WQ0035720_Application_20210223

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0035720
Applicant/Permittee Denali Water Solutions, LLC
Applicant/Permittee Address 3308 Bernice Avenue, Russellville, AR 72802
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Organization
Facility Name Denali Water Solutions DCAR
County
Fee Category Major
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $0
Complete App Date 02/23/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Kendall
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Jeff J Retzke
Email Address*
[e-mail]
electronic subntttal, confirmation of receipt, and other correspondence.
Project Information
........ ......... ............................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
2565034300
O Modification - Minor
G Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00035720
Fbs Current Existing permit number
Applicant/Permittee * Denali Water Solutions, LLC
Applicant/Permittee Address* 3308 Bernice Avenue, Russellville, AR 72802
Facility Name * Denali Water Solutions DCAR
Please provide comments/notes on your current submittal below.
If NCDEQ would like a copy of the current permit, please do not hesitate to let me know.
Thanks in advance for your consideration.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, ac.)
Renewal Application WQ0035720 Lake Kilby Drinking
7.8MB
Water Treatment Plant residuals 2-23-21.pdf
Upload only 1 FLFdocurrent (less than 250 M3). Miftiple docurrents mist be combined into one RJFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617

Signature
Submission Date 2/23/2021

Denali
WATER SOLUTIONS
Permit Renewal Application
Lake Kilby Water Treatment Plant
Distribution of Water Treatment Plant Residuals
State-wide Distribution
Permit No. WQ0035720
Denali Water Solutions, LLC
3308 Bernice Avenue
Russellville, AR 72802
February 23, 2021

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Table of Contents
A. Cover Letter
B. Distribution of Class A Residual!
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Denali
WATER SOLUTIONS
February 23, 2021
Mr. Nathaniel D. Thornburg
Branch Chief
Non -Discharge Branch
North Carolina Department of Environmental Quality
512 North Salisbury Street
1617 Mail Service Center
Raleigh, NC 27699-1617
3308 Bernice Avenue
Russellville, AR 72802
PO Box 3036 - Russellville, AR 72811
Phone: [phone]
RE: Renewal of Permit No. WQ0035720 - Lake Kilby Water Treatment Facility, Distribution of
Water Treatment Plant Residuals, State-wide Distribution
Dear Mr. Thornburg,
Denali Water Solutions (Denali) is submitting an application for the renewal of Permit No.
WQ0035720 - Lake Kilby Water Treatment Facility, Distribution of Water Treatment Plant
Residuals, State-wide Distribution. The permit, which was originally issued on January 20, 2012
and renewed on August 24, 2016, is set to expire on July 31, 2021.
Thank you for your assistance with this request. If you have any further questions, comments,
and/or concerns, please feel free to call me at 256.503.4300 or email me at
[e-mail].
Sincerely,
Jeff Retzke
Senior Environmental Manager, East Region
Denali Water Solutions

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
D) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
L APPLICANT INFORMATION:
1. Applicant's name: Denali Water Solutions, LLC
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Jimmy Mardis Title: Chief Environmental Officer
Applicant's mailing address: 3308 Bernice Avenue
City: Russellville State: Arkansas Zip: 72802
Telephone number: [phone] Email Address: jimmy.mardis&denaliwater.com
2. Consultant's name: N/A License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address: N/A
City: N/A State: N/A Zip: N/A
Telephone number: (N/A) Email Address: N/A
3. Fee submitted: 0 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00035720
Date of most -recently issued permit: 08/24/2016
Date of most -recently certified Attachment A (if different than the permit):
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Lake Kilby Water Treatment Plant
City: Suffolk State: Vir�nia Zip: 23434
Coordinates: Latitude: 36' 43' 48" Longitude: 76' 36' 08"
Datum: N/A Level of accuracy: N/A
Method of measurement: Google Earth Maps
County where facility is located: None. Suffolk is an independent City.
2. Facility contact (person familiar with residuals preparation):
Name: C.B. Umphlette, Jr. Title: Watershed Manager
Mailing address: 105 Maury Place
City: Suffolk State: Virginia Zip: 23434
Telephone number: [phone] ext 222 E-mail address: cumphlette@portsmouthhi hggualityh2o.org
FORM: DCAR 06-16 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: >30 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Bulk land applied on agricultural land as a soil conditioner
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (div ton)
3. Approximate amounts of the residuals received and processed at the facility: —2,500 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: —2,500 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): The storage for residuals generated by the Lake Kilby Water Treatment Plant
consists of a settling lagoon located off Cahoon Road in Suffolk, Virginia. The lagoon is generally operated so that a constant
outfall flow will equal the average input flows to the lagoon while maintaining a stable lagoon elevation.
6. Does the facility have a stormwater management plan? ® Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Storage area consists
of an uncovered 75-million gallon lagoon. No impervious surfaces surround the lagoon: therefore, only runoff from rain events
that exceed the infiltration capacity of the native soil along the perimeter of the lagoon will enter the lagoon.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
Q
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
1 NIA , attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineers Seal, Signature, and bate:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
1, Jimmy Mardis Chief Environmental Officer
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Lake Kilby Water Treatment Piant
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note. In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
wu��ozi
FORM: DCAR 06-16 Page 3 of 3

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
D) rrogram iniormation
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Denali
WATER SOLUTIONS
February 22, 2021
3308 Bernice Avenue
Russellville, AR 72802
PO Box 3036 • Russellville, AR 72811
Phone: 479A98-0500
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Subject: Permitting Signature Authority
To Whom It May Concern:
As an appropriate signing official for Denali Water Solutions (city/town or business name) as designated
by 15A NCAC 02T .0106(b), I hereby delegate authority to sign and certify all permit applications, reports
or other permit related documents to the following staff for the following permit types (sewer, spray, land
application) and/or permit numbers:
Position
Person Currently In Position
Permit Type or Permit Number
Senior Environmental Manager
Jeff Retzke
Distribution of Class A Residuals
(Lake Kilby Water Treatment
Plant, Suffolk, VA)
If you have any questions, please contact me at the following:
Permittee/Applicant name (please
print): Jimmy Mardis
Title: Chief Environmental Officer
Complete mailing address: 3308 Bernice Avenue
City: Russellville
Telephone
number.
Sincerely,
State: Arkansas
Email
[phone] Address:
ff"'L
sig at re
Zip: 72802
[e-mail]

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) iviarKetability Staiement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Program Narrative
The residuals produced at the Lake Kilby Water Treatment Plant located in Suffolk, VA will be
mechanically dewatered on -site with the use of belt filter presses. Leachate from the dewatering
activities will be returned to the lagoon. The dewatered residuals will be transported to land application
sites in NC in sealed tailgate end -dump trailers hauled by road tractors. The volume contained in each
trailer will vary, but will typically average 23 wet tons. Residuals will be staged in the field prior to
spreading with typical side-slinger spreaders. There are no constituents of concern contained in the
material and the amount of nitrogen (N) and other plant essential nutrients is relatively low (see
attached laboratory data). The application of residuals will be limited to field crops and forage which
may include corn, cotton, soybeans, wheat, oats, milo, grassland, and alfalfa. The actual dosage rate will
be determined by the nitrogen requirement for the crop selected and yield goals in accordance with the
North Carolina Realistic Yield Database (http://yields.soil.nres.edu) prescription. Approximately
200-300 acres will receive residuals annually. Typical application rates will range from 23-46 wet tons
per acre. In accordance with good agronomic practice, areas which are unseasonably wet, therefore
producing rutting or damage to the field, will not be utilized for residuals application during those
periods. Compensation will be provided in order to maintain a soil pH of 6.0 or greater.

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Marketability Statement
The residuals produced by the Lake Kilby Water Treatment Plant located in Suffolk, VA will be provided
to local area farmers as a soil conditioner. The addition of the fine particles (silt and organic matter)
contained in the water treatment plant residuals will assist the soil in maintaining a high water holding
capacity and improve soil structure. Lime will be will be provided for, in addition to the material, in
order to provide additional benefits to the farmer. Numerous farms are located within 30-35
miles of the facility, primarily in Gates County, and sufficient land is available to assimilate the
approximately 2,500 dry tons to be distributed annually.

