Loading...
HomeMy WebLinkAboutWQ0019960_Residual Annual Report 2020_20210222Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0019960 Applicant/Permittee City of Marion Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Asheville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * tim Horton Email Address* thorton@marionnc.org electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... ....................................................................................................................................... . Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 8286528843 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00019960 Has Current Existing permt number Applicant/Permittee Address* P.O Drawer 700, Marion, NC 28752 Facility Name * City of Marion RLAP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form} Engineering Rans, Specifications, Calculations, Bc.) 2020 Annual Land Application Report--Approved-- 1.92MB 2.11.2021.pdf Upload only 1 PCF docurrent (less than 250 M3). Maniple docurrents must be combined into one PDF file unless file is larger than upload linit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/22/2021 ,YlhCity of Marion ac 1 Annual Report ApplicationLand of r Permit No.a r' ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0019960 County: Facility Name (as shown on permit): Land Application Operator: McDowell U.S. Biosolids, Inc. Year: 2020 City of Marion Phone: 336-957-7878 Land application of residuals as allowed by the permit occurred during the past calendar year? 21 Yes C1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 8 Total number of fields utilized for land application during the year: 6 Total amount of dry tons applied during the year for all application sites: 58.06 Total number of acres utilizes for land application during the year: 56.9 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes r7l No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant Loading Rates in 15A NCAC 021'.1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .l 1 1 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. l l) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "l certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violatic d Pennittee Name and Title'(type or print) rr- of Perm LZ2t Date Signature of Preparer* Date Sij ature of [wand Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0019960 Laboratory: 1) Facility Name: City of Marion 2) Residual Source WQ # or NCO031879 3) NPDES #: 4) WWTP Name: Corpening Creek 5) Residual Analysis Data ETS Parameter m /k« ( g g) Conc. Limit (m /k r a Sample or Composite Date 6-2-2020 Percent Solids (%) NA 1.8 Arsenic 75 28.2 CadmiUtll 85 11.3 Copper 4,300 422 Chromium NA NA Lead 840 47.5 Mercury 57 1.5 Molybdenum 75 39 Nickel 420 20.2 Selenium 100 28.2 Zinc 7,500 1020 Total Phosphorus NA 23000 TKN NA 58400 Ammonia -Nitrogen NA 2800 Nitrate and Nitrite NA 511 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting fal information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0019960 Facility Name: City of Marion Residual Source NPDES # or WQ#: NCO0318789 WWTP Name: Corpening Creek Residual Analvsis Data Laboratory: 1) ETS 2) 3) 4) 5) ISample Parameter ni -� or Composite Date t Potassium "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Marion Total Dry Tons Applied (Annual): WQOO 19960 Cation Exchange Capacity (non 503 only): John Fisher Owner: John Fisher Predominant Soil Series: 9.9 Acres Permitted 9.9 Site #: 8.30 BrB2 F 1 Field #: Fl Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date 6/2/20 KAMM Total Phos- phorus MENEEMENEENE. Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total i 2 3 a 5! 