WQ0012346_Residual Annual Report 2020_20210222

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00012346
Applicant/Permittee US MCB Camp Lejeune
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd
.......................................................... ronc su_ -
Name * Daniel Straub
Email Address*
[e-mail]
Phone Number*
1-910-451-9122
Project Information
........ ................................................................................................................................................... ......... ............ .... .... ........ ... ... .... .... .... ... ... ... .... .... .... ... .... .... ......... .........
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0012346
Fbs Current Existing perm number
Applicant/Permittee Address* Commanding General ATTN:EMD 12 Post Lane Camp Lejeune NC 28547-2540
Facility Name * US MCB Camp Lejeune DCAR
Please provide comments/notes on your current submittal below.
MCB Camp Lejeune is submitting the 2020 Class A Residuals Application Annual Report.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 NCDEQ Class A Annual RPT_Final.pdf 10.9MB
Upload only 1 RDF docurrent (less than 250 IvB). Multiple documents rust be combined into one RDF file unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/22/2021

CLASS "A" WASTEWATER RESIDUALS
ANNUAL APPLICATION REPORT
YEAR 2020
UNITED STATES
MARINE CORPS BASE
CAMP LEJEUNE, N. C.
PERMIT NO. WQ0012346

CLASS "A" WASTEWATER RESIDUALS
ANNUAL APPLICATION REPORT FOR
THE YEAR 2020
MARINE CORPS BASE, CAMP
LEJEUNE PERMIT NO. WQ0012346
• Cover Letter..................................................................... SECTION 1
• Class A Annual Distribution and Marketing/Surface Disposal SECTION 2
Certification and Summary Form (Form DMSDF)........................
• Annual Residuals Sampling Summary Forms
SECTION 3
(Forms RSSF & RSSF-B)......................................................
• Residuals Analysis Lab Sheets including TCLP Lab Sheets ............... SECTION 4
Annual Pathogen & Vector Attraction Reduction Forms SECTION 5
• (Form PVRF 2T) and Vector Attraction Reduction Lab Sheets .............

,VOW
=1

SECTION 1
Cover Letter

UNITED STATES MARINE CORPS
MARINE CORPS INSTALLATIONS EAST -MARINE CCRPS BASE
PSC BOX 20005
CAMP LEJEUNE NC 28542-GCO5
5090.11
G-F/BEMD
FEB 18 2021
Mr. Nathaniel Thornburg
North Carolina Department of Environmental Quality
Division of Water Resources
Non -Discharge Permitting Branch 1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Mr. Thornburg:
In accordance with requirements of 15A NCAC 02T, the enclosed
forwards Marine Corps Base Camp Lejeune's (MCB CAMLEJ) Class "A"
Wastewater Residuals Annual Application Report 2020. The report was
prepared by Charles "Sonny" Scozzari, MCB CAMLEJ Wastewater and Land
Application Supervisor, for Permittee Robert A. Lowder, Director,
Environmental Management Division (EMD).
The following explanation is provided per instruction in the Class
"A" Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form and the Annual Pathogen and Vector Attraction
Reduction Form (PVRF 2T Rules).
For your awareness, our CROM tank was out of service for the
majority of the year. Bench scale samples were not collected during
the second quarter of 2020 while it was out of service. No residuals
were land applied during this period. ATAD Sludge Solids Analyses,
which also estimate percent solids removal, were however performed
during this time. Treated solids were stored on -site to the maximum
extent possible. Due to limited storage capacity, some were belt -
pressed and used as soil conditioner for daily cover at the Base
landfill. Fecal analyses and time and temperature requirements were
met prior to this land application. NCDEQ was notified of the CROM
tank maintenance and use of residuals at the Base landfill accordingly.
If you have any questions please contact Mr. Travis Voorhees,
Environmental Quality Branch, EMD, at [phone].
It
Directc
ironmental
Enclosure: Class "A" Wastewater Residuals Annual Application Report 2020
Copy to:
File (ODI# 26065)

SECTION 2
Class A Distribution & Marketing/Surface
Disposal Certification & Summary Forms
(Form DMSDF)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT If: W00012346 FACILITY NAME: US MCB Camp Lejeune AWWTP
PHONE: 91OA51-7190 COUNTY: ONSLOW OPERATOR: Charles "Sonny" Scozzari
FACILITY TYPE (please check one): © Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, H, and C)
Was the facility in operation during the past calendar year? Yes El No ❑ —► If No skip parts A. B, C and certify farm below
Part A":
Part B":
Month
Sources(s) (include NPDES N if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Nome(s)
Volume (dry tons)
Inlended use(s)
Jonuary
CAMLEJ A W W TP NCO063029
1.4
February
2.9
March
0
April
0
May
0
June
0
July
0
August
21.6
September
34A
October
19.3
November
0
December
0
Total from FORM DMSDF (sup)
0
0
0
0
Totals:
Annual (dry tuns):
0
80
0
0
Amendmenl(s) used:
Bulking Agent(s) used:
(supp)): Total Number orform DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No -► If No, Explain In Narritive
I. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies ofcertified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case ora deviation, prior authorization was received from the Division of Water Resources.
3. No contravention orGround Water Quality Standards occurred at a monitoring well.
"I certify, under pena_Ry of law, that the above information is, to the best ormy knowledge and belief, true, urcurate and complete. 1 am aware that there are significant
pena)Q for subrio tang fa a Information, including the possibility of fines and imprisonme� knMing violations."
ff Zr
Dale
different from Permittee)
**Preparer is defintdin 40.011 Part 503.91r) and 15A NCAC 3T .I 102 (26)
DENR FORM DMSDF (1=006)

Landfill Load Receipts
Load Date
LoadTime
Sludge
1/2/2020
14:09
16.74
1/3/2020
14:14
17.18
1/3/2020
13:10
17.80
1/6/2020
13:12
16.34
1/6/2020
14:14
16.34
1/7/2020
13:12
16.78
1/7/2020
13:13
17.28
1/7/2020
14:14
34.06
1/8/2020
13:13
33.01
1/8/2020
14:15
33.01
1/9/2020
13:14
17.88
1/9/2020
14:15
17.88
1/10/2020
14:15
34.45
1/10/2020
13:15
34.45
1/13/2020
14:16
18.15
1/13/2020
13:15
18.15
1/14/2020
14:16
16.78
1/14/2020
13:15
16.78
1/15/2020
14:16
34.87
1/15/2020
13:16
34.87
1/20/2020
13:07
16.74
4/8/2020
13:18
15.79
4/9/2020
13:17
15.73
4/10/2020
13:16
33.07
4/14/2020
13:18
33.51
4/15/2020
13:19
37.00
4/16/2020
13:21
32.97
4/16/2020
13:20
19.14
4/17/2020
13:20
17.18
VehiclelD
1
Wednesday, January 20, 2021 Page 1 of 3

Load Date
LoadTime VehiclelD
Sludge
4/17/2020
13:27
17.57
4/18/2020
13:21
33.16
4/20/2020
13:22
34.52
4/21/2020
13:23
51.52
4/22/2020
13:24
34.04
4/23/2020
13:25
34.07
4/24/2020
13:25
32.74
4/27/2020
13:26
51.61
4/27/2020
13:27
17.88
4/28/2020
13:28
35.69
4/29/2020
13:28
33.87
6/24/2020
13:46
33.02
6/25/2020
13:46
17.48
6/25/2020
13:46
17.53
6/26/2020
13:45
17.06
6/29/2020
13:45
31.25
7/1/2020
13:37
30.53
7/2/2020
13:44
17.11
7/6/2020
13:44
14.32
7/7/2020
13:44
14.39
7/8/2020
13:43
17.16
7/9/2020
13:43
17.38
7/10/2020
13:43
17.55
7/13/2020
13:42
33.19
7/16/2020
13:41
13.46
7/21/2020
13:41
12.48
7/23/2020
13:41
15.17
8/10/2020
13:42
10.80
8/12/2020
13:40
12.21
8/14/2020
13:40
12.04
8/18/2020
13:40
14.51
Wednesday, January 20, 2021 Page 2 of 3

Load Date
LoadTime VehiclelD
Sludge
8/19/2020
13:39
15.79
8/20/2020
13:39
16.31
8/21/2020
13:39
15.99
8/24/2020
13:38
18.07
8/26/2020
13:37
16.59
8/27/2020
13:36
31.22
8/28/2020
13:35
11.95
9/4/2020
13:37
16.03
9/8/2020
13:37
17.09
9/15/2020
13:35
15.86
9/16/2020
13:35
16.62
9/17/2020
13:34
10.42
9/22/2020
13:34
15.95
9/23/2020
13:34
17.15
9/24/2020
13:33
17.44
9/28/2020
13:33
11.68
9/30/2020
13:33
15.11
10/2/2020
13:32
16.37
10/5/2020
13:32
16.36
10/7/2020
13:32
16.67
10/13/2020
13:32
12.00
10/16/2020
13:31
16.30
10/20/2020
13:31
16.43
10/27/2020
13:30
15.72
11/3/2020
13:47
16.60
11/9/2020
13:30
15.61
11/10/2020
13:29
9.01
Total Sludge
1,859.58 Tons
Wednesday, January 20, 2021 Page 3 of 3

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
71
ite sweet cane syrup added Train 1 ReactorA 275 gallons Train 1 Reactor B 275 gallons
onday, January 6, 2020 Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Date sweet cane syrup added
Train 1 Reactor A 137 gallons Train 1 Reactor B 137 gallons
Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Monday, January 13, 2020
Date sweet cane syrup added
Train 1 Reactor A gallons Train 1 Reactor B gallons
Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A 250 gallons Train 3 Reactor B 250 gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Monday, September 14, 2020
Date sweet cane syrup added
Train 1 Reactor A gallons Train 1 Reactor B gallons
Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B 125 gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Thursday, October 8, 2020
Date sweet cane syrup added
Train 1 Reactor A gallons Train 1 Reactor B gallons
Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A 125 gallons Train 3 Reactor B gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Thursday, October 8, 2020
Date sweet cane syrup added
Train 1 Reactor A gallons Train 1 Reactor B gallons
Train 2 Reactor A 250 gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Thursday, October 8, 2020
Date sweet cane syrup added
Train 1 Reactor A 250 gallons Train 1 Reactor B gallons
Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Thursday, October 8, 2020
Wednesday, January 20, 2021 Page 1 of 2

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
to sweet cane syrup added Train 1 Reactor A Igallons Train 1 Reactor B Igallons
esday, October 13, 2020 Train 2 Reactor A gallons Train 2 Reactor B gallons
Train 3 Reactor A gallons Train 3 Reactor B 250 gallons
Train 4 Reactor A gallons Train 4 Reactor B gallons
Wednesday, January 20, 2021 Page 2 of 2

SECTION 3
Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - Q
WQ Permit Number: W00012346
Facility Name: US MCB CAMP LEJEUNE
Residual Source WQ # or N00063029
NPDES #:
WWTP Name: Camp Lejeune Advanced WWTP
Residual Analvsis Data
Laboratory: 1) EMD,ELS
2) Environmental Chemists, Inc.
3) Environment 1, Incorporated
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(m k )°
Sam le or Composite Date
1/15/20
07/22/20
11/17/20
Percent Solids (%)
NA
3.79
4.25
3.09
Arsenic
75
9.21
5A
32.4
Cadmium
85
<6.60
3
<16.0
Copper
4,300
274
266
292
Chromium
NA
19.6
16
20.8
Lead
840
12.6
13
<16.0
Mercury
57
<0.412
0.22
<0.521
Molybdenum
75
6.65
6
<16.0
Nickel
420
14.4
15
<16.0
Selenium
100
<6.60
<5.0
<16.0
Zinc
7,500
1170
1261
1440
Total Phosphorus
NA
63000
38670
62600
TKN
NA
51600
26510
58200
Ammonia -Nitrogen
NA
18800
960.6
26300
Nitrate and Nitrite
NA
14.7
5.98
1 63.5
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit For metals limits.
"I certify, under pen
to assure that quali
penalties fors mi
J
Signature of,
151aw, that this document was prepared under my direction or supervision in accordance with a system designed
1onnel properly gathered and evaluated the information submitted. I am aware that there are significant
Ise information, including the possibility of fines and imprisonment for knowing violations."
*Preparer Wdefined in 40 CFR Part 503.9(r) and 15A NCAC 2T . 1102 (26)
z Aoz. r
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ Permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0012346
Facility Name: US MCB CAMP LEJEUNE
Residual Source NCO063029
NPDES # or WQ#:
WWTP Name: Camp Lejeune Advanced WWTP
Residual Analvsis Data
Laboratory: 1) EMD,ELS
2) Environmental Chemists, Inc.
3) Environment I, Incorporated
4)
5)
Sample or po
MagnesiumParameter
' 1 1
-�
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to as e t,Oat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant enalt' s for submitting false information, including the possibility of fines and imprisonment for knowing violations."
f Preparer'
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
MAS ZDZI
Date
DENR FORM RSSF - B (12/2006)

