NC0000272_Analytical Fecal Coliform Date per Request_20180101 (3)

WWTP Laboratory Worksheet Date: MAR 0 5 R I F
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd -8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute 5b 680
Time Collected i 4� ` ' o (o`s r �.� Js to o� to -FrIe /&* /�o f'' / �v /tom/ 30 Minute 3 n
Collected By: c_ v� �� J f^ �-- �� �i3 SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: /2S,a LL VSS Low Lift Acd Swer Pr EffluentSec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd -8Hr
Time Out: j ot�f4 Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: "/ Filter ID , Z171-5 #1 AS #2 # #31) Std.900to1100 STD BLK SPK Ft+Slds gms �//7
Weighed By: Filter + solids - gms J, � % /, f : � /, 8� /, /, % Sec Eff l /� �(j p/"� Ft Tare gms J, s /, i/�
Calculated By:, " Filter Tare - gms a&o , . Avg. pprn TSS l S /06y
Checked By: QC TSS ppm lx2 p x2 r,y1 ;y 8 /5 /5 `7 L; (x2) /G�57y 0 V5) TSS (x4)
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. J J V52
Prim Infl Prim Effl Sec Effl Prim Infl Prim Eff I Sec Effl Prim Infl Prim Effl Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids -gms / 6Z Time Collected:
Filter + solids - gms -73 /, /l 2 77 / 1,�3 ' /o y(9 Filter Tare -gms /, �a2 Sample pH (Adjusted)
Filter Tare - gms / I, 167-7 1. /D a,7 , ja /, I/g; /, 3zr<j . /O7& 4, �; /1$8 Total Susp. Solids � Bkup Sample pH (Adj)
Total Suspnd. Solids jx2 p /2 1,-2_ x2 /2 /3 x2 Say© 1 /1_3 /2 S Total Susp.Solids(x4) v50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant 3 Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 69r-14 122 Q.C.
Crucible + Solids q,qz5 18. 7(),' 3 Verification 1000 umho std 44WIlIL 123 1000,2000,5000+/-10%
Crucible Tare I q re.e.8 27 Verification 14.9 umho std 124 14.9 std. (5.1 to 40.7)
Solids CQ �o/ v47 Canton / 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS Fiberviile /0 �, /' 285 Cell Constant 4.75 to 5.25
Crucible +Ash j�q c 5 $, Sec. Effluent 36. 125 1,000,2,000,&5,000 Stds
Ash 1� p$ Sec Eff Dup '�(). 126 are purchased.
ppm Non-Volatile S j(�d q3X 08 Sec Eff Avg `30 16o7 286 14.9 std. Made from
M LVSS J Q ©( Mid Range 2nd Source FOR 2000 umho std �� Z0. �z 132 the 1,000 std.
% Volatile 1 30, 9,1,0
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier Q -1 99 Feet/Minute 1
#5 Clarifier � ' z— 2
#6 Clarifier 3

WWTP Laboratory Worksheet Date: MAR 0 5 201
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: /. O Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30�Sjeed/5SmpI 5 3 5 50 _ 150 200 250 /piiiaw
Initial D.O. By: 3 Bottle Int.D.Oppm l� .CCU �%C 7 ` � ,G % J`7 � �— ,c/ ' 9,G�7
5 Day D.O. By J No. SDayD.O.ppm / ?, 8� 7 3.Z3 X. l s. /... 11,57 ?30 c� lJ S.oo 7 ';
Time Analyzed: 41 V Sample Source/Var.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: JJB 1 Bottle InitD.O ppm �5. 7r q8 yC� ,o '`' � ' j r Ct� 61' 3.� 1
Checked By: QC: No. MayD.O.ppm 8y 3.75 3.07 8 8'9 �l; 7,6l 8y 8
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: /� %� 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: ' i 7, 1S 7 AM Z,3 9 AM 10 Seed/0.3 Smpl 10 seed/0.5 Smpl el"1r), �
Preserved pH: /. 5 3.SG 11 AM 1 PM y,og
Checked By: P 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
13(3
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: 5°i-
