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HomeMy WebLinkAboutWQ0007349_Residual Annual Report 2020_20210219Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0007349 Applicant/Permittee Yadkin Valley Sevmer Authority Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Zach Key Email Address* zachkey@usbiosolids.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3369577871 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00007349 Fbs Current Existing permt number Applicant/Permittee Address* PO Box828 Elkin, NC 28621 Facility Name * Yadkin Valley Sewer Authority RLAP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Rc.) 2020 Annual Report-YVSA.pdf 1.54MB Upload only 1 FLFdocurrent (less than 250 NB). Miltiple documents rust be contained into one FDFfile unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/19/2021 2020 Yadkin Valley Sewer Authority 2020 Annual Report Land Application Program Permit No. WQ0007349 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0007349 County: Sorry Year: 2020 Facility Name (as shown on permit): Land Application Operator: Yadkin Valley Sewer Authority US Biosoilds, Inc. Phone: 336-957-7871 Land application of residuals as allowed by the permit occurred during the past calendar year? �d Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Total number ofapplication fields in the permit:1 10 Total number of fields utilized for land application during the year:1 2 Total amount of dry tons applied during the year for all application sites:f 44.17 Total number of acres utilizes for land application during the year: 16.2 Part B - Annual Comnianee Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pl I was adjusted as specified in the pertnit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was perflormed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 021' .1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .I 1 I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring we] I or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runotTof residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." %Vl C o I J c ii r� 5 7C'� �'c . ✓c �irrc Name and Title (type or print) /I.V YL+C 1llfl� Signature of Preparer* Signature of Permittee Date 3 OL t -1-J Date Sizilature of Appl ier a-3- a ail Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0007349 Facility Name: Yadkin Valley Sewer Authority Residual Source WQ # or WQ0007349 NPDES #: WWTP Name: Yadkin Valley Sewer Authority 1?-;.11 A1.,;. Tl-f- Laboratory: 1) 2) 3) 4) 5) Waypoint Analytical Parameter (mg/kg) Conc. Limit (mg/kg) Sample or Composite Date 10-5-20 Percent Solids (%) NA 291 Arsenic 75 17.2 Cadmium 85 3.45 Copper 4,300 614 Chromium NA 32.9 Lead 840 23.7 Mercury 57 0.717 Molybdenum 75 8.62 Nickel 420 17.2 Selenium 100 17.2 Zinc 7,500 614 Total Phosphorus NA 33900 TKN NA 65200 Ammonia -Nitrogen NA 2690 Nitrate and Nitrite NA 1 167 3 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalti s for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Prcparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - S Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0007349 Facility Name: Yadkin Valley Sewer Authori Residual Source WQ0007349 NPDES # or WQ#: WWTP Name: Yadkin Valley Sewer Authority Residual Analvsis Data Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) . - Parameter ®- ----------Potassium - "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) al3 l �l Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkin Valley Sewer Authority Total Dry Tons Applied (Annual): 23.66 Permit #: WQ0007349 Cation Exchange Capacity (non 503 only): Operator: Bill Hinson Owner: Bill Hinson Predominant Soil Series: FcB2 Acres Used: 9.3 Acres Permitted: 9.3 Site #: BH-01 Field #: BH-01 Residual Analvsis Data (Heavv Metals and Total Phosphorus use mz/ka, % Solids use Raw Percent #): Sample or Com- posite Date 10/5/20 z 3 a 5 6' 7 8 9 1.91 11 F 12 % Solids 2.91 Arsenic 17.2 Cadmium 3.45 Copper 614 Chromium 32.9 Lead 23.7 Mercury 0.717 Molyb- denum Nickel 17.2 Selenium 17.2 Zinc 614 Total Phos- horus 33900 Annual fleavv Metal Field LoadinEs (Calculated in lbs/acre): Total 1' ? 