NC0000272_Analytical Fecal Coliform Date per Request_20180101 (6)

WWTP Laboratory Worksheet ®ate: MAR 2 2 E8
Sludge Volume index
2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Composites 1st - 8 hr. Comp. p• ^
Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS / PE Sec Effl 5 Minute �� �(J 900 8 3
tf /D i° /W //°.�3'O //°�� 30 Minute �' j � y8o a
Time Collected f,/r" /�" 7 �° �J�. SVI 30
Collected By: Z-C pM 'Tw 3'C ° �v� 6
(24 Hour Composites)
78 79 80 Recycle Sludge Solids
Total Sus ended Solids Std Methods 2540 D 503 359 -:::361 12 76 77 13 p
s LL VSS Low Lift, Acd Swer, Pr EffluentSec Eff Sec Eff. Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Analyzed:Y : //—/°
Out: �° Sample Size - ml 50 50 � 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Time ,Z /, �3 , o� J.Zf78
Put U B 6 Filter ID yo�� #1 AS :,- #2 #3 #3D std.gooto11oo STD BLK SPK Ft+Skis gms
P p Y J Ft Tare gms b
Weighed By: j0 Filter+ solids - gms 3848 4/747 . 1 so /137 i o /, Sec Eff /•>G�a / /oy4
TSS 1301 2
Calculated'By: J,)6 Filter Tare - gms /7 ! o /tya /076 1077 / / `� Avg. ppm / / 1,�0T/ TSS (x4) so?d ��O y9fV
Checked By: qC TSS ppm x2 3ss x2 ��4 f/z /s/ /5 ?y /5 r2 ,t3 c > 9/y -o.oc:Uoz nisi
- hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids � Waste Solids Susp. Soilds Avg. S/3f V52
FTotalpended Solids 1st 8 p AOX Wkly Comp. Sec Eff
Prim Infl Prim Effl Sec EffI Prim Infl Prim EffI Sec EffI Prim Infl Prim Effl Sec Effl Sample Volume=25ml Collected Be - ml 50 100 200 50 100 200 50 100 200 Sample ID �• !9 '3 Time Collected:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms �O? /� Sample H (Adjusted)
Filter+ solids - gms /, ��� /, r o /, 1o7G LO -3 �l oY /,i zt i,o Filter Tare - gms 1737 P p )
/o /o$ 3 /, 38 y9 /./0 7 Rio /. 1 ys Total Susp. Solids a fy8 � Bkup Sample pH (Adj)
Filter Tare - gms /. �. 1�t~35 f• t/ v50 Nitric Acid to obtain ph<2
Total Suspnd. Solids x2 g g /a y /2 �j/ x2 D� /2 (p x2 Z�y ,rz/ /2 32 Total Susp.Solids(x4)
Conductivity
Test Method: Std Methods 2510-B Cell Constant ,3 Analyzed B
Mixed Liquor Solidsy:
Var.# Cal umho/cm Conductivity
Sample Volume=25m1 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample T�mp °C Sample umho/cm 122 Q�C•
Crucible ID 1 2 3 Calibration 5000 umho std U
Crucible + Solids q// /g �/ Verification 1000 umho std �Q�
123 1000,2000,5000+1-10%
6O �Z Q $'� 124 14.9 std. (5.1 to 40.7)
Crucible Tare q g(O j j $ Gy/ Verification 14.9 umho std 6'-- •
�' 284 S.E. Dup Diff.<8.4 umho
Solids 75 766 v47 Canton / � �''
285 Cell Constant 4.75 to 5.25
(x4) = MLSS 30I 1 oxco Z175 Fibervi{le
1 Sec. Effluent '76 3l3c� 125 1,000,2,000,&5,000 stds
Crucible + Ash /�, �8,G S'97 3/Z(o
/' � 2 , � 126 are purchased.
Ash /83 Sec Eff Dup
V4$ SEC Eff Avg
286 14.9 std. Made from
ppm Non-Volatile 77- �32 /�09 132 the 1,000 std.
M LVSS 3s� 2 8 z 2 g Mid Range 2nd Source FOR 2000 umho std ��
Volatile
2n
1st - 8Hr d - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Blankets 300 P 700 P 1100 P 300 A Time A B C D
00 00 A
Time 7 A 11 ?/ 7/ -7y IlFeet/Minute 1
#4 Clarifier 2
#5 Clarifier j G f1i 6 �s
3
#6 Clarifier