(24 Hour Composites) 2nd Source Verification std Time: $' "i Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: 3 Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMA�g PE Turb Pr Eff PdCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: Sample pH /d.D o73 -7 6 7. (,, .Y .S 7.S- D AL 7. �,
pH(24 Hour Composites) Adjusted Color pH -7.(0 74, '.6 SE Avg (� 76 7,4o .('
Analyzed By: P Analysis ppm / i3/ 131 /9/ 1441 /33 57,27 &197 9
Calculated By: f�r, X Factor
Analyzed By: i2o, Sample ppm 7 191 ALP 71 142 .3% /21 i.s'i /9/ 44 33 `"7 "7 1 1% Ja
Checked By: Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I , / The Analyst's Initials On This Worksheet Certify That
Sample Source Spike /' S/N 1455680 All Stds +/- 10% P-std mg/I The Analyst Has Done The Test To His/Her Ability
Sample pH r #9017 Hi-Color July2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm JHach DR 3900 All Except PI New True Collected By: and use
X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected:
Sample ppm #9017 Hi-Color July1017 Time Analyzed: /#' tf Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: Time 700 A 300 P T5 Avg
Master QC Signature: p4r By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl T6 Avg

VWVTP Laboratory Worksheet Date: MAR G 6 �tiYs;
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec Effl Low Lift Prim EffI Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute 5 0 ���
Time Collected `� <�5 �� "SS 30 Minute
Collected By: r� tj ^✓, Tc�' c, 7 / 1— S? �� SVI 30
(24 Hour Composites)
Total Suspended Solids, Std Methods.2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp bup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 81-Ir 3rd - 8Hr
Time Out: > , } Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: Filter ID , '1165 #1 AS #2 #3 #3D Std.900to1100 STD BLK SPK Ft+Slds gms / 193 , 9/G3 E,
g 7® �; d //,5� D H� C7 Sec Eff / C�.�t� Ft Tare gms /,OBI d /I l 3
Weighed By: Filter + solids - ms 1 11,
Calculated By:, F— h Filter Tare - gms q78 D to 7C Avg. ppm )0159 TSS
Checked By: QC P'j' TSS ppm x2 q�r- x2 /5 / /5 (X2) O.S - Uzi/ u5) TSS (x4) �IqS- '
Total Suspended Solids 1st - 8 hr. Comp. 2nd -8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. ��IQO V52
Prim Infl Prim Effl Sec Effl Prim Infl Prim Eff I Sec Effl Prim Infl Prim Effl Sec Effl Sample volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter+ Solids - gms /, 171Y1 Time Collected:
Filter+ solids - gms 17 /a0 7 1/6a �• l$ �o Filter Tare - gms Sample pH (Adjusted)
Filter Tare -gms ; D9 g(o /, %03 /, %�� 93 /5& %. //y� Total Susp. Solids q Bkup Sample pH (Adj)
Total Suspnd. Solids x2 -7-1 /2 x2 S /2 x2 /7yd 5 3 /2 !y Total Susp.Solids(x4) 7 v50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd -.8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std �, �c�L- 122 '�000 Q.C.
Crucible + Solids 77 S/ 18, 10q3Verification 1000 umho std j. "s 123 1000,2000,5000+/-10%
Crucible Tare 7, g 1 21,113U 1, (y tp Verification 14.9 umho std v ).. 124 14.9 std. (5.1 to 40.7)
SOIIdS / V47 Canton 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS & 3�� �SS Fibervilie f �� / 285 Cell Constant 4.75 to 5.25
Crucible +Ash W q 654414 Sec. Effluent ]` 125 1,000,2,000,&5,000 Stds
Ash I X3 /4/3 Sec Eff Dup Xril ,Q �"� 126 are purchased.
ppm Non-Volatile 33,-�-- '7 v48 Sec Eff Avg �' % ' 286 114.9 std. Made from
M LVSS A09 w Cab 3 Mid Range 2nd Source FOR 2000 umho std l �. / 132 the 1,000 std.
