NC0024911_Regional Office Physical File Scan Up To 2/23/2021 - Ash Lagoon

231 HAYWOOD STREET, ASHEVILLE, NC 28801
TEL.[phone] FAC.828.281.3351
WWW. ALTA MONT F N V IRON ANTA L.COM
Transmitted by email
[e-mail]
July 26, 2012
Mr. Dennis Lance
Metropolitan Sewerage District of Buncombe County
2225 Riverside Drive
Asheville, North Carolina 28804
Subject: Monitoring Well Repairs .
Metropolitan Sewerage District of Buncombe County
Asheville, North Carolina
Dear Mr. Lance,
Altamont Environmental, Inc. (Altamont) completed repairs to monitoring wells MW-1 R and MW-3 on the
Buncombe County Metropolitan Sewerage District (MSD) property.
Background
The North Carolina Department of Environment and Natural Resources ('DENR) recently performed a site
inspection and required MSD to perform repairs on the above mentioned monitoring wells. MSD contacted
Altamont on July 9, 2012 in order to repair the monitoring wells based upon the DENR inspection.
Monitoring Well Repairs
On July 16, 2012, Altamont stamped the well information for monitoring well MW-1R onto a new monitoring
well tag and installed the tag onto the "stick up" well casing. The well construction record for MW-1R is
included with this letter. Altamont also repaired the broken hinge on the outer "stick-up" casing for MW-3.
Please feel free to call or respond with any questions or comments related to this project.
Sincerely,
ALTAMONT ENVIRON TAL, INC.
Evan Yurkovich
Enclosures: MW-1R Well Construction Record
R\Buncombe County\MSD\Monitoring Well Surface Completion Repair\Ltr-Lance-Well Repair.Docx

NONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of) nvironment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 2054
1. WELL CONTRACTOR:
STEPHEN SLOAN
Well Contractor,(Indlvidual) Name
GEOLOGIC EXPLORATION, INC.
Well Contractor Company Name
STREET ADDRESS 176 COMMERCE BLVD
STATESVILLE NC 28625
CllyorTown State Zip Code
70( 4 )- 872-7686
Area code- Phone number
2. WELL INFORMATION:
SITE WELL ID#(itapplicable) MWAR
STATE WELL PERMIT#(irapplicable)
DWQ or OTHER PERMIT #(if applicable)
WELL USE (Check Applicable Box) Monitoring KI Munlclpal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection ❑
Irrigation❑ Other ❑ (list use)
DATE DRILLED 08/02/06
TIME COMPLETED AM ❑ PM ❑
3. WELL LOCATION:
CITY. ASHEVILLE
COUNTY BUNCOMBE
2226 RIVERSIDE DRIVE
(Street Name, Numbers, Community, Subdl ision, Lot No., Parcel, 7Jp Code)
TOPOGRAPHIC / LAND SETTING:
❑Slope ❑Valley ❑Flat ❑Ridge ❑ Other
(check appropriate box)
LATITUDE 3 _ May be in degrees,
minutes, seconds or
LONGITUDE in EL decimal format
Latitude/longitude source: ❑GPS ❑Topographic map
(location of well must be shown on a USGS topo map and
attached to this form if not using GPS)
4. FACILITY -is the name of the business where the well Is located.
FACILITY ID #(If applicable)
NAME OF FACILITY METROPOLITAN SEWAGE DISTRICT
STREET ADDRESS 2225 RIVERSIDE DRIVE
ASHEVILLE NC
City or Town Slate Zip Code
CONTACT PERSON Na.OENNSWlCEVEIM1WO IF y9EW�GE �6mICF aF eUllCd 86 CO.
MAILING ADDRESS 2225 RIVERSIDE DRIVE
ASHEVILLE NC 28804
City or Town State Zip Code
Area code - Phone number
5. WELL DETAILS:
a. TOTAL DEPTH: 14.5
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO 91
c, WATER LEVEL Below Top of Casing: 7.0 Fr.
(Use'+• if Above Top of Casing)
d. TOP OF CASING IS 2.5
FT. Above Land Surface -
'Top of casing terminated
at/or beiow, land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA
METHOD OF TEST NIA
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
From 7o
From To
From To
From Tc
From To
From To
6. CASING:
' TThickness/
Depth
Di
1lar�eter 5�g aS M1Ceriai
a
PV
From 0.0
Ft FI
From Tc
FL ­
From To
From
Ft.
7. GROUT: Depth
Material Method
From 0.0 To 2'0
Ft Portland bentonite SLURRY
From To
Ft.
From To
Ft.
8. SCREEN: Depth
Diameter Slot Size Material
From 4.5 To 14.5
FL2.0 in. .010 in, PVC
From To
Ft. In, In.
From To
Ft. in. in.
9. SAND/GRAVEL PACK:
Depth
Size Material
From 3.5 To 14.6
Ft, 2040 Fine Silica Sand
From To
Ft.
From To
Ft.
10. DRILLING LOG.
From To
0.0 5.0
5.0 6.0
11.0 12.0
12.0 14.0
14.0 14.5
Formation Description
RED/BROWN SILTY SOIL
PARTIALLY WEATHERED ROCK
GRAY MICACEOUS SILT
PARTIALLY WEATHERED ROCK
BROWN SILTY SOIL
PARTIALLY WEATHERED ROCK/MEDROCK
11. REMARKS:
Benlonite seal from 2.0 to 3.6 Feet.
I DO HEREBY CERTiFYTHAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WRH
15A NCAC WELLCONSTRUCTIONSTAN ARDS, AND THAT A COPY OF THIS
RECORD ENP VIDE E OWNER.
10 08/30/06
SIGNATUR OF CERTIFIED WELL CONTRACTOR DATE
STEPHEN SLOAN
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b
1617 Mail Service Center- Raleigh, NC 27699-1617 Phone No. [phone] ext 668. Rev. 7105

NON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 2854
1. WELL CONTRACTOR:
STEPHEN SLOAN
Well Contractor,(Individual) Name
GEOLOGIC EXPLORATION, INC.
Well Contractor Company Name
STREET ADDRESS 176 COMMERCE BLVD
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 )- 872-7686
Area code- Phone number
2, WELL INFORMATION:
SITE WELL ID #(if applicable) MW-1 R
STATE WELL PERMIT#(if applicable)
DWQ or OTHER PERMIT #(if applicable)
WELL USE (Check Applicable Box) Monitoring KI Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection ❑
Irrigation❑ Other ❑ (list use)
DATE DRILLED 08/02/06
TIME COMPLETED
AM ❑ PM ❑
3. WELL LOCATION:
CITY: ASHEVILLE
COUNTY BUNCOMBE
2225 RIVERSIDE DRIVE
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
❑Slope ❑Valley ❑Flat ❑Ridge ❑ Other
(check appropriate box)
LATITUDE 3
May be in degrees,
- ' -
minutes, seconds or
LONGITUDE
in a decimal format
Latitude/longitude source: ❑GPS ❑Topographic map
(location of well must be shown on a USGS topo map and
attached to this form if not using GPS)
4. FACILITY- Is the name of the bustness where the well is located.
FACILITY ID #(if applicable)
NAME OF FACILITY METROPOLITAN SEWAGE DISTRICT
STREET ADDRESS 2225 RIVERSIDE DRIVE
ASHEVILLE NC
City or Town Slate Zip Code
CONTACT PERSON MM DENNIS tANCEMIETROPOUTAN SEWAGE Dt.ICr OF BUNCOMBE Co.
MAILING ADDRESS 2225 RIVERSIDE DRIVE
ASHEVILLE NC 28804
City or Town State Zip Code
Area code - Phone number
5, WELL DETAILS:
a. TOTAL DEPTH: 14.5
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO KI
c. WATER LEVEL Below Top of Casing: 7.0 FT.
(Use "+" if Above Top of Casing)
d. TOP OF CASING IS 2.5
FT. Above Land Surface'
'Top of casing terminated atlor below land surface may require
a variance in accordance with 15A NCAC 2C .0118,
e. YIELD (gpm): NIA
METHOD OF TEST NIA
f. DISINFECTION: Type N/A
Amount N/A
g. WATER ZONES (depth):
From To
From To
From Tc
From To
From To
From To
6. CASING:
Thickness/
DepFrom
r�et
I�C s� 4� Material
0.0
Toot4.6
Ft.
Her
2
From
To
Ft.
From
Tc
Ft.
7. GROUT:
Depth
Material Method
From 0.0
To 2 ' 0
Ft.
Portland bentanite SLURRY
From
Tc
Ft.
From
Tc
Ft.
8. SCREEN:
Depth
Diameter
Slot Size Material
From 4.5
To 14.5
Ft.2.0 in.
.010 in, PVC
From
Tc
Ft. in.
in.
From
Tc
Ft.in.
in.
9. SANDIGRAVEL PACK:
Depth
Size
Material
From 3.5
To 14.5
Ft, 20-40
Fine Silica Sand
From
To
Ft.
From
To
Ft.
10. DRILLING LOG
From To
0.0 5.0
Formation Description
REDIBROWN SILTY SOIL
5.0 6.0
PARTIALLY WEATHERED ROCK
6.0 11.0
GRAY MICACEOUS SILT
11.0 12.0
PARTIALLY WEATHERED ROCK
12.0 14.0
BROWN SILTY SOIL
14.0 14.5
PARTIALLY WEATHERED ROCK/BEDROCK
11. REMARKS:
Bentonite seal from 2.0 to 3.5 Feet.
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15ANCAC WELLC NSTRUCTI STANQARDS,AND
THAT ACOPY OFTHIS
RECORD EN P VIDE E V 11; OWNER.
7_%0 08/30/06
SIGNATUR OF CERTIFIED WELL CONTRACTOR DATE
STEPHEN SLOAN
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b
1617 Mail Service Center- Raleigh, NC 27699-1617 Phone No. [phone] ext 568. Rev, 7/05

WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 2854
I. WELL CONTRACTOR:
STEPHEN SLOAN
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC.
Well Contractor Company Name
STREET ADDRESS 176 COMMERCE BLVD
STATESVILLE NC
City or Town Slate Zip Code
Area code - Phone number
2. WELL INFORMATION:
SITE WELL ID # (ifapplicable) MW-1
STATE WELL PERMIT tt (if applicable)
COUNTY WELL PERIIIIT#(ifapplicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use): 21 Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery ❑ InjectIon ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY BUNCOMBE QUADRANGLE NAME
NEARESTTOWN: ASHEVILLE
2225 RIVERSIDE DRIVE
(Skeet/Road Name, Number, Community, Subdivision, Lot No., Parcel. Zip Code)
TOPOGRAPHIC / LAND SETTING:
❑ Slope' ❑ Valley ❑ Flat [-]Ridge[-] Other
(Check appropriate setting)
LATITUDE May be in degrees,
mhrules, seconds, or in a
LONGITUDE decimal format
Latitude/longitude source: ❑ GPS ❑ Topographic map
(Location of hell mast be shotrn on a USGS topo Wrap and
attached to this form ifnor using GPS.)
4a. FACILITY- The name of the business where the well is locnted. Complete 4a and4b.
(If a residential well, slip 4a: complete 4b, well owner information only.)
FACILITY ID #(ifapplicable)
NAME OF FACILITY METROPOLITAN SEWAGE DISTRICT
SIREETADDREss 2225 RIVERSIDE DRIVE
ASHEVILLE NC 28804
City or Town State Zip Code
4b. CONTACT PERSONAVELL OWNER:
NAME DENNIS LANCEIMErROPOLITAN SEWAGE DISTRICT OF BUNCOMBE CO.
STREET ADDRESS 2225 RIVERSIDE DRIVE ASHEVILLE, NC
5. WELL DETAILS:
a. Total Depth: 14.0 ft. Diameter:2•0 in.
b. Water Level (Below Measuring Point): ft.
Measuring point is it. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
b. Casing Removed: N/A ft. in.
7. DISINFECTION: N/A
(Amount of 659/o-75% calcium hypochlorile used)
8. SEALING MATERIAL:
Nent Cement Sand Cement
Cement '" lb. Cement-- lb.
Water— gal, Water"" gal.
Bentonite
Bentonile lb.
Type: ©Slurry ❑Pellets
Water gal.
Other
Type material PORTLAND BENTONITE SLURRY
Amount 2.8 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF NiATERLkL:
VIA TREMIE PIPE
10. WELL DIAGRAM: Draw a detailed sketch of the well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations. and depths and
types of fill materials used.
11. DATE WELL ABANDONED 8/2/06
1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF
THIS RECWD HAS
`BEEN
�PROVIDED TO THE WELL OWNER. ` 1
SIGNATUREFJF CERTIFIED WELL CONTRACTOR I DATE
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(Tire private well owner must be nn individual who aqsonnilyabandons hiseher residential well
in accordance with 15A NCAC 2C .0113.)
STEPHEN SLOAN
PRINTED NAME OF PERSON ABANDONING THE WELL
Submit a copy to the owner and the original to the Division of Water Quality within 30 days. Form GW-30
Attn: Information Management,1617 Mail Service Center — Raleigh, NC 27699-1617, Phone No. [phone] ext 568. Rev. 5/06

County:
BUNCOMBE
Sample ID:
AB64904
River Basin
a0F WA94
G�
PO Number #
10G0740
Report To
AROAP
r
Date Received:
10/26/2010
Collector:
J STEPP
Time Received:
08:30
p
Labworks LoginlD
SMATHIS
Region:
ARO
Report Generated:
11/12/10
Sample Matrix:
GROUNDWATER
D ate Reported:
12/29/2011
Loc. Type:
MONITORING WELL
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: BUNCOMBE COUNTY MSD
Location ID:
BUMSD2R
Collect Date: 1012112010
Collect Time: 12:17
Sample Depth
CAS # Analyte Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
LAB
Sample temperature at receipt by lab
0.4
°C
10/26/10
SMATHIS
MET
7440-22-4
Ag by ICPMS
5.0
5.0 U Q1
ug/L
EPA200.8
11/2110
ESTAFFORDI
7440-38-2
As by ICPMS
2.0
2.0 U Q1
ug/L
EPA200.8
11/2110
ESTAFFORDI
7440-38-3
Ba by ICP
10
51 Q1
ug/L
EPA200.7
10/28/10
ESTAFFORDI
7440-47-3
Cr by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L
EPA245.1
11/4/10 -
ESTAFFORDI
7439-92-1
Pb by ICPMS
10
10 U Q1
ug/L
EPA200.8
1112/10
ESTAFFORDI
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to hSp:U oortai.nwenr.ora/weblw - mb wftngo/pou,�s �,tpnut' QualfHer CodcS <htP paLaLQcdq rio,�q[w b Iabf,�,E7fl.LL4iESh.7rist>
Page 1 of 1

qVC
(DWO Laboratory, Section
Results
County:
BUNCOMBE
Sample ID:
AB64780
River Basin
10F W ATF9Q
PO Number #
ARO
Report To
AROAP
Date Received:
10121/2010
v� Y
Collector:
J STEPP
r
Time Received:
13:20
Region:
ARID
p
Labworks LoginlD
KJIMISON
Sample Matrix:
GROUNDWATER
Report Generated:
11/29/10
Loc. Type:
MONITORING WELL
D ate Reported:
12/29/2011
Emergency Yes/No VisitlD
CDC Yes/No
Loc. Descr.: MSD MW-2R
Location ID: BUMSD211 Collect Date: 10/21/2010 Collect Time: 12:36 Sample Depth
CAS # Analvte Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
Others
Sample temperature at receipt by lab 3.1 °C 10/21/10 SMATHIS
Coliform, MF Fecal in liquid 1 1 B2 CFU/100ml APHA9222D-20th 10/21/10 CGREEN
Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone]
For a detailed description of the qualifier codes referto hto:/!°ortaLnw°nr.orR/webl�w/ia.bL�S?B!!ftleccn_s_i,.tgo�t O,qa„IjHg,LodgS <htu:U uortaLncdenGo web/wC/lab/rtaRnNo/techassisb
Page 1 of 1

,,;;: , . --
County:
BUNCOMBE
Sample ID:
AB64901
River Basin
Report
�pF WATFAQ
PO Number#
10G0737
To
AROAP
r
Date Received:
10/26/2010
Collector:
J STEPP
j
Time Received:
08:30
p
Labworks LoginlD
SMATHIS
Region:
ARO
Report Generated:
11/12/10
Sample Matrix:
GROUNDWATER
D ate Reported:
12/29/2011
Loc. Type:
MONITORING WELL
Emergency Yes/No VisitlD
COC Yes/No
Loc. Descr.: BUNCOMBE COUNTY MSD
Location ID: BUMSDIR Collect Date: 10/2112010 Collect Time: 11:35 Sample Depth
CAS # Analvte Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
LAB
Sample temperature at receipt by lab 0.4 °C 10/26/10 SMATHIS
MET
7440-22-4
Ag by ICPMS
5.0
5.0 U Q1
ug/L
EPA200.8
1112/10
ESTAFFORD1
7440-38-2
As by furnace
2.0
2.0 U,Q1
ug/L
EPA200.9
10/29/10
ESTAFFORDI
7440-38-3
Ba by ICP
10
160 Q1
ug/L
EPA200.7
10/28/10
ESTAFFORD1
7440-47-3
Cr by ICPMS
10
15 Q1
ug/L
EPA200.8
11/2110
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L
EPA245.1
11/4/10
ESTAFFORDI
7439-92-1
Pb by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to nm:// oorcai went.ora/weh/ ,n ry1.o/eea,assistaoauai xe eo os <ht aorcaLncdengorxLwen(�:.fl[yab(sim,erNo/techas,lst>
Page 1 of 1

County:
BUNCOMBE
Sample ID:
AB64777
River Basin
�0F WArF9Q
PO Number#
ARO
Report To
AROAP
Date Received:
10121/2010
Collector:
J STEPP
Time Received:
13:20
p
Labworks LoginlD
KJIMISON
Region:
ARO
Sample Matrix:
GROUNDWATER
Report Generated:
11/29/10
D ate Reported:
12/29/2011
Loc. Type:
MONITORING WELL
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD MW-1 R
Location ID:
BUMSDIR
Collect Date: 1012112010
Collect Time: 11:35
Sample Depth —::2
Result/
Method
Analysis
CAS # Analvte Name PQL
Units
Validated by
Qualifier
Reference
Date
Others
Sample temperature at receipt by lab
3.1
°C
10/21/10
SMATHIS
Collform, MF Fecal in liquid 1
7
CFU/100ml APHA9222D-20th
10/21/1.0
CGREEN
Residue —Suspended In liquid 6.2
974
mg/L APHA2540D-20th
10/27/10
CGREEN
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to;[/P.oLtai..aS.G_s,,oreJweb,LuAab/staFlnfloRecna .pp2t. Oyariner caa�, �_[(�onai,�cee�..orpf,rvsb[�ygQabJ},�jflnM1o/techassLt>
Page 1 of 1

.�W, .. .-
-WC (DWO Laboratory Section Results
County: BUNCOMBE
Sample ID:
AB64902
River Basin
PO Number#
10G0738
Report To AROAP
�(AVATF19G3
T-
Date Received:
10126/2010
r0
r
Collector: J STEPP
j
�
Time Received:
08:30
Region: ARID
P
Labworks LoginlD
SMATHIS
Sample Matrix: GROUNDWATER
Report Generated:
11/12/10
Loc. Type: MONITORING WELL
D ate Reported:
12/29/2011
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: BUNCOMBE COUNTY MSD
Location ID: BUMSD3 Collect Date: 10I2112010 Collect Time: 11.58 Sample Depth
CAS # Analyte Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
LAB
Sample temperature at receipt by lab 0.4 °C 10/26/10 SMATHIS
MET
7440-22-4
Ag by ICPMS
5.0
5.0 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
7440-38-2
As by ICPMS
2.0
2.0 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
7440-38-3
Ba by ICP
10
75 Q1
ug/L
EPA200.7
10/28/10
ESTAFFORDI
7440-47-3
Cr by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L
EPA245.1
11/4/10
ESTAFFORD1
7439-92-1
Pb by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Fore detailed tlescrip0on of the qualifier codes referto nt°:// oortalnmencora✓web/wnnae/staenFlo/temavrtaoaoa oua.iine..r._4aaq, <htp;jj p.,9 ncd�4ssxLwec�yyy/ia¢�:h,,flnN 1ie�n„hssa
Page 1 of 1

County:
BUNCOMBE
Sample ID:
AB64778
River Basin
OF WATF9
Q�
PO Number #
ARO
Report To
AROAP
�O�
r
Date Received:
10/21/2010
Collector:
J STEPP
P
Time Received:
13:20
Labworks LoginlD
KJIMISON
Region:
ARO
Report Generated:
11/29/10
Sample Matrix:
GROUNDWATER
Date Reported:
12/29/2011
Loc. Type:
MONITORING WELL
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD MW-3
Location ID:
BUMSD3
Collect Date: 10121/2010
Collect Time: 11:56
Sample Depth
CAS # Analyte Name PQL Result/ Units Method Analysis Validated by
Qualifier Reference Date
Others
Sample temperature at receipt by lab 3.1 °C 10/21/10 SMATHIS
Coliform, MF Fecal in liquid 1 152 CFU/100ml APHA92220-20th 10/21/10 CGREEN
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed daSCfiplfo0 of qualifier codes fatal to ht :// oona�.�wencorq(y;eb,�wg l/�,.p •wen' feemas,�staoata nva�ine„r_cgde, <.htp:[L{g,�9i„nc_d, enr.o_rpj vy�eb[�v lac tan No tShay^,,jsT;
Page 1 of 1

County:
BUNCOMBE
Sample ID:
AB64903
River Basin
�0F \NAgp
PO Number #
10G0739
Report To
AROAP
�fl
r-
Date Received:
10126/2010
Collector:
J STEPP
P Y
Time Received:
08:30
Labworks LoginlD
SMATHIS
Region:
ARO
Report Generated:
11/12/10
Sample Matrix:
GROUNDWATER
Date Reported:
12/29/2011
Loc. Type:
MONITORING WELL
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: BUNCOMBE COUNTY MSD
Location ID: BUMSD4 Collect Date: 10/21/2010 Collect Time: 12:17 Sample Depth
CAS # Analyte Name
LAB
PQL Result/ Method Analysis
Qualifier Units Reference Date Validated by
Sample temperature at receipt by lab
0.4
°C
10/26/10
SMATHIS
MET
7440-22-4
Ag by ICPMS
5.0
5.0 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORDI
7440-38-2
As by furnace
2.0
2.0 U,Q1
ug/L
EPA200.9
10/29/10
ESTAFFORD1
7440-38-3
Ba by ICP
10
92 Q1
ug/L
EPA200.7
10/28/10
ESTAFFORD1
7440-47-3
Cr by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2110
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L
EPA245.1
11/4/10
ESTAFFORD1
7439-92-1
Pb by ICPMS
10
10 U Q1
ug/L
EPA200.8
11/2/10
ESTAFFORD1
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to htp;// portal�gwen(:.orpj;/.9.p� dab stLf nfiojjy+cf,nf.f_iM[)uta Qu; liner Codes <htp,;([porta1.ncdeor.ora/w.b[ �I b(staHPN..L[echas:J�t�
Page 1 of 1

County:
BUNCOMBE
River Basin
Report To
AROAP
Collector:
J STEPP
Region:
ARO
Sample Matrix:
GROUNDWATER
Lac. Type:
MONITORING WELL
Emergency Yes/No VisitlD
COC Yes/No
Sample ID:
AB64779
pF wATFQ
Q1
PO Number#
ARO
.�a
Date Received:
10121/2010
Time Received:
13:20
P Y
Labworks LoginlD
KJIMISON
Report Generated:
11/29/10
Date Reported:
12/29/2011
Loc. Descr.: MSD MW-4
Location ID: BUMSD4
Collect Date:
10/21/2010
Collect Time: 12:17
Sample Depth
Result/
Method
Analysis
CAS # Analvte Name PQL
Units
Validated by
Qualifier
Reference
Date
Others
Sample temperature at receipt by lab
3.1
°C
10/21/10 SMATHIS
Conform, MF Fecal in liquid 1
1 B2
CFU/100ml APHA9222D-20th
10/21/10 CGREEN
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Fora detailed description of the qualifier codes refer to hto'// mnal.nwen,.org/webhm/lab/staflnf,Lt-th,slst#Data Qualiaer codes<hto:// Donal.ncdenr.ora/weblwanab/seaneohechassist
Page 1 of 1

ROY COOPER
Govervtor
MICHAEL S. REGAN
NCB....� &e retai y
Water Resources S. JAY ZIMME.RMAN
Gnvironmentai Quality Direclor
August 15, 2017
Peter Weed, Director
Treatment and Maintenance Division
Metropolitan Sewerage District of Buncombe County
2028 Riverside Drive
Asheville, North Carolina 28804
Subject: Compliance Evaluation Inspection and GW59 Review
N PDES Permit No. WQB&29Ht n c,_,, a4 2 l\
Metropolitan Sewerage District
Buncombe County, NC
Dear Mr. Weed,
On June 13, 2017, 1 accompanied Mark Swan of Pace Analytical as he collected water samples from
four groundwater monitoring wells associated with the 17-acre incinerator ash basin located off
Riverside Drive in Buncombe County. The intent of the site inspection was to evaluate the sampling
methods and well performance as well as the collection of subsequent split samples. The State's
water samples were analyzed by the Division of Water Resources (DWR) analytical laboratory. A
copy of the analytical results is attached to this letter.
Pace Analytical is currently using a HDPE bailer to purge water from the wells and collect
groundwater samples. A common problem with bailers is they tend to produce turbulence within
the well casing, which can lead to the resuspension of accumulated sediments. Turbidity samples
collected during the June 2017 sampling event indicate excessive suspended sediment at three of
the four monitoring wells. Turbidity concentrations at monitoring wells MW1R, MW2R, MW3, and
MW4 were 1000 NTU, 5.2 NTU, 400 NTU, and 85 NTU respectively.
The presence of excess suspended sediments is problematic, particularly for samples destined for
metals analysis,'because it becomes difficult to differentiate between sediments attributable to
formation materials and the more mobile constituents, which are subject to federal and state
groundwater standards. Therefore, DWR has developed a policy that addresses the preparation of
groundwater samples for metals analysis. A copy of the Metals Determination policy is attached to
this letter.
You will be required to implement a low -flow sampling technique to ensure the turbidity
concentrations are less than 10 NTUs at the time of sampling. It is important to note that low -flow
sampling does not require a specific flow rate or purge volume. -Low -flow sampling utilizes an
adjustable rate pump (E.g. peristaltic pump) with typical flow rates on the order of OA -- 0.5 L/min.
State of North Carolina I Environmental Quality I Water Resources
2090 U.S.1•.lighway 70, Swannanoa, North Carolina 28778
828-296-4500

Peter Weed
August 15, 2017
Page 2 of 2
Water level, field, parameters (E.g. temperature, pH, specific conductivity, dissolved oxygen, &
oxidation reduction potential), and turbidity are all-measured.simultaneously. A groundwater
sample is typically collected after the field parameters and water level have stabilized and the
turbidity concentration is below 10 NTUs. Please implement these changes to your groundwater
monitoring program as soon as possible.
It is important to note that during the June 13, 2017 sampling event there was an exceedance of the
groundwater standard (15A NCAC 02L .0202) for ammonia at monitoring well MW4. The DWR
analytical results noted additional exceedances of the applicable groundwater standards for the
following constituents: chromium, iron, lead, manganese, and vanadium.
DWR will not be taking any immediate action regarding the exceedance of the applicable
groundwater standards for ammonia and various metals. As you may be aware, the Asheville
Regional Office (ARO) believes the current monitoring well network is located withih .your
compliance boundary, which is defined as 500 feet from the waste boundary or at the property
boundary, whichever is closer to the source. The waste boundary for your facility not only includes
the ash basin but the wastewater treatment works as well. Therefore, the ARO is recommending
that a new monitoring well network be established on the appropriate regulatory boundary as a
part of your NPDES permit renewal.
One of the difficulties in establishing a compliance boundary for your Riverside Drive facility is
knowing the location of your western property boundary. The Buncombe County Geographic
Information Systems (GIS) website shows your property boundary on the east -side of Riverside
Drive. Your staff have indicated the western property boundary resides in the middle of the French
Broad River. Please provide documentation such as a deed or land survey that clearly identifies
the location of your western property boundary.
Please feel free to contact me if you have additional questions or concerns. I can be reached at
[phone] or [e-mail].
Sincerely,
Brett Lavert
Water Quality Regional Operations
Asheville Regional Office
Attachment: DWR laboratory analytical results
Metals Determination Policy Memo dated May 13, 2013
Low -flow sampling of Water Quality Parameters Used In Determining Groundwater Stability
cc: ARO File-

AC39775 North Carolina D;-»-;.on of Water Resources Water Scien^-c Section Laboratory Results
...
-I
Loc. Descr.: ,
Metroaelitan Sewage District 2028 Ri.,, -Je Dr Asheville, NC
County:
BUNCOMBE Collector:
B LAVERTY
VisitlD
MW1
Region:
ARO Report To
ARO
Location ID:
1P11MSDMW1
River Basin
Collect Date:
06/13/2017
Priority
COMPLIANCE
Emergency
Collect Time:
11_48
Sample Matrix:
GROUNDWATER
COC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
rinal Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # Analyte Name PQL Qualifier Reference Date
LAB
Sample temperature at receipt by lab 1.1 °C 6115/17
Validated by
MSWIFT
NH3 as N in liquid
0.02
NUT
0.02 U
mg/L as N
EPA350.1 REV 2
6/15/17
CGREEN
NO2+NO3 as N in liquid
0.02
0.02 U
mg/L as N
EPA353.2 REV 2
6116/17
CGREEN
Phosphorus -total as P in liquid
0.02
0.21
mg/Las P
EPA365.1 REV 2
6/22117
CGREEN
Total Kjeldahl N as N in liquid
0.2
0.26
mg/Las N
EPA351.2 REV
6/21/17
CGREEN
7440-22-4
Ag by furnace
1.0
MET
1.0 U, J2
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORD1
7429-90-5
Al by ICP
50
42000
ug/L
EPA200.7 Rev4.4
6/30/17
ESTAFFORD1
7440-36-0
Antimony by ICPMS
10
IOU
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-38-2
As by furnace
2.0
2.0 U
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORD1
7440-38-3
Ba by ICP
10
290
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-41-7
Be by ICP
5.0
5.0 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-70-2
Ca by ICP
0.10
7.3
mg/L
EPA200.7 Rev4.4
6129/17
ESTAFFORD1
744043-9
Cd by furnace
0.50
0.50 U
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORD1
7440484
Cobalt by ICP
50
50 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
744047-3
Cr by ICP
5.0
18
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-50-8
Cu by ICPMS
2.0
15
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7439-89-6
Fe by ICP
50
26000
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U, Q2
ug/L
EPA245.1 Rev3
7/14/17
ESTAFFORD1
7440-09-7
K by ICP
0.10
7.1
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7439-93-2
Li ICP
25
25 U
ug/L
EPA200.7 Rev4.4
7113/17
ESTAFFORD1
7439-95-4
Mg by ICP
0.10
8.8
mg/L
EPA200.7 Rev4A
6/29/17
ESTAFFORD1
7439-96-5
Mn by ICP
10
1100
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7439-98-7
Mo by ICPMS
10
IOU
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-23-5
Na by ICP
0.10
4.0
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-02-0
Ni by ICPMS
2.0
12
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7439-92-1
Pb by ICPMS
2.0
20
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7782-49-2
Se by furnace
1.0
1.0 U
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORD1
7440-24-6
Sr by ICPMS
10
100 P
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-28-0
Thallium (TI) ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-62-2
V by ICP
10
27
ug/L
EPA200.7 Rev4.4
7/13/17
ESTAFFORD1
7440-66-6
Zn by ICPMS
10
67
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL
Page 1 of 3

%C DVAk L-a^—torySection Resufts/Sampfe Comments/Quafifier(D-4 *.ions
pie ID: AC39775 s
CAS.# Analyte Name PQL Result/ Method Analysis
Qualifier Units Reference Date Validated by
Sample Comments
MET: Ag-J2, estimated- LFB failed to meet QC criteria (72.4%)
MET: Hg=Q2-Estimated; Holding Time exceeded following receipt by lab
due to instrument issues.
NCDEQ-WSS-Chemistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "U". The PQL is used for the qualified result(S) to call
B1 Coliform-Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters repor
B2 Coliform-Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform-Countable membranes with more than 60 or 80 colonies. The value reported is calculated using the count from the smalle:
B4 Coliform-Filters have counts of both >60 or 80 and <20. Reported value is estimated or is a total of the counts on all filters reported
B5 Coliform-Too many colonies were present; too numerous to count (TNTC). TNTC is generally defined as >150 colonies.
B6 Col iform-Esti mated Value. Blank contamination evident.
B7 Coliform-Many non-coliform or non-enterococcus colonies or interfering non-coliform or non-enterococcus growth present. In this cc
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than "<" valu,
BB2 MPN-All wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD-The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
G2 BOD-The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea!
G3 BOD-No sample dilution met the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at least 1.0 mg/L.
G4 BOD-Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration de
G5 BOD-The glucose/ glutamic acid standard exceeded the range of 198 ± 30.5 mg/L.
G6 BOD-The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.
G7 BOD-Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated foi
G8 BOD-Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated for
G9 BOD-The DO depletion of the dilution water blank produced a negative value.
J1 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 2 of 3

.NC D`W P f-oboratory Section li�psufts/Sampfe Comments/Quaff,�r finitions
Sample ID: AC39775
CAS # Analyte Name PQL Result/ Method Analysis
Qualifier Units Reference Date Validated by
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, pl
J5 Temperature limits exceeded (samples frozen or >6°C) during transport or not verifiable (e.g., no temperature blank provided): non-
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
R This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrument/method. Th
A Temperature limits exceeded (samples frozen or >6°C) during storage, the data may not be accurate.
J9 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
J11 The reported value is determined by a one -point estimation rather than against a.regression equation. The estimated concentration
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are "out of control". The sample is non -homogenous (e.g., VOA soil). The reported value is the lower 1,
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence of s
N3 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N4 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holding time exceeded prior to receipt by lab.
Q2 Holding time exceeded following receipt by lab.
P Elevated PQL* due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit*. The number value repot
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed -field error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s'
Y Elevated PQL* due to insufficient sample size.
Z1 Inability to analyze the sample.
Z2 Questions concerning data reliability.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or " Ll" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 3of3

AC39866 North Carolina D----ion of Water Resources Water Scier. o- Section Laboratory Results
Loc. Descr.: METROPOLITAN SEWERAGE DISTRi%, i t.J28 RIVERSIDE DR
County: BUNCOMBE
Collector:
B LAVERTY
VisitlD
MW1
Region: ARO
Report To
ARO
Location ID:
1P11MSDMW1
River Basin
Collect Date:
06113/2017
Priority
COMPLIANCE
Emergency
Collect Time:
11_48
Sample Matrix:
GROUNDWATER
COC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39866
PO Number#
ARO
Date Received:
06114/2017
Time Received:
10_50
Labworks LoginlD
KJIMISON2
Delivery Method
Hand Delivered
Final Report Date:
7/25/17
Report Print Date:
08/11/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # AnalVte Name PQL Qualifier Reference Date Validated by
ARO
Sample temperature at receipt by lab 4.1 °C 6/14/17 RBYRD
Turbidity 1 1000 J7 NTU SM 2130 B-2001 6/14/17 ESTAFFORDI
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC39773 North Carolina D,,»-;.on of Water Resources Water Scien(--- Section Laboratory Results
Loc. Descr.: I Metropolitan Sewage District2028 Rie Dr Asheville. NC
County: Buncombe
Collector:
B LAVERTY
VisitlD
MW2R
Region: ARO
Report To
ARO
Location ID:
1P11MSDMW2R
River Basin
Collect Date:
06/13/2017
Priority
COMPLIANCE
Emergency
Collect Time:
11_02
Sample Matrix:
GROUNDWATER
COC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39773
PO Number#
Date Received:
06/15/2017
Time Received:
08:15
Labworks Loginib
TASCENZO1 .
Delivery Method
NC Courier
Final Report Date:
7/28/17
Report Print Date:
08/11/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # Analyte Name PQL Qualifier Reference Date
LAB
Sample temperature at receipt by lab 1.1 °C 6/15/17
Validated by
MSWIFT
NH3 as N in liquid
0.02
NUT
0.02 U,J3
mg/Las N
EPA350.1 REV
6/15/17
CGREEN
NO2+NO3 as N in liquid
0.02
3.6
mg/L as N
EPA353.2 REV 2
6/16/17
CGREEN
Phosphorus -total as P in liquid
0.02
0.02
mg/L as P
EPA365.1 REV 2
6/22/17
CGREEN
Total Kjeldahl N as N in liquid
0.2
0.20 U
mg/L as N
EPA351.2 REV 2
6/21/17
CGREEN
7440-22-4
Ag by ICPMS
1.0
MET
1.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7429-90-5
All by ICP
50
50 U
ug/L
EPA2001.7 Rev4.4
6/29117
ESTAFFORD1
7440-36-0
Antimony by ICPMS
10
10 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-38-2
As by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-38-3
Ba by ICP
10
63
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-41-7
Be by ICP
5.0
5.0 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-70-2
Ca by ICP
'0.10
39
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-43-9
Cd by ICPMS
0.50
0.50 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-48-4
Cobalt by ICP
50
50 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-47-3
Cr by ICPMS
5.0
5.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-50-8
Cu by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7439-89-6
Fe by ICP
50
50 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-97-6
Hg 245.1
0.2
0.20 U, Q2
ug/L
EPA245.1 Rev3
7/14/17
ESTAFFORDI
7440-09-7
K by ICP
0.10
9.5
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-93-2
Li ICP
25
25 U
ug/L
EPA200.7 Rev4.4
7/13/17
ESTAFFORD1
7439-95-4
Mg by ICP
0.10
11
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7439-96-5
Mn by ICP
10
300
ug/L
EPA200.7 Rev4.4
6/29117
ESTAFFORDI
7439-98-7
Mo by ICPMS
10
10 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-23-5
Na by ICP
0.10
15
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-02-0
Ni by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7439-92-1
Pb by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7782-49-2
Se by ICPMS
1.0
1.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-24-6
Sr by ICPMS
10
160
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-28-0
Thallium (TI) ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-62-2
V by ICP
10
.10 U
ug/L
EPA200.7 Rev4.4
7/13/17
ESTAFFORDI
7440-66-6
Zn by ICPMS
10
10, U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 3