WW'TP Laboratory Worksheet Date: Hif,,R 2 5
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: &Wo Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: jJ6 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smp1 5 3 5 50 150 200 250 /pillow
Initial D.O. By: „�)t Bottle InH.D.Oppm 6100 8 14 8 /8 8!7 $ oy S 8,03 Sty �Ga 8y
5 Day D.O. By NO. SDayD.O.ppm !•8 J-5A vZ• S3 zy �,5'�f 31 . ! S X� 3� 6 8 �' y y S`7 �� 68 G, 60 88 6.,'� ftO �.IR,r i51 p, L
Time Analyze Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: 3 30 8 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: 90 Bottle InitD.Oppm 8.oz 8 l 1/7 8.08
�oA zo 2G ,� ss yy I:a9 S.z 3.6 S6 f.q8 G� o?,G3 7o
Checked By. C: No. mayD.O.ppn ,B 3,
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: /Iv 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT -• SFT 200 Seed/6mL Spk
Preserved By: JJr 8 17 7 AM •� 3.(5 Q 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl 8. 8'
Preserved pH: �,� ZZ •$,03 11 AM 1 PM
Checked By: 3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1st 8hr 2nd 8hr 3rd 8hr
qy z7
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Pht)iohieti'ric Time: !` •G— ,,
r
�,�(24 Hour Composites) 2nd Source Verification std Time: 5 ,� Time: True Filtered Apparent(Unfikered) Std FOR FOR
Time Analyzed: ,�� Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PdCIEff Aerinf LL Acid Swr Sec. Eff. 500 Blank
Checked By: Sample pH JZ, / z.,c> 5,0
pH(24 Hour Composites) Adjusted Color pH �. .(® �lF �P SE Avg " - �.(� �.
Analyzed By: JaL- Analysis ppm 23(, oe Z(--0 2,60 413.7- Z-yL 3�g� IZ3 �l9
Calculated By: a DL X Factor / / ( / / / / /
Analyzed By: ,fat..- Sample ppm qZ Z3 9 KIV Z---Ya 7-01 2(,-0 Z(, �r V3 q Z10 3B .3V, r /2-3 V q/% 4,13 b
Checked By: fJ Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 1 164 1 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/l ��a 0..3Z 0,3 The Analyst's Initials On This Worksheet Certify That
Sample Source Spike ✓ S/N 1455680 All Stds +/- 10% P-std mg/I o! The AnalysL4as Done The Test To His/Her Ability
Sample pH #9017 Hi_Color *2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: i. jpodl JJ6 and use
X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected: /OW f*o dsr
Sample ppm #9017 Hi Color JuWO17 Time Analyzed: /,Q."� /.. //.�' Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 F Analyzed By:
e'Ov 6D!/ ,rD✓ Time 700 A 3 00 P T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl 0 C� T6 Avg

VVWTP Laboratory Worksheet Dater Jill MAR 2 6 2.018
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 811r 3rd - 8Hr Average
Low Lift Prim Eff I Sec Effl Low Lift Prim Effl Sec'EffI Low Lift Prim EffI Sec Effl Prim Infl AS/ PE Sec Effl 5 Minute a,50 FFO g7d
Time collected 4Dsa " �� ass aso ass /Os%o rps� /D /1 ,° // °r 30 Minute y50 Soo y�7
Collected By: jDi- jap Tw JU1_ .lap Tt-) 1 Rt'z V-'c SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods_2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: �y�P LL VSS Low Lift Acd Swer "P'r Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: z==A Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: sg& Filter ID 3411 #1 AS #2 #3 #31) Std.900to1100 STD BLK SPK Ft+Slds gms 227Z ZZY
Weighed �By: ��6 Filter + solids - gms 3383 `/ Sa /, 1 s.r J s �, i.1/9.t Sec Eff // 03 �oyG Ft Tare gms , 0792 7 os
Calculated By: ili Filter Tare - gms I tzs `a Z 31 1047 1,o*77 iO4 Avg. ppm /. 1132 1,ioyS TSS /z�7 /z3F,
Checked By: "'QC TSS ppm x2 �s� x2 ,�y� /.'t/ q /5 zy /5 z6 ��° (X2) 9y3 +0.6001 vs) TSS (x4) 5-7� y7 6 y9sz
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. yg,3 V52
Prim Infl Prim Eff I Sec Eff) Prim Infl Prim Eff) Sec Effl Prim Infl Prim Effl Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By: Jue
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms /, �'�j Time Collected: //=P
Filter+ solids - gms (z�� /', �/ ���f 15 S� �D ' /.// 1, 373 s /1t3 Filter Tare - gms 1Q,70 Sample pH (Adjusted) i
Filter Tare - gms /, D�195 5 �. I I l,D /• 11�5 '� 1'15 / 1091Ey
Total Susp. Solids Bkup Sample pH (Adj)Total Suspnd. Solids x2 5`r` /2 3� x2 g 5� /2 x2 60$ /17 Total Susp.Solids(x4) p -, v50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant ,q 3 Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std �.� 22- (� !� 122 �� Q.C.
Crucible + Solids 7 Y�72 Sa/ /g �y Verification 1000 umho std �� 22. 123 1000,2000,5000+/-10%
Crucible Tare I 8I Off/ , y S Verification 14.9 umho std 124 14.9 std. (5.1 to 40.7)
Solids 7 5 cY 739 07 Canton l 3(J Z 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS 6 301(" zIse, 30is Fiberville l( t 1-f 07-. 1 285 Cell Constant 4.75 to 5.25
Crucible + Ash 752% Z /8 G 596 Sec. Effluent ?0 ilm ZS". 7 Zq ot 125 1,000,2,000,&5,000 Stds
Ash /7/ Sec Eff Dup 30 '7 2--q 19 126 are purchased.
ppm Non-Volatile 3 {�, a s v48 Sec Eff Avg I ,�] ' ) 286 14.9 std. Made from
M LVSS �j (p , ,27.Z 31 z Mid Range 2nd Source FOR 2000 umho std {� 'S 7-) , 1 D 132 the 1,000 std.
%Volatile �C�.p Z 7`.
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier `7 `7-1- 7 kz 7 $ Feet/Minute 1
#5 Clarifier ? `7 7 7 7 2
#6 Clarifier _ 3