SECTION 4
Residuals Analysis Lab Sheets
including TCLP Lab Sheets

TCLP Analysis Lab Sheets

envirochem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Lab ID Sample ID:
20-31090 Site: CROM Tank
Test
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 31, 2020
Customer PO #:
Customer ID: 12060026
Report #: 2020-12299
Project ID: Crom Tank
Collect Date/Time Matrix
7/22/2020 8:50 AM Solid/Sludge
Method
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
Results
<0.02 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.0005 mg/L
<0.05 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
0.681 mg/L
<0.050 mg/L
<0.050 mg/L
<0.050 mg/L
0.681 mg/L
<0.050 mg/L
<0.050 mg/L
<0.250 mg/L
<0.050 mg/L
<0.003 mg/L
<0.003 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
<0.01 mg/L
Sampled by
Williams
Date Analyzed
08/03/2020
08/03/2020
08/03/2020
08/03/2020
08/03/2020
08/03/2020
08/03/2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/31 /2020
07/30/2020
07/30/2020
08/05/2020
08/05/2020
08/05/2020
08/05/2020
Report # 2020-12299 Page 1 of 2

:"envirochem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 31, 2020
Customer PO #:
Customer ID: 12060026
Report #: 2020-12299
Project ID: Crom Tank
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
08/05/2020
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
08/05/2020
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
08/05/2020
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
08/05/2020
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
08/05/2020
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
08/05/2020
RCI
Cyanide
EPA 335 4
0.059 mg/kg
07/31 /2020
Sulfide
SM 4500 S D
3.91 mg/kg
07/28/2020
Ignitabillty
SW 846 method 1010
>190 °F
07/28/2020
pH
SW 846 Method 9045D
7.88 units
07/28/2020
TCLP Metals
Arsenic
EPA 200 7
<1.0 mg/L
08/06/2020
Barium
EPA 200.7
<1.0 mg/L
08/06/2020
Cadmium
EPA 200.7
<1.0 mg/L
08/06/2020
Chromium
EPA 200 7
<1.0 mg/L
08/06/2020
Lead
EPA 200.7
<1.0 mg/L
08/06/2020
Selenium
EPA 200 7
<1.0 mg/L
08/06/2020
Silver
EPA 2007
<1.0 mg/L
08/06/2020
Mercury
EPA 245.1
<0.0002 mg/L
08/06/2020
Comment:
Reviewed by:
Report # 2020-12299 Page 2 of 2

TCLP Analysis Lab Sheets for
Residuals Sent to Landfill

lenvi
rochem
ANALYTICAL. & CONSULTING CHEMISTS
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info it en% ironmentalchemtsts.com
USMC Camp Lejeune
Date of Report: Mar 27, 2020
G-F/EMO/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2020-02890
Project ID: Camp Lejeune MCB
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
20-06988 Site: BNRA
2/18/2020
2-00 PM Solid/Sludge EJ Ruberte
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW 848 Method 8081B13510
<l} 02 mg/L
02/26/2020
Endrin (TCLP)
SW 846 Method 8081B13510
<0.0005 mglL
02/26/2020
Heptachlor (TCLP)
SW 846 Method 8081/3/3510
<0.0005 mg/L
02/26/2020
Heptachlor epoxide (TCLP)
SW 846 Method 8081Bi3510
<0 0005 mg/L
02/26/2020
Lindane (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
02/26/2020
Methoxychlor (TCLP)
SW 846 Method 8081 B13510
<0.0005 mg/L
02/26/2020
Toxaphene (TCLP)
SW 846 Method 8081 B13510
<0.05 mg/L
02/26/2020
1,4-Dichlorobenzene (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/28/2020
2,4,5-Trichlorophenol (TCLP)
SW 846 method 827a13510
<0.050 mg/L
02/28/2020
2,4,6-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/28/2020
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/28/2020
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/28/2020
Hexachloro-1,3-butadiene (TCLP)
SIN 846 method 8270/3510
<0,050 mg/L
02 28.12020
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/28/2020
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/28+2020
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/28/2020
Nitrobenzene (TCLP)
SW 846 method 627013510
<0.050 mg/L
02/28/2020
o-Cresol (TCLP)
SW 845 method 827013510
<0.050 mg/L
02/28/2020
Pentachlorophenol (TCLP)
SW 846 method 827013510
<0.250 mg/L
02/28/2020
Pyridine (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/28/2020
2,4,5-TP (TCLP)
SW646 Method 8151A
<0.003 mg/L
02126i2020
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
02/26/2020
1, 1 -Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0 01 mg/L
02/27/2020
1,2-Dichloroethane (TCLP)
SW646 Method 8260/5030
<0.01 mg/L
02/27/2020
Benzene (TCLP)
SW846 Method 826015030
<0 01 mg/L
02/27/2020
Carbon Tetrachloride (TCLP)
SW846 Method 826015030
<0 01 mg/L
02/2712020
Repot #' 2020-02890
Paw sof?

[enviro . echem
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab + 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 289411 . 910.347.5843 l ab/Fax
inforenvironmentalehemists.rom
LISMC Camp Lejeune
Date of Report: Mar 27, 2020
G-FIEMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2020-02890
Project ID: Camp Lejeune MCB
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/27/2020
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/27/2020
Methyl ethyl ketone (TCLP)
SW846 Method 826015030
0.05 mg/L
02/27/2020
Tetrachloroethylene (TCLP)
SW846 Method 826015030
<0.01 mg/L
02/27/2020
Trichloroethylene (TCLP)
SW846 Method 826015030
<0 01 mg/L
02/27/2020
Vinyl Chloride (TCLP)
SW846 Method 826015030
<0 01 mg/L
02/27/2020
RCI
Cyanide
EPA 335 4
0 030 mg/kg
02/24/2020
Sulfide
SM 4500 S ❑
0 66 mglkg
02?28/2020
Ignitability
SW 846 method 1010
>205 °F
02/25/2020
pH
SW 846 Method 9,549D
7 32 units
02/28/2020
TCLP Metals
Arsenic
EPA 200 7
<1.0 mg/L
02/26/2020
Barium
EPA 200 7
<1.0 mg/L
02/26/2020
Cadmium
EPA 2007
<1.0mg/L
02/26/2020
Chromium
EPA 200 7
<1.0 mg/L
02/26/2020
Lead
EPA 200 7
<1.0 mg/L
02/26/2020
Selenium
EPA 200 7
<1.O mg/L
02/26/2020
Silver
EPA 200 7
<1.0 mg/L
02/26/2020
Mercury
EPA 245 1
<0.0002 mg/L
02/26/2020
Comment:
Reviewed by:
Report # 2020-02890 Page 2 of 2

RESEARCh & ANA1yTICAt
I.-AboiuT4RIE5, INC.
Analytical/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as MCB Camp LeJune
(A Commanding General GF/EMD/EQB/Eavironmental Lab Project, collected 21 July 2020)
Dyring Beds
EPA HW Quantitation Results Characteristic
Number Contaminant LimitfinelLl (mall, Level(me/L) EPA Method
1. TCLP METALS
D-004 Arsenic
0.01
BQL
5.00
6010
D-005 Barium
0.1
0.160
100
6010
D4)06 Cadmium
0.005
BQL
1.00
6010
D-007 Chromium
0.01
BQL
5.00
6010
D-008 Lead
0.005
BQL
5.00
6010
D-M Merduy
0.002
BQL
0.200
7470
D-010 Selenium
0.1
BQL
IRO
6010
D-011 Silver
0.01
BQL
5.00
6010
II- TCLP VOLATILES
D-018 Benzene
0.050
BQL
0.500
8260
D-019 Carbon Tenachloride
0.050
BQL
0.500
8260
D-021 Cdorobcnzmte
0.050
BQL
t00
8260
D-022 Chloroform
0.100
BQL
6.00
8260
D.028 1,2-Dichlotoethane
0.050
BQL
0.500
8260
D-029 1,1-Dichlomethylene
0,050
BQL
0.700
8260
D-035 Methyl Ethyl Ketone
0.500
BQL
200
8260
D-039 Tenachlomethylene
0.050
BQL
0.700
am
D-040 Trichloroethylene
0.050
BQL
0.500
8260
D-043 Vinyl Chloride
0.050
BQL
0.200
8260
III. TCLP SEMI-VOLATILES
D-023 &Cmosol
20.0
BQL
200
8270
D-024 M-Creosol
20.0
BQL
200
8270
D-025 p-Creosol
20.0
BQL
200
8270
D-026 Creosol
20.0
BQL
200
8270
D-027 1,4-Dichlorobenzene
0.750
BQL
7.50
9270
D-030 2,4-Dininmoluene
0.050
BQL
0.130
8270
D-032 Hexachlorobenzene
0.050
BQL
0.130
8270
D-033 Hexachlorobutadiene
0.050
SQL
0.500
8270
D•034 Hexachloroethene
0.300
BQL
3.00
9270
D-036 Nitrobenzene
0.200
BQL
2.00
$270
D•037 Pentaehlorophenal
10.0
BQL
to0
$270
D-038 Pyridine
0,500
BQL
5,00
9240
D-041 2,4,5-Trichloropherml
40.0
BQL
400
8270
D-042 2,4,6-Trichloraphehul
0.200
BQL
2.00
8270
IV. TCLP PESTICIDES/HERBICIDES
D-020 Chlordane
0.003
BQL
0.030
goal
D-016 2,4-D
1.000
SQL
10.0
8151
D-0I2 Endrin
0.002
BQL
0.020
goal
D-031 Heptachlor
0.0008
SQL
0.008
9081
D-013 Lindane
0.040
BQL
0.400
SCSI
D-014 Methoxychlor
IMo
BQL
10.0
9081
D-015 Toxaphere
0.050
BQL
0.5m
9081
D-0I7 2,4,5-:MSil-)
C500
BQL
I.00
8151
V, REACTIVITY
D-003 Cyanide
1.0
BQL
9010
D-003 Sulfide
5.0
BQL
9030
VI. CORROSIVITY
D-002 pH
Std. Units
7.39
9045
VIL IGNITABILITY
D-001 Ignitability
WNt
1010
VHl.TCLP MISCELLANEOUS
Paint Filter Test
NFL
Sample Number
85117-01
Sample Date
0712120
Sample Time (brs)
0930
Sample Matra
Solid
mg/kg - milligrams per kilogram - parts per million (ppm)
NFL - No Free Liquids
WNI = Will Not Ignite
mglL - milligrams per Liter a pauper million (ppm)
BQL - Below Quamitation Limits
FLP - Free Liquids Present

RESEARCh & ANAlyTICAL
LAboRATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
I —ATGO /iFlA CTC— TCa ■ 1
COMPAN f
JOB NO.
W
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=
i
tea• rry Zip
.I h 5 pZ
�Q�y Zpv p' cQ C�zM1Lacy
Z i~ U~ �• p 2
Q• \y �O O p c° p �Q
ry yob pF p Q-p Q' Q" Q' �c
ryzyti
REQUESTED ANALYS4S
STREE ' ADDRESS
PROJECT
CITY. STATE. ZIP
LEi�4 i
t �i,'j.11� C h
SAMPLER NAME (PLEASE PRI
Daniel E saulsg+vEl
CONTACT PHONE
SAMPLER SIGNATURE
SAMPLE NUMBER
(LAB USE ONLY)
DATE
TIME
C4tdP
GRAB
TEMP
'C
Res
CI
Ema'u
GII�ORINE
REMOVED
nut
SAMRE
MArRIx
Lsnlm
SAMPLE LOCATION! IA,
LAT I.
5' µ r
RELINQUISHED B
DATEPO
•
ECEIVE $
EMARKS:
r� } n 1 IJC.�
SAMPLE TEMPERATURE AT RECEIPT � ` { °C
RELINQU&tD BY _
C�
D TEfTI E
/
RECEIVED BY
m

1ST QUARTER

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
Date Collected
Date Received:
Sample:
Sample ID: T1B
FC Wastewater
Jan 15, 2020
Jan 15, 2020
Quarterly Sludge
Date of Report: Feb 11, 2020
Report No.: 02112020 TlB
Lab ID: 227, 94
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
pH
7.64
SU
1/15/2020
SM 4500 H+ B
ELS
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
Certified By:
L 9�) �t—
UREND. ACOSTA

I
Environmental Chemists, Inc.
660'.) Windmill 'Wav I Wilmington, NC 1-84105 o Q-10,"92,022-, Lab * 9"(1392,4424 Fax
f Bowse rtmom Road, Manteo, NC 27954 6 25-,473,570-1 Lab/Pax
W-'Fi'm-',tivtc)ni >,,a�j,j,icksonvile,NC10,347.�8431-ab"-'
D Fax
ini I o,,envirc,.,nnienta'clien-ists,co--,TI
USMC Camp Lejeune
Date of Report: Feb 10, 2020
G-F/EMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2020-01144
Project ID: Camp Lejeune MCB
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-02862 Site: T1 B
1/15/2020 8:03 AM Solid/Sludge Williams
Test
Method
Results
Date Analyzed
PAN
Calculation
19300 mg/kg
02/10/2020
Used 30% Mineralization Rate
SAR
Calculation
0,710
02/10/2020
Nitrate Nitrogen (calc)
Nitrite Nitrogen
EPA 353,2
50,2 mg/kg
01/23/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
14,7 mg/kg
01/28/2020
Nitrate Nitrogen
Subtraction Method <0,53 mg/kg
02/1012020
Sludge Residuals
Aluminum
EPA 2007
52400 mg/kg
01/28,12020
Arsenic
EPA 2007
9,21 mg/kg
01/28/2020
Cadmium
EPA 200.7
<6,60 mg/kg
01/28/2020
Calcium
EPA 200.7
49100 mg/kg
01/28/2020
Chromium
EPA 200.7
19.6 mg/kg
01/28/2020
Copper
EPA 200.7
274 mg/kg
01/28/2020
Lead
EPA 2003
12,6 mg/kg
01/28/2020
Magnesium
EPA 200.7
2900 mg/kg
01/28/2020
Molybdenum
EPA200.7
6.65 mg/kg
01/28/2020
Nickel
EPA 2007
14.4 mg/kg
01/28/2020
Potassium
EPA 2001
3590 mg/kg
01/28/2020
Selenium
EPA 200.7
<6.60 mg/kg
01/28/2020
Sodium
EPA 2003
3090 mg/kg
01/28/2020
Zinc
EPA 200.7
1170mg/kg
01/28/2020
Total Solids
SM 2540 B
379%
01/23/2020
pH
SM 4500 H B
7.87 units
01/23/2020
Ammonia Nitrogen
SM 4500 NH3 C
18800 mg/kg
01/28/2020
Total Kjeldah! Nitrogen (TKN)
SM 4500 Org B
51600 mg/kg
01/30/2020
Report #:: 2020-01144
Page 1 of 2

