107?O Date Time %
Customer Remarks / SrWal
Conditions / Possible Hazards: Type of Ice Used:
t Blue Dry None
SHORT HOLDS PRESENT (02 hours): Y N NIA
Sample T
Temper
lure
lure Into:
Packing Material Used---
Lab Tracking d:
Temp Blank Recc
ved: Y N }A'
Therm IDb: Y
= t1: ,'C;
Cooler 1 Temp U
on Receipt: oC
Radchem samplelsl screened 1<50D cpm): Y N NAB
�j
Samples received via:
FEDE%
Cooler 1 Therm
«. Factor. t_: DC
Rpli
UPS Client
Courier Pace Courier
Cooler 1 Correct
Temp; ict oC
�IC,,
y:ISienaiurc
Datemrne:
geceevcci by/Company: (Signature)
Date/Timo: _
MT1L LAB USE ONLY
Comments:
4, Al-
V' i5egnaiure)
Dalelrime:
ReCeived by/Company: {SlgnaturC}
_
Da[e(Time "
Table it:
Atctnum:
Rehnqu ea ay/Camp
Trip Blank Recgiv
Y N (-5,
Template:
��t
HCL MCOH
7SP Other
lekngwshed by/Comp
-y: (Signature)
Date/Time:
_.!"-S:.%_`.�I
Received by/Company: (Signature)
Date/Time:
Prelogin:
Non Conformance(—
PM.
_
__
--
_-- ---
PB -- —�-
YES / NO
Iof:
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DOCurnent Name:
Document Revised: February 7, 2018
aeeAnalytical z
Semple Condition Upon Recelpt(SCUR)
Page I of 2
Document No.:
Issuing Authority:
F•CAR•CS•033•Rev.06
Pace Carolinas Quality office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Eeceptlons: VOA, Coliform, TOC, Oil and Grease, ❑RO/8015 (waterl DOC, LEHg
"Bottom half of box Is to list number of battle
Project # ' 0# ; 9246711 S
PM: TIN Due Dale: 03/l2/20
CLIENT: 92-Statesvil
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preswuative
pit upon receipt
Date praservadon adjusted
7sme preserv"tfan
adjusted
Amount of Preservaslue
added
Let e
Note: Whenever there is a discrepancy affecting Nonh Carollna campllance samples, a copy of this form wftl be sent to the North Carolina DETINR Certfflcallan Office h,e.
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 28 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 34 of 34

ANNUAL PATHOGEN AND VECTOR FORMS

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Clevelad
W WTP Name: Cleveland W WTP
Monitoring Period: From 1/l/2020
WQ Permit Number: WQ0011431
NPDES Number: NCO049867
To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time.'temp) ❑
I Alt B (Alk Treahnent)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogenas ❑
If applicable to alternatiia perfortned (Class _1 only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Tl�ennophilic ❑
Beta Ray ❑
Ganunn RaN, ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Densin- (R)
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Criss B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑ JL-
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analyticaf
Tech-
ni e
Minimum
Geo. Mean
Maximo
Units
Fecal CoIiform
2 x 10 to the
6th power
per gram of
total solids
1biPN
<1527
i
<1575
mpn/g
0
annual
grab
9221 ce201
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 21
JAIT4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
reouirements.)
(M
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
&1_6m � 1 k01`J a a i f' CcJ�y CY
Preparer Name and Title (type or pint) Land Af plier Name and Title (if applicable)(type or print)
Aa,Lwl &4i4j_j I —L 11 -2-C)
Signature of Preparer* Date Signif6e of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T _ 1102 (26)
DENR FORM PVRF 02T (12/2006)

Town of Cleveland
Non -Discharge Permit No. W00011431
2019
Sample Date
Fecal Coliform
MPN/ ram dry weight
Log
02/26/20
1,527
3.18
02/26/20
1,515
3.18
02/26/20
1,550
3.19
02/26/20
1,575
3.20
02/26/20
1,563
3.19
02/26/20
1,527
3.18
02/26/20
1,575
3.20
Total 1 22.33
Average 3.19
Geometric Mean 1,547 Fecal Coliform - MPN/gram dry weight
Geometric Mean of Less than 2,000,000 mets Class B -Alternative 1 Pathogen Reduction
Fecals 2049[3856] Page 1

