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HomeMy WebLinkAboutNC0000272_Analytical Fecal Coliform Date per Request_20180101 (2) WWTP Laboratory Worksheet ®ate: MAR 2 9 2018 Sludge Volume Index Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Low Lift Prim EffI Sec EffI Low Lift Prim EffI Sec Effl Low Lift Prim Effl Sec EffI Prim Infl AS/ PE Sec Effl 5 Minute 2,Zo 900 Ob 191 Time Collected 6 'l;W ZjV X—�° AS'/f 10"5 p D" p 00 f °s p /�5 p //°j 30 Minute IV o soo 500 Collected By: TDa TRP/C,. -VIO ;0r<p e w* jij G Tw t,) w c SVI 30 (24 Hour Composites) Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids Time Analyzed: 1 N5 + LL VSS. Low Lift `Acd Swer Pr Effluent Sec Eff Sec Eff Dp, Dup.Diff<5.1 1000Stnd Blank Spike smp vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Time Out: /45 4 Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID Put Up By: w Filter ID 30.+PI1 #1 AS #2 #3 #31D Std.900to1100 STD BLK SPK Ft+Sldsgms t / ZyIf Weighed By: 7 Filter+ solids - gIms 3 q.q 3 67 �, _ '? / /33 a. /, 1116 Z, 0 L J. //,ff Sec Eff / /,,3 /, Ft Tare gms 41011 ? l G, Calculated By: T,-,, Filter Tare - gms /0 Y 1 ;, 0 4-7 2- Avg. ppm /, /.. j 1 TSS i/gy lz-vye llqq Checked By: QC TSS ppm x2 �� x2 ^�j S 3 9� /5 S /5 ,< cx2� ,�� us1 TSS (x4) y 6 �74° Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. y?�,s V52 Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec Effl Prim Infl Prim EffI Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By: Filter ID PI PE 1A PI PE 2A PI PE 3A Filter+ Solids - gms , /z Time Collected: Filter + solids - gms y �� S ` y� / 3880 % S /, / ,7 , i Filter Tare - gms /. /1 Sample pH (Adjusted) Filter Tare - gms �, ? 4 iobo 4 /oi3 /. /oY7 /. // 73 8zs /. 11�3 5 /a 9 Total Susp. Solids 711 Bkup Sample pH (Adj) Total Suspnd. Solids x2 2258 Sy /2 32 x2 /3gG 7 /2 z8 x2 A(o51 /2 Total Susp.Solids(x4) 2876 V50 Nitric Acid to obtain ph<2 Conductivity Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant Analyzed By: C� Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity Crucible ID 1 2 3 Calibration 5000 umho std O S30 nm L4 $ SO 122 �D� Q.C• Crucible + Solids jq q 3° 11,171,77 / , 7 155 Verification 1000 umho std OS30 �)M 53 123 1000,2000,5000+/-10% Crucible Tare /4 8G 93 /9 S'/G o /T eo-VIII Verification 14.9 umho std ©1930 r-:I 124 14.9 std. (5.1 to 40.7) Solids 7y/ 7�(<, v47 Canton 0p t{ S�P M � �y .�Q K° 284 S.E. Dup Diff. <8.4 umho .25 (x4) = MLSS 9�N y8 $ `j �91'Z Fiberville © $ 5o oM � 4` 12S .L' 125 1,00Cell Constant ,00 S s Crucible +Ash / 8G q /9 pay? . (o�°7y Sec. Effluent Q�' I C) >� aq , "� 125 �,000,2,000,&5,00o stds Ash Sec Eff Dup Q /0 M q a-19 '0 126 are purchased. ppm Non-Volatile 728 V48 Sec Eff Avg Q g/O M ,a ") 9 .1 286 14.9 std. Made from M LVSS 216 212o t 1 o�f 3 S Mid Range 2nd Source FOR 2000 umho std O © (1/� ! Q c� 132 the 1,000 std. Volatile ?G,z 75:s 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities Blankets 1st - 8Hr 2nd - 8Hr Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D #4 Clarifier 8 ?t J.)$ G 7 Feet/Minute 1 #5 Clarifier 7 j4C 6, 7 2 3 #6 Clarifier I I L F WWTP Laboratory Worksheet Date: MAR 2 9 2018 BOD (24 Hour Composites) Standard Method 5210 B Time Put Up: UZ. p Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent Put Up By: 7-w' ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 - 50 150 200 250 /pillow Initial D.O. B •7/-,j Bottle IniLD.0ppm n Z a 2S'0 �,� �� 07 ?"05 Z55 ` '03 13,0s q `; v� a,05 y 7 �7 a-�a 1317? l�4 /, � 3 ys � 1118 (13 3. 