Environmental Chemists, Inc.
710 B + scrtowri Road, x, anted, NC 27954 -, 2252,473,57021 Lab,/Fox
2-57-A W; .niii,,tt; -i'[ -;ghu ay, i cksonilie, N C 28 `40 o l") 34 = 8 t3 I ah j FE D:
4-12 Post Lane
Camp y NC r
547
Attention: Alberta Y, Okamoto
Total Phosphorus SM 4500 P F
Mercury SW846 74716
Comment:
Reviewed by: � � a
ill fo{ 7 '.I�1<1 �7tl bit .fib. i.' �fi sts.com
Report:
Date of
Customer s ♦*
Customer ID:
26
• • / • l
Project ID: Camp Lejeune MCB
63000 mg/kg 02/03/2020
<0.412 mg/kg 01/24/2020
Report :: 2020-01144 Page 2 of 2

6602 Windmill Way Wilmington, NO 28405
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-0223 FAX [phone]
4M
Analytical Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS. OLS CERTIFICATION # 37729 [e-mail]
&
CLIENT:
PROJECT NAME: Carrin Leieune MCB_
REPORT NO:
ADDRESS: G-FIEMD/ElDB/Environmental Laboratory
CONTACT NAME: Alberta Y. Qkamatri
PO NO:
12 Post Lane
REPORT TO: Lauren Acosta
PHONEIFAX: 910-451-0020 fax [phone].
Camp I eieUrip N1(' 2R-SA
I COPY TO:
email: [e-mail], lauren.acosta@USMCA
Sampled Bv: SAMPLE TYPE: I = Influent E = Effluent W = Well, ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
2L
'0
'2
E 0
0
U
ku
M
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
0
2
T I
S LUD'
E Q
T—\
p
x
uminum, Arsenic, Cadmiun
-h;;GMi4AM, QqppeiF,
G)
P
4agnesium, Molybdenum,
G
G
C
P
'J!cK-ea-,--P-or-assium,-go—fflu—m,
gelenium, Zinc,
G
G7
C
P
Mercury Sludge, Nitrite,
lit ate. Nit-rat-e-Uit-rite
G
G
C
P
KN, Total Solids/Soils
t, I
G
G
C
P
f)_L.UU�je_,ftl11111U11.LU, 7107-71
Phosphorus, Calcium, SAR,
G
G
C
P
PAN
G
G
C
P
G__
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Daterrime
1.
JAIJ r
1r­,ed (2L21—
Refrigerator
"loev's-
2.
Refrigerator w.
/ ILNl
D111,114,
"'I -"--""Accented: 41'
pie
ed: lVt7 Time:
-TUkNAROUND:
...... . .... ...... .

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
DATE COLLECTED:
/` !S 20
DATE: <�
COLLECTED
TIME: s BY: Gr✓iria J
TIME: (D (3
ANALYZED BY: METHOD: 4500H+ B - 2000
SAMPLE
TIME
TIME
VOLUME
TEMP
pH (SU)
COLLECTED
ANALYZED
mLs
RECOVERY
BUFFER 4.00
60
-4O
BUFFER 10.00
60
!'
CHECK BUFFER 7.00
;
r ­
100
DUP F
O lg
DD
a
U
CHECK BUFFER 7.00
�g
60
!
�v
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
� a &/inns
Si nature•
/
Date Collected:'
"-- ✓d zv
Time Collected:
o sa3
Location of sample:
T1S
Truck Loading Station
Comp/Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH ***
Report all results as mg/kgmg/kg dry wt.
Was sample dechlorinated?
n/a
Preservation:
Ice
Regulatory Sample:
Yes
Field
Comments:
Relinquished by:
Date
Time
Received by:
Date
Time

2ND QUARTER
Note: No land application of residuals
occurred during the 2nd Quarter due to the
CROM tank being out of service for
maintenance.

From: Acosta CIV Lauren D
To: Straub CIV Daniel R
Subject: RE: Class A Annual report
Date: Monday, January 4, 2021 9:36:38 AM
Attachments: 4TH OTR 20 RESIDUALS 17NOV2020 REV.pdf
1ST OTR 20 RESIDUALS 153AN2020.pdf
No 2nd quarter results since the tanks were down for maintenance. No spraying was done during
this time.
1st quarter report - Mercury & Total Phosphorus are on page 2 of the report. You can remove the
ELS top sheet and COC's from report before adding to your annual report.
Revised 4th quarter report is attached which includes PAN.
R/
Lauren
Privacy Act - 1974 As amended applies, this E-Mail may contain information
which must be protected IAW DoD 5400.11R, and is For Official Use Only
(FOUO). This email and any files transmitted with it are intended solely
for the use of the individual or agency to which they are addressed. If you
have received this email in error, please notify me immediately.
For Official Use Only - Privacy Sensitive: Any misuse or unauthorized
disclosure may result in both civil and criminal penalties.
The originator of this correspondence does not have the authority to
obligate the Government. Any request for information is being used to
estimate costs and availability for planning purposes only and does not
constitute a commitment to purchase goods or services.
From: Straub CIV Daniel R <[e-mail]>
Sent: Monday, January 4, 2021 9:32 AM
To: Acosta CIV Lauren D <[e-mail]>
Subject: Class A Annual report
Lauren,
Can you please resend me the 2020 2nd Quarter Quarterly Sludge Report? I seem to have misplaced
it.
Also, it looks to me like Mercury and Total Phosphorous are missing from the 1st quarter lab results
(report #2020-01144) and PAN is missing from the 4th quarter lab results (report # 2020-19693).
Thanks,
Dan Straub

MCB Camp Lejeune
EMD Water Quality
Privacy Act - 1974 As amended applies, this E-Mail may contain information
which must be protected IAW DoD 5400.11R, and is For Official Use Only
(FOUO). This email and any files transmitted with it are intended solely
for the use of the individual or agency to which they are addressed. If you
have received this email in error, please notify me immediately.
For Official Use Only - Privacy Sensitive: Any misuse or unauthorized
disclosure may result in both civil and criminal penalties.
The originator of this correspondence does not have the authority to
obligate the Government. Any request for information is being used to
estimate costs and availability for planning purposes only and does not
constitute a commitment to purchase goods or services.

3RD QUARTER

ENWOhNUM To hCUP(mul
Drinking Water IDt 37715
114 OAKMONT DRIVE
GREENVILLE, W C. 27858
USMC CAMP LEJEUNE
COMMANDING GENERAL
MCIEAST-MARINE CORPS BASE
CAMP LEJEUNE ,NC 28542-0005
PARAMETERS
PH (not to be used ror reporting)
Aluminum, (dry wt, basis), mglltg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mglkg
Cadmium (dry ►vt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry ►►•eight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (calc)
Total Nitrogen, mg)kg (calc)
'rotal Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt,),mglkg
Nitrate Nitrogen(dry wt.), mg/kg
Nitrite Nitrogen(dry wt.), mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mglkg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample hate Analyst Code
7.5
07/23/20
TMR
4500HB-11
49807
08/13/20
LFJ
EPA200.7
5.4
08/12/20
MTM
311313-04
56561
08/13/20
LFJ
EPA200.7
3.0
09/11/20
MTM
311313-04
266
08/13/20
LFJ
EPA200.7
16
08/13/20
LFJ
EPA200.7
13
08/13/20
MTM
311313-04
2582
08/13/20
LFJ
EPA200.7
0.22
07/28/20
MTM
EPA7471 B
15
08/21/20
LFJ
EPA200.7
2902
08/13/20
LFJ
EPA200.7
C5.0
08/19/20
MTM
31135-04
1691
08/21/20
LFJ
EPA200.7
1261
08/21/20
LFJ
EPA200.7
1.9
26516
07131 /20
Si.l
4.25
07/27/20
HJO
2540G-11
c 26510
07/30/20
TLH
351.2 112-93
c 960,6
07/28/20
TTY1
350.1 112-93
c 3.99
07/29/20
DTL
353.2 112-93
c [ 1.99
07/29/20
DTL
353.2 112-93
c 38670
07/30/20
TCW
365.4-74
c 5.98
07/30/20
DTL
353.2 112-93
8151
07/31/20
SEJ
6
08/13/20
LFJ
EPA200.7
PHONE [phone]
FAX [phone]
ID#; 168
DATE COL,LECTEDi 07/22/20
DATE REPORTED ; 08/27/20
REVIEWED BY:
c Uncartifiad data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
. P.O. Boix 7085,114 Oakmant Dr. _
P.iQr 1 of 1
Greenville. NC 27858
environment 1 inc.com
DISINFECTION
CHLORINE NEUTRAtJlEUATCALLECTION
Phone [phone]$ •Fax [phone]
CHLORINE
1+68 Week 1
CLIENT;
w
pH CHECK (LAB)
P
P
P
P
P
P
P
P
P
P
CONTAINER TYPE, P!G
ISMC CAMP LEJEUNE
.'ON9 ANDING GENERAL
❑ NONE
1CIEAST-MARINE CORPS SASE,
:AMP LEJEUNE NC 18542
A
A
A
A
A
A
A
A
A
A
CHEMICAL PRESERVATION
A•NONE ❑-NAOH
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1114) 451-5977
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La z
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SAMPLE LOCATION
DATE
TIME
S1vd a Sam to
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CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES CALL CTED BY:
(Please Print)
� wrc.(�cfi ms
SAMPLES RECEIVED IN LAB AT 'Y�C
RELINQUISHED BY (SIG.) (SAMPLER)
DAMMME
B 5LG-
DATETIMEE
COMMENTS:
M
R INQUI HE BY (SI
DATE/TIME
RE. ED B
s DATEMME
7 l DW
' z
RELINQUISH (SIG.)
DAT ET1ME
RECEVED�.} T jDATFMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a T" for composite sample or a "G" for
FORM as Grab sample in the blocks above for each parameter requested. N 2 376417

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
l l_r i4+I.1jq q tol 0 IT
2Zf 20 TIME:
0950
COLLECTED
BY: W(W.+,nS
DATE: �- �� TIME: 6 q D;,—
ANALYZED BY: METHOD: 4500H+ B - 2000
SAMPLE
TIME
TIME
VOLUME
TEMP
pH (SU)
COLLECTED
ANALYZED
mLs
RECOVERY
BUFFER 4.00-TT
60
�•
��
BUFFER 10.00iiiYl�t
60
CHECK BUFFER 7.00
60
�• ( J
CROM TANK
NO')-
100
'120.9
CROM TANK DUP
�','.7
1 O0
3
-7- `'JD
�
1.0
CHECK BUFFER 7.00
60
FORM UPDATED: SEPTEMBER 2012 CHECKED BY: Lie

4TH QUARTER

enviroehem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-FIEMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y- Okamoto
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910-392,0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington 1-iighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inforii environmentalcltetnists.com
Revised Report:
Dec 22, 2020
Original Report Date:
Dec 15, 2020
Report #:
2020-19693
Customer ID:
12060026
Project JD: Cram Tank
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-50082 Site: CROM Tank 11/17/2020 7:40 AM Solid/Sludge Rubert E
Test Method Results Date Analyzed
PAN
Calculation
22800 mg/kg
12/22/2020
SAR
Calculation
0,620
12/15/2020
Total Nitrogen
Total Nitrogen
62700 mg/kg
12/22/2020
Nitrate Nitrogen (talc)
Nitrite Nitrogen
EPA353.2
<28.8mg/kg
11/20/2020
Nitrate Nitrogen
SubtractoonMelhod
63.5mg/kg
12/15/2020
Sludge Residuals
Aluminum
EPA 200.7
69900 mg/kg
12/03/2020
Arsenic
EPA 200-7
32-4 mg/kg
11/20/2020
Cadmium
EPA200.7
<16.0 mglkg
11/2012020
Calcium
EPA 200.7
51100 mg/kg
11/20/2020
Chromium
EPA 200.7
20.8 mq/kg
11/20/2020
Copper
EPA 200.7
292 mg/kg
11J20/2020
Lead
EPA 200.7
<16.0 mg/kg
11/20/2020
Magnesium
EPA 200-7
2070 mg/kg
11/20/2020
Molybdenum
EPA 200-7
<16.0 mglkg
11/20/2020
Nickel
EPA 200.7
<16.0 mg/kg
11/20/2020
Potassium
EPA 200.7
3230 mg/kg
11/20/2020
Selenium
EPA 200.7
<15,0 mg/kg
11/20/2020
Sodium
EPA 200.7
2970 mg/kg
11/20/2020
Zinc
EPA 200-7
1440 mg/kg
12104/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
63.5 mg/kg
11 /25/2020
Total Solids {°/oJ
SM 2540 B
3 0g %
11/24/2020
pH
SM 4500 H 8
8,33 units
12/09/2020
Ammonia Nitrogen
SM 4500 NH3 C
26300 mg/kg
11/19/2020
Total Kjeldahl Nitrogen (TKN)
SM 4500 Qrg B
58200 mglkg
11/19/2020
RepoA #. 2020.19693 Page 1 of 2

enviroeheF"'00' --
6h�
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-FIEMl71ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Total Phosphorus
Mercury
Comment
Reviewed by:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
SM 4504 P F
SW046 74 71B
infola environmentalchemismcom
Revised Report: Dec 22, 2020
Original Report Date: Dec 15, 2020
Report #: 2020-19693
Customer ID: 12060026
Project ID: Crom Tank
62600 mg/kg 12/02/2020
<0.521 mg/kg 11/20/2020
Results reported on a dry weight basis. pH and SAR reported on an as received basis. Revised to
add TN and PAN.
C
Report # 2020-19693 Page 2 or 2