NC (Dl, C - ztory Section WSsufts/Sampfe Comments/QuaCfier D-", tions
iple ID: AC39773
Result/ Method Analysis
ld'1J tt I-X1101Y10 IV01110
UT NH3-J3-Estimated; LFM recovery was 84% due to matrix interference.
ET: Hg-Q2-Estimated; Holding Time exceeded following receipt by lab
due to instrument issues.
Qualifier Units Reference Date Validated by
Sample Comments
NCDECIMSS-Chemistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "U". The PQL is used for the qualified result(S) to call
B1 Coliform-Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters repor
B2 Coliform-Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform-Countable membranes with more than 60 or 80 colonies. The value reported is calculated using the count from the smaller
B4 Coliform-Filters have counts of both >60 or 80 and <20. Reported value is estimated or is a total of the counts on all filters reported
B5 Coliform-Too many colonies were present; too numerous to count (TNTC). TNTC is generally defined as >150 colonies.
B6 Coliform-Estimated Value. Blank contamination evident.
B7 Coliform-Many non-coliform or non-enterococcus colonies or interfering non-coliform or rion-enterococcus growth present. In this cc
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than "<" valu
BB2 MPN-All wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD-The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
G2 BOD-The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea!
G3 BOD-No sample dilution met the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at least 1.0 mg/L.
G4 BOD-Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration dE
G5 BOD-The glucose/ glutamic acid standard exceeded the range of 198 ± 30.5 mg/L.
G6 BOD-The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.
G7 BOD-Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated foi
G8 BOD-Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated for
G9 BOD-The DO depletion of the dilution water blank produced a negative value.
J1 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 2 of 3

NCO" r-6oratory Section 9?§sults/SampfeComments/Quafifr-''°'-,finitions
Sample ID: AC39773
CAS # Analyte Name PQL Result/ Method AnalVsls
Qualifier Units Reference Date Validated by
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, pl
J5 Temperature limits exceeded (samples frozen or >6'C) during transport or not verifiable (e.g., no temperature blank provided): non-
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
J7 This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrument/method. Th
A Temperature limits exceeded (samples frozen or >6°C) during storage, the data may not be accurate.
A The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
J11 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are "out of control'. The sample is non -homogenous (e.g., VOA soil). The reported value is the lower 1
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence of a
N3 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N4 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holding time exceeded prior to receipt by lab.
Q2 Holding time exceeded following receipt by lab.
P Elevated PQL* due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit*. The number value repot
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed -field error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s
Y Elevated PQL* due to insufficient sample size.
Z1 Inability to analyze the sample.
Z2 Questions concerning data reliability.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 3 of 3

AC39864 North Carolina D---ion of Water Resources Water Scien--- Section Laboratory Results
Loc. Descr.: I
METROPOLITAN SEWERAGE DISTR
_ )28 RIVERSIDE DR - MW2R
County:
Buncombe Collector:
B LAVERTY
VisitlD
Region:
ARO Report To
ARO
Location ID:
1P11MSDMW2R
River Basin
Collect Date:
06/13/2017
Priority
COMPLIANCE
Emergency
Collect Time:
11_02
Sample Matrix:
GROUNDWATER
COC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39864
PO Number#
ARO
Date Received:
06/14/2017
Time Received:
10_50
Labworks LoginlD
' KJIMISON2
Delivery Method
Hand Delivered
Final Report Date:
6128/17
Report Print Date:
08/11/2017
If this report is labeled preliminary.report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Method Analysis
CAS # Analyte Name PQL Qualifier Units Reference Date Validated by
ARO
Sample temperature at receipt by lab 4.1 °C 6/14/17 RBYRD
Turbidity 1 5.2 NTU SM 2130 B-2001 6114/17 ESTAFFORD1
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC39774 North Carolina D--ion of Water Resources Water Scien--^ Section Laboratory Results
Loc. Descr'.`. . Mthr000litan Sewaoe District 2028 Ri._.v.Je Or Asheville. NC
County: Buncombe
Collector:
B LAVERTY
VisitlD
MW3
Region: ARO
Report To
ARO
Location ID:
1P11MSDMW3
River Basin
Collect Date:
06/13/2017
Priority
COMPLIANCE
Emergency
Collect Time:
11_28
Sample Matrix:
GROUNDWATER
COC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39774
PO Number#
Date Received:
0611512017
Time Received:
08_15
Labworks LoginlD
TASCENZOI
Delivery Method
NC Courier
Final Report Date:
7/281l7
Report Print Date:
08/11/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # Analyte Name PQL Qualifier Reference Date
LAB
Sample temperature at receipt by lab 1.1 °C 6/15/17
Validated by
MSWIFT
NH3 as N in liquid
0.02
NUT
0.02 U
mg/Las N
EPA350.1 REV 2
6/15/17
CGREEN
NO2+NO3 as N in liquid
0.02
4.0
mg/L as N
EPA 353.2 REV 2
6116/17
CGREEN
Phosphorus total as P in liquid
0.02
0.26
mg/L as P
EPA 365.1 REV 2
6/22/17
CGREEN
Total Kjeldahl N as N in liquid
0.2
0.20 U
mg/L as N
EPA 351.2 REV 2
6/21/17
CGREEN
7440-22-4
Ag by furnace
1.0
MET
1.0 U, J2
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORDI
7429-90-5
Al by ICP
50
16000
ug/L
EPA200.7 Rev4.4
6129/17
ESTAFFORD1
7440-36-0
Antimony by ICPMS
10
20P
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-38-2
As by furnace
2.0
2.0 U
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORDI
7440-38-3
Ba by ICP
10
380
ug/L
EPA200.7 Rev4.4
6129/17
ESTAFFORDI
7440-41-7
Be by ICP
5.0'
5.0 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-70-2
Ca by ICP
0.10
3.7
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-43-9
Cd by furnace
0.50
0.50 U
ug/L
EPA200.9 Rev2.2
7110/17
ESTAFFORDI
7440-48-4
Cobalt by ICP
50
50 U
ug/L
EPA200.7 Rev4A
6/29/17
ESTAFFORDI
7440-47-3
Cr by ICP
5.0
27
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-50-8
Cu by furnace
2.0
4.8
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORDI
7439-89-6
Fe by ICP
50
21000
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U, Q2
ug/L
EPA245.1 Rev3
7/14/17
ESTAFFORDI
7440-09-7
K by ICP
0A0
9.2
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDY
7439-93-2
Li ICP
25
25 U
ug/L
EPA200.7 Rev4A
7/13/17
ESTAFFORDI
7439-95-4
Mg by ICP
0.10
7.9
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-96-5
Mn by ICP
10
320
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-98-7
Mo by ICPMS
10
20 P
ug/L
EPA200.8 Rev5A
6/29/17
ESTAFFORD1
7440-23-5
Na by ICP
0.10
3.4
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-02-0
Ni by ICPMS
2.0
10
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7439-92-1
Pb by furnace
2.0
8.2
ug/L
EPA200.9 Rev2.2
7/14/17
ESTAFFORDI
7782-49-2
Se by furnace
1.0
1.0 U
ug/L
EPA200.9 Rev2.2
7/10/17
ESTAFFORDI
7440-24-6
Sr by ICPMS
10
-130
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-28-0
Thallium (TI) ICPMS
2.0
4.0 P
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-62-2
V by ICP
10
36
ug/L
EPA200.7 Rev4.4
7/13/17
ESTAFFORD1
7440-66-6
Zn by ICPMS
10
83
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL
Page 1 of 3

.NCDVA , t -`--storySection Q�sufts/Sampfe Comm ents/Qua[zfwr4'-L 'tions
iple ID: AC39774
CAS # Analyte Name PQL FKesuly Method Analysis
Qualifier Units Reference Date Validated by
Sample Comments
MET: Ag-J2, estimated-LFB failed to meet QC criteria (72.4%)
MET: Hg-Q2-Estimated; Holding Time exceeded following receipt by lab
due to instrument issues.
MET: Mo, Sb & TI - P - Elevated PQL- Matrix interference.
NCDEQ-WSS-Chemistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "U". The PQL is used for the qualified result(S) to call
B1 Coliform-Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters repor
B2 Coliform-Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform-Countable membranes with more than 60 or 80 colonies. The value reported is calculated using the count from the smalle:
B4 Coliform-Filters have counts of both >60 or 80 and <20. Reported value is estimated or is a total of the counts on all filters reported
B5 Coliform-Too many colonies were present; too numerous to count (TNTC). TNTC is generally defined as >150 colonies.
B6 Coliform-Estimated Value. Blank contamination evident.
B7 Coliform-Many non-coliform or non-enterococcus colonies or interfering non-coliform or non-enterococcus growth present. In this cc
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than "<" valu.
BB2 MPN-All wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD-The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
G2 BOD-The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea!
G3 BOD-No sample dilution met the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at least 1.0 mg/L.
G4 BOD-Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration de
G5 BOD-The glucose/ glutamic acid standard exceeded the range of 198 ± 30.5 mg/L.
G6 BOD-The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.
G7 BOD-Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated fol
G8 BOD-Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated for
G9 BOD-The DO depletion of the dilution water blank produced a negative value.
J1 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 2 of 3

.NC DW, - 5oratory Section 9?ssurts/Sampre Comments/Qualifi, "'-finitions
Sample ID: AC39774
Result/ Method Analysis
ugairrier units Kererence uaie vauoaiea Dy
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, pl
J5 Temperature limits exceeded (samples frozen or >6°C) during transport or not verifiable (e.g., no temperature blank provided): non-
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
R This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrument/method. Th
A Temperature limits exceeded (samples frozen or >6°C) during storage, the data may not be accurate.
A The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
J11 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are 'but of control'. The sample is non -homogenous (e.g., VOA soil). The reported value is the lower i
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence of e
N3 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N4 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holding time exceeded prior to receipt by lab.
Q2 Holding time exceeded following receipt by lab.
P Elevated PQL* due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit*. The number value repot
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed -field error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s
Y Elevated PQL* due to insufficient sample size.
Z1 Inability to analyze the sample.
Z2 Questions concerning data reliability.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 3 of 3

AC39865
Loc. Descn:
County:
Region:
River Basin
Emergency
COC Yes/No
North Carolina D.7--ion of Water Resources Water Scienr— Section Laboratory Results
M9TRO'POLITAN SEWERAGE DISTRI. 1 w28 RIVERSIDE DR- MW3
Buncombe Collector:
B LAVERTY
VisitlD
MW3
ARO Report To
ARO
Location ID:
1P11MSDMW3
Collect Date:
06/13/2017
Priority
-COMPLIANCE
Collect Time:
11:28
Sample Matrix:
GROUNDWATER
Sample Depth
Loc. Type:
MONITORING WELL
Sample ID:
AC39865
PO Number#
ARO
Date Received:
06/14/2017
Time Received:
10_50
Labworks LoginlD
KJIMISON2
Delivery Method
Hand Delivered
Final Report Date:
7125117
Report Print Date:
08/11/2017
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # Analyte Name PQL Qualifier Reference Date Validated by
ARO
Sample temperature at receipt by lab 4.1 °C 6/14/17 RBYRD
Turbidity 1 400 NTU SM 2130 B-2001 6/14/17 ESTAFFORD1
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC39772 North Carolina Di ' 'on of Water Resources Water Scienr-- Section Laboratory Results
Loc. Descr.c
• Mttr000litan Sewage District 2028 Rig-_.-_._e
Dr Asheville, NC
County:
Buncombe Collector:
B LAVERTY
VIsitlD
MW4
Region:
ARO Report To
ARO
Location ID:
1P11MSDMW4
River Basin
Collect Date:
06/13/2017
Priority
COMPLIANCE
Emergency
Collect Time:
10_43
Sample Matrix:
GROUNDWATER
COG Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39772
PO Number#
Date Received:
06/16/2017
Time Received:
08_15
Labworks LoginlD
TASCENZO1
Delivery Method
NC Courier
Final Report Date:
7/28117
Report Print Date:
08/11/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Units Method Analysis
CAS # Analyte Name PQL Qualifier Reference Date
LAB
Sample temperature at receipt by lab 1.1 °C 6/15/17
Validated by
MSWIFT
NH3 as N in liquid
0.02
NUT
1.3
mg/Las N
EPA350.1 REV
6/15/17
CGREEN
NO2+NO3 as N in liquid
0.02.
0.02 U
mg/L as N
EPA353.2 REV 2
6116117
CGREEN
Phosphorus total as P in liquid
0.02
0.07
mg/L as P
EPA365.1 REV 2
6122/17
CGREEN
Total Kjeldahl N as N in liquid
0.2
2.3
mg/Las N
EPA351.2 REV 2
6/21/17
CGREEN
7440-22-4
Ag by ICPMS
1.0
MET
1.0 U
ug/L
EPA 200.8 Rev5.4
6/29117
ESTAFFORDI
7429-90-5
Al by ICP
50
1400
ug/L
EPA200.7 Rev4.4
6/30/17
ESTAFFORDI
7440-36-0
Antimony by ICPMS
10
10 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-38-2
As by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-38-3
Ba by ICP
10
67
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-41-7
Be by ICP
5.0
5.0 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-70-2
Ca by ICP
0.10
39
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-43-9
Cd by ICPMS
0.50
0.50 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-48-4
Cobalt by ICP
50
50 U
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7440-47-3
Cr by ICPMS
5.0
5.0 U
ug/L
EPA200.8 Rev5.4
6129/17
ESTAFFORDI
7440-50-8
Cu by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6129/17
ESTAFFORDI
7439-89-6
Fe by ICP
50
11000
ug/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-97-6
Hg 245.1
0.2
0.20 U, Q2
ug/L
EPA245.1 Rev3
7/14/17
ESTAFFORDI
7440-09-7
K by ICP
0.10
8.8
mg/L
EPA200.7 Rev4A
6/29/17
ESTAFFORDI
7439-93-2
Li ICP
25
25 U
ug/L
EPA200.7 Rev4.4
7/13/17
ESTAFFORDI
7439-95-4
Mg by ICP
0.10
13
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORDI
7439-96-5
Mn by ICP
10
3500 J2
ug/L
EPA200.7 Rev4A
6/30/17
ESTAFFORDI
7439-98-7
Mo by ICPMS
10
10 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-23-5
Na by ICP
0.10
24
mg/L
EPA200.7 Rev4.4
6/29/17
ESTAFFORD1
7440-02-0
Ni by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7439-92-1
Pb by ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7782-49-2
Se by ICPMS
1.0
1.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
7440-24-6
Sr by ICPMS
10
150
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-28-0
Thallium (TI) ICPMS
2.0
2.0 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORDI
7440-62-2
V by ICP
10
10 U
ug/L
EPA200.7 Rev4.4
7113/17
ESTAFFORDI
7440-66-6
Zn by ICPMS.
10,
10 U
ug/L
EPA200.8 Rev5.4
6/29/17
ESTAFFORD1
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL
Page 1 of 3

.NC (DTVX f -1;^ atory Section q?§suits/Sample Comments/Quafifier (P-4-tions
nple ID: AC39772
Result/ Method Analysis
�IP1J tr rll Cl YLV IVQII IG
r`'" Qualifier Units Reference Date Validated by
Sample Comments
failed to meet QC acceptance criteria (17%rec)
Hg-Q2-Estimated; Holding Time exceeded following receipt by lab
due to instrument issues.
NCDEQ-WSS-Chemistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "U". The PQL is used for the qualified result(S) to call
B1 Coliform-Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters repor
B2 Coliform-Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform-Countable membranes with more than 60 or 80 colonies. The value reported is calculated using the count from the smalle
B4 Coliform-Filters have counts of both >60 or 80 and <20. Reported value is estimated or is a total of the counts on all filters reported.
B5 Coliform-Too many colonies were present; too numerous to count (TNTC). TNTC is generally defined as >150 colonies.
B6 Coliform-Estimated Value. Blank contamination evident.
B7 Coliform-Many non-coliform or non-enterococcus colonies or interfering non-coliform or non-enterococcus growth present. In this c(
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than "<" valu
BB2 MPN-All wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD-The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
G2 BOD-The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea;
G3 BOD-No sample dilution met the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at least 1.0 mg/L.
G4 BOD-Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration de
G5 BOD-The glucose/ glutamic acid standard exceeded the range of 198 ± 30.5 mg/L.
G6 BOD-The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.
G7 BOD-Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated foi
G8 BOD-Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated for
G9 BOD-The DO depletion of the dilution water blank produced a negative value.
J1 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 2 of 3

NC DW - 5oratory Section 1ssufts/Sampfe Comments/QuaCzfiM r"�-Rnitions
Sample ID: AC39772
CAS # Analyte Name PQL Result/ Method Analysis
Qualifier Units Reference Date Validated by
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, pl
J5 Temperature limits exceeded (samples frozen or >6°C) during transport or not verifiable (e.g., no temperature blank provided): non-
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
J7 This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrument/method. Th
A Temperature limits exceeded (samples frozen or >6°C) during storage, the data may not be accurate.
A The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
J11 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are 'but of control". The sample is non -homogenous (e.g., VOA soil). The reported value is the lower 1
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence of
N3 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N4 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the labor
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holding time exceeded prior to receipt by lab.
Q2 Holding time exceeded following receipt by lab.
P Elevated PQL* due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit*. The number value repot
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed -field error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s
Y Elevated PQL* due to insufficient sample size.
Z1 Inability to analyze the sample.
Z2 Questions concerning data reliability.
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 3 of 3

AC39663 * North Carolina D' ion of Water Resources Water Scien--- Section Laboratory Results
Loc. Descr.: ' METROPOLITAN SEWERAGE DISTRI— —28 RIVERSIDE DR - MW4
County: Buncombe
Collector:
B LAVERTY
VisitlD
Region: ARO
Report To
ARO
Location ID:
1P11MSDMW4
River Basin
Collect Date:
06113/2017
Priority
COMPLIANCE
Emergency
Collect Time:
10_43
Sample Matrix:
GROUNDWATER
CDC Yes/No
Sample Depth
Loc. Type:
MONITORING WELL
Final Report
Sample ID:
AC39863
PO Number#
ARO
Date Received:
06/14/2017
Time Received:
10_50
Labworks LoginlD
KJIMISON2
Delivery Method
Hand Delivered
Final Report Date:
6/28/17
Report Print Date:
08/11/2017
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/ Method Analysis
CAS # Analyte Name PQL Qualifier Units Reference Date Validated by
ARO
Sample temperature at receipt by lab 4.1 °C 6/14/17 RBYRD
Turbidity 1 85 NTU SM 2130 B-2001 6/14117 ESTAFFORD1
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or " U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

,
A--
YA
RMEWAR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Pat McCrory Charles Wakild, P. E.
Governor Director
May 13, 2013
AMMORANDUM
TO: Aquifer Protection Section Supervisors
Laboratories, Consultants, Permittees, and Interested Parties
FROM: S. Jay Zimmerman, P.G.
Section Chief
John E. Skvarla, III
Secretary
SUBJECT: Aquifer Protection Section Policy for Metals Determinations Required by.Title 1 SA, North
Carolina Administrative Code, Subchapter 2L
BACKGROUND
This policy supersedes the January 7, 2011 policy that addresses the preparation of groundwater samples for
metals analyses. This policy is implemented to establish statewide consistency in the handling of groundwater
samples collected to determine compliance with groundwater standards in Title 15A, North Carolina
Administrative Code,. Subchapter 2L (1 SA NCAC 2L). It also addresses treatment of groundwater quality
samples for metal analyses and is applicable as -follows:
15A NCAC 2L .0202(g),.whick addresses Class GA Standards for groundwater, states ... "the
standard refers to the total concentration in micrograms per liter of any constituent in a dissolved,
colloidal or particulate form which is mobile in groundwater."
The purpose of collecting and analyzing groundwater samples is to obtain a representation of constituents that
are mobile in groundwater. This can usually be achieved with few problems when clear samples are collected
from wells that have been properly constructed and developed so that sediment in the water is minimal.
However, for those samples that are'not clear, it is difficult to differentiate between sediment that rd iresents
formational material versus mobile particulates or precipitates. Recently established -EPA and USOS metals
sampling protocols requiring turbidity level measurements have.provided-some additional guidance regarding
this distinction. Well water samples that are highly turbid on a-eontinuous basis -may be a result of improper
well construction. Therefore, it should be noted that the sampling procedures in this policy are not intended to
be used in.lieu of proper well construction standards found in 15A NCAC 02C .0100.
METHODOLOGY
mole re arati n for metals analysis b Standard Method 3030C for com Hance with oundwater standards
in 1 SA NCAC 2L will no longer be required. The basic preparation requirements of 3030C for determination
of total metal concentrations in unfiltered samples are already incorporated and addressed in current methods
from sources listed in 15A NCAC 2L .0112. Those sources include 40 CFR Part 136, which addresses
approved methods under the Clean Water Act.
AQUIFER PROT1'MON SECTION
1636 Mail Service Center, Raleigh, North Carolina27699-1636
Location: 512N. Salisbtuy St. Raleigh,North Carolina 27604
Phone: [phone] FAX [phone]FAX: [phone]
Internet: wm newaternualihaotc
Wcon&Carofina
kunallrf
an Hm,al nnnnrtwritvt Affirmative Action EmntMer

APS Metals Policy Update
May 13, 2013
Page 2 of 2
In order to ensure that any required analysis reflects as --little bias`as possible due to the presence of sediment in
samples being analyzed for metals that are n iobile (i.e: dissolved aiid colloidal phases), the following sample
eollecdon protocols, based on EPA/CJSGS guidance, are:required:
1. Redevelop wells, if necessary, to ensure turbidity levels are <10 NTU or until turbidity levels are
stable. Turbidity is considered stable when three consecutive measurements vary no more than 10%.
Turbidity measured in the field using a portable meter is not currently defined by certification .
rules as a field parameter. Field turbidity measurements are used to determine adequate purging and
are not reported for permit compliance; therefore, certification -is notrequired. - Collectors must,
however, follow equipment manufacturers' approved procedures for turbidity -measurements when
using portable meters in the field for purging during sample collection.
2. Use speck groundwater sample collection techniques such as low flow/low stress purging and
sampling using an adjustable rate pump to minimize turbidity. Use the same pump for purging and
sampling without removing it from the well. -Purge wells before sampling to ensure turbidity levels .
are <10 NTLL or vary no more than 10%, and other field parameter measurements are stable. If the
turbidity level is >t 0 NTU and has not stabilized within five well volumes, but is within +/- 5 NTU
between measurements and decreasing, additional purging should be considered. It is at the discretion
of the sample collector, however, whether or not to collect a sample or to continue purging•to collect
the best sample possible. Report the turbidity level with other field parameters for each sampling
event.
3. Collect unfiltered samples acidified with 5 mL of concentrated nitric acid per liter of sample (more -if
necessary) to achieve a pH• < 2 at the -time of collection. Acid may be added to the.samples in -the -field
at the time of collection or may be added to the clean containers prior to transport to the field.
Samples must be acidified at least 24 hours prior to analysis,, and have a hold time of six months in
accordance with preservation requirements speolfiedlin 40 CFR Part 136. The following exception is
allowed: _
In accordance with 40 CPR Part 136.3, an aqueous sample maybe collected and shipped
without acid preservation. However, acid must be added at least 24 hours before analysis td
- dissolve anymetals that adsorb to the container walls. If the sample must be analyzed.within
24 hours of eollectibn, add the acid immediately. t. .
Samples collected for mercury. analysis and any other sampling requirements must -be based.oh the -
requirements speoifed!in 40 CFR.:Part 136 and the. sample submission protocols of the -Division of
Water*Quality (DWQ) certified laboratory analyzing the samples.
Samples must be prepared and analyzed by a laboratory certified by -the DWQ using methods from.sources
listed in 15A NCAC 2L A 112. - Water supply well samples with turbidity <1 NTU are excluded from
preliminary laboratory preparation procedures as indicated in the sources listed in 15A NCAC 2L .'0112.
For bulher information or questions, -please contact staff at (919) 807=64641n.the Cem#al .Office.
cc:'KentWiggins -DWQLabaratory'Sectioa _...............:........• _-.._ :.
Dana Satterwhite= DWQ Laboratory Certification..
Roy Byrd — DWQ Laboratory Section
Grover Nicholson — Division of Waste Management Underground Storage Tank Section
Betty Wilcox
Files

■■.■.■ Y S I Environmental Pere Data For a Healthy Planet.0 Ap ote
mwor �rri■rrr
mm■1 NEON Low -Flow Sampling of Water Quality Parameters Used in
LAU1 Determining Groundwater Stability
An Overview
In April 1996, the US EPA .Office of Research and
Development, Office of Solid Waste and Emergency Response,
developed and published a document entitled Low -Plow (Minimal
Drawdown) Ground -Water Sampling Procedures (Publication
EPA540/S-951504). Since then, the use of low -flow sampling
in ground water has increasingly been used to support site
assessment and remedial performance monitoring objectives.
There are many documents on this subject and this particular
document isn't intended to be all-inclusive. For the purposes
of this paper, the focus will be primarily on the watei quality
parameters used to indicate stable well situations,
The document states that "the most common ground
water purging and sampling methodology is to purge
wells using bailers or high speed pumps to remove 3-5...
casing volumes followed by -sample collection" (p. 2).: '.
Adverse impacts can occur through this method affecting
sample quality by increasing levels of turbidity. An
overestimation of certain analytes - namely metals
or hydrophobic organic compounds - may
affect results with this method through _
the inclusion of otherwise immobile
artifactual particles. Filtration of these:..
turbid particles has proved undesirable:
in rectifying the turbidity problem.,
and may, in fact, bias the results of
contaminant concentration on the low:..
side by potentially removing mobile
(contaminant -associated) particles.
These problems can often be mitigated
by rising low -flow purging and sampling -
to reduce sampling -induced turbidity.
The benefits of -low-flow
sampling include (pp. 5,6):
• Samples which are representative
of the mobile load of contaminants
present (dissolved and colloid -associated)
• Minimal disturbance of the sampling point thereby
minimizing sampling artifacts
• Less operator variability and greater control
• Reduced stress on the formation (minimal drawdown)
• Less mixing of stagnant casing water with formation water
• Reduced need for filtration and therefore less time required
by the operator
• Smaller purging volumes decrease potential disposal costs
• Better sampling consistency
In order to minimize the hydraulic stress placed on an
aquifer during purging and sampling, the technique of using low -
flow sampling is recommended. This is typically done through
the use of an adjustable rate pump to remove wafer from the
screened zone at a rate that will cause minimal drawdown of
the water level in the well. Drawdown is measured in the well
concurrent witli pumping using a water level meter. Low -flow
sampling does not require a specific flow rate or purge volume.
"Low -flow refers -to the velocity with which water enters the
pump intake and that is imparted to the formation pore water in
the immediate vicinity of the well screen. Water level drawdown
provides the best indication of the stress imparted by a
..given flow rate for a given hydrological situation"
(p. 5) Typical flow rates on the order of 0.1-0.5
Lhnin are used, but this depends on site -specific
hydrogeology (p. 5) Low -flow sampling relies
on the ability to collect samples after water level
and measured field parameters stabilize over
three consecutive readings taken three to
five minutes apart
It's important to note that, "parameter
selection in monitoring program design
is most often dictated by the regulatory
status of the site. However, background
water quality constituents, purging
indicator parameters, and contaminants
all represent targets for data collection
programs. The tools and procedures
.":used in these programs should be equally
rigorous and applicable to all categories of
data, since all maybe needed to determine
or support regulatory action" (p. 4).
YSt 556 MPS and 5o83 flow tall for groundwater
applications or anytime water is pumped from its
source.
Parameter Stabilization
It is recommended that water quality
parameters be used to determine purging
needs prior to sample collection in each well. Stabilization of
parameters such. as pH, specific conductance, dissolved oxygen
[DO], oxidation-reduction potential [ORP], temperature, and
turbidity should be used to determine when formation water .is
accessed during purging, In general, the order of stabilization is
pH, temperature, and specific conductance, followed by [ORPj,
[DO], and turbidity... Performance criteria for determination of
stabilization should be based on water -level drawdown, pumping
rate, and equipment specifications for measuring indicator
parameters" (p. 5). - (continued)
©2005 YSI Environmental [phone] Fax [phone] [e-mail] www.ysi.com
1006 A532-01

. j
T S I Environmental Pure Data for a Healthy Planet.' Ap Ole
Instruments such as the YSI 556 multiparameter instrument can
simultaneously measure parameters while utilizing a flow cell to
give continuous data.
The document also states, "It should be noted that
turbidity is a very conservative parameter in terms of stabilization.
Turbidity is always the last parameter to stabilize. Excessive purge
times are invariably related to the establishment of too stringent
turbidity stabilization criteria. It should be noted that natural
turbidity levels in ground water may exceed 10 nephelometric
turbidity units (NTU)" (p. 5). -
The YSI 556 muftiparometer instrument simultaneously measures
parameters while utilizing a flow cell to give continuous data. This method
reduces the chance that changes in chemical concentrations are induced
by the sampling technique.
"In -line water quality indicator parameters should be continuously
monitored during purging" (p. 7). Water level drawdown should
also be checked periodically as a guide to flow rate adjustment
with the goal being minimal drawdown (<O.1 m) during purging
(p.7). "Measurements of water quality parameters should be
taken every three to five minutes if the above suggested rates
are used. Stabilization is achieved after all parameters being
measured have stabilized for three successive readings. In lieu of
measuring all five parameters, a-nunimum subset would include
PH, conductivity, and turbidity or DO. Three successive readings
should be within ± 0.1 for pH, ± 3% for conductivity, ± 10 my
for [ORP], and ± 10% for turbidity and DO... [These] guidelines
are provided for rough estimates" (p. 8)
Many 'state agencies encourage the use of low -flow
sampling because it's designed to collect a sample that most
truly represents the water in the screened section of the aquifer
surrounding the monitoring well. It does not come from water
that is mixed within the well by a bailer or inertial sampler, nor
does it come from an average of water that flowed the full length
of a long screened hiterval.
Conclusion
The low -flow sample can most often be trusted to
best represent the contamination or lack thereof in the aquifer
because it was producedby a process that minimizes stress on the
aquifer or well. Low -flow sampling also reduces the variability
in sampling technique that is inherent in traditional bailing
and purging procedures. In summary, low -flow reduces the
physical and chemical stresses, reduces the variability in sample
procedures; increases the ability to determine well stabilization by
continuously monitoring water quality parameters, and reduces
the chance that changes in chemical concentrations are induced
by the sampling technique.
For additional information please contact
YSI Environmental
Tel.[phone]
US 800 897 4151
Fax [phone]
Email. environmental@ysixom
Web. www.ysi.com
YSI 5080, ground water
(lard -sided carrying case
:. with enough space for
the YSI 556 MPS, a 4- or
I0-meter cable, Now cell,
manual, membrane kit,
probe guard, batteries,
.and calibration solutions.
References
U.S. Environmental Protection Agency. EPA540IS-95/504 Low -Flow
(Minimal Drawdown) Gtound-Water Sampling Procedures. ONLINE.
1996. Office of Research and Development & office of Solid Waste and
Emergency Response. -
Available: httpa//www.epa.gov/ahaaivue/ptibs/issue.htnd [6 Dec. 2005].
02005 YSI Environmental [phone] Fax [phone] environmentalOysixom www.ysi.com
1006 A532-01

A*A
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory John E. Skvarla, III
Governor Secretary
December 9, 2014
Thomas E. Hartye
Metropolitan Sewerage District of Buncombe County
2028 Riverside Dr
Asheville, NC 28804
SUBJECT: Groundwater Sampling Results
Permit No. NCO024911.
French Broad River Wastewater Reclamation Facility
Buncombe County
Dear Mr. Hartye:
On October 20, 2014, I collected groundwater samples from the subject facility's groundwater compliance wells
sequentially with your laboratory contractor, Pace Analytical Services, Inc. A copy: of the results is attached for
your records.
If you have any questions, please call me at 828-296-4500.
Sincerely,
4
Andrew Moore
Environmental Senior Technician
Asheville Regional Office
Enc.: Laboratory Analytical Report
"09MAs , illil 0el�'s
MSC 1617-Central Files -Basement
ec: Roger Edwards, ORC
G:\WR\WQ\Buncombe\Wastewater\Non-discharge\MSD\Metropolitan Sewer District Groundwater Monitoring\October 20, 2014\SS Results 10202014.doc
Water Quality Regional Operations — Asheville Regional Office
2090 U.S. Highway 70, Swannanoa, North Carolina 28778
Phone: [phone] FAX: [phone]
Internet: http://portal.nedenr.org/web/wq
An Equal Opportunity \ Affirmative Action Employer

�a6oratorv'.S'ectwn 12esu�
County: BUNCOMBE OF WATF�9 Sample ID: AC13861
River Basin O� QG f PO Number # ARO
Report To AROAP rij r Date Received: 10/20/2014
—! Time Received`. 13:16
Collector. AMOORE,
Labworks LoginlD KJIMISON2
Region: ARID
Sample Matrix: GROUNDWATER Final Report Date: 11/25/14
Report. Print Date: 12/OB/2014
Loc.-Type: Monitoring Well FI118� Rep01t}
Emergency Yes/No vISItID
COC Yes/No
Loc. Descr.: MSD
Location ID: 1P011MSD MW1R Collect Date: 10/20/2014 Collect Time: 12:00 , Sample Depth
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory. purposes.
CAS # Analyte Name
-
PQL
ResuIV
Qualifier -' -
Metnoa
Units
Reference
Analysis
Date
Validated by
Others
Sample temperature at receipt by lab
4.2
°C
10/20/14
RBYRD
Coliform, MF Fecal in liquid
1
16
CFU/100ml APHA9222D-20th
10/20/14-
CGREEN
Total Dissolved Solids In liquid
12 '
56
mg/L APHA2640C-1STH
10/27/14
_CGREEN
i
Laboratory Section>> 1623 Maii Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to hto:// qualiffer Cc4dn <ht •// o mi de /web/wo/lab/ 8 H hechasstzo
Page 1 of 1

r.
County:
BUNCOMBE
Sample ID: AC13819
River Basin
PO Number # 14G0423
Report To
O G
AROAP
s's Date Received: 10/22/2014
-t Time Received: 07:55
Collector:
A MOORE
LoginlD MSWIFT
Region:
ARIDLabworks
Final Report Date: 11/24/14,
Sample Matrix:
GROUNDWATER
F11181I
Report Print Date: 92/08/2014
l oc. Type:
MONITORING WELL .R@pOrt
Emergency Yes/No
COC Yes/No
Visitl D
Loc. Descr.: MSD
Location ID: 1P011MSD_MW1R CollecbDate: 10/20/2014 Collect Time: 12:00 Sample Depth
If this report is labeled preliminary report, the results havenot:been validated: Do not use for Regulatory purposes.
CAS #
LAB
Analvte Name
Sample temperature at receipt by lab
PQL
Kesulu-
Qualifier
2.8
Units
°C
IVleulua
Reference
rulalvsls
Date
10/22/14
Validated by
MSWIFT
WET
Ion Chromatography
_TITLE_-
mg/L
EPA 300. 0 rev2.1
10/24/14,
' MOVERMAN
Chloride',
1:0
2.7
mg/L
EPA 300.0 rev2.1
, 10/24/14
MOVERMAN
Fluoride
"'0.4
0.4 U
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
' Sulfate ,
2.0`
;.5.9
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Bromide.' '
1.0
1.0U
mg/L.
EPA300.0rev2.1
10/24/14
MOVERMAN
NUT
NH3 as in liquid
0.02
6.03
mg/LasN
EPA350.1 REV
10/22/.14 .
CGREEN
MET .
7440-22-4
Agby ICPMS
1.0
1.0 U
ug/L
EPA200.8
10/28/14
ESTAFFORD1.:;, '
7440-38-2
AS by ICPMS'
2.0
2.0 U
ug/L
EPA200.8
10/28/14..
ESTAFFORDI '
7440-38-3
Ba by ICP`
10
25
ug/L
EPA200.7
10/29/14
' rESTAFFORDI
7440-47-3
Cr by ICPMS
10
'
IOU
ug/L
EPA200.8
10/28/14
ESTAFFORD1
7438-97-6
Hg 245.1
0-2
",0.20 U-
ug/L
EPA245.1
11/5/14' :
ESTAFFORD1
7439-92-1
Pb by ICPMS
2.0
2.O U
ug/L
EPA200.8
10/28/14.
ESTAFFORD
Laboratory Section>> 1623 Mail Service center, Raleigh, NC 27699-1623 (919) 7333908
For a detailed description of the qualifier codes refer to Qualifier Codes hm/J I cdenr orc/web/wallab/stafin o i chasnse>
Page 1 of 1