38 , �3 $ /� /, rf7 `� �, -1 5 Day D.O. By No. wD.O.ppm Time Analyzed: `jsS P Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate, Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate Date Analyzed: -3- 8 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 ' 30 100 200 300 Calculated By: Bottle IniLD.O ppm .r2 �� `d,U3 .00 j `'.0 �� �Stl c� 7 9 9 zZ3 a� LL LJ7 Checked By: QC. No. SDayD.O.ppm 7.q8 3 I,r 3.7 y $ y 5s * / • 9 .G '� • 3 7 ! 76 ! a 3 Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177 Time Preserved: x%� 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk Preserved By: C ' q 7 AM . S .a 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl ���, �7 Preserved pH: , 5 3 ,y 11 AM , p , (y 1 PM / G'>. S$ Checked By: 3 PM 5 PM 7 PM 9 PM SFT SFT -.-- 11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl 3AM 5AM Chk Stcl Pri Influent True Color 1.0 1 St 8hr 2nd 8hr 3rd 8hr l73 y3 ID Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: 5" " (24 Hour Composites) 2nd Source Verification std Time: , Time: True Filtered Apparent(unfiltered) Std FOR FOR Time Analyzed: 113EP Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank Checked By: Sample pH /, q Q•o q.0 799 .0 9 . 2 0 pH(24 Hour Composites) Adjusted Color pH ,4P 76. SE Avg Analyzed By: Z-C. Analysis ppm Calculated By: X Factor Analyzed By: Sample ppm q� �q Z 503 y I t✓t Gv 0 &o 149 5f' a/3 12k �0 3,34 � -I Checked By: Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175 Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I d O,Gy .34 S5 The Analyst's Initials On This Worksheet Certify That Sample Source Spike S/N 1455680 All Stds+/- 10% P-std mg/I /Ia3 ps' .,0 5 The Analyst Has Done The Test To His/Her Ability Sample pH Y #9017 Hi Color_July2017 S.E. Dup Diff<2.6mg/L New Pump setting Q.C. Database Adjusted Color pH Lo color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration Analysis ppm Hach DR 3900 All Except PI New True Collected By: '7C and use X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: ((' P I 55P fLF Sample ppm #9017Hi_ColorJuy2017 Time Analyzed: Ilog? ATime Sulfide 1st 2nd Eff Avg Variable No. 180 �-IlLo Color Hach#125 Analyzed By: �6 700 A 300 P IT5 Avg Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH Illltlal final !Checked By: Pri. Effl 0 'e� T6 Avg WWTP Laboratory Worksheet Date: MAR 3 6 2018 Sludge Volume Index 24 hour composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. ( p ) Effl Spec Eff Low Lift Prim Effl Sec Eff Low Lift Prim Eff Sec Eff Prim Infl AS/ PE Sec Effl 5 Minute 900 90- y a Low Lift Prim ° 30 Minute Vro ys� Time Collected G ys� `yr� 6s' ,Z�l° '�y Collected B : �E� TF ��6 �C� T F JAB � � �1.� �!� � E-�' SVI 30 Co Y (24 Hour Composites) Total°Suspended Sol ids - Std Methods 2540 D 503 359- F:: �.� 361 12 76 77 13 78 79 80 Recycle Sludge Solids aS LL VSS Low Lift Acd Sv�rer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike smp v Ile-iD 1st - 8Hr 2nd - 8Hr 3r - 8Hr Time Analyzed: � Time Out: /�' Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample D 9 p #1 AS #2 #3 #3D Std.900to1100 STD BLK SPK Ft+Slds gms fr 1,z24' , o/7 V . Put Up By:, �,� Filter I 3y 3 Sec Eff /, 1 9y 0(,b Ft Tare gms /,0T/9 A i071 A / 3-3 Weighed By: Filter + solids - gms 3y,3'f oS • dG ,2 / q9 j' 119f ��3 8 ids TSS '/.T3 Filter Tare - gms 6$ A /®/8 �. a fo B � f/ / v �, d"r�G /. /d 90� Avg. ppm /. , Calculated By: e.� � TSS (x4) ys3z Yese Sea Checked By: QC TSS ppm x2 S3o x2 B 191, �� /5 /8 �5 �� �� cX2> 9/� , (nil us1 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. 