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED _
DATE -COLLECTED: f % - �-� (.b2 U TIME: 0-7Ll 0 BY; �,,1oz �"-�C FS
DATE: I . 11- 7-Dw
ANALYZED BY:
TIME:
METHOD: 4500H+ B - 2000
074<
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
RECOVERY
BUFFER 4.00
60
�=0
BUFFER 10.00
60
CHECK BUFFER 7.00
60
(0- 00
CROM TANK
0140
�
100
43.(;70
CRDM TANK DUP
�q"�p
100
J' 51
CHECK BUFFER 7.00
0141
60
-7o l
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

SECTION 5
Annual Pathogen &Vector Attraction
Reduction Forms (Form PVRF 2T)
and Vector Attraction Reduction Lab
Sheets

1ST QUARTER

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WWTP Name: Camp Lejeune Advanced W WTP
Monitoring Period: From 1 1 2020 To
WQ Permit Number:
NPDES Number:
3; 31.2020
WQ0012346
NC0063029
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time temp) 0
I Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Beat Drying ❑
Ileat Treatment ❑
Thermophilic
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
�' Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na yhca
Tech -
nigue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 s 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
4.18
8.06
30.99
am
0
WeekIy
Grab
922n1E
Salmonella bacteria
(in lieu of Fecal
colirorm)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) © jAlt. 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Nam/
a nd 'tie (type or print) Land Applier N and Title (if applicable)(type or print)
— ��\11 %// Signat e f Pre ate Signat a of La pplierritapplicable) Date
*Prep
a is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T . 102 (26)
DENR FORM PVRF 02T (1212006)

ATAD TRAIN 1 QUARTERLY SUMMARY
Date
1/2/2020
1/7/2020
1/9/2020
1/9/2020
1/14/2020
1/14/2020
1/15/2020
1/16/2020
1/16/2020
1/16/2020
1/21/2020
1/23/2020
1/23/2020
1/27/2020
1/28/2020
1/30/2020
2/5/2020
Train 1 Feed
Train 1A
Train 1B
Volume T Solids V Solids
Temp
T Solids V Solids Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform
(gal) %
%
Deg C
% % (MPN/g)
Deg C
%
%
(MPN/g)
4.1
63.3
3.8
50.2
4.3
65.9
3.7
53.3
4.3
65.9
3.7
53.3
4.2
64.3
3.6
52.4
4.8
62.8
3.7
53.1
53.0
47.6
4.2
64.3
3.6
52.4
30.99
4.0
64.8
3.6
52.3
30.99
4.4
64.9
3.7
57.0
4.3
65.3
3.6
56.0
3.6
56.0
3.6
52.4
5.07
3.3
51.5
2.9
52.8
Comments
Wednesday, January 20, 2021 Page 1 of 2

Train 1 Feed Train 1A Train 1B
Date Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform Comments
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
No. of Entries 10
10
�
12 12 �2
Total 0
Min 4�
56
53 == 31
48 F3 50 S�
Geom. Mean �0 4�
64
53 �� 31
48 �4 53 13
Max S�
66
53 L_]l 31
48 F4 57 31
Wednesday, January 20, 2021 Page 2 of 2

ATAD TRAIN 2 QUARTERLY SUMMARY
Train 2 Feed
Date Volume T Solids V Solids
(gal) % %
1/2/2020 4.1 63.3
1/13/2020
Train 2A Train 2B
Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g) Deg C % % (MPN/g)
3.8 50.2
No. ofEntries 000
0
0
Total 0
Min 4�
F 63
L_]j
� IF 4 50
Geom. Mean 4�
763
--0
0 �0 50 �0
Max 4�
763
I L_] 1
174 50
Comments
Wednesday, January 20, 2021 Page 1 of 1

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 02/03/2020
Report No.: 2020-0002 Lab ID: 227
Sample ID:
FEED
Date Collected:
1/2/2020
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.13
%
1/9/2020
SM 2540 G
ALT
o Volatile Solids
63.32
%
1/9/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
1/2/2020
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
1/9/2020
SM 2540 G
ALT
o Volatile Solids
50.21
%
1/9/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/7/2020
Collected By:
WILLIAMS
Time Collected:
0811
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.27
%
1/9/2020
SM 2540 G
ALT
o Volatile Solids
65.87
%
1/9/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 5

Sample ID:
T1B
Date Collected:
1/7/2020
Collected By:
WILLIAMS
Time Collected:
0811
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.74
1/9/2020
SM 2540 G
ALT
o Volatile Solids
53.26
%
1/9/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/9/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.23
%
1/15/2020
SM 2540 G
ALT
o Volatile Solids
64.32
%
1/15/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
1/9/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.55
%
1/15/2020
SM 2540 G
ALT
o Volatile Solids
52.38
%
1/15/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/14/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.75
%
1/15/2020
SM 2540 G
ALT
o Volatile Solids
62.77
o
01/15/2019
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 5

Sample ID:
TlB
Date Collected:
1/14/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.66
1/15/2020
SM 2540 G
ALT
o Volatile Solids
53.10
o
01/15/2019
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/16/2020
Collected By:
WILLIAMS
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.96
1/16/2020
SM 2540 G
ALT
o Volatile Solids
64.84
%
1/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
1/16/2020
Collected By:
WILLIAMS
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.55
%
1/16/2020
SM 2540 G
ALT
o Volatile Solids
52.25
%
1/16/2020
SM 2540 G
ALT
Fecal Coliforms
30.99
MPN/gram
1/16/2020
SM 9221 C E
ALT
Sample ID:
FEED
Date Collected:
1/21/2020
Collected By:
WALKER
Time Collected:
0813
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.40
1/21/2020
SM 2540 G
LA
o Volatile Solids
64.90
%
1/21/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 5

Sample ID:
TlB
Date Collected:
1/21/2020
Collected By:
WALKER
Time Collected:
0813
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.66
%
1/21/2020
SM 2540 G
LA
o Volatile Solids
56.98
%
1/21/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
1/23/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.30
%
1/27/2020
SM 2540 G
ALT
o Volatile Solids
65.25
%
1/27/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
1/23/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.64
%
1/27/2020
SM 2540 G
ALT
o Volatile Solids
56.00
%
1/27/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
1/27/2020
Collected By:
WILLIAMS
Time Collected:
0730
Date
Analyte
Results
Units
Method
Analyzed By
Analyzed
o Total Solids
3.55
1/27/2020
SM 2540 G
ALT
o Volatile Solids
52.44
1/27/2020
SM 2540 G
ALT
Page 4of5

Fecal Coliforms 5.07 MPN/gram 1/27/2020 SM 9221 C E LA
Sample ID:
T1B
Date Collected:
1/28/2020
Collected By:
WILLIAMS
Time Collected:
1030
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.32
%
1/30/2020
SM 2540 G
AYO/LA
o Volatile Solids
51.54
%
1/30/2020
SM 2540 G
AYO/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
1/30/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.94
%
1/30/2020
SM 2540 G
AYO/LA
o Volatile Solids
52.77
%
1/30/2020
SM 2540 G
AYO/LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 5 of 5

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 03/03/2020
Report No.: 2020-0003 ATAD Lab ID: 227
Sample ID:
1A
Date Collected:
2/4/2020
Collected By:
WILLIAMS
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.81
%
2/4/2020
SM 2540 G
ALT
o Volatile Solids
50.64
%
2/4/2020
SM 2540 G
ALT
Fecal Coliforms
6.41
MPN/gram
2/4/2020
SM 9221 C E
LA
Sample ID:
T1B
Date Collected:
2/6/2020
Collected By:
WALKER
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.71
%
2/6/2020
SM 2540 G
ALT
o Volatile Solids
48.49
%
2/6/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
2/6/2020
Collected By:
WALKER
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.85
%
2/6/2020
SM 2540 G
ALT
o Volatile Solids
64.16
%
2/6/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 4

Sample ID:
TlB
Date Collected:
2/11/2020
Collected By:
WALKER
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.31
%
2/11/2020
SM 2540 G
ALT
o Volatile Solids
51.65
%
2/11/2020
SM 2540 G
ALT
Fecal Coliforms
4.18
MPN/gram
2/11/2020
SM 9221 C E
ALT
Sample ID:
FEED
Date Collected:
2/11/2020
Collected By:
WALKER
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.73
%
2/11/2020
SM 2540 G
ALT
o Volatile Solids
62.68
%
2/11/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
2/13/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.89
%
2/13/2020
SM 2540 G
ALT
o Volatile Solids
55.68
%
2/13/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
2/13/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.37
2/13/2020
SM 2540 G
ALT
o Volatile Solids
63.43
%
2/13/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 4

Sample ID:
TlB
Date Collected:
2/18/2020
Collected By:
WILLIAMS
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.70
%
2/19/2020
SM 2540 G
ALT
o Volatile Solids
52.24
%
2/19/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
2/21/2020
Collected By:
WILLIAMS
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.80
%
2/25/2020
SM 2540 G
AYO
o Volatile Solids
53.08
%
2/25/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
2/25/2020
Collected By:
WILLIAMS
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.87
%
2/25/2020
SM 2540 G
AYO
o Volatile Solids
64.17
%
2/25/2020
SM 2540 G
AYO
Fecal Coliforms
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
2/27/2020
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.38
3/2/2020
SM 2540 G
AYO
o Volatile Solids
61.24
%
3/2/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 4

Certified By:
L REN D. ACOSTA
Page 4 of 4

REPORT NO. 2020-001-BS
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 02/24/2020
Report No.: 2020-001-BS
Lab ID: 227
Date Collected: 1/21/2020 Time Collected: 1 0700 Collected By: I LA
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.99
%
1/21/2020
SM 2540 G
LA
B-S
o Volatile Solids
53.88
%
1/21/2020
SM 2540 G
LA
B-S DUP
o Total Solids
1.98
%
1/21/2020
SM 2540 G
LA
B-S DUP
o Volatile Solids
54.51
1/21/2020
SM 2540 G
LA
QUALITY CONTROL - 1/21/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.99 %
0.5 %
o Volatile Solids
54.20 %
1.16 %
Date Collected: 1/24/2020 Time Collected: 1 0730 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.94
1/27/2020
SM 2540 G
ALT
B-S
o Volatile Solids
52.98
%
1/27/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.92
%
1/27/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
52.64
%
1/27/2020
SM 2540 G
ALT
QUALITY CONTROL - 1/24/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.93
1.0 %
o Volatile Solids
52.81 °
0.6 %
Page 1 of 3

REPORT NO. 2020-001-BS
Date Collected: 1/30/2020 Time Collected: 1 0730 Collected By: I AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.88
%
1/30/2020
SM 2540 G
AYO/LA
B-S
o Volatile Solids
52.09
%
1/30/2020
SM 2540 G
AYO/LA
B-S DUP
o Total Solids
1.88
%
1/30/2020
SM 2540 G
AYO/LA
B-S DUP
o Volatile Solids
52.01
%
1/30/2020
SM 2540 G
AYO/LA
QUALITY CONTROL - 1/30/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.88 %
0 %
o Volatile Solids
52.05 %
0.2 %
Date Collected: 2/6/2020 Time Collected: 1 0730 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.51
%
2/6/2020
SM 2540 G
ALT
B-S
o Volatile Solids
49.49
%
2/6/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.52
%
2/6/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
49.58
%
2/6/2020
SM 2540 G
ALT
QUALITY CONTROL - 2/6/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.52 %
1.0 %
o Volatile Solids
49.54 %
0.2 %
Page 2 of 3