County: BUNCOMBE
...... uua%, L Sample ID:
AC13820
River Basin -
+ PO Number #
14GO424
Report To AROAP
r Date Received:
1012212014
Time Received:
07:66
Collector: A MOORE
¢
Labworks LoginlD
MSWIFT
Region: ARO
Final Report Date:
11/24/14
Sample Matrix: GROUNDWATER
Final Report Report Print Date:
.1210812014
Loc. Type: MONITORING.WELL
Emergency Yes/No
VisitlD
j
COG Yes/No
Loc. Descr.: MSD
Location ID: 1P011MSD MW3
Collect Date: 10/20/2014
Collect Time: 11:30
Sample Depth
If this report is labeled preliminary report, • the results have not been validate&I Do not use for Regulatory purposes.
ResulfL: , j_ Method
Analysis
�.n.�x
LAB
nllalv�c l�aulc
Sample,temperature at receipt by lab
r .,ice.
Qualifier
2.8
°C
Reference
Date
.10/22/14
-
MSWIFT
WET
7439-97-6
Ion Chromatography
TITLE_
mg/L.
EPA 300.0 rev2.1
10/24/14,
MOVERMAN
Chloride
1.0'
1.0 U
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Fluoride
0.4
0.4 U
mg/L.-
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Sulfate'
2.0
2.0 U
mg/L
EPA 300.0'rev2.1
10/24/14 >
MOVERMAN
Bromide
1.01
1.0 U
mg/L
ERA300.0 rev2.1
10/24/14
MOVERMAN
NUT
NH3 as N in°liquid
0:02.
0.02 U
mg/Las N
EPA350.1 REV 2
10/22/14
CGREEN
MET
7440-22-4,
Ag by ICPMS
1.0
1.0 U
ug/L''
EPA200.8
10/28/14
ESTAFFORDI
7440-38-2
'As by ICPMS
2.0`
2.0 U
ug/L
EPA200.8
10/28/1.4
: ESTAFFORDI
7440-38-3
Be by ICP
10,
88
ug/L
EPA200.7
10/29/14
ESTAFFORD1 "
7440-47-3
Cr by ICPMS
10
10 U
ug/L
EPA200.8
10/28/14
ESTAFFORD1
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L,
EPA245.1
17 /14
ESTAFFORD1
"7439-92-1
Pb by ICPMS
2.0
2.0 U
ug/L .
EPA200.8
10/28/14
ESTAFFORD1
Laboratory Section>> 1623 Mail Service center, Raleigh, NC 27699-1623 [phone]
For a detaileddescription of the qualifier codes referto he d/ n ❑al ncden ore/ eb/ an b1 tafi-flo/t hassist#Daq 4u ne r Code, <hto,//bomi.ncdencor¢/web/wo/lab/staenf ftechassisn
Page 1.of 1

County: BUNCOMBE
dF r{p-�� Sample ID:
AC13821
River Basin
p PO Number #
14GO425
Report To AROAP,
C�r'jQ Date Received:
10/22/2614
Time Received:
07:55
Collector. A MOORE
Labworks LoginlD
MSWIFT
Region:. ARO
- Final Report Date:
11/24/14
Sample Matrix: -GROUNDWATER
F1113� R@pblt Report Print Date:
12108/2014
Loc. Type: MONITORING WELL
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD
Location ID: 1P011MSD_MW4
-Collect, Date: 10/41.2014
Collect Time: 11:00
Sample• Depth
If this report is labeled preliminary report, the results have not been validated, Do not use for Regulatork purposes.
nt.9Sulu - MIMI rvu /7I iaiyata .. Validated by
CAS # Analvte Name PQL Units
Qualifier Reference Date
LAB
Sample temperature at receipt by lab
2.8
°C
10/22/14
MSWIFT
WET
7439-97-6 Ion Chromatography
TITLE_
mg/L
EPA 300. 0 rev2. 1
10/24/14
MOVERMAN
Chloride
1.0-
13
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Fluoride
0.4
0.4 U
mg/L
EPA 300.0 rev2.1
10/24/14.
MOVERMAN
Sulfate
2.0'
41
mg/L ,-
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Bromide
1.0
1.01 U
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
NUT
NH3 as N in liquid
0.02
1.5
mg/LasN
EPA350.1 REV
10/22/14
CGREEN
MET
7440-22-4
Ag by ICPMS
1.0
1.0 U
ug/L
EPA200.8
10/28/14
ESTAFFORD1
7440-38-2
As by ICPMS
2.0 ' _
..2.9
ug/L
EPA200.8
10/28/14
ESTAFFORD1
7440-38-3
Ba by ICP
10
73
ug/L
EPA200.7
10/29/14
ESTAFFORD1 .
7440 47-3
Cr by'ICPMS
10
10 U
ug/L
EPA200.8
10/28/14
ESTAFFORD1,
7439-97-6.
Hg 245.1
0.2
0.20 U
ug/L,
EPA245.1
11/5/14
ESTAFFORD1
7439-92-1.
Pb by ICPMS
2.0
2.0 U
ug/L
E7200.8
10/28/14
ESTAFFORD1
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description ofthe qualifier codes referto hty.[Lpomi cd °r eb/wan b/st fi fl /a h eiiaoata au Veer cod­htu�f/ ml Kd . wlwebl a/I b/u finfio/c h°�si:n
Page 1 of 1

` wu L:aboratorv.S'ectwn
WesuG
County: BUNCOMBE O WA%9
Sample ID:
AC13822
River Basin 4� �G
PO Number #
14GO426
Report To AROAP'
Date Received:
10/22/2014
"t
Time Received:
07:66
Collector. A MOORE ¢ "c
`>
Labworks LoginlD
MSWIFT
Region: ARO
Final Report Date:
11/24/14
Sample Matrix: GROUNDWATER
FIIIa� iz@port
Report Print Date:
12/08/2014
Loc. Type: MONITORING WELL
Emergency Yes/No VisitlD
COC Yes/No
Loc. Descr.: MSD
LocationID: 1P011MSD_MW2R
Collect Date: 10/20/2014
Collect Time: 10:40
Sample Depth
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. -
Resultt'
Method
Analysis
CAS #
Analvte Name
PQL
-
Qualifier.
Units
Reference
Date
Validated by
LAB
Sample temperature at receipt by lab
2,8
°C
10/22/14
MSWIFT
WET
7439-97-6
Ion Chromatography
_TITLE
mg/L
EPA 300. 0 rev2.1
10/24/14
MOVERMAN
Chloride
1.0
'9.6
mg/L
EPA 300. 0 rev2.1
10/24/14
MOVERMAN
Fluoride
0.4
0.4 U
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Sulfate
2.0
63
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
Bromide
1.0
1.0 U
mg/L
EPA 300.0 rev2.1
10/24/14
MOVERMAN
NUT
NH3 as N in liquid 0.02 0.03 mg/Las N EPA 350.1 REV 2 10/22/14 CGREEN
MET
7440-224
Ag by ICPMS
1.0
1.0 U
ug/L
EPA200.8
10/28/14
ESTAFFORDI
7440-38-2
As by ICPMS
2.0
2.0 U
ug/L
EPA.200.8
10/28/14
ESTAFFORD1
7440-38-3
Ba'byICP
10 '
48
ug/L
EPA200.7
10/29/14
ESTAFFORDI
7440-47-3
Cr by ICPMS
10
IOU
ug/L
EPA200.8
10/28/14-
ESTAFFORDI
7439-97-6
Hg 245.1
0.2
0.20 U
ug/L
EPA245.1
11/5/14
ESTAFFORDI
7439-92-1
Pb by ICPMS
2.0
2.0 U
ug/L
EPA200.8
10/28/14
ESTAFFORD1
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to hrn:// nanai ncdenr or°/wet/wo4abinaflneo/t ctiass(stMa a aaareer cedes htall nomi.ncdencom/weblwanab/swflnxohechassis
Page 1 of 1

County: BUNCOMBE OF wpr��9 Sample ID: AC13858
River Basin Da AG PO Number# ARO
Report To AROAP Date Received: 10/20/2014
y Time Received: 13:16
Collector: A MOORE
Labworks LoginlD KJIMISON2
Region: ARO
Final Report Date: 11/25/14
Sample Matrix: GROUNDWATER Report Print Date: 12/08/2014
Loc. Type: Monitoring Well Fl�la� Report
Emergency Yes/No VisitlD
COC Yes/No
Loc. Descr.: MSD
Location ID:. 1P011MSD MW2R Collect Date: 10/20/2014 Collect Time: 10:40 Sample Depth
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes,
Result/ Method Analysis
ur» tr rvnatyte tvatne rt ct Uniw - -- -- -
Qualifier Reference Date
Others
Sample temperature at receipt by lab 4.2 °C 10/20/14 RBYRD
Coliform, MF Fecal in liquid 1 1.132 CFU/100ml APHA9222D-20th 10/20/14 CGREEN
Total Dissolved Solids in liquid r 12 260 mg/L APHA254OC-18TH 10/27/14 CGREEN
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919), 733-3908
For a detailed description of the qualifier codes refer to hta/!w IWQAfinfio/bassist#DQ-1iffer c°a he •/I t a f ebf bl. fi fiolt ha^ ie
Page 1 of 1

Ij,wu L.ayoratory.yawn
iwesut
County: BUNCOMBE
CIF NNArF�9
Sample ID:
AC13859
River Basin.
p .
PO Number #
ARO
Report To AROAP
r,
Date Received:
10120/2014
Time Received:
13:15
Collector. AMOORE
Labworks LoginlD
KJIMISON2
Region: ARO
Final Report Date:
11/25/14
Sample Matrix: GROUNDWATER
Final Report
Report Print Date:
12/08/2014
Loc. Type: Monitoring Well
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD
Location ID: 1P011MSD_MW4
Collect Date: 1012012014
Collect Time: 11:00.
Sample Depth
If this report is labeled preliminary report, the results have not been validated Do
not use for Regulatory purposes.
Result/
Method
Analysis
CAS # Analyte Name PQL
Qualifier
Units
Reference
Date
Validated by
Others
Sample temperature at receipt by lab
4.2
°C
10/20/14
RBYRD
COliform, MF Fecal in liquid 1
1 B2
CFU/100mi APHA9222D-20th
10/20/14
CGREEN
Total Dissolved Solids in liquid 12
212
mg/L APHA2540C-18TH
10/27/14
CGREEN
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to hto:n aortal nm-nroroJwes/waflabistaeneo/teehassi.taoata Cluanee. Code. <htc// aortal.mdenr.ora/web!wa/lab/,ta8nfio/techassist>
Page 1 of 1

County: BUNCOMBE
: Wq'� "".
Sample ID:
AC13860
River Basin
qQ�
PO Number #
ARO
OHO
Report To AROAP
Date Received:
10/20/2014
PCollector.
Time.Received:
13:15
A MOORE
_
Labworks LoginlD
KJIMISON2
Region: ARO
Final Report Date:
11/25/14
Sample Matrix: GROUNDWATER
FItlB� REpOit
Report Print Date:
12/O8/2014
Loc. Type: Monitoring Well
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD
Location ID: - 1P011MSD MW3
Collect Date: 10/20/2014
Collect Time: 11:30
Sample Depth
If this report is labeled preliminary report; the results have not been validated. Do not use for Regulatory purposes.
Results
Method
Analysis
vno rr rtuciytc rvainC rWL- Uima - -----
Qualifier Reference Date
Others
Sample temperature at receipt by lab 4.2 'C 10/20/14 RBYRD
Collform, MF Fecal in liquid 1 1 B2 CFU/100ml APHA9222D-20th 10/20/14 CGREEN
Total Dissolved Solids in liquid 12 37 mg/L APHA2540C-18TH 10/27/14 CGREEN
Laboratory Section>> 1823 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes referto om oodaorora/wee/wanxe/s«a( eo c Jy_sis<aoac�guanee� ceec. y/ wrtai Mdenr w/webl-41 .bn!L./.'h9 I�t>
Page 1 of 1

`h U`WU Laboratory section
(Nesut)
County:
BUNCOMBE
W ArF9
Sample ID:
AC13861
River Basin
OF
Q
PO Number #
ARO
Report To
AROAP
r -.
Date Received:
10/2012014
=
Time Received:
13:16
Collector:
A MOORE
Q <'
:• ..: • :c' ,
Labworks LoginlD
KJIMISON2
Region:
ARO
Final Report Date:
11/25/14
Sample Matrix:
GROUNDWATER
FIhal R6e br-t
Report Print Date:
12/08/2014
Loc. Type:
Monitoring Well
Emergency Yes/No
VisitlD
COC Yes/No
Loc. Descr.: MSD
Location ID:
1P011MSD MW1R
Collect Date: 10/2012014
Collect Time: 12:00
Sample Depth
If this report is labeled preliminary report; the results have not been validated. Do not use for Regulatory purposes.
CAS # Analyte Name
Others
Result/ Metnocl Analysis Validated by
PQL Qualifier Units Reference Date
Sample temperature at receipt by lab
4.2
°C
10/20/14
RBYRD
C011form, MF Fecal in liquid
1
16
CFU/100ml APHA9222D-20th
10/20/14
CGREEN
Total Dissolved Solids in liquid
12
56
mg/L APHA2540C-1STH
10/27/14
`CGREEN
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer to hw// a ml cde e/ eb/waA bf•t fi fl /t ba3. If taData Qualifler cede•. <hta.-// o0 0l ncdenr are/web/wa/labl t,Bnflo/techasslst>
Page 1 of 1

t r ,
w
A, - 7.,
NCD NR
North Carolina Department of Environment and Natural Resources
Division of Water Resources
Water Quality Programs
Pat McCrory Thomas A. Reeder
Governor Director
February 14, 2014
CERTIFIED MAIL
RETURN RECEIPT REQUESTED - 70121010 00021967 8227
Thomas E. Hartye
Metropolitan Sewerage District of Buncombe County
2028 Riverside Drive
Asheville, NC 28804
Subject: Exceedances of North Carolina Groundwater Standards
Permit No. NCO024911
French Broad River Wastewater Reclamation Facility
Buncombe County
Dear Mr. Hartye,
John E. Skvarla, III
Secretary
Staff of the North Carolina Division of Water Resources (DWR), Water Quality Regional Operations Section
(WQROS) reviewed current and historical Groundwater Quality Monitoring: Compliance Report Forms (GW-59
Forms) for the subject facility. The review revealed the following exceedances of either a Title 15A North
Carolina Administrative Code (NCAC) 2L .0202 groundwater quality standard or an interim maximum allowable -
concentration (IIVIAC) for groundwater established in accordance with 15A NCAC 2L .0202:
1. Ammonia was detected in compliance monitoring well MW-4 in excess of the RVIAC of 1,500
micrograms per liter (µg/L) in the sample collected October 10, 2013. Ammonia has been detected above
the IMAC in every routine monitoring event going back to August 2011 when the IMAC for ammonia
was established.
2. Fecal coliform bacteria have consistently been detected above the 15A NCAC 2L .0202 groundwater
standard for coliform organisms in background monitoring well MW-1R since 2010. Prior to 2010 total
coliform bacteria were consistently detected in MW-1R.
Please provide a response to these findings detailing the cause of the ammonia groundwater exceedance in
compliance monitoring well MW-4 and the fecal coliform bacteria detected in background monitoring well MW-
1R by April 14, 2014. 1
Water Quality Regional Operations — Asheville Regional Office
2090 U.S. Highway 70, Swannanoa, North Carolina 28778
Phone: [phone] FAX: [phone]
Internet httpl/portal.nodenrorg/Weblwq
An Equal Opportunity 1 Affirmative Action Employer

Metropolitan Sewerage District of Bi mbe County
Permit N C0024911
February 14, 2014
Page 2 of 2
If you have any questions concerning this matter, please contact Andrew Moore via email at
[e-mail] or at [phone].
Sincerely,
G. Landon Davidson, P.G.
Regional Supervisor
Water Quality Regional Operations Section
40RUM ARO'=Wate Quality- File
Water Quality Central Files

r
of North Carol ria
Department of, Envir-orirnent,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governorma
Jonathan B. Howes, Secretary [DE H ICI F A. Preston Howard, Jr., P.E., Director .
Asheville Regional Office
GROUNDWATER SECTION
March 24, 1997
Mr_. W. H. Mull
Metropolitan Sewerage District
Post Office Box 8969
Asheville, North Carolina 28814
Dear Mr. Mull:
Subject: Groundwater Monitoring Requirements
NPDES Permit No. MC0024911
MSD Buncombe County WWTP
Buncombe County
Permit No. NCO024911 Part III(D) issued on August 28, 1995 states
that groundwater monitoring may be required to determine
compliance with groundwater standards. This letter serves as
written notice of groundwater monitoring requirements for Permit
No. NC0024911,
GROUNDWATER REQUIREMENTS
1. The three (3) existing downgradient monitor wells, and one
upgradient monitor well shall,be-sampled every January and
July for the following parameters:
NO3 Ammonia Nitrogen
pH" Water Level
'Chloride Total Coliforms
Arsenic Barium
Cadmium Chromium
Lead Mercury
Selenium Silver
Total Dissolved Solids TOC
Volatile Organic Compounds - In July Only by EPA Method
6230D (Capillary - Column), "Standard Methods For
The Examination of Water and Wastewater";`17th ed.,
1989.
The measurement of water levels must be made prior to
sampling for the remaining parameters. The depth to water
in each well shall be measured from the surveyed point on
the top of the casing.
Interchange Building, 59 Woodfin Place C FAX [phone]
Asheville, North Carolina 28801 N4An Equal Opportunity/Affirmative Action Employer
Voice 704-251 6208 50% recycles/ 10% post -consumer paper

Mr. W. H. Mull
March 24, 1997
Page 2
The measuring points (top of well casing) of all monitoring
wells shall be surveyed to provide the relative elevation of
the measuring point for each monitoring well.
If TOC concentrations greater than 10 mg/1 are detected in
any downgradient monitoring well, additional sampling and
analysis must be conducted to identify the individual
constituents comprising this TOC concentration. If the TOC
concentration as measured in the background monitor well
exceeds 10 mg/l, this concentration will be taken to
represent the naturally occurring TOC concentration. Any
exceedances of this naturally occurring TOC concentration in
the downgradient wells shall be subject to the additional
sampling and analysis as described above.
If any volatile organic compounds are detected by Method
6230D, then the Asheville Regional Office groundwater
supervisor (704-251-6208) must be contacted immediately for
further instructions regarding any additional follow-up
analyses required. The results of all initial and follow-up
analyses must be submitted simultaneously.
The results of the sampling and analysis must be received on
Form GW-59 (Groundwater Quality Monitoring: Compliance
Report Form) by the Groundwater Section, Permits and
Compliance Unit, P.O. Box 29578 Raleigh, N.C. 27626-0578
every February and August.
2. The Compliance Boundary for the disposal system is specified
by regulations in 15 NCAC 2L, Groundwater Classifications
and Standards. An exceedance of Groundwater Quality
Standards beyond the Compliance Boundary is 'subject to the
penalty provisions applicable under General Statute 143-
215.6(1)a. The sale of property, by the Permittee, which is
within or contiguous to the disposal site, may alter the
location of the Compliance Boundary.
For facilities permitted prior to December 30, 1983, the
Compliance Boundary is established at a distance of 500 feet
from the waste disposal lagoon, or the property boundary,
whichever is less.
If the title to any property, which may affect the location
of the Compliance Boundary is changed, the Permittee shall
notify the DEM Director within 14 days. The Director shall
then establish a modified Compliance Boundary which will be
done as a modification to the Permit.

Mr. W. H. Mull
March 24, 1997
Page 3
The REVIEW BOUNDARY for this disposal system is specified by
regulations in 15 NCAC 2L, Groundwater Classifications and
Standards. A REVIEW BOUNDARY is established around disposal
systems midway between the Compliance Boundary and the
perimeter of the waste disposal area. When the
concentration of any substance equals or exceeds the maximum
allowable concentration of that substance at the REVIEW
BOUNDARY, as determined by monitoring, the Permittee shall
either (i) demonstrate, through predictive calculations or
modeling, that natural site conditions, facility design and
operational controls will prevent a violation of standards.
at the Compliance Boundary, or (ii) submit a plan for the
alteration of existing site conditions, facility design or
operational controls that will prevent a violation of
standards at the Compliance Boundary, and implement that
plan upon its approval by the Director.
3. Any additional groundwater quality monitoring, as deemed
necessary by the Division, shall be provided.
If you have any comments or questions, please call Kay Dechant at
[phone].
Sincerely,
Roy M. avis
Regional Supervisor
\lkd
cc: Bob Cheek
David A. Goodrich
Betty Wilcox

/' "Cry
S E vV 6t8,4a&C 015 Tie /C_-r
/Ak
m> -neoPo Li T
LAW�`�`�
// d 7/97
ENGINEERING AND ENVIRONMENTAL SERVICES, INC.
January 24, 1997 JAN 2 7 1991 i
Groundwater Section
_ Asheville rmxionai once
North Carolina Department of Environment,
Health, And Natural Resources
Groundwater Section
Asheville, North Carolina 28814
Attention: Ms. Kay Dechant
Hydrogeologist
Subject: Request for Reduction of Sampling Frequency
Tri-Annual Sampling Program
Metropolitan Sewerage District
Asheville, North Carolina
Law Engineering Project Number 30290-5-4492.15
Dear Ms. Dechant:
On behalf of the Metropolitan Sewerage District (MSD) of Buncombe County, Law Engineering
and Environmental Services, Inc. (LAW) is writing this letter to formally request a reduction in the
frequency of the on -site monitoring at the MSD facility and that selected parameters be deleted
from the analytical requirements.
The North Carolina Department of Environment, Health and Natural Resources - Division of
Environmental Management (NCDEM) required MSD to provide a system for regular ground -water
quality monitoring within the specified compliance boundary around their sludge/ash storage
reservoirl.
As a part of the expansion and upgrading of the MSD facility, NCDEM issued MSD an
Authorization to Construct on November 17, 1989. In order to allow the use of the existing sludge
storage lagoon as an ash storage lagoon, the original Authorization to Construct was amended in a
letter from Mr. George T. Everett of the NCDEM to Mr. William H. Mull of the MSD, titled
Amendment to Authorization to Construct, dated March 11, 1991. The amendment required that a tri-
annual sampling program be initiated and maintained to monitor the ground -water quality in the
vicinity of the ash storage lagoon. NCDEM required that the monitoring program evaluate ground-
water samples for the presence of selected inorganic parameters, selected metals, and volatile organic
compounds (VOCs). VOCs are analyzed only during the September sampling event.
' NCAC Title 15, Subchapter 2L Groundwater Classification and Standards, Section .0107 Compliance
Boundary and Section .0108 Review Boundary, effective November 8, 1993.
FOUR INTERCHANGE BOULEVARD • GREENVILLE, SC 29607
[phone] • FAX [phone]

ills. Kay Dechant
January 23, 1997
,�Ak Page 2
During April 1990, LAW installed and sampled three monitoring wells, designated as MW-1, MW-2
and MW-3, around the lagoon. Monitoring well MW-2 was damaged during MSD's construction
activities and was later abandoned and replaced by monitoring well MW-2R. One additional
downgradient monitoring well, designated MW-4, was installed at the compliance boundary on July
23, 1996.
The onsite monitoring wells, with the exception of MW-4, have been sampled three times a year
(February, June and September) for the past seven years. Historically, the concentrations of
detected parameters in the ground water have not changed significantly. LAW believes that there
is presently a sufficient amount of baseline analytical data to warrant a reduction in the sampling
frequency.
In our opinion, a reduction in sampling frequency will not have an effect on the long-term
monitoring goals at the site. At=this_tiine,. LAW=proposes--b.iamival sampling at the site___ Our
proposed:sampling-events would be iri-January -and July_ of each year -with the N_ CDEM_sampling-,,-
split and VOC analysis occurring during the month -of July.
Additionally, LAW proposes that selected parameters which have not been detected, or have not
been detected at significant concentrations, be deleted from the scope of the monitoring program.
LAW proposes that the following parameters be deleted from the required ground -water analyses:
Chloride -:The maxi rium defected_ concentration ofchloride at the -site Was 38 milligrams_per:liter
(mWI), which is well below the maximum contaminant level (MCL)2 of 250 mg/1.
_Nitroi�enr (as: ammonia)_ -!The maximum detected concentration of nitrogen as ammonia at the site
was!0.9_mg/l/l dnd this parameter is typically not detected above the method detection level.
Nitroeri:(as=nitrate) ; The maximum detected concentration of nitrogen as nitrate at the site has
been 9.5_ mg/lain the abandoned monitoring well MW-2. The maximum detected concentration of
nitrate in the existing monitoring wells has been 6.5 mg/I and the concentrations do not appear to
be increasing over time. Tfie MCL for nitrate is 10 mg/I.
.Arse-i iyArsenic was detected in LAW's split samples from monitoring wells MW-2R and MW-4
in the September 1996 sampling event at concentrations which exceed the MCL. Hd—wexe
NGDEM'_s_`s.plit samples did"notdetect arsenic -above -the_- method- detection -levels., Prior to the
September 1996 sampling event, arsenic had not been detected in the ground water samples
collected from the on -site monitoring wells. Based on the historical data, and NCDEM's
analytical data, it is unlikely that arsenic is a contaminant at this site. The recent changes in the
arsenic concentrations are likely due to the September 1996 analysis being conducted at a different
laboratory than the historical analyses.
dVlererrvr= Mercury has not been detected in monitoring wells MW-1, MW-2, MW-2R and MW-3.
Mercury was detected by LAW in the ground -water from MW-4 during the September 1996
'- NCAC Title 15, Subchapter 2L Groundwater Classification and Standards, Section .0102 Groundwater
Quality Standards, Paragraph (g) Class GA Standards, effective October 19, 1993. c

AkMs. Kay Dechant
January 23, 1997
Page 3
sampling event at a concentration of 0.000309 mg/l. However, NCDEM's split sample did not
detect mercury in MW-4. The MCL for mercury is 0.0011 mg/l.
aBaT�i fifi-, The maximum detected concentration of barium detected at the site has been 6.69 mg/1
in MW-3 during the 1990 sampling event. The maximum detected concentration of barium since
1990 has been 0.816 mg/1 in abandoned monitoring well MW-2. The MCL for barium is 2.0 mg/l.
,Cadmium' - Prior to the September 1996 sampling event, the only detected concentration of
cadmium at the site was 0.0006 mg/l in monitoring well MW-3 during the May 1990 sampling .
event. The September 1996 sampling event detected cadmium in each monitoring well at
concentrations which exceed the MCL. However, NCDEM's split samples did not detect
cadmium above the method detection level. The recent changes in the cadmium concentrations
are likely due to the September 1996 analysis being conducted at a different laboratory than the
historical analyses.
Selenium pThe only detected concentration of selenium at the site was 0.069 mg/1 in monitoring
well MW-1 during the September 1993 sampling event. The MCL for selenium is 0.05 mg/l.
;SilverF; The only detected concentrations of silver at the site were from the May 1990 sampling
Jevent. The maximum detected concentration for that sampling event was 0.001 mg/l. The MCL
for silver is 0.018 mg/l.
LAW appreciates your consideration and cooperation in this matter. We look forward to your
review comments and approval of the above requests. Should you have any questions or require
additional information please call, [phone].
Sincerely,
LAW ENG ERIN9 AND ENVIRONMENTAL SERVICES, INC
Robert E. MacPhee
Project Hydrogeologist
Project Manager
�as-AQL'
Paul S. Johnstone
Senior Hydrogeologist
Manager, Environmental Services
REM/rem
I Igvl2401 sys 1 userl bmacphee I projects I msd (letters I trans971 biannpsj. doc

DATE: =f
TIME: 20,,,)
NAME/COMPANY :
ARO QQMFLAINT/TELEPHONE LOG
D214BER.-
6q
SUMMARY OF COMMUNICATION(who what when; where, how, how)
POSSIBLE SOURCE/OWNER PHONE #
LOCATION/ADDRESS
CITY COUNTY
ASSIGNED TO: DATE: RESPOND BY:

MEETING WITH MSD
May 8, 1996
Attendees: Don Link, Kay Dechant, Ann Rumbough, Max Haner,
Mark Fender, Stan Boyd.
The elevated levels of dissolved solids (MW-2R, M87j5) in
exceedance of 2L standards was discussed. MSD was asked to do
additional monitoring to try to characterize the source. For the
June 1996 sampling event they shall sample for sulfate, calcium,
magnesium, sodium, potassium, hardness - both carbonate and
noncarbonate. Both downgradient monitor wells shall be sampled.
for volatile and semivolatile compounds. F
A proposal for a downgradient well at the 500 foot
compliance boundary is due by June 30, 1996. The upgradient well
may be replaced due to a history of coliform bacteria.

s ;u STATE p
P� rM.,,,
State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James B. Hunt, )r., Governor Let ter of Transmittal Ann B. Orr
Regional Manager
Jonathan B. Howes, Secretary
Date:
County:
Enclosed please find a copy of the following for your use:
If you have any questions, please contact me at 7041251-6208
Enclosures
Sincerely,
Ka Duch n
Y
Hvdrogeologist
Interchange Building, 59 Woo(Ifin Place, Asheville, N.C. 28801 • 'Telephone [phone]

State of North Carolina
Department of Environment, Health, and Natural Resources .
Asheville Regional Office
James G. Martin, Governor Ann B. Orr
William W. Cobey, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
i October 30, 1992
Mr. Stan Boyd
Metropolitan Sewage District of Buncombe County
Post Office Box 8969
Asheville,, North Carolina 28807
Dear Mr. Boyd:
Subject: Review of Report of Tri-Annual Groundwater)
Well Sampling/Monitoring Well Abandonment and Replacement
Metropolitan `Sewage District
Permit No. NCO024911
Buncombe County, North Carolina
This letter is to acknowledge receipt and acceptance of the subject report
dated September 28, 1992 submitted by Law Engineering.
I concur with the conclusions and recommendations contained therein. If
you have any comments or questions, please contact me at [phone].
Sincerely,
i7l�Dechant
Hydrogeologist.
LKD/ge
cc: Betty Wilcox
Robert E. MacPhee
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 • Telephone [phone]
An Equal Opportunity ,Affirmative Action Employer

I-Kf)
Hendon Engineering Associates
I N CO R P O R ATE D
TELEPHONE [phone]
e ADDRESS REPLY TO P. O. BOX 7623
306 WEST HAYWOOD STREET . ASHEVILLE, NORTH CAROLINA 28802
HARRY H. HENDON
(1904-1973)
H. D. HUBER
M. G. BUCKLEY, JR. April 9, 1992
R. F. HOLBROOK
J. 0. BREWER
W. H. DUKE
W. L. MORRIS, JR.
Ms. Kay.Dechant
N.C. Department of Environment, Health
and Natural Resources
59 Woodfi.n Place
Asheville, NC 28801
Subject: Project 800, Section 1
Additions to Wastewater Treatment Plant
Metropolitan Sewerage District of Buncombe County
EPA C370391-08
Dear Ms. Dechant:
H. E. RYAS, JR.
S. S. KANE
W. P. CONNER
Enclosed is a sketch showing the location of the monitoring well
which was selected at the meeting on the job site on March 12, 1992.
At that meeting you requested Russ McBrayer, our representative at
the job site, if he could send a sketch of the location.
Very truly yours,
HENDON ENGINEERING ASSOCIATES, INC.
By
Harry/E. Byas, Jr., P.E.
HEB:d
Enclosure
W800-April.9D
cc: Mr. Stan Boyd, w/enc.
Mr. Singh Kahlon, w/enc.
Mr. Russ McBrayer, w/enc.

State of North Carolina
[department of Environment, Health, and Natural Resources
AClievillc Regional Office
I�nl < < �lartin, C�r��crnc�r Ann B. Orr
Williarn W ( ol)et, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
February 25, 1992
Mr. William it. Mull
Metropolitan Sewage District of Buncombe County
Post Office Box 8969
Asheville, North Carolina 28807
Dear Mr. Mull:
Subject: Groundwater Compliance Monitoring
Metropolitan Sewage District (MSD) of
Buncombe County
Amendment to Authorization to Construct
Permit No. NCO024911
Buncombe County, North Carolina
As .required by the subject Authorization to Construct,
the three existing groundwater monitor wells shall be sampled
every February, June, and September.
On February 17, 1992, representatives from our office met
with Robert MacPhee of Law Engineering to split samples from
Elie groundwater monitor. wells. At that time, it was noted
that MW-2 was damaged and samples were not collected from that
well.
MSD is required to properly abandon MW-2 and submit the
enclosed well abandonment record upon completion.
MW--2 shall be replaced at a location 250 feet
r3nwnc1r.adi.ent of the waste boundary (1-agoon) . It is my
11T1(1-T-.st-nnrli ng that the 250 feet location would be in the
vi(,inity of the incinerator presently under construction. To
minimize 1_1ireat of damage from construction traffic and
egiripment, MSD may postpone replacement of MW-2 until
construction of the incinerator is nearing completion.
Replacement of MW-2 shall be completed, and groundwater
samples obtained prior to start up of the incinerator.
I, , �• h l"i'l. I11iHin1, S'I W" "b6i Hwv A•.hrvillc. N.C. )RR111 0 T-h•phrnir 7(}1251 (,2(1R

Mr. William if. Mull
February 25, 1992
Page 2
Please contact me for coordination of locating the
proposed replacement well.
Sincerely,
Laura Kay Dechant
Hydrogeologist
T,KD/gc
cc: Mark Fender
Robert MacPhee
Bob Cheek

A,,. SLATr, .._
rr,nv iJ r>ry
State of North Carolina I 1 1
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James G. Martin, Governor Ann B. Orr
William W. Cobey, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
February 6, 1992
Mr. William H. Mull
Metropolitan Sewage District of Buncombe County
Post Office Box 8969
Asheville, North Carolina 28807
Dear Mr. Mull:
r
Subject: Buncombe County MSD Phase IV
Amendment to Authorization to Construct
Permit No. NCO024911
Buncombe County, North Carolina
In -accordance with the policy of the Division of
Environmental Management to ensure the good quality of North
Carolina's groundwater, the referenced Authorization to
Construct requires several activities related to groundwater
monitoring. The following guidelines are presented to assist
you in complying with those requirements:
GROUNDWATER REQUIREMENTS
1.) The three (3) existing monitor wells shall be
sampled every February, June, and September for the
following parameters:
NO3 (10.0) Ammonia Nitrogen
TD5 (500.0) TOC
pH (6.5-8.5 standard units) Water Level
Chloride (250.0) Total Coliforms (1/100ml)
Arsenic (0.05) Barium '
Cadmium (0.005) Chromium (0.05)
Lead (0.05) Mercury
Selenium Silver
T.S.S. (Total Suspended Solids)
Volatile Organic Compounds - In September Only (by
method 1 or 2 below)
Interchange Building, 59 Wixxifin Place, Asheville, N.C. 28801 • Telephone 70425"208
An Equal'Opportunity Affirmative Action Employer

Mr. William H. Mull
February 6 1992
Page 2
Method 1: Method 6230D (Capillary - Column),
"Standard Methods For The Examination Of
Water and Wastewater", 17th ed., 1989
Method 2: Method 502.2 "Methods For the `
Determination Of Organic Compounds In
Drinking Water", U.S. EPA - 600/4-88/039
The measurement of water level must be made prior to
sampling for the remaining parameters.
The measuring points (top of well casing) of all
monitoring wells shall be surveyed relative to mean
sea level (M.S.L.). The depth of water in each well
shall be measured form the surveyed point on the top
of the casing. The water level elevations shall
then be determined relative to M.S.L.
The numbers in parentheses represent the maximum
allowable concentration in groundwater for the
various analytical parameters, as specified in 15
NCAC 2L (Groundwater Classifications and Standards).
Unless otherwise specified, the units for these
concentrations are expressed as milligrams per
liter.
If TOC concentrations greater than 10 mg/1 are
detected in any downgradient monitoring well,
additional sampling and analysis must be conducted
to identify the individual constituents comprising
this TOC concentration. If the TOC concentration as
measured in the background monitor well exceeds 10
mg/1, this concentration will be taken to represent
the naturally occurring TOC concentration. Any
exceedances of this naturally occurring TOC
concentration in the downgradient wells shall be
subject to the additional sampling and analysis as
described above.
If any volatile organic compounds are detected by
method 623OD, or the equivalent method 502.2, then
EPA Methods 604-and 611 must also be run to detect
other organic compounds which may be present. The
results of all analyses specified in the monitoring
requirements, including 604 and 611 if required,
must be submitted simultaneously.

Mr. William H. Mull
February 6, 1992
Page 3
The results of the sampling and analysis shall be
sent to the North Carolina Division of Environmental
Management on Form GW-59 (Compliance Monitoring
Report Form) every March, July, and October.
2. The Compliance Boundary for the disposal system is
specified by regulations in 15 NCAC 2L, Groundwater
Classifications and Standards. An exceedance of
Groundwater Quality Standards beyond the Compliance
Boundary is subject to the penalty provisions
applicable under General Statute 143-215.6(1)a. The
sale of property, by the Permittee, which is within
or contiguous to the disposal site, may alter the
location of the Compliance Boundary.
For facilities permitted prior to December 30, 1983,
the Compliance Boundary is established at a distance
of 500 feet from the waste disposal lagoon, or the
property boundary, whichever is less.
If the title to any property, which may affect the
location of the Compliance Boundary is changed, the
Permittee shall notify the DEM Director within 14
days. The Director shall then establish a modified
Compliance Boundary which will be done as a
modification to the Permit.
The REVIEW BOUNDARY for this disposal system is
specified by regulations in 15 NCAC 2L, Groundwater
Classifications and Standards. A REVIEW BOUNDARY is
established around disposal systems midway between
the Compliance Boundary and the perimeter of the
waste disposal area. When the concentration of any
substance equals or exceeds the maximum allowable
concentration of that substance at the REVIEW
BOUNDARY, as determined by monitoring, the Permittee
shall either (i) demonstrate, through predictive
calculations or modeling, that natural site
conditions, facility design and operational controls
will prevent a violation of standards at the
Compliance Boundary, or (ii) submit a plan for the
alteration of existing site conditions, facility
design or operational controls that will prevent a
violation of standards at the Compliance Boundary,
and implement that plan upon its approval by the
Director.
3.) Any additional groundwater quality monitoring, as
deemed necessary by the Division, shall be provided.