6 7 8; 9 14 11 12 - r.3 DT/Ac./ c App. Event 0.84 Arsenic 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047 Cadmium 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Copper 0.707 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.707 Chromic ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080 Mercury 0A03 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 denurn Nickel 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Selenium 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.047 Zinc 1.710 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.710 Total Phos- 38.548 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 38.548 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signattr of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: FI Acres Utilized: 9.9 Land Owner: John Fisher Annual Dry Tons Applied: 8.2941 Site #: F1 Acres Permitted: 9.9 Operator: John Fisher Predominant Soil Series: BrB2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 239 Crop 2 Name: Crop 2 Max. PAN: -= o QLiquid Volume applied (enter one) Solids/ Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, W'Q#. Fert., Animal Waste. etc) Soil Cond. tI)r�. act Moi, , , I recip, Past 24 Mrs. nahes > ' �' 0 < x � ° v' o TKN m glkg z D ;' o 23 �� _ mglk 9 Nitrate and Nitrite m !k g g PAN Applied t lbs/acre) Name of Type p P Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 7-2020 110500 1.8 0.838 NCO031879 dry, 0 s 0.5 0.3 58400 2800 511 31.151 NA Fescue 0.000 0.000 0.000 0.000 0.000 0,000 0,000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 110500 As Cd u Cr Pb H Mo Ni Se Zn P 31.151 0.000 Lime A lied Annuallbs/acre 0,047 0.019 707 ####### 0.080 0.003 0,065 0.034 0.047 1.710 38.548 Date Ibs/ac Prior Years Cumulative lbs/ac 0.103 0.046 15.27 0 0.828 0.322 0.243 0.393 0.101 15.683 12-2020 2000 Current Cumulative Ibs/ac 0.150O.ObS 977 ####### 0.908 0.325 0.308 0427 0.148 17.393 Permitted C. P. L. R.**** 36 34 NA 1338 267 15 NA 374 89 2498 Permit PAN Limit Ist/2nd Crop 239 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 2'-3--Q3 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anserobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loadina Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Marion Total Dry Tons Applied (Annual): WQ0019960 Cation Exchange Capacity (non 503 only): John Fisher Owner: John Fisher Predominant Soil Series: 2.4 Acres Permitted: 2.4 Site #: F2 Field #: 1.46 BrB2 F2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): WWBEIR Corn- po TotalDate ' o . � iii Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2, A 5 6 7 8 9 10 11 12 I DT./ Ac./ w33 o App y went 0.61 Arsenic 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Cadmium 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 0.515 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.515 Chromiu #4#### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ##4### Lead 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0,048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 denum Nickel 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Selenium 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Zinc 1.244 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.244 Total Phos- 28.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 28.060 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signa re of�Landpp-lie-r-­­ Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: John Fisher Operator: John Fisher Crop I Name: Fescue WQ Permit #: WQ0019960 Field #: F2 Annual Dry Tons Applied: 1.4637 Site #: F2 Predominant Soil Series: BrB2 Crop 1 Max. PAN: 239 Crop 2 Name: Acres Utilized: 2.4 Acres Permitted: 2.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o 0) p ei Volume applied (enter one) Solids/ liquid Cu. Yds Gallons % Solids Volume Applied per Acre (pry Tons/Ac) Residual Sources (NPDES #. WQ#. Fert., Animal Waste, etc) Soil Cond. (Dry. Wet.y. Moist} Preci p Past 24 lirs. �cnes D � -I F - - F. c w = - G" X ry W - `= ? TKN mglkg z A c _ 3 mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop t Crop 2 Crop I Crop 2 7-2020 19500 1.8 0.610 NCO031879 dn• 0 s 0.5 0.3 58400 2800 511 22.676 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp { attach FORM FSF supp to this form): TOTALSI 01 19500 As Cd Cu Cr Pb Hg Mo I Ni Se Zn P 22.676 0.000 Lime Applied Annuallbs/acre 0.034 0.014 0.515 ####### 0.058 0.002 0.048 0.025 0.034 1.244 28.060 Date Ibs/ac Prior Years Cumulative Ibs/ac 0.132 0.172 4.016 0 0.611 0.032 1.81 0.288 0.078 11.589 0 Current Cumulative lbs/ac 0.166 0.186 4.531 ####### 0.669 0.034 1.858 0.313 0.112 12.833 Permitted C. P. L. R.