REPORT NO. 2020-001-BS
Date Collected: 2/13/2020 Time Collected: 1 0730 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.52
%
2/13/2020
SM 2540 G
ALT
B-S
o Volatile Solids
48.28
%
2/13/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.53
%
2/13/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
48.78
%
2/13/2020
SM 2540 G
ALT
QUALITY CONTROL - 2/13/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.53 %
1.0 %
o Volatile Solids
48.53 %
1.0 %
Date Collected: 2/19/2020 Time Collected: 1 0730 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.38
%
2/19/2020
SM 2540 G
ALT
B-S
o Volatile Solids
46.68
%
2/19/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.39
%
2/19/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
47.19
%
2/19/2020
SM 2540 G
ALT
QUALITY CONTROL - 2/19/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.39 %
0.7 %
o Volatile Solids
46.94 %
1.1 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 13.4 %
Certified By:
L REN D. ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
em
(00
% TS
% VS
% VS Avg
Analyst
1/21/2020
BENCH
16.9
1.99
53.88
54.20
LA
BENCH-DUP
1.98
54.51
1/24/2020
BENCH
22.7
1.94
52.98
52.81
ALT
BENCH-DUP
1.92
52.64
1/30/2020
BENCH
218
1.88
52.09
52.05
AYO/LA
BENCH-DUP
1.88
52.01
2/6/2020
BENCH
23.9
1.51
49.49
49.54
ALT
BENCH-DUP
1.52
49.58
2/13/2020
BENCH
23.8
1.52
48.28
48.53
ALT
BENCH-DUP
1.53
48.78
2/19/2020
BENCH
22.8
1.38
46.68
46.94
ALT
BENCH-DUP
1.39
47.19
INITIAL VS (%)
54.20
FINAL VS (%)
46.94
VS 13.4%
REDUCTION
VS REDUCTION= (INITIAL VS -FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

2ND QUARTER
Note: No land application of residuals
occurred during the 2nd Quarter due to the
CROM tank being out of service for
maintenance.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
NPDES Number: NCO063029
Monitoring Period: From 4/ 1 /2020 To 6/30/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
I Alt B (Alk Treatment) El
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Path ens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma R2X ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Coulpsting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data -
Parameter
Allowable Level
Pathogen Density
Number o
Excee
Frequency
Sample
Analytical
Tech.
Minimu
Geo. Mean
Maxima
Units
in Sludge
I
dences
of Anal cis
y
Type
ni ue
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFIJ
1000 mpn per gram
SM
of total solid (dry
Weekly
Grab
weight)
922 l E
Salmonella bacteria
3 MPN per 4 grams
(in lieu or fecal
total solid (dry
coliform)
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying • Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including tine and imprisonment"
Preparer NOnf 9(d Title (type or print)
Sign#bre of Preparer*
Land Applier
7JL I9 I L
Date Sianaturg
Title (if applicable)(type or print)
of LanSApplier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ATAD TRAIN 3 QUARTERLY SUMMARY
Train 3 Feed
Train 3A
Train 3B
Date Volume
T Solids V Solids
Temp
T Solids
V Solids Fecal Coliform
Temp
T Solids V Solids Fecal Coliform Comments
(gal)
% %
Deg C
%
% (MPN/g)
Deg C
% % (MPN/g)
6/25/2020
30.2
3.1
58.4
Train 3A was loaded on 06/24/2020
6/25/2020
3.1
6/26/2020
32.4
6/26/2020
32.4
6/27/2020
34.5
6/28/2020
36.8
6/29/2020 45,000
35.7
33.9
6/30/2020
37.7
39.6
No. of Entries
0 0
777F
2 7F
I �
727-F�
Total as,000
Min 45,000
17307
3�
F58
34
Geom. Mean 45,000
34
0
58
37
F0 �0
Max 45,000
L� �I
38
0
58
40
L__] L__]
Wednesday, January 20, 2021 Page 1 of 1

3RD QUARTER

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WWTP Name: Camp Lejeune Advanced W WTP
Monitoring Period: From 7? 1 '2020 To
WQ Permit Number:
NPDES Number:
9 30 2020
WQ0012346
NC0063029
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time:temp) El
I Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 131
Beat Drying ❑
1 IIeat Treatment ❑
1 Thermophilic El
Beta Ray ❑
I Gamma Ray ❑
1 Pasteurization ❑
Class B:
JAIL (1) Fecal Density ❑
1 Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g ty
a
Excec-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
aximurr
Units
Fecal CoIiform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
I000 mpn per gram
of total solid (dry
weight)
4.65
6.25
19.12
gram'
0
Weekly
Grab
922 lI lv
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) �J,
JAIL 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1 106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer 1y¢mq/ano�Citle (type or print)
of
Land Appligr Nand Title (if applicable)(type or print)
y 1Jr r
J
Date 5it=.na re of
is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .I 102 (26)
plier (if applicable)
Date
DENR FORM PVRF 02T (12/2006)

ATAD TRAIN 2 QUARTERLY SUMMARY
Date
9/6/2020
9/7/2020
9/8/2020
9/9/2020
9/10/2020
9/11/2020
9/12/2020
9/13/2020
9/14/2020
9/15/2020
9/16/2020
9/17/2020
9/18/2020
9/19/2020
9/20/2020
9/21/2020
9/22/2020
9/23/2020
Train 2 Feed Train 2A Train 2B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform Comments
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
9/24/2020 36,000
Wednesday, January 20, 2021 Page 1 of 2

Train 2 Feed Train 2A Train 2B
Date Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
9/25/2020 29.7
9/26/2020 31.9
9/27/2020 33.8
9/28/2020 35.7
9/29/2020 4.5 53.0
9/29/2020 40,500 33.9 34.0 4.5 53.0
9/30/2020 33.9 40.8
No. of Entries
0 0 �
©--
727F 2 �F�
Total 76.soo
Min 36,000
17307
L�
34 F4 53
Geom. Mean 38,184
0 0 �
7337 --07377
F4 53 �0
Max 40,500
L_] 17367
L_] 17417
F4 53
Comments
Wednesday, January 20, 2021 Page 2 of 2

CROM TANK QUARTERLY SUMMARY
CROM Tank
Date T Solids
V Solids
Fecal Coliform Comments
%
%
(MPN/g)
7/23/2020 3.9
4.65
8/5/2020 2.5
7.00
8/11/2020 4.1
5.00
8/18/2020 3.4
5.29
8/25/2020 3.4
47.7
5.28
8/25/2020 3.4
5.28
9/1/2020 3.3
5.52
9/8/2020 3.2
5.60
9/15/2020 3.1
5.75
9/22/2020 3.1
5.70
9/22/2020 4.3
47.7
9/29/2020 3.7
4.90
No. of Entries 12
11
2
Min F2
48
�S
Geom. Mean 3�
F 48
�S
Max 44
48
�7
Wednesday, January 20, 2021 Page 1 of 1

ATAD TRAIN 3 QUARTERLY SUMMARY
Train 3 Feed
Train 3A
Train 3B
Date
Volume T Solids V Solids Temp
T Solids V Solids Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform
(gal) % % Deg C
% % (MPN/g)
Deg C
%
%
(MPN/g)
7/1/2020
43.3
44.0
7/2/2020
2.8
7/2/2020
48.1
47.6
7/2/2020
51.4
7/5/2020
62.1
53.4
7/6/2020
62.1
54.4
7/7/2020
7/7/2020
2.3
7/7/2020
50.7
7/8/2020
58.5
55.1
7/9/2020
58.6
53.7
7/9/2020
3.7
4.84
7/9/2020
3.7
7/9/2020
41.4
7/10/2020
31,500 48.7
52.6
7/11/2020
47.8
54.8
7/12/2020
55.9
54.9
7/13/2020
1.7
11.00
7/13/2020
52.4
Comments
Lab error
Wednesday, January 20, 2021 Page 1 of 6

Train 3 Feed
Train 3A
Train 3B
Date
Volume T Solids V Solids
Temp
T Solids V Solids Fecal Coliform
Temp
T Solids V Solids Fecal Coliform
(gal) % %
Deg C
% % (MPN/g)
Deg C
% % (MPN/g)
7/13/2020
1.7
7/13/2020
58.6
55.8
7/14/2020
18,000
54.9
55.4
7/15/2020
18,000
55.4
53.6
7/16/2020
4.1 52.3
2.6 51.2
7/16/2020
18,000
56.2
55.4
7/17/2020
60.3
55.4
7/18/2020
63.1
55.2
7/19/2020
62.8
54.7
7/20/2020
30.000
54.2
49.8
7/21/2020
7/21/2020
4.6 55.5
4.1 50.4
7/21/2020
42.9
59.2
7/22/2020
50.0
59.7
7/23/2020 36,000
51.0
57.3
7/23/2020
4.2 54.6
4.5 48.0
7/24/2020
51.9
60.5
7/25/2020
58.3
61.1
7/26/2020
63.8
60.2
7/27/2020 37,800
53.6
58.1
7/28/2020
50.4
60.2
Comments
SPLIT TRAIN
SPLIT TRAIN
SPLIT TRAIN
Wednesday, January 20, 2021 Page 2 of 6

Date
Train 3 Feed Train 3A Train 3B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
4.8 49.9
7/28/2020
7/29/2020
18,000
7/30/2020
18,000
7/31/2020
18,000
8/1/2020
8/3/2020
8/3/2020
18,000
8/4/2020
8/5/2020
8/5/2020
8/6/2020
36,000
8/7/2020
8/8/2020
8/9/2020
8/10/2020
18,000
8/11/2020
18,000
8/11/2020
8/12/2020
18,000
8/13/2020
18,000
8/13/2020
8/14/2020
18,000
53.7
61.7
55.8
62.4
56.8
63.1
61.0
62.9
52.5
57.9
60.0
62.7
57.7
61.0
54.7
61.5
48.0
54.3
42.1
51.9
45.4
54.9
50.9
60.7
50.9
62.1
53.8
62.6
57.6 62.7
55.0 63.0
55.5 62.9
4.7 46.2
4.8 48.1
4.8 47.3
Comments
SPLIT TRAIN
Wednesday, January 20, 2021 Page 3 of 6

Date
8/15/2020
8/16/2020
8/17/2020
8/18/2020
8/18/2020
8/19/2020
8/20/2020
8/21/2020
8/22/2020
8/23/2020
8/24/2020
8/25/2020
8/25/2020
8/26/2020
8/27/2020
8/28/2020
8/29/2020
8/30/2020
8/31/2020
9/1/2020
9/1/2020
Train 3 Feed Train 3A Train 3B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
18,000 55.8 62.9
18,000 55.8 62.7
18,000 55.6 62.5
9,000
59.3
63.0
61.7
62.9
18,000
57.6
61.7
54.7
61.0
58.0
61.2
59.5
61.0
18,000
57.1
60.1
18,000
55.3
59.5
18,000
54.1
58.8
18,000
54.1
58.8
18,000
53.1
58.0
18,000
53.0
57.5
55.5
57.5
18,000
54.6
57.2
9,000 5.0 56.5
54.4
57.0
4.8 49.9
4.5 47.7
4.5 47.7
4.3 48.5 5.52
4.8 48.2
Comments
Wednesday, January 20, 2021 Page 4 of 6

Train 3 Feed
Train 3A
Train 3B
Date
Volume
T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform Comments
(gal)
%
%
Deg C % % (MPN/g)
Deg C
%
%
(MPN/g)
9/2/2020
18,000
52.9
56.6
9/3/2020
18,000
4.9
56.3
50.5
56.0
4.6
48.5
9/3/2020
4.6
48.5
9/4/2020
18,000
49.4
55.3
9/5/2020
9,000
51.5
55.1
9/6/2020
54.4
55.3
9/7/2020
18,000
54.3
55.0
9/8/2020
4.2
49.4
9/8/2020
54.8
55.4
4.2
49.4
3.24
9/9/2020
55.8
53.9
9/10/2020
4.3
46.9
9/10/2020
18,000
4.9
55.1
51.8
53.6
4.3
46.9
9/11/2020
53.7
52.9
9/12/2020
52.8
53.7
9/13/2020
53.5
51.8
9/14/2020
53.1
52.0
9/15/2020
5.2
47.4
9/15/2020
18,000
5.1
57.8
48.2
54.4
5.2
47.4
5.75
9/16/2020
46.8
54.3
9/17/2020
9/17/2020
40,500
45.0
50.6
4.5
46.9
Wednesday, January 20, 2021 Page 5 of 6

Train 3 Feed
Train 3A
Train 3B
Date Volume
T Solids
V Solids
Temp
T Solids
V Solids Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform
(gal)
%
%
Deg C
%
% (MPN/g)
Deg C
%
%
(MPN/g)
9/17/2020
4.5
46.9
9/18/2020
42.0
51.1
9/19/2020
44.4
53.3
9/20/2020
47.7
55.5
9/21/2020
52.0
53.7
9/22/2020 40,000
5.0
56.4
48.6
51.2
4.3
49.6
5.57
9/22/2020
4.3
49.6
9/23/2020
47.1
50.5
9/24/2020
4.4
50.7
9/24/2020
52.3
52.9
4.4
50.7
9/25/2020
54.6
53.4
9/26/2020
55.8
54.2
9/27/2020
55.8
54.6
9/28/2020
54.7
54.3
9/29/2020
4.2
48.0
9/29/2020 18,000
4.6
56.9
52.7
54.0
4.2
48.0
4.88
9/30/2020
48.2
52.8
No. of Entries 40
©©
89
5]F4
85
36
31
�7
Total sia,aoo
Min 9,000
5 I
55
42
4�
41
50
F2
46
�3
Geom. Mean 19,271
5 I
56
53
4�
51
F 57
FS
49
S�
Max 40,500
5I
58
64
5 ]
55
63
54
52
11
Comments
SPLIT TRAINS
Wednesday, January 20, 2021 Page 6 of 6