Mr. William H. Mull
February 6, 1992
Page 4
A supply of forms (GW-59) on which the analytical results
must be reported are attached. Instructions are provided on
the reverse of the white copy of each 4-part form. The
analytical results should be sent to the address shown at the
top of the form and are due in our Raleigh office no later
than the last working day of the month following sample
collection.
If you have any questions, please do not hesitate to
contact me at [phone].
Sincerely,
Laura Kay Dechant
Hydrogeologist
LKD/gc
Attachments
cc: Bob Cheek
Betty Wilcox
Mark Fender

TAN 30 192 16:34 ENG ?42 P01
1wLAW eNaiN111115"1Na
gwiechniCal, eny1m mental & Watft cdjon metenaY9 oaneultwtS
FOUR INTERCHANGE BOULEVARD
GREENVILLE, SOUTH CAROLINA aged?
[phone]
FAC'S YA �.-E COVER SBEET
Phone 803 j288-5116 FAX [phone]
Date: _ ! .
From �4 M
Please deliver to.
Time-. b - 2
;IAM 3 01932
Firm Dept.
J
City
�4,,,,1\ State _--
r._,_..�,L
FAX Number ` 2S Telephone
Number of Pages (including this sheet) 2-1
!ON
Remarks
if you have arU.Woblerns receiving this irarsmittaj,.Rlease :rail 803/288-5116.

TAN 30 ' 92 16: 34 1 fahl ENG V� _ _ 742 P02
LAW ENGINEERING
GEOTECHNICAL, ENVIRONMENTAL
8 C014STRUCTION MATERIALS
C014SULTANTS
January 30, 1992
Metropolitan Sewerage District
Buncombe County, North Carolina
Triannual Sampling Analytical Methods
°.�: Engineering Job Number 2490444501
ANALYSIS
EPA METHOD NUMBER
NO3
353.2
AMONIA NITROGEN
350.1.
TOTAL ®ISM=LVED SOLIDS (TDS)
160.1
TOTAL SUSPENDED SOLIDS (TSS)
160'.2
TOTAL ORGANIC CARBON (TOC)
415.1
TOTAL COLLII=ORMS
SM909A
CHLORIDE
325.3
ARSENIC
7060
CADMIUM
7131
LEAD
7421
BARRIUM
CHROMIUM
6010
7191
MERCURY
7470
SILVER
7761
SELENIUM
7740
VOLATILE ORGANIC COMPOUNDS _(VOC) _. -_- - -_.
_ __. 502.2✓
** QAJQC samples will be collected and analyzed for VOC's method 502.2
1
UR INTERCHANGE BOULEVARD
)REENVILLE, SOUTH CAROLINA 29607
31 288.511 S
306 WEST HAYWOOD STREET, SUITE 2
ASHEVILLE, NORTH CAROLINA 28801
[phone]

490
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
February 1, 1991
MEMORANDUM
TO: Cecil G. Madden, Jr.
Engineering Management Unit
Construction Grants Section
THROUGH: Bob Cheek
FROM: Gale Johnson 4411-(
SUBJECT: Buncombe County MSD
Ash Disposal in Existing Sludge Lagoon
EPA Project No. C370391-08
GW90192
The Groundwater Section has reviewed the above referenced
project and has the following comments:
1. The three (3) existing monitor wells shall be sampled
every February, June, and September for the following
parameters:
VINO (10.0) rAmmonia Nitrogen
✓TD� (500.0) -TOC
,,,pH (6.5-8.5 standard units) Water Level
'Chloride (250.0) Total Coliforms (1/100ml)
C.� Arsenic (0.05 barium
�n /Cadmium (0.005) Chromium (0.05)
,/Lead (0.05) Mercury
Selenium Silver
T..S.S. (Total Suspended Solids)
Volatile Organic Compounds - In September Only (by
method 1 or 2 below)
Method 1: Method 6230D (Capillary - Column), "Standard
Methods For The Examination of Water and
Wastewater", 17th ed., 1989
Method 2: Method 502.2 "Methods For The Determination
Of Organic Compounds In Drinking Water", U.S.
EPA - 600/4-88/039
The measurement of water level must be made prior to
sampling for the remaining parameters.
n
J1!

I
I
The measuring points (top of well casing) of all
monitoring wells shall be surveyed relative to mean sea
;level (M.S.L). The depth of water in each well shall
'be measured from the surveyed point on the top of the
casing. The water level elevations shall then be
,determined relative to M.S.L..
;The numbers in parentheses represent the maximum
;allowable concentrations.in groundwater for the
;various analytical parameters, as specified in 15
NCAC 2L [Groundwater Classifications and Standards].
:Unless otherwise specified, the units for these
;concentrations are expressed as milligrams per liter.
r
JIf TOC concentrations greater than 10 mg/1 are detected
?in any downgradient monitoring well, additional
sampling and analysis must be conducted to identify the
!individual constituents -comprising this TOC
!concentration. If the TOC concentration as measured in
!the background monitor well exceeds 10 mg/l, this
concentration will be taken to represent the naturally
occurring TOC concentration. Any exceedances of this
naturally occurring TOC concentration in the
downgradient wells shall be subject to the additional
sampling and analysis as described above.
If any volatile organic compounds are detected by
method 6230D, or the equivalent method 502.2, then EPA
methods 604 and 611 must also be run to detect other
organic compounds which may be present. The results of
all analyses specified in the monitoring requirements,
including 604 and 611 if required, must be submitted
simultaneously.
The results of the sampling and analysis shall be sent
to the N.C. Division of Environmental Management on
Form GW-59 [Compliance Monitoring Report Form] every
March, July, October.
2. -The Compliance Boundary for the disposal system is
specified by regulations in 15 NCAC 2L, Groundwater
Classifications and Standards. An exceedance of
Groundwater Quality Standards beyond the Compliance
Boundary is subject to the penalty provisions
applicable under General Statute 143-215.6(1)a. The
sale of property,' by the Permittee, which is within or
contiguous to the disposal site, may alter the location
of the Compliance Boundary.
For facilities permitted prior to December 30, 1983,
the Compliance Boundary is established at a distance of
500 feet from the waste disposal lagoon, or the
property boundary, whichever is less.

If the title to any property which may affect the
location of the Compliance Boundary is changed, the
Permittee shall notify the DEM Director within 14 days.
The Director shall then establish a modified Compliance
Boundary which will be done as a modification to the
Permit.
!The REVIEW BOUNDARY for the disposal system is
,specified by regulations in.15 NCAC 2L, Groundwater
,Classifications and Standards. A REVIEW BOUNDARY is
!established around disposal systems midway between the
;Compliance Boundary and the perimeter of the waste
,disposal area. When the concentration of any substance
lequals or exceeds the maximum allowable concentration
!of that substance at the REVIEW BOUNDARY, as determined
jby monitoring, the permittee shall either (i)
;demonstrate, through predictive calculations or
jmodeling, that natural site conditions, facility design
and operational controls will prevent a violation of
standards at the Compliance Boundary; or., (ii) submit a
,plan for the alteration of existing site conditions,
jfacility design or operational controls that will
!prevent a violation of standards at the Compliance
!Boundary, and implement that plan upon its approval by
;the Director.
i
t
3. }Any additional groundwater quality monitoring, as
;deemed necessary by the Division, shall be provided.
I
GJ/hl
i
cc: Do.,
Central Files
Permit Issuance Files

�w
State of North Carolina
Department of Environment, Health, and Natural Resources
! Division of Environmental Management
! 512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Gov emor George T. Everette, Ph.D.
William W. Cobey, Jr., Secretary Director
4
July 16, 1990
t -
r
Mr. William H. Mull
Metropolitan Sewerage District of Buncombe County
Post Office Box 8969
Asheville., N.C. 28814
Dear Mr. Muill :
SUBJECT: Ash Storage Lagoon
Buncombe County
GW90192
I
As part of the Division of Environmental Management's
comprehensive approach in addressing the impact of waste
treatment, storage, or disposal projects -on the environment,
your permitiapplication has been forwarded to us for assessment
of the potential impact of the project on groundwater quality.
Our initial review indicates that the data submitted is
not sufficient to make this.assessment.
1 .
Before{your application can be processed therefore, you
are requested to submit the following information to the
GroundwaterlSection.
1. Information as to the presence or absence of any wells
located within 500 feet of the waste treatment/disposal
facility. Any such wells should be accurately located
on the site map, and labeled as to their primary usage
(e. drinking water, monitoring, etc.).
2. A'hydrogeologic description of the subsurface, to a
depth of 20 feet or bedrock,. whichever is less. The
number of borings shall be sufficient to define the
following for the area underlying each major soil type
- atI, the disposal site:
f
Pollution Prevention Pays
I
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
1

(i) significant changes in lithology underlying
the site; I
(ii) the vertical permeability of the
unsaturated zone and the hydraulic
conductivity of the saturated zone; and
(iii) depth to the mean seasonal high water table
(if definable from soil morphology or from
evaluation of other applicable available
data).
3. It should be noted that as per 15A NCAC 2H .0219 (e),
waste shall not be applied or discharged onto or below
the land surface when the vertical separation between
the waste -and the seasonal high water table is less
than one foot. If the area to be utilized has a
separation of less than three feet, a demonstration
must be made using predictive calculations or modeling
methods, acceptable to the Director, that such
placement will not result in contravention of
classified groundwater standards.
4. Boring logs and well construction details for all
ekisting monitoring wells. Such information should
include ground surface elevations at each well location
and static water level measurements.
Please feel free to contact the Groundwater Section, at
[phone], if clarification or information is required.
T
Sincerely,
M. Gale hnson
Hydrogeologist
Permits Group
MGJ/ja/90192.
cc: orb. n,:v:e►vx Hg'ona Gro-??C'S�aer Stxpetrvi
Cecil G. Madden, Jr. Construction Grants ec i
Central Files
Permit;Issuance Files
Law Engineering
1100 Thousand Oaks Blvd.
Golden!0aks Business Park
\6,
Greenville South Carolina 29607
JUL lr 5 1990
Groundwater Section
4sheville Regional Office

I
REVIEW BY
FACILITY NAME
LOCATION ,
TYPE OF DISPOSAL
DESCRIPTION OF F
GROUNDWATER SECTION ��-�--,�
DIVISION OF ENVIRONMENTAL MANAGEMENT GW #[L— �
RD OF WASTE DISPOSAL PERMIT APPLICATION REVIEW
a
DATE ���. o FIELD INVESTIGATION ? Y
COUNTYi�co��.�� ��
( LAGOON, ETC.)
fi.S4 &'510054
DESIGN CAP. (GPD )-
..� iv q
SIZE OF IMPOUNDMENT ( FT. SQ) o► c r S & / OR S¢E OF APPLjCATION AREA
HMON. SLUDGE MUN. W. WATER: PRIMARY []SECONDARY. TERTIARY
[]IND• SLUDGEIT�.. W. WATER OTHERS
DISTANCE FROM WASTE •SOURCE TO NEAREST: STREAM
FT., WELL FT.
FOR WELL: TYPE OF USE . DEPTH
PUMP RATE ( EST. )
WHAT DESIGN CONDITIONS WILL REDUCE / INCREASE CHANCE OF GW CONTAMINATION:
I
T NATURAL SITE
I
WILL REDUCE / ING�REASE CHANCE OF GW CONTAMINATION: w
[p�
A " a G,,._► c _ ��� I � 11 r->
DEPTH TO: BEDROCK "'1- S FT. ,SEASONAL HIGH W. T.
—O_ FT. , ANNUAL W. T. FLUX : FT.
SURFICIAL AQUIFER BEDROCK / ARTESIAN AQUIFER
GEN. LITHOLOGY v,* _ fl.
HYD. CONE. 1G FT./DAY MEASURED FT MEASURED
ESTIMATED /DAY
THICKNESS /� a ESTIMATED
NO. OF MONITOR WELLS: PROPOSED: UP DOWN
;EXISTING: UP�_ DOWN --,a_
FROM WORKSHEET: SITE NUMERICAL DESCRIPTION = �` ��
T 1 2 3 4 5 b GA 6B
SITE GRADE (HYDROGEOL.) _ ® ITUATION GRADE _
PROPOSED SAMPLING SCHEDULE & PARAMETER($) :
X n A ! r-_ . .
..- i
IT
ZIN
mng*wm lwiww&f[�lIII_i
r'ilaw
r
OJ'
1 f;

i
WASTE DISPOSAL . -:RMIT APPLICATION REVIL.. WORKSHEET .
Foatty: �. CIS Q
roun�'
Vif
.HVIgWgr ;
C '
Orife : � j
Mimi
Determine the dktonce Point volts 0 1
on Pond between can- 2 J 4 6 6 7 8 9 b /
'Q0
tominotion source and Distance In 2000
ote r supply (Vwel Of I 1000 - 20M 150 - 299 78 - 149 50 74 JS - 4p 20 - 34 10 - 19 0-9
-9 D+donce
wPt. Volue
stroom). CWonceh 62004 100)-3100 251-Am 1 1 (Step 1)
�hwle the depth
to the water lable
below boss of con-
lorninolbn Source
more than 5 % of
the year.
� water
table gradient
from contomh-
atlon sRe
Stec l
+mate of
.rmeobHlry-
sorptlon for the
waste disposal stle.
O
bet J 100 - 6200 601 - 1000 161 - 2S0 61 - 100 -160 JI-60 0 - JO
Note- Ilf water Cobb h perrmeoble bedrock pt. enolue -6. in poorly permeable bedrock
Pt. Value . 4
Pant slue 0 1 2 3 4 b 6 7 B 0
Meters 00+ 30d0 20.29 12-29 8-11 5-7 3-4 15-25 6-1 0
Feet 200+ 91-200 61-90 36.60 26.35 16-25 9-15 3a 0.2 0
Water table
Grader* Gradient
Grakiert
Gtodettt Gradient
gradient and
flow dtictbn
away ham almost
lea than
lea than greater
oil water flat
2 percent
2 percent thm 2
supplies that
toward
towoed percent
ore closer
water
water tad
than 1000
supply btd
supply water
meters
not the
and is the wppfy,
:i
ontictpatod
articfpoted but rot
direction of
direction of to antf.
now
}low clpoted
j
direction
Of flow
C/) A flow - Pock > t00low
leer be
Ind
skrfaoe
L
�, eC
(3) l cck+m- - bedrock
;
poorly
Permeable
LL
O
O�
(4)11 column - bedrock -
O
or eery
Permeable
ir- � C
Clay with
no more Said wlfh Said with
than50% 15-30% low than
rtr_
Grader
Pam«
than 2
percent
toward
Water
and Is the
anticipated
dWoctlon
of flow
Clean
gravel or
CJeon f -w coarse
--�` f— Pt-
W.I. (Step 2)
Gradient Pt, Valle
(Step 3)
More than 30
OA
2A
4A
6A
ISl1
9A
Moe than 95
I
I'
II
I
II
I II
I
II
I
11
25-29
OB
IC
1D
2F
3E
4G
F 6E
7F
OE9
OM
75.94
-24
OC
2C
lE
30
4D
5E
5G 6F
7G
8F
9H
9N
60 -74
15 - 19
CO
38
1F
4C
4E
6C
SH 7D
7H
t!G
91
90
46 - 59
10 -14
OE
40
2D
68
4F
6D
51 7E
71
OD
91
9P
26 - 45
3 - 0
is
6B
2E
7B
5C
7C
5.1 ED
7.1
9E
9K
9a
10 - 27
Less than J
18
EB
3C
8C I
5D
9B
5K 9C 1
7K
9F I
9L,
9P
Leo than 1
Bedrock of land surloce; I. 57. I I .92
wore : tr nedrock at land surface, use 10 (plus appropnlote letter)
31+a 5
Degree of conbdenee In accuracy of Values A . Very confident
B . fairly confident
C -wish low conflderoe
51eo 6e
Point of concern with regard to car.—,.oM source h : W . near by wel
S - spring / stream
B - perimeter of comspsartoe
Slla�► Addllfo al QudM w (Chcb Only One)
D . Cone of dePreolon of nearby pumping wel has.
Of r,A Ike►y. influence cortamhav flew
E - Dktance in Step 1 based on separation from
oor4amha11 puma Kther than point source
F • Wool* source in Pourtd,w er discharge area
"VA m1Nnd grouxrwaten oar OnlillatiOn at depth / dMan-voe
i
K - Meo underlain by coverois lirmestone
6
Y�I
Category
(Step 4)
a
ConAdence
(Step 5)
z
Point of Cone -ern
(Step 6A)
M - Fl ld mondirtg Under dire higlify 1 kely
Quolrfbr
P - Slue has poor petcoiatlon potential (value of 3 of Isla In Slop 4) (Step 68)
O - Wade sauce In groundwater recharge area
T - Water table in wry Ngtty flowed of oaverou rock
y - We underlain by 1 or more artesian oquirem

WASTE DISPOSAL PERMIT APPLICATION REVIEW WORKSHEET (CONT.)
Ste Wniorlcol dcucrbtbn /�
I _� �L � .6
Told Stop 1 Sbp 2 Step J Sep 4 Stop 6 Step 6A Stop 68
i
( Add Steps 1- 4 (Omit lettws )
SNte Grade 8os•d on Hydrogeoloplc Porarnetem
S1!>z.4
Hazard Potential MIaft Identltwr ( WM )
( Choose One) O G 1
B E H i
A C F
HPMI
I
1+22i i
(1) MxneflCal sme
Oes«btbn (ham Step 7 )
I
Q) PAR VAWE (Stop• s)
STUATKA RATING : (1) - f2)
(table below)
SITUATION GRADE
n? $ft mo cal M
(i • table below)
,4t•o 10 SRUATION GRADE
t e moo o n{
(see table below)
Tout
Penn / Sorp. KMA
2
(� •
2p
in
SITUATION RATING TABLE
To be used t« Step V ( Natural) and Stop 10 ( Modllled )
(step 10)
SITUATION RATING PROBABILITY OF
(iCombkned Vol-) CONTANATI(M DEGREE OF ACCEPTABILITY GRADE
N
MI
B or les krproboble Probablyaoo•ploble A
-7 to J 9 Probobty 000spbble « B
Jb.J �aN
9 Aoosptano• l+roerbtr C
I44 to #7 F�obaby Pmbot* ur"oosp4abl• D
•B«more VeryPnobable Ahxdcertaintoto be F
unocceptable
The prob"ty of ccnlomomka an ham sMuatlons having vokme be 17 and - 7 Is dlfflCllt to oof•poiQ•
eotlsfoctorfyner . Tt•for•,1Ns range
of vakws lepnseMed by grad« B and C. Y destined «V y by a 4uatbn mok
Aoc•ptaa• or r•)•ctlon d as stle liar the Mended purpose Y a r•sponsblAly of the particular r pulotmy operncy
and may,d•pend oft sp•cld r•atkem•nts of the agency Or an feaebWy and execution of approved
enghee ft of 0 this ( Stage 4).

State of North Carolina
Department of Natural Resources and Community Development
Asheville Regional Office
James G. Martin, Governor Ann B. Orr
William W. Cobey, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
j WATER QUALITY SECTION
` ,July 3 , 1990
MEMO
To: Bill Hoffman, Supervisor
Engineering Management Unit
I Construction Grants
Through: Roy M. Davis, Regional Supervisor1�
Division of Environmental Manageenneent
,Forrest R. Westall
Regional Water Quality Supervisor
From: Max. L. Haner ,
Environmental Chemist: /
Subject: Staff Recommendations
Authorization for Disposal of Ash
in Existing Sludge Lagoon
MSD of Buncombe County (NCO024911)
EPA Project Number C370391-08
The MSD proposal for use of the existing 8 acre wwtp sludge lagoon for
disposal of ash from the sludge incinerator has been reviewed and the
following comments and recommendations are offered. It is noted that
this proposal is consistent with conditions contained in MSD's
.11/17/89 Authorization to Construct: for its sludge dewatering and
incineration project which required this separate submittal for final
disposal of the ash. At a 40 MGD design flow (current average flow
27.8 MGD; see attached DMR summary), MSD proposes to add approximately
67,146 gpdjof 5% ash solids to the lagoon; expected to dewater to a
50% solids1content (14 dry tons ash/day - 204 cubic feet). Currently
the lagoon1has a total volume of some 8.68 mill -ion cubic feet (64.92
million gallons), having been modified from original volume of some
6.93 million cubic feet (52 million gallons) in 1988 by increasing the
height of the dike 5 feet. The lagoon was relatively full of solids
prior to modification and since none of these solids have been removed
from the lagoon-, an extremely conservative estimate of the available
capacity for proposed ash disposal would be equal to the additional
volume created by the modification; approximately 1.74 million cubic
feet (13 million gallons). If managed properly and considering that
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Page 2
Bill Hoffman
July 3, 1990
(1) the premodified lagoon was not uniformly full and (2) that there
may be some additional dewatering of the wastewater sludge created by
the addition of the heavier weighted ash, the expected use of this
lagoon for ash disposal may well exceed the projected 7.31 years
created by the 1988 lagoon modification. There is little agreement
from this review that the life of the lagoon without cleaning would
reach 20 years.
Therefore, it is recommended that use of the existing sludge lagoon
for ash disposal be approved as requested. As there remains some
question of the effective life of this lagoon at the expected usage,
it is further recommended that this approval be conditioned to require
within 24 months of this approval, development of a formal plan for
removal and final disposal of solids from this lagoon, or otherwise
handling ash generated by the incinerator. The recommendation
submitted by ARO's Groundwater Section for another downgradient
monitoring well at the 500 foot Compliance Boundary is fully supported.
Should you have questions or wish to discuss this matter in more
detail, plea'se contact me.
xc: Cecil Madden

LAW ENGINEE..,-ANG
FOUR INTERCHANGE BOULEVARD
GREENVILLE, SOUTH CAROLINA 29607
Telephom [phone]
Facsimile [phone]
FACSMU COVER SHEET
Date: G -o
� � Time: ��Z'• �� AM/PM
. ^, ::......' ,
From:
Please deliver to:
..Namez°
Firm
'Fax 'Number
'Total Number of Pages Being Transmitted (including cover sheet):
Description/Remarks AV ki 1A-e
If you have any problems receiving this transmittal, please call [phone] immediately.
]'hark youl
0
T Od 6t76 856cL L6c C-08 ' JN I aE]3N I DN3 MUD SS : T T 06, S T NI f
A

EnWRIGHT
E N V I R 0 P4 M E N T A L
CERTIFICATE OF ANALYSIS
CLIENT: Law Engineering
PROJECT: CVE-2377
DATE SAMPLED: 05/01/90
DATE RECEIVED: 05/02/90
LAB CERTIFICATION N0:
23127
DATE REPORTED: 06/07/90
LAB NO.:
90-F165-01 90-F165-02 90-F165-03 90-F165-04
90-FI65-05
SAMPLE1b:
Bailer Rinse AW:g — NW_3
_ R-1 —JLIR31ank
Pars:
Total Dissolved Solids
----
180
52 ----
PH (units)
6.1
6.6
517 T- -
Chloride
---- 23
9
7 --"-
Nitrite Nitrogen
0.01
<O,Oi.
<0.01 -�--
Nitrate Nitrogen
---- 9.5
0.6
<0.1 ----
sulfide
-- <1
<1
<1
,Lead
---- 0.012
.13
0.010 _as_
'l
,,.*'Mercury iug/1)
Selenium
---- <015
---- <0.010
<0.5
<0,500
<0.5 ----
<0.050 µ�w
l
Arsenic
---- <0.405
<0.025
<0.005 ----
11 ` %I
Silver
0,001
0.001
<0.001 -
Cadmiun
_--_
<0.0005
0.0006
0.00 --µ
Barium
---- 01861
m]
0.213 ----
Chronium
0.061
0.478
0.035 ----
Ammonia Nitrogen
---- <0.3
0.96
<0.3 ----
Total Organic Carbon
<1
1-""
Total Coliform
,wµi <1
<1 *
<1 -'--
(Colonies/1001al)
* i8o confluent non-coliform growth,
2 Enwright Environmental Consulting Laboratories, Inc.
(25 Woods Lake Rd. 29607) PO Sox 17467 Greenville, SC 29606 803 225-0707
.lad E't?6 826L L6c. 208 ' SN I dEEN I ONEI JIU-1 9S : T T 06, S T Nnf

Lacy Engineering
GVE-2377
Laboratory Report, Page 3
LAB NO.: 90-PI65-01 90-F165-02 90-F165-03 90-F165-04 90-F165-05
SAMPLE_ID: Bailer Rinse U-2 U-3 MW-1 TriD Blank
Acid Extractables by Method 8270; (ug/1)
2-Chloropbenol. ----
<10
<10
<10 ---_
2,4-Dichlorophenol --
<10
<10
<10 ----
2-Hethyl-4,6-Dinitrophenol ----
<30
<30
<30 ----
2,4-Dimethylphenol --
<10
<10
<10 ----
2,4-Dhitrophenol ----
<45
<45
<45 ----
2-Nitrophenol ----
<10
<10
<10 ----
4-Nitrophenol ----
<10
<10
<10 ----
P-Chloro-H-Cresol ----
<10
<10
<10 ----
Pentachlorophenol ----
<10
<10
<10 ----
Phenol ----
<10
<10
<10 ----
2,4,6-Trichlorophenol ----
<10
<10
<1.0 ----
�l iL ractables by..Method 82701
(ng/1)
Acenaphthene ----
<10
<10
<10 ----
Beuidine ---
<50
<50
<50 ----
Bis(chloromethyl)ether
<10
<10
<10 ----
Bis(2-chloroethoxy)methane ----
<10
<10
<10 ----
Bis(2-chloroethyl)ether ----
<10
<10
<10 --
Bis(2-chloroisopxopyl)ether----
<10
<10
<10 ----
Bromophenyl Phenyl Ether ----
<10
<10
<10 ----
Chloroethyl Vinyl Ether ----
<10
<10
<10 --�T
Chlorophenyl Phenyl Ether ----
<10
<10
<10 ----
2-Chloronaphthalene ----
<10
<10
<10 ----
3,3-Dichloxobet Zidine ----
<10
<10
<10 ----
2,4-Dinitrotoluene ----
<10
<10
<10 ----
2,6-Dinitrotoluene ----
<10
<10
<10 ----
112-Diphenylhydrazine ----
<10
<10
<10 ----
Fluoranthene ----
<10
<10
<10 ----
Hexachloroben2ene ----
<10
<10
<10 ----
Hexachlorobutadiene ----
<10
<10
<10 ----
Hexachlorocyclopentadiene ----
<1.0
<10
<10 ----
Hexachloroethane ----
<10
<10
<10 -µ -
Isophrone ----
<10
<10
<10 ----
Led sys 626z LGE 2rae•9Nid33N19N3 MH7 9s:TT e61 51 NFIt

Law Engineering
OVE-2377
Laboratory Report, Page 4
LAB NO.: 90-F165-01 90-F165-02 90-PI 65-03 90-P165-04 90-F165-05
SAXPLE ID: Bailer-Rin. MW-2 MW-KW-1 Trip Blank
BIN Extactables by Motbod 9270: (ug/1) Cont.
Naphthalene ----
<10
<10
<10 ----
Nitrobenzene ----
<10
<10
<10 ----
N-Nitrosodimethylamine ----
<10
<10
<10 ----
Il-Ilitrosodiphenylamine ----
<10
<10
<10 -�
N-Nitroso-di-n-Propylamine ----
<10
<10
<10 ----
1,2,4-Trichlorobenzene ----
<10
<10
<10 -----
Bis(2-ethylhextl)Phthalate ----
<10
<10
<10 ----
Butyl Benzyl Phthalate ----
<10
<10
<10 ----
Diethyl Phthalate ----
<10
<10
<10 ----
Dimethyl Phthalate ----
<10
<10
<10 _-__
Di-n-Butyl Phthalate
<10
<10
16
Di-n-Octyl Phthalate ----
<10
<10
<10 ----
Aeenaphthylene ----
<10
<10
<10 ----
Anthracene ----
<10
<10
<10 ----
Denu (A)Anthracene ----
<10
<10
<10 ----
Benzo(Bj luoranthene ----
<10
<10
<10 ----
Benzo(K)Fluoranthene ----
<10
<10
<10 4 -_
Benzo(GHI)Perylene - --
<10
<10
<10
Benzo(A)Pyrene ----
<10
<10
<10 ----
3,4-Benzofluoranthene ----
<10
<10
<10 ----
Chrysene µ---
<10
<10
<10 ----
Dibenzo(A,R)Anthracene ----
<10
<10
<10 ----
Pluorene
<10
<10
<10 ----
Indeno(1,2,3-CD)Pyrene ----
<10
<10
<10 -�
Phenanthrene ----
<10
<10
<10 ----
Pyrene ----
<10
<10
<10 ----
Aldrin ----
<10
<10
<10 ----
Dieldrin ----
<10
<10
<10 ----
Chlordane ----
<10
<10
<10 ----
O,P-DDE ----
<10
<10
<10 ----
O,P-DDD ---w
<10
<10
<10 ----
0,P-DDT ----
<10
<10
<10 ----
P,P-DDE ----
<10
<10
<10 ----
P,P-DDD ----
<10
<10
<10 ----
P,P-bDT ----
<10
<10
<10 -----
b«d 6176 826L LGE 2138 ' JN I DEN I ONE MU-1 LS : T T 86 , S T Nnf

Law Engineering
GVE-2377
Laboratory Report, Page 5
LAB NO.;
90-F165-01 90-F165-02
90-F165-03
90-F165-04 H 4 165-05
SAMPLE ID:
Bailer Rime.
AW-3
KW-1 _ J, io Blank
N Extractables by
Method 8270: (ug/1) cont.
Endosulfan I
---- <10
<10
<10
Endosulfan II
---- <10
<10
<10 ----
Endosulfan Sulfate
---- <10
<10
<10 ---
Endrin
---- <10
<10
<10
Endrin Aldehyde
---- <10
<10
<10 ----
Heptachlor
---- <10
<10
<10 ----
Heptachlor Epoxide
---- <10
<10
<10 ----
A-BAC
---- <10
<10
<10 ----
B-BHC
---- <10
<10
<10 ----
Lindane
---- <10
<10
<10 ----
D-BUC
<10
<10
<10 ----
ToXaphene
-- - <10
<10
<10 ----
Aroclor 1016
---- <150
<150
<150 --
Aroclor 1221
---- <150
<150
<150 ----
Aroclor 1232
---- <150
<150
<150 ----
Aroclor 1242
---- <150
<150
<150 ----
Aroclor 1248
---- <150
<150
<150 ----
Aroclor 1254
-_ - <150
<150
<150 __-_
Aroclor 1260
---- <150
<150
<150 ----
Aroclor 1262
---W <150
<150
<150 ----
The above results are reported in milligrams per liter unless otherwise noted.
Analytical methods are those approved by the U.S. Environmental Protection
Agency.
kgb
Respectfully submitted,
ENWRIGHT ENVIRONMENTAL
CON - TING LABORATORIES, INC.
Charles H. Reece, Ph.D.
Laboratory Manager
S8d 6V6 826L L6 208 ' JN I 33N I JN8 MUD LS : T T 06, S T Nnf

L 4 .
LAW ENGINEERING
geotechnical, environmental & constriction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
[phone]
October 27, 1989`
Or; n 1989
Matrfa,
Metropolitan Sewerage District of Buncombe
Sewerage I}ist>7ct
of Couut3!
P.O. Box 8969
Asheville, North Carolina 28814
Attention: Mr. William H. Mull
0
Subject: Results of Ground -Water and Surface Water
Chemical Analysis
Metropolitan Sewerage District
Asheville, North Carolina
Law Engineering Job Nu>ber, •AVE-2265 ,
Gentlemen:
As authorized by your acceptance of our. -York Authorization Sheet,
dated September 27, 1989, Lauz_H gineerin4 has completed the sampling
and chemical analysis of thte ground water from the one piezometer
and the two surface water springs/seeps at the site in Asheville,
North Carolina.
The field sampling effort, which was conducted by Mr. George
Maalouf, entailed the following tasks:
1. On August 15 and 16, 1989 the appropriate sampling
containers were assembled and prepared with the necessary
preservatives. The Law Environmental National Laboratory in
Kennesaw, Georgia was informed of the sampling.event and the
date they would be receiving the samples.

Metropolitan Sewerage District
Law Engineering Job Number AVE-2265
October 27, 1989
Page 2
2. On August 16, 1989 three samples were collected from the
piezometer and from the two springs/seeps. Prior to
collection of the ground -water samples the bailer,
constructed of a 3 foot long 1.6 inch diameter teflon pipe,
was decontaminated with the following procedures:
a') Laboratory detergent and distilled water rinse;
b) Dilute hydrochloric acid rinse;
c) Pesticide grade Isopropanbl rinse; and
d) Distilled water rinse:
Ground -water pH and specific conductivity were measured in the field
at the time of sampling.
The surface water samples from the springs/seeps were not of
sufficient depth to allow submersion of the sample containers, and
therefore depressions were scooped out of the channel bottom and
allowed to clear prior to sampling.
3) The samples were collected into the appropriate vessels
(VOA vials and 1 liter glass and plastic jars), marked with
identifying numbers and shipped in a refrigerated container
by overnight carrier to the Law Environmental National
Laboratories in Kennesaw, Georgia for analysis. Appropriate
chain -of -custody records were maintained.
4) The samples were analyzed for halogenated and aromatic
volatile organics (EPA Methods 601 and 602), Acid Base
Neutral Extractables (semi -volatile, EPA Method 3510/8270)
and for eight selected metals (arsenic, barium, cadmium,
chromium, lead, mercury, selenium, silver).
LAW ENGINEERING

Metropolitan Sewerage District
Law Engineering Job Number AVE-2265
October 27, 1989
Page 3
Laboratory analyses indicate that trace concentrations of 1,2-
dichloroethane and chlorobenzene are present. (The trace levels of
1,2 dichloroethane may be due to possible laboratory contamination.)
Concentrations of all other parameters tested was below North
Carolina's Maximum Contaminant levels (MCL's) and therefore no
direct regulatory concern is implied.
We appreciate the opportunity to provide our professional services
during this -project. If you have any questions concerning this
report; please do not hesitate to call.
Sincerely,
LAW ENGINEERIN97,
Robert E. MacPhee
Hydrogeologist
(--V74
Thomas L. Lammons, P.G.
Environmental Services Manager
/jgw.b

LAW ENVIRONMENTAL, INC.
112 TOWNPARK DRIVE
KENNESAW GEORGIA 30144-5599
404-421-3400
September 12, 1989
Law Engineering, Inc.
1100 Thousand Oaks Blvd.
Greenville, SC 29607
Attention: Tom Lammons
LE Job Number: AVE-2265
LENL Job Number: 12024
t
Subject: Chemical Analysis of Samples Received
on 8/17/89
Dear Mr. Lammons:
Law Environmental National Laboratories has completed its
analysis of your samples and reports the results on the following
pages. These results relate only to the contents of the samples
as submitted. This report shall not be reproduced except in hill
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
MAENVIR:ONMENITAL S
Zhanna Geskin
GC/MS Laboratory S ervisor
Clifford H. McBride
QA/QC Coordinator
Attachment: Data Report
Invoice

.d ENVIRONMENTAL NATIONAL LABOI
TEST DATA REPORT
RIES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-01
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Cust. No. :
--- Sample Information ---
Station ID : MSD-WELL-1 Sampled Date/Time : 08/16/89 14:30
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
i
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270 N/A 08/21/89 JAS
Ext/Acid Extractables/W 3510/8270 N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane EPA 601 ug/l 1.0 ND 08/18/89 OL
Bromoform EPA 601 ug/l 2.0 ND 08/18/89 OL
Bromomethane EPA 601 ug/1 12 ND 08/18/89 OL
Carbon tetrachloride EPA 601 ug/1 1.2 ND 08/18/89 OL
Chloroethane EPA 601 ug/1 5.2 ND 08/18/89 OL
2-Chloroethylvinyl ether EPA 601 ug/1 1.3 ND 08/18/89 OL
Chloroform EPA 601 ug/l 1.0 ND 08/18/89 OL
Chloromethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Dibromochloromethane EPA 601 ug/l 1.0 ND 08/18/89 OL
1,2-Dichlorobenzene EPA 601 ug/l 1.5 ND 08/18/89 OL
1,3-Dichlorobenzene EPA 601 ug/l 3.2 ND 08/18/89 OL
1;4-Dichlorobenzene EPA 601 ug/l 2.4 ND 08/18/89 OL
Dichlorodifluoromethane EPA 601 ug/l 18 ND 08/18/89 OL
1,1-Dichloroethane EPA 601 ug/1 1.0 �N-D-�-1 08/18/89 OL
1,2 Dichloroethane EPA 601 ug/l 0.3 '—O,5.331-38 08/18/89 OL S
1,1-Dichloroethene EPA 601 ug/1 1.3 ND 08/18/89 OL
Trans-1,2-Dichloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2-Dichloropropane EPA 601 ug/1 1.0 ND 08/18/89 OL
cis-1,3-Dichloropropene EPA 601 ug/1 3.4 ND 08/18/89 OL
Trans-1,3-Dichloropropene EPA 601 ug/1 3.4 ND 08/18/89 OL
Methylene Chloride EPA 601 ug/l 2.5 ND 08/18/89 OL
1,1,2,2-Tetrachloroethane EPA 601 ug/l 0.3 ND 08/18/89 OL
Tetrachloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,1,1-Trichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Signed ` <

I ENVIRONMENTAL NATIONAL LABC
TEST DATA REPORT
.TIES
Date 09/12/89
Page 2
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Trichloroethene EPA 601 ug/1 1.2 ND 08/18/89 OL
Trichlorofluoromethane EPA 601 ug/l 3.2 ND 08/18/89 OL
Vinyl Chloride EPA 601 ug/l 1.8 ND 08/18/89 OL
Benzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Chlorobenzene EPA 602 ug/1 1.0 0---9i:7 08/18/89 OL
Ethylbenzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Toluene EPA 602 ug/1 1.0 ND 08/18/89 OL
-- GC/MS ANALYSIS RESULTS --
Isophorone EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethoxy)methane EPA 8270 ug/l 10 ND 09/11/89 MC
1,2,4-Trichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Naphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chloroaniline EPA 8270 ug/l 20 ND 09/11/89 MC
Hexachlorobutadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Methylnaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorocyclopentadiene EPA 8270 ug/1 10 ND 09/11/89 MC
2-Chloronaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethyl) ether EPA 8270 'ug/1 10 ND 09/11/89 MC
1,3-Dichlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
1,4-Dichlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
1,2-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Benzyl Alcohol EPA 8270 ug/l 20 ND 09/11/89 MC
bis(2-Chloroisopropyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachloroethane EPA 8270 ug/l 10 ND 09/11/89 MC
N-Nitroso-di-n-propylamine EPA 8270 ug/l 10 ND 09/11/89 MC
Nitrobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Nitroaniline EPA 8270 ug/1 50 ND 09/11/89 MC
Acenaphthylene EPA 8270 ug/l 10 ND 09/11/89 MC
Dimethyl phthalate EPA 8270 ug/l 10 ND 09/11/89 MC
2,6-Dinitrotoluene EPA 8270 ug/1 10 ND 09/11/89 MC
Acenaphthene EPA 8270 ug/l 10 ND 09/11/89 MC
3-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
Dibenzofuran EPA 8270 ug/1 10 ND 09/11/89 MC
2,4-Dinitrotoluene EPA 8270 ug/l 10 ND 09/11/89 MC
Fluorene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chlorophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Diethylphthalate EPA 8270 ug/l 10 ND 09/11/89 MC
4-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
4-Bromophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Phenanthrene EPA 8270 ug/1 10 ND 09/11/89 MC
Anthracene EPA 8270 ug/l 10 ND 09/11/89 MC
Signed e���'''� ��.