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation ana maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Information Sheet
The residuals produced by the Lake Kilby Water Treatment Plant located in Suffolk, VA are provided to
you by the following:
Contact:
Jeff Retzke
Company:
Denali Water Solutions
Mailing Address:
3308 Bernice Avenue
City:
Russellville
I State:
AR
Zip:
72802
Telephone:
[phone]
Email:
[e-mail]
The application of the residuals to the land shall only be applied in accordance with the instructions on
this information sheet. The following shall be strictly followed:
• No residuals shall be applied to any site that is flooded, frozen, or snow-covered
• Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or
stored residuals into any surface waters
• Residuals shall be applied at or below recommended rates for the intended use
• The following setbacks shall be maintained:
Structure/Source
Liquid Residuals
Cake Residuals
Private or public water supply sources
100 ft
100 ft
Surface waters (streams -intermittent and
perennial, perennial waterbodies, and wetlands)
100 ft
25 ft
Surface water diversions (ephemeral streams,
waterways, ditches)
25 ft
0 ft
Groundwater lowering ditches (where the bottom
of the ditch intersects the SHWT)
25 ft
0 ft
Wells with the exception to monitoring wells
100 ft
100 ft
Bedrock outcrops
25 ft
0 ft

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Operation and Maintenance Plan
Operational Functions
The City of Portsmouth, Virginia, Department of Public Utilities, Lake Kilby Water Treatment Plant,
located at 105 Maury Place in Suffolk, Virginia, discharges residuals to the Lake Kilby Water Treatment
Plant (LKWTP) lagoon off Lake Cohoon Road in Suffolk, Virginia. The residuals, which generally consist of
aluminum hydroxide solids, are a byproduct of the sedimentation and filtration process to produce
potable water. The residuals at the LKWTP lagoon will be seasonally dredged and mechanically
dewatered on -site with the use of belt filter presses. Leachate from the dewatering activities will be
returned to the lagoon. In accordance with the requirements of the City of Portsmouth, Denali will
perform this service once per year; typically in the fall. The dewatered residuals will be transported to
land application sites in North Carolina in sealed tailgate end -dump trailers hauled by road tractors for
beneficial reuse.
The volume contained in each trailer will vary, but will typically average 23 wet tons. To prevent
adherence of the residuals to the transport vehicle, the end -dump trailers will be equipped with full rear
mud flaps. This will prevent the residuals from adhering to the tires and undercarriage of the transport
vehicle, thereby preventing residuals from being tracked onto roadways. Residuals adhering to the mud
flaps will be scraped off in the permitted field before the truck returns to the roadway. Residuals will be
staged in the field prior to spreading with typical side-slinger spreaders.
There are no constituents of concern contained in the material and the amount of nitrogen (N) and
other plant essential nutrients is relatively low (see attached laboratory data). The application of
residuals will be limited to field crops and forage which may include corn, cotton, soybeans, wheat, oats,
milo, grassland, and alfalfa. The actual dosage rate will be determined by the nitrogen requirement for
the crop selected and yield goals in accordance with the North Carolina Realistic Yield Database
(http://yields.soil.nres.edu) prescription. Approximately 250 acres will receive residuals annually. The
principal method of application will be surface application and the typical application rates will range
from 23-46 wet tons per acre. Denali will provide financial compensation to the recipients in order for
them to purchase lime to maintain a soil pH of 6.0 or greater.
In accordance with good agronomic practice, areas which are unseasonably wet, therefore producing
rutting or damage to the field, will not be utilized for residuals application during those periods.
Operational provisions will be taken to prevent soil loss through erosion. Provisions will include contour
application and avoidance of areas where surface drainage patterns result in concentrated flow of
runoff from rainfall. The amount of residuals applied will not exceed the hydraulic capacity of the soil at
the time of each application. If a subsequent pass across a field is necessary to achieve the desired
application rate, sufficient drying time will be allowed between passes.
A summary of equipment to be employed on this project is as follows:
• 3-4 belt presses
• 3-6 24 yd3 end dumps. The number will vary depending on travel time to the land
application sites.

• 1-2 high floatation application vehicles
• 1 pump/dredge
Maintenance Schedules
As previously mentioned, and in accordance with the requirements of the City of Portsmouth, Denali will
perform this service once per year; typically in the fall. Residuals distribution on the land application
sites will be uniform throughout the allowed areas. To ensure adequate control of the application rate
for each site, the equipment used for spreading the residuals will be calibrated by measuring the
amount handled on a known square footage. While the rate of discharge from the application vehicle is
fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to achieve
application rates.
Safety Measures
The potential for employee injuries and equipment accidents during land application operations is
minimized by strict adherence to the following:
• New employee orientations;
• Safe work procedures as delineated in Denali's Land Application Safety Manual. Special
training as needed;
• Use of personal protective equipment as required;
• Weekly and/or monthly documented safety meetings;
• Compliance with applicable OSHA standards and Department of Transportation (Federal and
State) trucking safety regulations;
• Prompt dissemination of useful safety information and "lessons learned" to local operating
levels;
• Immediate reporting and investigation of any incidents or "near misses";
• Documented site safety inspections conducted by the Project Manager or his/her designate;
• Unannounced site safety inspections conducted by the corporate Safety Manager and
region Safety Coordinators;
• A safety awards program to recognize individuals and projects with exemplary safety
performance; and
• A disciplinary program to correct or eliminate negligent behavior with regard to safety.
Safety is our Number 1 priority. The Project Manager is totally responsible for on -site safety and can
rely on corporate and region safety representatives to assist whenever necessary.
Careful attention to safe working conditions and methods of operation (e.g. the proper method of lifting
heavy objects and the operation of heavy equipment only by trained and competent operators) should
preclude most of the potential for safety hazards in the land application operation. Should an accident
occur, the Project Manager will be informed immediately and will thoroughly investigate and complete
an accident report, including the workman's compensation and liability forms.

Spill Response Plan
It is our goal at Denali Water to have no accidental spills/discharges when loading, transporting, or
unloading cake/dewatered sludge. However, the following spill containment, notification, and cleanup
procedure has been developed and should be followed in the event of an accidental spill or discharge:
• Identify the source of the spill/discharge and attempt to curtail or stop the flow.
• Immediately contact your supervisor. Explain your situation as thoroughly as possible. This will
allow your supervisor to assess the situation and take the appropriate action.
• Do not leave your vehicle unattended. Stay with your vehicle unless directed otherwise by the
proper authorities. Always comply fully with all requests from plant personnel, law
enforcement, or emergency personnel who may respond to the spill.
• Secure the spill site as soon as possible. Cake/dewatered sludge can be slippery. Take any
necessary steps to prevent sludge from being washed or tracked away from the immediate spill
site. Collect as much sludge as possible from the surface of the ground or pavement to help
prevent the sludge from being absorbed into the ground, and/or prevent run-off. Do not
attempt to wash away any spilled sludge.
• If the spill occurred at a customer site, contact the facility personnel at the location where you
were working when the spill/discharge occurred. Do not alarm them. Be calm, exact, and to the
point when describing the incident. Ask for their assistance if necessary.
• If the spill/discharge was large enough to require a site visit from your supervisor, do not leave
the area and do not remove or change any equipment. This will allow your supervisor
determine the correct cause of the incident.
• When all clean-up procedures have been completed, apply a cover of Ag lime to the area to
prevent odor and insect problems.
• It is the responsibility of the supervisor to follow up on all accidental spills/discharges. A
standard Spill Report Form must be filled out and turned in to a Denali Water Solutions
Environmental Manager.
• A Denali Water Solutions Environmental Manager will notify the regulatory authorities of the
spill/discharge.
• In the event of a large spill, Denali will contact IMS, A Hepaco Company, at 929 Professional
Place, Chesapeake, VA 23320 to assist with the cleanup. The 24-Hour Emergency Response
number is [phone].
Inspection Plan
To ensure that residuals are continuously applied at the correct application rate and in a manner
consistent with the Plan of Operations, Johnny Woods, a Project Manager with Denali, will be in direct
charge of the field operations, controlling the amount of residuals delivered to each field and conducting
daily field inspections. Field inspections will include ensuring that buffer flags are in place, residuals are

applied uniformly at the designated application rate, setbacks are observed, trucks are unloading at
proper locations, trucks are not driving over residuals, trucks are cleaned before leaving the application
site, and land application equipment is maintained in working condition.
Sampling and Monitoring Plan
Sample collection of the product will be overseen by Jeff Retzke, Senior Environment Manager with
Denali, and submitted to a certified laboratory for heavy metals (As, Cd, Cu, Pb, Hg, Mo, Ni, Se, Zn) to
determine compliance with Ceiling Concentrations or Monthly Average Concentrations, nutrients, and
pathogen reduction analysis [per 15A NCAC 02T.1106(a) and (b)(2)]. Tracking of the residual applied and
acreage applied will be accomplished through submittal of daily truck reports and weekly totals to the
Denali Environmental Department in combination with the analysis from labs. Annual reports will be
compiled by the Denali Environmental Department and submitted to NCDENR, Division of Water
Quality, Information Processing Unit on, or before, March 15Y of each year.
A more specific sampling schedule follows:
1. Nutrient and Metals
a. Frequency: Monitoring frequencies will be based on the actual dry tons applied per year
as established in 40 CFR 503 and 15A NCAC 02T.1111.
b. Sampling location: Output of belt presses (composite of multiple presses).
c. Laboratory: A&L Eastern Labs, Richmond, Virginia, or other North Carolina Certified lab.
2. Pathogen Reduction (fecal testing)
a. Not required since the Lake Kilby Class A water plant residual is not mixed with residuals
that were generated during the treatment of domestic wastewater, the treatment of
animal processing wastewater, or the biological treatment of industrial wastewater.
The Lake Kilby Class A water plant residual does not meet the definition of 'Biological
Residuals'.
3. Vector Attraction Reduction
a. Not required since the Lake Kilby Class A water plant residual is not mixed with residuals
that were generated during the treatment of domestic wastewater, the treatment of
animal processing wastewater, or the biological treatment of industrial wastewater.
The Lake Kilby Class A water plant residual does not meet the definition of 'Biological
Residuals'.
4. TCLP
a. Frequency: Once per Permit cycle.
b. Sampling location: Output of belt presses (composite of multiple presses).
c. Laboratory: Analytical Environmental Services, Inc. in Atlanta, Georgia, or other North
Carolina certified lab.
Land application activities are monitored on a daily basis through the use of Truck Reports/Daily Reports
and on a weekly basis through the use of a Weekly Report. These reports, along with residuals analysis
information and field specific information, provide the data used for preparation of annual reports.