11591.3 V52 Total Suspended Solids 1st - 8 hr. Comp AOX Wkly Comp. Sec Eff Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec Effl Sample Volume=25m1 Collected By: Sample Size - ml 50 100 200 50 100 200 50 10 0 Filters Sample Ids - gms Time Collected: Filter ID PI PE 1A PI PE 2A PI PE S /9G „TOS Filter Tare - gms io Sample pH (Adjusted) Filter + solids - gms / //57 /./z1r z /22 q6� �����y� ����� y$ Total Sus Solids G8o Bkup Sample pH (Adj) Filter Tare - gms /o /o y 4 //to /.//n !. // �'�� � f /2 Total Susp.Solids(x4) z�zo v50 Nitric Acid to obtain ph<2 Total Suspnd. Solids x2 /022 83 �2 ro x2 /�io //1 /2 x2 Conductivity Cell Constant Analyzed By: (= Mixed Liquor Solids Test Method: Std Methods 2510-B Var.# Cal umho/cm Conductivity 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Sample Volume=25m1 Q C 3 Calibration 5000 umho std Ct 3 7 b 122 50, jO Crucible ID 1 2 .L3• 123 1000,2000,5000+/-10% Crucible + Solids / yt ,�t,sootS Verification 1000 umho std S � t 0 Crucible Tare /7 g qo -ft.ytq/ / 4V Verification 14.9 umho std 5 .I O Z 3.3 Q 6 124 14.9 std. (5.1 to 40.7) I �� ��; L� 284 S.E. Dup Diff. <8.4 umho Solids 70Z 7r O a v47 Canton d��`�� 285 Cell Constant 4.75 to 5.25 043 'a 8 Fiberville d�1 - l 3 . 1 ��•2 (x4) = M LSS 2 80 1 g 2 b• �Q 3 125 1,000,2,000,&5,000 Stds Crucible + Ash 7 8 oN z/ y A.GG 1 a Sec. Effluent C - Sec Eff Dup �, 2, 3 b vs 126 are purchased. Ash I lG 8 r 08 Sec Eff Avg 'y �� 286 14.9 std. Made from � -� � 2 g'�- ppm Non-Volatile G 672 �'SO2 / /Q0b 132 the 1,000 std. MLVSS z/s2 1 lv 8 Mid Range 2nd Source FOR 2000 umho std t(�', � a (` Volatile 76.4 74 ��i a 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities Blankets 700 P 300 A C D 1100 A 3°° 11 P °° P Time A B Time 700 A Feet/Minute 1 #4 Clarifier g 8 i �� oZ �o"Z � � 2 #5 Clarifier 71 7 — 3 #6 Clarifier WWTP Laboratory W�orksheet Date: MAR 3 6 2018 BOD (24 Hour Composites) Standard Method 5210 B Time Put U /yp SampleSourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent 50 /pillow p 3 5 50 150 Put Up By: £G3 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpf 5 ,� 63 -7. �9 /� p/. . 63 Initial D.O. By: Bottle InitD.0ppm 717 7. 03 ? gOZ ?`�- 7 93 ?88 7G Go 165 3 �Ga �S y ss �88 o� G.lic 33s e 5 Day D.O. BY J B No. MayD.O.ppm `� 73 X.83 `� y �� Time Analyzed: ys sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate 5 3 4 3Q 100 200 300 Date Analyzed: y y is ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 D P7. 1 / 3 � 7.f6 -71 6� ?, 67 02- Calculated By: ��8 �/ Bottle Inft.D.O pPm 7 �. ?. 7, a ?a �• �S3 �� •Z•1 G.98 S. ?H 3 Z1 Z 4!-Jr Checked By: t 4C. i NO. 5DayD.O.ppm �O2 7.?G �S y,90 �6 K 2y tl 98 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177 Ammonia Standard /48 200 Seed/6mL Spk Time Preserved: "!" 40 Seed/6 Std Time NH3 Do NH3 DO NH3 Do Time NH3 Time SFT. SFT • g 7 Am • 3• 3� 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl I G 7- 4 Preserved By: '�'C I 1 PM / I �`3S rved pH: /. 3. �3 11 AM Prese 3 PM 5 PM 7PM 9PM Checked By.. SF' SFT 11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl 3AM 5AM Pri Influent True Color Chk Std 1st 8hr 2nd 8hr 3rd 8hr 1.0 G 8 d Yo Spectro Photometric Time: Color 100ml prepared sample Laboratory Control Std Mid Range Std FOR FOR (24 Hour Composites) 2nd Source verification std Time: " Time: True Filtered Apparent(Unfiltered) PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec,Eff. SOO Ellan Time Analyzed: Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg 9 ® ` / Y / Checked By: Sample pH $ & SE Avg 7, 7.Cr 7p pH(24 Hour composites) Adjusted Color pH Analyzed By: Analysis ppm 17q174 j ► / / Calculated By: X Factor / /�— l7 �7 i7 17 / / �3 �Fl�a `�'3t /9 ESL' '� Analyzed By: Sample ppm 03 9� '' /� Checked By: Variable No. 62 63 67 64 324 ,'£ ; 329 22/65 23/66 171 172 173 174 37 103 108 141-- 144 355 NPDES Reported 87 175 Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd . Avg Hach DR 3900 Color Q.C. Sec Eff P mg/I 0.fr o g2 .7-3 8� The Analyst's Initials On This Worksheet Certify That SE Color Spike The Analyst Has Done The Test To His/Her Ability Sample Source SpikeF,v S/N 1455680 All Stds+/- 10% P-std mg/I A oS i.o Q Sample pH #9017Hi_Color_JuW017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database r Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration Adjusted Color pH Lo Colo Hach DR 3900 All Except PI New True Collected By: ;"'`C, py:�1 i� and use Analysis ppm • X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected: '0"VY 1001 ® � #so,7 Hi cDio�J�y2o,7 Time Analyzed: 1f&Ij id,Ole /010 Sulfide 1st 2nd Eff Avg Analyzed By: �r�+ !e'�� �� Time 700 A 3°° P Sample ppm T5 Avg Variable No. 180 Lo Color Hach#125 ,O T6 Av Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl er 9 0 WWTP Laboratory Worksheet Date: IAR Sludge Volume Index 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr„ Average Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. Low Lift Prim Effl ...Sec Effl Low Lift Prim Ella Sec Effl Low Lift Prim Effl . Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute 400 8�8o c�� �`73 Time Collected so �sd 6 f1 2=° zY°P ?ASP Dts ��� �J ! f �O 30 Minute Collected By: ZEc TEi6 RED �'fr ��� �G SVI 30 (24 Hour Composites) Total Suspended Solids std Methods 2540 D 503 359 361 12 76 77 13 5, 78 79 80 - Recycle Sludge Solids Time Analyzed: / �S/r° LL VSS Low Lift Acd Swer Pr EffluentSec Eff Sec Eff Dp Dup.Diff<44 1000Stnd Blank Spike smp vol-25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Time Out: l /,t Sample Size - ml 50 50 100 10 500 500 Blnk<.0004 50 0 500 Sample ID fir . aa9/ Put Up By: �i ]Filter ID ,?�53&a #1 AS #2 #3 #3D Std.900to1100 STD BLK SPK Ft+Slds gms �,yo ? Filter + solids - gms , y`j5� . 3O �• /.3/ oagA . B Sec Eff ,SS' , /089 Ft Tare gms 1.102r f��9j' /GO Weighed By: �£16 g Calculated By: Filter Tare - gms yD.6 p�� : ,��'� , // �. b�� `i d� Avg. ppm f, �' �$ TSS !� s oioy Checked By: QC TSS ppm x2 $ ax2 ,� �$ �f6 /5 1-5 /5 15 �� (X2) $ (/sl TSS (x4) yy�o ,� So?y Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. y(o'l V52 Prim Infl Prim Eff I Sec Eff I Prim Infl Prim Effl Sec Effl Prim Infl Prim Effl Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By: Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms 4 /7.17 Time Collected: Filter + solids - gms /, S8 ,, �.ioGy i.34i l.ito� , 38� �. /a/4� 3 Filter Tare - gms t t Sample pH (Adjusted) Filter Tare - gms i , �;�079 /io39 1./065' �.lr1G �,31y2 1� �d� �. �a0 Total Susp. Solids 6sr Bkup Sample pH (Adj) /2 zo x2 G $ /2 /y Total Susp.Solids(x4) 2�zo v50 Nitric Acid to obtain ph<2 Total Suspnd. Solids x2 fo �yo 52 /2 ,z x2 s7o6 2S .S Conductivity Test Method: Std Methods 2510-B Cell Constant .g Analyzed By: )E•� Mixed Liquor Solids Sample Volume=25m1 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Calumho/cm Conductivity Crucible ID 1 2 3 Calibration 5000 umho std �p>� z.� � Q 122 �� Q•C• Crucible + Solids i1,437o .. 