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 08/12/2020
Report No.: 2020-0005 ATAD Lab ID: 227
Sample ID:
T3B
Date Collected:
7/2/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.81
%
7/7/2020
SM 2540 G
ALT
o Volatile Solids
51.44
%
7/7/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
7/7/2020
Collected By:
ERNESTO
Time Collected:
0755
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.29
%
7/7/2020
SM 2540 G
ALT
o Volatile Solids
50.69
%
7/7/2020
SM 2540 G
ALT
Fecal Coliforms
NR*
MPN/gram
SM 9221 C E
* Not reported - Fecal sample invalid due to quality control failure.
Sample ID:
T3A
Date Collected:
7/9/2020
Collected By:
RUBERTE
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
%
7/9/2020
SM 2540 G
ALT
o Volatile Solids
41.44
%
7/9/2020
SM 2540 G
ALT
Fecal Coliforms
4.84
MPN/gram
7/9/2020
SM 9221 C E
ALT
Page 1 of 4

Sample ID:
T3B
Date Collected:
7/13/2020
Collected By:
WILLIAMS
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.70
%
7/13/2020
SM 2540 G
ALT
o Volatile Solids
52.39
%
7/13/2020
SM 2540 G
ALT
Fecal Coliforms
10.53
MPN/gram
7/13/2020
SM 9221 C E
ALT
Sample ID:
FEED
Date Collected:
7/14/2020
Collected By:
ACOSTA
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.77
%
7/16/2020
SM 2540 G
ALT
o Volatile Solids
56.34
%
7/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3A
Date Collected:
7/16/2020
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.06
%
7/16/2020
SM 2540 G
ALT
o Volatile Solids
52.34
%
7/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
7/16/2020
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.62
7/16/2020
SM 2540 G
ALT
o Volatile Solids
51.16
%
7/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 4

Sample ID:
T3A
Date Collected:
7/21/2020
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.57
%
7/22/2020
SM 2540 G
ALT
o Volatile Solids
55.49
%
7/22/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
7/21/2020
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.08
%
7/22/2020
SM 2540 G
ALT
o Volatile Solids
50.41
%
7/22/2020
SM 2540 G
ALT
Fecal Coliforms
19.12
MPN/gram
7/21/2020
SM 9221 C E
DES
Sample ID:
T3A
Date Collected:
7/23/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.21
%
7/28/2020
SM 2540 G
AYO
o Volatile Solids
54.61
%
7/28/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
7/23/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.51
7/28/2020
SM 2540 G
AYO
o Volatile Solids
47.97
%
7/28/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 4

Sample ID:
FEED
Date Collected:
7/28/2020
Collected By:
ACOSTA
Time Collected:
0733
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
6.30
%
7/28/2020
SM 2540 G
AYO
o Volatile Solids
53.47
%
7/28/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
7/28/2020
Collected By:
ACOSTA
Time Collected:
0733
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.87
7/28/2020
SM 2540 G
AYO
o Volatile Solids
49.30
%
7/28/2020
SM 2540 G
AYO
Fecal Coliforms
4.65
MPN/gram
7/28/2020
SM 9221 C E
AYO
Sample ID:
T3B
Date Collected:
7/28/2020
Collected By:
ACOSTA
Time Collected:
0733
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.80
%
7/28/2020
SM 2540 G
AYO
o Volatile Solids
49.92
%
7/28/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
7/30/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.74
%
7/31/2020
SM 2540 G
AYO
o Volatile Solids
48.07
%
7/31/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
LAUREN D. ACOSTA
Page 4 of 4

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 09/09/2020
Report No.: 2020-0006 ATAD Lab ID: 227
Sample ID:
T3B
Date Collected:
8/5/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.73
%
8/5/2020
SM 2540 G
ALT
o Volatile Solids
46.15
%
8/5/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
8/5/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.51
%
8/5/2020
SM 2540 G
ALT
o Volatile Solids
55.34
%
8/5/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
8/5/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.49
%
8/5/2020
SM 2540 G
ALT
o Volatile Solids
50.35
%
8/5/2020
SM 2540 G
ALT
Fecal Coliforms
7.23
MPN/gram
7/9/2020
SM 9221 C E
ALT
Page 1 of 4

Sample ID:
T3B
Date Collected:
8/11/2020
Collected By:
RUBERTE
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.77
%
8/11/2020
SM 2540 G
ALT
o Volatile Solids
48.11
%
8/11/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
ALT
Sample ID:
FEED
Date Collected:
8/11/2020
Collected By:
RUBERTE
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.70
%
8/11/2020
SM 2540 G
ALT
o Volatile Solids
56.45
%
8/11/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
8/11/2020
Collected By:
WILLIAMS
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.09
%
8/11/2020
SM 2540 G
ALT
o Volatile Solids
47.88
%
8/11/2020
SM 2540 G
ALT
Fecal Coliforms
4.87
MPN/gram
8/11/2020
SM 9221 C E
ALT
Sample ID:
T3B
Date Collected:
8/13/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.78
8/18/2020
SM 2540 G
ALT
o Volatile Solids
47.27
%
8/18/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 4

Sample ID:
CROM
Date Collected:
8/18/2020
Collected By:
RUBERTE
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.40
%
8/18/2020
SM 2540 G
ALT
o Volatile Solids
47.52
%
8/18/2020
SM 2540 G
ALT
Fecal Coliforms
5.29
MPN/gram
8/18/2020
SM 9221 C E
ALT
Sample ID:
FEED
Date Collected:
8/18/2020
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.23
%
8/24/2020
SM 2540 G
ALT
o Volatile Solids
58.13
%
8/24/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
8/18/2020
Collected By:
J. ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.75
%
8/24/2020
SM 2540 G
ALT
o Volatile Solids
49.88
%
8/24/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
8/20/2020
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.75
8/24/2020
SM 2540 G
ALT
o Volatile Solids
48.42
%
8/24/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 4

Sample ID:
T3B
Date Collected:
8/25/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.54
%
8/26/2020
SM 2540 G
ALT
o Volatile Solids
47.70
%
8/26/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
8/25/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.88
8/26/2020
SM 2540 G
ALT
o Volatile Solids
56.14
%
8/26/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
8/25/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.40
%
8/26/2020
SM 2540 G
ALT
o Volatile Solids
47.74
%
8/26/2020
SM 2540 G
ALT
Fecal Coliforms
5.28
MPN/gram
8/25/2020
SM 9221 C E
ALT
Sample ID:
T3B
Date Collected:
8/27/2020
Collected By:
J. ACOSTA
Time Collected:
0817
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.49
%
9/1/2020
SM 2540 G
ALT
o Volatile Solids
48.18
%
9/1/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
LAUREN D. ACOSTA
Page 4 of 4

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 10/5/2020
Report No.: 2020-0007 ATAD Lab ID: 227
Sample ID:
T3B
Date Collected:
9/l/2020
Collected By:
J. ACOSTA
Time Collected:
0817
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.31
%
9/l/2020
SM 2540 G
ALT
o Volatile Solids
48.52
%
9/1/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/l/2020
Collected By:
J. ACOSTA
Time Collected:
0817
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.98
%
9/l/2020
SM 2540 G
ALT
o Volatile Solids
56.52
%
9/l/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
9/l/2020
Collected By:
J. ACOSTA
Time Collected:
0817
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.25
%
9/1/2020
SM 2540 G
ALT
o Volatile Solids
47.82
%
9/l/2020
SM 2540 G
ALT
Fecal Coliforms
5.52
MPN/gram
9/l/2020
SM 9221 C E
ALT
Page 1 of 6

Sample ID:
T3B
Date Collected:
9/3/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.55
%
9/8/2020
SM 2540 G
AYO
o Volatile Solids
48.46
%
9/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/3/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.92
%
9/8/2020
SM 2540 G
AYO
o Volatile Solids
56.27
%
9/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
9/8/2020
Collected By:
J. ACOSTA
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.15
%
9/8/2020
SM 2540 G
AYO
o Volatile Solids
49.44
%
9/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
9/8/2020
Collected By:
J. ACOSTA
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.24
9/8/2020
SM 2540 G
AYO
o Volatile Solids
49.44
%
9/8/2020
SM 2540 G
AYO
Fecal Coliforms
5.6
MPN/gram
9/8/2020
SM 9221 C E
AYO
Page 2 of 6

Sample ID:
T3B
Date Collected:
9/10/2020
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.33
%
9/11/2020
SM 2540 G
AYO
o Volatile Solids
46.88
%
9/11/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/10/2020
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.88
%
9/11/2020
SM 2540 G
AYO
o Volatile Solids
55.10
%
9/11/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
9/15/2020
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.19
%
9/16/2020
SM 2540 G
ALT
o Volatile Solids
47.35
%
9/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/15/2020
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.08
9/16/2020
SM 2540 G
ALT
o Volatile Solids
57.81
%
9/16/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 6

Sample ID:
CROM
Date Collected:
9/15/2020
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.13
%
9/16/2020
SM 2540 G
ALT
o Volatile Solids
49.02
%
9/16/2020
SM 2540 G
ALT
Fecal Coliforms
5.75
MPN/gram
9/15/2020
SM 9221 C E
ALT
Sample ID:
T3B
Date Collected:
9/17/2020
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.52
9/21/2020
SM 2540 G
AYO
o Volatile Solids
46.88
%
9/21/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/22/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.01
%
9/24/2020
SM 2540 G
AYO
o Volatile Solids
56.42
%
9/24/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
9/22/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.34
%
9/24/2020
SM 2540 G
AYO
o Volatile Solids
49.64
%
9/24/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 6

Sample ID:
CROM
Date Collected:
9/22/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.13
%
9/24/2020
SM 2540 G
AYO
o Volatile Solids
49.05
%
9/24/2020
SM 2540 G
AYO
Fecal Coliforms
5.7
MPN/gram
9/22/2020
SM 9221 C E
AYO
Sample ID:
T3B
Date Collected:
9/24/2020
Collected By:
ACOSTA
Time Collected:
0925
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.39
9/24/2020
SM 2540 G
AYO
o Volatile Solids
50.66
%
9/24/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
9/29/2020
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.62
%
10/1/2020
SM 2540 G
AYO
o Volatile Solids
56.91
%
10/l/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
9/29/2020
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.49
10/1/2020
SM 2540 G
AYO
o Volatile Solids
53.02
%
10/l/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 6

Sample ID:
T3B
Date Collected:
9/29/2020
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.22
%
10/1/2020
SM 2540 G
AYO
o Volatile Solids
48.02
%
10/1/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
9/29/2020
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.68
%
10/1/2020
SM 2540 G
AYO
% Volatile Solids
47.25
%
10/1/2020
SM 2540 G
AYO
Fecal Coliforms
4.88
MPN/gram
9/29/2020
SM 9221 C E
DES
Certified By:
LIiOREN D. ACOSTA
Page 6 of 6

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
em
( DO%
TS
% VS
% VS Avg
Analyst
7/20/2020
BENCH
19.2
6.32
1.72
56.23
55.50
ALT
BENCH-DUP
1.69
54.76
7/28/2020
BENCH
26.0
NOT
RECORDED
1.63
54.32
54.29
AYO
BENCH-DUP
1.64
54.25
7/31/2020
BENCH
25.6
NOT
RECORDED
1.60
53.80
53.93
AYO
BENCH-DUP
1.61
54.05
8/5/2020
BENCH
26.0
NOT
RECORDED
1.53
52.19
52.31
ALT
BENCH-DUP
1.54
52.43
8/14/2020
BENCH
25.4
4.72
1.58
52.36
52.26
ALT
BENCH-DUP
1.59
52.16
8/21/2020
BENCH
24.1
4.56
1.72
50.13
50.07
ALT
BENCH-DUP
1.74
50.01
INITIAL VS (%)
55.50
FINAL VS (%)
50.07
VS 9.8%
REDUCTION
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

REPORT NO. 2020-002-BS
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 08/31/2020
Report No.: 2020-002-BS
Lab ID: 227
Date Collected: 7/20/2020 Time Collected: 1 1335 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.72
%
7/22/2020
SM 2540 G
ALT
B-S
o Volatile Solids
56.23
%
7/22/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.69
%
7/22/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
54.76
7/22/2020
SM 2540 G
ALT
QUALITY CONTROL - 7/22/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.71 %
1.8 %
o Volatile Solids
55.50 %
2.7 %
Date Collected: 7/28/2020 Time Collected: 1 1025 Collected By: I AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.63
7/28/2020
SM 2540 G
AYO
B-S
o Volatile Solids
54.32
%
7/28/2020
SM 2540 G
AYO
B-S DUP
o Total Solids
1.64
%
7/28/2020
SM 2540 G
AYO
B-S DUP
o Volatile Solids
54.25
%
7/28/2020
SM 2540 G
AYO
QUALITY CONTROL - 7/28/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.64
0.6 %
o Volatile Solids
54.29
0.1 %
Page 1 of 3

REPORT NO. 2020-002-BS
Date Collected: 7/31/2020 Time Collected: 1 0644 Collected By: I AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.60
7/31/2020
SM 2540 G
AYO
B-S
o Volatile Solids
53.80
%
7/31/2020
SM 2540 G
AYO
B-S DUP
o Total Solids
1.61
%
7/31/2020
SM 2540 G
AYO
B-S DUP
o Volatile Solids
54.05
%
7/31/2020
SM 2540 G
AYO
QUALITY CONTROL - 7/31/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.61 %
0.6 %
o Volatile Solids
53.93 %
0.5 %
Date Collected: 8/5/2020 Time Collected: 1 1310 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.53
8/5/2020
SM 2540 G
ALT
B-S
o Volatile Solids
52.19
%
8/5/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.54
%
8/5/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
52.43
%
8/5/2020
SM 2540 G
ALT
QUALITY CONTROL - 8/5/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.54 %
0.6 %
o Volatile Solids
52.31 %
0.5 %
Page 2 of 3