Table of Contents
A. Cover Letter
B. Distribution of Class A Residual!
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source venerating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Denali Water Solutions, LLC
Status
Code °
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
Lake Kilby Water
Treatment Facility
Lake Kilby Water Treatment
Facility
Suffolk, an
Independent City
VA0006301
—2,400
—2,400
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Lake Kilby Water Treatment Plan
2. Facility permit holder is: Federal, L; State, 0 Local Government, or 0 Private.
Facility permit issued by: Div. of Water Resources, 0 Div. of Environmental Health,
or Other (explain: Virginia Department of Environmental Quality).
3. Facility contact person and title: C.B. Umphlette, Jr., Watershed Manager
Complete mailing address: 105 Maury Place
City: Suffolk
Telephone number: [phone] ext. 222
4. Facility physical address: 105 Maury Place
City: Suffolk State: Virginia
Coordinates: Latitude: 36' 43' 48"
Datum: _
State: Virginia Zip: 23434
E-mail address: cmphlette&portsmouthhighaualityh2o.org
Zip: 23434
Longitude: 76' 36' 08"
Level of accuracy: _
Method of measurement: Google Earth Maps
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
j other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes ® No
7. Facility permitted/design flow: 3_2 MGD and facility average daily flow: 1.4 MGD
8. Average amount of residuals being generated at this facility 2,000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The Lake Kilby Water Treatment Plant uses a conventional chemical coagulation
(aluminum Dolvhvdroxide)_ sedimentation. and filtration Drocess. Residuals are generated from clarifier sludge blow
downs, filter backwash operations, and filter to waste operations of the water production processes.
Type and volume of residuals storage (i.e., outside of residuals treatment units): The storage for the residuals consists of a
settling pond (lagoon) which is used to receive the residuals generated during the production of potable water. The lagoon
is generally oDerated so that a constant outfatt flow will canal the average input flow white maintaining a stable Dool
elevation.
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
FORM: RSC 06-16 Page 1 of 5

Biological ;Q Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: AES / Reed & Associates and Date of analysis: 8/3/2015 / 5/16/2019
Passed corrosivity test: yes no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes no. Flashpoint: = OF (> 140°F)
Passed reactivity test: 11yes Igno. HCN: <1.00 mg/kg (<250) & H2S: 152 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
< 0.05
Hexachlorobenzene
0.13
< 0.025
Barium
100.0
< 0.5
Hexachloro-1,3-Butadiene
0.5
< 0.025
Benzene
0.5
< 0.025
Hexachloroethane
3.0
< 0.025
Cadmium
1.0
< 0.005
Lead
5.0
< 0.05
Carbon Tetrachloride
0.5
< 0.025
Lindane
0.4
< 0.025
Chlordane
0.03
< 0.025
Mercury
0.2
< 0.0002
Chlorobenzene
100.0
< 0.025
Methoxychlor
10.0
< 0.025
Chloroform
6.0
< 0.025
Methyl Ethyl Ketone
200.0
< 0.5
Chromium
5.0
< 0.01
Nitrobenzene
2.0
< 0.025
m-Cresol
200.0
< 0.02
Pentachlorophenol
100.0
< 0.1
o-Cresol
200.0
< 0.025
Pyridine
5.0
< 0.025
p-Cresol
200.0
< 0.02
Selenium
1.0
< 0.05
Cresol
200.0
< 0.02
Silver
5.0
< 0.01
2,4-D
10.0
< 0.004
Tetrachloroethylene
0.7
< 0.025
1,4-Dichlorobenzene
7.5
< 0.025
Toxaphene
0.5
< 0.1
1,2-Dichloroethane
0.5
< 0.025
Trichloroethylene
0.5
< 0.025
1,1-Dichloroethylene
0.7
< 0.025
2,4,5-Trichlorophenol
400.0
< 0.025
2,4-Dinitrotoluene
0.13
< 0.025
2,4,6-Trichlorophenol
2.0
< 0.025
Endrin
0.02
< 0.005
2,4,5-TP (Silvex)
1.0
< 0.004
Heptachlor and its Hydroxide
0.008
< 0.005
Vinyl Chloride
0.2
< 0.025
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical, Richmond, VA and Date of analysis: 11/4/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
9.30
Cadmium
85
39
<0.585
Copper
4,300
1,500
37.8
Lead
840
300
14.2
Mercury
57
17
<0.0912
Molybdenum
75
n/a
<1.46
Nickel
420
420
13.3
Selenium
100
100
4.49
Zinc
7,500
2,800
74.9
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 17.1 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
rmcronutnent parameters:
Laboratory: Waypoint Analytical, Richmond, VA and Date of analysis: 11/4/2020
Parameter
Result
(mg1kg)
Aluminum
90,600
Ammonia -Nitrogen
292
Calcium
1,350
Magnesium
655
Nitrate -Nitrite Nitrogen
31.1
pH (Standard Unit)
6.7
Phosphorus
1,060
Potassium
116
Sodium
271
Total Kjeldahl Nitrogen
10,500
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): <5.00
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This
rate is a (check one): JW default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: Approved by NCDENR
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
4,260
6,458
Injection/Incorporation
4,406
6,604
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: None Known.
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
q Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
q Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
q Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
JA Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, 0 heat drying, 77 heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
El gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
J Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
J Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: El aerobic digestion, air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
11 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
El Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
El Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
El Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
El Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Table of Contents
A. Cover Letter
B. Distribution of Class A Residual!
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
q Frocess Flow uiagram/iNarrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

VICINITY MAP
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CONTRACT REMOVAL OF RESIDUALS PROJECT
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SEPTEMBER 2011
L
INDEX TO DRAWINGS
SHEET DWG.
No. No. DESCRIPTION
1 G-1 COVER SHEET, LOCATION MAP, AND INDEX TO DRAWINGS
2 C-1 LAGOON SITE PLAN AND SAMPLING DATA
3 C-2 DEWATERING AREA
4 C-3 DEWATERING AREA DETAILS
CITY OF PORTSMOUTH
DEPARTMENT OF PUBLIC UTILITIES
801 CRAWFORD STREET
PORTSMOUTH, VIRGINIA 23705
[phone]
CONTACT: MR. BRYAN FOSTER
ENGINEER
CH2M HILL
11818 ROCK LANDING DRIVE
SUITE 200
NEWPORT NEWS, VIRGINIA 23606
[phone], EXT. 41622
CONTACT: MR. ZACHARY CANODY

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Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Program Narrative
The residuals produced at the Lake Kilby Water Treatment Plant located in Suffolk, VA will be
mechanically dewatered on -site with the use of belt filter presses. Leachate from the dewatering
activities will be returned to the lagoon. The dewatered residuals will be transported to land application
sites in NC in sealed tailgate end -dump trailers hauled by road tractors. The volume contained in each
trailer will vary, but will typically average 23 wet tons. Residuals will be staged in the field prior to
spreading with typical side-slinger spreaders. There are no constituents of concern contained in the
material and the amount of nitrogen (N) and other plant essential nutrients is relatively low (see
attached laboratory data). The application of residuals will be limited to field crops and forage which
may include corn, cotton, soybeans, wheat, oats, milo, grassland, and alfalfa. The actual dosage rate will
be determined by the nitrogen requirement for the crop selected and yield goals in accordance with the
North Carolina Realistic Yield Database (http://yields.soil.nres.edu) prescription. Approximately
200-300 acres will receive residuals annually. Typical application rates will range from 23-46 wet tons
per acre. In accordance with good agronomic practice, areas which are unseasonably wet, therefore
producing rutting or damage to the field, will not be utilized for residuals application during those
periods. Compensation will be provided in order to maintain a soil pH of 6.0 or greater.