: ENVIRONMENTAL NATIONAL LABOR' .LIES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
Fluoranthene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
N-Nitrosodiphenylamine
Pyrene 4
Butyl benzyl phthalate
3,3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
bis(2-ethylhexyl)phthalate
Di-n-octyl phthalate
2-Chlorophenol
Phenol
2-Methylphenol
4-Methylphenol
2-Nitrophenol
2,4-Dimethylphenol
2,4-Dichlorophenol
Benzoic Acid
4-Chloro-3-methylphenol
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
4,6-Dinitro-2-methylphenol
Pentachlorophenol
--- SERIES 8000
Barium, Total
Mercury, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Lead, Total
Selenium, Total
Silver, Total
Total Metals Prep: Aqueous ICP
Total Metals Prep: Aqueous Furnce
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC.
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
20
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
50
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/l
50
ND
09/11/89
MC
EPA
8270
ug/l
50
ND
09/11/89
MC
EPA
6010
mg/l
0.1
ND
08/18/89
MC
EPA
7470
mg/l
0.0005
ND
'08/21/89
OL
EPA
7060
mg/l
0.005
ND
08/18/89
MC
EPA
7131
mg/1
0.002
ND
08/18/89
MC
EPA
7191
mg/l
0.005
0.006 ,-
08/18/89
MC
EPA
7421
mg/l
0.005
ND
08/18/89
MC
EPA
7740
mg/l
0.005
ND
08/18/89
MC
EPA
7761
mg/1
0.01
ND
08/18/89
MC
EPA
3010
N/A
08/17/89
HH
EPA
3020
N/A
08/17/89
GSP
Signed

ENVIRONMENTAL NATIONAL LABOF
TEST DATA REPORT
.tIES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-02
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Station ID
: MSD-S-1
Matrix
: W
Type
: GRAB
Collector
: GM
Remarks
--- Sample Information ---
Cust. No. .
Sampled Date/Time : 08/16/89 15:10
Received ate/Time : 08/17/89 10:00
Received-From/By : GM/CLM
Chain of Custody : 6473
Number of Containers : 6
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270
Ext/Acid Extractables/W 3510/8270
N/A 08/21/89 JAS
N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/l
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/1
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/1
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane.
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
0.3
[0..597.
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
._. EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA.
601
ug/l
0.3
1r9.7`?_`
08/18/89
OL
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Signed z�z

ENVIRONMENTAL NATIONAL LABOR
TEST DATA REPORT
JES
Date 09/12/89
Page 2
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
60l
ug/1
1.0
ND'
08/18/89
OL
Trichloroethene
EPA
601
ug/l
1.2
ND-
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/l
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
Benzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/l
1.0
E1 55a
08/18/89
OL
Ethylbenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Isophorone
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachloroethane
.EPA
8270
ug/1
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Signed

• ENVIRONMENTAL NATIONAL LABOID_:IES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-02
Project No. : AVE-2265
-.-- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Pyrene 1
EPA
8270
.ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate.
EPA
8270
ug/l
10
ND
09/11/89
MC
3.3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11./89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/l
0.1
0.1
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/l
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed ��

ENVIRONMENTAL NATIONAL LAB(.' ,IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-03
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-S-2 Sampled Date/Time : 08/16/89 15:45
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
0
--- Test Data ---
Parameter.............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/1
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/l
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/1"
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
.18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/1
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
�--��.6�
08/18/89
OL
Tetrachloroethee
EPA
601
ug/1
1.0
ND
+ 08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Signed

ENVIRONMENTAL NATIONAL LABOF .1ES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
Benzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Isophorone
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/1
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
,
Signed

ENVIRONMENTAL NATIONAL LABO
TEST DATA REPORT
.1ES
Date 09/12/89
Page 3
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/1
10
ND
0.9/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/l
0.1
ND
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/l
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/1
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/l
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed �l-

• ENVIRONMENTAL NATIONAL LABOFO IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-04
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : TRIP BLANK Sampled Date/Time : / /
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 2
Remarks :
0
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/1
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/1
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/1
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/1
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/1
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane/- o ,A-
EPA
601
ug/l
0. 3 73fam `1._53
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/1
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/1
2.5
ND
08/18/89
OL
1,1, 2, 2-Tetrachloroethane.e-'
EPA
601
ug/l
0.3
E2..1-3'6
08/18/89
OL
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,2-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
Signed -451, �/

ENVIRONMENTAL NATIONAL LABO .IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-41o9-o4
Project No. : AVE-2265
Test Data
Parameter...............................Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Benzene
EPA 602
ug/l
1.0 ND
08/18/89
OL
Chlorobenzene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Ethylbenzene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Toluene
EPA 602
ug/l
1.0 ND
08/18/89
OL
c
Signed

LAW ENVIRONMENTAL NATIONAL LABORATORIES
Project Number: AVE-2265
Project Name: Metro Sewarage,District
Lab Sample ID: 89-4109-01 Client ID: MSD-Well-1
COMPONENT
TENTATIVELY IDENTIFIED COMPOUNDS
VOLATILES
QUANT. SCAN EST. CONC.-
ION NO. AREA ug/1
2-Ethyl-4-methyl-1,3-dioxolane
87
1073
23189
65
3-Ethyl-3-pentanol
45
1206
742.17
210
Diisopropyl ether
45
1230
73606
200
.1-Chloro-5-iodo-pentane
69
1236
32834
92

o LAW ENVIRONMENTAL, INC.
NATIONAL LABORATORY
112 TOWNPARK DRIVE
KENNESAW, GEORGIA 30144
o [phone] Sq-(-loci _
PROJECT NAME 0
SAMPLIRS (SIG'NATUPt
CHAIN OF CUSTODY RECORD
SAMPLING NAME OF FACILITY: T jiv-4
INFORMATION
STREET ADDRESS:
CITY/STATE:
OB NO. In
w �Q�
_z .c
.J Q It p°.aN
Q H � •a a
F- Z MCP,` d, xa
ZIP:
/ G U O e O pb x �e� ,�
SAMPLING ATE e �D n I"' ILG ,pP �,�� �0 �.
m d W` O F0� Q \ Q \�� ��lb°c
TIME u O SAMPLE STATION DESCRIPTION p eA ; r, '�G \Q �� °ti y ,
Z ` LENL LAB NO. .
M 6 3111
l n � w r'I 14
�1 W t1 A- - 0,
fir►` n r310,1/ 4-9
RE 1 QUISHE BY
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
RECEIVED BYI
DATE/TIME
�(
11G010
IGNA U E)
U
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
RELINQUISHED BY:
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
R IVE T LABO DRY:
DATE/TIME
I17: bL
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
(S GNATUR
RECOVERY WE L - RW
DISTRIBUTION: ORIGINAL AND YELLOW COPIES ACCOMPANY SAMPLE SHIPMENT TO LABORATORY'.
SOURC[ RCRA MONITORING WELL - MW
PINK COPY R
AINED BY SAMPLERS.
YE LOW COPY RETAINED BY LABORATORY.
CODES: SOILSEDIMENT-SO
/
P106a
SLUDGE-SL
REMARKS:
e-
NPDES DISCHARGE - ND
E' to , (
DRINKING WATER - DW
u
HAZARDOUS WASTE -HW
SLIRFACF WATER -SW
mi

17 'j6yy�ed�
AL
LAW ENGINEERING
geotechnical, environmental & construction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
[phone]
October 13, 1989
State of North Carolina
Department of Natural Resources
and Community Development
Division of Environmental Management
Groundwater Division
P.O. Box 370
Asheville, North Carolina 28802-0370
Attention: Mr. Don Link
Subject: Surface and Groundwater Analytical Results
Metropolitan Sewerage District
Highway 251
Asheville, North Carolina
Law Engineering Job Number AVE-2265
Gentlemen:
Attached are copies of the analytical results of ground -water
samples collected from one boring and springs located on the
Metropolitan Sewerage District Plant property.
If you have any questions concerning the data submitted please do
not hesitate to call.
/kp.a
Sincerely,
LAW E NEERI
r
Robert MacPhee
Hydrogeologist
.� 2
Thdmas L: Lamm ns
Environmental Services Manager
i

I
c =.
LAW ENVIRONMENTAL, INC.
112 TOWNPARK DRIVE
KENNESAW GEORGIA 30144-5599
404-421-3400
September 12, 1989
Law Engineering, Inc.
1100 Thousand Oaks' Blvd.
Greenville, SC 29607
Attention: Tom Lammons
LE Job Number:. AVE-2265
LENL Job Number: 12024
Subject: Chemical Analysis of Samples Received
on 8/17/89
Dear Mr. Lammons:
Law Environmental National Laboratories has completed its
analysis of your samples and reports the results on the following
pages. These results relate only to the contents of the samples
as submitted. This report shall not be reproduced except in hill
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
A ENVIRONMENTAL S
Zhanna Geskin
GC/MS Laboratory S ervisor
Clifford H. McBride
QA/QC Coordinator
Attachment: Data Report
Invoice

ENVIRONMENTAL NATIONAL LABOR, LES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-01
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-WELL-1 Sampled Date/Time : 08/16/89 14:30
Matrik : W Received Date/Time : 08/17/89 10:00
Type,: GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270 N/A 08/21/89 JAS
Ext/Acid Extractables/W 3510/8270 N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane EPA 601 ug/l 1.0 ND 08/18/89 OL
Bromoform EPA 601 ug/1 2.0 ND 08/18/89 OL
Bromomethane EPA 601 ug/1 12 ND 08/18/89 OL
Carbon tetrachloride EPA 601 ug/1 1.2 ND 08/18/89 OL
Chloroethane EPA 601 ug/1 5.2 ND 08/18/89 OL
2-Chloroethylvinyl ether EPA 601 ug/1 1.3 ND 08/18/89 OL
Chloroform EPA 601 ug/l 1.0 ND 08/18/89 OL
Chloromethane EPA 601 ug/l 1.0 ND 08/18/89 OL
Dibromochloromethane EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2-Dichlorobenzene EPA 601 ug/1 1.5 ND 08/18/89 OL
1,3-Dichlorobenzene EPA 601 ug/l 3.2 ND 08/18/89 OL
1,4-Dichlorobenzene EPA 601 ug/l 2.4 ND 08/18/89 OL
Dichlorodifluoromethane EPA 601 ug/1 18 ND 08/18/89 OL
1,1-Dichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2 Dichloroethane EPA 601 ug/1 0.3 ,O. r53 08/18/89 OL S
1,1-Dichloroethene EPA 601 ug/l 1.3 ND 08/18/89 OL
Trans-1,2-Dichloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2-Dichloropropene EPA 601 ug/1 1.0 ND 08/18/89 OL
cis-1,3-Dichloropropene EPA 601 ug/l 3.4 ND 08/18/89 OL
Trans-1,3-Dichloropropene EPA 601 ug/1 3.4 ND 08/18/89 OL
Methylene Chloride EPA 601 ug/l 2.5 ND 08/18/89 OL
1,1,2,2-Tetrachloroethane EPA 601 ug/1 0.3 ND 08/18/89 OL
Tetrachloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,1,1-Trichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Signed e� ��

ENVIRONMENTAL NATIONAL LABOR1
TEST DATA REPORT
DIES
Date 09/12/89
Page 2
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane EPA 601 ug/l 1.0 ND 08/18/89 OL
Trichloroethene EPA 601 ug/l 1.2 ND 08/18/89 OL
Trichlorofluoromethane EPA 601 ug/l 3.2 ND 08/18/89 OL
Vinyl Chloride EPA 601 ug/l 1.8 ND 08/18/89 OL
Benzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Chlorobenzene ;;�p EPA 602 ug/1 1.0 19 08/18/89 OL
Ethylbenzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Toluene EPA 602 ug/1 1.0 ND 08/18/89 OL
-- GC/MS ANALYSIS RESULTS --
Isophorone EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethoxy)methane EPA 8270 ug/l 10 ND 09/11/89 MC
1,2,4-Trichlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
Naphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chloroaniline EPA 8270' ug/l 20 ND 09/11/89 MC
Hexachlorobutadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Methylnaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorocyclopentadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Chloronaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
1,3-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,4-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,2-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Benzyl Alcohol EPA 8270 ug/l 20 ND 09/11/89 MC
bis(2-Chloroisopropyl) ether EPA 8270 ug/1 10 ND 09/11/89 MC
Hexachloroethane EPA 8270 ug/1 10 ND 09/11/89 MC
N-Nitroso-di-n-propylamine EPA 8270 ug/1 10 ND 09/11/89 MC
Nitrobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
Acenaphthylene EPA 8270 ug/l 10 ND 09/11/89 MC
Dimethyl phthalate EPA 8270 ug/l 10 ND 09/11/89 MC
2,6-Dinitrotoluene EPA 8270 ug/1 10 ND 09/11/89 MC
Acenaphthene EPA 8270 ug/1 10 ND 09/11/89 MC
3-Nitroaniline EPA 8270 ug/1 50 ND 09/11/89 MC
Dibenzofuran EPA 8270 ug/l 10 ND 09/11/89 MC
2,4-Dinitrotoluene EPA 8270 ug/1 10 ND 09/11/89 MC
Fluorene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chlorophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Diethylphthalate EPA 8270 ug/1 10 ND 09/11/89 MC
4-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
4-Bromophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
Phenanthrene EPA 8270 ug/1 10 ND 09/11/89 MC
Anthracene EPA 8270 ug/1 10 ND 09/11/89 MC
Signed

ENVIRONMENTAL NATIONAL LABOR)
TEST DATA REPORT
TIES
Date 09/12/89
Page 3
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/1
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/l
0.1
ND
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
0..006 ,0
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/1'
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/l
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed Win, -��

ENVIRONMENTAL NATIONAL LABOR
TEST DATA REPORT
HIES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-02
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Station ID MSD-S-1
Matrix : W
Type GRAB
Collector GM
Remarks :
--- Sample Information ---
Cust. No.
Sampled Date/Time :
Received Date/Time :
Received From/By :
Chain of Custody :
Number of Containers :
--- Test Data ---
08/16/89 15:10
08/17/89 10:0o
GM/CLM
6473
6
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
Ext/Acid Extractables/W
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2 Dichloroethane
1,1-Dichloroethene
Trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Trans-1,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
1,1,1-Trichloroethane
3510/8270
N/A
08/21/89
JAS
3510/8270
N/A
08/21/89
JAS
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/l
2.0
ND
08/18/89
OL
EPA
601
ug/l
12
ND
08/18/89
OL
EPA
601
ug/l
1.2
ND
08/18/89
OL
EPA
601
ug/l
5.2
ND
08/18/89
OL
EPA
601
ug/l
1.3
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.5
ND
08/18/89
OL
EPA
601
ug/l
3.2
ND
08/18/89
OL
EPA
601
ug/1
2.4
ND
08/18/89
OL
EPA
601
ug/1
18
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
0.3
0 5J, it
08/18/89
OL
EPA
601
ug/l
1.3
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
3.4
ND
08/18/89
OL
EPA
601
ug/l
3.4
ND
08/18/89
OL
EPA
601
ug/1
2.5
ND
08/18/89
OL
EPA•6oi
ug/l
0.3
_ 97 40-
08/18/89
OL
EPA
601
ug/1
1.0
ND-
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
Signed i

ENVIRONMENTAL NATIONAL LABORA.
TEST DATA REPORT
:ES
Date 09/12/89
Page 2
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Chloride
Benzene
Chlorobenzene
Ethylbenzene
Toluene
-- GC/MS ANALYSIS RESULTS --
Isophorone
bis(2-Chloroethoxy)methane
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
2-Methylnaphthalene
Hexachlorocyclopentadiene
2-Chloronaphthalene
bis(2-Chloroethyl) ether
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
bis(2-Chloroisopropyl) ether
Hexachloroethane
N-Nitroso-di-n-propylamine
Nitrobenzene
2-Nitroaniline
Acenaphthylene
Dimethyl phthalate
2,6-Dinitrotoluene
Acenaphthene
3-Nitroaniline
Dibenzofuran
2,4-Dinitrotoluene
Fluorene
4-Chlorophenyl phenyl ether
Diethylphthalate
4-Nitroaniline
4-Bromophenyl phenyl ether
Hexachlorobenzene
Phenanthrene
Anthracene
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/1
3.2
ND
08/18/89
OL
EPA
601
ug/1
1.8
ND
08/18/89
OL
EPA
602
ug/1
1.0
ND
08/18/89
OL
EPA
602
ug/1
1.0
1355 40w
08/18/89
OL
EPA
602
ug/1
1.0
ND
08/18/89
OL
EPA
602
ug/1
1.0
ND
08/18/89
OL
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
20
ND
09/11/89
Mc
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
20
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
Signed

ENVIRONMENTAL NATIONAL LABOF
TEST DATA REPORT
.LIES
Date 09/12/89
Page 3
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter ............................ Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09411/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
3.3'-Dichlorobenzidine
EPA
8270
ug/1
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/1
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/1
0.1
0.1
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/l
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed

ENVIRONMENTAL NATIONAL LABORA IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-03
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-S-2 Sampled Date/Time : 08/16/89 15:45
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/1
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/1
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/1
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/1
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/1
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/1
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/1
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/1
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
0 46.
08/18/89
OL
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Signed/(�

L ENVIRONMENTAL NATIONAL LABORA,
TEST DATA REPORT
:ES
Date 09/12/89
Page 2
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/1
3.�
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8,
ND
08/18/89
OL
Benzene
EPA
602
ug/1
1.01
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS =-
Isophorone
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/1
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA,8270
ug/1
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Signed �. =1'► C

-ENVIRONMENTAL NATIONAL LABOR
TEST DATA REPORT
.IES
Date 09/12/89
Page 3
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270-
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3,31-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/1
0.1
ND
08/18/89
MC
Mercury, Total
EPA
7470
mg/1
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/l
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed

L ENVIRONMENTAL NATIONAL LABORAS
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-04
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
.ES
Cust. No. .
Station ID : TRIP BLANK Sampled Date/Time : / /
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 2
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2 Dichloroethane
1,1-Dichloroethene
Trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Trans-1,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Chloride
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
2.0
ND
08/18/89
OL
EPA
6ol
ug/1
12
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
6ol
ug/1
5.2
ND
08/18/89
OL
EPA
601
ug/1
1.3
ND
08/18/89
OL
EPA
6ol
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.5
ND
08/18/89
OL
EPA
601
ug/1
3.2
ND
08/18/89
OL
EPA
601
ug/1
2.4
ND
08/18/89
OL
EPA
601
ug/1
18
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/l
0.3
08/18/89
OL
EPA
6ol
ug/1
1.3
ND'-
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
3.4
ND
08/18/89
OL
EPA
601
ug/1
3.4
ND
08/18/89
OL
EPA
601
ug/l
2.5
ND
08/18/89
OL
EPA
601
ug/l
0.3
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/1
3.2
ND
08/18/89
OL
EPA
601
ug/1
1.8
ND
08/18/89
OL
Signed czr,�5,--

ENVIRONMENTAL NATIONAL LABOF .IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-04
Project No. : AVE-2265
Test Data
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Benzene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Chlorobenzene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Ethylbenzene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Toluene
EPA 602
ug/1
1.0 ND
08/18/89
OL
Signed

LAW ENVIRONMENTAL, INC.
C 2�— NATIONAL LABORATORY
112 TOWNPARK DRIVE
KENNESAW, GEORGIA 30144
[phone]
PROJECT NAME
Pifro • s (,Jrare�G� '70 ► 5t-)rc
SAMPL)IRS (SIGNATUM) ,
CHAIN OF CUSTODY RECORD
SAMPLING NAME OF FACILITY:
INFORMATION
STREET ADDRESS:
CITY/STATE:
OB NO. U)
W
Z Al
/ p O O U Psa .a`e
SAMPLING ATE 4- �D ' o F- GO P•t� �O apt pb x Pie
`
m d W O �ek�°� Q �'b G Q PF pQa
TIME m Z Oo� SAMPLE STATION DESCRIPTION p eA i v Q y °ti �G ho<
� ��niiw�ii��■�� - �i
RE I QUISHED BY
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
-114/ i /0
IGNA U E)
(SIGNATURE)
(SIGNATURE)
RELINQUISHED BY:
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
ORIGINAL AND YELLOW COPIES ACCOMPANY SAMPLE SHIPMENT TO LABORATORY.
-,DISTRIBUTION:
Iw PINK COPY R
AINED BY SAMPLERS.
YE LOW COPY RETAINED
BY LABORATORY.
,` REMARKS:
�I--
e
I� �
ZIP:
LENL LAB NO.
L//n9_rlI
RECEIVED BYI DATE/TIME
(SIGNATURE)
R IVE T LABO RY: DATE/TIME
(SAG ATUR
RECOVERY WE L - RW
SOURCE RCRA MONITORING WELL - MW
CODES: SOIL/SEDIMENT - SO
SLUDGE-SL
NPDES DISCHARGE - NO
DRINKING WATER - OW
r� HAZARDOUS WASTE - HW
SURFACE WATER - SW

LAW ENGINEERING
5 geotechnical, environmental & construction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
• '" w = [phone]
October 13, 1989
State of North Carolina
Department of Natural Resources
and Community Development
Division of Environmental Management
Groundwater Division
P.O. Box 370
Asheville, North Carolina 28802-0370
Attention: Mr. Don Link
Subject: Surface and Groundwater Analytical Results
Metropolitan Sewerage District
Highway 251
Asheville, North Carolina
Law Engineering Job Number AVE-2265
Gentlemen:
Attached are copies of the -analytical results of ground -water
samples collected from one boring and springs located on the
Metropolitan Sewerage District Plant property.
If you have any questions concerning the data submitted please do
not hesitate to call.
/kp.a
Sincerely,
LAW E EERI
Robert MacPhee
HydMgeologist
t�f
Th mas L Lamm ns
Environmental Services Manager '
,z
n li7i!" li 1. •�• �. i �.
I

LAW ENVIRONMENTAL, INC.
-Pv J1LLE, v.C. 112TONNPARKDRIVE
10NEM W GEORGIA 30144-5599
404421-3400
September 12, 1989
Law Engineering, Inc.
1100 Thousand Oaks' Blvd.
Greenville, SC 29607
Attention: Tom Lammons
LE Job Number:. AVE-2265
LENL Job Number: 12024
Subject: Chemical Analysis of Samples Received
on 8/17/89
Dear Mr. Lammons:
Law Environmental National Laboratories has completed its
analysis of your samples and reports the results on the following
pages. These results relate only to the contents of the samples
as submitted. This report shall not be reproduced except in full
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
A ENVIRONMENTAL S
Zhanna Geskin
GC/MS Laboratory S ervisor
t 1�� , 'e
Clifford H. /MVcBride
QA/QC Coordinator
Attachment: Data Report
Invoice

ENVIRONMENTAL NATIONAL LABOR. -IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-01
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-WELL-1 Sampled Date/Time : 08/16/89 14:30
Matri.t : W Received Date/Time : 08/17/89 10:00
Type.: GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
J#
Bromodichloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/1
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1.3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/1
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
0.3
Ot:53
. 08/18/89
OL S
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND a
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/1
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
ND
08/18/89
OL
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Signed
4L47 A ��

' ENVIRONMENTAL NATIONAL LABORA 'IFS
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane EPA 601 ug/l 1.0 ND 08/18/89 OL
Trichloroethene EPA 601' ug/l 1.2 ND 08/18/89 OL
Trichlorofluoromethane EPA 601 ug/l 3.2 ND 08/18/89 OL
Vinyl Chloride EPA 601 ug/l 1.8 ND 08/18/89 OL
Benzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Chlorobenzene EPA 602 ug/1 1.0 149, 08/18/89 OL
Ethylbenzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Toluene EPA 602 ug/l 1.0 ND 08/18/89 OL
-- GC/MS ANALYSIS RESULTS --
Isophorone EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethoxy)methane EPA 8270 ug/l 10 ND 09/11/89 MC
1,2,4-Trichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Naphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chloroaniline EPA 8270' ug/l 20 ND 09/11/89 MC
Hexachlorobutadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Methylnaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorocyclopentadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Chloronaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
1,3-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,4-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,2-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Benzyl Alcohol EPA 8270 ug/l 20 ND 09/11/89 MC
bis(2-Chloroisopropyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachloroethane EPA 8270 ug/l 10 ND 09/11/89 MC
N-Nitroso-di-n-propylamine EPA 8270 ug/1 10 ND 09/11/89 MC
Nitrobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
Acenaphthylene EPA 8270 ug/l 10 ND 09/11/89 MC
Dimethyl phthalate EPA 8270 ug/l 10 ND 09/11/89 MC
2,6-Dinitrotoluene EPA 8270 ug/l 10 ND 09/11/89 MC
Acenaphthene EPA 8270 ug/l 10 ND 09/11/89 MC
3-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
Dibenzofuran EPA 8270 ug/l 10 ND 09/11/89 MC
2,4-Dinitrotoluene EPA 8270 ug/l 10 ND 09/11/89 MC
Fluorene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chlorophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Diethylphthalate EPA 8270 ug/l 10 ND 09/11/89 MC
4-Nitroaniline EPA 8270 ug/1 50 ND 09/11/89 MC
4-Bromophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
Phenanthrene EPA 8270 ug/l 10 ND 09/11/89 MC
Anthracene EPA 8270 ug/l 10 ND 09/11/89 MC
1
Signed �G.

Date 09/12/89
Page 3
ENVIRONMENTAL NATIONAL LABORA .TIES
TEST DATA REPORT
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method..:. Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
Fluoranthene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
N-Nitrosodiphenylamine
Pyrene
Butyl benzyl phthalate
3.3'-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
bis(2-ethylhexyl)phthalate
Di-n-octyl phthalate
2-Chlorophenol
Phenol
2-Methylphenol
4-Methylphenol
2-Nitrophenol
2,4-Dimethylphenol
2,4-Dichlorophenol
Benzoic Acid
4-Chloro-3-methylphenol
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
4,6-Dinitro-2-methylphenol
Pentachlorophenol
--- SERIES 8000
Barium, Total
Mercury, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Lead, Total
Selenium, Total
Silver, Total
Total Metals Prep: Aqueous ICP
Total Metals Prep: Aqueous Furnce
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270-
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
20
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
0270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
6010
mg/1
0.1
ND
08/18/89
MC
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
EPA
7060
mg/1
0.005
ND
08/18/89
MC
EPA
7131
mg/1
0.002
ND
08/18/89
MC
EPA
7191
mg/1
0.005
,94,Qpk� .0
o8/18/89
MC
EPA
7421
mg/1
0.005
ND
08/18/89
MC
EPA
7740
mg/1'
0.005
ND
08/18/89
MC
EPA
7761
mg/l
0.01
ND
08/18/89
MC
EPA
3010
N/A
08/17/89
HH
EPA
3020
N/A
08/17/89
GSP
Signed z4, 6m
C16z'I

ENVIRONMENTAL NATIONAL LABORA -IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-02
Project No. : AVE-2265 Cust. No. :
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Sample Information
Station ID MSD-S-1 Sampled Date/Time : 08/16/89 15:10
Matrix : W Received Date/Time : 08/17/89 10:00
Type GRAB Received From/By GM/CLM
Collector GM Chain of Custody : 6473
Number of Containers 6
Remarks
--- Test Data ---
?arameter .............................. Method.... Units Det. Limit Results... Test Date Analy
--ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
E.xt/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
i
3romodichloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
3romoform
EPA
601
ug/1
2.0
ND
08/18/89
OL
3romomethane
EPA
601
ug/l
12
ND
08/18/89
OL
carbon tetrachloride
N,hloroethane
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/l
5.2
ND
08/18/89
OL
?-Chloroethylvinyl ether
',hloroform
EPA
601
ug/l
1.3
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
3hloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
)ibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
L,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
L,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
L,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
)ichlorodifluoromethane
EPA
601--
ug/l
18
ND
08/18/89
OL
L91-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
L,2 Dichloroethane
EPA
601
ug/l
0.3
0 5, it
08/18/89
OL
L,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
7rans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
L,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
;is-1,3-Dichloropropene
'raps-1,3-Dichloropropene
EPA
601
ug/l
3.4-
ND
08/18/89
OL
EPA
601
ug/l
3.4
ND
08/18/89
OL
(ethylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
.,1,2,2-Tetrachloroethane
EPA,
601
ug/l
0.3
047 40
08/18/89
OL
.etrachloroethene
EPA
601
ug/l
1.0
ND-
08/18/89
OL
.,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Signed

ENVIRONMENTAL NATIONAL LABORA. -TES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.. Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
L,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
rrichloroethene
EPA
601
ug/l
1.2
ND
08/18/89
OL
rrichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Jinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
3enzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
',hlorobenzene
EPA
602
ug/1
1.0
1._55 4mr
08/18/89
OL
3thylbenzene
EPA
602
ug/1
1.0
08/18/89
OL
toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Csophorone
EPA
8270
ug/1
10
ND
09/11/89
MC
)is(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
L,2,4-Trichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Japhthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
iexachlorobutadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
iexachlorocyclopentadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270-
ug/1
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/1
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
V-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Vitrobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
iexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
?henanthrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Signed

ENVIRONMENTAL NATIONAL LABOR" TIES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3.3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/1'1/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/1
0.1
0.1
08/18/89
MC
Mercury, Total
EPA
7470
mg/1
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/1
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed �."

L .'ENVIRONMENTAL NATIONAL LABORP
TEST DATA REPORT
.IES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-03
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Cust. No. :
Station ID : MSD-S-2 Sampled Date/Time : 08/16/89 15:45
Matrix : W Received Date/time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
/
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/1
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/1
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/1
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/1
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/1
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/1
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/1
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
-08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/1
0.3
q,_,,6,
08/18/89
OL
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Signed

ENVIRONMENTAL NATIONAL LABORK LES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/l
3.�
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.&
ND
08/18/89
OL
Benzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/l
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS =-
Isophorone
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
9270
ug/l
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/l
10
ND
09/11./89
MC
2,6-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/l
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8276
ug/l
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
�..=''1 Z
Signed

L- ENVIRONMENTAL NATIONAL LABORA' LES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270-
ug/1
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/1
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/1
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/1
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
'ND
09/11/89
MC
--- SERIES 8000
3arium, Total
EPA
6010
mg/1
0.1
ND
08/18/89
MC
Kercury, Total
EPA
7470
mg/1
0.0005
ND
08/21/89
OL
4rsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
cadmium, Total
EPA
7131
mg/1
0.002
ND
08/18/89
MC
chromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/1
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed c

L- ENVIRONMENTAL NATIONAL LABORA'-
TEST DATA REPORT
[ES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-41o9-o4
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Cust. No. :
Station ID
: TRIP BLANK
Sampled Date/Time :
/ / ;
Matrix
: W
Received Date/Time :
08/17/89 10:00
Type
: GRAB
Received From/By :
GM/CLM
Collector
: GM
Chain of Custody
: 6473
Number of Containers
: 2
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/l
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/1
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2 Dichloroethene
EPA
601
ug/l
0.3
1, 53.
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/l
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethene
EPA
601
ug/l
0.3
2.1„
08/18/89
OL
Tetrachloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/l
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/l
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/l
1.8
ND
08/18/89
OL
Signed

ENVIRONMENTAL NATIONAL LABOR" IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-04
Project No. : AVE-2265
Test Data
Parameter ..............................
Method....
Units
Det.
Limit Results...
Test Date
Analy
-- ORGANIC ANALYSIS RESULTS --
Benzene
EPA 602
ug/l
1.0
ND
08/18/89
OL
Chlorobenzene
EPA 602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA 602
ug/l ,
1.0
ND
08/18/89
OL
Toluene
EPA 602
ug/1
1.0
ND
08/18/89
OL
t
Signed

LAW ENVIRONMENTAL, INC. CHAIN OF CUSTODY RECORD 0 4 / J
NATIONAL LABORATORY SAMPLING NAME OF FACILITY: 0
112 TOWNPARK DRIVE INFORMATION
KENNESAW, GEORGIA 30144 STREET ADDRESS:
[phone] i— % CITY/STATE: ZIP:
PROJECT NAME JOB NO. In
SAMPL RS (SIGNATU ) _ �
P z �P`% °`10�o x�a0
/ p O xs
SAMPLING DATE O �'O• ,p@'� �� �ep�\ pb ,�. % P
m L O �00 Q Q\ Q ��t�°p e��°c Q �� V
TIME Z pp� SAMPLE STATION DESCRIPTION 0eP 0
t7 u G 2 �� �y ��' �� �� �� 0° �� �� `► LENL LAB NO.
w/o -a
�lll A - 2, -
R"IjFQUISHE BY �(DATEMME RECEIVED BY: RELINQUISHED BY: RECEIVED BYt DATE/TIME
IGNA U E) 8-11`l i /0 (SIGNATURE) (SIGNATURE) (SIGNATURE)
RELINQUISHED BY: DATE/TIME RECEIVED BY: RELINQUISHED BY; 7&71AU14�
RY: _DA' DATE/TIME
I to
(SIGNATURE)I I - I (SIGNATURE) I (SIGNATUR
DISTRIBUTION: ORIGINAL AND YELLOW COPIES ACCOMPANY SAMPLE SHIPMENT TO LABORATORY.
It PINK COPY R AINED BY SAMPLERS. YE LOW COPY RETAINED BY LABORATORY.
REMARKS: `
(SfGNATURX
RECOVERY WE L - RW
SOURCE RCRA MONITORING WELL - MW
CODES:' SOIL/SEDIMENT - SO
SLUDGE-SL
NPDES DISCHARGE - ND
DRINKING WATER - DW
HAZARDOUS WASTE - HW

t LAW ENGINEERING
r geotechnical, environmental & construction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
[phone]
October 13, 1989
State of North Carolina
Department of Natural Resources
and Community Development
Division of Environmental Management
Groundwater Division
P.O. Box 370
Asheville, North Carolina 28802-0370
Attention: Mr. Don Link
Subject: Surface and Groundwater Analytical Results
Metropolitan Sewerage District
Highway 251
Asheville, North Carolina
Law Engineering Job Number AVE-2265
Gentlemen:
Attached are copies of the ,analytical results of ground -water
samples collected from one boring and springs located on the
Metropolitan Sewerage District Plant property.
If you have any questions concerning the data submitted please do
not hesitate to call.
Sincerely,
LAWE.
EERI
Robert MacPhee
Hydrogeologist
��i:�
i
Th mas L. Lamm ns
Environmental Services Manager
/kp.a

�1�rF
� f� j J '� • ..ram
September 12, 1989
Law Engineering, Inc.
1100 Thousand Oaks' Blvd.
Greenville, SC 29607
Attention: Tom Lammons
LE Job Number:- AVE-2265
LENL Job Number: 12024
Subject: Chemical Analysis of Samples Received
on 8/17/89
Dear Mr. Lammons:
C
LAW ENVIRONMENTAL, INC.
112 TUNNPARK DRIVE
KENNESAW GEORGIA 30144-5599
404-421-3400
Law Environmental National Laboratories has completed its
analysis of your samples and reports the results on the following
pages. These results relate only to the contents of the samples
as submitted. This report shall not be reproduced except in hill
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
A ENVIRONMENTAL S
Zhanna Geskin
GC/MS Laboratory S ervisor
Clifford H. McBride
QA/QC Coordinator
Attachment: Data Report
Invoice