**** 36 34 NA 1338 267 15 NA 374 89 2498 Permit PAN Limit Ist/2nd Crop 239 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 7.7-264 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobiaily digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL, METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Marion WQ0019960 John Fisher Owner: 7 Acres Permitted: Total Dry Tons Applied (Annual): 8.79 Cation Exchange Capacity (non 503 only): John Fisher Predominant Soil Series: HaC 7 Site #: F3 Field #: F3 Re.6dttal Analvsis Data (Heavy Metals and "Total Phosphorus use ma/ka, % Solids use Raw Percent #): Com- posite Date',IIIIIIIII III RAW M. Phos- tit Annual Heavv Metal Field I,oadinas (Calculated in lbs/acre): Total 1, 2 3 4; 5 6 7 8 9 10-` 11 121 App- Event 1.26 14 Arsenic 0.071 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.071 Cadmium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Copper 1.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.059 Chromium ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.098 denum Nickel 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.051 Selenium 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 Zinc 2.560 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.560 Total Phos- 57.730 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 57.730 11orus t certtly, unuer penalty oT taw, mar ants uocument was prepares unuer my tttrectton or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". _ _A_J �_ o -- Sign ure of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F3 Acres Utilized: 7 Land Owner: John Fisher Annual Dry Tons Applied: 8.7820 Site #: F3 Acres Permitted: 7 Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN: -� tj Volume applied (enter one) Solids/ I,icluid Cu. Yds Gallons % Solids Volume Applied per Acre {Dry Tons/Ac) Residual Sources (NPDES # W'Q#, Pert., Animal Waste. etc) Soi1 Cond. (Dry, Wet Moist) Nrecip. Past 24 Hrs. ret,es D s �' �� ° = is - r = * 'I'KN mg/kg z ?' o �. mglkg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name ol'Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 7-2020 117000 1.8 1,255 NCO031879 dry 0 s 0.5 0.3 58400 2800 511 46.648 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 1 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): FO"I'ALS:l 01 117000 As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 46.648 0,000 Lime Applied Annuallbs/acre 0.071 0,028 1.059 ####### 0.119 0.004 0.098 0.051 0.071 2.560 57.730 Date lbs/ac Prior Years Cumulative lbs/ac 0.353 0.143 9.888 1.763 1.46 0.051 0,639 0.624 0.349 27.39 12-2020 2000 Current Cumulative lbs/ac 0,424 0.171 10.947 ####### 1.579 0.055 0.737 0.675 0.420 29.950 Permitted C. P. L. R.**** 36 34 NA 133$ 1 267 1 IS 1 NA 374 1 89 1 249$ Permit PAN Limit lst/2nd Crop I202 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [ Signature of Land Applier ? -1. Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Marion - WQ0019960 John Fisher Owner: 6.7 Acres Permitted: Total Dry Tons Applied (Annual): 6.34 Cation Exchange Capacity (non 503 only): John Fisher Predominant Soil Series: HaC 6.7 Site #: F4 Field #: F4 D-;,a-1 A-nlva;o nata ruPa'vv MPtaIC anti Tntal Phncnhorus use mg/kg. % Solids use Raw Percent #): . Corn- .o Date Total Phos- phorusMEMENEENEENE Annual Heavv Metal Held loadings Walculated to lbs/acre): Total ?_ 2 3 !! _ 4 5 fi 7 8! 9 10 j 11 12 DT/Ac./ ° App. Event 0.95 Arsenic 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 0.799 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.799 Chromium ###44# 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4##### Lead 0.090 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090 Mercury 0.003 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 denum Nickel 0.038 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.038 Selenium 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Zinc 1.932 0.000 0.000 0.000 f 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.932 Total Phos- 43.562 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 43.562 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: John Fisher Operator: John Fisher Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: F4 Annual Dry Tons Applied: 6,3426 Site #: F4 Predominant Soil Series: HaC Crop 1 Max. PAN 202 Crop 2 Name: Acres Utilized: 6,7 Acres Permitted: 6.