Volatile 7 -7
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier 9 17 1 Feet/Minute 1
#5 Clarifier —' '—` ` 2
#6 Clarifier �—` —� -- 3

MUP Laboratory Worksheet Date: P11AIl, Cy 6 A'
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate See Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: 3 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed!5Smpl 5 3 5 50 `" 150 200 256 /pillow
Initial D.O. By: Bottle Ink.D.Oppm ��X ,, 3 /� . / // ' A
�E/ q ,� ' 1 go As C �� i 3 5
5 Da D.O. By No. WayD.O.ppm 7 `l q -3. 70 �!' /l ,,P �/ �` _3r 5 t ' G• 1 . ��
Y 5
Time Analyze sa 10 Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEfif Filtrate
Date Analyzed:.3-/l/8 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: Bottle IniLD.Opp�n tv. 8 , / .� ® e- -3
QC: �3 I �. 50 3 �` 7 °� � 3.5 �. �3 1�,� �•g � '� �6�
Checked By: f t NO. SDayD.O.�m ,o
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: 1 rS 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: Z-7 7 AM c ,& 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl . '? 41
Preserved pH: /,S l �f. /`/ 11 AM 1 PM ,
Checked By: 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
/S3 3
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time:
(24 Hour Composites) 2nd Source Verification std Time: Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: Sample pH /17 21 74 97 #7
pH(24 Hour Composites) Adjusted Color pH 7& .4o '-1 1l•C T6 -A SE Avg 1'
Analyzed By: Analysis ppm 16 �O �� 11� I##a / 1 /07 AIWI 963 3
Calculated By: X Factor f I / /' I k
Analyzed By: Sample ppm 94 v9 890 497 164 Q k\1 kk3 /16 139 /o f -&3- 1-'45 W17 S
Checked By: FT Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike JHach DR 3900 Color Q.C. Sec Eff P mg/I 3 3 , 30 ,33 The Analyst's Initials On This Worksheet Certify That
Sample Source Spike S/N 1455680 All Stds+/- 10% P-std mg/I ,D3 1.60 The Analyst Has Done The Test To His/Her Ability
Sample pH #9017 Hf_ColorJuly2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: '-WB and use
X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected. p /
Sample ppm #9017 Hi ColorJuly2017 Time Analyzed: ' _ /Ar j1� Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: SP Time 700 A 300 P T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl T6 Avg

VWUTP Laboratory Worksheet Date: V1AR G 7 2�Vn it 9
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 81-ir Average
Low Lift Prim EffI Sec Effl Low Lift Prim EffI Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute 50 41:50 (a
Time Collected j�$0 (� p GS5 4i s� �. s� F. �ss �3 5� 3s F ac ` , a` . 30 Minute �� 3�� �
Collected By: J(,, DM 7� c; Try+ I7w� fit- b✓ `-I.j 71 SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: J'!s 4 LL VSS " Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp V01=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: 5° / Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: 7 u) Filter ID 3q 3611/ #1 AS #2 #3 #3D std.9ooto11oo STD BLK SPK Ft+Slds gms /, a 3
Weighed By: i"i,•J Filter + solids - gms 3 q. 3qa% 1, 2aO . /3 O 5 /. 0 g'/ 1 j Sec Eff % /6-; /,/) Ft Tare gms / a Yq /, /gq 1, 113
Calculated By: Filter Tare - gms . �a� /a s" , 1 CIS 1 b77q 10-73 Avg. ppm f, 1152 /, /0&-3 TSS /aa JS
Checked By: c > 05/- 0,0,-Vo (is) TSS (x4)
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. �/-27 S V52
Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec Effl Prim Infl Prim EffI Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter+ Solids -gms X 4/3 Time Collected:
Filter + solids - gms SS I. 1/3 /, 2, /, ,9N & , %/qV Filter Tare - gms /�o Sample pH (Adjusted)
Filter Tare -gms ]x2
2� /0T/ 1. 1042 ; / z Y7 3? /. /00' l /, //?hi Total Susp. Solids I/0 Bkup Sample pH (Adj)
Total Suspnd. Solids L/S2 S /2 °I x2 /2 x2 7yz /2 Total Susp.Solids(x4) 2 Iqo v50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant ,3 Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std � � -Z: ��� 122 Q.C.
Crucible + Solids Ll 17.2940 ,?0.�3 Verification 1000 umho std e7-7.� 123 1000,2000,5000+/-10%
Crucible Tare 'g, 76661q, g S5 Ik 6 42 q Verification 14.9 umho stdA 22d� 72. 124 14.9 std. (5.1 to 40.7)
Solids (�3Z =,� ? 5"�j 07 Canton 284 S.E. Dup Diff. <8.4umho
(x4) = MLSS $-�9 3-6-0, 9�2� Fiberville ,/ � � -3Z!5�k 285 Cell Constant 4.75 to 5.25
Crucible +Ash ,��a/ gs�3 (� 9 Sec. Effluent Zo(40 125 1,000,2,000,&5,000 Stds
Ash < p Sec Eff Dup �ZZ-OO 126 are purchased.
ppm Non-Volatile q32 v48 Sec Eff Avg 286 14.9 std. Made from
M LVSS 9 3 6 3 Mid Range 2nd Source FOR 2000 umho std 132 the 1,000 std.