` a ENVIRONMENTAL NATIONAL LABOR. RIES
TEST DATA REPORT
)ate 09/12/89
?age 1
--- Project Information ---
Lab Number : 89-4109-01
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-WELL-1 Sampled Date/Time : 08/16/89 14:30
Matrirt : W Received Date/Time : 08/17/89 10:00
Type.: GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
?arameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
J#
3romodichloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
3romoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
3romomethane
EPA
601
ug/l
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
Chloroethane
EPA
601,
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/1
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
0.3
0..53 •
08/18/89
OL S
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/l
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
ND
08/18/89
OL
retrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
��
Signed

ENVIRONMENTAL NATIONAL LABORA PIES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Chloride
Benzene
Chlorobenzene
Ethylbenzene
Toluene
-- GC/MS ANALYSIS RESULTS --
Isophorone
bis(2-Chloroethoxy)methane
1,2,4-Trichlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
2-Methylnaphthalene
Hexachlorocyclopentadiene
2-Chloronaphthalene
bis(2-Chloroethyl) ether
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
bis(2-Chloroisopropyl) ether
Hexachloroethane
N-Nitroso-di-n-propylamine
Nitrobenzene
2-Nitroaniline
Acenaphthylene
Dimethyl phthalate
2,6-Dinitrotoluene
Acenaphthene
3-Nitroaniline
Dibenzofuran
2,4-Dinitrotoluene
Fluorene
4-Chlorophenyl phenyl ether
Diethylphthalate
4-Nitroaniline
4-Bromophenyl phenyl ether
Hexachlorobenzene
Phenanthrene
Anthracene
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/l
3.2
ND
08/18/89
OL
EPA
601
ug/l
1.8
ND
08/18/89
OL
EPA
602
ug/l
1.0
ND
08/18/89
OL
EPA
602
ug/l
1.0
1A...
08/18/89
OL
EPA
602
ug/l
1.0
ND
08/18/89
OL
EPA
602
ug/l
1.0
ND
08/18/89
OL
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/1 20 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/1 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 20 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/1 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 50 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/1 10 ND 09/11/89
EPA 8270 ug/1 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 50 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 50 ND 09/11/89
EPA 8270 ug/1 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
EPA 8270 ug/l 10 ND 09/11/89
Signed
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC
MC

ENVIRONMENTAL NATIONAL LABORR +IES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.:.. Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
Fluoranthene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
N-Nitrosodiphenylamine
Pyrene
Butyl benzyl phthalate
3.31-Dichlorobenzidine
Benzo(a)anthracene
Chrysene
bis(2-ethylhexyl)phthalate
Di-n-octyl phthalate
2-Chlorophenol
Phenol
2-Methylphenol
4-Methylphenol
2-Nitrophenol
2,4-Dimethylphenol
2,4-Dichlorophenol
Benzoic Acid
4-Chloro-3-methylphenol
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
2,4-Dinitrophenol
4-Nitrophenol
4,6-Dinitro-2-methylphenol
Pentachlorophenol
--- SERIES 8000
Barium, Total
Mercury, Total
Arsenic, Total
Cadmium, Total
Chromium, Total
Lead, Total
Selenium, Total
Silver, Total
Total Metals Prep: Aqueous ICP
Total Metals Prep: Aqueous Furnce
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
20
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/l
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
0270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
10
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
8270
ug/l
50
ND
09/11/89
MC
EPA
8270
ug/1
50
ND
09/11/89
MC
EPA
6010
mg/l
0.1
ND
08/18/89
MC
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
EPA
7060
mg/l
0.005
ND
08/18/89
MC
EPA
7131
mg/1
0.002
ND
08/18/89
MC
EPA
7191
mg/1
0.005
q--J ,�
08/18/89
MC
EPA
7421
mg/1
0.005
ND
08/18/89
MC
EPA
7740
mg/1'
0.005
ND
08/18/89
MC
EPA
7761
mg/1 .
0.01
ND
08/18/89
MC
EPA
3010
N/A
08/17/89
HH
EPA
3020
N/A
08/17/89
GSP
Signed

r"
= ENVIRONMENTAL NATIONAL LABORA -IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-02
Project No. : AVE-2265 Cust. No. :
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Sample Information
Station ID : MSD-S-1 Sampled Date/Time : 08/16/89 15:10
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers 6
Remarks
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
3510/8270
N/A
08/21/89
JAS
Ext/Acid Extractables/W
3510/8270
N/A
08/21/89
JAS
-- ORGANIC ANALYSIS RESULTS --
i
3romodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
3romoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
3romomethane
EPA
601
ug/l
12
ND
08/18/89
OL
carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
OL
3hloroethane
EPA
601
ug/l
5.2
ND
08/18/89
OL
?-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
"hloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
)ibromochloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
L,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
L,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
L,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
OL
)ichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
L,1-Dichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
L,2 Dichloroethane
EPA
601
ug/l
0.3
0t5,9 it
08/18/89
OL
L,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
7rans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
L,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
;is-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Tans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
?ethylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
.,1,2,2-Tetrachloroethane
EPA,
601
ug/1
0.3
0,,97 40
08/18/89
OL
.etrachloroethene
EPA
601
ug/l
1.0
kD-
08/18/89
OL
.,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Signed

I ENVIRONMENTAL NATIONAL LABORA 1TES
TEST DATA REPORT
Date 09/12/89
?age 2
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
?arameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
L,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
rrichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
rrichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Jinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
3enzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
3hlorobenzene
EPA
602
ug/1
1.0
1.5-5 41aw
08/18/89
OL
3thylbenzene
EPA
602
ug/1
1.0
IRD
08/18/89
OL
Coluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Csophorone
EPA
8270
ug/1
10
ND
09/11/89
MC
Dis(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
L,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Japhthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
iexachlorobutadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
?-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
iexachlorocyclopentadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
?-Chloronaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
'ois(2-Chloroethyl) ether
EPA
8,270
ug/l
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/1
10
ND
09/11/89
MC
K-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Kitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270.
ug/1
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Signed zi /21;-7 �/

ENVIRONMENTAL NATIONAL LABOR' .:IES
Date 09/12/89 TEST DATA REPORT
Page 3
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/1
10
ND
09411/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/1
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene'
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1.
10
ND
09/11/89
MC
3.3'-Dichlorobenzidine
EPA
8270
ug/1
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/1
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIFS 8000
Barium, Total
EPA
6010
mg/1
0.1
0.1
08/18/89
MC
Mercury, Total
EPA
7470
mg/1
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/1
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/1
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/1
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed �j�`

ENVIRONMENTAL NATIONAL LABOR"' .IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-03
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Sample Information
Station ID : MSD-S-2 Sampled Date/Time : 08/16/89 15:45
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270
Ext/Acid Extractables/W 3510/8270
N/A 08/21/89 JAS
N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
1#
Bromodichloromethane
EPA
601
ug/1
1.0
ND
08/18/89
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
Bromomethane
EPA
601
ug/l
12
ND
08/18/89
Carbon tetrachloride
EPA
601
ug/l
1.2
ND
08/18/89
Chloroethane
EPA
601
ug/l
5.2
ND
08/18/89
2-Chloroethylvinyl ether
EPA
601
ug/1
1.3
ND
08/18/89
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
Dibromochloromethane
EPA
601
ug/l
1.0
ND
08/18/89
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
1,4-Dichlorobenzene
EPA
601
ug/l
2.4
ND
08/18/89
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
1,1-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
1,2 Dichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
Trans-1,2-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
1,2-Dichloropropane
EPA
601
ug/l
1.0
ND
08/18/89
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
0.,b-
08/18/89
Tetrachloroethene
EPA
601
ug/1
1.0
ND
08/18/89
1,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
Signed
CVvzr
f
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL
OL

ENVIRONMENTAL NATIONAL LABORA' IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/l
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/l
3.�-
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8-
ND
08/18/89
OL
Benzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS =-
Isophorone
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/1
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/l
10
ND
09/11./89
MC
2,6-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/l
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
.
Signed

I - ENVIRONMENTAL NATIONAL LABORA'� IES
Date 09/12/89
TEST DATA REPORT
--
Page 3
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270-
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
--- SERIFS 8000
3arium, Total
EPA
6010.
mg/l
0.1
ND
08/18/89
MC
Kercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
4rsenic, Total
EPA
7060
mg/l
0.005
ND
08/18/89
MC
cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
'Whromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
MC
total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed c

L. ENVIRONMENTAL NATIONAL LABORA`
TEST DATA REPORT
IES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-04
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Cust. No. .
Station ID
: TRIP BLANK
Sampled Date/Time
: / /
Matrix
: W
Received Date/Time
: 08/17/89 10:00
Type
: GRAB
Received From/By
: GM/CLM
Collector
: GM
Chain of Custody
: 6473
Number of Containers
: 2
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/l
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/1
1.2
ND
08/18/89
OL
Chloroethane
EPA
601,.
ug/l
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/l
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/l
1.5
ND
08/18/89
OL
1.3-Dichlorobenzene
EPA
601
ug/1
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601.
ug/l
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
0.3
1,63,.
08/18/89
OL
1,1-Dichloroethene
EPA
601
ug/l
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/l
1.0
ND
08/18/89
OL
cis-1.3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/l
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/l
0.3
2.1
08/18/89
OL
Tetrachloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1,2-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Trichloroethee
EPA
601
ug/l
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/l
1.8
ND
08/18/89
OL
Signed

r ENVIRONMENTAL NATIONAL LABOP"' IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-04
Project No. : AVE-2265
Test Data
Parameter ..............................
Method....
Units
Det.
Limit Results...
Test Date
Analy
-- ORGANIC ANALYSIS RESULTS --
Benzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/l
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/l
1.0
ND
08/18/89
OL
It
Signed

LAW ENVIRONMENTAL, INC.
NATIONAL LABORATORY
112 TOWNPARK DRIVE
7 KENNESAW, GEORGIA 30144
[phone] q '
Dq-
PROJECT NAME
SAMPL)fRS (SIGNATU¢,E) ,
CHAIN OF CUSTODY RECORD d 4 / J
SAMPLING NAME OF FACILITY: D
INFORMATION
STREET ADDRESS:
CITY/STATE: ZIP:
OB NO. N
It
W
z c
a Q V% �P
O O G� PSc ta`e
SAMPLING ATE �" � o U.
m i O FAO Q \ Q \�Q ���C
TIME i oo� SAMPLE STATION DESCRIPTION 6
0 u G Z �� �� �� �� �� �� LENL LAB NO.
V M m SA - 6 -1/0-a
I
o
-U
RE I QUISHE BY
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
RECEIVED BY:
DATE/TIME
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
RELINQUISHED BY:
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
R C. IVE T LABO RY:
`(
DATE/TIME
1 u
7
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
IS GNATUR
RECOVERY WE L - RW
DISTRIBUTION: ORIGINAL AND YELLOW COPIES ACCOMPANY SAMPLE SHIPMENT TO LABORATORY. SOURCt RCRA MONITORING WELL - MW
L PINK COPY R AINED BY SAMPLERS. YE LOW COPY RETAINED BY LABORATORY. CODES: SOIL/SEDIMENT -SO
SLUDGE SL
REMARKS: NPDES DISCHARGE - ND
I�se) now DRINKING WATER - DW
` HAZARDOUS WASTE - HW
�el�I-! W�TIO _CW

e h -U
-21-1 29 15049 FROM " LAW ENVIRONMENTAL
TO 91704251G311200 P.01
LAW ENVIRONMENTAL INC.
112 TDMWM MVE
KOMMAW WOWA 30144.5599
PAX NUMOIER 404-421- 3 484
# iw ik i1t � �► rM dd # # rlr # �1 +� # +� i # # # i # i t$ i� Ai i * i i � # i
NS 4
COS f
Locazt :
NAME a
COMPANY:
LOCATION..-
LEPH pp.d i

-4-21-1989 15:49 FROM LAW ENUIRONMENTAL TO 917042518011200 P.02
LAW ENVIRONbWTAG NATIONAL LABORATORIES
TEST ENTRY FORM
ate 08/17/89
age 1
- Project Information ---
Lab Neer 89-4109-01
Project No. oust. No.
Project Name MEMO. SEWABAG8 DISTRICT
Manager: TOM LAMMONS Results Due 08/2%/89
Sample Information
Station ID :
Matrix :
Type o
Collector :
Remarks
MSA-WELL-1
W
GRAB
GPI
Sampled Date/Time :
Received Date/Time :
Received From/By
Chain of Custody
'.� J Number of Containers
c.
0A
08/16/8 9 14:30
08/07/89 1.0:00
: GM/CLM
: 6473
6
----Test Data ---
Parameter ...... .. ..... . . . .. ... .. .. . . . ..
Method. . . .
Units
Det.
Limit
ReSults.. .Test Date Anialy
--= ORGANIC
ANALYSIS RESULTS --
5002
Bromodichloromethane
EPA
601
ug/l
1.0
��n
-�=---- _
5003
Bromoform
EPA
601
,gig/1
2.0
5004
Bromomethane
EPA
601
ug/1
12
r l
5005
Carbon tetrachloride
F-PA
,601
ug/1
1.2
'4/
.5007
Chloroethane
EPA
601
ug/1
5.2
5008
2-Chloroe --': ' - ,,: ny7. ether
EPA
601
UU111
1.3
Iva,
5009
Chloroform
EPA
601
ug/
—
3010
Chloromethanne
EPA
601
ug/ l-
5011
Dibromochl orometin., e
IPA
601
ug/i
5012
1; 2-Dicky + orobenzene
EPA
601
u /?
1.5
5013
1,3-Dichlorobenzt�ne
EPA
601
ug/1
3.2
5014
1,4-Dichlorobenzene
EPA
601
ug/1
2.4
r�?�
5015
Dichlorodifluoromethane
EPA
601
ug/1
18--
5016
1,1-Dichloroethane
FDA
601
ug/1
Q
--

-4-21-1939 15:50 FROM LAIJ 2K]U i ROf,irlEf-]TAL TO 917042516311200 P. 0:3
LAW QVIT2NMENTAL NATIONAiL Wjn0RATORILEZ-
TEST ENTRY FORM
te
ge project Information
Lub Number 89-hog-oi
Project No. Cost. No. :
Projev z, METRO, SEWARABE DISTRICT
�vaager: TQM LAMMONS Results Due : 08/21/89
sample Information
Station ID : MSA-WELL-1 Mpled Date/Time : 08/16/89 14:30
Matrix : W Received Dats/Time : 08/07/89 10:00
Type : GRAB Received From/By ; GM/CLM
*Collector I GN Chajn of Oustody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
het ...... ...... I-- ...... -- hod—. Units Dat. Limit Results— Test Date Analy
- ORGANIC ANALYSIS RESULTS --
5017
1f2 Dichloroethane
EPA
601
Ug/1
0.3
5518
1,1-Dichloroet%ene
EPA
601
ug/l
10
5019
Trans-1,2-Dichicroethene
EPA
601
ugli
1.0
5020
1,20ichloropropane
EPA
601
w/1
QVY
5021
cis-1,3-Dichloropropene
EPA
60!
ugf :1
3e
5022
Trans-1,3-Dichloropropene
EPA
601
Ug/1
3.4
5023
Methylene Chloride
EPA
601
ugli
2.5
5024
1,1,2,2-Tetrachloroethane
EPA
601
ug/1
0.3
5025
Tetrash] -;herne
EPA
601
ag/l
LWT-
5026
1,1,1nalchJunwathane
EPA
601
Ug/1
2.5 A i
5027
1.1,2-TriahloroGthane
EPA
601
ug/l
too 00
5028
TrIchloroethene
EPA
601
Ug/l
1.2
5029
Trichlorofluoromethane
EPA
6oi
ug/1
3,2
5030
Vinyl Chloride
EPA
601
ugll
1.8

-4-21-1999 15: 50 FROM LAW ENI) I PONPIE1,1-1 AL TO 91.7042516311200 P.04
LAW NATIONAL UBORAT CIRIT—'S
TEST MAY FORM
-e 08/17/89
project 11r.formatior.
Lab Number 89-4109-01 cust, No.
pl,oject No.
Project MMO. SENIARAGE DISn- ICT
manager: TOM LUMONS Resin is DI -le 08/21/89
Sample Info .—Ly-atiOn
Station ID :
MSA-WEEK-L-1
vampled
osli6/89 14:r
matrix :
W
08/0-1,39 10,
(f 00
Type
G84B
pteck-i-ved From/By
M/Cul
Collector
GH
Chain of Cust0dQ7
6173
Number of Con-tainers
6
Remarks -,
--- Test Data ---
aramieter.................
Met'hod.
.
Test Date A�naly
,IC ANpALYSIS RFSULTS
5041 Benzene
A
602
ug/I
1.0
5042 Chlorobenzene
=P A
6 C-1 Z
Ug/I
1.0
5046 Ethylbenzene
EPA
602
1
1.2 g,f
.0
1,
500 Toluene
EPA
6,02'
u-S/I
1.0
5200 C-G VOC SCREM-11iG

-1-21-1329 15:51 FROM LAW -9,1VIRONMENTAL TO 917042516311200 P.05
-E-S
LAW
TMT EXTRY FOR14
to 08/17/89
projeC- Information,
Lab Number 89-4109-02 Cuss. No.
Project: No.
Project Name 14MO. S)3'WA?,kGE DISTRICT
Resl�llts Due 08/21/89
14anager: TON LM00NS
Sample Information
Station ID : WA-S-1 Samplod D'ate/Tim-e 08/16/89 15:10
Matrix : W Received Date/Tiffie 08/07/89 10:00
Type : G?,AB Recelved FrOMMY
Collector : Chin of CustOdY e 6473
Numbev Of" Containers 6
Remarks :
--- Test Data ---
Method....
Units
Det�
rnv
Uit
Results... Test Date Analy
ORGANIC ANALYSIS RESULTS
r,00,2 Bromodichloromethane
1
0>A 601
U01
1.0
5003 Br=OrOrm
=—A 601
'gig/ 1
2.0
5004 Broii-- -��ne
F-r-A 6ol
UgYJ
11)
005 Carbon tetraChloride
tPA 6oi
Ug/I
5007 Chloroethane
BPA 601
1}S/l
5.2
5008 2-Chloroethylviny1 ether
EPA 6oi
Ug/1
I.i
1-'009 Chloroform
EPA 601
Ug/1
GI-5
I
zv/ 92-
5010 Chloromethan�
spA 6oi
Ugli
5011 Dibromochloromethane
EPA 601
5012 1 12 -Dichlorobenzene
A 601
UgIl
1.5
5013 1,3-Dichiorobenzene
A
Epn 601
Ug/11
5.2
lm4 1,4-Dichlorolbenzene
EPA 601
'agi /1
2_4
502.5 Dichlorodif luoromethane
EPA 603.
UgIl
501.6 1, 1-bichloroethwie
EPA 601
-ag/1
.2e

_4-21-193 15:51 FROM Lril.'.1 EHII IROhdt"IEINTAL TO 9170425167311200 P.06
Tk P ems- y Fo-m
L.,qb Number a 89- 41,09-0
ProJect din. �:���. �4.
Manager: -LOM LAINM NS
t t
=,Plen%ae/Tame
08/16/80 155a10
: GM
rlh,:��jn of Custody
6473
1'di_Q�l'iEZ $d 4Collector
-s4 1enntaine s
z Y
--- Test Vara
-
- t i-�-
-.
t' ai-_
L;et
L - 4t � � is . ! ast Date. -AnalY
-_
s
-,
,P; r /
- ® k�'' �a ? ANALYSIS it
r
$%
5019 j-i ge;'s 3''1q -iFiyy if �.Liav %trZ pAk
P,��'L3.
:%^�1
UgI
? a'e,!
7020 1, 2-Dichloropi ..�e'd'ara
t • f"
's_�'_'
�ULa t..L =,"1 e 3-1-1ScfiloopoEeP
I
tU
m024 1,1 ,
E,A
601.
U /
,1
o f
--
y{p+�,���jj �7 -�a tf}
, s Ad � 1J3, �d` b+==.e_ed�i
1j2-7 1 ,� .^J. ✓-e'. or yy��we
ZED, �
bits.
�
?.^��
50129 Tr.icdSd.V&o.fil*.ao3od`2483anY
MP is
?Meta
U��
Q
!y
y e

-21-1 89 15: 52 FROM LAb,I Er I i I ROHIMENTAL TO 91704_516 11200 P. `J7
rp
Y ;.i
Projectr;a.7 �c�sta No.
Name 1s� � �, ��.�� �. ,ti
Manager- TOM I, ANIONS Rosi-, is Due- . 08 ,21 /89
Sample lnf0=l- -', 0n
T
-1
Sa pled4` / T«
08 16/8 :10
Matrix
a is
Rece _ e Da3-,/7-m
�,8f07/89 I-0:00
Type
GRAB
Peceivsd FrOM/BY
e GIA/OL_d
Collector
GM
?°;� - of rustody
6473
yyc
V-f rC--ntai ner ?
a 6
Remarks
--- Test Data ---
.yUA L ;"s , .ea«s« ....
14� lYy
f
'
ml- F,
d zA v l n< y 3a l
5G2
ul 1 1
110
5046 v.hyl enzene
R- A
0602
ug f ;
1
J 4
5200 Gi: i oc SCREaIIN0
— ---- _ _

1-21-1939 15- 52 FROIM LHl,1 E,-JV IPCIHMEHTAL TO 91 042c16 M200 P.08
TEST E;1IR R, FORM
;e 08/17/89
r,e i
Lab Number i 89-4109-03
Project No. Cueta No.
project Neme a nSTIM0;. 5EWA c2-1 D SIMICT
Manage- . TOM LMR-101 R esv, is Due 09 �lj8�a
S=ple j i�clb 4s�
Station 1D
MSA-S-2
ap --cl mate Pni me t
081/16/89 1 :45
Maui%
W
:lF-ce-4v-ad :ate/,Time a
CNS 0 /89 1-0:00
Type
RAM
� �� ��'.�e� r rom/ R'r e
MIMI
Collector
(V
C h -a irx *f` t- uS .
64735
�e0dy
:VIGM,03r- o 4'Vil "i9 ydrsi sJ a
6
L
---' `i-st Data ---
:ramete
LiYut
F'esultw,an Tlesa Date tin-aly
n ORGANIC
NIAL SIS ?FSUL7S>s�
r y
4 l)
01j
Riom0forn
FYA
601
U.g/y1
210? ,
1.2
�5005
Caibon tetrachloride
EPA
601
1.;g/1
i008
2-Chloroe L-hy ioyl v?
M A
6o
1-I1 I
j
,^-009
Chloroform
601
ug:./
FPA
60i
Ug/
5o,i4
1a'i—Dichlol.'l`.bernzene
EPA
601
tigil
.*e'ei�

-1-211-1969 IFD�52 FROM LAW DIV) I RO[ IME1 MHL TICI 917042516311200 P.09
N MIX,
A - rNNAL
I A ORT
LXORAM -1Z
TIE-STE ENTRY FORIUM
to 08/1"1/89
ge 2
Project
la-forz-at'fyr, ---
Lab Number
19-4109-o3
Fvoject No.
Cust. No. -
Project- Name a
NMR00. SEWAIRAGE, DISTRICT
Manager.-
EOM LAMMIS5
IRA-Sults D42e -. OSV-21/89
Sam-plo 11---for-ralatlon
Station ID :
MSAI-S-2
(38/1-6/089 15 44 5.
Matrix
t 41
Dat,!!�/Tim-- i
08 0 -7 y 89 1 Q 100
Type
TRJW
lRecelved Prom./By
GII/MM
C,ollecto-1
GM
Chaift of Custody
06473
Nuz'Der of Containe-ws
6
Remarks .
--- 'rest Data ---
,rr
......... IkJiiltz D�t. A2-- -ir, RaSU'tST-q- J)tre Analv
501`7
14,2. Dichlo�on-t-th-qne
50118
1 , 1-Dichloroetlh e, i i e
=PPA
EEO!
3 Ol 9
T--nanz-1 2-Dichlarornhene
ZPA
160-13
I gl
-.0
5020
1,2-Dichloroprop&rie
&:'---A
(SIOI
O
-4,
250-1
c-L-s--1 , 31-Dichlor-oprogene
PA
6D 0 1
U
5022
Trarls- 1 , 3 -Dichloroptropene
3,7,!? A-
6 C) I
Ll
5M
Yl--th-lene Chloride
'&P A
b- 0 1
U---
5 0 2 4
-Te Loroethane
E—P A
fS C, 11
ugly
1 1 , I -Tri chlb-, roe thmte
Ug/l
y;502j6 -
5027
1, 1, '-Trj
'
502U
Tpichloroethene
MPA
601.
OU
0 2) q-
Tri chloro f luorome tihvan e
pip P%
�i o 1
0 !R0
Vlilvl Chloride
EIPA
601
ug,

-,o-21-1989 1'5:53 FROM LAW ENUIR01HMENTAL TO 917042516311200 P.10
T AnrIPATOP YV.i22
TEST- -MMURY FORM
Ce 08/17/89
3
Project Information ---
Lab Number 89-42.09-03
Project firs: Cost. No.
ProJect Name o MEM10. SEWARPM DISTRICT
Manager: TOM LAB MONS ROSA-'Its Due 08/21/89
Sample Into=a-tioa
Station AD :
TCsA-S-2
Sampled Date/Time
08/16/8Q 15:45
Matrix
: W
Received Date/Time
081107/89 10:00
Type
V,,,AB
Rec;elvand From./By
G-mycul
Collector
CM
Chaip. of Custody
6473
N=-tber of Containers
6
Remarks .
--- Test Data ---
aramp"�-er ...... .....
Method, Un4-8 Det.
Jm4t Results. Test Date Ana'y
- ORGA141C ANALYSIS R=--ULV5
5041 Benzene
EPA 602
ug/1 4-1.0
1-1Z L L
5042 Chlorobenzene,
EPA 602'
ugli :L.0
OF
5046 --,thylbenzene
EPA 602
lu g I
5047 Toluene
KA 602
u; g, I 190
5200 GC VOC SCREENING

".a-21-1989 1_S�c^ FROM L AW1 EhdUTlPOl'-dMEPJTHL
TI1 ?1' 042251G3,11c2p P.11
5 "i 9'-)9 f n g NATIONA
} A T' `R
TEST ONTRY FORM
;e 1
Lab M=ber : c89-4109-04
Pnoj €ct No. . Dust. NO.
Projscl-- Nye d MZ,MO. MWAP GE DISMICT
n e--. TO M L, t a•b10NS Re-su is Oto i
ciample xnl oru, ati=an-
Matrix
. W
Date%'TLme, ,
�� j i� � ,`9 11` 0
J.Ype
rs'
a =Sias Vrom/'sy
Collector
GM
Cha±n of Custody
6473
N her o3 Cur LAC.° i i`ieI'8-w
2
Remarks :
--- Test Data __-
rameteis .. i . , ..... , . .. . . . . . -. ...
, . , . !4et- z
'U'Units
De
Umit Tess D-U e
,MkI l," AINATeYSIS R ESIT:T S --
tljf„72
i3rood3ch.6oL{JkM etsi¢nr:
�'�f`6Y
4'1
5a 1
_b
)iJ;�'f
Bimrc-mow
U;1
3�007
Chlor oethane
EPA
601
i-,gi 1
i . 2
?'i �'V��:1y.` ether
'"P,•°�.l
61aI
��
5009
Chloroform'}-1!
0l ry
�'J A
.�'? is�'CYY1. i�i`9Ls� i.,'_'.'�%'•
'i?'i%a.
4-1f i
5017'
1 , 42-D ch oilolie zene
EPA
601
Ugl
3013
1 g 3a4ili�'Ldlor-fi�'e��'zene
�
�4 s
301
b i .ilifN2 1% V .' i 4Y s\
4_._l%'_-
15c,i
�J lr�
21.4
it
5015
8�2 1`e : ,;A wiYLi =` •&�:Y: 2 S F
L a�
!'"Y
I t
1
its' _ _
<< +I
j
c e
J .--

_,3-21-1' Jti 1C 54 FROtI1 LAll) J Ehwii rfaMDATAL T? 91 70ci2516311'20tFi F. 1c
LAW
NATIONAL
I l
TST FORE
to 08/17/80,
2
t ab et 4
8- 9-4109-04
Pi j-ct No.
Ousts No.
Project ?game
MErh--O. SIEWAPAGR DTS aCT
Manager,
a g x 4.,
TOM
nn lta Due . 2 a g
S pl e lsaa orm tioxi
Station I'
TRIP B—LW
S =-o" e m Date 1"-`-Ie .
;' ;
Matrix
W
R-- ei.ved Date./Time
Type pe
{R.An
ceed F r Om /By ,
Received
�7
'Fec4F
1u�
A
tiiof .q}.t
f;
ybo
er Of
_-- Test Date e---
f �qep j s e t
'0
siyy,�•�ES„�� ®a
17,
Dii�++>>4ss�##�..�
1
E-
�>�
i:: 1
_ �sy.
i, ,
d
c_J
? ! i`? 3 '2,..ja+`• 1Ci`d! (;3,` .7z°r>_?=R"i£?$�-1'�' d " cAl
5022 pr`L1y. eerie t�P 'w�•'+�a3 tE f ,g. Q
5023 Methylene Chloride _PA (801 U.g I �a
'�
5025 1 '',.`achl )vors thene Ep . _icea f r, h
,• 'i,�--�
;02 71
-y 1 y 2-Tii.�miahlo it.4reth E"snp-
.}LDS
Si.Y
i
aF.ea'c1 +. t
p r
502Q
f.rich [ o %_✓1 E do *_Jw!--tiync—
�f-
Y0_
g I5030
_
Vinyl.
-
-•fir

-,21-1969 !'-:7:54 FROM LRkl EI-A) I RI-jHflD'JTAL TO 317041-25irG-1311200 P. 13
Lab 'I'li'limbar
"Q -
hlo�
�j
-ly
Rema:,ks -,
04'1.
7
0
042�
PJ Ty! P! 1 --

AUG-21-1969 15:35 FROM L ENVIRONMENTAL TO 9 t2543299200 P.01
(-:-91 1 .
LAW ENVIAD11111 MI . INC.
►,z �or�t+iwic awuE
SOS-5594
FAX NtJM81ER 404-421-0486
* * * • * * * r * + * i * * ♦ * * * * * * * * * * * * * * * * * *
k•
RAMS A-
ZACATsON:
TELE7M0KZ-s - 2f- I �-
i
OtSb[pAHy t /t/ L� -
LOCAfiIONe
TeeUpE A li
(Ple4dt--6=Iude VCUY Idflr, ai►�.e„� na��
THE TOTAL MMmn op pAnB, =CL==r THE. COVER LETTER IS:
IF .YOU Do tM ARCEM W4 of TILE PAUS srr PWID com TxoN, PLEASE
CALL (404) 11M ASR G Yr,'�

AUG-21-1989 15:35 FROM I^" Ef4VIRONMENTAL TO 9""-42543299200 P.02
LAW ENVIRONWTAL NATIONAL LARMTORM
TEST ENTRY FOR14
Date 09/17/89
Page 1
--- Project Information ---
Lab Nunber
89-410q-Oi
Project No.
Cust. No.
Protect Name
ME=. SEWARAGE DISTRICT
Manager:
TOM LAM ONS
Results Due
K�
08/2%/89
--- Sample Information ---
Station ID :
MSA-WM.L-1
Sampled Date/Time :
08/16/8 9 14:30
Matrix :
W
Received Date/Time :
08/07/89 10;00
Type :
GRAB
Received From/By ;
GM/=
Collector :
GM
Chain of custody :
6473
Number of Containtxe
� u �
6
Remarks :
--- Test Data ---
parawator ............. .............
Method....
Units
Det. Limit
Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5002
Eromodichloromethane
EPA
601
ug/1
1.0
5003
Bromoform
EPA
601
ug/1
2.0
XV
500u
Bromozathaae
EPA
601
ug/l
12
�/ n
5005
Carbon tetrachloride
EPA
601
ug/l
1.2
4/ D
5007
Chloroethene
EPA
601
ug/l
5.2
5008
2-Chloroethylv:Lnyl.ether
EPA
601
ug/l
1.3
5009
Chloroform
EPA
6ol
Ug/1
%:;,
n
5010
Chloromethane
EPA
601
ug/1
.G:$' r.C.
X/V
5011
Dibromochlaromethane
EPA
601
u9/1
j —AY,ho
y
5012
1.2-Dichlorobenzene
EPA
601
ug/1
1.5
5013
i,3-Dichlorobenzene
EPA
601
u9/1
3.2
t9
5014
1,4-Dich1orobenzene
EPA
601
ug/l
2.4
X/ o
5015
Dichlorodifluoromethane
SPA
601
ug/l
18
4110
5016
1.1-Dichloroethane
zPA
601
ug/l
_9w3 /.0
&10

AUG-21-1909 15:35 FROM I ENUIRONMEhITAL TO 42543299200 P.03
LAW ENVSRONMENTAL NATIONAL LABORATORIES
TEST ENTRY FORM
]ate 08/17/89
?age 2
-- Project Information ---
Lab Number : 89-4109-01
Project No. : Oust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS Results Due : 08/21/89
--- Sample Infor=tion ---
Station ID : MSA-WELL-1 Samplad Data/Time 08/16/89 14,30
Matrix : W Raceived Date/Timm : 08/07/89 10:00
Type : MM Ramived FroMAY GX/CLM
Collector : GM Chaim of Custody : 6473
Number of Containera : 6
Remarks :
--- Test Data •--
Psi rameter......... -....................
Method....
Units
Det.
Limit
Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5017
1,2 Dichloraethane
EPA 601 .
us/1
0.3
• ; , .�
5018
1,1-Dichloroothane
EPA 601
us/1
1.3
y j2
5019
Trans-1,2-Dichloreethe:te
EPA 6oi
u9/1
1.0
I/
5020
1.2-Dichlompropene
EPA 601
ug/l
A:#—
/r!n
5021
cis-1,3-Dichloropropene
EPA 601
ug/l
3.4
✓'�
5022
Trans-1.3-Dichloropropette
EPA 601
ug/l
3.4
5023
Methylene Chloride
EPA 601
ug/1
2.5
11D
5024
1,1,2,2-Tetrachloroethene
EPA 601
ug/l
0.3
5025
Tetrachloroethene
EPA 601
ug/l
Z4-
1,v
/y O
5026
1.1.1-Trichloroethaae
EPA 601
ug/1
f e
1.0
w
5027
1. 1. 2-Trichloroethane
EPA 601
u9/1
IQ%*,110
5028
Trichloroethene
EPA 601
ug/1
1.2
:f/1,-)
5029
Trichlorofluoromethane
EPA 601
ug/1
3.2
5030
Vinyl Chloride
EPA 601
ug/l
1.8

AUG-21-1989 15:36 FROM ENVIRONMENTAL TO 142543299200 P.04
ate 0h8/17/89
560 J
LAW ENVIRONMENTAL NATIONAL LABORATORIES
TEST ENTRY FORK
--- project Infomation ---
Lab Number :
89-4109-01
project No. :
oust. No. :
Project Name :
METRO. SEWARAGE DISTRICT
Manager:
TOM LAMMONS
Results Due :
08/21/89
--- Sample
Wormation ---
Station ID
MSA-WELL-1
Sampled bate/Time :
08/16/89 14:30
Matrix
W
Received Datc/Timm :
08/07/89 10:00
Type
GRAB
Received From/By
GM/=
Collector
am
Chain of Custody
6473'
Number of Containers
6
Remarks
--- Test Data ---
'arameter ..............................
Method....
Units
Det. Limit Results... Test Date Analyo
-- ORGANIC ANALYSIS RESULTS --
5041 Benzene
EPA
602
ug/1
1.0 14140
3042 Chlorobemene
zPA
602
ug/l
1.0 �
5046 Ethylbenzene
EPA
602
ug/1
L.0 y d
.5047 Toluene,
•IPA
602
ug/1
1.0 /y,/
5200 GC vac SCR"r.=;G

RUG-21-1969 15:36 FROM 1 ENVIRONMENTAL TO 42543299200 P.05
LAW MIRONiDriVTAL NATIONAL LABORATORIES
TEST ENTRY FORM
late 08/17/89
--- Project Information ---
Lab Number : $9-410g-o2
Project No. : Cuab. No. :
Project Name : METRO. SEWARACE DISTRICT
Maneger: TOM LAMMONS Results Due 08/21/89
Sample Information ---
Station ID : MSA-5-1 Sampled Date/Time
08/16/89 13:10
Matrix W Received Date/Time
08/07/89 10:00
Type GRAB Received From/By
GM/CLM
Collector ON Chain of Custody
6473
Humber or Containers
6
Remarks
--- Test Data ---
Parameter..............................
Method....
Units
Dec.
Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5002 Bromodichloromethane
EPA 6ol
ug/l
1.0
5003 Bromororm
EPA 601
ug/1
Z.O.
NYC
5004 Bromomethane
EPA 601
ugll
12
,mil 0
5005 Carbon tetrachloride
EPA 601
ug/1
1.2
.,iV P
;007 Chloraethane
EPA 601
ug/1
5.2
tr 17
5008 2-Chloroethylvinyl ether
EPA 601
ug/1
1.3
41;9
5009 Chloroform
EPA 601
ug/1
04
1:0
_.dL 0
5010 Chloroaethaae
EPA 601
ug/1
,.III-
i I C
,/Vo
5011 Dibromochloromethane
EPA 601
ug/1
►�
,rah
;012 1,Z-Dichlorobenzene
EPA 601
ug/1
1.5
K13 1,3-Dichlorobenzene
EPA 601
u9/1
3.2
5014 IA-Dichlorobenaene.
EPA 601
ug/1
2.4
5015 Dichlorodifluoromethene
EPA 601
ug/1
18
5016 1,1-Dichloroethane
EPA 601
u9/1
04
11b
Y19