Page 1 of 1
EXAMPLE
WATER TREATMENT PLANT
T
SURFACE WAFER SUPPLY
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file:///C:/Users/j of£retzke/Documents/Virginia/Portsmouth,%20VA/Surface-Water-Treatme... 8/5/2016

Table of Contents
A. Cover Letter
B. Distribution of Class A Residual!
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) vicinity iviai
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Flan
c) Residuals Quality Information Laboratory Reports

Residuals Production Rate Quantitative Justification
The residuals produced at the Lake Kilby Water Treatment Plant located in Portsmouth, VA are stored in
a 75 million gallon lagoon. The lagoon is generally operated so that a constant outfall flow equals the
average input flows to the lagoon, while maintaining a stable pool elevation. This means that the
volume of the lagoon, in general, is stable. The bottom 20% of the lagoon (-15,000,000 gallons)
contains solids, at an average of 3.6%. Based on that information and the following equation, the dry
tons located in the lagoon can be calculated:
15,000,000 gallons 8.34 Ibs 3.6 Ibs dry 1 dry ton
lagoon X 1 gallon X 100 Ibs wet X 2000 Ibs dry - 2,251.8 dry tons

Table of Contents
A. Cover Letter
B. Distribution of Class A Residuals
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Sampling Plan
1. Nutrient and Metals
a. Frequency: Monitoring frequencies will be based on the actual dry tons applied per year
as established in 40 CFR 503 and 15A NCAC 02T.1111.
b. Sampling location: Output of belt presses (composite of multiple presses).
c. Laboratory: A&L Eastern Labs, Richmond, Virginia, or other North Carolina Certified lab.
2. Pathogen Reduction (fecal testing)
a. Not required since the Lake Kilby Class A water plant residual is not mixed with residuals
that were generated during the treatment of domestic wastewater, the treatment of
animal processing wastewater, or the biological treatment of industrial wastewater. The
Lake Kilby Class A water plant residual does not meet the definition of 'Biological
Residuals'.
3. Vector Attraction Reduction
a. Not required since the Lake Kilby Class A water plant residual is not mixed with residuals
that were generated during the treatment of domestic wastewater, the treatment of
animal processing wastewater, or the biological treatment of industrial wastewater. The
Lake Kilby Class A water plant residual does not meet the definition of 'Biological
Residuals'.
4. TCLP
a. Frequency: Once per Permit cycle.
b. Sampling location: Output of belt presses (composite of multiple presses).
c. Laboratory: Analytical Environmental Services, Inc. in Atlanta, Georgia, or other North
Carolina certified lab.

Table of Contents
A. Cover Letter
B. Distribution of Class A Residual!
a) Form DCAR 08-13
i) Delegation Letter
b) Program Information
i) Program Narrative
ii) Marketability Statement
iii) Information Sheet
c) Operation and Maintenance Plan
C. Residuals Source Certification
a) Form RSC 11-13
b) Residuals Source Generating Facility
i) Vicinity Map
ii) Process Flow Diagram/Narrative
iii) Residuals Production Rate Quantitative Justification
iv) Sampling Plan
c) Residuals Quality Information Laboratory Reports

Waypointo
ANALYTICAL
10/26/2020
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 20-290-0002
Project Description: Lake Kilby WTP 2019 1 &2 of 6
Jeff Retzke/ Denali Water
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/16/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-290-0002
Client Project Description: Lake Kilby WTP 2019 1&2 of 6
Jeff Retzke/ Denali Water
Lab No
Client Sample ID
Matrix
Date Collected Date Received
Method
Lab ID
73967
1
Solids
10/16/2020
73967
1
Solids
10/16/2020
4500NO3F-2011
WP MTN
73967
1
Solids
10/16/2020
SW-7471B
WP MTN
73967
1
Solids
10/16/2020
SM-4500-NH3C
WP MTN
73967
1
Solids
10/16/2020
6010D
WP MTN
73967
1
Solids
10/16/2020
SM-2540G
WP MTN
73967
1
Solids
10/16/2020
AOAC 955.01
WP MTN
73967
1
Solids
10/16/2020
9045D
WP MTN
73967
1
Solids
10/16/2020
SM-4500-NH3C-TKN
WP MTN
73968
2
Solids
10/16/2020
73968
2
Solids
10/16/2020
SM-4500-NH3C-TKN
WP MTN
73968
2
Solids
10/16/2020
SM-4500-NH3C
WP MTN
73968
2
Solids
10/16/2020
SM-2540G
WP MTN
73968
2
Solids
10/16/2020
4500NO3F-2011
WP MTN
73968
2
Solids
10/16/2020
AOAC 955.01
WP MTN
73968
2
Solids
10/16/2020
9045D
WP MTN
73968
2
Solids
10/16/2020
SW-7471B
WP MTN
73968
2
Solids
10/16/2020
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-290-0002
Lab No : 73967
Sample ID : 1
Project Lake Kilby WTP 2019 1&2 of 6
Report Date : 10/26/2020
Information : Jeff Retzke/ Denali Water Received : 10/16/2020
REPORT OFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled:
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
78.3
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Calcium Carbonate Equivalent
5.9
% - dry
0.1
1
10/21/20 13:00
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
410
mg/Kg -
dry
115
1
10/23/20 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
102
mg/Kg -
dry
22.4
1
10/21/20 14:41
ZBD
4500NO3F-2011
Organic N
7790
mg/Kg -
dry
1150
1
10/23/20 10:00
CALCULATION
pH
6.8
S.U.
1
10/22/2015:04
ADM
9045D
Total Solids
21.7
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Total Volatile Solids
47.5
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Total Kjeldahl Nitrogen
8200
mg/Kg -
dry
1150
1
10/23/20 10:00
JPJ
;M-4500-NH3C-TKI`
Phosphorus
1080
mg/Kg -
dry
23.0
1
10/22/20 02:31
JTR
6010D
Aluminum
163000
mg/Kg -
dry
115
5
10/23/20 00:09
JTR
6010D
Arsenic
6.91
mg/Kg -
dry
2.30
1
10/22/20 02:31
JADS
6010D
Calcium
2890
mg/Kg -
dry
230
1
10/22/20 02:31
JTR
6010D
Cadmium
<0.461
mg/Kg -
dry
0.461
1
10/22/20 02:31
JADS
6010D
Chromium
105
mg/Kg -
dry
1.15
1
10/22/20 02:31
JADS
6010D
Copper
45.9
mg/Kg -
dry
2.30
1
10/23/20 00:04
JTR
6010D
Iron
21800
mg/Kg -
dry
46.1
1
10/22/20 02:31
JTR
6010D
Lead
9.45
mg/Kg -
dry
1.38
1
10/22/20 02:31
JADS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 8

•
0
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Project
Lake Kilby WTP 2019 1&2 of 6
Jeff Retzke
Report
Date : 10/26/2020
1001 Fraser Ave
Information : Jeff Retzke/ Denali Water
Received : 10/16/2020
Huntsville , AL 35801
'�awl
�.
"� k' 0 I-ly
Pauric Mc Groary Ph.D., CPA
Report Number : 20-290-0002
REPORT OFANALYSIS
Agronomist
Lab No : 73967
Matrix:
Solids
Sample ID : 1
Sampled:
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Magnesium
544
mg/Kg
- dry
23.0
1
10/22/20 02:31
JADS
6010D
Manganese
5070
mg/Kg
- dry
11.5
5
10/23/20 00:09
JTR
6010D
Mercury <0.0635
mg/Kg
- dry
0.0635
1
10/21/20 13:08
DDB
SW-7471B
Molybdenum
2.12
mg/Kg
- dry
1.15
1
10/22/20 02:31
JADS
6010D
Nickel
19.0
mg/Kg
- dry
1.15
1
10/22/20 02:31
JADS
6010D
Potassium
119
mg/Kg
- dry
46.1
1
10/22/20 02:31
JTR
6010D
Selenium
<2.30
mg/Kg
- dry
2.30
1
10/23/20 00:04
JTR
6010D
Sodium
239
mg/Kg
- dry
115
1
10/22/20 02:31
JADS
6010D
Zinc
113
mg/Kg
- dry
5.76
1
10/22/20 02:31
JADS
6010D
Sulfur
10600
mg/Kg
- dry
46.1
1
10/22/20 02:31
JTR
6010D
Sodium Absorption Ratio
<23.0
mg/Kg
- dry
23.0
1
10/22/20 02:31
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 8

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-290-0002
Lab No : 73968
Sample ID : 2
Project Lake Kilby WTP 2019 1&2 of 6
Report Date : 10/26/2020
Information : Jeff Retzke/ Denali Water Received : 10/16/2020
REPORT OFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled:
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
81.6
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Calcium Carbonate Equivalent
4.9
% - dry
0.1
1
10/21/20 13:00
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
212
mg/Kg -
dry
136
1
10/23/20 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<27.1
mg/Kg -
dry
27.1
1
10/21/20 14:42
ZBD
4500NO3F-2011
Organic N
8860
mg/Kg -
dry
1360
1
10/23/20 10:00
CALCULATION
pH
6.7
S.U.
1
10/22/2015:04
ADM
9045D
Total Solids
18.4
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Total Volatile Solids
49.0
%
0.010
1
10/21/20 16:53
CJR
SM-2540G
Total Kjeldahl Nitrogen
9080
mg/Kg -
dry
1360
1
10/23/20 10:00
JPJ
;M-4500-NH3C-TKI`
Phosphorus
1080
mg/Kg -
dry
27.2
1
10/22/20 02:46
JTR
6010D
Aluminum
189000
mg/Kg -
dry
136
5
10/23/20 00:18
JTR
6010D
Arsenic
7.77
mg/Kg -
dry
2.72
1
10/22/20 02:46
JADS
6010D
Calcium
1780
mg/Kg -
dry
272
1
10/22/20 02:46
JTR
6010D
Cadmium
<0.543
mg/Kg -
dry
0.543
1
10/22/20 02:46
JADS
6010D
Chromium
130
mg/Kg -
dry
1.36
1
10/22/20 02:46
JADS
6010D
Copper
35.8
mg/Kg -
dry
2.72
1
10/23/20 00:13
JTR
6010D
Iron
23300
mg/Kg -
dry
54.3
1
10/22/20 02:46
JTR
6010D
Lead
11.0
mg/Kg -
dry
1.63
1
10/22/20 02:46
JADS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 5 of 8