REPORT NO. 2020-002-BS
Date Collected: 8/14/2020 Time Collected: 1 1400 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.58
8/18/2020
SM 2540 G
ALT
B-S
o Volatile Solids
52.36
%
8/18/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.59
%
8/18/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
52.16
%
8/18/2020
SM 2540 G
ALT
QUALITY CONTROL - 8/18/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.59 %
0.6 %
o Volatile Solids
52.26 %
0.4 %
Date Collected: 8/21/2020 Time Collected: 1 1305 Collected By: I ALT
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.72
%
8/24/2020
SM 2540 G
ALT
B-S
o Volatile Solids
50.13
%
8/24/2020
SM 2540 G
ALT
B-S DUP
o Total Solids
1.74
%
8/24/2020
SM 2540 G
ALT
B-S DUP
o Volatile Solids
50.01
%
8/24/2020
SM 2540 G
ALT
QUALITY CONTROL - 8/24/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.73 %
1.2 %
o Volatile Solids
50.07 %
0.2 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 9.8 %
Certified By:
LAUREN D. ACOSTA
Page 3 of 3

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
DATE COLLECTED:
2Zr2o TIME:
DATE: Y ?107,-0
ANALYZED BY:
0956
COLLECTED
BY:
TIME: 6 K D;,—
METHOD: 4500H+ B - 2000
SAMPLE
TIME
TIME
VOLUME
TEMP
pH (SU)
%
COLLECTED
ANALYZED
mLs
RECOVERY
BUFFER 4.00
60
4,D0
BUFFER 10.00
60
1^^�
CHECK BUFFER 7.00
60
io-�LJ
CROM TANK
100
CROM TANK DUP
100
3 - [7
�
1.00
CHECK BUFFER 7.00
60
7OWLTAKI 19L111:1QW42IlAkI=A:Yallm
CHECKED BY: Vw

4TH QUARTER

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE WQ Permit Number: W00012346
WWTP Name: Camp Lejeune Advanced WWTP
Monitoring Period: From 101:1 2020 To
NPDES Number: NCO063029
1231 2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) El
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
Alt.D (No Prior Test)
1 Process to Further Reduce Pathogenes ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 131
Heat Drying ❑
Heat Treatment ❑
Thermophilic 21
Beta Ray ❑
1 Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Com ostin ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g ty
a
Exece-
dences
Frequency
of Analysis
Sample
Type
na ytuca
Tech -
ni ue
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th pokver
per gram of
total solids
MPN
CFU
1000 mpn per gram
oftotal solid (dry
weight)
4.81
8.27
180.15
MPN/
gram
0
Weekly
Grab
SM
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I ►rei ht)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 1(40-day bench) ❑
Alt. 3 (30-day bench) r❑
Wt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
AIt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
!l-
Preparer Name nd itle (type or print) Land Appli N
2
*zi `1
Sign a a of Prepa r* Date Signa a of Lai
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Title (if applicable)(type or print)
pplier (if applicable) Date
DENR FORM PVRF 02T (12/2006)

ATAD TRAIN 2 QUARTERLY SUMMARY
Date
10/1/2020
10/1/2020
10/2/2020
10/3/2020
10/4/2020
10/5/2020
10/6/2020
10/7/2020
10/8/2020
10/9/2020
10/10/2020
10/11/2020
10/12/2020
10/13/2020
10/14/2020
10/15/2020
10/16/2020
10/17/2020
10/18/2020
Train 2 Feed Train 2A Train 2B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
35.8 46.8
35.6
48.3
34.7
51.6
34.7
55.9
35.0
58.5
18,000
34.4
57.4
35.1
58.6
18,000
36.5
55.6
37.4
59.3
39.0
59.3
42.0
59.8
44.9
59.7
18,000
44.4
56.6
27,000
45.9
57.5
27,000
43.1
54.1
40.7
54.3
42.9
57.7
44.0
59.5
4.5 53.5
Comments
Wednesday, January 20, 2021 Page 1 of 2

Train 2 Feed
Date Volume T Solids V Solids
(gal) % %
10/19/2020
Train 2A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
41.1
Train 2B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
54.7
No. ofEntries ���7197--
7197F —1� F —1��
Total ioa,000
Min 18,000
17347
L� 1
7477 F5 53
Geom. Mean 21,169
0 0 ]
7397 -0 -0
56 FS 53 �0
Max 27,000
a 17467
L � I7607FS
53
Comments
Wednesday, January 20, 2021 Page 2 of 2

ATAD TRAIN 3 QUARTERLY SUMMARY
Date
10/1/2020
10/1/2020
10/2/2020
10/3/2020
10/4/2020
10/5/2020
10/6/2020
10/7/2020
10/8/2020
10/9/2020
10/10/2020
10/11/2020
10/12/2020
10/13/2020
10/14/2020
10/14/2020
10/14/2020
10/15/2020
10/15/2020
Train 3 Feed Train 3A Train 3B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
4.3 47.7
72,000
49.5
50.7
51.0
50.9
50.1
45.1
42.3
46.4
50.3
51.9
52.6
52.7
52.3
51.4
50.6
58.4
52.7
52.6
51.6
50.6
49.9
45.7
43.9
46.8
48.0
48.3
45.7
48.6
49.4
51.5
51.9
4.1
19.00
Comments
Wednesday, January 20, 2021 Page 1 of 2

Train 3 Feed
Date Volume T Solids V Solids
(gal) % %
10/16/2020
10/17/2020
10/18/2020
10/19/2020
Train 3A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
50.2
48.7
47.6
43.6
Train 3B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
51.7
51.2
50.4
48.9
No. ofEntries 0��
19 ���
19 ���
Total �z,000
Min 72,000
a 17427
�� 58
7447 F4 48 19
Geom. Mean 72,000
0 0 ]
7497 - 58
7497 74 48 19
Max 72,000
53 58
53 F4 48 19
Comments
Wednesday, January 20, 2021 Page 2 of 2

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 10/5/2020
Report No.: 2020-0008 ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
10/06/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.35
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
50.70
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/06/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.94
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
47.62
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/06/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.67
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
57.66
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 7

Sample ID:
CROM
Date Collected:
10/06/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.01
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
49.51
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
5.98
MPN/gram
10/6/2020
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
10/08/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.53
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
50.70
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/08/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.28
%
10/8/2020
SM 2540 G
AYO
o Volatile Solids
50.03
%
10/8/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/13/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.56
10/15/2020
SM 2540 G
ALB
o Volatile Solids
57.05
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 7

Sample ID:
T2B
Date Collected:
10/13/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.56
%
10/15/2020
SM 2540 G
ALB
o Volatile Solids
50.31
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/13/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.48
%
10/15/2020
SM 2540 G
ALB
o Volatile Solids
48.72
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/15/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.65
%
10/15/2020
SM 2540 G
ALB
o Volatile Solids
48.55
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/15/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.60
10/15/2020
SM 2540 G
ALB
o Volatile Solids
47.73
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 7

Sample ID:
CROM
Date Collected:
10/15/2020
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.12
%
10/15/2020
SM 2540 G
ALB
o Volatile Solids
47.98
%
10/15/2020
SM 2540 G
ALB
Fecal Coliforms
5.77
MPN/gram
10/15/2020
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
10/20/2020
Collected By:
ACOSTA
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.19
10/21/2020
SM 2540 G
ALB
o Volatile Solids
51.16
%
10/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/20/2020
Collected By:
ACOSTA
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.41
%
10/21/2020
SM 2540 G
ALB
o Volatile Solids
47.15
%
10/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
10/20/2020
Collected By:
ACOSTA
Time Collected:
0947
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.91
%
10/21/2020
SM 2540 G
ALB
o Volatile Solids
48.49
%
10/21/2020
SM 2540 G
ALB
Fecal Coliforms
6.19
MPN/gram
10/20/2020
SM 9221 C E
ALB
Page 4 of 7

Sample ID:
T2B
Date Collected:
10/22/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.08
%
10/26/2020
SM 2540 G
AYO
o Volatile Solids
48.00
%
10/26/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/22/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.14
10/26/2020
SM 2540 G
AYO
o Volatile Solids
45.24
%
10/26/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
10/22/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.58
%
10/26/2020
SM 2540 G
AYO
o Volatile Solids
56.99
%
10/26/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
10/27/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.28
10/29/2020
SM 2540 G
ALB
o Volatile Solids
48.86
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 7

Sample ID:
T3B
Date Collected:
10/27/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.99
%
10/29/2020
SM 2540 G
ALB
o Volatile Solids
47.11
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4A
Date Collected:
10/27/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.52
10/29/2020
SM 2540 G
ALB
o Volatile Solids
54.42
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
10/27/2020
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.98
%
10/29/2020
SM 2540 G
ALB
o Volatile Solids
60.22
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
10/27/2020
Collected By:
WILLIAMS
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
1.87
%
10/29/2020
SM 2540 G
ALB
o Volatile Solids
51.42
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
9.63
MPN/gram
10/27/2020
SM 9221 C E
AYO
Page 6 of 7

Sample ID:
T2B
Date Collected:
10/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
%
10/29/2020
SM 2540 G
ALB
o Volatile Solids
48.80
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
10/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.02
10/29/2020
SM 2540 G
ALB
o Volatile Solids
46.51
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
10/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.24
%
10/29/2020
SM 2540 G
ALB
o Volatile Solids
49.63
%
10/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 12/9/2020
Report No.: 2020-0009 ATAD Lab ID: 227
Sample ID:
T2B
Date Collected:
11/03/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.18
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
50.55
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/03/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.05
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
48.60
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
11/03/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.90
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
47.95
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 8

Sample ID:
FEED
Date Collected:
11/03/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.49
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
63.11
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/03/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.90
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
49.17
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
6.14
MPN/gram
11/3/2020
SM 9221 C E
DES
Sample ID:
T2B
Date Collected:
11/05/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.21
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
49.84
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/05/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.95
11/5/2020
SM 2540 G
DES
o Volatile Solids
46.21
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 8

Sample ID:
T4B
Date Collected:
11/05/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.50
%
11/5/2020
SM 2540 G
DES
o Volatile Solids
47.21
%
11/5/2020
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
11/10/2020
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.06
%
11/12/2020
SM 2540 G
ALB
o Volatile Solids
48.72
%
11/12/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/10/2020
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
5.51
%
11/12/2020
SM 2540 G
ALB
o Volatile Solids
45.37
%
11/12/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
11/10/2020
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.87
11/12/2020
SM 2540 G
ALB
o Volatile Solids
49.88
%
11/12/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 8

Sample ID:
FEED
Date Collected:
11/10/2020
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.46
%
11/12/2020
SM 2540 G
ALB
o Volatile Solids
63.39
%
11/12/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/12/2020
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.97
11/12/2020
SM 2540 G
ALB
o Volatile Solids
48.57
%
11/12/2020
SM 2540 G
ALB
Fecal Coliforms
6.06
MPN/gram
11/12/2020
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
11/12/2020
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.91
%
11/16/2020
SM 2540 G
AYO
o Volatile Solids
49.88
%
11/16/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/12/2020
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.12
%
11/16/2020
SM 2540 G
AYO
o Volatile Solids
47.22
%
11/16/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 8

Sample ID:
T4B
Date Collected:
11/12/2020
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.73
%
11/16/2020
SM 2540 G
AYO
o Volatile Solids
48.70
%
11/16/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
11/17/2020
Collected By:
RUBERTE
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.69
11/18/2020
SM 2540 G
AYO
o Volatile Solids
49.13
%
11/18/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/17/2020
Collected By:
RUBERTE
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.70
%
11/18/2020
SM 2540 G
AYO
o Volatile Solids
49.44
%
11/18/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
11/17/2020
Collected By:
RUBERTE
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.47
11/18/2020
SM 2540 G
AYO
o Volatile Solids
49.24
%
11/18/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 8

Sample ID:
FEED
Date Collected:
11/17/2020
Collected By:
RUBERTE
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.33
%
11/18/2020
SM 2540 G
AYO
o Volatile Solids
60.65
%
11/18/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/17/2020
Collected By:
RUBERTE
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.86
11/18/2020
SM 2540 G
AYO
o Volatile Solids
48.28
%
11/18/2020
SM 2540 G
AYO
Fecal Coliforms
6.27
MPN/gram
11/17/2020
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
11/18/2020
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.81
%
11/23/2020
SM 2540 G
AYO
o Volatile Solids
51.72
%
11/23/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/18/2020
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.65
%
11/23/2020
SM 2540 G
AYO
o Volatile Solids
51.23
%
11/23/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 6 of 8

Sample ID:
T4B
Date Collected:
11/18/2020
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.76
%
11/23/2020
SM 2540 G
AYO
o Volatile Solids
50.65
%
11/23/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1A
Date Collected:
11/24/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.29
11/25/2020
SM 2540 G
AYO
o Volatile Solids
57.06
%
11/25/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
11/24/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.73
%
11/25/2020
SM 2540 G
AYO
o Volatile Solids
50.47
%
11/25/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
11/24/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
11/25/2020
SM 2540 G
AYO
o Volatile Solids
48.72
%
11/25/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 7 of 8

Sample ID:
T4B
Date Collected:
11/24/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.77
%
11/25/2020
SM 2540 G
AYO
o Volatile Solids
49.61
%
11/25/2020
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
11/24/2020
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.91
11/25/2020
SM 2540 G
AYO
o Volatile Solids
47.71
%
11/25/2020
SM 2540 G
AYO
Fecal Coliforms
6.16
MPN/gram
11/24/2020
SM 9221 C E
ALB
Certified By:
L REN D. ACOSTA
Page 8 of 8