Analytical Results r STATESVILLF
ANALYTICAL
Bio Green Services
383 Potts Road
Advance, NC 27006
Receive Date:
02/26/2020
Reported:
02/27/2020
For:
Cleveland Digester Fecals
Comments:
GM <1547
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200226-20-01
Fecal Coliforms
CD-1
<1527
MPN/g
SM92210E-2006
02/26/2020
CE
200226-20-01
Percent Solids
CD-1
1.31
%
SM254DB-2011
02/26/2020
CE
200226-20-02
Fecal Coliforms
CD-2
<1515
MPN/g
SM92210E-2006
02/26/2020
CE
200226-20-02
Percent Solids
CD-2
1.32
%
SM254DB-2011
02/26/2020
CE
200226-20-03
Fecal Coliforms
CD-3
<1550
MPN/g
SM92210E-2006
02/26/2020
CE
200226-20-03
Percent Solids
CD-3
1.29
%
SM254OB-2011
02/26/2020
CE
200226-20-04
Fecal Coliforms
CD-4
<1575
MPN/g
SM92210E-2006
02/26/2020
CE
200226-20-04
Percent Solids
CD-4
1.27
%
SM25406-2011
02/26/2020
CE
200226-20-05
Fecal Coliforms
CD-5
<1563
MPN/g
SM92210E-2WB
02/26/2020
CE
200226-20-05
Percent Solids
CD-5
1.28
%
SM25409-2D11
02/26/2020
CE
200226-20-06
Fecal Coliforms
CD-6
<1527
MPN/g
SM92210E-2006
02/26/2020
CE
200226-20-06
Percent Solids
CD-6
1.31
%
SM2540B-2011
02/26/2020
CE
200226-20-07
Fecal Coliforms
CD-7
<1575
MPN/g
SM92210E-20D6
02/26/2020
CE
200226-20-07
Percent Solids
CD-7
1.27
%
SM2540B-2011
02/26/2020
CE
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cart #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 200226-20-01 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-02 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-03 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-04 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-05 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-06 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200226-20-07 Temp on Arrival: 2.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Address: '31S3
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Contact Person: Phone #
PC 9 Requisitioned by:
Customer
Sample ID
Lab•ID rt
20022 .Z0.01
rime samp}ad
iGreb Ony)
Date Sampled
(scab Only)
a
r 2
Z0.0Z
2Q-43
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m.0q
130
20.06
p
"T,ATFS`ft•lAr
AMALYTH' A1.
122 COlnt Street • P.O. Box 228
{
Sloicivilic, NC 28687
1
[phone]
Chain of
Custody Record
I'Mmelm Mhos Cd for iumlysis
Relinquished by: Time _�j'. y Qpm Date 1 a� LQ1
Deceived by: Time 19 (tO am, pm Date 2/� 20
Relinquished by; Time am, pm Date _/ 1
Received by:
Q!2mpositg 5aWpling tli-
Tiime begin am, pm Date __14/
Time end am, pm Date
ComoOslite Eimp-11ng #2:
Time begin am, pm Date
Time end am, pm bate
Time am, pm Dale
Lab Comments.
CAS d�;'.
Sampled by:
Transported by: 5-
Holding times met:
Compliance work:
Nan -compliance work:
samples Transported On Ica:
Initials:

Analytical Results STATESVILLE
ANALYTICAL
Bio Green Services
383 Potts Road
Advance, NC 27006
Receive Date: 1213012020
Reported: 12/31/2020
For: BG Cleveland
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
201230-18-01 Sulfide BGC 39600 ug/L "ACM31 12/31/2020 CL
Respectfully submitted,
Dena Myers
NC Cart 9440,
NCOW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/972/4697
Pagel of 3

client, 1—
Jt c-
I —
NL 2464;
s":A"17
aiwok a
Custody Revord
Aeldrons: _-�
Contact %rson:P' Phone 0
I" 'd - ' �', FAxg
PO a
eaalamw
Lt,V 7"" 9wWod
quisitioned by:
Wasl,,IAM Win.
20.12
Relinquished by,
Recui%md 4y;
Relinquished by:
Ruceived by,
Time buS*i -- Ain. pm Dale
Time and ­am,prn Dale _t__J_
Time begin_—_. am. pm Dale _)__/_
TiFTIV 0t%0_-_ _ 010, Pin DaIU
Time 2,:; am, a pm Dat Sampled by: f e'-
Time 12 0 5- arn, Pm- Date —Tr4nsporied
Time am. pm Dolt) I Holding Imes Met:
Time um. pm Data Compliance work.
Non-compliance work:
Barriplou Ta�Vqjod On Im.
6

SOIL SAMPLES

Page 1 of 1
Report Number: 21-015-0935
Account Number: 46646
Send To: BIO-GREEN SERVICES INC
383 POTTS RD
ADVANCE NC 27006
Waypoint
ANALYTICAL
'Every acre... Every year.
SOIL ANALYSIS REPORT
Date Received: 01/15/2021 Date Of Analysis: 01/18/2021 Date Of Report: 01/18/2021
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyrical.com
Grower: Town of Cleavland
Analytical Method(s): Mehiich 3 SMP Buffer pH Loss On Ignition water pH
NC = !North Carolina Fertility Index Value
OM
W!V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
%M3
Sail
K
Mg g
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pp m Rate
ppm Rate
P H
Index
meg1100g
meg1100g
8GCL1
22345
4.0
119
9 VL
23 VL
248 VH
872 M
24 VL
5A
6.79
1.4
8.0
I MIN
M
NC = 7
NC = 12
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NON
S.
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm lute
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
mslcm Rate
BGCL1
0.7
25.8
54,5
1.3
17.5
11 L
2.3 M
90 VH
63 VH
1.6 H
0.2 VL
NC=23
NC=57.5
NC=563
NC=80.0
values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Date Received: 01/15/2021
Date Of Report, 01/18/2021
Explanation of symbols: % (percent), ppm (parts per million), Ibs1A This report applies to samples) tested. Samples are retained a
(pounds per acre), mslcm (milli -mhos per centimeter), meg1100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 a lbs/A, Soluble Salts mslcm x 640 = ppm. Analysis prepared by: waypoint Analytical V rginia, Inc.
SOIL FERTILITY RECOMMENDATIONS
by. 1nwrc f11 Goo
Pauric Mc Groary Ph-D., CPAg
Sample ID
Yield Goal
Lime
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Field ID
Intended Crop
Tons
Tons1A
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
I
Ib1A
Ib1A
Ib1A
Ib1A
Ib1A
MIA
Ib1A
fb1A
Ib1A
Ib1A
SGCL1
Fescue Hay
4
0.8
200
120
180
0
10
0
0
0
070
1
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.