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° .ate- o Ga Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTonsrAc) Residua! Sources (NPDFS #, WQ#, Fert.. Animal Waste. etc) Soil Cond. (Dry. Moisi} Precip. Past 24 Mrs. rcnes > K � F. " r t c - j C 0 TKN mglkg �' = 3 po mglkg Nitrate and Nitrite mglkg PAN Applied ( Ibs/acre) Name of Crop "Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7-2020 84500 1.8 0.947 NCO031879 dry 0 s 0.5 0.3 58400 2800 511 35.198 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): r0TA1..S: a 84500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 35.198 0.000 Lime Applied Annuallbs/acre 0.053 0.021 0.799 ####### 0.090 0,003 0.074 0.038 0.053 1.932 43.562 Date lbs/ac Prior Years Cumulative lbs/ac 0.341 0.884 12.479 2.109 1.759 0.062 0.632 0.755 0.351 30.412 12-2020 1000 Current Cumulative lbs/ac 0.394 0.905 13,278 ####### 1.849 0.065 0.706 0.793 0.404 32.344 Permitted C. P. L. R.**** 36 34 NA 1 1338 267 1 15 1 NA 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 202 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .A4 Signature of Land Applier k3-;#A Date *Application Method: S - Surface, 1N - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Marion Total Dry Tons Applied (Annual): 15.62 WQ0019960 Cation Exchange Capacity (non 503 only): Brain Kay Owner: Brian Kay Predominant Soil Series: 17.2 Acres Permitted: 17.2 Site #: R1 Field #: Rl HaC Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, °lam Solids use Raw Percent #): Corn- posite Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 21 d; 5 6; 7 8; 9 10 11 i12 DT/Ac./ 0 App- Event 0.91 ' Arsenic 0.051 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 10.051 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.021 Copper 0.766 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.766 Cliromiurn ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.086 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.086 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071 denum Nickel 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.037 Selenium 0.051 0.000 0.000 0.000 0.000 0A00 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Zinc 1.852 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.852 Total Phos- 41.768 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 41.768 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 4001 Signa ure of Land pplier � Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Brian Kay Operator: Brian Kay Crop 1 Name: fescue WQ Permit #: WQ0019960 Field th RI Annual Dry Tons Applied: 15.6125 Site #: RI Predominant Soil Series: HaC Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 17.2 Acres Permitted: 17.2 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: L o Y a' o VolumeSoil applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTcnsrAc) Residual Sources (NPDES #, WQ#. Fert.. Animal Waste. etc) Cond. (Dry. wet. Moist) Prccip. Past 24 firs. metes D K � 8 - r ro ? - 5 x iti 0 I'KN mglkg y. mg/kg Nitrate and Nitrite mg/kg PAN Applies! { lbs/acre) Name, of CropType Receiving Residual Application Crop17 Crop 2 Crop I Crop 2 7-2020 208000 1.8 0.908 NCO031879 dry 0 s 0.5 0.3 58400 2800 511 33.750 NA Fescue 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 208000 As Cd Cu Cr Pb H Mo Ni Se Zn P 33.750 0.000 Lime Applied Annuallbs/acre 0.051 0.021 0.766 ####### 0.086 0.003 0.071 0.037 0.051 1.852 41.768 Date lbs/ac Prior Years Cumulative lbs/ac 0.151 0.079 10.257 1.475 1.545 0.059 1.33 0.635 0.192 25.99 12-20 1000 Current Cumulative lbs/ac 0.202 0.100 11.023 ####### 1.631 0.062 ).401 0.672 0.243 27.842 Permitted C. P. L. R.