Volatile G q
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier 9 17 Feet/Minute 1
#5 Clarifier 2
#6 Clarifier 3

WWTP Laboratory Worksheet Date: MAR G 7 --19
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: 1140 P Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: TWI ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpi 5 f 3 5 50/ �7 150 200 250 /pillow
Initial D.O. By: I Bottle InILD.OpPm �� r .�� �� ^ �.� ��� �j I� i 57� � L ,'c 1 ��� /J�
5 Day D.O. By so NO. SDeyD.O.VW� 3� S 1 3.9a o,,$8 D �f. 8 .,?a. 6 •ooz 7, 5 l.�� V. �'S4 1( a
Time Analyzed. A/S Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed:;-1A,16 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: Bottle InILD.O ppm l I 15 a% I% $ "'
Checked B : rQC: No. WayD.O.ppm ?J .oS � 'q-S za 3.9� � � S 9 <g� �180 `�` IR S� .�� �• �3 / '� 3 Y ��'" 9
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: I 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6ml- Spk
Preserved By: 4, 7 AM , 2 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl z
Preserved pH: .5' �/��0 11 AM 1 PM � �
Checked By: FT 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
F ';3 q
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time:
(24 Hour Composites) 2nd Source Verification std Time: 5 s°- Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: i, Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMMg PE Turb Pr Eff PriClEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: Sample pH /0.7 0 ?' 7•a 7.4 / .`l ;.o '7, g
pH(24 Hour Composites) Adjusted Color pH 7,Cy 74, SE Avg 7 Lo 7 ,(a 7-
Analyzed By: Analysis ppm ///,o 11 15? pq7 $ 7 0 /
Calculated By: X Factor V I / / / /
Analyzed By: Sample ppm 93 g 1 84A Zl& !S /117 M? 527Ako IT& / 71 SC?7 P-
Checked By: fj— Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/1 .at) •3 ,3g 5- The Analyst's Initials On This Worksheet Certify That
Sample Source Spike S/N 1455680 All Stds +/- 10% P-std mg/I /.pS ,jJ? ,p7 The Analyst Has Done The Test To His/Her Ability
Sample pH #9017 Hi_color Juty2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: RtF�- GV, ';W and use
X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: io
io10 2
Sample ppm #9017 Hi_Color_Jul2017 Time Analyzed: I° o0 100 Sulfide 1st 2nd Eff Avg
Variable No. 180 1 1 11-o Color Hach#125 Analyzed By: 6V V I 13V Time 700 A 300 P T5 Avg
Master QC Signature: "r By signing this I verify that all QC parameters have been checked COD pH initial final lChecked By: Pri. Effl 1 0 T6 Avg

WWTP Laboratory Worksheet Date:
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec EffI Low Lift Prim Effl Sec EffI Low Lift Prim Effl Sec Eff I Prim Infl AS/ PE Sec EfflE30Minute
nute �0 off® So y
��. �� 6o S� >° o;d !os—P /Ossl°Time Collected �, ,� . . `�Collected By: 3'C p/1'1 '{� /U'� Rew jjg JuB JuB JJ8
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: //£1_9 LL VSS' Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: �W Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: J,J6 Filter ID 3525 #1 AS #2 #3 #3D Std.900to1100 STD BLK SPK Ft+Slds gms /C1 1"Z
Weighed By: JJs Filter+ solids - gms I. 12 r il IDS, INI Sec Eff ?G o y Ft Tare gms /,1121
Calculated By: JJ6 Filter Tare - gms !7S 1, 1060 / 2Vf / /.o77y /. /o� Avg ppm /,i/yo i>oy� TSS Q9� 0� oya
Checked By: QC TSS ppm x2 S-o x2 qro 70 y9 �5 �;Z �5 // /� c i 072 ro, *0o2 lis> TSS (x4) 776 9�6
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. y// V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim Effl Sec Effl Prim Infl Prim EffI Sec EffI Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter+ Solids - gms /, 16191 Time Collected:
Filter + solids - gms (* E3 Q �� l i >, zos Filter Tare - gms , /06,5 Sample pH (Adjusted)
Filter Tare - gms A-) `' ' k q0 ® -6- f /ois /,//02 ! Total Susp. Solids Bkup Sample pH (Adj)
Total Suspnd. Solids x2 (r Flo (o l2 x2 S�(� /2 l a� x2 3i2 57 �2 / Total Susp.Solids(x4) 8 v50 Nitric Acid to obtain ph<2
y Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant ` Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 122 Q.C.