AUG-21-1989 15:37 FROM L=NVIRONMENTAL TO 9 t2543299200 P.06
LAW ENVIROHMMAL NATIONAL LABORATORIES
TEST E MY FOPA
,ate 08/17/89
'age 2
--- Project Information ---
Lab Number 82-4109-02
Project No. Oust. No.
Project Name METRO. MARAGE DISTRICT
Manager; TOM LAWNS
Station ID MSA-S-1
Matrix W
Type GRAB
Collector GM
Remarks :
Results Due : 08/21/89
---Sample Information ---
Sampled Date/Time :
08/16/89 15:10
Received Date/Time :
08/07/69 10:00
Received Prom/By :
pM/CLM
chain of custody :
6473
Number of Containers
6
--- Test Data ---
Pammeter ...............0.6....6....... Method.... Units Det. Lla1.t Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5017 1,2 Dichloroethane
WA 601
ug/1
.
5018 l.l-Dichloroethene
EPA 601
ug/1
1.3
5019 Trans-l.2-Dichloroethene
EPA 60I
ug/1
1.0
AID
5020 1,Z-Dichloropropane
EPA 601
ug/1
�6:� 1 G
/`✓ K7
5021 cis-1.3-Dichloropropene
EPA 601
u9/1
3.4
,v.17
50-22 Trans-1.3-Dichloropropene
EPA 601
ug/1
3.4
Ned
5023 Methylene Chloride
EPA 601
ug/1
2.5
'IV 0 -
5024 1.1,2,2-Tetrachloroethane
EPA 601
u9/1
.0.3
.5025 Tetrachloroethene
EPA 601
ug/1
%,0
Y2
5026 1,1.1-Trichloroethane
EPA 601
ug/1
.,Av3- b0
•&19
5027 1.1.2-Trichloroethane
EPA 601
ug/l
4%Pe b o
Alt
5028 Trichloroethene
SPA 601
ug/l
1.2
AIJ9
5029 Trichlorofluoromethene
EPA 601
ug/1
3.2
4Z 0
5030 vinyl Chloride
EPA 601
ug/l
1.8
JV0

AUG-21-1989 15:37 FROM Li '.NVIRONMENTAL TO 9 2543299200 P.07
LAW FTIITIRONXE NrAL NATIONAL LABORATORIES
TEST ENTRY FORM
ate 08/17/89
age 3
Project Information ---
Lab 'Number : 89-4109-02
Project No. : Cust. No. :
Project Name : =R0. SEWARAGB DISTRICT
Manager: TOM LAMMONS Results Duo : 08/21/89
Sample Information ---
Station ID
MSA-S-1
Sampled Date/Time :
08/16/89 15:10
Matrix :
W
Received Date/Time :
08/07/89 10:00
Type
OW
Received From/By :
GM/CLM
Collector
am
Chain of Custody
6473
Number of Containers
6
Remarks :
--- Test Data ---
'2arameter .............................. Method....
Units
Det.
Lindt Results... Test Date Analy
-- ORGANIC ANALYSIS RFSULTS --
5041 Benzene
EPA 602
ug/1
1.0
5042 Chlorobenzene
EPA 602
ug/1
1.0
1, �
5046 Ethylbenzene
EPA 602
ug/1
1.0
5047 Toluene
EPA 602
Ug/1
1.0
504
.EPA 60Z..
•u8/1
5200 GC vOC SCREENING

AUG-21-1989 15:37 FROM L E-WIRONMENTAL TO 9 12543299200 P.08
LAW IWVIRONMMAL NATIONAL LABORATORIES
TEST RN TRY FORM
at* 08/17/89
Aim 1
--- Project Information ---
Lab Number :
89-4109-03
Project No. .
Cuat. No. .
Project Name :
WM0. SEWARACM
DISMCT
Manager:
TOM L.ANIlRM
Results Due :
08/21/89
-- Sample Information ---
Station ID
MSA-S-2
Sampled Date/Time z
08/16/89 15:45
Matrix ;
W
Received Date/Time
08/07/89 10:00
Type
MW
Received Prom/By
cis/CLM
Collector
CM
Chain of Custody
6473
Number of Containers
6
Remarks
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... 'Test Date Andy
-- ORGANIC ANALYSIS RESULTS
5002 Bromodiehloromethane
EPA 601.
ug/l
1.0
5003 Bromoform
zPA 601
ug/l
2.0
5004 Bromomethane
EPA 601
ug/l
12
i005 Carbon tetrachlorift
EPA 601
ug/l
1.2
/V t%
5007 Chloroethane
EPA 601
ug/i
5.2
/t/'+�
5608 2—Chloroethylvinyl ether
EPA 601
ug/1
1.3
/V A
5009 Chloroform
EPA 60l
u9/1
.D, f,
V
5010 Chloromethane
EPA 601
ug/1
Al n
5011 Dibromochloromethane
EPA 601
ug/1
D,.9-i.4
V
5012 1.2-Dichlorobenzene
EPA 601
ug/1
1.5
IV /I
5013 1 3-Dichlorobenzene
SPA 601
ug/1
3.2
'94-
5014 1,4-Dichlorobenzene
EPA 601
ug/1
2.4-
AI
5015 Dichiorodifluoromethane
EPA 601
ug/1
18
�/�
5016 1,1-Dichioroethane
EPA 601
ug/1
=T. 1,0

AUG-21-1999 15: 3B FROM ENV ] ROIAMEhdTAL TO 942543299200 P. 09
LAW MTVIRONMMaAL NATIONAL LABORATORIES
TEST ENTRY FO'W
)ate 08/17/89
'age 2
-- Project Information ---
i.ah Numbest : 89-4109-03
Project No. Oust. No.
Project Name MEMO. SEWARAGE DISTRICT
Manager: TOM LAMMONS Results Due 08/21/89
Sample Information ---
Station ID MBA-3-2 Sampled Date/Time
08/16/89 15:45
Matrix W Received Date/Time
08/07/89 10100
Type GRAB Received From/By
GMJCLM
Collector ON chain of Custody
6473 -
Number of Containers
6
Remarks :
--- Test Data ---
Parameter ..............................
Method....
Urdts
bet. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5017 1,2 Dichloroethane
EPA 601
ug/1
41.3 1-10
5018 1,1-Dichloroethene
EPA 601
u9/1
1.3
/- ^�
5019 Trans-1,2-Dichloroethene
EPA 601
ug/1
1.0
,y_,D
5020 1,2-Dichloropropane
EPA 601
ug/l
K8:# l
/1/ 0
5021 cis-1,3-Dichloropropene
EPA 601
ug/1
3.4
sd--Y!
5022 Trans -I 3-Dichloropropene
EPA 601
ug/l
3.4
'
�K?
5023 Methylene Chloride
EPA 601
ug/i
2.5
IV 0 —
5024 1,1,2,2-Tetrachloroethane
EPA 601
ug/1
0.3
5025 Tetrachloroethene
EPA 601
ug/1
5026 1,1.1-Trichloroethane
EPA 601
ug/2
.4:;3I;t�y
5027 1,1.2-T'richl.oroethane
EPA 601
ug/1
-G.X %; .'
/!1n
5028 Trichloroethene
EPA 601
ug/1
1.2
Ale
5029 Trichlorofluoromethane
EPA 601
ug/l
3.2
/Vo_
%30 Vinyl Chloride
EPA 601
ug/i
1.8

AUG-21-1989 15:38 FROM ENVIRONMENTAL TO D42543299200 P.10
LAW ENVIRDNWTAL NATIONAL LABORATOKM
TEST ENTRY FORM
Sate 08/17/89
Page 3
-- Project Information ---
Lab Numbor 89-4109-03
Project No. oust. No.
Project Nano : MEIM. SEWARAG2 DISTRICT
Manager: TOSS LAMWNS
Sample Information ---
P.esults Due : 08/21/89
Station ID : HSA-S-2 Sampled Date/Time :
o8/16/89 15A5
Matrix : W PAweived Data/Tuna :
08/07/89 14:00
Type : GRAB Recoived From/Sy :
CICLM
Collector : GM Chain of Custody :
6473
Numbor of Contafnera :
6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit results... Teat Date Analy
-- OROANIC ANALYSIS RESULTS --
5041 Benzene
EPA 602
u6/1 1.0
1414
5042 Chlorobenzene
EPA 602
Ug/l 1.0
5046 Et:iylbenzene
EPA 602
ug/1 1.0
5047 Toluene
EPA 602
Ug/1 1.0
y►r✓a
-EPA ..Any
5Z00 GC vOC SCREENING

AUG-21-1969 15:39 FROM ENVIRONMENTAL TO 042543299200 P.11
LAW ENVIRONbWTAL NA=CNAL LABORATORIES
TEST ENTRY FORM
r'nto 08/17; 89
Page 1
--- Project Information
LabNumber : 89-4109-o4
Projaat No. : Cust. No. :
Project Name s METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS Results Due : 08/21/89
Sample Information ---
Station ID : TRTP BLANK Sampled Date/Time : / / .
Matrix : W Received Date/Time : 08/07/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : CM chasm of Custody 6473
Number of Containers 2
Remarks s
--- Teat Data ---
Parnmeter .............................. Method.... Units Det. Limit Results... Teat Date Analy
-- ORGANIC ANALYSIS RESULTS --
5002 Bromodichloromethane
5003 Bromoform
5004 Bromamethane
5005 Carbon tetrachloride
5007 Chloroethane
15008 Z-Chloroethylvinyl ether
5009 0nlorororm
3010 Chloromethane
5011 Dibromochloromethane
5012 1.2-Diehlorobeazene
5013 1.3-Dichlorobenzene
5014 1.4-Dichlorobenzene
5015 Dichlorodifluoromethane
5016 1,1-Dichloroethane
EPA 601
ug/1
1.0
EPA 601
UK/1
2.0
EPA 601
ug/l
12
EPA 601
ug/1
1.2
EPA 601
ug/l
5.2
EPA 6o1
ug/l
1.3
EPA 601
ug/l
..4r5.
EPA 6ol
ug/1
;v.a- /, 41
EPA 601
ug/1
-&wiR. I 10
EPA 601
ug/1
1.5
EPA 601
ug/1
3.2
EPA 601
ug/1
2.4
EPA 601
ug/1
15
EPA 601
ug/ 1
,
'IV0

FUG-21-1989 15:39 FROM ENVIRONMENTAL TO 342543299200 P.12
LAW NATIONAL LABORATORIES
T9 T ENTRY FORM
Date 08/17/89
Page 2
---'Project Information ---
Lab Number : 89-4109-ok
Project No. : Cust. No. :
Project Names : MFTAO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Station ID : TRYP BLANK
Matrix W
Type MAD
Collector CM
Remarks :
Results Due : 08/21/89
--- Sample Information ---
Bampled Date/Time : / / :
Received Date/Time 08/07/89 10:00
Received From/By QM/CLM
Chain of Custody 6473
Number of Containers 2
--- Teat Data ---
Parameter ........ 6.... I ................
Method....
Units
Det. Limit
Results... Test Date Andy
-- ORGANIC ANALYSIS RESULTS --
1,2 Dichloroethane
601
� ; �
5017
EPA
ug/l
0.3
►
5018
1.1-Dichloroethene
EPA 601.
ug/l
1.3
/V d
5019
Trans-1,2-Dichloroetheno
EPA 601
ug/l
1.0
/Y 1�
5020
1, 2-Dichloropropone
EPA 601
Ug/1
¢sue
oy 'D
5021
cis-1.3-Dichloropropene
EPA 601
ug/l
3.4
MT
5022
Trans-1,3-Dichioropropene
EPA 601
ug/l
3.4
,v 4
5025
Methylene Chloride
EPA 601
ug/l
2.5
/ice a
5024
1.1.2,2-Tetrachloroethane
EPA 601
ug/l
0.3
ai= i1.1
5025
Tetrachloroethene
EPA 601
ug/1
"9 ),L
0
5026
1,1,1-Trichloroethene
EPA 601
Ug/1
.0-3--
5027
1.1.2-Trschloroethane
EPA 601
ug/1
$..;p,, 1, t
ri _
5028
Trichloroethene
EPA 601
ug/1
1.2
/Y o
5029
Trichlorofluoromethsne
EPA 601
u9/1
3.2
er-Q�
5030
Vinyl Chloride ,
EPA 601
ug/1
1.8
/1/Q

AUG-21-1989
15:40 FROM
E11V]RONMEh4TRL TO )42543299200 P.13
LAW
ENVIRONMENTAL NATIONAL LABORATORIM
TEST ENTRY FORM
Date o8/17/8g
Page 3
--- Project Information ---
Lab Number :
89-4109-04
Project No. :
Cust. No.
Project Name :
MEMO. SEWARAGE DISTRICT
Manager:
TOM LAWNS
Results Due
08/2i/89
--- Sample Information ---
Station ID :
TRIP BLANK
Sampled Date/Time
s
Matrix :
W
Received Date/Time
: 08/07/89 10:00
Type :
GRAB
Received From/Sy
: GM/CLM
Collector :
GH
Chain of Cuetocly
6473
Number of Containers
2
Remarks
--- Toot Data ---
Parameter .............................. mathod.... Units Det. Limit Results.., Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
5D41 Benzene
EPA 602
ug/l
1.0
AM
5042 Chlorobenzene
EPA 602
ug/i
1.0
10
5046
k'Q-A 6U;d
US/1
1.0
f''� J
5047 Toluene
EPA 602
us/1
1.0
+ 7.1. •
2:0-:
A �..
5200 CO VOC SCREENING
TOTAL P.13

M 5 /D
MSDMetropolitan Sewerage District of
Buncombe County, North Carolina
W. H. Mull, P.E., Engineer -Manager
P.O. Box 8969, Asheville, N.C. 28814
Telephone: Area Code 704-254-9646
Telecopier [phone]
John S. Stevens, General Counsel
S
Z!NNT
Mr. M. Gale Johnson
Permits Group
North Carolina Department of Environment,
Health & Natural Resources
Division of Environmental Management
Post Office Box 27687
Raleigh, North Carolina 27611-7687
Frank S. Smith III, Chairman
M. Leon Williams, Vice -Chairman
Steven T. Aceto
Charles M. Dent
E. Charles Dyson
M. Wayne Edwards
George E. Ivey
Richard P. Maas
Diane K. McDonald
Jackie W. Pope
Marvin E. Waddey
August 21, 1990
Subject: Asheville Storage Lagoon, Buncombe County GW 90192
Dear Mr. Johnson:
Submitted herewith are two (2) copies of Law Engineering's "Report of
Monitoring Well Installation and Ground Water Chemical Analysis", dated August 2,
1990, that should provide the additional data requested in your July 16, 1990 letter.
The four recommendations contained in this report are proposed as conditions
of your permit approval. T.he -construction of the Sludge Incineration Facility began
last month and we hope not to, delay the Contractor for any of his equipment
approvals or construction related to ash disposal in the lagoon.*
We will be glad to meet with you to answer any questions or concerns about
this permit request.

Mr. M. Gale Johnson
\Permits Group
North Carolina Department of Environment,
;Health & Natural Resources
August 21, 1990
Page 2.
To help expedite your reviews, we have hand -carried one (1) copy of this
report to Mr. Don Link, Asheville Regional Ground Water Supervisor.
Thank you very much for your efforts in reviewing our permit request.
Very truly/yours,
W. H. rV q]1, P.E.
Enginee anager
WHM/cnr
Enclosures
cc: UV Don-L_irik, W/enclosure
Mr. Cecil G. Madden, w/enclosure
Mr. Robert E. MacPhee
Mr. William Morris
Mr. Robert Holbrook

e STATE
333 '1 3 S.
State of North Carolina
Department of Environment, Health, and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
I
James G:'Mardn, Govemor
William W. Cobey, Jr., Secretary
August 24, 1990
Mr. William H. Mull, P.E.
Engineer -Manager
Metropolitan Sewerage District of Buncombe County
Post Office Box 8969
Asheville, North Carolina 28814
Dear Mr. Mull:
George I Everett, PKD.
Director
Subject: Pretreatment Permit
Groundwater Remediation Program
Metropolitan Sewerage District
Buncombe County
I am informed by, Mr. Roy Davis of this Division's Asheville
:.Regional Office, that you are hesitant to accept pretreated
groundwater into the collection system of the Metropolitan Sewerage
District (MSD) out of concern that such action would:
1) Require the issuance of a pretreatment permit having a TTO
limit.
2) Require monitoring by the MSD of all other pretreatment
permit discharges to the MSD for the same pollutants which
would enter with the groundwater.
3) Require the MSD to prepare a new headworks analysis, and
4) Ultimately lead to the issuance of a revised NPDES Permit
with new limits and monitoring requirements.
For all practical purpose none of the above is correct.
Permits for groundwater remediation pretreatment systems
discharging to POTW's, must be issued in accordance with the
requirements of Title 15A; NCAC 02H .0916 and .0917. However, these
dischargers are not significant industrial users (SIUs) unless they
meet the criteria established 15A NCAC 2H.0903(b)(9). I find it
unlikely that any properly designed groundwater -remediation project
ronutlon Pre ern m rays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]

with an average daily flow of less than 25,000 GPD would need to be
considered an SIU. Therefore, it is unlikely that any of
concerns would be realized. your
i
This Division 'encourages the use of POTW's by groundwater,
remediation projectsl wherever possible. In compliance with the
regulations and in order to ensure that POTWs do not have to deal with
concern such as those discussed above, the Division reviews
pretreatment permitsi issued to groundwater remediation projects.
However, unless a specific project is identified as an SIU, it will
not be necessary for; the POTW to; submit the data, track or, provide the enforcement action verification that compliance
are required for
SIUs in the pretreatment program.
1 -
I would suggest that you continue to draft and submit
pretreatment permits for groundwater remediation projects in
accordance .with your approved program. Should the occasion arise that
the Division's Staff feels that a specific project might be considered
an SIU, we will work with MSD to establish pretreatment permit
conditions which woulid preclude the need to assign the project SIU
status.
I sincerely hope 1I have answered some of your questions relating
to this issue. Please do not hesitate to contract me if we need to
discuss this matter fulrther.
i
Sincerely,
xc: George
Steve
Trevor
Perry
Roy M.
T. Everett
Tedder
Clements
Nelson
Davis
Douglas S. Fi an
Pretreatment Program Coordinator

'State 6f North Carol!
Department of Eftroi(Irnent,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. W. H. Mull, Eng. Mgr.
Post Office Box 8969
Asheville, North Carolina 28814
Dear Mr. Mull:
�EHNR
August 29,1995
Subject: NPDES Permit Issuance
Permit No. NCO024911
MSD Buncombe County WWTP
Buncombe County
In accordance with the application for a discharge permit received on November 30, 1993, the
Division is forwarding herewith the subject NPDES permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between
North Carolina and the US Environmental Protection Agency dated December .6, 1983.
If any parts, measurement frequencies or sampling iequirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30)
days following receipt of this letter. This request must be in the form of, it written petition, conforming to
Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative
Hearings, Post Office Drawer 27447, Raleigh, North Carolina"2761;1-7447. Unless such demand is
made, this decision shall be final and binding.
Please take notice this permit is not transferable. Part Il, EA addresses the requirements to be
followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be required by
the Division of Environmental Management or permits required by the Division of Land Resources,
Coastal Area Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Susan Wilson at telephone number
[phone], extension 555.
Sincerely,
Original Signtd By
DAvld A. Goodrich
A. Preston Howard, Jr., P.E.
cc: Central Files
Asheville Regional Office
Mr. Roosevelt Childress, EPA
Permits and Engineering Unit
Facilities Assessment Unit
Aquatic Survey and Toxicology
Technical Assistance & Certification Group
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
Telephone [phone] FAX [phone]
60% recycled/ 109% post -consumer paper

Permit No. NCO024911
STATE OF NORTH CAROLINA,
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-2IS. 1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Mangement Commission,
and the Federal Water Pollution Control Act, as amended,
Metropolitan Sewerage District of Buncombe County
is hereby authorized to discharge wastewater from a facility located at
NC Highway 251
north of Asheville
Buncombe County
to receiving waters designated as the French Broad River in the French Broad River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts 1,
II, and III hereof.
The permit shall become effective October 1, 1995.
This permit and the authorization to discharge shall expire at midnight on September 30, 2000.
Signed this day August 28, 1995.
Original Signed By
David A. Goodrich
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Mangement Commission

12.. Record Keeping
The permittee shall retain for a minimum of three years records of monitoring activities
and results, along with support information including general records; water quality
records, and records of industrial impact on the POTW;
13. Funding aiid Financial Report
the peiniilite& 'shall maintain adequate funding Arid staffing levels" to accomplish the
objectives of its approved pretreatment prograiri
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local
limits modifications, POTW monitoring of their Significant Industrial Users (SIUs),
and Monitoring Plan modifications, shall be considered a permit modification and shall
be governed by 15 NCAC 211.0114 and 15A NCAC 2H .0907.
No construction of wastewater treatment facilities or additions to add to the plant's treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until
Final Plans and Specifications have been submitted to the Division of Environmental
Management and written approval and Authorization to Construct has been issued.
The permittee shall, upon written notice from the Director of the Division of Environmental
Management, conduct groundwater monitoring as may be required to determine the
compliance of this NPDES permitted facility with the current groundwater standards.
MEMN • J-1 •:,
All POTWs must provide adequate notice to the Director of the following:
I. Any new introduction of pollutants into. the POTW from an indirect discharger which
would be subject to section 301 or 306 of CWA if it were directly discharging those
pollutants; and
2. Any substantial change in the volume or character of pollutants being introduced into
that POTW by a source introducing pollutants into the POTW at the time of issuance of
the permit.
3. For purposes of this paragraph, adequate notice shall include information on (1) the
quality and quantity of effluent introduced into the POTW; and (2) any anticipated
impact of the change on the quantity or quality of effluent to be discharged from the

DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
March 5, 1991
MEMORANDUM
TO: Jack Floyd, Groundwater Section _
Raleigh Central Office
FROM: Fred C. Hankinson, Hydrogeological Technician
Asheville Regional Office
SUBJECT: Carolina Power & Light Asheville Steam Plant
Ash Disposal Program
Permit No. WQ0004714
This application is for renewal of general permit No. 13407 allowing the
use of ash for structured fills, brick mixtures, secondary road overlay, etc.
These uses decease discharge to the fly ash basin and do not require
groundwater monitoring at this time. Any groundwater quality monitoring, as
deemed necessary by the Division, shall be provided as in the existing permit.
.;
FCH/gc

/- C iz
DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
MEMORANDUM
TO: zery-, L-i ,ti 1C-
DATE: Feb Zo, Iqq 1
FROM: Jack Floyd%
w r ' 7 4-- "
4-0 1'e- 4
SUBJECT: Application for—�LRenewal/Amendment of Permit No.
New Permit
Facility Name C1��- - A<skevo Ili der m pla%,t A-,h 17ispbs0.l
n
County I�c'Yc e�� PAO 9 Pa nq
Type of Project: �,� 1�o`C4 �rcgmm
Central Office Contact: (J&cC)gcl
Applicable Permit Numbers: WQ 000M--1 q GW Q/vS 7-
EPA AC
We have received a copy of the above referenced application,
which was sent to your regional office for comment on or about
Pe_b Z7 , 1991
You should review the application package for completeness
and adequacy of relevant information and submit your request for
additional information to me (via telephone or memo) by
Imp ( , 19glso that all required information can be
requested from the applicant at one time. A copy of our formal
request to the applicant for additional information will be
provided to you.
If you do not require additional information from the
applicant to complete your evaluation of the project, you should
review the application package and submit your comments to me by
fwo-.L 1 , 1991
If a copy of the application package has not been made
available to your office, PLEASE LET ME KNOW IMMEDIATELY so that
a copy can be forwarded to you as soon as possible.
JF:ja/Appl.shl
FEB 2 2 1991
nd
lie

1- 9-92 11:03
State of, North Carollm
Department of ErMrmment. Health, and Natural Resourm
DW*n of FxMrcnmenW Management
512 North Salsburl Street 0 Raleigh, North Cmdna 27611
IN= C& NWft. Caverwr
Wuvn W. COW Jr, Secretary
March 11, 1991
Ceo*T. Everett DhWAW Ph.D.
I . . . . . . ...JI
..
ym of Bm=te Cmanty
"hwille, 11orth Ca=jina 26807
pL= 10=MU C=ty MW use 1%'
Permit No., =0024913.
?mWamt, to
Alithwizatim to Comtn=t
A Pz jet No, C370391-09
EP
BuncoffibO Camtl'
Dear Mr, Nall:
m7
tion for the OvJ%t project hae'bom A supporting documnta
reviewed
satisfactory, - -
and fCUrA to be
sat Novetabor 17, 3.989, is
The Autharizatim to Construct, ism
he=W wended to allow use of the existing AIUd96 '3t0mg4 lag= AS
T itions.
following additional cmd
ash storage lagoon, subject to the
All in the Authoriziti= to C0n9+LMCt ismmd
resin in full f=* and affect,
The amwAnd Autl=izAtIm to Constn= is issued in accordame
idth Part -IM' paragraph
-C of tTM pe=ijt m, N00024911i iammd JWm
"
&all be B*Jwt to rGV=tiCn Unleas the mastmatOr
in accordance with the al:
Inwtea
tmtmt facnities are om!ikt
isl and are in cC
conditMIiAyd*
plump rpscificaitiow, ArA suMorting do=mt
nmitutjws specified inperr,%Jt tic. MC002491L.'
with the ms arA
acmptable sludge anslysis and a
The Parmittee shall have an
slu&je T(micity characterisUc Leachate Proaed=e (T.C.L.P.) armlyGiB
Di -vision of Environmental manWORKMt,
which have been approved by the
water Quality Mee= prior to the disposal of any shidge fm the now
vast water =6Cktmmt Plant. Copiesof the analyses, mpPort:Im
40=mats, and apprmals shall be witmitted to the Divicion of
k ■Ashwille regional Office.
1,
V'M
R 5A ;�ffl
foftikm PWAUftP PAP
TeIemh&-w9I%-735-7015

�p i ,�Fa#'
ear}i�
Page 2 '�'''� /'�� l/
>{4, 11w aludg,e and or ash generated from these treatment faciIJUSa
Y'r =0t be diapoead of in acc=%Unce with G.B. 143-215,1 and in a manner
�ec7 by the North Carolina Division of Pnvironmantai YAnagemnt.
sposing, selling or fret distribution of wet, dried, mmpostad
sludge or sludge -like materials frcm wastrawater facilities witi'mt
prior review and approval by this Division will be auY;ect tQ the
enf=erent authority of the Environmental manaqamnt Cannission.
Within 24 montho of this approval, the Farmittae shall. provide a
fQemal Plon f= removal and final dispcsal of the solids from this
lagoon, or aun=Cr method of handling ash genaratecl by the incinerator.
1r The three (3) existing mvnitar wells shall be supled every
February, . Jl use , and Septwiber for the following Palrametsers t
NO (10, 0) Am ania I�itsogQn
TR (500.0) TOC
PH (8.5-8.5 standard units) Water revel
Chloride (250.0) Total Ce1iforms (1I10(hl)
Arsenio (0.05) Barium
Cadmim� (0.005) Chromitau (0,05)
Lead l0.05) mroury
seiemt= silver
T,s*S, (Total S165pended Solids)
volatile Organic OaPounda - Zn September Only (by
method 1 or 2 balm)
Method 1: Method 6230D (Capillary - Column), "Starlaard
Methods for The Ex=natien Of water arA
Wastawater", 17th ad,, 1989
Method 21 Method 502.2 "Mthods For The Deterntinatlon Of
Organic Cmq=unds In Drinking Water", U.S. FIFA
- 60014-8®1039
The and*0=etn mt of wat air IVmI toast be made prior to em plisag ftr
the remaining parmv t rs.
'n a measuring points (top of well easing) of e.11 monitoring wells
srieil be surveyed relative to man sea level (1�=, s.L.) . The depth
of water in each well shall be m msured fran the surveyed point on
the top of the casing. The water level elevations shall then be
determirad relative to M.S.L.
The numbers it, parentbames represent th,s maxim= allowab3..s
content ration in roursdwater for the various ana3y tical
parameter`s, ae s 15 NrAC 2L {Groundwater
Classifications and- Standards) . Unless otherwise specified, tht
units for these concentrations axe expressed as milligrarr+s per
liter.

1- 9-92 - 11;02 --_ - ',SDI ; _704'7ff
Page 3
1
If TOC concentrations greater titan 10 rq/1 are &tactmd in any
�r dosvngradiint indniteriryg well, additional searplinq az,d analysis
A rust be c onduCted to i,dmtify the individual conftitwnts
ccr*rising this TW wncentration. if the TOC concentration as
yAy;, ` mea►eured in the back end monitor well excesda 10 me this
concentration wi het an to represent the naturally occwring
TOC concentration. Any exceedances of this Naturally occurring
, ...:;. Toe oono"tration in the downgradient wells shall be avbject to
`... the additional sampling and analysis as desaribed above.
I€ any volatile organic ccupowxWo are datefted by method 623CO,
cr the equivalent rmthod 502.2, then EPA methods 604 and 611 must
also be run to detect ether •organic you -xis which mmy be
present. The results of all analyses specified in the monLi t orittg
requirewnta, including 604 and 611 if raxed, st gWmube aurmitt*d
simItarwouzly:
• f
The results of the . ampling and analysis shall be sent to the
North Carolina Division of Environmental-Managwmt on Form Gw-59
(Cactali,ance Vwitoring Report Fozm) every March, july, October.
2. The liance, Bour�det�.y. fox the disposal system is specified by
rea'in 15 MAC 2L, Groundwater Classifications Ord
5tAndards. An''exceWance of (kour&Ater quality Standards
b yond the Ccirpliance Boundary is subject to the penalty
pmpisiena applic&le under General statute 143-215.6 (1) a. The
sale of pm+oPe=ty, , by the Pe=&ittes, which is within or contiguous
to the disposal sits, may alter the Location of the Ccriplience
- Houraiexy.. ,
For faoiliti*x parnLitt&i prior to December 30, 1983, the
Cmpliancre bour4ary is cetablished at a distame of 500 feet frcu�
the waste disposal lagoon, or the property boundary, whichav4r is
lass.
If the title to any proparty,- which my af£aat the lorAtien of the
Cangliance B=xl ry is changed, the Pun-ittee shall Notify the DM
DirectGi' within 14 days. The Director shall theft satablish a
modified Oenpliance Boundary which will be dace as a< mXLificaticm
to the Pe=ni.t.
The REvM BC+ONDM for the dioppeal system is specified by
requlat cna n 2L, Croundwactrar Classifications and
Standards. A REVIEW BOUMPM is established around disposal
systems midway Fetweean t e�iian(e Boundary and the perimeter
of the waste diepl area. When the aerxzntratior: of any
substance eg"is; or excAeda the maximaa allowable concentration of
that substance at the Fmv Rv SaUN MY, as determirwd by
nonitoring, the Fwzittee!' s gal MT=r (i) denwotrate, ti =qh

.4SD�: 704:..267
nuvrw r
Page 4
prsdiative calculatbzns or mocloling, that natural site conditions,
facility design and gmrational controjs will Fee=t a violation
of standards at the OmVliance EQumlaxyl or (U) submit a plea
for the alteration of existing cite candit`orm, facility design at
operational controls that will grement a violation of staneLmras at
the ftplLu= $onndary, and iRPIMent that plan upon its approval
by tv3 Director.
3* Any additional groundmter quality mmit=ing, as deemad t msaary
by the Division, ahhall ba provided.
If yQu have any questions or :teed additional information, please
contaat Mr. sill Hoffman, at [phone].
CiGMaak .
cc . ilera= Engineering
&. Dennis Ranmy
bt. Don Safrit
Mr, Jyh C. Lin, Health services
Asheville Regional office
CE - Charlotte
EPA
Mr. Tw F'ahnest,ock
bir, Dori LVane
Mrs. Valerie Lancaster
Mr. Cecil Madden
Pm
GPP

SM110
NORTH CAROLINA DEPARTMENT OF .
"3 ENVIRONMENT, HEALTH & NATURAL RESOURCES'
59 Woodfin Place, Asheville, North Carolina 28801
704/251-6208 (Phone) 704/251-6452 (FAX)
TO:
w
FAX NO.:
FROM:
..?-.�
a
DATE:
A V,
W
Number of Pages,
including cover
page:
COMMENTS:

State of North Carolina
Department of Environment, Health, and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor November 17, 1989
William W. Cobey, Jr., Secretary
Mr. William H. Mull, Engineer -Manager
MSD of Buncombe County
P. 0. Box 8969
Asheville, North Carolina 28807
R E C E I V E D SUBJECT:
Water Quality SectiOT
i
NOV 2 7 1989
R. Paul Wilms
Director
Buncombe County MSD
Permit No. NCO024911
Authorization to Construct
Wastewater Treatment Facilities
EPA Project No. C370391-08
Buncombe County
Dear Mr. Mull: ,Asheville Regional Office
,Asheville, North Carolina
The final plans and specifications for the subject project have been
reviewed and found to be satisfactory.
Authorization is hereby granted for modifications to the existing 40
MGD wastewater treatment facility to consist of the following items:
A non -potable water supply system to consist of a raw water pump
station and a 174 GPM non -potable water treatment system including
flocculation dissolved air flotation sand filtration system, an alum
storage tank, an alum feed pump, a polymer feed tank with an electric
mixer and a polymer feed pump, dual non -potable water service pumps,
and dual hydropneumatic tanks.
A constant pressure water reuse pump station with three (3) 1,300 GPM
turbine pumps, one (1) 200 GPM turbine pump and a flow meter with
strainer.
Modifications of the existing two (2) 100 foot diameter digestion tanks
including removal of existing tops, existing piping, existing draft
tubes; and installation of new perth gas piping/mixing, new recircula-
tion piping, two (2) new dual membrane reticulated dome tops; modifi-
cation of existing digester control house including dual 25 Hp circu-
lation pumps, dual water to sludge heat exchangers, and four (4) 200
SCFM positive displacement digester gas blowers; and a new 2,283 square
foot generator (digester gas) building with four (4) 400 GPM recircula-
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

- 2 -
tion pumps, dual water to water heat exchangers, dual 2,800,000 BTU/THR
sludge heaters, dual heat engines with 450 KW generators, three (3)
digester gas filters, and modification of three (3) existing gravity
thickened sludge pumps to yield 360 GPM capacity.
A new sludge handling facility with 25,920 square foot heated building,
to house two (2) 6,000 gallon bulk liquid polymer feed equipment;
sludge d.ewatering equipment with four (4) two -meter gravity belt
thickeners, two (2) 240 GPM gravity belt thickened sludge pumps, three
(3) two -meter belt filter presses, three (3) 70 GPM belt dewatered
sludge pumps, two (2) two -meter ultra press filters, and two (2) dry
cake positive displacement feed pumps, with a thermal converter system
including duel preheat blowers, an air to air heat exchanger, dual
fluidizing air blowers, a 17 foot diameter fluidizer bed thermal
converter, venturi gas scrubber with dual scrubber ash pumps, an 18
foot diameter ash thickener, dual 125 GPM thickened ash pumps, a
building drainage/sidestream pump station with three (3) 825 GPM
submersible pumps, the lime stabilizaticn system including lime
storage, a 10 foot diameter weight hopper, dual lime slakers, dual 150
GPM sludge grinder pumps, a 3,750 gallon lime mixing tank with a 7.5 Hp
mixer and dual lime transfer pumps, three (3) lime slurry transfer
pumps, a 14 foot diameter slurry stabilization and storage tank with 15
Hp mixer; a 600 KW steam turbine generator system including boiler
feedwater equipment, deaerating heater, waste heat boiler economizer
and the steam turbine, associated yard pipe, electrical work and site
work.
Do not proceed with construction until the Authorization -to -Award
package, EEO, and MBE documentation/certification have been reviewed, and
you are in receipt of our approval, if Federal funding is desired for
project construction.
The permittee shall employ an actively State certified wastewater
treatment plant operator to be in responsible charge of the wastewater
treatment facilities. Such operator must hold a valid State Certificate of
the grade at least equivalent to the classification assigned to the waste-
water treatment facilities by the Certification Commission. When a new
chief operator must be obtained to be in responsible charge of the new
facilities, it is required that this be done by the time the construction of
the facilities is 50% complete.
The Authorization. -to -Construct is issued in accordance with Part III,
Paragraph C of NPDES Permit No. NC0024911, issued June 15, 1989 and shall
be subject to revocation unless the wastewater treatment facilities are
constructed in accordance with the approved plans, specifications, and
supporting doeume_nrs; and are in. compliance with the conditions and
limitations specified in Permit No. NC0024911.
This Authorization. to Construct does not imply approval. of the use of
the existing sludge storage lagoon as an ash storage lagoon. A separate
submittal with all supporting documentation requesting permission. to use the

- 3 -
existing sludge storage lagoon as an ash storage/disposal lagoon must be
presented for review and approval to the Water Quality Section of the
Division of Environmental Management prior to placing the thermal converter
into operation.
The permittee shall have an acceptable sludge analysis and a sludge
E.P. toxicity analysis which have been approved by the Division of Environ-
mental Management, Water Quality Section prior to the disposal of any sludge
from the new wastewater treatment plant. Copies of the analyses, supporting
documents, and approvals shall be submitted to the Division of Environmental
Management's Asheville Regional Office.
The sludge and or ash generated from these treatment facilities must be
disposed of in accordance with G.S. 143-215.1 and in a manner approved by
the North Carolina Division of Environmental Management. The disposing,
selling or free distribution of wet, dried, composted sludge or sludge -like
materials from wastewater facilities without prior review and approval by
this Division is illegal.
During the construction of the proposed additions/modifications, the
permittee shall continue to properly maintain and operate the existing
wastewater treatment facilities at all times, and in such a manner, as
necessary to comply with the effluent limits specified in the NPDES Permit.
In the event that the facilities fail to perform satisfactorily,
including the creation of nuisance conditions, the Permittee shall take
immediate corrective action, including those as may be required by this
Division, such as the construction of additional. or replacement wastewater
treatment or disposal facilities.
You are reminded that it is mandatory for the project to be constructed
in accordance with the North Carolina Sedimentation Pollution Control Act,
and, when applicable, the North Carolina Dam Safety Act. In addition, the
specifications must clearly state what the contractor's responsibilities
shall be in complying with these Acts.
One (1) set of final approved plans and specifications is to be
forwarded to you, one (1) set to the Environmental Protection Agency (EPA),
and one (1) set to the Corps of. Engineers.
A copy of the approved plans and specifications shall be maintained or.
file by the Owner for the life of the project.
Upon completion of construction_ and prior to operation of this
permitted facility, a certification must be received from a Professional
Engineer certifying that the permitted facility has been installed in
accordance with the approved plans and specifications. Mail the Certifica-
tion to the Permits and Engineering Unit, P. 0. Box 27687, Raleigh, North
Carolina 27611-7687. (Engineer's Certification. Form is attached.)

