HomeMy WebLinkAboutWQ0040918_Monitoring - 11-2020_202012297
• - W-59A COMPLIANCE REPORT FORM ermit ;-!1" V V
q I a
(Subaru one each aw n taring periad with GW--59 forms.)
j
Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A)
YES
O
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is 'NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
standards in the spade provided below:
exceeding �.i
(`nui_y �-3 `� N St
nj
5
For the constituents identified in question 4 above, have standards been excdeA&d previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is 'NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
� W ards, car ntiation(s) re rted, and sample collection date for each occurre ce (for the last two years).
MvJ—a
mw-a, ,
�1-1�-ao�.°I�t•s <<-1�-ao ���s
Are the monitoring wells list din section 5 located at or beyond the review boundary?
YE
NO
If the answer is "YES", a groundwater quality problem may be occqqr� n�gs-CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", mo►#ItblHho wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is 'YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Vio/a6"Qn
fine1s, and/orpenalties. j Q
1, WWS C� l S 6&u) S-� Ul l
MW —3 C --gy p _ -c�� (Ooa OCc j C\
0 Tcev) 4. aA
g
The person completing tWs portion (GW-59A) of the monitoring report shOild sign below anOAmifthis
form with G W-59 forms for required wells to the address provided at the top of the current G "$ form.
l hereby acknowkKige that the above rformation was evaluated and the informabon submitted itiVft
report (Compliance Report GW ) is complete to the best of my knowledge.
an
Signature of Pe ittee (or Authorized Agent) Date
"-I,
GW-59A 12/8/2003
—�X\w — 3 eD �4 --wN) — �) ��ico-( UAorrfA
-- R-- ao �, Ste—
o -73-1 0
0 SAS
L ` - ` � 1-" oZ Vy 7 Ii--_. `-- —
r)-`I -ao 33,3v�
_--6 - Ck.- a o _ -
SUBMIT FORM
PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORMA
Facility Name:
Permit Name (If
Facility Address:
act Person:
Location/Site
hq
or
Telephone#: __a93-
No. of wells to be sampled:
PERMIT NumberQ01JAZi Ixiration Date: 0
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
k-Ingoon ❑ Remediatlon: Infiltration Gallery
'Spray Field ❑ Remedlation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from ermit):VV *~\ Date sample collected�1� `' 1" FIELD ANALYSES:
Well Depth: o ® ft. Well Diameter: In. pH 00400:'t, units Temp. 00010 S°C
Depth to Water Level 82546:ft. below measuring point Screened Interval: ft. to ft. Spec, Cond. 00004: µMhos
Measuring Point Is _ft. above land surfac Relative M.P. Elevation: ft. Odor 000m: t 9,�
Volume of water pumped/bailed before sampling: gallons Appearance
Samples for metals were collected unfiltered: I] YES ❑ NO and field acidified: 0 YES ❑ NO
LABORATORY INFORMATInKI --+ �.
Date sample analyzed:\ —�� �� �`�- `�—
PARAMETERS NOTE: Valu es sho Id reflect c
COD 00335 mg/L
Coliform: MF Fecal 31616 s /100mL
Coliform: MF Total 31504 /100mL
(Note: Use MPN method for highly turbid samples)
solved Sollds:Total 70300 mg/L
pH (Lab) 00403 units
TOC ooseo_�Q, mg/L
Chloride 00940 mg/L
Arsenic 01002 ug/L
Grease and Oils 00552 mg/L
Phenol 32730 ug/L
Sulfate 00945 mg/L
:cific Conductance 00095 µMhos
Total Ammonia oosao mg/L
(Ammonia Nitrogen; NH. as N; Ammonia Nitrogen, Total)
TKN as N 00625
mg/L
For Remedlation Systems Only (Attach Lab Reports):
,,_ao— aboratory Name:
�
�V1 �'O .cy�
Certification No,��
and collafdal concentrations.
Nitrite (NO2) as N 00615
mg/L
Pb - Lead oio5i ug/L
Nitrate (NO3) as N 00620 mg/L
Zn - Zinc 01092 mg/L
Phosphorus: Total as P oo665 y', / () mg/L
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
AI -Aluminum olio5
mg/L
Ba - Barlum 01007
ug/L
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
uglL
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? P"' Yes (1) ❑ No (0)
K - Potassium 00937
mg/L
VOC 7873 method # S l 6''Rme
Mg - Magnesium 00927
mg/L
method #
Mn - Manganese oio55
ug/L
method #
NI - Nlckei 01067
ug/L
method #
Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
WELL
DRY at
time of
here:0
SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER (QUALITY MONITORING:
COMPLIANCE REPORT FORM
earyor iype PERMIT Number �� p (ration Date:
Facility Name: Aq�(b� f1 �{���e�-- Non -Discharge UIC
Permit Name (if different)rrr:� NPDES Other
Fac Iity Address: TYPE OF PERMITTED OPERATION BEING MONITORED
S'3 County \'
goon ❑ Remediatlon: Infiltration Gallery
tr;tzdel (zIp)
� � e(�p� Telephone � Ly'°Spray Field ❑Remedlation:
Contact Person:
6 33 ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:m e No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other:
...,,... �..�....� .,'.'„-. ' ,,.aa
WELL ID NUMBER (from Permit):
Date sample collected:,' �— o ®
•FIELD ANALYSES:
If WELL
Well Depth: �ft.
Well Diameter:f,), in.
pH 0040041 units Temp. 000io:l6/ 9 °C
WAS
DRY at
Depth to Water Level 82546: ,,11_4 ft. below measuring point
Screened Interval: ft. to ft.
Spec, Cond. 00094: µMhos
time of
Measuring Point Is _ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: 0
sampling,
Volume of water pumped/balled before sampling:
Appearance
check
_gallons
Samples for metals were collected unfiltered: ® YES ❑ NO
and field acidified: 0 YES ❑ NO
here:
LABORATORY INFORMATION k \ — — _ r%,
Date sample an
PARAMETERS
COD 00335
_mg/L
Coliform: MF Fecal 31616� ,
/100ml-
Collform: MF Total 31504
/100ml-
(Note: Use MPN method for highly turbid samples)
Issolved Sollds:Total 70300_
®
mg/L
pH (Lab) 00403
units
TOC oosao ` 3 mg/L
Chloride oosao mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
Specific Conductance 000s5_
µMhos
Total Ammonia ooeto
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
TKN as N 00625
mg/L
For Remedlation Systems Only (Attach Lab Reports):
':10—Qp .aboratory Name:
V1 t 6� Certification No.
and colloidal concentrations.
�! _
Nitrite (NO2) as N oo615
mg/L
Pb - Lead olo51 ug/L
Nitrate (NO3) as N 00620 mg/L
Zn - Zinc 01092 mg/L
Phosphorus: Total as P 00655 mg/L
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Al - Aluminum oil oe
mg/L
Ba - Barium 01007
ug/L
Ca - Calcium oogis
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe- Iron 01045
ug/L
method
(Specify test and method #. TTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? (1) ❑ No (0)
K - Potassium 00937
mg/L
VOC 7873 method #cSrj�1 caca_
Mg - Magnesium 00927
mg/L
method #
Mn - Manganese olo55
ug/L
method #
NI - Nickel 01067
ug/L
method #
Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name:
Permit Name (If d
Facility Address.
Contact Person: �CC
Well Location/Site Name:
SUBMIT FORM ON YELLOW PAPER ONLY
3arly or Type
11 VC
S ck-d-
S County
-aq3 -3�3l�
of wells to be sampled:
^!.1211
S r jQ'+' , .VRrIN {Ii l�lcl�IICbHf N,t�7 eAA+�9h f
PERMIT Number(g0gftpiration Date:
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
I -Lagoon ❑ Remediation: Infiltration Gallery
Dray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
onrvir�nvta nvrvretutr t rvty _,(1� '' ``\\
WELL ID NUMBER (from Permit): \' �w '—�
Date sample collected: `� " — O
FIELD ANALYSES:
If WELL
WAS
r
Well Depth: 1 s ft.
Well Diameter: In.
pH oogooS,S units
Temp. 000io: °C
DRY at
Depth to Water Level 8254e:!26 1�� ft. below measuring point
Screened Interval: ft. to ft.
Spec. Cond. 00094:
µMhos
time of
Measuring Point Is ft. above land surface
Relative M.P. Elevation: ft. ^
Odor 000e5: O fAQ.
sampling,
check
Volume of water pumped/balled before sampling: _gallons
Appearance
W
here:
Samples for metals were collected unfiltered: 0 YES ❑ NO
and field acidified: N YES ❑ NO
LABORATORY INFORMATION -
Date sample analyzed: - `� $�
-
0 -aQLaboratory Name: EAU\
coe.�ne.�
Certification No.
PARAMETERS NOTE: Values sh uid reflect d1sigolved and colloidal concentrations.
COD oo335 _
mg/L
Nitrite (NO2) as N oo615
mg/L
Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 '�
/100ml-
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Issolved Sollds:Total 70300_
mg/L
Al -Aluminum o1105
mg/L
pH (Lab) 00403 _
units
Be - Barlum 01007
ug/L
TOC ooelo _
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug1L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #"LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? fN Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia ooelo mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
mg/L
NI - Nickel 010e7
ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facllity Name:
Permit Name (if d
Facility Address:
act Person:
Locatlon/Site Name: (V
S _ T, —
or
County
ilephone#: l 0- 3w 3
No. of wells to be sampled:_
PERMIT Number0j-�004f6q/expiration Date:
Non -Discharge UIC
NPDES Other
_ TYPE OF PERMITTED OPERATION BEING MONITORED
- agoon ❑ Remediatlon: Infiltration Gallery
Spray Field ❑ Remedlation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
�cv naryneiM i w�V
NU WELL ID MBER (from
jI11
Date sample collected: llO�
FIELD ANALYSES:
If WELL
`Permit):
Well Depth: 1 ft.
Well Diameter: 21" In.
pH 0040015i►l units Temp. 000io: eC
WAS
DRY at
Depth to Water Level 82545: �. Q; ft. below measuring point
Screened Interval: ft. to ft.
Spec. Cond. 00094: µMhos
time of
Measuring Point Is _ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085:
sampling,
Volume of water pumped/bailed before sampling: 1 6—gallons
Appearance
check
Sam les for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ® YES ❑ NO
I la!' 1t2ATnDV IRICr10e11AT1nn1 ♦ _
O'6
here:
Date sample analyzed: fj fj-t
PARAMETERS NOTE: Values sifould reflect
COD 00335 mg/L
Collform: MF Fecal 31616 ,�/100mL
Coliform: MF Total 31504 /100mL
(Note: Use MPN method for high turbid samples)
solved Sollds:Total 70300 mg/L
pH (Lab) 00403_ _units
TOG oosao mg/L
Chloride oosao �L 5Q� mg/L
Arsenic 01002 ug/L
Grease and Oils 00552 mg/L
Phenol 32730 ug/L
Sulfate 00945 mg/L
;cific Conductance 00065 _ µMhos
Total Ammonia oosio _ mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia N�, Tota )
TKN as N 00625
mg/L
For Remedlation Systems Only (Attach Lab Reports):
q- Laboratory Name:
) ry
��\
Certification No._
d and colloidal concentrations.
Nitrite (NO2) as N oo615
mg/L
Pb - Lead olo5i ug/L
Nitrate (NO3) as N 00620 ! mg/L
Zn - Zinc 01092 mg/L
Phosphorus: Total as P 00555 Q,_mg/L
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Al -Aluminum oilo5
mg/L
Be - Barlum 01007
ug/L
Ca - Calcium oosio
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron 01045
ug/L
(Specify test and method #.,ATTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? V Yes (1) ❑ No (0)
K - Potassium 00937
mg/L
VOC 7873 method #aAO a
Mg - Magnesium 00927
mg/L
method #
Mn - Manganese olo55
ug/L
method #
NI - Nickel 01067
ug/L
method #
Influent Total VOCs: mg/L
Effluent Total VOCs:
mg/L
VOC Removal%
ip-invironmental Chemists, Inc.
Go ^� °I 4 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab = 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
SHighway, Jacksonville, NC 28540 910.347.5$43 Lab/Fax J 255-A Wilmington
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Dec 02, 2020
Post Office Box 856 Customer PO M
Warsaw NC 28398 Customer ID: 08110011
Attention: Amy Elmore Report #: 2020-19581
Project ID: AG Protein
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-49840 Site: MW-1 11/17/2020 12:00 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Tan/Turbid
11/17/2020
Depth to water, ft.
Depth to Water, Ft.
5.7 feet
11/17/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
11/20/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
11/17/2020
Odor
Qualitative
None
11/17/2020
Total Dissolved Solids (TDS)
SM 2540 c
72 mg/L
11 /18/2020
Temperature
SM 2550 B
21.5 C
11/17/2020
Chloride
SM 4500 Cl E
< 5 mg/L
11/24/2020
pH
SM 4500 H B
4.9 units
11 /17/2020
Total Phosphorus
SM 4500 P F
4.70 mg/L
11/24/2020
Total Organic Carbon (TOC)
SM 5310 B
2.7 mg/L
11/17/2020
1, 1, 1,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1,1-Trichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1,2,2-Tetrachloroethane
SM 62008
<0.5 pg/L
11/24/2020
1,1,2-Trichloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
11124/2020
1,1-Dichloroethene
SM 6200B
<0.5lig/L
11/24/2020
1,1-Dichioropropene
SM 6200B
<0.5 pg/L
11/24/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2,3-Trichloropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2,4-Trimethylbenzene
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dibromoethane
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dichloroethane
SM 6200B
<0.5pg/L
11/24/2020
Report #:: 2020-19581 Page 1 of 12
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 = 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info@environmentalchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO M
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report M 2020-19581
Project ID: AG Protein
1,2-Dichloropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5pg/L
11/24/2020
1,3-Dichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
1,3-Dichloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,4-Dichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
2,2-Dichloropropane
SM 62008
<0.5 pg/L
11/24/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
11/24/2020
4-Chlorotoluene
SM 6200E
<0.5 pg/L
11/24/2020
Benzene
SM 6200B
<0.5 pg/L
11/24/2020
Bromobenzene
SM 52008
<0.5 pg/L
11/24/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
11/24/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
11/24/2020
Bromoform
SM 62006
<0.5 pg/L
11/24/2020
Bromomethane
SM 6200B
<0.5 pg/L
11/24/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
11/24/2020
Chlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
Chloroethane
SM 6200B
<0.5 pg/L
11/24/2020
Chloroform
SM 6200B
<0.5 pg/L
11/24/2020
Chloromethane
SM 6200B
<0.5 pg/L
11/24/2020
cis-1,2-Dichloroethene
SM 6200B
<0.5pg/L
11/24/2020
cis- 1, 3-Dichloropropene
SM 62006
<0.5pg/L
11/24/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
11/24/2020
Dibromomethane
SM 62006
<0.5 pg/L
11/24/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
11/24/2020
Ethylbenzene
SM 62008
<0.5 pg/L
11/24/2020
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
11/24/2020
Isopropylbenzene
SM 6200B
<0.5pg/L
11/2412020
M+P Xylene
SM 62006
<1.0 pg/L
11/24/2020
Methylene chloride
SM 6200B
<0.5 pg/L
11/24/2020
Naphthalene
SM 6200B
<0.5 pg/L
11/24/2020
Report #1 : 2020-19581
Page 2 of 12
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
info@environmentalchemists.com
Smithfield Hog Productions - Warsaw
Post Office Box 856
Warsaw NC 28398
Attention: Amy Elmore
n-Butylbenzene
SM 62008
n-Propylbenzene
SM 6200B
ortho-Xylene
SM 6200B
p-Isopropyltoluene
SM 62008
sec -Butyl benzene
SM 6200B
Styrene
SM 5200B
tert-Butyl benzene
SM 6200B
Tetrachloroethene
SM 6200B
Toluene
SM 6200B
Trans-1,2-Dichloroethene
SM 6200B
Trans- 1,3-dichloropropene
SM62DOB
Trichloroethene
SM 6200B
Trichlorofluoromethane
SM 6200B
Vinyl chloride
SM 5200B
Fecal Coliform
SM 9222D MF
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
Nitrate+Nitrite-Nitrogen
EPA 353.2
Nitrate Nitrogen
Subtraction Method
Date of Report: Dec 02, 2020
Customer PO #:
Customer ID: 08110011
Report #: 2020-19581
Project ID: AG Protein
<0.5 pg/L
11/24/2020
<0.5pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5pg/L
11/24/2020
<0.5pg/L
11/2412020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/24/2020
<0.5 pg/L
11/2412020
<0. 5 pg/L
11/24/2020
<1 Colonies/100ml-
11/17/2020
< 0.02 mg/L
2.61 mg/L
2.61 mg/L
11 /18/2020
11/24/2020
11/25/2020
Report #:: 2020-19581 Page 3 of 12
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab , 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ., 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
infoCa environmentalchemists.com
Smithfield Flog Productions - Warsaw Date of Report: Dec 02, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Amy Elmore Report #: 2020-19581
Project ID: AG Protein
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-49841 Site: MW-2 11/17/2020 12:15 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
White/Tan
11/17/2020
Depth to water, ft.
Depth to water, Ft.
11.4 feet
11 /17/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
11/20/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
11/17/2020
Odor
Qualitative
None
11/17/2020
Total Dissolved Solids (TDS)
SM 2540 C
140 mg/L
11/18/2020
Temperature
SM 2550 B
16.7 C
11/17/2020
Chloride
SM 4500 Cl E
6 mg/L
11/24/2020
,pH
SM 4500 H B
4.8 units
11/17/2020
Total Phosphorus
SM 4500 P F
0.73 mg/L
11/24/2020
Total Organic Carbon (TOC)
SM 5310 B
1.3 mg/L
11/17/2020
1,1,1,2-Tetrach loroethane
SM 6200B
<0.5 pg/L
11/24/2020
1, 1, 1 -Trichloroetha ne
SM 6200B
<0.5 pg/L
11/24/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1-Dichloroethene
SM 6200B
<0.5pg/L
11/24/2020
1,1-Dichloropropene
SM62008
<0.5pg/L
11/24/2020
1,2, 3-Trichlorobenzene
SM 6200B
<0. 5 pg/L
11/24/2020
1, 2, 3-Trich loropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
1,2,4-Trimethylbenzene
sM62008
<0.5pg/L
11/24/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dibromoethane
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dichlorobenzene
SM62o08
<0.5pg/L
11/24/2020
1,2-Dichloroethane
SM 6200B
<0.5pg/L
11/24/2020
Report # � 2020-19581 Page 4 of 12
c�ct 0 co G IaIIn
ANALYTICAL & CONSULTING CHEMISTS
finvir®nmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 1 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info@environmentalchemists_com
Smithfield Hog Productions -Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
1,2-Dichloropropane
SM 6200B
<0.5pg/L
11/2412020
1,3,5-Trimethylbenzene
SM 6200B
<0.5pg/L
11/24/2020
1,3-Dichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,3-Dichloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,4-Dichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
2,2-Dichloropropane
SM 5200B
<0.5 pg/L
11/24/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
11/24/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
11/24/2020
Benzene
SM 6200B
<0.5 pg/L
11/24/2020
Bromobenzene
SM 6200B
<0.5 pg/L
11/24/2020
Bromochioromethane
SM 6200B
<0.5 pg/L
11/24/2020
Bromodichloromethane
SM 62008
<0.5 pg/L
11/24/2020
Bromoform
SM 5200B
<0.5 pg/L
11/24/2020
Bromomethane
SM 62008
<0.5 pg/L
11/24/2020
Carbon tetrachloride
SM 6200B
<0.5 pg/L
11124/2020
Chlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
Chloroethane
SM 6200B
<0.5 pg/L
11/24/2020
Chloroform
SM 6200B
<0.5 pg/L
11/24/2020
Chloromethane
SM 62006
<0.5 pg/L
11/24/2020
cis- 1,2-Dichloroethene
SM 62008
<0.5pg/L
11/24/2020
cis- 1,3-Dichloropropene
SM 6200B
<0.5 pg/L
11/24/2020
Dibromochloromethane
SM 62008
<0.5 pg/L
11/24/2020
Dibromomethane
SM 6200B
<0.5 pg/L
11/24/2020
Dichlorodifiuoromethane
SM 6200B
<0.5pg/L
11/24/2020
Ethylbenzene
SM 5200B
<0.5 pg/L
11/24/2020
Hexachlorobutadiene
SM 6200B
<0.5pg/L
11/24/2020
Isopropylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
M+P Xylene
SM 62008
<1.O pg/L
11/24/2020
Methylene chloride
SM 6200B
<0.5 pg/L
11/24/2020
Naphthalene
SM 6200B
<0.5 pg/L
11/24/2020
Report #:: 2020-19581
Page 5 of 12
ANALYTICAL & CONSULTING CHEMISTS
-Environmental a issg Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info@environmentalchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
n-Butylbenzene
SM 6200s
<0.5 pg/L
11/24/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
11/2412020
p-Isopropyltoluene
SM 6200B
<0.5pg/L
11/24/2020
sec -Butyl benzene
SM 6200B
<0.5 pg/L
11/2412020
Styrene
SM 6200B
<0.5 pg/L
11/24/2020
tert-Butyl benzene
SM 620as
<0.5 pg/L
11/24/2020
Tetrachloroethene
SM 6200B
<0.5 pg/L
11/2412020
Toluene
SM 6200B
<0.5 pg/L
11/24/2020
Trans-1 ,2-Dichloroethene
SM 6200s
<0.5 pg/L
11/24/2020
Trans-1,3-dichloropropene
SM62008
<0.5pg/L
11/24/2020
Tiichooroethene
SM 6200B
<0.5 pg/L
11/24/2020
Trichlorofluoromethane
SM 6200s
<0.5 pg/L
11/24/2020
Vinyl chloride
SM 6200s
<0.5 pg/L
11/24/2020
Fecal Coliform
SM 9222D MF
<1 Colonies/100ml-
11/17/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/18/2020
Nitrate+Nitrite-Nitrogen EPA 353.2 16.4 mg/L 11/24/2020
Nitrate Nitrogen Subtraction Method 16.4 mg/L 11/25/2020
Report #:: 2020-19581 Page 6 of 12
Environmental Chemists, Inc.
1 1 3 9 e 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab = 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
sM, 255-A Wilmington Highway, Jacksonville, NC 28540 _ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Dec 02, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Amy Elmore Report #: 2020-19581
Project ID: AG Protein
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-49842 Site: MW-3 11/17/2020 12:30 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
Tan/Brown
11/17/2020
Depth to water, ft.
Depth to water, Ft.
6.6 feet
11/17/2020
Ammonia Nitrogen
EPA 350.1
1.6 mg/L
11 /20/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
11/17/2020
Odor
Qualitative
None
11/17/2020
Total Dissolved Solids (TDS)
SM 2540 c
134 mg/L
11/18/2020
Temperature
SM 2550 B
21.2 C
11/17/2020
Chloride
SM 4500 Cl E
6 mg/L
11/24/2020
pH
SM 4500 H B
5.5 units
11/17/2020
Total Phosphorus
SM 4500 P F
3.13 mg/L
11/24/2020
Total Organic Carbon (TOC)
SM 5310 B
34.0 mg/L
11/17/2020
1, 1, 1,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1, 1, 1 -Trichloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1,2-Trichloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1-Dichloroethane
SM 6200B
<0.5pg/L
11/24/2020
1,1-Dichloroethene
SM 6200B
<0.5pg/L
11/24/2020
1,1-Dichloropropene
SM 6200B
<0.5pg/L
11/24/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
1,2,3-Trichloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,2,4-Trichlorobenzene
SM 6200B
<0.5 µg/L
11/24/2020
1,2,4-Trimethylbenzene
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dibromoethane
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dichloroethane
SM62008
<0.5pg/L
11/24/2020
Report #:: 2D20-19581 Page 7 of 12
Environmental Chemists, Inc®
(R 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
G�� �) J
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
SM, 255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Smithfield Hog Productions -Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
1,2-Dichloropropane
sM 5200B
<0.5 pg/L
11 /24/2020
1,3,5-Trimethylbenzene
sM 62008
<0.5 pg/L
11/24/2020
1,3-Dichlorobenzene
sM6200B
<0.5pg/L
11/24/2020
1,3-Dichloropropane
sM6200B
<0.5pg/L
11/24/2020
1,4-Dichlorobenzene
sM 62008
<0.5 pg/L
11/24/2020
2,2-Dichloropropane
sM6200B
<0.5pg/L
11/24/2020
2-Chlorotoluene
sM 6200a
<0.5 pg/L
11/24/2020
4-Chlorotoluene
sM 6200B
<0.5 pg/L
11/24/2020
Benzene
sM 6200a
<0.5 pg/L
11/24/2020
Bromobenzene
sM 6200B
<0.5 pg/L
11/24/2020
Bromochloromethane
sM 6200a
<0,5 pg/L
11/24/2020
Bromodichloromethane
sM 6200B
<0.5 pg/L
11/24/2020
Bromoform
sM 6200a
<0.5 pg/L
11/24/2020
Bromomethane
sM 62008
<0.5 pg/L
11/24/2020
Carbon tetrachloride
sM 6200a
<0.5 pg/L
11/24/2020
Chlorobenzene
sM 6200B
<0.5 pg/L
11/24/2020
Chioroethane
sM 6200a
<0.5 pg/L
11/24/2020
Chloroform
sM 6200B
<0.5 pg/L
11/24/2020
Chloromethane
sM 6200a
<0.5 pg/L
11/24/2020
cis- 1,2-Dichloroethene
sM6200B
<0.5pg/L
11/24/2020
cis-1,3-Dichloropropene
sM62009
<0.5pg/L
11/24/2020
Dibromochloromethane
sM 6200B
<0.5 pg/L
11/24/2020
Dibromomethane
sM 6200a
<0.5 pg/L
11/24/2020
Dichlorodifluoromethane
sM 6200a
<0.5 pg/L
11/24/2020
Ethylbenzene
sM 6200B
<0.5 pg/L
11/24/2020
Hexachlorobutadiene
sM 62008
<0.5 pg/L
11/24/2020
Isopropylbenzene
SM 6200a
<0.5 pg/L
11/24/2020
M+P Xylene
sM 6200a
<1.0 pg/L
11/24/2020
Methylene chloride
sM6200B
<0.5pg/L
11/24/2020
Naphthalene
sM6200B
<0.5pg/L
11/24/2020
Report #:: 2020-19581
Page 8 of 12
�M I
ANALYTICAL & CONSULTING CHEMISTS
1-13
milivironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info@environmentalcliemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
n-Butylbenzene
SM 62008
<0.5 pg/L
11/24/2020
n-Propylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
ortho-Xylene
SM 6200B
<0.5 pg/L
11/24/2020
p-Isopropyltoluene
SM 62008
<0.5pg/L
11/24/2020
sec -Butyl benzene
SM 62008
<0.5 pg/L
11/24/2020
Styrene
SM 6200B
<0.5 pg/L
11/24/2020
tert-Butylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
Tetrachloroethene
SM 6200B
<0.5pg/L
11/24/2020
Toluene
SM 62008
<0.5 pg/L
11/24/2020
Trans-1,2-Dichloroethene
SM 6200B
<0.5 pg/L
11/24/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5pg/L
11/24/2020
Trichloroethene
SM 6200B
<0.5 pg/L
11/24/2020
Trichlorofluoromethane
SM 6200B
<0.5pg/L
11/24/2020
Vinyl chloride
SM 6200B
<0.5 pg/L
11/24/2020
Fecal Coliform
SM 9222D MF
33 Colonies/100ml-
11/17/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
0.04mg/L
11/18/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
0.95mg/L
11/24/2020
Nitrate Nitrogen
Subtraction Method
0.91 mg/L
11/25/2020
Report #:: 2020-19581 Page 9 of 12
Environmental Cheists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com
Smithfield Hog Productions -Warsaw Date of Report: Dec 02, 2020
Post Office Box 856 Customer PO M
Warsaw NC 28398 Customer ID: 08110011
Attention: Amy Elmore Report M 2020-19581
Project ID: AG Protein
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-49843 Site: MW-4 11/17/2020 12:50 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
Tan/Brown
11/17/2020
Depth to water, ft.
Depth to Water, Ft.
1.6 feet
11/17/2020
Ammonia Nitrogen
EPA350.1
< 0.2 mg/L
11/20/2020
Gallons bailed before sampling
Gallons Bailed before sampling
10 gallons
11/17/2020
Odor
Qualitative
Sulfur
11/17/2020
Total Dissolved Solids (TDS)
SM 2540 c
123 mg/L
11 /18/2020
Temperature
SM 2550 B
19.3 C
11/17/2020
Chloride
SM 4500 Cl E
20 mg/L
11/24/2020
pH
SM 4500 H B
5.8 units
11/17/2020
Total Phosphorus
SM 4500 P F
1.22 mg/L
11/24/2020
Total Organic Carbon (TOC)
SM 5310 B
0.8 mg/L
11/17/2020
1, 1, 1,2-Tetrachloroethane
SM 6200E
<0.5 pg/L
11/24/2020
1, 1, 1 -Trichloroethane
SM 62006
<0.5 pg/L
11/24/2020
1,1,2,2-Tetrachloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1,2-Trichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1,1-Dichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
1, 1 -Dichloroethene
SM 6200B
<0.5 pg/L
11 /24/2020
1,1-Dichloropropene
SM 6200B
<0.5pg/L
11/24/2020
1,2,3-Trichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2,3-Trichloropropane
SM 6200B
<0.5 pg/L
11/24/2020
1,2,4-Trichlorobenzene
SM62008
<0.5pg/L
11/24/2020
1, 2,4-Trimethyl benzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dibromo-3-Chloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,2-Dibromoethane
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,2-Dichloroethane
SM 6200B
<0.5 pg/L
11/24/2020
Report # : 2020-19561 Page 10 of 12
_ $M
ANALYTICAL & CONSULTING CHEMISTS
ID
Environmentale ists9Inca
6602 Windmill Way, Wilmington, NC 28405 = 910.392.0223 Lab 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 , 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info@environmentalchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
1,2-Dichloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,3,5-Trimethylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
1,3-Dichlorobenzene
SM 6200B
<0.5pg/L
11/24/2020
1,3-Dichloropropane
SM 6200B
<0.5pg/L
11/24/2020
1,4-Dichlorobenzene
SM 6200B
<0.5 pg/L
11/24/2020
2,2-Dichloropropane
SM 6200B
<0.5 pg/L
11/24/2020
2-Chlorotoluene
SM 6200B
<0.5 pg/L
11/24/2020
4-Chlorotoluene
SM 6200B
<0.5 pg/L
11/24/2020
Benzene
SM 6200B
<0.5 pg/L
11/24/2020
Bromobenzene
SM 6200B
<0.5 pg/L
11/24/2020
Bromochloromethane
SM 6200B
<0.5 pg/L
11/24/2020
Bromodichloromethane
SM 6200B
<0.5 pg/L
11/24/2020
Bromoform
SM 62006
<0.5 pg/L
11/24/2020
Bromomethane
SM 62008
<0.5 pg/L
11/24/2020
Carbon tetrachloride
SM 62008
<0.5 pg/L
11/24/2020
Chlorobenzene
SM 6200E
<0.5 pg/L
11/24/2020
Chloroethane
SM 5200B
<0.5 pg/L
11/24/2020
Chloroform
SM 6200B
<0.5 pg/L
11/24/2020
Chloromethane
SM 6200E
<0.5 pg/L
11/24/2020
cis- 1,2-Dichloroethene
SM 6200B
<0.5pg/L
11/24/2020
cis- 1,3-Dichloropropene
SM 6200B
<0.5pg/L
11/24/2020
Dibromochloromethane
SM 6200B
<0.5 pg/L
11 /24/2020
Dibromomethane
SM 6200B
<0.5 pg/L
11/24/2020
Dichlorodifluoromethane
SM 6200B
<0.5 pg/L
11/24/2020
Ethylbenzene
SM 6200B
<0.5 pg/L
11/24/2020
Hexachlorobutadiene
SM 6200B
<0.5 pg/L
11/24/2020
Isopropylbenzene
SM 6200B
<0.5pg/L
11/24/2020
M+P Xylene
SM 6200B
<1.0 pg/L
11/24/2020
Methylene chloride
SM 6200B
<0.5 pg/L
11/24/2020
Naphthalene
SM 6200B
<0.5 pg/L
11/24/2020
Report #:: 2020-19581
Page 11 of 12
,; sM
ANALYTICAL & CONSULTING CHEMISTS
EnvironmentalChemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
inro@environmentaIchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 02, 2020
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention: Amy Elmore
Report #: 2020-19581
Project ID: AG Protein
n-Butylbenzene
SM 6200E
<0.5 µg/L
11/24/2020
n-Propylbenzene
SM 6200B
<0.5 µg/L
11/24/2020
ortho-Xylene
SM 6200B
<0.5 µg/L
11/24/2020
p-Isopropyltoluene
SM 6200B
<0.5µg/L
11/24/2020
sec-Butylbenzene
SM 62006
<0.5 µg/L
11/24/2020
Styrene
SM 6200B
<0.5 µg/L
11/24/2020
tert-B utyl benzene
SM 62008
<0.5 µg/L
11/24/2020
Tetrachloroethene
SM 6200B
<0.5 µg/L
11/24/2020
Toluene
SM 6200B
<0.5 µg/L
1112412020
Trans-1,2-Dichloroethene
SM 6200B
<0.5µg/L
11/24/2020
Trans-1,3-dichloropropene
SM 6200B
<0.5µg/L
11/24/2020
Trichloroethene
SM 6200B
<0.5 µg/L
11/24/2020
Trichiorofluoromethane
SM 6200B
<0.5 µg/L
11/24/2020
Vinyl chloride
SM 6200B
<0.5 µg/L
11/24/2020
Fecal Coliform
SM9222DMF
<1 Colonies/100ml-
11/17/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 0.02 mg/L 11/18/2020
Nitrate+Nitrite-Nitrogen EPA353.2 1.21 mg/L 11/24/2020
Nitrate Nitrogen Subtraction Method 1.19 mg/L 11/25/2020
Comment:
Reviewed by:
Report #:: 2020-19581 Page 12 of 12
Date: jAX
Anal%st-
Certification A! 9a
Facilih Name: A ,Ira
Permit9. 0'a 00V%Srj0
Reference Method SSI4500 H-B -201 1 Instrument [D 6,4,
Calibration Time Cal Buffer 4 0 s u Cal Buffer 10 0 s u Check Buffer 7.0 s u Comments
'pH check buffer must read % tthin = 0 1 pH units of the buffer's true value
4 su buffer Lot,' Ricca 2001 B20 Exp 1/2022 7 su buffer Lot=.: Ricca 2009993 Exn, 7,2022 10 su buffer Lot-7 Ricca 1001791 7-2021
Sam re I,3cation Sample Collection
p
Sample Analysis
pH Result IdPost-analysis Buffer
I Comments DataQualiFers
f Time•
Time
s u Check values u
M w�—
�-
/[ S7.
/LrL
I S•��
► Post analysis buffer check is required «hen performing analyses at multiple sampling locations and must be within = 0 1 unitss of the buffer's true value
A11 pH values in pH un±ts (i e , s u ) Record all data to the nearest 0 DI s u and report to the nearest 0 1 s u
Total Residual Chlorine (TRC)
Reference Method SM 450o Cl-G201 1. Flach 8167 HR ( Please circle aritilicable Method Instrument ID
Post -anal) sis
Dail} Chock Time check Sample Sampi�
Check Sid Sample TRC Result
Standard Result Standard Location Collection Analysis Q Comments Data Qualifier,
eL or mg L (when anahzin� Anahzed µ> L ormg'L
µ` at multiple sites) Time Timz7
TRC Daily Check Standard true talus µgfL or mg11, acceptance range or mg'L
Check standards must recover %v ithin _l0°, u of the check standards true value
Annual Calibration Curve Verification Date: LOT# Exp. Date
Reagent Blank Value. When applicable Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
Reference Method S:`4 4500 0 G: 2u:1 1 Instrument ID
• Post -anal} sis calibration I
Calibraunn Calibration variable Meter reading %enfication (when necessan )
Ventica ion or °o efficiency Comments
Time Barometne a ftercalibration Theoretical Calculated
Temperature pressure Value me L Value meL
I I I I Use this rove %then performing a %erincation instead of
calibration
Sample Location Sample Collection 'Sample Analysis DO reading
P Time Time ma L Comments Data Qualifiers
• When performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed
` [f sample is measured directly inthe stream and or onsite. only time anal} zed could be recorded with a nore that they are measured in situ or immediately
Temperature
Reference Method Ski 2550 B-2010 Instrument ID.
Sample 'Sample Temperature
Sample Location Collection Anaysis I °C CommentsData Qualifiers
Time Time
/!A V t I .s %% e_ 1 /. S
3 L I, it.
` If sample is measured d;rec j m the stream and or on site, only time anahzed would be recorded. with a note that the% are measured in situ or immediate!}
Annual Venfication Date )&w�
Field Personnel Note: Q k.001
Rev 9-2020
Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client�`L l`" ] Eu�) Date: Report Number:
f
Receipt of sample: ECHEM Pickupt Client Delivery ❑ UPS [7 Far1F rn nthor r'1
❑ YES
❑
NO
N/A
1. Were custody seals present on the cooler?
YES
[O'riginal
❑
NO
N/A
2. If custody seals were present, were they intact/unbroken?
temperature upon receipt _.__�—°C Corrected temperature upon receipt C.
How temperature taken:
❑ Temperature Blank tj Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
10
NO
3.
If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
I ❑
NO
4.
Were proper custody procedures (relinquished/received) followed?
YES
113
NO
5.
Were sample ID's listed on the COC?
YES
❑
NO
6.
Were samples ID's listed on sample containers?
YES
❑
NO
7.
Were collection date and time listed on the COC?
YES
❑
NO
8.
Were tests to be performed listed on the COC?
IR YES
❑
NO
c?
nirl camnlcc 7rrivo in nr- r ..t ; F L. � �a l
[X YES
10
NO
110. Did samples arrive in good condition for each test?
YES
10
NO
111. Was adequate sample volume available?'
LV YES
10
NO
112. Were samples received within proper holding time for requested tests?
YES
❑
NO
113. Were acid preserved samples received at a pH of <2?
YES
10
NO
114, Were cyanide samples received at a pH >12?
O YES
10
NO
15. Were sulfide samples received at a pH >9?
YES
ID
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
19 YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
10
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 NCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
_ ENVIRONMENTAL CHEMISTS, INC OFFI E:9101392-02 3f1FAX910392-44245
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Ag Protein (Magnolia,NC)
REPORT NO: 1� - i,
ADDRESS:
CONTACT NAME:
Permit Number: W00040918
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO: Amy Elmore
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
-' w
E h
m a
E° C!
ct7
o
c
° E
"
�W
m
g z
PRESERVATION
ANALYSIS REQUESTED
t
Time
Temp
i
$
u
_
H
o
y
0
z
o
w
c
9
MW:
ro f�
tL�J
C
P
9�� cj
X
Chloride, NO2,TDS,
G
G
B
Depth to water:
C
P
�'
X
INH3,NO3,Total P
G
G
Gallons bailed: { ®
C
P
X
TOC
G
G
H field): �•
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
X
VOC's November only)
G
G
Color: 4A j ¢d,
C
P
G
G
Odor: sij .L_
C
P
G
G
C
P
G
G
C
P
G
G,
Total of 4 wells due march, july, november: MW1,2,3,4. Site located on Bonham Road, Magnolia, NC.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
,®
Temperature when Received °C: Accepted: Rejected: Resample a ested:
Delivered By: Received By: Date: '/ 1 h Time:
Comments: T R AROUND:
y
Way
ton
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910i1392-02 3'IFAX9910'392-44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Ag Protein Magnolia,NC)
REPORT NO: 0 — 06(3 %
ADDRESS:
CONTACT NAME:
-
Permit Number: W00040918
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO: Amy Elmore
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludge. Other:
Sample IdentificationE
Collection
y
w
E o
`o
'"
`o m
" E
inz
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
oz
J
x
o
"_
0
0
Z
0
o
MW
X
Chloride, NOUDS,
G
G
Depth to water: j lt
C
P
X
Z
INH3,NO3,Total P
G
G
Gallons bailed: f
C
P
X
TOC
G
G
pH (field): -
C
P
X
Fecal Coliform
G
G
De to water:
C
P
VOC's (November only)
G
HX
G
Color. �• ,.,
C
P
G
G
Odor: A j o„e.
C
P
G
G
C
P
G
G
C
P
G
G
Total of 4 wells due march, july, november:
MW1,2,3,4.
Site located on Bonham Road, Magnolia, NC.
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
i emNeratUre when mecelvea -c: _ Accepted: v Reje ted: Resattap�e R quested:
Delivered By: FGC-E Received By: P� Date: 1-1 12Z Time:
Comments: TURNAROUND:
ll Way
on, NC
ndm
EE � �e� ENVIRONMENTAL CHEMISTS' INC OFFICE: 9 0,392-0223'IFAX 910392-44245
Analytical &Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Ag Protein (Magnolia,NC)
REPORT NO: ZO — f
ADDRESS:
CONTACT NAME:
Permit Number: W00040918
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO: Amy Elmore
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil. SL = Sludge. Other:
Sample Identification
Collection
d d
~
�
a a
E `o
cf7
3 `o
c J
`o E
t
"
CW
m
g Z
PRESERVATION
ANALYSIS REQUESTED
D to
Time
Tempa
z m
$
u
_
o
m
_
h
°
=
x
o
z
G
W
x
MW.
Lf• L
C
P
X
Chloride, NOUDS,
G
G
Depth to water: 9� •�
C
P
X
L"
NH3,NO3,Total P
G
G
Gallons bailed: / d
C
P
X
TOC
G
G
H (field):
C
P
X
I Fecal Coliform
G
G
Depth to water:
C
P
X
VOC's (November only)
G
G
Color: 4w. u (®,J
C
P
G
G
Odor: W'k
C
P
G
G
C
P
G
G
C
P
G
G
Total of 4 wells due march, july, november:
MW1,2,3,4.
Site located on Bonham Road, Magnolia, NC.
Transfer
Relinquished By:
DatelTime
Received By:
Date/Time
1.
2.
I emperature When Received -G: Accepted: L-� R 'ected: Resampl Requested:
Delivered By: Received By:_ Date: —MY? 1 Time:
Comments: TURNAROUND:
E4E1#:k:)
Analytical & Consulting Chemists
Client: Smithfield Hog Production -Warsaw
ADDRESS:
�Sampled By:
Sample Identification
MW: y
Depth to water:
Gallons bailed: t a
PH (field): S• �1
Depth to water:
�_
Color: !' 6(�r
Odor: S-41-W
otal of 4 wells due
Transfer
1
INC 6602WindmillWayWilmington,NC28405 ENVIRONMENTAL CHEMISTS
OFFICE: 910-392-0223 FAX 910-392-4424
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: Ag Protein (Ma nolia,NC) REPORT NO: CD0
CONTACT NAME: Permit Number: WQ0040918
REPORT TO: Kraig Westerbeek PHONE/FAX:
COPY TO: Amy Elmore email:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO =
ollection
W PRESERVATION
a °
m F E° 0 c° .2 E Q M o � 0 o 0 0 T
Time Temp v, u ° u .I Z = = s i Z F-
0
3 c G G � S� X
Chloride
C P
november: MWI,2,3,4. Site located on Bonham Road, Magnolia, NC.
Relinquished By:
Date[Time Ave
Temperature when Received °C: Accepted:
Delivered By: Received By:
Comments:
SL = Sludge, Other:
ANALYSIS REQUESTED
TDS
Resam a Requested:
Date :I 1 2 Time:
TURNAROUND:
Date/Time