**** 36 34 NA 1338 267 15 NA 374 1 89 1 2498 Permit PAN Limit l st/2nd Crop 1 202 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier P-3- Date *Application Method: S - Surface, 1N - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Permit #: WQOO19960 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Operator: Brain Kay Owner: Brian Kay Acres Used: 13.7 Acres Permitted: 13.7 Site #: 17.56 Predominant Soil Series: HaC R2 Field #: R2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- Annual Heavy Mctal Field Loadings (Calculated in lbs/acre): Total 1 21 3 a 5 6? 7; 811 9i 14! 112i App. iv Event 1.28 Arsenic 0.072 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.072 Cadmium 0.029 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Copper 1.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.082 Chromium ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 1 0.122 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.122 Mercury 1 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0100 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Nickel 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Selenium 0.072 0.000 0.000 0-000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072 Zinc 2.615 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.615 Total Phos- 58.972 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 58.972 horus I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sign ure of Land Applier Date DENR FORM MFISF (1919nnri) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Brian Kay Operator: Briars Kay Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: R2 Annual Dry Tons Applied: 17.5640 Site #: R2 Predominant Sail Series: HaC Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 13.7 Acres Permitted: 13.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o - 1 o Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDF.S #. WQ#. Fert.. Animal Waste, etc) Soil Coed. {Dry. Wet. MoisI) Precip. I ast 24 }1rs. inches > K � F * n" 2 x 1'KN mg/kg z D .;' a mglkg Nitrate and Nitrite mglkg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 7-2020 234000 1.8 1.282 NCO031879 dry 0 s 0.5 0.3 58400 2800 511 47.669 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): RAAB 01 234000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 47.669 1 0.000 Lime Applied Annuallbs/acre 0.072 0.029 1.082 ####### 0.122 0.004 0.100 0.052 0.072 2.615 58.972 Date lbs/ac Prior Years Cumulative lbs/ac 0.159 0.086 10.76 0.065 1.386 0.341 1.039 0.602 0.179 25.62 0 Current Cumulative lbs/ac 0.231 0.115 11.842 ####### 1.508 0.345 1.139 0.654 1 0.251 28.235 Permitted C. P. L. R.**** 36 34 NA 1 1338 1 267 1 15 NA 1 374 1 89 2498 Permit PAN Limit I st/2nd Crop 1 202 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." J^- Signature of Land Applier 3- 7vJ. Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Marion WWTP Name: Corpening Creek Monitoring Period: From 1/l/2020 To WQ Permit Number: NPDES Number: 12/31 /2021 W Q0019960 NCO031879 Pathogen Reduction (15A NCAC 02T .1.106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time./temp) ❑ IIt B (Alk Treatment) ® Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ 1leat'freatment ❑ Therinophiltc ❑ Beta Ray ❑ Ganima Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ® Composting ❑ lAeroble Digestion ❑ Anaerobic Digestion. ❑ _. If applicable to alternative performed (Class A or Class B) complete the following monitorin data: Parameter Allowable Level in Sludge g Pathogen Density Numbera dences Frequency of Analysis Sample Type na Analytical Tech- niaue Minimum Geo. MeanMaximuml Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 2210 4452 10080 MPN/g 0 7 grab sm9221 CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) 5d Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." i Dennis Key US Biosolids, Inc. Preparer Ne,and Titl (type or print} band Applier Name and Title (if applicable}(type or print) Signature of Preparer* Date Sigii4ture of 