- 4
i'
% JT�
_r
If you have any questions or need additional information, please
contact Mr. Bill Hoffman, at [phone].
i
Attachment
CGM:vk
cc: Hendon Engineering
Mr. Dennis Ramsey
Mr. Don Safrit
Mr. Jyh C. Lin, Health Service
Asheville Regional Office
CE - Charlotte
EPA
Mr. Tom Fahnestock
Mr. Don Evans
Ms. Valerie Helms
Mr. Cecil Madden
Mr. John Campbell
EMU
GPF
S ncerely,
R. Paul Wil

SENT
(� nG:rm
--`0GPF
DIVISION OF ENVIRON11ENTAL MANAGEMENT
GROUNDWATER SECTION
April 11, 1989Qf
TO: Mr. Cecil Mad -den
Construction Grants
APR ? ? 1989 :`i ,-
J G2P,i� !.� cCi,��id
FROM: Mil k.e Cleary mpe ; :'NE iti iGr';'ii�fl ,GEr%F(�) ^: ;
Groundwater Section
SUBJECT: Buncombe County MSD �, Asheville Regional Office
C370391-01
Buncombe County
We are: in receipt of the materials concerning the
subject ash. storage lagoon. The following additional
information is needed for our review of. the 'project:
]_. A site -specific map of the lagoon site, with
topographic contours (contour interval should not
exceed 10 feet or 25 percent of total site relief,
whichever is less), show-ng property` boundaries
and the location of all wells, springs, lakes,
ponds, or other surface drainage features within
500 feet of the lagoon. Wells should be labeled
as to their primary usage (drinking water, process
water, monitoring, etc.)
2. Construction details for existing lagoon, if
available.
3. A characterization of groundwater quality in the
vicinity of the lagoon. This characterization
should be accomplished by the installation of
monitoring wells for -the purpose of describing the
lithology in the area, and for collecting
groundwater quality samples from the water table
aquifer. The locations, well construction details
and sampling methods should be by approval of the
Asheville Regional Office, from which a well
construction permit must be obtained.
Groundwater samples shall be obtained from each
monitoring well and analyzed for the following
parameters:
Nitrate pH
Total Dissolved Solids Chlorides

7
}
A
Total Coliforms Sulfate
Total Organic Carbon Water Level
Ammonia Nitrogen Cu, Cd, Zn
TOX
The measurement of water level'should be taken
prior to sampling for the other parameters.
Lithologic logs, well construction details and the
analytical results of the sampling should be
submitted to the Groundwater Section, Division of
Environmental Management.
Since the existing unlined sludge lagoon has been in
operation for 20 years, and it is known that bedrock occurs
at shallow depths on the site, there is a strong likelihood
that groundwater contamination has occurred in the vicinity
of the lagoon. As such, this site may not be suitable for
the proposed storage of ash. The Groundwater Section has no
objection to issuance of a permit to construct the
incinerator, provided that the applicant is made aware than
an alternate method of ash disposal may be necessary.
Please .feel free to contact the Groundwater Section, at
[phone], if clarification or information is required.
MDC/ tej
cc; Bob Cheek
Mike Cleary
Central Files
Permit Issuance Files

DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
April 21, 1989
MEMORANDUM
To: Bill Hoffman, Supervisor
Engineering Management Unit
Construction Grants
Through: Roy M. Davis, Regional Supervisor IV
Division of Environmentat Management
Forrest R. Westal
Regional Water Qu upervisor
From: Max L. Haner
Environmental Chemist / ARO—AW4
Subject: Staff Recommendations
Authorization to Constr,zct Approval
MSD of Buncombe County (NCO024911)
Sludge Dewatering/Incineration Project
EPA Project No. C370391-08 W
Subject project has been reviewed and found acceptable with
addition of a few minor items. The proposed wastewater
treatment plant improvements concern construction of the sludge
handling part of the facility and pri:narily includes
modifications to the existing digesters and digester -control
house, modifications to the sludge thickener pumping station,
and construction of the sludge handling building to house in
part the belt filter presses, the thermal convertor (fluidized
bed incinerator), the ash thickening and stabilization units
with transfer to the sludge lagoon, and the venturi scrubber
(air emission). This sludge handling project is not referenced
as a part of the existing JOC or its proposed amendment. The
only requirement is that the RBC-microscreen facility be in
compliance with final limits contained in NPDES permit on or
before October 1, 1990 (proposed JOC amendment). Construction of
this project should not interfere with or result in compliance
problems with the overall treatment facility as long as the
Order of Construction, Item 33 on page 6-16 of the
specifications is followed and the full RBC system is in
operation prior to cleaning and modifications to the digesters.

PPPPPPP'
Page 2
April, 1989.Memo
MSD Sludge Handling
In review of the work proposed for cleaning of the
digesters prior to modification, an observation due to the age
of the facility is that the bottom'30-40% of each unit is likely
to contain grit and other solids which cannot be pumped but will
need to be removed by clamshell or other such mechanic -al
equipment. Also, this material will be extremely odorous and
should be treated with lime for stabilization prior to
depositing in a part of the sludge lagoon. Due to the expected
consistency of this bottom material, it should already be
weighted such that a curtain or screen considered for placement
in the lagoon to keep this material in a single area should not
be necessary. This office does concur that separate approval for
the final disposal area for the ash from the thermal convertor
is proper and it is so recommended. However, to rule out future
use of the sludge lagoon for final ash disposal at this time
would not be appropriate. A final agency position on this
question should be reached following submission of a complete
permit application for ash disposal.
Washwater from cleaning of the digester after solids
removal should be directed to the head of the wastewater
treatment facility. Problems with existing valves should be
corrected before digester work begins to allow the washwater to
handled in this manner.
Upon resolution of the above items and satisfactory `
engineering review;; it is recommended that the approval be
issued.
xc: Don Link
Mike Cleary
MLH

/ySO
&"e'" d" .z
LAW ENGINEERING
geotechnical, environmental & construction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
[phone]
November 1, 1989
State of North Carolina
Department of Natural Resources
and Community Development
Division of Environmental Management
Groundwater Division
P.O. Box 370
Asheville, North Carolina 28802-0370
Attention: Mr. Don Link
Subject: Report of Ground Water and Surface Water Chemical
Analysis
Metropolitan Sewerage District
Highway 251
Asheville, North Carolina
Law Engineering Job Number AVE-2265
Gentlemen:
Attached is a copy of the Report of Ground Water and Surface Water
Chemical Analysis for samples collected from one boring and springs
located on the Metropolitan Sewerage District Plant property.
If you have any questions concerning the data submitted please do
not hesitate to call.
/jgw.a
Sincerely,
7er�t
gMacPhee
ERI
H - ogeologist
ff
Hy
L. Lammons
Environmental Services Manager
fib✓ %3 1�?f;y
GrUUndwafer Section
ftieville RpjQional Office
Eii 9
L i ��

ALLAW ENGINEERING
geotechnical, environmental & construction materials consultants
1100 THOUSAND OAKS BLVD.
GOLDEN OAKS BUSINESS PARK
GREENVILLE, SOUTH CAROLINA 29607
[phone]
October 27, 1989
Metropolitan Sewerage District
P.O. Box 8969
Asheville, North Carolina 28814
Attention: Mr. William H. Mull,
Subject: Results of Ground -Water and Surface Water
Chemical Analysis
Metropolitan Sewerage District
Asheville, North Carolina
Law Engineering Job Number AVE-2265
Gentlemen:
As authorized by your acceptance of our work Authorization Sheet,
dated September 27, 1989, Law Engineering has completed the sampling
and chemical analysis of the ground water from the one piezometer
and the two surface water springs/seeps at the site in Asheville,
North Carolina.
The field sampling effort, which was conducted by Mr. George
Maalouf, entailed the following tasks:
'1. On August 15 and 16, 1989 the appropriate sampling
containers were assembled and prepared with the necessary
preservatives. The Law Environmental National Laboratory in
Kennesaw, Georgia was informed of the sampling event and the
date they would be receiving the samples.

Metropolitan Sewerage District
Law Engineering Job Number AVE-2265
October 27, 1989
Page 2
2. On August 16, 1989 three samples were collected from the
piezometer and from the two springs/seeps. Prior to
collection of the ground -water samples the bailer,
constructed of a 3 foot long 1.6 inch diameter teflon pipe,
was decontaminated with the following procedures:
a) Laboratory detergent and distilled water rinse;
b) Dilute hydrochloric acid rinse;
c) Pesticide grade Isopropanol rinse; and
d) Distilled water rinse.
Ground -water pH and specific conductivity were measured in the field
at the time of sampling.
The surface water samples from the springs/seeps were not of
sufficient depth to allow submersion of the sample containers, and
therefore depressions were scooped out of the channel bottom and
allowed to clear prior to sampling.
3) The samples were collected into the appropriate vessels
(VOA vials and 1 liter glass and plastic jars), marked with
identifying numbers and shipped in a refrigerated container
by overnight carrier to the Law Environmental National
Laboratories in Kennesaw, Georgia for analysis. Appropriate
chain -of -custody records were maintained.
4) The samples were analyzed for halogenated and aromatic
volatile organics (EPA Methods 601 and 602), Acid Base
Neutral Extractables (semi -volatile, EPA Method 3510/8270)
and for eight selected metals (arsenic, barium, cadmium,
chromium, lead, mercury, selenium, silver).
LI

Metropolitan Sewerage District
Law Engineering Job Number AVE-2265
October 27, 1989
Page 3
Laboratory analyses indicate that trace concentrations of 1,2-
dichloroethane and chlorobenzene are present. (The trace levels of
1,2 dichloroethane may be due to possible laboratory contamination.)
Concentrations of all other parameters tested was below North
Carolina's Maximum Contaminant levels (MCL's) and therefore no
direct regulatory concern is implied.
We appreciate the opportunity to provide our professional services
during this project. If you have any questions concerning this
report, please do not hesitate to call.
Sincerely,
LAW ENGINEERING
Robert E. MacPhee
Hydrogeologist J
�Z
Thomas L. Lammons, P.G.
Environmental Services Manager
/jgw.b

LAW ENVIRONMENTAL, INC.
1 `w 112 TOWNPARK DRIVE
KENNESAW,GEORGIA 30144-5599
404-421-3400
September 12, 1989
Law Engineering, Inc.
1100 Thousand Oaks Blvd.
Greenville, SC 29607
Attention: Tom Lammons
LE Job Number: AVE-2265
LENL Job Number: 12024
Subject: Chemical Analysis of Samples Received
on 8/17/89
Dear Mr. Lammons:
Law Environmental National Laboratories has completed its
analysis of your samples and reports the results on the following
pages. These results relate only to the contents of the samples
as submitted. This report shall not be reproduced except in full
without the approval of Law Environmental National Laboratories.
If there are any questions, please do not hesitate to contact us.
Sincerely,
A ENVIRONMENTAL S
Zhanna Geskin
GC/MS Laboratory S ervisor
"4�s � "
Clifford H. McBride
QA/QC Coordinator
Attachment: Data Report
Invoice

I ENVIRONMENTAL NATIONAL LABORS.
TEST DATA REPORT
RIES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-01
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Station ID : MSD-WELL-1
Matrix : W
Type : GRAB
Collector : GM
Remarks :
--- Sample Information ---
Cust. No. .
Sampled Date/Time
Received Date/Time
Received From/By
Chain of Custody
Number of Containers
--- Test Data ---
08/16/89 14:30
08/17/89 10:00
GM/CLM
6473
6
Parameter ............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270
Ext/Acid Extractables/W 3510/8270
N/A 08/21/89 JAS
N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Bromoform
EPA
601
ug/l
2.0
ND
08/18/89
OL
Bromomethane
EPA
601
ug/1
12
ND
08/18/89
OL
Carbon tetrachloride
EPA
601
ug/1
1.2
ND
08/18/89
OL
Chloroethane
EPA
601
ug/1
5.2
ND
08/18/89
OL
2-Chloroethylvinyl ether
EPA
601
ug/1
1.3
ND
08/18/89
OL
Chloroform
EPA
601
ug/l
1.0
ND
08/18/89
OL
Chloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Dibromochloromethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichlorobenzene
EPA
601
ug/1
1.5
ND
08/18/89
OL
1,3-Dichlorobenzene
EPA
601
ug/l
3.2
ND
08/18/89
OL
1,4-Dichlorobenzene
EPA
601
ug/1
2.4
ND
08/18/89
OL
Dichlorodifluoromethane
EPA
601
ug/l
18
ND
08/18/89
OL
1,1-Dichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,2 Dichloroethane
EPA
601
ug/l
0.3
0.53
08/18/89
OL S
1,1-Dichloroethene
EPA
601
ug/1
1.3
ND
08/18/89
OL
Trans-1,2-Dichloroethene
EPA
601
ug/1
1.0
ND
08/18/89
OL
1,2-Dichloropropane
EPA
601
ug/1
1.0
ND
08/18/89
OL
cis-1,3-Dichloropropene
EPA
601
ug/l
3.4
ND
08/18/89
OL
Trans-1,3-Dichloropropene
EPA
601
ug/1
3.4
ND
08/18/89
OL
Methylene Chloride
EPA
601
ug/1
2.5
ND
08/18/89
OL
1,1,2,2-Tetrachloroethane
EPA
601
ug/1
0.3
ND
08/18/89
OL
Tetrachloroethene
EPA
601
ug/l
1.0
ND
08/18/89
OL
1,1,1-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Signed

I ENVIRONMENTAL NATIONAL LABORA TIES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Trichloroethene EPA 601 ug/1 1.2 ND 08/18/89 OL
Trichlorofluoromethane EPA 601 ug/1 3.2 ND 08/18/89 OL
Vinyl Chloride EPA 601 ug/1 1.8 ND 08/18/89 OL
Benzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Chlorobenzene EPA 602 ug/1 1.0 1.9 08/18/89 OL
Ethylbenzene EPA 602 ug/1 1.0 ND 08/18/89 OL
Toluene EPA 602 ug/1 1.0 ND 08/18/89 OL
-- GC/MS ANALYSIS RESULTS --
Isophorone EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethoxy)methane EPA 8270 ug/l 10 ND 09/11/89 MC
1,2,4-Trichlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
Naphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chloroaniline EPA 8270 ug/l 20 ND 09/11/89 MC
Hexachlorobutadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Methylnaphthalene EPA 8270 ug/1 10 ND 09/11/89 MC
Hexachlorocyclopentadiene EPA 8270 ug/l 10 ND 09/11/89 MC
2-Chloronaphthalene EPA 8270 ug/l 10 ND 09/11/89 MC
bis(2-Chloroethyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
1,3-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,4-Dichlorobenzene EPA 8270 ug/l 10 ND 09/11/89 MC
1,2-Dichlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
Benzyl Alcohol EPA 8270 ug/l 20 ND 09/11/89 MC
bis(2-Chloroisopropyl) ether EPA 8270 ug/l 10 ND 09/11/89 MC
Hexachloroethane EPA 8270 ug/1 10 ND 09/11/89 MC
N-Nitroso-di-n-propylamine EPA 8270 ug/l 10 ND 09/11/89 MC
Nitrobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
2-Nitroaniline EPA 8270 ug/1 50 ND 09/11/89 MC
Acenaphthylene EPA 8270 ug/1 10 ND 09/11/89 MC
Dimethyl phthalate EPA 8270 ug/l 10 ND 09/11/89 MC
2,6-Dinitrotoluene EPA 8270 ug/1 10 ND 09/11/89 MC
Acenaphthene EPA 8270 ug/l 10 ND 09/11/89 MC
3-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
Dibenzofuran EPA 8270 ug/1 10 ND 09/11/89 MC
2,4-Dinitrotoluene EPA 8270 ug/l 10 ND 09/11/89 MC
Fluorene EPA 8270 ug/l 10 ND 09/11/89 MC
4-Chlorophenyl phenyl ether EPA 8270 ug/l 10 ND 09/11/89 MC
Diethylphthalate EPA 8270 ug/1 10 ND 09/11/89 MC
4-Nitroaniline EPA 8270 ug/l 50 ND 09/11/89 MC
4-Bromophenyl phenyl ether EPA 8270 ug/1 10 ND 09/11/89 MC
Hexachlorobenzene EPA 8270 ug/1 10 ND 09/11/89 MC
Phenanthrene EPA 8270 ug/l 10 ND 09/11/89 MC
Anthracene EPA 8270 ug/1 10 ND 09/11/89 MC
Signed

ENVIRONMENTAL NATIONAL LABORA .LIES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-01
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/1
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/l
0.1
ND
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/l
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/l
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
0.006 =
08/18/89
MC
Lead, Total
EPA
7421
mg/1
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/1'
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/l
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed ' �'�l '16

ENVIRONMENTAL NATIONAL LABORA _TIES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-02
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-S-1 Sampled Date/Time : 08/16/89 15:10
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W
Ext/Acid Extractables/W
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2 Dichloroethane
1,1-Dichloroethene
Trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Trans-1,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
1,1,1-Trichloroethane
3510/8270
N/A
08/21/89
JAS
3510/8270
N/A
08/21/89
JAS
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/l
2.0
ND
08/18/89
OL
EPA
601
ug/l
12
ND
08/18/89
OL
EPA
601
ug/l
1.2
ND
08/18/89
OL
EPA
601
ug/1
5.2
ND
08/18/89
OL
EPA
601
ug/1
1.3
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.5
ND
08/18/89
OL
EPA
601
ug/l
3.2
ND
08/18/89
OL
EPA
601
ug/1
2.4
ND
08/18/89
OL
EPA
601
ug/1
18
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
0.3
0.59
o8/18/89
OL
EPA
601
ug/l
1.3
ND
o8/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
3.4
ND
08/18/89
OL
EPA
601
ug/1
3.4
ND
08/18/89
OL
EPA
601
ug/l
2.5
ND
08/18/89
OL
EPA-601
ug/l
0.3
0.97
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
,17
Signed

i ENVIRONMENTAL NATIONAL LABORA. iIES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/l
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/1
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/1
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
Benzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
1.55
08/18/89
OL
Ethylbenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Isophorone
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/1
20
ND
09/11/89
MC
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/l
10
ND
09/11/89
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/1
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/1
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Signed 4'y

i ENVIRONMENTAL NATIONAL LABORA_ .,IES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-02
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/1
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
3,3`-Dichlorobenzidine
EPA
8270
ug/1
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/1
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/l
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
'Pentachlorophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/1
0.1
0.1
08/18/89
MC
Mercury, Total
EPA
7470
mg/l
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/1
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/l
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/l
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed ',-7 "�

L . ENVIRONMENTAL NATIONAL LABORA_ .,IES
TEST DATA REPORT
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-03
Project No. : AVE-2265 Cust. No.
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
--- Sample Information ---
Station ID : MSD-S-2 Sampled Date/Time : 08/16/89 15:45
Matrix : W Received Date/Time : 08/17/89 10:00
Type : GRAB Received From/By : GM/CLM
Collector : GM Chain of Custody : 6473
Number of Containers : 6
Remarks :
--- Test Data ---
Parameter .............................. Method.. Units Det. Limit Results... Test Date Analy
-- ORGANICS PREP RESULTS --
Ext/Base Neutrals/W 3510/8270 N/A 08/21/89 JAS
Ext/Acid Extractables/W 3510/8270 N/A 08/21/89 JAS
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Bromoform EPA 601 ug/1 2.0 ND 08/18/89 OL
Bromomethane EPA 601 ug/1 12 ND 08/18/89 OL
Carbon tetrachloride EPA 601 ug/1 1.2 ND 08/18/89 OL
Chloroethane EPA 601 ug/l 5.2 ND 08/18/89 OL
2-Chloroethylvinyl ether EPA 601 ug/1 1.3 ND 08/18/89 OL
Chloroform EPA 601 ug/1 1.0 ND 08/18/89 OL
Chloromethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Dibromochloromethane EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2-Dichlorobenzene EPA 601 ug/1 1.5 ND 08/18/89 OL
1,3-Dichlorobenzene EPA 601 ug/1 3.2 ND 08/18/89 OL
1,4-Dichlorobenzene EPA 601 ug/l 2.4 ND 08/18/89 OL
Dichlorodifluoromethane EPA 601 ug/l 18 ND 08/18/89 OL
1,1-Dichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2 Dichloroethane EPA 601 ug/l 1.0 ND 08/18/89 OL
1,1-Dichloroethene EPA 601 ug/l 1.3 ND 08/18/89 OL
Trans-1,2-Dichloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,2-Dichloropropane EPA 601 ug/1 1.0 ND 08/18/89 OL
cis-1,3-Dichloropropene EPA 601 ug/1 3.4 ND 08/18/89 OL
Trans-1,3-Dichloropropene EPA 601 ug/l 3.4 ND 08/18/89 OL
Methylene Chloride EPA 601 ug/l 2.5 ND 08/18/89 -OL
1,1,2,2-Tetrachloroethane EPA 601 ug/1 0.3 0.46 08/18/89 OL
Tetrachloroethene EPA 601 ug/1 1.0 ND 08/18/89 OL
1,1,1-Trichloroethane EPA 601 ug/1 1.0 ND 08/18/89 OL
Signed/(�juv

L. ENVIRONMENTAL NATIONAL LABORA� _1ES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
1,1,2-Trichloroethane
EPA
601
ug/1
1.0
ND
08/18/89
OL
Trichloroethene
EPA
601
ug/l
1.2
ND
08/18/89
OL
Trichlorofluoromethane
EPA
601
ug/l
3.2
ND
08/18/89
OL
Vinyl Chloride
EPA
601
ug/1
1.8
ND
08/18/89
OL
Benzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Chlorobenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Ethylbenzene
EPA
602
ug/1
1.0
ND
08/18/89
OL
Toluene
EPA
602
ug/1
1.0
ND
08/18/89
OL
-- GC/MS ANALYSIS RESULTS --
Isophorone
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethoxy)methane
EPA
8270
ug/1
10
ND
09/11/89
MC
1,2,4-Trichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Naphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chloroaniline
EPA
8270
ug/l
20
ND
09/11/89
MC
Hexachlorobutadiene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Methylnaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorocyclopentadiene
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chloronaphthalene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-Chloroethyl) ether
EPA
8270
ug/1
10
ND
09/11/89
MC
1,3-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,4-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
1,2-Dichlorobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzyl Alcohol
EPA
8270
ug/l
20
ND
09/11/89
MC.
bis(2-Chloroisopropyl) ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachloroethane
EPA
8270
ug/1
10
ND
09/11/8,9
MC
N-Nitroso-di-n-propylamine
EPA
8270
ug/l
10
ND
09/11/89
MC
Nitrobenzene
EPA
8270
ug/l
10
ND
09/11/89
MC
2-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Acenaphthylene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dimethyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2,6-Dinitrotoluene
EPA
8270
ug/l
10
ND
09/11/89
MC
Acenaphthene
EPA
8270
ug/l
10
ND
09/11/89
MC
3-Nitroaniline
EPA
8270
ug/l
50
ND
09/11/89
MC
Dibenzofuran
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrotoluene
EPA
8270
ug/1
10
ND
09/11/89
MC
Fluorene
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Chlorophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Diethylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitroaniline
EPA
8270-
ug/l
50
ND
09/11/89
MC
4-Bromophenyl phenyl ether
EPA
8270
ug/l
10
ND
09/11/89
MC
Hexachlorobenzene
EPA
8270
ug/1
10
ND
09/11/89
MC
Phenanthrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
,
Signed

L_ ENVIRONMENTAL NATIONAL LABORA,. .IES
TEST DATA REPORT
Date 09/12/89
Page 3
Lab Number : 89-4109-03
Project No. : AVE-2265
--- Test Data ---
Parameter .............................. Method.... Units Det. Limit Results..: Test Date Analy
-- GC/MS ANALYSIS RESULTS --
Di-n-butylphthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Fluoranthene
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzo(b)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(k)fluoranthene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(a)pyrene
EPA
8270
ug/1
10
ND
09/11/89
MC
Indeno(1,2,3-cd)pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Dibenz(a,h)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Benzo(g,h,i)perylene
EPA
8270
ug/1
10
ND
09/11/89
MC
N-Nitrosodiphenylamine
EPA
8270
ug/1
10
ND
09/11/89
MC
Pyrene
EPA
8270
ug/l
10
ND
09/11/89
MC
Butyl benzyl phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
3,3'-Dichlorobenzidine
EPA
8270
ug/l
20
ND
09/11/89
MC
Benzo(a)anthracene
EPA
8270
ug/l
10
ND
09/11/89
MC
Chrysene
EPA
8270
ug/l
10
ND
09/11/89
MC
bis(2-ethylhexyl)phthalate
EPA
8270
ug/l
10
ND
09/11/89
MC
Di-n-octyl phthalate
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Chlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
Phenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Methylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2-Nitrophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dimethylphenol
EPA
8270
ug/1
10
ND
09/11/89
MC
2,4-Dichlorophenol
EPA
8270
ug/1
10
ND
09/11/89
MC
Benzoic Acid
EPA
8270
ug/1
50
ND
09/11/89
MC
4-Chloro-3-methylphenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,6-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4,5-Trichlorophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
2,4-Dinitrophenol
EPA
8270
ug/l
10
ND
09/11/89
MC
4-Nitrophenol
EPA
8270
ug/1
50
ND
09/11/89
MC
4,6-Dinitro-2-methylphenol
EPA
8270
ug/l
50
ND
09/11/89
MC
Pentachlorophenol
EPA
8270
ug/l
50
ND
09/11/89
MC
--- SERIES 8000
Barium, Total
EPA
6010
mg/l
0.1
ND
08/18/89
MC
Mercury, Total
EPA
7470
mg/1
0.0005
ND
08/21/89
OL
Arsenic, Total
EPA
7060
mg/1
0.005
ND
08/18/89
MC
Cadmium, Total
EPA
7131
mg/1
0.002
ND
08/18/89
MC
Chromium, Total
EPA
7191
mg/1
0.005
ND
08/18/89
MC
Lead, Total
EPA
7421
mg/l
0.005
ND
08/18/89
MC
Selenium, Total
EPA
7740
mg/1
0.005
ND
08/18/89
MC
Silver, Total
EPA
7761
mg/1
0.01
ND
08/18/89
MC
Total Metals Prep: Aqueous ICP
EPA
3010
N/A
08/17/89
HH
Total Metals Prep: Aqueous Furnce
EPA
3020
N/A
08/17/89
GSP
Signed r

L. ENVIRONMENTAL NATIONAL LABORAi
TEST DATA REPORT
IES
Date 09/12/89
Page 1
--- Project Information ---
Lab Number : 89-4109-04
Project No. : AVE-2265
Project Name : METRO. SEWARAGE DISTRICT
Manager: TOM LAMMONS
Station ID : TRIP BLANK
Matrix : W
Type : GRAB
Collector : GM
Remarks :
--- Sample Information ---
Cust. No. .
Sampled Date/Time
Received Date/Time
Received From/By
Chain of Custody
Number of Containers
--- Test Data ---
: o8/17/89 lo:oo
: GM/CLM
: 6473
2
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2 Dichloroethane(
1,1-Dichloroethene
Trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Trans-1,3-Dichloropropene
Methylene Chloride
1,1,2,2-Tetrachloroethane-e—'
Tetrachloroethene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl Chloride
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
2.0
ND
08/18/89
OL
EPA
601
ug/1
12
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/l
5.2
ND
08/18/89
OL
EPA
601
ug/1
1.3
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.5
ND
08/18/89
OL
EPA
601
ug/1
3.2
ND
08/18/89
OL
EPA
6ol
ug/1
2.4
ND
08/18/89
OL
EPA
601
ug/1
18
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
0.3
1.53
08/18/89
OL
EPA
601
ug/1
1.3
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
3.4
ND
08/18/89
OL
EPA
601
ug/1
3.4
ND
08/18/89
OL
EPA
601
ug/l
2.5
ND
08/18/89
OL
EPA
601
ug/1
0.3
2.1
08/18/89
OL
EPA
601
ug/l
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.0
ND
08/18/89
OL
EPA
6o1
ug/1
1.0
ND
08/18/89
OL
EPA
601
ug/1
1.2
ND
08/18/89
OL
EPA
601
ug/l
3.2
ND
08/18/89
OL
EPA
601
ug/l
1.8
ND
o8/18/89
OL
Signed e -4A9_1 czcx;�

L ENVIRONMENTAL NATIONAL LABORA; .IES
TEST DATA REPORT
Date 09/12/89
Page 2
Lab Number : 89-4109-04
Project No. : AVE-2265
Test Data
Parameter .............................. Method.... Units Det. Limit Results... Test Date Analy
-- ORGANIC ANALYSIS RESULTS --
Benzene
EPA 602
ug/1
1.0 ND
08/18/89 OL
Chlorobenzene
EPA 602
ug/1
1.0 ND
08/18/89 OL
Ethylbenzene
EPA 602
ug/1
1.0 ND
08/18/89 OL
Toluene
EPA 602
ug/1
1.0 ND
08/18/89 OL
Signed

LAW ENVIRONMENTAL, INC. CHAIN OF CUSTODY RECORD
NATIONAL LABORATORY
112 TOWNPARK DRIVE
KENNESAW, GEORGIA 30144
® [phone] ¢q_L y
'
SAMPLING ✓ D / I "
NAME OF FACILITY: /i
INFORMATION
STREET ADDRESS:
CITY/STATE: ZIP:
PROJECT NAME 'BOO
1 Y t Ae"L— �J I� s %I�C� ll
JOB NO.
N
W
J Q
Fa- FZ
O U
~
O
O
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O� � p �� Oa x PS
G
F��G Q Q Q \�a e'�° Q\ V P� OQa\G
p
a° �� �,V v' V Q �� �v' °ti. ��o�
�� ` � LENL LAB NO.
SAMPLcdRS (SIGNATU )
SAMPLING DATE �D �D
TIME
m
19
ILW
U
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Ul
O
SAMPLE STATION DESCRIPTION
t0
M
MSA -We'u
6
3
-wo -ca
JLI
w
Vc- 041-(5.
ri
r-yloq-v '
RE 1 QUISHE BY
eal
(DATE/TIME
U /P'J 1 !J • �D
RECEIVED BY:
RELINQUISHED BY:
RECEIVED BYI
DATE/TIME
IGNA U E)
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
RELINQUISHED BY:
DATE/TIME
RECEIVED BY:
RELINQUISHED BY:
/Rtj% IVE�jT LAV010RY:
DATE/TIME
7
(SIGNATURE)
(SIGNATURE)
(SIGNATURE)
(S GNATUR
DISTRIBUTION: ORIGINAL AND YELLOW COPIES ACCOMPANY SAMPLE SHIPMENT TO LABORATORY.
PINK COPY RETAINED BY SAMPLERS. YELLOW COPY RETAINED BY LABORATORY.
REMARKS:
L RECOVERY WELL! -RW
SOU RC[ RCRA MONITORING WELL - MW
CODES: SOIL/SEDIMENT - SO
SLUDGE - SL
NPDES DISCHARGE ND
I-- DRINKING WATER - DW
/, HAZARDOUS WASTE - HW
6yl CIIRFwaf F WATF'R - SW

LAW ENVIRONMENTAL NATIONAL LABORATORIES
Project Number: AVE-2265
Project Name: ' Metro Sewarage District
Lab Sample ID: 89-4109-01 Client ID: MSD-Well-1
TENTATIVELY IDENTIFIED COMPOUNDS
X 7/1T_A T T T.VC
COMPONENT
QUANT.
SCAN
EST. CONC.
ION
NO.
AREA
ug/l
2-Ethyl-4-methyl-1,3-dioxolane
87
1073
23189
65
3-Ethyl-3-pentanol
45
1206
74217
210
Diisopropyl ether
45
1230
73606
200
1-Chloro-5-iodo-pentane
69
1236
32834
92

DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
April 17, 1989
r�'� .
TO:
Mr. Cecil Madden
Construction Grants JUN 2 ?_ 1989
FROM:
mikEr Cleary'M.P(o GroundwateCSecti0n
Asheville Regional office
SUBJECT:
Buncombe County MSD
C370391-01
Buncombe County
We
are in receipt of the materials concerning the
subject
ash storage lagoon. The following additional
information is -needed for our review of the project:
1.
A site-sp.ecific map of the lagoon site, with
topographic contours (contour interval should not
exceed 10 feet or 25 percent of total site relief,
whicr.ever is less), showing property houndariPs__
ca_ _Locc..�=_:: of all`- weirs, springs, lakes,
ponds, or other surface drainage features within
500 feet of the lagoon. Wells should be labeled
as to their primary usage (drinking water, process
water, monitoring, etc.)
-� 2.
Construction details for existing lagoon, if
.r
available.
3. A characterization of groundwater quality in the
vicinity of the lagoon. This characterization
should be accomplished by the installation of
monitoring wells for the purpose of describing the
lithology in the area, and . for collecting
groundwater quality samples from the water table
aquifer. The locations, well construction details
and sampling methods should be by approval of the
Asheville Regional Office, 'from which a well
construction permit must be obtained.
Groundwater. campies shall be ohtainod fr.c:m each
monitoring well -and analyzed for the following
parameters:
Nitrate pH
Total Dissolved Solids Chlorides

Total Coliforms
Total Organic Carbon
Ammonia Nitrogen
TOY
Sulfate
Water Level
Cu, Cd, Zn
Euvel sh
of ould be taken m.asi�.c�
prior to sampling for -the other parameters.
Lithologic logs, well construction details and the
analytical results. of the sampling should be
submitted to the Groundwater Section, Division of
Environmental Management.
Since the existing unlined sludge -lagoon has been in
operation for 20 years, and it is known that bedrock occurs
at shallow depths on the site, there is a strong likelihood
that groundwater contamination has occurred in the vicinity
of the lagoon. As such, this site may not be suitable for
the proposed storage of ash. The Groundwater Section has no
objection to issuance of a permit to construct the
incinerator, provided that the applicant is made aware than
an alternaty e method of ash disposal may be necessary.
Please feel free to contact the Groundwater Section, at
('919) 733-3221, if clarification or information is required.
cc: Bob Cheek
Mike Cleary
Central Files
Permit Issuance Files

■ Complete+tams 1„2rid 3. Also complete A
RestnctedaQeiry is desired. X
■ our name and address on the reverse
North Ckwlina Deparfinerit-c
r . A
Environment andNatural Resource�� ,�/Division of Water Qualit
Water Quali _Regional Operation
NCDENk- 2090 U.S. Highway 70-; annanoa, NC 2877
Thomas E. Hartye, P
General Manager
Metropolitan Sewerage District SIR
c®Type
of Buncombe County, North Carolling ertified M
2028 Riverside Drive egister
Asheville, NC 28804 ❑ insured Mal
' 4. Restricted Deli
❑ Agent
❑ Addresse
G. Deliver
P' edNam aeo
Ysd@erentfrom 'item 1?
s i�ier0, ress below: N
zr
8Mro m
SLm
CD
_•m
— to q
0 FTI
CL
4 EXP all v
Return Receipt Me
C.O.D.
ewryfikt a Fee) ❑
handis
7012 1010 0002 1967 8227
PS Fnrm qR1 it iFohnmrv; 9nnd I r : f DnrnP.q*vRBtiim RPnPint 102595-02-M-15,
❑ Agent
❑ Addresse
G. Deliver
P' edNam aeo
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s i�ier0, ress below: N
zr
8Mro m
SLm
CD
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— to q
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C.O.D.
ewryfikt a Fee) ❑
handis
7012 1010 0002 1967 8227
PS Fnrm qR1 it iFohnmrv; 9nnd I r : f DnrnP.q*vRBtiim RPnPint 102595-02-M-15,
handis
7012 1010 0002 1967 8227
PS Fnrm qR1 it iFohnmrv; 9nnd I r : f DnrnP.q*vRBtiim RPnPint 102595-02-M-15,

UNITED STATES POSTAL SERVICC
First -Class Mail
Postage & Fees Paid
USPS
Permit No. G-
• Sender: -Please print your name, address, and ZIP+4 in this box •
ANDAEW MOORE
NCDENR-DVVR-WQRO
2090 U.S. HIGHWAY 70
SWANNANOA NC 28778 '
_j
''i1111i, I'll , fill] III11!,I