3 4 5' 8 7 8 9 10 11 12i DTIA c.l e A pp. Event 2.54 " Arsenic 0.088 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.088 Cadmium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Copper 3.124 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.124 Chromium 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.167 Lead 0.121 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.121 Mercury 0.004 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.044 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 denum Nickel 0.088 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.088 Selenium 0.088 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.088 Zinc 3.124 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 3.124 Total Phos- 172,483 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 172.483 horus 1 certify, under penauy of taw, tnat this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: YVSA Land Owner: Bill Hinson Operator: Bill Hinson Crop 1 Name: Fescue WQ Permit #: WQ0007349 Field #: BH1 Annual Dry `tons Applied: 23.6627 Site #: BHI Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 9.3 Acres Permitted: 9.3 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: p s ❑ Volume applied (enter one) Solids/ l,iyuid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDF.S #_ WQ#. Fert.. Animal Waste. ctc) Soil Cond. Wet. Moist) Precip. Past 24 I Irs. inches D K- i;: 6 _ _^ c y 2 N K. x N ] KN mg/kg z Y e �. mg/kg Nitrate and Nitrite mglkg PAN Applied Name of CropTSpe a Receiving. Residual Application Crop 1 Crop 2 Crop i Crop 2 6-2020 130000 2.91 1.696 W00007349 dry 0 s 0.5 0.3 65200 2690 1687 1 73.906 NA Fescue 9-2020 65000 2.91 0.848 WQ0007349 dry i} s 0.5 0.3 65200 2690 1687 36.953 NA Fescue 0.000 0.000 0.000 0.000 o.00o 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 1950001 As Cd Cu Cr Pb H Mo Ni Se Zn P 110.858 0.000 Lime Applied Annual lbs/acre 0.088 0.019 3.124 0.167 0.121 0,004 0.044 0.088 0.088 3.124 172.483 Date lbs/ac Prior Years Cumulative Ibslac 0.556 0.078 21.837 2.133 1.455 0.06 0.266 1.074 0.219 31.287 12-20 2000 Current Cumulative lbs/ac 0.644 0.096 24.961 2.300 1.576 0.064 0.310 1.162 0.307 34.411 Permitted C. P. L. R.**** 36 34 1338 NA 1 267 15 NA 1 374 1 89 2498 Permit PAN Limit Ist/2nd Crop 1 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier ©ate *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loadinz Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Yadkin Valley Sewer Authority Total Dry Tons Applied (Annual): WQ0007349 Cation Exchange Capacity (non 503 only): Bill Hinson Owner: Bill Hinson Predominant Soil Series: 6.9 Acres Permitted: 20.51 Fcl32 6.9 Site #: BH-05 Field #: BH-05 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ##): Sample or Com- posite Date _.... ..1 10/5/20 2; ...._1 3 _._.... a! 5' _ 6 _.__..) 7 _ S', _._ 9 10J 11 12 Solids 291 Arsenic 17.2 Cadmium 3.45 Copper 614 Chromium 32.9 Lead 23.7 Mercury 0.717 Molyb- denum g 62 Nickel 17.2 Selenium 17.2 Zinc 614 Total Phos- horus 33900 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1', 21 2 a' S 6 7 81 9', 10E 11' 12! DT/Ac./ o App. r. Event 2.97 Arsenic 0.102 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Cadmium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 3.650 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.650 Chromium 0.196 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.196 Lead 0.141 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.141 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 denum Nickel 0.102 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Selenium 0.102 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Zinc 3.650 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.650 Total Phos- 201,502 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 201.502 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applie r a'3-')0a1 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" 1N A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: YVSA WQ Permit #: WQ0007349 Field #: BH5 Acres Utilized: 6.9 Land Owner: Bill Hinson Annual Dry Tons Applied: 20.5076 Site #: BH5 Acres Permitted: 6.9 Operator: Bill Hinson Predominant Soil Series: Fc$2 Cation Exchange Capacity (non 503): Cron I Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN: s o Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre D Tons/Ac (Dry i Residual Sources (NPDFS #, WQ#. Fert., Animal Waste. etc) Sii1 Cond. (Dry_ Wet. Moist) Precip. Past 24 Hrs. ncnes > n o w c = �' ro a - N I'KN mg/kg Z > a mg/kg Nitrate and Nitrite mglkg PAN Applied (lips/acre) Name of Crop'l'ype Receiving Residual Application pp Crop 1 Crop 2 Crop I Crop 2 6-2020 84500 2.91 1,496 WQ0007349 dry 0 s 0.5 0.3 65200 2690 1687 64.748 NA Fescue 9-2020 84500 2.91 1.486 WQ0007349 dry 0 s 0.5 0.3 65200 2690 1687 64.748 NA Fescue 0.000 0.000 0,000 0.000 1 0.000 0.000 0.000 0.000 0,000 0.000 o.00o 0,000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 169000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 129.4951 0.000 Lime Applied Annuallbs/acre 0.102 0.021 3.650 0.196 0.141 0,004 0.051 0.102 0.102 3.650 201.502 11 Date Ibs/ac Prior Years Cumulative lbs/ac 0.14 0,039 11.992 1.239 0.835 0.038 0.148 0.598 0.117 18.003 12-20 2000 Current Cumulative lbs/ac 0.242 0,060 15.642 1.435 0.976 0.042 0.199 0.700 0.219 21.653 Permitted C. P. L. R.**** 36 34 1338 NA 267 IS NA 374 89 2498 Permit PAN Limit Ist/2nd Crop 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 7-1- 2021 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Yadkin Valley Sewer Authority WWTP Name: Yadkin Valley Sewer Authority Monitoring Period: From I/l/2020 To WQ Permit Number: WQ0007349 NPDES Number: NCO020567 12/31 /2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt` A (tithe/temp) LJ I Alt B (Alk Treatment)® 7Alt. C (Prior Testing)® Alt.D (No Prior Test) 0 1 Process to Further Reduce Pathogengs If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Li Heat Drying ® Heat. Treatment 0 Thertnophilic 3 Beta Ray Ll Gatntna Ray CJ Pasteurization LJ Class B: JAIL (1) Fecal Density D Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying ® Cotn ostin Aerobic Digestion LJ Anaerobic Digestior El If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- ences Frequency of Analysis Sample Type Analytical Tech - Minimum Minimu Geo. Mean Maximu Units Decal Coliform 2 x 10 to the 6th power per gram of total solids MPN 65573 68115 70175 MPN/g 0 7 grab sm9221 Ct iJ 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) i.-j Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) 0 Alt. 4 (Spec. O, uptake) j Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization L] Alt 7 (Drying - Stable) L,I I Alt. 8 (Drying - Unstable) Alt. 9 (injection) Lj Alt. 10 (Incorporation) ll No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." L "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." P� —TTA-V�Qtk. 01'p—c Dennis Key US Biosolids, Inc. Prep rer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signa ure of Lan Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (12/2006) Waypointo ANALYTICAL 46381 Southern Soil Builders Dennis Key 958 Hoots Road Roaring River , NC 28669 Report Number : 20-280-0003 Lab No : 73889 Sample ID : YUSA 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 11 Fax 804.271-6446 www.waypaintanaloraI.com Project US Biosolids Inc Information REPORT OFANAL IKSIS Report Date : 10/14/2020 Received : 10/06/2020 (7Q0C(y Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 10/5/2020 11:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 97.1 % 0.010 1 10/12/2017:50 FMM SM-254OG Test Results Units MQL DF Date ITime By Analytical Analyzed Method Ammonia Nitrogen 2690 mg/Kg - dry 862 1 10/13/20 14:00 JPJ SM-4500-NH3C Nitrate+Nitrite-N 167 mg/Kg - dry 165 1 10/13/20 13:51 ZBD 4500NO3F-2011 organic N 62400 mg/Kg - dry 8620 1 10/13/20 10:00 CALCULATION pH 6.1 s.u, 1 10/12/2016:30 ADM 9045D Total Solids 2.91 % 0.010 1 10/12/20 17:50 FMM SM-2540G Total Kjeldahl Nitrogen 65200 mg/Kg - dry 8620 1 10/13/20 