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 1/14/2021
Report No.: 2020-0010 ATAD Lab ID: 227
Sample ID:
TlA
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.92
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
53.27
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.62
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
48.23
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.38
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
48.98
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 1 of 13

Sample ID:
T4B
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.82
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
48.13
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0824
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.19
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
61.28
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/01/2020
Collected By:
ACOSTA
Time Collected:
0857
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.68
%
12/l/2020
SM 2540 G
ALB
o Volatile Solids
48.12
%
12/l/2020
SM 2540 G
ALB
Fecal Coliforms
6.72
MPN/gram
12/l/2020
SM 9221 C E
ALB
Sample ID:
TlA
Date Collected:
12/3/2020
Collected By:
RUBERTE
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.76
12/3/2020
SM 2540 G
ALB
o Volatile Solids
52.18
%
12/3/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 2 of 13

Sample ID:
T2B
Date Collected:
12/3/2020
Collected By:
RUBERTE
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.62
%
12/3/2020
SM 2540 G
ALB
o Volatile Solids
48.22
%
12/3/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/3/2020
Collected By:
RUBERTE
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.40
%
12/3/2020
SM 2540 G
ALB
o Volatile Solids
48.55
%
12/3/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
12/3/2020
Collected By:
RUBERTE
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.75
%
12/3/2020
SM 2540 G
ALB
o Volatile Solids
47.66
%
12/3/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/3/2020
Collected By:
RUBERTE
Time Collected:
0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.28
12/3/2020
SM 2540 G
ALB
o Volatile Solids
60.77
%
12/3/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 3 of 13

Sample ID:
CROM
Date Collected:
12/7/2020
Collected By:
RUBERTE
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.66
%
12/7/2020
SM 2540 G
ALB/AYO
o Volatile Solids
49.06
%
12/7/2020
SM 2540 G
ALB/AYO
Fecal Coliforms
6.77
MPN/gram
12/7/2020
SM 9221 C E
ALB
Sample ID:
FEED
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.79
12/9/2020
SM 2540 G
ALB
o Volatile Solids
62.77
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1A
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.83
%
12/9/2020
SM 2540 G
ALB
o Volatile Solids
50.20
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.76
%
12/9/2020
SM 2540 G
ALB
o Volatile Solids
48.17
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 4 of 13

Sample ID:
T3B
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.41
%
12/9/2020
SM 2540 G
ALB
o Volatile Solids
49.17
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.72
12/9/2020
SM 2540 G
ALB
o Volatile Solids
48.54
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/8/2020
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.65
%
12/9/2020
SM 2540 G
ALB
o Volatile Solids
48.64
%
12/9/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
12/10/2020
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.36
12/17/2020
SM 2540 G
LA
o Volatile Solids
53.60
%
12/17/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 5 of 13

Sample ID:
T2B
Date Collected:
12/10/2020
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.82
%
12/17/2020
SM 2540 G
LA
o Volatile Solids
48.02
%
12/17/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/10/2020
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.36
12/17/2020
SM 2540 G
LA
o Volatile Solids
49.34
%
12/17/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
12/10/2020
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.73
%
12/17/2020
SM 2540 G
LA
o Volatile Solids
50.00
%
12/17/2020
SM 2540 G
LA
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/14/2020
Collected By:
ACOSTA
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.72
%
12/14/2020
SM 2540 G
ALB
o Volatile Solids
48.37
%
12/14/2020
SM 2540 G
ALB
Fecal Coliforms
180.15
MPN/gram
12/14/2020
SM 9221 C E
DES
Page 6 of 13

Sample ID:
FEED
Date Collected:
12/15/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.40
%
12/17/2020
SM 2540 G
ALB
o Volatile Solids
62.61
%
12/17/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
12/15/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.70
12/17/2020
SM 2540 G
ALB
o Volatile Solids
48.44
%
12/17/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/15/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.54
%
12/17/2020
SM 2540 G
ALB
o Volatile Solids
50.69
%
12/17/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/15/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.33
%
12/17/2020
SM 2540 G
ALB
o Volatile Solids
48.00
%
12/17/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 7 of 13

Sample ID:
T4B
Date Collected:
12/15/2020
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.70
%
12/17/2020
SM 2540 G
ALB
o Volatile Solids
48.18
%
12/17/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T1B
Date Collected:
12/17/2020
Collected By:
RUBERTE
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.57
12/21/2020
SM 2540 G
ALB
o Volatile Solids
48.16
%
12/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/17/2020
Collected By:
RUBERTE
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.65
%
12/21/2020
SM 2540 G
ALB
o Volatile Solids
50.88
%
12/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/17/2020
Collected By:
RUBERTE
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.33
%
12/21/2020
SM 2540 G
ALB
o Volatile Solids
48.09
%
12/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 8 of 13

Sample ID:
T4B
Date Collected:
12/17/2020
Collected By:
RUBERTE
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.77
%
12/21/2020
SM 2540 G
ALB
o Volatile Solids
48.73
%
12/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/17/2020
Collected By:
RUBERTE
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.81
12/21/2020
SM 2540 G
ALB
o Volatile Solids
47.90
%
12/21/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
TlB
Date Collected:
12/22/2020
Collected By:
WILLIAMS
Time Collected:
1100
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.42
%
12/22/2020
SM 2540 G
ALB
o Volatile Solids
49.19
%
12/22/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/22/2020
Collected By:
WILLIAMS
Time Collected:
1100
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.58
12/22/2020
SM 2540 G
ALB
o Volatile Solids
49.69
%
12/22/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 9 of 13

Sample ID:
T3B
Date Collected:
12/22/2020
Collected By:
WILLIAMS
Time Collected:
1100
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.34
%
12/22/2020
SM 2540 G
ALB
o Volatile Solids
48.31
%
12/22/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/22/2020
Collected By:
WILLIAMS
Time Collected:
1100
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.06
12/22/2020
SM 2540 G
ALB
o Volatile Solids
63.79
%
12/22/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/22/2020
Collected By:
WILLIAMS
Time Collected:
1100
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
2.77
%
12/22/2020
SM 2540 G
ALB
o Volatile Solids
48.01
%
12/22/2020
SM 2540 G
ALB
Fecal Coliforms
7.22
MPN/gram
12/22/2020
SM 9221 C E
ALB
Sample ID:
T1B
Date Collected:
12/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.25
%
12/29/2020
SM 2540 G
ALB
o Volatile Solids
49.29
%
12/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 10 of 13

Sample ID:
T2B
Date Collected:
12/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.36
%
12/29/2020
SM 2540 G
ALB
o Volatile Solids
48.30
%
12/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.51
12/29/2020
SM 2540 G
ALB
o Volatile Solids
48.25
%
12/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
FEED
Date Collected:
12/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.19
%
12/29/2020
SM 2540 G
ALB
o Volatile Solids
61.32
%
12/29/2020
SM 2540 G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
CROM
Date Collected:
12/29/2020
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.74
%
12/29/2020
SM 2540 G
ALB
o Volatile Solids
46.29
%
12/29/2020
SM 2540 G
ALB
Fecal Coliforms
4.81
MPN/gram
12/29/2020
SM 9221 C E
ALB
Page 11 of 13

Sample ID:
T1B
Date Collected:
12/31/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.20
%
1/4/2021
SM 2540 G
DES
o Volatile Solids
50.96
%
1/4/2021
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T2B
Date Collected:
12/31/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.98
1/4/2021
SM 2540 G
DES
o Volatile Solids
52.21
%
1/4/2021
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T3B
Date Collected:
12/31/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
3.34
%
1/4/2021
SM 2540 G
DES
o Volatile Solids
53.06
%
1/4/2021
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID:
T4B
Date Collected:
12/31/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.33
%
1/4/2021
SM 2540 G
DES
o Volatile Solids
52.95
%
1/4/2021
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Page 12 of 13

Sample ID:
FEED
Date Collected:
12/31/2020
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
o Total Solids
4.22
%
1/4/2021
SM 2540 G
DES
o Volatile Solids
38.90
%
1/4/2021
SM 2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA
Page 13 of 13

REPORT NO. 2020-003-BS
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 12/16/2020
Report No.: 2020-003-BS
Lab ID: 227
Date Collected: 11/6/2020 Time Collected: 0800 Collected By: I DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
2.12
%
11/12/2020
SM 2540 G
DES
B-S
o Volatile Solids
49.95
%
11/12/2020
SM 2540 G
DES
B-S DUP
o Total Solids
2.13
%
11/12/2020
SM 2540 G
DES
B-S DUP
o Volatile Solids
49.76
%
11/12/2020
SM 2540 G
DES
QUALITY CONTROL - 11/06/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
2.13 %
0.5 %
o Volatile Solids
49.86 %
0.3 %
Date Collected: 11/12/2020 Time Collected: 0937 Collected By: I LA
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.98
%
11/16/2020
SM 2540 G
AYO
B-S
o Volatile Solids
49.46
%
11/16/2020
SM 2540 G
AYO
B-S DUP
o Total Solids
1.99
%
11/16/2020
SM 2540 G
AYO
B-S DUP
o Volatile Solids
49.51
%
11/16/2020
SM 2540 G
AYO
QUALITY CONTROL - 11/12/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.99
0.5 %
o Volatile Solids
49.49 %
0.1 %
Page 1 of 3

REPORT NO. 2020-003-BS
Date Collected: 11/16/2020 Time Collected: 0720 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.93
11/16/2020
SM 2540 G
AYO
B-S
o Volatile Solids
49.12
%
11/16/2020
SM 2540 G
AYO
B-S DUP
o Total Solids
1.94
%
11/16/2020
SM 2540 G
AYO
B-S DUP
o Volatile Solids
49.31
%
11/16/2020
SM 2540 G
AYO
QUALITY CONTROL - 11/16/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.94 %
0.5 %
o Volatile Solids
49.22 %
0.4 %
Date Collected: 11/23/2020 Time Collected: 0806 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.91
o
0
11/23/2020
SM 2540 G
AYO
B-S
o Volatile Solids
48.09
%
11/23/2020
SM 2540 G
AYO
B-S DUP
o Total Solids
1.91
%
11/23/2020
SM 2540 G
AYO
B-S DUP
o Volatile Solids
48.16
11/23/2020
SM 2540 G
AYO
QUALITY CONTROL - 11/23/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.91 %
0 %
o Volatile Solids
48.13 %
0.1 %
Page 2 of 3

REPORT NO. 2020-003-BS
Date Collected: 11/30/2020 Time Collected: 0737 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.82
%
12/1/2020
SM 2540 G
ALB
B-S
o Volatile Solids
47.50
%
12/1/2020
SM 2540 G
ALB
B-S DUP
o Total Solids
1.83
%
12/1/2020
SM 2540 G
ALB
B-S DUP
o Volatile Solids
47.67
%
12/1/2020
SM 2540 G
ALB
QUALITY CONTROL - 11/30/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.83 %
0.5 %
o Volatile Solids
47.59 %
0.4 %
Date Collected: 12/7/2020 Time Collected: 0740 Collected By: I ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
o Total Solids
1.79
%
12/7/2020
SM 2540 G
ALB
B-S
o Volatile Solids
48.68
%
12/7/2020
SM 2540 G
ALB
B-S DUP
o Total Solids
1.79
%
12/7/2020
SM 2540 G
ALB
B-S DUP
o Volatile Solids
48.70
%
12/7/2020
SM 2540 G
ALB
QUALITY CONTROL - 12/7/2020
B-S/B-S DUP
Average
%RPD
o Total Solids
1.79 %
0 %
o Volatile Solids
48.69 %
0 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION 2.3 %
Certified By:
L REN D. ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
em
( DO%
TS
% VS
% VS Avg
Analyst
11/6/2020
BENCH
2O.8
6.61
2.12
49.95
49.86
DES
BENCH-DUP
2.13
49.76
11/12/2020
BENCH
23.7
4.19
1.98
49.46
49.49
AYO
BENCH-DUP
1.99
49.51
11/16/2020
BENCH
21.8
7.76
1.93
49.12
49.22
AYO
BENCH-DUP
1.94
49.31
11/23/2020
BENCH
2O.3
5.76
1.91
48.09
48.13
AYO
BENCH-DUP
1.91
48.16
11/30/2020
BENCH
2O.8
7.91
1.82
47.50
47.59
ALB
BENCH-DUP
1.83
47.67
12/7/2020
BENCH
14.7
9.94
1.79
48.68
48.69
ALBIAYO
BENCH-DUP
1.79
48.70
INITIAL VS (%)
49.86
FINAL VS (%)
48.69
VS 2.3%
REDUCTION
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01 /2020

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED _
DATE COLLECTED: f % - �-� Lb2 U TIME: 0-7L/ 0 BY; U C'- - 11Z
DATE:
ANALYZED BY:
TIME: 014<
METHOD: 4500H+ B - 2000
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
RECOVERY
BUFFER 4.00
60
+01.
BUFFER 10.00
60
100
CHECK BUFFER 7.00
60
(0- 00
CROM TANK
0140
e-
100
f3.S�
CROM TANK DUP
V 'O
100
J- S 1
CHECK BUFFER 7.00
0141
60
-7o l
FORM UPDATED: SEPTEMBER 2012 CHECKED BY: