NC0000272_Analytical Fecal Coliform Date per Request_20180101

WWTP Laboratory Workaheet Date:
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec EffI Low Lift Prim EffI Sec Eff I Low Lift Prim EffI Sec Eff I Prim Infl AS / PE Sec Effl 5 Minute D g9C7 So 85
Time Collected �SS/ 41 -'S1 7&0/. 0lp o�ss)° �`�" �os-'P /o="P /DAP ° // 30 Minute ao .5"/c� ySo Go
�� r7 .- I g0a� j.3 S �;� ��6 ,rib SVI 30
Collected By: ��. C� �'��
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 ecycle Sludge Solids
Time Analyzed: /�°f' LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp• Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m s 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: :5 Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID '
Put Up By: JdAf Filter ID 3yg #1 AS #2 #3 #31D Std.900to1100 STD BLK SPK Ft+Slds gms o3(- G 91 Xx
Weighed By: UO6 Filter + solids - gms " q o o1/ Sec Eff z/ / ,toYB Ft Tare gms , jl90 / frz8
Calculated By: Filter Tare - gms 4 o q s, I&S foq6 674 s- /, lay Avg. ppm oSo TSS do/5 /O7 /093
Checked By: QC TSS ppm jx2 Z9z x2 ySy 1G 3 /5 8 /5 $ (x2) qS,2 -o.oaor (/s) TSS (x4) yOG.a 1 y3A, I #m
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. VXV V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim Eff I Sec Effl Prim Infl Prim Effl Sec Eff I Sample Volume =25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms i / 6 3 Time Collected:
Filter+ solids - gms J3g8 /, !/o?� A / 05a hQ51 , o?yoZ Al2x2
394 N7 o Filter Tare - gms a Sample pH (Adjusted)
Filter Tare - gms ;3 /. /o6 Alc>3 �, /O /. 4/o71 /,i /, Total Susp. Solids S'7/ Bkup Sample pH (Adj)
Total Suspnd. Solids x2 3 SS /2 /D x2 3�$ (o GSo G! /2 g Total Susp.Solids(x4) Ia eq v501 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant UC-As Analyzed By: �,�•
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 5 •�S An��r� �.�S �{-� �,. 122 Sow Q•C•
Crucible + Solids . q,2 9. 905 g, S Verification 1000 umho std S \S t1\ �\ ,S ��S 123 1000,2000,5000+/-10%
Crucible Tare /$ o Verification 14.9 umho std \cj 2\, \ 124 14.9 std.(5.1 to 40.7)
9, 8 n
Solids S$ (y g v47 Canton \0�.� t"1r ,�,, ��- ,S 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS 3 �o o�y � XG71 ,tSo/ Fiberville \�'-35 Ah �02 285 Cell Constant 4.75 to 5.25
Crucible +Ash �'/(�3 SS 13 G szl Sec. Effluent \O', O `��\ , \Q� 125 1,000,2,000,&5,000 Stds
Ash g 5 Sec Eff Dup \O', KE h Z` '\ , \�S\ 126 are purchased.
3 yv v48 Sec Eff Avg �,,� .`j \�� 286 14.9 std. Made from
ppm Non-Volatile sc
M LVSS ,ZZ14 Z0,99iMid Range 2nd Source FOR 2000 umho std \\'• 2tJ�\ q � 132 the 1,000 std.
%Volatile go7.q BG,y z
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier Cl 47
Feet/Minute 1
#5 Clarifier I YAS 8 2
r#6—Clarifier 3

WWTP Laboratory Worksheet Date: 1,,1[�\R G- D 2 8
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: &W Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: Jj6 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 50 150 200 250 /pillow
Initial D.O. By: Jig Bottle Init.D.oppm got F,10 g ?, F. X� 8: 86.3 •7
5 Day D.O. By No. 5DayD.O.ppm 3X 71 ,76 /y LIg, v 1$� . l oL �� a.� �9 �, ye 57 �f 9a s`� y�!8 �� . 5�3 7.� �`8 / /Xs . �o 262 r /y'
Time Analyzed: sue' Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Fiitrate
Date Analyzed:, ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: Bottle Init.D.Oppm 8,0 8./ 8;/0 1 8o2 Too$ • 31 SL r.Z f. ' XX
Checked By: QC. No. 5DayD.O.pm 17 1 9-1/ 3. 15 ll 5:6 qSo V 7Z -/, syH56 -,!r 2� Z7$
. �
S. y8
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: af 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: ZrD L Z 8 8;/ 7 AM 3,� 3 . 3 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl 179 8,S'
Preserved pH: 4 S A/.,30 11 AM 1 PM G
Checked By: T 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 11st 8hr 2nd 8hr 3rd 8hr
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: 5
d
(24 Hour Composites) 2nd Source Verification std Time: s%' Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: //W Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMA�g PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec. Eff 500 Blank
Checked By: -r Sample pH o,/ z.Z 7• 8:a 7 2 /o Z.X 12
pH(24 Hour Composites) Adjusted Color pH 7 ev 74 71(_0 74-0 SE Avg •G 7.6 7.4 7.4 Z 4 7,ro
Analyzed By: U•'D` Analysis ppm 1 XV7 8'89 y9y zof 1.ro J45� e zoY /71 1rS- /d 9 7 rZ8
Calculated By: O'DL X Factor I
Analyzed By: r Sample ppm 91 287 88'9 f9N 10Y Zra Ns 1f a /� •ro 3.o 20 7 In 164 F28 /"/ % o
Checked By: p1r Variable No. 62 63 67 1 64 324 329 22/65 23/66 171 172 173 1 174 37 103 108 141 144 355 1 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I . 5 63 o.S`J o.s r The Analyst's Initials On This Worksheet Certify That
Sample Source Spike S/N 1455680 All Stds+/- 10% P-std mg/I /03 ,0 Orr The Analyst Has Done The Test To His/Her Ability
Sample pH ✓#9011 Hi_color_Juty2017 S.E. Dup Diff<2.6mg/L New Pump setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr 4SEProcess Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: -XD4 g,Dv and use
je
X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected: 10� 1D�°
Sample ppm #9017 Hlcolor July2017 Time Analyzed: 11—"f 11tV //,W Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 I I I I Analyzed By: rbv BDv 6AV Time 700 A 300 P T5 Avg
[Master QC Signature: rf, By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: rT, ft Pri. Effl 0 d T6 Avg

WWTP Laboratory Worksheet Date: 1 p e �t s
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec Effl Low Lift Prim EffI Sec Effl Low Lift Prim EffI . Sec EffI Prim Infl AS/ P.E Sec Effl 5 Minute 178 d 7V O n 0 6
Time Collected (ss G$s/�1 eo S ssjo 3 Y' /b�P ate' o;�` 30 Minute O �/ y7o y3
Collected By: �L ��- .5� o� �P° Ulf ��� =��� �!S SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 ® 79 80 Recycle Sludge Solids
Time Analyzed: LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 81-Ir 2nd - 8Hr 3rd - 8Hr
Time Out: Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: .1i6 Filter ID boo #1 AS #2 #3 #313 Std.900to1100 STD BLK SPK Ft+Slds gms , /S, O ,1
Weighed By: jj C Filter + solids - gms 3yz 1 41.1161 /s- /.o ,iioz Sec Eff A I s- ,/es-3 Ft Tare gms /, 0807 /, 10 5/
Calculated By: JJg Filter Tare - gms A jf soon zso ' i o 1 4 Aptal Avg. ppm j S s TSS /0a?(0 ° y8 14s
Checked By:f1"QC TSS ppm x2 35 x2 59.Z dg o /5 /5 g (x2; 9.'® l�s, TSS (x4) y/0V 4(/9a zIt
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. 41/4 V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec EffI Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms 43.5 Time Collected:
Filter + solids - gms /3,S(, l l0$02 �. // 4r 3G 8 /o?0-5 �• /��"� zG z /zoa Filter Tare - gms /OS Sample pH (Adjusted)
Filter Tare - gms /, "1 , /0 a A 111; 5 /088 11-50 /,10 /, Total Susp. Solids 113kup Sample pH (Adj)
Total Suspnd. Solids x2 'r$y 5', /2 /0 x2 60 ,5_5- /2 '� x2 0 53 /2 f8 Total Susp.Solids(x4) 3/ oL V50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant A3 Analyzed By: S.
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Va 2 Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 5 y �® h 2�� � 12 S� Q.C.
Crucible + Solids /�. $'�/O , y8> !$,7o3S Verification 1000 umho std S M 123 1000,2000,5000+/-10%
Crucible Tare $ o t, ya S 8,G 96 Verification 14.9 umho std \0 \MMM\ ��.�j �..� .Cj 124 14.9 std. (5.1 to 40.7)
Solids Go$ G3 639 v47 Canton ,Q . S� A\"� 6 .2 ��}. 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS q3 X o153� zssG �SoB Fiberville `�'.V) K ` .�,, ,� 285 Cell Constant 4.75 to 5.25
Crucible +Ash q S/ I siz Sec. Effluent V0�• 35 Ate �.. �' \°�4''"\ 125 1,000,2,000,&5,000 stds
Ash qs Sec Eff Dup �Q��cJ �� 2°� ,�" � �� 126 are purchased.
ppm Non-Volatile 380 3$ e4. v48 Sec Eff Avg M 2 ,� `� 286 14.9 std. Made from
M LVSS O5a a 159 Zo9.Z .2 099 Mid Range 2nd Source FOR 2000 umho std Z.SS , \ 2.2.E `�e 132 the 1,000 std.
Volatile 41, q PI,P
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier 9 -/ 8 z $ Feet/Minute 1
#5 Clarifier 7 7� 7� 2
#6 Clarifier A -- 3

UTP Laboratory Worksheet Date: ?"I
VW C4
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: y Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: Jwjif ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpi 5 3 5 50 150 200 250 /pillow
Initial D.O. By: JJ6 Bottle 11nitD.0ppm Faz B.oG �1 8ov Z3 Fox ZS >?0 5G t o/ �q 0,0 e� 8/0 9� �3' /So yt /S'� �
5 Day D.O. By JJ6 No. WayD.D.ppm 3 ? 2 y� 3 ffb 3,/8 0,3 S.00 S.yY - - 40 - -- ?,�.� _ Z<3� S.gt 33'
Time Analyzed: Jy Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Litt Sec Effluent - Sec Effluent SecEff Dup /61 SeCEff Filtrate
Date Analyzed: 3 s-111 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl _ 5 5 3 4 30 100 200 300
Calculated By: .1j6 Bottle InitD.Oppm 8,02 8oS 8.0/ ' 80� 800 r,02 802 T%7 8y
Checked B QC. No. SDayD.O.ppm 9 zZ Zy ?
S8 41 �Y 114 /sS 2Se.
y: � 3A z4y .�9s ,?3s' ssy y 98 ss3 Y. ��� 707 s67 G, /G
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: //ttv? 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3- Time SFT SFT 200 Seed/6mL Spk
Preserved By: 3",DG 8,os' 7 AM 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl z83 8s'o
Preserved pH: /,S
,�g�' 11 AM 1 PM S,lD
Checked By: P 1' 13 PM 15 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 j 1 st 8hr 2nd 8hr I 3rd 8hr
L 3.-
Color 100ml prepared sample Laboratory Control Std Mid Range Spectfo Photometric Time: °AM
(24 Hour Composites) 2nd Source Verificationstd Time: Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: J/1T Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriC{Eff Aerinf LL Acid Swr Sec.Eff. 5OO Blank
Checked By: t'" Sample pH /0.3 X.0 Ici 71 73 T,T ?Y 16,-T X.a 7°19
pH(24 Hour Composites) Adjusted Color pH 7,G 7 e. T& ^7.Le SE Avg 7.4 7,6 7,G 7,6 G 7,r..o
Analyzed By: 704 Analysis ppm 93 z 7 g92 Y94 x/S .Z7' /6q /�H z1/ 17d !S7 Zoos Tilt �' 7
Calculated By: 4 X Factor / r
Analyzed By: T01- Sample ppm 93 Z87 899 4194 z!S 7 /g` /6`f / `� /� Z 11/ �7d �S 29005 RMX 4P
Checked By: Variable No. 1 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141. 144 1 , 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg. NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/1 S , y� p ,T p 38 The Analyst's initials On This Worksheet Certify That
Sample Source Spike S/N 1455680 All Stds +/- 10% P-std mg/I �,0 I oa o The Analyst Has Done The Test To His/Her Ability
Sample pH #9017 Hi Color-July2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE jProcess Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: ZrD4, T9P Wf and use
X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected: /41y-r D
Sample ppm #9017 Hi_Color_JuW017 Time Analyzed: //'OW Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 jAnalyzed By: jT P 7it P Time 700 A 300 P T5 Avg
Master QC Signature: T' By signing this I verify that all QC parameters have been checked COD pH initial. final IChecked By: rT, rf f T JPri. Effl 0 T6 Avg

WWTP Laboratory Worksheet Date: MAR 1 1 2018
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd -8Hr 3rd - 8Hr Average
LowqLiftP-rim EffI Sec Effl Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec EffI Prim Infl AS/ PE Sec Effl 5 Minute 8-70Time Collected �f: QD Ste'p ass' �j°b !� : /o 4 /0 /O s-/ . /1.. lI°=i // f' 30 MinuteCollected ry: � �i J J i3 JJ �S SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 .76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: j! fo.r LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: oZ!°f} Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID /, oZtw
Put Up By: JJ B Filter ID 314,36 s� #1 AS #2 #3 #3D std.soocol loo STD BILK SPK Ft+Slds gms , /0yv / a L6 1. 07141
Weighed'By: JJ S Filter + solids - gms !/, S/„3 ,$$ , / ® /•S3 / Sec Eff , /6 ,/oSa? Ft Tare gms //8 /. j`//
Calculated By: jj 13 Filter Tare - gms oZ I /. job /. q /. /099 /. 6778 /. /067 Avg. ppm 1,, 1141 , /051 TSS 06O )77 loo?6 _
Checked By: QC TSS ppm x2 854/ x2 / jq co /5 /0 /5 C1 /0 (.2) 10$6 . CTov (is) TSS (x4) ,? v y3/G Z/080
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim Effl Sec EffI Prim Infl Prim Effl Sec EffI Sample Volume=25ml AOX Wkly Comp. Sec Eff
SampleCollected By:
Size - ml 50 100 200 50 100 200 50 100 200 Sample ID y:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms Time Collected:
Filter + solids - gms / j �0 !O 0 /� / / a 8✓! p� /49 . / 9a Filter Tare - gms /, f J %8 Sample pH (Adjusted)
Filter Tare - gms D /0 7 /. 041 A /. /o G G /8 / .383 . /0,58 A P a7 /. $� Total Susp. Solids �/,$ Bkup Sample pH (Adj)
Total Suspnd. Solids jx2 15114. 47 /2 <R x2 / ,Zo .5 y /2 /D x2 4q�_ 1/2 G Total Susp.Solids(x4) 171t.y6p 0 V50 Nitric Acid to obtain ph<2
Conductivity
Test Method: Std Methods 2510-B Cell Constant 1-INS Analyzed By: 'S . .
Mixed Liquor Solids
Sample Temp °
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled C Sample umho/cm Va cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std S .\� t 2�"IL\R 122SUZ Q•C•
Crucible + Solids 140 y . 70 12 Verification 1000 umho std `� �� 2�. 1� 123 1000,2000,5000+/-10%
Crucible Tare 19, , $ ,1039 Verification 14.9 umho std '. �O .� �..�.� 124 14.9 std. (5.1 to 40.7)
Solids (� qp? (� vl7 Canton W. 30 A� 284 S.E. Dup Diff. <8.4 umho
Soli = MLSS �/72 0 25oc> a�/ 93 Fiberville W. h `.� ��„'J ,�j 285 Cell Constant 4.75 to 5.25
Crucible +Ash G�7 / , aZo1 8. �S�oZ� Sec. Effluent k�'•CYJ N 2°�� ���� 125 1,000,2,000,&5,000 stds
Ash /O p /d$ Sec Eff Dup W. �� 2°` . \ ���3 126 are purchased.
ppm Non-Volatile a C/a$ 3,� v48 Sec Eff Avg C Z� . Wo 132 14.9 std. Made from
M LVSS p l/ aO$Q O�p 8 a Otp y Mid Range 2nd Source FOR 2000 umho std �.�• �.J 4� 2� 132 the 1,000 std.
Volatile
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 p 1100 P 3°° A Time A B C D
#4 Clarifier Cl9 q g Feet/Minute 1
#5 Clarifier 7 , 7/ 2
----- 3
#6 Clarifier `

WWTP Laboratory Worksheet Date: �9,°,JR I I
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: �° SampleSourceNar.No. lank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: S513 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smp1 5
3 5 50 150 200 250 /pillow
Initial D.O. By: '3J)'33 Bottle Init.D.Oppm 8•/3 8 1 ? CQQ ,„ `C7 08
1g / -3 , 63
5 Day D.O. By W No. MayD.O.pp. / D 1; 5..7
Time Analyzed:d: s sample sDDrceNar.ND. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: 3 ,w ;F m! Sample 0 30 Seed/6 Std 30 Seed/3Smp1 5 l 5 Q 3Q 4 30 / 100 20©0 30Q0 ry
Calculated B Bottle Ini4D.0 ppm �• I �•+ . 1 S C'J .0 . / �� g I jJ C7 'a3 '� f� �• � C7 � �� �9 ' !
y q aa3 ohs •�� 5,5 ` 0 �� 33 a?sy �,j` +7S �
Checked By: QC. No. 5DeyD.0.ppm `� G �/. 3 ° t�
Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Ammonia 200 Seed/6mL S k
Time Preserved: /
�a 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT p
7 AIVI � 2. 2:� 3. 9 AM � 10 Seed/03 Smpl 10 Seed/0.5 Smpl �� •S 7
Preserved By: SDI- ) g• PM
Preserved pH: 1. S ! / 11 AM
Checked By: r
3PM 5PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0A Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1 st 8hr I 2nd 8hr I 3rd 8hr
1.0 Sy p3 /y3
loom)prepared sample Laboratory Control Std Mid Range Spectro Photometric Time:
Color p p `
OR
(24 Hour Composites)
2nd Source Verification std Time: 5 ,� Time: True Filtered Apparent(Unfiltemd) Std E E
Time Analyzed:1 P,A Sample Source 100ppm 300ppm 900ppm 50oppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff 5OO Blank
Sam le H 9•1 z•2 "?• -7. q 7- p•1 � Z � 7.9
Checked By: p p
1-(0 �•` •� ••7 SE Avg �. �•(/ I.(OP �/ 7.
pH(24 Hour Composites)— Adjusted Color pH ?Z 5"7 S—XIO d00
Analyzed By: ) 1.- Analysis ppm lfo3 /$1 5/
Calculated By: p!' X Factor /
B : Sample ppm 92 Z�� 89a 49? ` AN - /fs3 /S t5! l51 51 •S fib /72 / ?.�1 5'74i D Ln
Analyzed y �DL p
checked By: Variable No. 62, 63 67 64 324 329 22/65 23/66ww� , 171 172 173 174 37 103 108 141 144 355 357 164 87 17
Nitrate Color
Colon`Calibration Curve Dates Phosphate 1st 2nd 3rd Avg' NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I . '�O , yS ` ,yS The Analyst's Initials On This Worksheet Certify That
Sample Source Spike ✓ -lacJSM1 DR All Stds +/- 10% P-std mg/I ,oa .D /,p The Analyst Has Done The Test To His/Her Ability
Sample pH
#9017 Hi_Color JUW017 { S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo.Color Hach#125 Test Method: NCASI 253. pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: JaLt° �i� and use
X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: le6K I0%°PA. 6A
Sample ppm
#9017 FIi_Color JDyzo17 Time Analyzed: ''°Puy %°t o 110,T fA't Sulfide 1st 2nd Eff Avg
Analyzed By: �.� � Time 700 A 3 00 P T5 Avg
Variable No. 180 Lo Color Hach#125 -E IT6 AvMaster QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: �'>1' Pri. Effl Q Ug

P
VWNTP Laboratory Worksheet Date: MAR 2 2018
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd -8Hr 3rd - 8Hr Average
Low Lift Prim Eff I Sec EffI Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute 1706 Rya
Time Collected ¢O �40 �Yt y ?� ps'� A) Ss / r°� / /0� /1°(� 30 Minute '.
Collected By: � SR� SVI30
(24 Hour Composites)
Total Suspended Solids std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike lsmp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd -8Hr
Time Out: of Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: Cgeo Filter ID -011-9897 #1 AS #2 #3 #3D std.9ooto1100 STD BLK SPK Ft+Slds gms 8S /.z/.tS 1.58
Weighed By: Filter + solids -gms f. f f, ! /at ,.3 f. D D /• /0 Sec Eff f. /� /� p 7a Ft Tare gms f 079 ioss7
Calculated By: Filter Tare - gms 3$6 4 /0/3 /, 12,59 4 log 8 4 D'y8 f o '7�S Avg. ppm , / ,5'S' /� 0'10 TSS /09z /068 ��9
Checked By:Pr QC TSS ppm x2 7a x2 /ov 3 ,3 /5 S /5 (x2> f�f! , o$oa Us1 TSS (x4) y.U8 yt7z -d1036
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. /f0?0?$ V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim EffI Sec Effl Prim Infl Prim Eff I Sec EffI Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms �, Py Time Collected:
Filter + solids - gms yp I.Io75 J, ja 9 1./ s /. / .3 f. / 3 , //A Filter Tare - gms 10e,I Sample pH (Adjusted) /:5
Filter Tare - gms 4 / 0 /./o y9 /o3 /. // //G 1. 1011S 1133. • / 6C) Total Susp. Solids 516 Bkup Sample pH (Adj) /.