10:00 JPJ iM-4500-NH3C-TKP Phosphorus 33900 mg/Kg - dry 172 1 10/10/20 03:34 ]ADS 6010D Aluminum 52800 mg/Kg - dry 172 1 10/10/20 03:34 ]ADS 6010D Arsenic <17.2 mg/Kg - dry 17.2 1 10/10/20 03:34 )ADS 6010D Calcium 10200 mg/Kg - dry 1720 1 10/10/20 03:34 ]ADS 6010D Cadmium <3.45 mg/Kg - dry 3AS 1 10/10/20 03:34 )ADS 6010D Chromium 32.9 mg/Kg - dry 8.62 1 10/10/20 03:34 ]ADS 6010D Copper 614 mg/Kg - dry 17.2 1 10/10/20 03:34 ]ADS 6010D Iron 27300 mg/Kg - dry 345 1 10/10/20 03:34 3ADS 6010D Lead 23.7 mg/Kg - dry 10.3 1 10/10/20 03:34 JADS 6010D Magnesium 3660 mg/Kg - dry 172 1 10/10/20 03:34 ]ADS 6010D Manganese 486 mg/Kg - dry 17.2 1 10/10/20 03:34 ]ADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 r Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46381 Southern Soil Builders Project US Biosolids Inc Dennis Key Report Date : 10/14/2020 958 Hoots Road Information : Received : 10/06/202G Roaring River , NC 28669 Pauric Mc Groary Ph.D., CPA Report Number: 20-280-0003 REPORT OFANAL YSIS Agronomist Lab No : 73889 Matrix: Solids Sample ID : YUSA Sampled: 10/5/2020 11:00 Test Results Units MQL OF Date / Time By Analytical Analyzed Method Mercury 0.717 mg/Kg _ dry 0.507 1 10/13/20 13:20 DDB SW-7471B Molybdenum <8.62 mg/Kg - dry 8.62 1 10/10/20 03:34 )ADS 6010D Nickel 17.2 mg/Kg - dry 8.62 1 10/10/20 03:34 )ADS 6010D Potassium 4760 mg/Kg - dry 345 1 10/10/20 03:34 )ADS 60101) Selenium <17.2 mg/Kg - dry 17.2 1 10110/20 03:34 DADS 6010D Sodium 2030 mg/Kg - dry 862 1 10/10/20 03:34 JADS 6010D Zinc 614 mg/Kg - dry 43.1 1 10/10/20 03:34 )ADS 6010D Sulfur S930 mg/Kg - dry 345 1 10/13/20 00:08 )ADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 SAMPLETRAN 'r)_' I %% hIt. in, kt);t,i k3chr3.,i;td V A S)vulhom Soil budded-, t4-9'.04 W; ti W Amlx 1w 46381 • •:I�i'•�It'3"i1 S:t�Err Submitted By �.�. Charge To Copy To US Biosolids, Inc. US Biosolids, Inc. i US Biosolids Inc, 958 Hoots Road 958 Hoots Road 958 Hoots Road Roaring River, NC 28669 Roaring River, NC 28669 Roaring River, NC 28669 Project � / V Sample Information Sample IB Lab NI xnber Callectrrin information Ob € se 1 oDate T,me -Yoe, I Container Information r lease Check Desired Tests N;,imber nt 3n.ties Type volume SL1 SL2 503 Metals Nitrogen series � PH i CC_ � Ag � CI � vutatlte Others Srrlld5 I g 3 :Onto Pi�SE�e a 3� Crab ie ` SJ'a j _- ..� � t ,.,lass — R,OML # t .- 07 GlassOve � �lasac _.._.. iI 1 t _....._ I I j Grab Gom�os'e Class ' Time Reim uistud B S nature Date Received By Si nature "ate O �. E Test Package Details S eciat instructions or Remarks tit.t i :11£31l f4teii': lt_ 503 Metals: A-semc� Cadm;um Cnroml rn.. Mercury. Molybdenum,, Lead, NTke3, Selen,un,. (copper & Zinc Incluci Ptl In SL22 Ltlr€x�rn �erirs: l.xt= i r a[d;tl�- 1a1.•,=-;t,.im N-.tt n CCE. Cal€au"i %/;)kj, (1-of L. rte .I ealeo Sludq(n E r m.. r..._.__..._� Q) tT ro a PAN Mineralization as decimal ITotal dry tanslyear jAcres I Applied on Rate 0.3 TKN 65200 NH3 1 2690 NO3 167 NO2 0 % Solids 0.0291 PAN Surface 20265 mg/kgmg/kg 40.53 lbs/dry ton 01 Ibs total PAN #DIVIO! Ibs PAN/acre PAN Injection 21610 m !k 43.22 lbs/dry ton 0 Ibs total PAN #DIVIO! Ibs PANlacre Dry Tonsl1000 gal. 0.121347 1st year PAN Surface lbs. 0 1st year PAN Injected Ibs. 0 Ibs.lacre Surface #DIV/0! Ibs./acre Injected #DIV/0! MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mglkg mglkg x .002 =lbsldry ton MR(TKN-NH3) + l(NH3)+NO3+NO2 =mglkg mg/kg x .002 =lbsldry ton 1000 X 8.34 X %solids X sp_gravity 2000 "=dry tons/1000gal." SAR Sodium Absorption Ratio Na : Sodium (MgIL) Equivalent weight: 23 Ca: Calcium (MgIL) Equivalent weight: 20 Mg : Magnesium (MgIL) Equivalent weight: 12 Milli Equivalent = MgIL 1 Equivalent weight Na M IL Ca M IL M MIL 59.07 1 296.82 1 106.5 Na NEI I 94-NEB I Mg-LMQ 2.568261 14.841 8.875 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent * Mg Milli equivalent)]0.5 power SAR = 0.745819 (From MgIL entered above) SAR= 0.417061 (From ME entered below) Na ME Ca (ME) Mq (ME) 0.29 1 0.328 I 0.639 The amour amount of t Permitting Analytical Results STATESVILLE ANALYTICAL