•
0
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
07274
Denali Water
Project
Lake Kilby WTP 2019 1&2 of 6
Jeff Retzke
Report
Date : 10/26/2020
1001 Fraser Ave
Information : Jeff Retzke/ Denali Water
Received : 10/16/2020
Huntsville , AL 35801
'�awl
�.
"� k' 0 I-ly
Pauric Mc Groary Ph.D., CPA
Report Number : 20-290-0002
REPORT OFANALYSIS
Agronomist
Lab No : 73968
Matrix:
Solids
Sample ID : 2
Sampled:
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Magnesium
679
mg/Kg
- dry
27.2
1
10/22/20 02:46
JADS
6010D
Manganese
2230
mg/Kg
- dry
2.72
1
10/22/20 02:46
JTR
6010D
Mercury <0.0847
mg/Kg
- dry
0.0847
1
10/21/20 13:09
DDB
SW-7471B
Molybdenum
1.51
mg/Kg
- dry
1.36
1
10/22/20 02:46
JADS
6010D
Nickel
13.9
mg/Kg
- dry
1.36
1
10/22/20 02:46
JADS
6010D
Potassium
114
mg/Kg
- dry
54.3
1
10/22/20 02:46
JTR
6010D
Selenium
<2.72
mg/Kg
- dry
2.72
1
10/23/20 00:13
JTR
6010D
Sodium
274
mg/Kg
- dry
136
1
10/22/20 02:46
JADS
6010D
Zinc
67.4
mg/Kg
- dry
6.79
1
10/22/20 02:46
JADS
6010D
Sulfur
13100
mg/Kg
- dry
54.3
1
10/22/20 02:46
JTR
6010D
Sodium Absorption Ratio
<27.2
mg/Kg
- dry
27.2
1
10/22/20 02:46
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
L Limit Exceeded
Page 6 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 20-290-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
® No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
® No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ISamantha Clarke Date & Time: 10/16/2020 11:43:17
Page 7 of 8

SAMPLE
¢�z
7621 Whitepine Road Richmond V, Denali water 11.40.43
TSTQDY
upportale aleastcm.com
Account #
Lake KitbV W 1 P LaIS IbL
i Submitted By
a
Copy To
L Jeff Retake/Denali Water 20: DEW
jeff.retzkeadenaliwater.com
3308 Bernice Avenue
Jeff's Cell: 256.503.4300
Russellville, AR 72802
Project Lake Kilby WTP 2019 1&2 0 6
Sample Information
Lab Number
Collection information
Container Information
Please Check Desired Tests
Number
503
Nitrogen
Volatile
Sample 10
(Lab Use
Only)
Type
Date
Time
of Bottles
Type
Volume
SL1
SL2
Metals
Series
pH
CCE
Ag
Cl
Solids
others
Grab
Standard Compoa
1 _
+
_ Glass
x
X
pint
w/Aluminum, CCE
Composite
Plastic
qt
and S.A.R.
~ r `
Grab
%
1
_ Glass
x
az
pint
same as above
x Plastic
Cam osite
Grab
Glass
02
Plastic
pint
Composite
qt
Grab
Glass
— —
Oz
—
Plastic
pint
Composite
Relin ui d B (Signature)
Date
Jime
Received B (Signature)
bate
Time
Test Package Detailils
Special Instructions or Remarks
SL1: Total Solids (Moisture) Total K.leldahl Nitrogen, phosphorus and Potassium
SL2: 9asic Test SL I plus Sulfur, Calcium, Magpesium,5odium_ Iron, Aluminum, Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum. Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
ice
Nitrogen Series: total k1eldahl. Ammonium, Nitrate & OrWic Nitrogen
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Waypointo
ANALYTICAL
11 /16/2020
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 20-310-0005
Project Description: Lake Kilby WTP 2019 5&6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/5/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-310-0005
Client Project Description: Lake Kilby WTP 2019 5&6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74112
5
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
74113
6
Solids
11/04/2020
11:40
11/05/2020
4500NO3F-2011
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C
WP MTN
6010D
WP MTN
SM-2540G
WP MTN
AOAC 955.01
WP MTN
9045D
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-4500-NH3C
WP MTN
SM-2540G
WP MTN
4500NO3F-2011
WP MTN
AOAC 955.01
WP MTN
9045D
WP MTN
SW-7471B
WP MTN
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-310-0005
Lab No : 74112
Sample ID : 5
Project
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Lake Kilby WTP 2019 5&6
REPORT OFANALYSIS
Report Date : 11/16/2020
Received : 11/05/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
83.7
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Calcium Carbonate Equivalent
9.7
% - dry
0.1
1
11/09/20 10:25
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
681
mg/Kg -
dry
153
1
11/12/20 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<31.0
mg/Kg -
dry
31.0
1
11/12/20 15:47
CLP
4500NO3F-2011
Organic N
12300
mg/Kg -
dry
1530
1
11/12/20 10:00
CALCULATION
pH
6.7
S.U.
1
11/09/2016:44
ADM
9045D
Total Solids
16.3
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Total Volatile Solids
51.8
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Total Kjeldahl Nitrogen
13000
mg/Kg -
dry
1530
1
11/12/20 10:00
JPJ
;M-4500-NH3C-TKI`
Phosphorus
1190
mg/Kg -
dry
30.7
1
11/12/20 00:10
TJS
6010D
Aluminum
96300
mg/Kg -
dry
307
10
11/12/20 19:06
TJS
6010D
Arsenic
9.45
mg/Kg -
dry
3.07
1
11/12/20 00:10
TJS
6010D
Calcium
1500
mg/Kg -
dry
307
1
11/12/20 00:10
TJS
6010D
Cadmium
<0.613
mg/Kg -
dry
0.613
1
11/12/20 00:10
TJS
6010D
Chromium
148
mg/Kg -
dry
1.53
1
11/12/20 00:10
TJS
6010D
Copper
43.3
mg/Kg -
dry
3.07
1
11/12/20 00:10
TJS
6010D
Iron
22900
mg/Kg -
dry
61.3
1
11/12/20 00:10
TJS
6010D
Lead
16.6
mg/Kg -
dry
1.84
1
11/12/20 00:10
TJS
6010D
Qualifiers/ B
Analyte detected in blank
DF Dilution Factor
Definitions L
Limit Exceeded
MQL Method Quantitation Limit
Page 3 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-310-0005
Lab No : 74112
Sample ID : 5
Project
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Lake Kilby WTP 2019 5&6
REPORT OFANALYSIS
Report Date : 11/16/2020
Received : 11/05/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Magnesium
724
mg/Kg -
dry
30.7
1
11/12/20 00:10
TJS
6010D
Manganese
2360
mg/Kg -
dry
3.07
1
11/12/20 00:10
TJS
6010D
Mercury
<0.0871
mg/Kg -
dry
0.0871
1
11/10/20 12:42
DDB
SW-7471B
Molybdenum
<1.53
mg/Kg -
dry
1.53
1
11/12/20 00:10
TJS
6010D
Nickel
14.5
mg/Kg -
dry
1.53
1
11/12/20 00:10
TJS
6010D
Potassium
125
mg/Kg -
dry
61.3
1
11/12/20 00:10
TJS
6010D
Selenium
5.66
mg/Kg -
dry
3.07
1
11/12/20 00:10
TJS
6010D
Sodium
291
mg/Kg -
dry
153
1
11/12/20 00:10
TJS
6010D
Zinc
84.0
mg/Kg -
dry
7.67
1
11/12/20 00:10
TJS
6010D
Sulfur
14800
mg/Kg -
dry
61.3
1
11/12/20 00:10
TJS
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
11/12/20 00:10
CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions L Limit Exceeded
DF Dilution Factor
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-310-0005
Lab No : 74113
Sample ID : 6
Project
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Lake Kilby WTP 2019 5&6
REPORT OFANALYSIS
Report Date : 11/16/2020
Received : 11/05/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
82.9
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Calcium Carbonate Equivalent
9.2
% - dry
0.1
1
11/09/20 10:25
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
292
mg/Kg -
dry
146
1
11/12/20 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
31.1
mg/Kg -
dry
30.1
1
11/12/20 15:48
CLP
4500NO3F-2011
Organic N
10200
mg/Kg -
dry
1460
1
11/12/20 10:00
CALCULATION
pH
6.7
S.U.
1
11/09/2016:44
ADM
9045D
Total Solids
17.1
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Total Volatile Solids
52.4
%
0.010
1
11/09/20 17:05
FMM
SM-2540G
Total Kjeldahl Nitrogen
10500
mg/Kg -
dry
1460
1
11/12/20 10:00
JPJ
;M-4500-NH3C-TKI`
Phosphorus
1060
mg/Kg -
dry
29.2
1
11/12/20 00:15
TJS
6010D
Aluminum
90600
mg/Kg -
dry
292
10
11/12/20 19:11
TJS
6010D
Arsenic
9.30
mg/Kg -
dry
2.92
1
11/12/20 00:15
TJS
6010D
Calcium
1350
mg/Kg -
dry
292
1
11/12/20 00:15
TJS
6010D
Cadmium
<0.585
mg/Kg -
dry
0.585
1
11/12/20 00:15
TJS
6010D
Chromium
133
mg/Kg -
dry
1.46
1
11/12/20 00:15
TJS
6010D
Copper
37.8
mg/Kg -
dry
2.92
1
11/12/20 00:15
TJS
6010D
Iron
20300
mg/Kg -
dry
58.5
1
11/12/20 00:15
TJS
6010D
Lead
14.2
mg/Kg -
dry
1.75
1
11/12/20 00:15
TJS
6010D
Qualifiers/ B
Analyte detected in blank
DF Dilution Factor
Definitions L
Limit Exceeded
MQL Method Quantitation Limit
Page 5 of 8

Waypointo
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 20-310-0005
Lab No : 74113
Sample ID : 6
Project
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Lake Kilby WTP 2019 5&6
REPORT OFANALYSIS
Report Date : 11/16/2020
Received : 11/05/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Magnesium
655
mg/Kg -
dry
29.2
1
11/12/20 00:15
TJS
6010D
Manganese
2110
mg/Kg -
dry
2.92
1
11/12/20 00:15
TJS
6010D
Mercury
<0.0912
mg/Kg -
dry
0.0912
1
11/10/20 12:44
DDB
SW-7471B
Molybdenum
<1.46
mg/Kg -
dry
1.46
1
11/12/20 00:15
TJS
6010D
Nickel
13.3
mg/Kg -
dry
1.46
1
11/12/20 00:15
TJS
6010D
Potassium
116
mg/Kg -
dry
58.5
1
11/12/20 00:15
TJS
6010D
Selenium
4.49
mg/Kg -
dry
2.92
1
11/12/20 00:15
TJS
6010D
Sodium
271
mg/Kg -
dry
146
1
11/12/20 00:15
TJS
6010D
Zinc
74.9
mg/Kg -
dry
7.31
1
11/12/20 00:15
TJS
6010D
Sulfur
13200
mg/Kg -
dry
58.5
1
11/12/20 00:15
TJS
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
11/12/20 00:15
CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 6 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 07274
Customer Name: Denali Water
Report Number: 20-310-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 11/05/2020 13:34:49
Page 7 of 8

SAMPLE Tl
7621 Whilepinc Road Richmond VA 2
IIIII IIII illlilllllll 11111IIIIIIIIII III IIIIIIIII�IIIIIIII 074
2
Denali Water 13.30:27
Lake Kilhy WTP 2019 5&5
13TODY
pportal e(w al east ern s nm
Account #
Submitted By Charge To Copy To
PO: DEW [e-mail]
Jeff RetzkelDenali Water
3308 Bernice Avenue Jeff's Cell: 256.503.4300
Russellville, AR 72802
Project Lake Kilby WTP 2019 O & of 6
aafn le Information[
Lab Number
Collection Information
Container Information
Please Check Desired Tests
Sample ID
(Lab Use
Only)
Type
mate
Time
Number
Type
Volume
SL1
SL
ta
Nitrogen
pH
CCE
Ag
Cl
Volatile
Others
Of Bottles
ls
Metals
Series
Solids
�41J 1 2
Grab
�
r
1
Glass
oz
�lnt
Standara Compos'
w/Aluminum, CCE
I
�O
x Plastic
Composite
qt
and S.A.R.
Grab
f
1
Glass
Plastic
Oz
x inE
Same as above
Composite
l
V
Grab
Glass
— olnt
Plastic
�t
Corn site
Grab
Glass
oz
Plastic
lnt
lComposite
I
I
I
I—
qt
Time
l uuis (Signature)
Date
Time
Received 8 : (Signature)
Date
r
L
Test Packa a Details
Special Instructions or Remarks
SLI: Total Solids (Moisture) Total Kieldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnesiuttt Sodium, Iron, Aluminum, Manganese, Copper And Zinc
19
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
Nitrogen Series: Total Kieldahl, Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

CLIENT: Pancopia
SAMPLE RECEIPT
ATTN: Bill Cumbie
DATE: 5/16/2019 TIME: 1535
ADDRESS: 1100 Exploration Way, Suite 302
GRAB COLLECTION
REED,,
ssoctl+��
CITY: Hampton, VA 23666
DATE: 5/15/2019 TIME: 2143
PHONE: [phone]
COLLECTED BY: CLIENT
EMAIL/[e-mail]
PICK UP BY: CLIENT
NUMBER OF CONTAINERS: 2
GOOD CONDITION © Good ❑
Other (See C-O-C)
SPECIAL NOTES:
REPORT NO: 19-08628 8:32
RE: PORTSMOUTH LAGOON
SAMPLE ID: Lagoon
SAMPLE NO 19-08628
EPA
Regulatory
HW
Method
JRA
level
Parameter
No.
Number
QL (mg/L)
(mg/L)
Result (mg/L)
Analyst/Date/Time
Toxic Characteristic Leaching Procedure by SW-846 Method 1311
Arsenic
D004
6010D
0.050
5
< 0.050
AME
5/24/2019
1505
Barium
D005
6010D
0.500
100
< 0.500
AME
5124/2019
1505
Benzene
D018
8260D
0.025
0.5
< 0.025
SDT
5/23/2019
0921
Cadmium
D006
6010D
0.005
1
< 0.005
AME
5/24/2019
1505
Carbon Tetrachloride
D019
8260D
0.025
0.5
< 0.025
SDT
5/23/2019
0921
Chlordane
D020
8270E
0.025
0.03
< 0.025
CLH
5/30/2019
1941
Chlorobenzene
D021
8260D
0.025
100
< 0.025
SDT
5/23/2019
0921
Chloroform
D022
8260D
0.025
6
< 0.025
SDT
5/23/2019
0921
Chromium
D007
6010D
0.010
5
< 0.010
AME
5/24/2019
1505
o-Cresol
D023
8270E
0.025
200
< 0.025
CLH
5/30/2019
1941
m/p-Cresol
D024
8270E
0.02
200
< 0.02
CLH
5/30/2019
1941
Cresol
D026
8270E
0.02
200
< 0.02
CLH
5/30/2019
1941
2,4-D
D0 M
8151A
0.004
10
< 0.004
ADT
6/4/2019
2236
1,4-Dichlorobenzene
D027
8260D
0.025
7.5
<0.025
SDT
5/23/2019
0921
1,2-Dichloroethane
D028
8260D
0.025
0.5
< 0.025
SDT
5/23/2019
0921
1, 1 -Dichloroethylene
D029
8260D
0.025
0.7
<0.025
SDT
5/23/2019
0921
2,4-Dinitrotoluene
D030
8270E
0.025
0.13
< 0.025
CLH
5/30/2019
1941
Endrin
D012
8270E
0.005
0.02
< 0.005
CLH
5/30/2019
1941
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23606
[phone] • Fax: [phone]
Pagel of 3
VELAP# 460013
EPA# VAOOOII

SAMPLE ID: Lagoon
SAMPLE NO 19-08628
EPA
Regulatory
HW
Method
JRA
level
Parameter
No.
Number
QL (mg/L)
(mg/L)
Result (mg/L)
Analyst/Date/Time
Heptachlor (+epoxide)
D031
8270E
0.005
0.008
< 0.005
CLH
5/30/2019
1941
Hexachlorobenzene
D032
8270E
0.025
0.13
< 0.025
CLH
5/30/2019
1941
Hexachloro-1,3-butadiene
D033
8270E
0.025
0.5
<0.025
CLH
5/30/2019
1941
Hexachloroethane
D034
8270E
0.025
3
< 0.025
CLH
5/30/2019
1941
Lead
D008
601OD
0.050
5
<0.050
AME
5/24/2019
1505
Lindane
D013
8270E
0.025
0.4
< 0.025
CLH
5/30/2019
1941
Mercury
D009
7470A
0.0002
0.2
< 0.0002
SDT
5/22/2019
1346
Methoxychlor
D014
8270E
0.025
10
< 0.025
CLH
5/30/2019
1941
Methyl ethyl Ketone
D035
8260D
0.5
200
< 0.5
SDT
5/23/2019
0921
Nitrobenzene
D036
8270E
0.025
2
< 0.025
CLH
5/30/2019
1941
Pentachlorophenol
D037
8270E
0.1
100
< 0.1 M
CLH
5/30/2019
1941
Pyridine
D038
8270E
0.025
5
< 0.025
CLH
5/30/2019
1941
Selenium
DOW
601OD
0.050
1
<0.050
AME
5/24/2019
1505
Silver
DO] 1
601 OD
0.010
5
< 0.010
AME
5/24/2019
1505
Tetrachloroethylene
D039
8260D
0.025
0.7
< 0.025
SDT
5/23/2019
0921
Toxaphene
D015
8270E
0.1
0.5
< 0.1
CLH
5/30/2019
1941
Trichloroethylene
D040
8260D
0.025
0.5
< 0.025
SDT
5/23/2019
0921
2,4,5-Trichlorophenol
D041
8270E
0.025
400
< 0.025
CLH
5/30/2019
1941
2,4,6-Trichlorophenol
D042
8270E
0.025
2
< 0.025
CLH
5/30/2019
1941
2,4,5-TP
DO 17
8151 A
0.004
1
< 0.004
ADT
6/4/2019
2236
Vinyl Chloride
D043
8260D
0.025
0.2
< 0.025
SDT
5/23/2019
0921
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23606
[phone] • Fax: [phone]
Page 2 of 3
VELAP# 460013
EPA# VA00015