Total Suspnd. Solids x2 fg?g 39 /2 5 x2 5az 39 /2 5 jx2 13,34 1 yv /2 oq ITotal Susp.Solids(x4) z3yy v501 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant t Analyzed By: ,>Oj/
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1
2 3 Calibration 5000 umho std zz-, y 122 5C�06 Q.C.
Crucible + Solids v,� ' �" 123 1000,2000,5000+/-10%
17. T c -Z . y876 B. Verification 1000 umho std . 0U ,� ) 7
Crucible Tare /'7 g// ,Zh g24S /8.6M/2 Verification 14.9 umho std j; Z,/, 124 14.9 std. (5.1 to 40.7)
Solids S G�3 /1 v47 Canton ' ,C> Z,S, 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS qq 238 Fiberville TO RV; 51, 7 t. 1 285 Cell Constant 4.75 to 5.25
Crucible + Ash i?,9207 ,Z! /8. So3 Sec. Effluent ;rig ,4 Z-7. J Z 125 1,000,2,000,&5,000 stds
Ash ,� / Sec Eff Dup �t 1(� ',�; � '7� � 126 are purchased.
ppm Non-Volatile 3� 3� v48 Sec Eff Avg �";t o / 27.� j Z L� 2s6 14.9 std. Made from
M LVSS / 9z zo 8 a o80 AaV5 IMidRange 2nd Source FOR 2000 umho std to:zo Al �r , i' 132 the 1,000 std.
Volatile 83. 7 &'3 s
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 11°°A 3°° P 7°° P 11°° P 3°°A Time A B C D
$ 8 z 2 Feet/Minute 1
#4 Clarifier 9
#5 Clarifier ? 7
i / -7 2
#6 Clarifier i — 3

WWTP Laboratory Worksheet Date: MAR iz zoit
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: 10/to Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: mi Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 50 150 200 250 /pillow
Initial D.O. By: Bottle [InILD.0ppm ,o .CD g,v_3 8 .0 � ,03 8 07 g•o� /O G. 8 . !�, (3.5 Day D.O. By No. ayD.O.pgn J 3 7. `�S l 3•�`d $ . 5� °? < .a5 7. 7
Time Analyzed: �,' p Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: g f7 ie ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 : . 100 200 300
Calculated By: �- Bottle InitD.Oppm �D •0(0 8.Q3 8.03. •o3, Orj g,UG S. I 9•3o g•a
Checked By. QC. No. 5DayD.O.pWn l�87. �� y�� a� 3.�� �� .�3 �� s;5 ,3 s. �� L� � �w Ill ��� %-r . Z/ 70 �5' . a
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: // a`o 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: �' j� I— 12.Cq 7 AM Z 9 AM 10 Seed/0.3 Smpl - 10 Seed/0.5 Smpl v
Preserved pH: ). $ ! 11 AM 1 PM p2
_J
Checked By: �' 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
/z 7 / S�
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time:
(24 Hour Composites) 2nd Source Verification std Time: j'""° Time: True Filtered Apparent(unfiltered) Std FOR FOR
Time Analyzed: /' Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: ft Sample pH Z. `1 .q
pH(24 Hour Composites) Adjusted Color pH � I,& ILL _7 Co SE Avg 7. (, 7. 6 7 ( -7-�, 76
Analyzed By: �L_ Analysis ppm /ZZ /10 / / ,1 /&57 625— Z&3
Calculated By: L_ X Factor
Analyzed By: J),)_ Sample ppm ve Is- z 1,76 /31 13 /3 16'6
Checked By: JVariable No. 62 1 63 67 64 324 329 22/65 1 23/66 171 172 173 1 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd JAv NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/l 0.3G o.;y 01 The Analyst's Initials On This Worksheet Certify That
Sample Source Spike SIN 1455680 All Stds +/- 10% P-std mg/I e 9 ,0_3 The Analyst Has Done The Test To His/Her Ability
Sample pH #9017Hi_ColorJuy2017 S.E. Dup Diff<2.6mg/L New Pump setting .C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swrrocess Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: P nd use
X Factor SIN 1505038 PI New True:NCASI 71.01 Time Collected:
Sample ppm #9017 Hi Color Juy2017 1 L Time Analyzed: /C" /��p J�-S.P Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: •-5V-10 J_RP �V-P Time 700 A 300 P T5 Avg
Master QC Signature: fOf By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl A:r T6 Avg