U.S. Biosoilds Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/17/2020 Reported: 03/19/2020 For: YVSA Comments: GM 68,115 MPNIg Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200317-37-01 Fecal Coliforms 1 68966 MPNIg SM92210E-2006 03/18/2020 WC 200317-37-01 Percent Solids 1 3.48 ova SM25 O8.2011 03/18/2020 WC 200317-37-02 Fecal Coliforms 2 69565 MPNIg SM92210E-2006 03/18/2020 WC 200317-37-02 Percent Solids 2 345 % SWWR-2911 03/18/2020 WC 200317-37-03 Fecal Coliforms 3 66667 MPNIg SM92210E-20os 03/18/2020 WC 200317-37-03 Percent Solids 3 360 % SM254OB-2011 03/18/2020 WC 200317-37-04 Fecal Coliforms 4 67989 MPNIg SM92210E-2006 03/18/2020 WC 200317-37-04 Percent Solids 4 353 % SM25405-2011 03118/2020 WC 200317-37-05 Fecal Coliforms 5 70175 MPN/g SM92210E-2006 03/18/2020 WC 200317-37-05 Percent Solids 5 342 % SM254OB-2011 03/18/2020 WC 200317-37-06 Fecal Coliforms 6 67989 MPNIg SM92210E-2006 03/18/2020 WC 200317-37-06 Percent Solids 5 353 % SM25AOB 2011 03/18/2020 WC 200317-37-07 Fecal Coliforms 7 65573 MPNIg SM92210E-20M 03/18/2020 WC 200317-37-07 Percent Solids 7 3.66 % SM254OB-7011 03/18/2020 WC Respectfully submitted. Dena Myers NC Cert #440, NCDW Cert #37755. EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 Client, TATFSMI_I_F. Address: o r+,f 6 ^_ �� ; owt it ct Ra l] 1ZZe MM srr«, • ra � zza slM�,A,E8, 2u 963, P944t k �$C7 7 Canted Perron: Phone * Fes* 3 c•� ry Chain of Requieilioned by: Custody Record G ID N SampNIDf rebonyy (�+�_�?_..�....... w '"'" ------ T Y �s I 2GQ3J�. 37. r -- :1-17 p0 _ 2 - -- ---- — 0 x _— Relinquished by: Time _L�Lo dm, pm Date ! r�i! DO Sampled by: Aecoived by: - ._ j Time I000am, pm Dais 3�'7� Transported by Relinquished by: - Time am, pm Date _l �l Holding times met: f fr Received by: Time am, pm Date . 1 Compliance work: Composite Settnnling I ; _ Time begin am, pm Date Non-compliance work: Tune end am. pm Date _____l_1_ lab Comments: 3ampkw Transposed On be: Time begin am, pm Dale ---.J_. Tkm end am, pm Date 0o W 00 U z ai a Y LA co rV rV Q m 0 Analytical Results U.S. Biosolids Inc 958 Hoots Road Roaring River, NC 28669 Receive Date: 07/30/2020 Reported: 09/08/2020 For: YVSA Comments: 4 STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200730-22-01 30 Day Benchscale YVSA Respectfully submitted, 'Op 'j,O, I Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 % taa625-R-92Ya 07/30/2020 WC PO Box 228 a Statesville, NC 28687 • 704/872/4697 Page 1 of 3 Condition of Receipt Sample Number 200730-22-01 Temp on Arrival: 4.5 Parameter Schedule: Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 3 Client: '^ A S TAT FS V I I, L. iF ANALtr1tCA#. 122 coed swa • P.U. Box = sw.w.ills, NC 2607 r' C7N1 N72.I647 Own of Custody Record Address: as iT V r !Y V `Q contact Person: "none" 336- y �� • s3 (? � * PO 0_ Requlsiitoned by: rime Dare! Cuseorrra 3wnple IDN Lab -ID N 1" Sampled (Grab Orgy) Dole Sampled (Omb Onp aldf rarsmeltn r quated for.mJr»s --_---. _---_ . w T ww Relinquished by: Received by: Relinquished by: Received by: Time begin am, pm Date/ Time end aril, pm Date Comooatte SamRjjng2: Time begin--- - am, pm Date-- Time end am, pm Date _.-_-. -- !J // ! -j _ ! ! Time V Time Time ---.._- Time Lab Commends: am, @ Date �J� 1 0 Sampled by l,,1 vv am,goDate 2 �! Transported by: am, pm Date - Holding Holding limes met: am, pm Date �_1� Compliance work: Non-compliance work: — Samples Transported On Ice: Indiab: I I n 00 W 00 N l.1 ai a 00 N N x 0 CO O CL �' ZAnalytkjlo I ANALYTICAL RESULTS Project: YVSAIUS BIO Pace Project No.: 92470434 Papa Analytical Services, LLC 9800 Kincey Ave. SuRe 100 Huntersville, NC 2OD78 (704)875-M2 Sample: 200317.36.01 Lab ID: 924704MOl Collected: 03/17/20 13:00 Received: 03120/20 09:30 Matrix: Solid Results reported on a 'dry welghr basis and are adjusted for percent molshwa, sample she and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Prsparation Method: 8151A Leachate Method/Date: 1311; 03126/20 10:33 Initial pH: 6.33: Final pH: 4.94 Pace National - Mt. Juliet 2,4,5-TP (Sitvex) N❑ mglL 0.00200 1 03127/20 08:22 03/27/20 