1910 8, ob Verification 1000 umho std $';�p 2 Z ./a 123 1000,2000,5000+/-10% 1701 , `I/ Verification 14.9 umho std S .QS 2 31- 124 14.9 std. (�3to 49'1)SI fo yt Crucible Tare �ifi9 �I (c2 (, v47 Canton �:4/� G � 284 S.E. Dup Diff. <8oT'umho gh Solids 64 Gs G ` (x4) = MLSS �6 ,� ,��, 653 Fiberville "1 .3d 1, y 3-7�, 285 Cell Constant 4.75 to 5.25 Crucible + Ash i 9 �s iq.8 s 58 Sec. Effluent :Z 1D , 2 '�"1 125 �,000,2,000,&5,00o stds Ash /S �� q3 Sec Eff Dup R;Z-v 'L6, `Z 7 '] S 126 are purchased. S 10, v48 Sec Eff Avg �1;Zo 2 7'7`'>) 286 14.9 std. Made from ppm Non-Volatile Goo SG M LVSS 207 Z057 o7614 �7'� Mid Range 2nd Source FOR 2000 umho std (b' 2 i . f'o / try 132 the 1,000 std. Volatile 776 7Fq, 7s.6 Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities 700 A 1100 A 300 p 700 P 1100 P 300 A Time A B C D Time r � � -� 1� �" Feet/Minute 1 #4 Clarifier 7 7 i2 zTZ 2 #5 Clarifier '7 d �i — .— 3 #6 Clarifier — WWTP Laboratory Worksheet Date: MAR 3 1 N18 BOD (24 Hour Composites) Standard Method 5210 B Time Put Up: SampleSource�/ar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent 3 5 50 15Q 200 25 /pillow Put Up By: ml Sample 0 50 Seed/6 Std 30 Seed/3Smp1 30 Seed/5Smpl 5 +0 �, 1eq4 ,�' 9. �S Initial D.O. By: �) Bottle 11nk.D.Oppm / ,C7 $ g.C2 g. o � g .Q3 l�� � .oy lsa 10 as 8� �Xf aoa of S,3G �� Yea 3za 5 Day D.O. By We No. SDeyD.O.ppm -�t" 7.96 G 3,79 Time Analyzed: q SampleSourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup $O'3/59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate 5 3 100 200 300 Date Analyzed: y ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 4 3�, C� g cf(o / �8 S.oB • o �l Calculated By: ,J Bottle In LD.O ppm �S •O / 7 76 g• l a 1� ?a �./q �I y;G s�+ g y l0 0 p 0 d8 b s?g S.oz !�� 1.G3 � 734 I� 7 Checked By: QC: No. 5DayD.O.ppm ?97 K.00 Y:YS 7 P Sec Eff Spike /177 Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank DO Time NH3 Time SFT SFT 200 Seed/6mL Spk Time Preserved: �0 40 Seed/6 Std Time NH3 DO NH3 DO NH3 nn Qkq 7 AIIW' 9AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl Preserved By: SG 1 PM Preserved pH: 3 7g 11 AM Checked By: 3 PM 5 PM -- . 7 PM 9 PM _ SFT SFT 11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl 3AM -5 AM Pri Influent True Color Chk Std 1st 8hr 2nd 8hr 3rd 8hr 1.0 lyr 0 Spectro Photometric Time: 5 Color 100ml prepared sample Laboratory Control Std Mid Range r Std FOR FOR (24 Hour Composites) 2nd Source verification std Time: �,. Time: True Filtered Apparent(Unfiltered) Time Analyzed: j Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg E Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff, 5OO Blank $. � g O Checked By: Sample pH ll� • 9 ;p .O ry 1 Le Le SE Avg [.4 7•te �•� `�� ��V (a pH(24 Hour composites) Adjusted Color pH 'qq �40 J..SLW i S� /p Analyzed By: Analysis ppm 1� Calculated By: � X Factor © 14 2q r �� 5514 r f 2 d10 / Analyzed By: Sample ppm Q �� / ` D / 357 164 Checked B ; Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 NPDES Reported 87 175 C y P Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg Hach DR 39QQ Color Q.C. Sec Eff FP mg/I O 53 O.S/ � The Analyst's Initials On This Worksheet Certify That SE Color Spike // The Analyst Has Done The Test To His/Her Ability Sample Source Spike ,,r S/N 1455680 All Stds +/- 10% P-std mg/I /.03 "0.0 Sample pH ✓ #9017Hi_ColorJul2017 S.E. Dup Diff<?.,3i11g/Lz` New Pump Setting Q.C. Database Adjusted color H Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration p Hach DR 3900 All Except PI New True Collected By: 3'C JG V �� and use Analysis ppm X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: W-0? gP Sample ppm L #9017 Hi_Cobr Juy2017 Time Analyzed: p�P ) P I Sulfide 1st 2nd Eff Avg Variable No. ::18�O Lo color Hach#125 Analyzed By: �� l3W 6V0 Time 700 A 3 P T5 Avg Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl of Ql T6 Avg