Crucible + Solids 1 /g a Verification 1000 umho std /r� - lr� .� 123 1000,2000,5000+/-10%
Crucible Tare ,�'�. �72Z� 1, Y7_7t, Verification 14.9 umho std J. 2, 124 14.9 std.(5.1 to 40.7)
Solids 04QC tl& 6 ya 07 Canton / Z 3'7 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS �( SGo zSz3 Flbervllle 285 Cell Constant 4.75 to 5.25
/`f 8 Gs/8
Sec. Effluent
Crucible +Ash �(} 6/0 125 1,000,2,000,&5,000 Stds
Ash ( //q Sec Eff Dup Q � � 126 are purchased.
ppm Non-Volatile �� ® y7G v48 Sec Eff Avg �� 286 14.9 std. Made from
M LVSS � ��' 108 Z/O Mid Range 2nd Source FOR 2000 umho std � /,� 132 the 1,000 std.
Q
Volatile 8/
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier 17 9 9 Y Feet/Minute 1
#5 Clarifier 7 lk 7 i 7 7 2
#6 Clarifier — 3

WWTP Laboratory Worksheet Date: ' 2 ' i
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: 019 Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: JJ6 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 50 150 200 250 /pillow
Initial D.O. By: jje Bottle IINVD.0.ppm
nt.D.Oppm 8.0/ 8.03 $ oy S.O$ 8.o S Ot o3 0 B.Dq 14
5 Day D.O. By No. / , 9a 3. 57 ,2� e?�a o2 '�q 0.3 �I7 -(f.24 `s -.!8 �� �.8 7� 7 rf r� /3f s gO 15/ s!y .c S9 �
Time Analyzed: Sf? Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: „3-/ ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 1 3 4 30 100 200 300
Calculated By: 60 Bottle W.D.0ppm $.oy L oa 8;0 8'03 Xao Sot o /d 9 -1/4
Checked By:�[-QC: NO. SDayD.O.ppm 6 . 88 /y y,�G 2V a,(S � y'.d ( S�� y•�5' 6 �, •88 ? 3 9� /�� 7, �r iVI �, .y3 S.�� ��y s;ylO
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: //! !� 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: /� 0 7 AM , jFZ 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl z8Z
Preserved pH: g- ,3,8 7 11 AM 1 PM X
Checked By: 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
oc ,� 1
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: ° ,,.
(24 Hour Composites) 2nd Source verification std Time: Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: I.,15W Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: Sample pH 10.6 z./ ? Co -7t'_o 7. 7, /010 Z 7&
pH(24 Hour Composites) Adjusted Color pH 1 74 7,6 7(.o '7-(o SE Avg 76 7 G 76 7.4 7,C. 7 Co
Analyzed By: REL Analysis ppm 9.2 Xr7 J 9 9G Z417 Z57 31 /3;1 198 !vG /Y 1174e 441 a
Calculated By: e&l X Factor
Analyzed By: REG Sample ppm Z Z87 '�i6 V74 ZIVrr 2S7 /31 /'tea i3a /3.73 48 7yG 7Y I4GG 44r /807 Lo /
Checked By: Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I e 4 O. Yv O qo The Analyst's Initials On This worksheet Certify That
Sample Source Spike ✓ S/N 1455680 All Stds +/- 10% P-std mg/I 1, ,,C r I The Analyst Has Done The Test To His/Her Ability
Sample pH #9017 Hi Color_July2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: ,egg rpv and use
X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: /O'ro? 100*0 /042
Sample ppm #9017 Hi_Color_July2017 Time Analyzed: //,ov //:r // Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: 6D` �pv od Time 700 A 3°° P T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl Q T6 Avg