16:37 93-72-1 2,4-D NO mg/L 0.00200 1 03127M 08:22 03/27/20 16:37 94-75-7 Surrogates 2,4-OCAA (S) 67A % 14.0-158 1 0&27120 08:22 03/27120 16:37 19719-28-9 U1411 TCLP Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3610C Leschate MethodlDate: EPA 1311; 03/26/20 16:12 Pace Analytical Services - Charlotte gamma-BHC (Lindane) NO ug/L 0.50 1 03/30120 17:06 04/01/20 15:39 58-89-9 Chlordane (Technical) ND ug/L 3-0 1 03l30120 17:06 04/01/20 15:39 57-74-9 Endrin ND ug/L 0.50 1 03/30/20 17:06 041010) 15:39 72-20-8 Heptachlor ND ug/L 0,50 1 0313012017:06 04101/2015:39 76-44-8 Heptachlor epoxide ND ug/L 0.60 1 03130l2017:06 0410112015:39 1024-57-3 MethoxydNor ND ug1L 1000 1 0313012017:06 0410112015:39 72-43-5 Toxaphene ND uglL 3.0 1 0313012017:06 04101/2015:39 0001-35-2 surrogates Decachlorobiphenyl (S) 78 % 10-138 1 03130/2017:06 04101/20 15:39 2051-24-3 Tahachloro-m-xylene (S) 13 % 10-110 1 03/30/20 17:06 04101/20 15:39 877-09-8 801i2 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311: 0312" 16:12 Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) NO ug/L 1000 1 03130/20 17:41 03/31120 23:26 12674-11-2 PCB-1221 (Aroator 1221) ND ug/L 1000 1 03/30/20 17:41 03/31120 23:26 11104-28-2 PCB-1232 (Aroclor 1232) NO ug/L 1000 1 03t30/20 17:41 03131/20 23:26 11141-16-5 PM1242 (Amclor 1242) NO ug/L low 1 0313WO 17:41 0313112023:26 53469-21-9 PCB-1248 (Anxdor 1248) ND uglL 1000 1 031301P0 17:41 03/31120 2326 12672-29-6 PCB-1254 (Aroclor 1254) NO uglL 1000 1 03130/20 17:41 03/31120 23:26 11097.69A PCB-1260 (Arodor 1260) NO ug/L 1000 1 03/30/20 17:41 0313112G 23:26 11096-82-5 Surrogates Decechbrobiphenyl (S) 19 % 10.132 1 03130/20 17:41 0313112023:26 21151-24-3 6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311: 04101120 16:10 Initial pH: 776; Final pH: 4.5 Pace Analytical Services - Asheville Arsenic ND mg/L 0.050 1 0410212011:11 W0212017:46 7440-38-2 Barium 0.37 m91L 0.25 1 04102(20 11:11 04/02120 1746 7440-39-3 Cadmium ND mg/L 0.0050 1 04/0212011:11 0410212017746 7440-43-9 Chromium NO mg1L 0.050 1 04102/20 11 11 04102l2017:46 7440-47-3 Lead ND mg1L 0.025 1 0410212011:11 0410212017:46 7439-92-1 Selenium ND mg/L 0.10 1 04102/2011:11 04)0212017746 778249-2 Silver ND mg1L 0.025 1 04/0212011:11 0410212017:46 7440-22-4 REPORT OF LABORATORY ANALYSIS This report shall nut be reproduced. etcept in ruil. Date: 04/03/2020 04:55 PM without the written consent of Pace Anatytical Services. LLC- Page 5 of 27 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 14 of 38 CeA 1aykafe ANALYTICAL RESULTS Pau Analytical Servicaa, LLC 9500 K"Ave. Suite 100 Hunlersville, NC 26078 (704)875-9092 Project: YVSAIUS BIO Pace Project No.: 92470434 Sample: 200317.36.01 Lab to: 92470434001 Collected: 0311712013:00 Received: 03120/2009:30 Mat7tx: Solid Results reported on a .dry weight' basis and are jqusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. dual 7470 Mercury, TCLP Analytical Me01od: EPA 7470A Preparation Method, EPA 7470A Leachate McModlDate: EPA 1311: 04101/20 16:10 Initial pH: 7.76; Final pH: 4.5 PaceAna"rat Services -Asheville Mercury NO mg1L 0.00020 1 0410212011:35 0410212015:57 7439,97-6 8270E TCLP RVE Anatyticat Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 1,4-Dichlombenzene ND ug1L 250 5 03131t2015:03 04101120 12:27 10646-7 2,4-Dinitrotoluene ND ug1L 250 5 0313112015:03 M01/2012:27 121-14-2 M1 Hexachioro-1,3-butadiene NO uglL 250 5 03/31/2015:03 0410112012:27 87-68-3 Hexachlorobenzene NO ug1L 250 5 03/31/20 15:03 04/01/20 12:27 118-74-1 Hexachloroethane ND ug1L 250 5 03131/20 15:03 04101/20 12:27 67-72-1 2-Methylphenopo-Creso4) NO uglL 250 5 0313112015:03 0410112012:27 95-48-7 3&4-Methylphenol(m&p Cresol) 1090 ug1L 250 5 03131120 15:03 04/01120 1227 15831-104 Nitrobenzene NO ug1L 250 5 03131120 15:03 0410112012:27 W95-3 Pentachlorophenoi NO ug1L 500 5 03131120 15:03 04101120 12:27 87.8&5 M1 Pyridine NO ug1L 250 5 03131/20 15:03 0410112012:27 110-W-1 2,4,5-Trichlorophenoi NO ug1L 250 5 03131/20 15:03 0410112012:27 95-95-4 M1 2,4,6-Trichlorophend NO ug1L 250 5 03131/20 15:03 0410i12012:27 88-06-2 