1-and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) C. Ceilificate of Analysis Nxny 1,,& fi-- I S-91 809.33 it .1. '1" Cxd. J, M. i. pl, 412 1 1 :": load NIIA SOng L, N sit -0 —ig 231- AjlI t L 17, 2 M F. Su9Jl.n PAN Mineralization as decimal ITgIal dry tons/year jAcres, Applied on Rate 0.3 TKN 58400 NH3 2800 NO3 511 NO2 0 % Solids 0.018 PAN Surface 185911mg/kg 1 37.182 lbsidry ton 0 Ibs total PAN �7#-DIVIOI Ilbs PAN/acre PAN Injection 19991 mg/kgmg/kg 39.982 lbstdry ton 0 11bs total PAN #DIVIO! Ibs PAN/acre Dry Tons/1000 gal. 0.07506� 1st year PAN Surface Ibs. 0 1st year PAN Injected Ibs. 0 Ibs.lacre Surface #DIV/0! Ibs./acre Injected #DIV/Of MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 mg/kg x .002 MR(TKN-NH3) + l(NH3)+NO3+NO2 mglkg x .002 =mg/kg =Ibs/dry ton =mg/kg =Ibs/dry ton 1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal." 2000 SAR Sodium Absorption Ratio Na : Sodium (Mg/L) Equivalent weight: 23 Ca : Calcium (Mg/L) Equivalent weight: 20 Mg: Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight Na M /L Ca M IQ M M /L 50.58 t 275.4 1 103.32 Na MEN Ca�ME� 13.77 Mg(M 2.19913 8.61 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power 1 SAR = 0.6574091(From Mg/L entered above) C SAR= 0.657376,(From ME entered below) Na (ME) 2.2 Ca (ME) Mg (ME) 1 13.8 1 8.6 The amour amount of E Permitting! Environmental Testing Solutions, Inc. Project name: City of Marion Collection date: 2-Jun-20 Date received: 2-Jun-20 Sample identification: Sludge 2 - Grab Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: 200602.538 Sample number: 199954 Parameter Method Result RL Units Date Analyzed Analyst Footnotes Arsenic-'FCE,P 6010 C <0.25 0.25 mg/L viotw-m MLR I Barium - WIT 6010 C <2.50 2.50 mg/L 16-Ju11-20 MLR I Cadmium = I'C'l.P 6010 C <0.05 0.05 mg/L 16-Jun-20 MLR I Chromium -TCLP 6010 C <0.10 0.10 mg/L 16-Jun-20 MLR I Lead -TCLP 6010 C <0.25 0.25 mg/L t6-Jun-2o MLR I Selenium - TCLP 6010 C <0.25 0.25 mg/l. 16-Jun-20 MLR 1 Silver - TCLP 6010 C <0.10 0.10 mg/L 18-Jun-20 MLR 1 Mercer - TCLP 7470A <0.0020 0.0020 mg/L 12-Jun-20 TLT 1 Full Scan TCLP Organics See attached sheets 1.2 Reactive Cvanide 335.4 <0.05 0,05 mg/kg 10-Jun-2o F:CHF,M 2 Reactive Sulfide SM 4500 S D 0.55 0.1 mg/kg s-Jun-2o ECIIEM 2 ignitability SW 846 1010 >190 190 °F 19-Jun-2o IiCI IIiM 2 Footnotes: RL = Reporting Limit. Values are reported do.vn to the Reporting Limit only. 1. Sample analyyed by Rogers & Callcott Environmental. 2. Sample analyzed by Einviro Chemists. Inc. Date reviewed: Data reviewed by: Kelley E. Keenan Signature: NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, wept in its entirety, without the written consent of Environmental Testing Solutions. Inc. The results in this report relate only to the samples submitted for analysis. Project name Collection date Date received: Marion WWTP 17-Feb-20 17-Feb-20 Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: 200217.500 Sample identification: Sludge 91- Grab Sample number: 196656 Date Parameter Method Result RL Units Analyzed Analyst Footnotes %TS SM 2540 G 1.7 0.10 % 17-Feb-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E 9520 3.l MPN 17-Feb-21) KEK Sample identification: Sludge #2 - Grab Sample number: 196657 Date Parameter Method Result RL Units Analyzed Analyst Footnotes oloTS SM 2540 G 1.8 0.10 % 17-Feb-20 KEK Mulitple rube Fermentation Procedure SM 9221-E 4140 3.6 MPN 17-Feb-20 KEK Sample identification: Sludge 43 Grab Sample number: 196658 Parameter Method Result RL Units bate Analyzed Analyst Footnotes %TS SM 2540 G 1.8 0.10 % 17-Fob-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E 10080 3.6 MPN 17-Feb-20 KEK Sample identification: Sludge #4 Grab Sample number: 196659 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 1.7 0.10 % 17-Feb-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E 2210 3.1 MPN _ 17-Feb-20 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: 01.22 . NC Certification Number: 600 Data reviewed by: Kellel E. Keenan SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 Signature: This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc The results in this report relate only to the samples submitted for analysis. i Environmental Testing Solutions, Inc. Proiect name: Marion WWTP Collection date: 24-Feb-20 Date received: 24-Feb-20 Sample identification: Sludge #5 - Grab Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828)350-9364 I-ax: (828)350-9368 Project number: 200224.501 Sample number: 196856 Parameter Method Result RL Units date Analyst Footnotes Analyzed %TS SM 2540 G 11.8 0.10 % 24-Fib-20 KEK Mulitple'l'ube Fermentation Procedure SM 9221-E 8100 3.6 MPN 24-Feb-20 KEK Sample identification: Slu�d,=e #6 - Grab Sample number: 196857 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 1.8 0.10 % 24-Feb-20 KEK Mulitple Tube Fermentation Procedure SM 9221-F 2340 3.6 MPN 24-F6-20 KEK Sample identification: Sludge #7 Grab Sample number: 196858 Parameter Method Result RL Units Date Analyst Footnotes Analyzed °loTS SM 2540 G 1.8 0.10 % 24-Feb-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E 2340 3.6 MPN 24-Feb-20 KEK Footnotes: RL Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 Signature: NC Drinking Water Certification Number: 37786 This report should riot he reproduced, eNepl in its emireth', without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. Fecal coliform, SM 9222-D Ammonia nitrogen, EPA 350.3 Residue - Total suspended solids, EPA 160.3 Bological oxygen demand, EPA 405.1 Fecal coliform, SM 9222-D Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level as C Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CW4in Creek 9960 4/28/2020 16 20 0906 TNorQen 001 /28/20 4/28/2020 1035 RGC 1000 0.73 25 25 0.2 8.1 1.0 ,nilliliters Yo Dry Solids legrees Celsius legrees Celsius 13.25 mg Oxygen/hr 1.81 mg Oxygen/g/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate:1 42 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. c CITY OR MARION CORPENING CREEK WASTE TREATMENT PLANT LABORATORY Teat Salida: In "Id and limisolld .Sarin lr s.-DriW at 103—IOSOC t S*vlard MNhoda-4 210 "i i TME IN: D9ZS a irssr �� rnA OU7% /z Twne Weighsd: ,3 r3 C A A F! TEMP IN: -C TEMP OUT: /03 -C IA• 31 X 100 A + Weight of dried residue * dish, mg; B weight of dish, w*ht of wat ssmpls + dlsh, trig _ i 4G Taw solids. 100 op c SOUR OXYGEN UPTAKE RATE D.O. WORKSHEET DATE:` 2����'� AERATION TIME i TIME: START: TEMPERATURE: < STOP: !4 3,0 ?J-?Vw ANALYST: -f3(/ f�c�, DO READING START TIME: RECORD DO READINGS Q intervals less than one MINUTE FOR AT LEAST 15 MIN Q� 1 Z' 2 �� 12 S1 Y 3 �, 13 - 7i 4 , Z� 14 �0 6 16 cPr� 77 8 (p, - 18O S 9 ! 19 �• ��'' 10 7�g� 20 Record the temperature at the end of the test: �-) s— �n 00 0 m m oQ � x 00 O N N d Q (l T m N N ey rl L s V " ate-+ 0) N Q! 'c cc CL co _E h tD Ln d m N ei Q1 00 h l0 Ln m N a-1 O (1/Vw) UOSAxp paAlossla Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-2011 Date: 4/28/2020 Time Sampled: 0906 Sampled By: TH Time Started Aeration: 0915 Time Ended Aeration:1030 Time Analyzed:1035 Analyzed By: RGC Total Time of Test: < 2 hrs. ( 1 hour 44 mins. ) Total time of test includes the time sample was aerated. NCDABCS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO17650 I I Iti I;f ka Client: John Fisher Advisor: Zach Key <� p>o '��, Predictive 400 Dairy Rd. Southern Soil Builders • Maggie Valley, NC 28751 958 Hoots Rd �> p Mehlich-3 Extraction Soil Re ort Roaring River, NC 28669 Sampled County: McDowell Links to Helpful Information Client ID: 478472 Advisor ID: 231531 Sampled: 11/23/2020 Received: 11/25/2020 Completed: 01/14/2021 Farm: Sample ID: F1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information j Lime History: 1-Fescue/OGrass/Tim, M 1.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and No in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu4 Na ESP SS-1 NO3-N 0.76 0.95 8.2 75 2.1 5.5 195 94 47 22 44 219 148 366 366 324 0.1 1 Sample ID: F2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B i Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in 9/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral I HM% WN CEC BS% Ac pH P-1 K-i Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.71 0.99 8.6 81 1,6 5.9 125 41 55 24 33 240 161 295 295 362 0.1 1 Sample ID: F3 Recommendations: Lime Nutrients (lb/acre) More Crop (tonstacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 1.0 120-200 0 0 0 0 0 0 0 0 Note: 12 3 2 - 0.0 I Test Results [units - WN in g/cm3; CEC and No in meq/100 cm3; NO3-N in mg/dm31: 11 Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-AN Mn-Al2 Zn-t Zn-Al Cu-I Na ESP SS-1 NO3-N 0.81 0.97 8.3 75 2.1 5.5 185 105 46 23 45 213 145 353 353 313 01 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner ofMriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL017650 John Fisher Page 2 of 3 Sample ID: F4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- FescuelOGrass/Tim, M 0.4 120-200 0 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldrr?): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%o S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 0.94 8.1 80 1.6 5.8 129 36 55 23 32 238 160 294 294 351 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO17650 John Fisher Page 3 of 3 I Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tontacre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-1 copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified), Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50, If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear' Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncaqr.qov/aqronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawnslgardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.aovlagronomilobDart4.htmtitsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pHJ describe the soil and its degree of acidity. The Zn-Al zinc availability index Zn-I zinc index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-1, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) available)) indicate levels of plant nutrients or other fertility measurement. Visit www.ncaaraovlaaronomiluvrst.htm NCDA&CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.govlagronomi/ Report No. FY21-SL020228 - •� , <. Client: Brian - Advisor Zach Key Pr@dlCtly@ AKa Lane Southern Soil Builders Tryon, NC 28782 958 Hoots Rd Mehlich-3 -� Soil Report Extraction Roaring River, NC 28669 i Sampled County : McDowell Links to Helpful Information Client ID: 504558 Advisor ID: 231531 Sampled:11123/2020 Received: 11/30/2020 completed: 01/29/2021 Farm: i Sample ID: R1 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.8 120-200 10 90 0 0 0 0 0 0 Note: 12 2 - 0.0 f i Test Results [units - WN in glcm3; CEC and Na in megJ100 cm3; NO3-N in mgldrrt3]: Sail Class: Mineral 1 HM% WIV CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.46 1.01 7.8 75 1.9 5.6 58 25 57 17 45 90 71 132 132 161 0,1 1 Sample ID: R2 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3, CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.04 11.8 90 1.2 6.0 86 53 75 13 39 109 82 220 220 I 114 0 1 1 North C, ro(ina — kh Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Actriculfure I j NCDABCS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO20228 Brian Kay Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity i If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index I ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is ' MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-A!1 Mn-availability index for crap 1 Mn-Al2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z 1 Mn-1 manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N mineral-organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. ; NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft, If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/aaronomi/obpart4.htmVifsfnd information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to ✓=ertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume o u The first seven values (soil class, HM /o, W/V, GEC, BS lo, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel Zn-1 zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.aovlaaronomiluyrst.htm