REPORT OF ANALYSIS
NoTL: - --- ---
JRA Quantification Level is the concentration of the lowest calibration standard above zero with a reliable signal.
Reproduction of this report is not permitted, except in full, without written approval from James R Reed & Associates.
The results on this report relate only to the sample(s) provided for analysis.
Results conform to NELAC standards, where applicable, unless otherwise indicated.
*SM 2011
M - Matrix spike % recovery outside QC acceptance range RESPECTFULLY SUBMITTED
Method 8270E-TCLP: Surrogate (2,4,6-tribromophenol) recovery Q,'
outside QC acceptance range +gam""' 62a�
Elaine Claiborne
Laboratory Director
06-Jun-19
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23605 VELAP# 450013
EPA# VA00015
[phone] 0 Fax: [phone]
e
Page 3 of 3

CHAIN OF CUSTODY
,�U"
Vl(c./19ANALYSES REQUESTED
Company Name: Pancopia
Company Contact: Bill Cumbie Telephone: [phone]
Results To: Bill Cumbie email: [e-mail]
Address: 1100 Exploration Way, Suite 302Q
Hampton, VA 23666
Project ID: Portsmouth - Lagoon
"WW= Wastewater, GW = Groundwater, DW - Drinking Water, HW - Hazardous Waste, OTHERS
Sampled By:
Relinquished By:
Received By:
Relinquished By:
Received By:
_for Compliance
_Not for Compliance
Date/Time: 5 ; 5 ,;
Date/Time:
Date/Time: t/jLr�+
Date/Time
Daten"ime: ,f�01
Preservatives:
1 = <6°C 6 = Na2S203+ HCI 10=Ascorbic Acid + HCI
2 = HNO3 7 = NaOH + ZnOAc 11=HCI
3 = H2SO4 8 = H2SO4+ FAS 12=Zinc Acetate + NaOH
4 = NaOH 9 = NH4CI 13=Na2SO3+ HCl
5 = Na2S203 14=Na2SO3+ H2SO4
Arrival Temp: i °C
JAMES R. REED and ASSOCIATES [phone]; FAX [phone]
770 Pilot House Drive, Newport News, VA 23606

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
August 03, 2015
Jeff Retzke
Denali Water Solutions
P.O. Box 3036
Russellville AR 72811
TEL:
FAX:
RE: Lake Kilby WTP
Dear Jeff Retzke: Order No: 1507L31
Analytical Environmental Services, Inc. received 1 samples on July 24, 2015 10:15 am
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative.
AES' certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/15-06/30/16.
-AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Organics,
Inorganics), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental
Microbiology (Fungal) Direct Examination, effective until 09/01/15.
These results relate only to the items tested. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
�fze'�/'w
Chantelle Kanhai
Project Manager
3080 Presi4enIial Drivc * Atlanta, Georgia 30340 - Tel: 770.45T8177 - Fax: 770-457_$188 • ` cll Free :80O.972.4389
W-WW.aesatlanta.com Page 1 of 8

ANALYTICAL ENVIRONMENTAL SERVICES, INC
3080 Presidential Drive, Atlanta GA 30340-3704
A S TEL.: [phone] / TOLL -FREE [phone] / FAX: [phone]
CHAIN OF CUSTODY
Work Order: ' 5� L3 I
I,,r.,. -7h; IN p..-,
COMPANY PADDRESSS
e44 �q
P,Q � 80A 3036
.ANALYSIS REQUESTED
l ��
Visit our website
nn /� p
Pa,Bit &3� K�sse��u,�� 11F wN
&Vlklle 0 ?;M
www.aesatlanta.com
4
to check on the status of
PHONE
" 3" J
FAX
3d
C�
~
Four results, place bottle
G
SAMPLED BY�N
J
SIGNATURE
t�
�
orders, etc.
o
x
S.4
LED
#
SAMPLE ID
c
d
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PRESERVATION (See codes)
o
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REMARKS
ATE
TIME
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2
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9
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ZIN USHED DATE/TIME
l:
RECEIVEDBY DATE/TIME
PRO.JECTINFORMATION
RECEIPT
1.
PROJECT NAME a
C,g�C�,. r l
_
16 w
Total # of Containers
2
PROJECT #: Tumaround Time Request
SITE ADDRESS:
n,I Standard 5 Business Days
3: P11I1u�v+ram ��
O 2 Business Day Rush
4
SEND REPORT TO: t Z O Next Business Day Rush
SPECIAL INSTRUCTIONS/COMMENTS: SHIPMENT METHOD INVOICE TO: Ls IG�z 4(9 O Same Day Rush (auth req.)
V�
OUT VIA : (IF DIFFERENT FROM ABOVE)
�� �av�� f� Other _
IN / / VIA: STATE PROGRAM(ifany): -N—C
CLIENT FedEx JPS MAIL COURIER
E-mail? Y / N; Fax? Y / N
GREYHOUND OTHER QUOTE#: PO# DATAPACKAGE: 1 H III IV
SAMPLES RECEIVED AFTER 3PM OR ON SATURDAY ARE CONSIDERED RECEIVED THE NEXT BUSINESS DAY. IF TURNAROUND TIME 1S NOT INDICATED, AES WILL PROCEED WITH STANDARD TAT OF SAMPLES,
SAMPLES ARE DISPOSED 30 DAYS AFTER REPORT COMPLETION UNLESS OTHER ARRANGEMENTS
ARE MADE.
Nn o ru nr CnnU lsz
, ....... I . .,,,.. .,.. - d— taid—) v v = vrmxmg vvater ltsianxs) v = vmer Ispeary) vv vv = Waste Water
PRESERVATIVE CODES: H+I = Hydrochloric acid + ice I = Ice only N = Nitric acid S+1 = Sulfuric acid + ice S/M+I = Sodium Bisulfate/Methanol + ice O = Other (specify) NA = None
White Copy - Original; Yellow Copy - Client

Analytical Environmental Services, Inc
Date: 3-Aug-15
Client: Denali Water Solutions
Project: Lake Kilby WTP Case Narrative
Lab ID: 15071,31
pH Analysis by Method SW90451):
Samples for pH Analysis by Method SW 9045D were received and analyzed outside holding time requirement of "immediate or
15 minutes".
Page 3 of 8

Analytical Environmental Services, Inc
Date: 3-Aug-15
Client:
Denali Water Solutions
Client Sample ID:
LAKE KILBY WTP
Project Name:
Lake Kilby WTP
Collection Date:
7/23/2015 2:30:00 PM
Lab ID:
15071,31-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatchID
Dilution
Factor
Date Analyzed Analyst
VOLATILES, TCLP SW1311/8260B
(SW5030B)
1,1-Dichloroethene
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
1,2-Dichloroethane
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
2-Butanone
BRL
1.0
mg/L 210746
50
07/28/2015 19:55
TH
Benzene
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Carbon tetrachloride
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Chlorobenzene
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Chloroform
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Tetrachloroethene
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Trichloroethene
BRL
0.50
mg/L 210746
50
07/28/2015 19:55
TH
Vinyl chloride
BRL
0.20
mg/L 210746
50
07/28/2015 19:55
TH
Surr:4-Bromofluorobenzene
88.2
68.7-127
%REC 210746
50
07/28/2015 19:55
TH
Surr: Dibromofluoromethane
114
77.4-121
%REC 210746
50
07/28/2015 19:55
TH
Surr: Toluene-d8
97
79.2-120
%REC 210746
50
07/28/2015 19:55
TH
Sulfide, Reactive SW846-7.3
(SW7.3.4.2)
Sulfide, Reactive
152
100
mg/Kg 210820
1
07/30/2015 09:00
PF
SEMIVOLATILES ORGANICS, TCLP
SW1311/8270D
(SW3510C)
1,4-Dichlorobenzene
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
2,4,5-Trichlorophenol
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
2,4,6-Trichlorophenol
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
2,4-Dinitrotoluene
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Hexachlorobenzene
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Hexachlorobutadiene
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Hexachloroethane
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
m,p-Cresol
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Nitrobenzene
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
o-Cresol
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Pentachlorophenol
BRL
0.50
mg/L 210795
1
07/30/2015 18:35
YH
Pyridine
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Cresols, Total
BRL
0.10
mg/L 210795
1
07/30/2015 18:35
YH
Surr:2,4,6-Tribromophenol
67.3
52.5-139
%REC 210795
1
07/30/2015 18:35
YH
Surr:2-Fluorobiphenyl
82.5
56-128
%REC 210795
1
07/30/2015 18:35
YH
Surr:2-Fluorophenol
80.3
49.4-119
%REC 210795
1
07/30/2015 18:35
YH
Surr:4-Terphenyl-dl4
92.5
58.7-137
%REC 210795
1
07/30/2015 18:35
YH
Surr: Nitrobenzene-d5
84.7
49.8-126
%REC 210795
1
07/30/2015 18:35
YH
Surr: Phenol-d5
84.9
46-121
%REC 210795
1
07/30/2015 18:35
YH
POLYCHLORINATED BIPHENYLS
SW8082A
(SW3550C)
Aroclor 1016
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Aroclor 1221
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Qualifiers: a Value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due
to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not confirmed
B Analyte detected in the associated method blank
<
Less than Result value
Page 4 of 8
> Greater than Result value
J
Estimated value detected below
Reporting Limit

Analytical Environmental Services, Inc
Date: 3-Aug-15
Client:
Denali Water Solutions
Client Sample ID:
LAKE KILBY WTP
Project Name:
Lake Kilby WTP
Collection Date:
7/23/2015 2:30:00 PM
Lab ID:
15071,31-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatchID
Dilution
Factor
Date Analyzed Analyst
POLYCHLORINATED BIPHENYLS SW8082A
(SW3550C)
Aroclor 1232
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Aroclor 1242
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Aroclor 1248
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Aroclor 1254
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Aroclor 1260
BRL
210
ug/Kg-dry 210657
1
07/28/2015 20:46
SH
Surr: Decachlorobiphenyl
97.4
36.1-138
%REC 210657
1
07/28/2015 20:46
SH
Surr: Tetrachloro-m-xylene
64.8
28.3-116
%REC 210657
1
07/28/2015 20:46
SH
PESTICIDES, TCLP SW1311/8081B
(SW3510C)
Chlordane
BRL
0.0050
mg/L 210718
1
07/29/2015 20:09
SH
Endrin
BRL
0.0010
mg/L 210718
1
07/29/2015 20:09
SH
gamma-BHC
BRL
0.00050
mg/L 210718
1
07/29/2015 20:09
SH
Heptachlor
BRL
0.00050
mg/L 210718
1
07/29/2015 20:09
SH
Heptachlor epoxide
BRL
0.00050
mg/L 210718
1
07/29/2015 20:09
SH
Methoxychlor
BRL
0.0050
mg/L 210718
1
07/29/2015 20:09
SH
Toxaphene
BRL
0.050
mg/L 210718
1
07/29/2015 20:09
SH
Surr: Decachlorobiphenyl
83.1
31.9-136
%REC 210718
1
07/29/2015 20:09
SH
Surr: Tetrachloro-m-xylene
63.7
32.7-110
%REC 210718
1
07/29/2015 20:09
SH
MERCURY, TCLP SW1311/7470A
(SW7470A)
Mercury
BRL
0.00400
mg/L 210660
1
07/29/201515:15
TA
Laboratory Hydrogen Ion (pH) SW9045D
(SW9045D)
pH
6.81
0.01
H
pH Units 210698
1
07/28/2015 10:00
JS
Ignitability SW1010A
Ignitability
180
0
>
°F R296765
1
07/28/2015 09:00
JC
ICPMETALS,TCLP SW1311/6010C
(SW3010A)
Arsenic
BRL
0.250
mg/L 210744
1
07/29/201519:07
TA
Barium
BRL
0.500
mg/L 210744
1
07/29/201519:07
TA
Cadmium
BRL
0.0250
mg/L 210744
1
07/29/201519:07
TA
Chromium
BRL
0.0500
mg/L 210744
1
07/29/201519:07
TA
Lead
BRL
0.0500
mg/L 210744
1
07/29/201519:07
TA
Selenium
BRL
0.100
mg/L 210744
1
07/29/201519:07
TA
Silver
BRL
0.0250
mg/L 210744
1
07/29/201519:07
TA
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.20
mg/L 210754
1
07/31/2015 11:34
AW
2,4-D
BRL
0.20
mg/L 210754
1
07/31/2015 11:34
AW
Surr: DCAA
75
49.6-143
%REC 210754
1
07/31/2015 11:34
AW
Qualifiers: ° Value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due
to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not confirmed
B Analyte detected in the associated method blank
<
Less than Result value
Page 5 of 8
> Greater than Result value
J
Estimated value detected below
Reporting Limit

Analytical Environmental Services, Inc
Date: 3-Aug-15
Client:
Denali Water Solutions
Client Sample ID:
LAKE KILBY WTP
Project Name:
Lake Kilby WTP
Collection Date:
7/23/2015 2:30:00 PM
Lab ID:
15071,31-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Cyanide, Reactive SW846-7.3 (SW7.3.3.2)
Cyanide, Reactive BRL 1.00 mg/Kg 210878 1 07/31/2015 10:00 PF
PERCENT MOISTURE D2216
Percent Moisture 52.9 0 wt% R296994 1 07/30/2015 10:00 PF
Qualifiers: .
Value exceeds maximum contaminant level
BRL
Below reporting limit
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
>
Greater than Result value
E
Estimated (value above quantitation range)
S
Spike Recovery outside limits due to matrix
Nan
Seecasenarrative
NC
Not confirmed
<
Less than Result value
J Estimated value detected below Reporting Limit Page 6 of 8

Analytical Environmental Services, Inc.
Sample/Cooler Receipt Checklist
Clientiloa t, "e- 561VIS Work Order Number 7U I5o
%A Checklist completed by
Signature Date
Carrier name: FedEx _ UPS ✓ C'urierClient US !Mail Other
Shipping container/cooler in good condition? Yes No
Custody seals intact on shipping container/cooler? Yes ✓ No
Custody seals intact on sample bottles? Yes _ No
Container/Temp Blank temperature in compliance? (0°=6°C)* Yes No _
CI#3s�
Not Present
Not Present
Not Present 1/
oo er 1 Cooler 42 Cooler #, Cooler 94 Cooler45
Chain of custody present?
Yes No
Chain of custody signed when relinquished and received?
Yes No
Chain of custody agrees with sample labels?
Yes ✓ No
Samples in proper container/bottle?
Yes No
Sample containers intact?
/
Yes ✓/ No
Sufficient sample volume for indicated test?
Yes ✓_ C*4'�o
_
All samples received within holding ?$'
p time.
Yes o
Was TAT marked on the COC?
Yes -� No
Proceed with Standard TAT as per project history?
Yes _
/No
Water - VOA vials have zero headspace? No VOA vials submitted ✓ Yes
Water - pH acceptable upon receipt?
Yes No
Adjusted?
Sample Condition: Good Other(Explain)
(For diffusive samples or AIHA lead) Is a known blank included?
See Case Narrative for resolution of the Non -Conformance.
Checked by
Yes _ No
Cooler #6
Not Applicable ✓
No
Not Applicable
* Samples do not have to comply with the given range for certain parameters.
\\Aes_server\I\Sample Receipt\My Documents\COCs and pH Adjustment Sheet\Sample_Cooler Recipt_Checklist_Revl.rtf
Page 7 of 8

Analytical Environmental Services, Inc Date: 3-Aug-15
Client: Denali Water Solutions
Project Name: Lake Kilby WTP Dates Report
Lab Order: 15071-31
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name
TCLP Date
Prep Date
Analysis Date
15071-31-001A
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
VOLATILES, TCLP Leached
07/27/2015
7/28/2015 2:38:00 PM
07/28/2015
15071-31-001B
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
TCLP SEMIVOLATILES ORGANICS
07/27/2015
7/30/2015 10:00:00AM
07/30/2015
15071-31-001B
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
HERBICIDES, TCLP Leached
07/27/2015
7/29/2015 2:00:00 PM
07/31/2015
15071-31-001B
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
MERCURY, TCLP Leached
07/27/2015
7/29/2015 10:40:00AM
07/29/2015
15071-31-001B
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
ICP METALS, TCLP Leached
07/27/2015
7/29/2015 10:44:00AM
07/29/2015
15071-31-001B
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
PESTICIDES, TCLP Leached
07/27/2015
7/29/2015 10:00:00AM
07/29/2015
15071-31-001C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
IGNITABILITY
07/28/2015
15071-31-001C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
Cyanide, Reactive
7/30/2015 10:00:00AM
07/31/2015
15071-31-001 C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
Sulfide, Reactive
7/30/2015 9:00:00 AM
07/30/2015
15071-31-001C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
POLYCHLORINATED BIPHENYLS
7/28/2015 11:00:00AM
07/28/2015
15071-31-001C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
Laboratory Hydrogen Ion (pH)
7/28/2015 10:00:00AM
07/28/2015
15071-31-001C
LAKE KILBY WTP
7/23/2015
2:30:OOPM
Sludge
PERCENT MOISTURE
07/30/2015
Page 8 of 8