M1 Surrogates Nitrobenzene-d5 (Sj 48 % 12-102 5 03131/20 15:03 04101I20 12:27 4166-60-0 D3 2-Fluombiphenyl(8) 40 % 13-107 5 03131/20 15:03 04101/20 12:27 321-60-8 Terphenyl-d14 (S) 43 % 21-132 5 03131/20 15:03 04/01/20 12:27 1718-51-0 Phenold6 (S) 27 % 10-110 5 03131120 15:03 04101120 12:27 13127-88-3 2-Flumphenot (S) 29 % 10-110 5 03131120 15:03 04101120 12:27 367-124 2,4,&Tribromophenol (S) 38 % 27-108 5 G313112G 15:03 04/01/20 12:27 118-7" 82800 MSV TCLP Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Benzene ND ug1L 100 20 03131/20 04:28 71-43-2 2-Butanone (MEK) ND ug1L 200 20 03/31M 04:28 78-93-3 Carbon tetrachloride ND ugfL 100 20 03131120 04:28 56-235 Chlorobenzene ND ug1L 100 20 03131/20 04:28 108-90-7 Chlorolotm ND ugR 100 20 03131120 04:28 67-W3 1,4-Dichlorobenzene NO uglL 100 20 031311200428 10646-7 1,2-Dichloroethane NO ugfL 100 20 0313112004:28 107-06-2 1,1-Dichloroethene ND ug1L 100 20 03131120 04:28 75-354 Tetrachloroethene NO uglL 100 20 03/3112004:28 127-184 Trichioroethene NO uglL 100 20 03/3112004:28 79-01.6 Vinyl chloride ND ug1L 100 20 03/3112004:28 75-014 Surrogates 1,2-Dichloroethaned4 (S) 102 % 70-130 20 03/31120 04:28 17060.07-0 Toluene-& (S) 107 % 67-135 20 03/31/20 04:28 2037-26-5 4-Bramofluorobenzene(S) 105 % 70-130 20 03/31/20 04:28 460-00-4 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, Date: D410312020 04:55 PM without Me written consent or Pace Analytical Services, LLC. Page 6 of 27 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 15 of 38 ANALYTICAL RESULTS Project: YVSAIUS 810 Pace ProjectNo.: 92470434 Pace Analytical Services, LLC 9800 Kincey Ave- Suite 100 Huntersolle, NC 28070 (704)875-9092 Sample: 200317.36.01 Lab ID: 92470434001 Collected: 03/17120 13:00 Received: 03120120 09:30 Matrix: Solid Results reported on a dry weight' basis and are adjusted for percent moisture, sample alze and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual Percent Moisture Analytical Method: ASTM D2974$7 Pace Analytical Services - Charlotte Percent Moisture 96.5 % 0.10 1 03/23120 15:25 1010 FlashpolMClosed Cup Analytical Method: EPA 1010A Pace Analytical Services - Asheville FEashpoint ;-200 deg F 70.0 1 03131120 10:48 9045 pH Soil Analytical Method: EPA 90450 Pace Analytical Services -Asheville pH at 25 Degrees C 6.7 Std. Units 0.10 1 03130120 14:27 9095 Paint Filter Liquid Test Analytical Method: EPA 9095B Pace Analytical Services -Asheville Free Liquids Fail 1.0 1 03/26120 15:08 T33C S Reactive Cyanide Analytical Method: EPA9014 Preparation Method: SW-W 7.3.3.2 Pace Analytical Services - Greensburg Cyanide, Reactive NO mg/kg 28.8 1 03123120 15:02 0312312015:36 734E Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2 Pace Analytical Services - Greensburg Sulfide, Reactive NO mg/kg 288 1 03/23120 15:02 03123/2015:03 H3 Sample: 200317.36.01 PCB Lab lC: 92470434002 Collected: 03/17/20 13:00 Received: 03120M 09:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual SM GCS PCB RYE PCB-1016 (Arodor 1016) PCB-1221 (Arodor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Arodor 1242) PCB-1248 (Arodor 1248) PCB-1254 (Arocior 1254) PCB-1260 (Arocior 1260) Decachhorobiphenyl (S) Date: 04103/2020 04-55 PM Analytical Method: EPA8W2A Preparation Method: EPA3510C Pace Analytical Services - Charlotte NO uglL 2.5 1 0313112015:55 04101/2022:13 12674-11-2 NO ug1L 2.5 1 03/31/20 15:55 04101120 22:13 11104-28-2 NO ugrL 2.5 1 03/31/20 15:55 04101/20 22:13 11141.16.5 NO ug1L 2-5 1 0313112015:55 04101/2022:13 53469-21.9 NO ug+L 2.5 1 0313112015:55 04101/2022:13 12672-29-6 NO ug1L 2.5 1 0313112015:55 04101/2022:13 11097-69-1 NO ugrL 2.5 1 03/31/20 15:55 04/01/20 22:13 11096.82-5 35 % 10-130 1 03Q1120 15:55 04/01/20 22:13 2051-24-3 REPORT OF LABORATORY ANALYSIS This report shall not the reproduced, except in full. Widwul the Written Consent of Pace Analytical Services, LLC_ Page 7 of 27 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 16 of 38 it S )giof.lud-s 'T"-' STATIFSVII-11 A* ANALY MAIL 122(ourt'%nmt - P.O.HoxM StatesvilKNC 29687 (704) 972-4W Chain of Cus"y Record Address: PO Contact Person: "0"' ' 33C sla-1 FAX" P(5-f— v Requisitioned by: Date) c6i7ww Sa m* ON Lab -ID Thm Swnpled (Grab Orgy) caw Sampled (Grab Orgo %*"I Manx W I w fa 0 o 7-((-Oo t#- red', Relinquished by: Time Iquo am, pm Date IL Sampled by; Received by: Time /q(iOam,pm Date Z>//'7?.o Transportedby Relinquished by: Time am, pm Date Holding times met: Received by: Time am, pm Date Compliance wok Comnaft Sampling-01; Time begin— am, pm Date Non-compliance work:____ Time and---..-----am,pm Date Lab Comments: Samples Trantpoded On low Composite Sampling #2: — Time begin —am, pm Date-1-1— Time end am, pm Date rn M to et OD 0 00 r- 00 tD 00 z ai 41 41 M V)4� 00 C%j C4 0 0. NCDAB,CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ Report No. FY21-SLO13289 i -p Predictive Client: Bill Hinson 537 Rock Ford Rd y Advisor: Zach Key Southern Soil Builders r Roaring River, NC 28669 958 Hoots Rd ��� ReportMehIICh-3 Extraction Roaring River, NC 28669 Sampled County : Wilkes Links to Helpful Information � Client ID: 478377 Advisor ID: 231531 Sampled: Received: 11/1112020 Completed: 12/02/2020 Farm: Sample ID: BH01 Recommendations: Lime Nutrients (lb/acre) More I Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B information Lime History: 1- FescuelOGrass/Tim, M 1.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- 0.0 i Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/drr?]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.49 0.97 7.5 72 2.1 5.5 129 85 50 17 51 155 110 201 201 352 0.2 3 Sample ID: BH02 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 1.0 120-200 0 30 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg1dm13]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.02 1.01 6.3 67 2A 5.4 116 57 47 16 42 125 92 317 317 650 0.1 2 Sample ID: BH03 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fesoue/OGrass/Tim, M 1.0 120-200 0 10 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units -WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dry?): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.76 1.01 5.9 66 2.0 5.4 215 75 45 15 50 142 102 399 399 832 0.1 2 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Aariculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO13289 Bill Hinson Page 2 of 3 Sample ID: BH04 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 1.5 120-200 0 70 0 0 0 0 0 0 Nate: 12 2 - 0.0 j Test Results [units - W!V in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/drr?]: Soil Class: Mineral HM% WfV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.97 0.96 7.1 63 2.6 5.2 329 33 45 16 60 116 87 580 580 939 0.2 3 Sample ID. BH05 Recommendations: Lime Nutrients (lb/acre) More I Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information i Lime History: 1-FescuelOGrass/Tim, M 1.8 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dry?]: i Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.19 0.90 6.5 55 2.9 5.0 301 84 36 13 90 160 113 407 407 756 02 3 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi! Report No. FY21-SLO13289 Bill Hinson B Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% %GEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate; CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent i Fertilizer HM% percent humic matter Recommendations for field crops or other ►arge areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies potash for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they Mq % %CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN Mn mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 to levels. If $, $pH, C or Z Mn-I manganese index Farmers and other commercial producers should pay special attention micronutrient pH$, M-O mineral -organic soil class I notations appear on the soil report, refer to Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.nca r. ov/a ronomi/ob art4.hf lnd information that P-I phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume Zn-AI zinc availability index The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaqr.govlauronomiluvrst.htm