WWTP Laboratory Worksheet Date: ����
�F,` MAR 2 6 2018
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: //y'P Sample SouroeNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent . Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: JJ6 ml Sample 0 50 Seed/6 Std 30 Seed/3Smpi 30 Seed/5Smpl 5 3 5 50 150 200 250 /pillow
Initial D.O. By: �6 Bottle Inft.D.Oppm T.05 S,/Y F, 46 8�G 8.o4r �0'7 8.06 S.gB 7� r77 893
7 l/ ,�.g y 2 3.7� 39 �•og y7 3.� 6s 61, y. s o 7s l3/ /sl 4.8
5 Day D.O. By No. MayD.O.pM •
Time Analyzed: ff Sample SouraeNvar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: 3-31-18 ml Sample 0 30 Seed/6 Std 30 Seed/3Smpi 5 5 3 4 . , 30 100 ` ' 200 300
Calculated By: Bottle InRD.Oppm 6 80 !� $/G ZWA 8,/y �,� "8:0� 57A .oy 67 800 ?Y //Y Y 8.�7 ly/` `00,547 ,�53 889 .ZGy :E
Checked By: QC: No. SDayD.O.ppm 7. `l 1 3.G 3.79 tf• o y a .�j .d .�' ,$G7'!
LAmmonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT - SFT 200 Seed/6mL Spk
Preserved By: ild �G g,i3 7 AM q.3 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl Z gZ 8 go
Preserved pH: 11 AM 11 PM
Checked By: 3 PM 15 PM
7 PM 9 PM SFT ., a SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Std Pri Influent True Color
1.0 1 st 8hr 2nd 8hr 3rd 8hr
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: b
(24 Hour Composites) 2nd Source Verification std Time: 5 Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: Z Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAVg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: Sample pH //.Q /•9 1 - g /0•1D 9.2 119 0 —_3
pH(24 Hour Composites) Adjusted Color pH ,Lo Tee /.G, 1•f o SE Avg ? '7,(,p C o 7, %(�
Analyzed By: Analysis ppm t'o7C. f .C) ,10 [o JO;
Calculated By: X Factor
Analyzed By: Sample ppm 85 g89 95 C794 &740 u) Z>ID o 310 27 SILO 26 2 09 /S 6 /-U b-bg 49L
Checked By: r T Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 , 103 108 141 144 355. '7 357 164 87 1 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 [All
olor Q.C. Sec Eff P mg/I 3 , -7 0.Zo 0,Z7 The Analysts Initials On This Worksheet Certify That
Sample Source Spike ✓ S/N 1455680 Stds+/- 10% P-std mg/I �� 0.9The Analyst Has Done The Test To His/Her Ability
Sample pH ✓ #9017 HiColor JuW017 E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: i2g-4 a,e ,loss and use
X Factor S/N 1505038 PI New True:NCASI 71.01 Time Collected: /0�w / 1
Sample ppm #9017 HLColor_Juy2017 Time Analyzed: !1-W //# //.!r Sulfide 1st 2nd Eff Avg
Variable No. 180 1 Lo Color Hach#125 Analyzed By: 1F 3'F J'F Time 700 A 300 P T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final Checked By: Pri. Effl T6 Avg

WWTP Laboratory Worksheet
Date: MAR
Sludge Volume index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low Lift Prim Effl Sec EffI Low Lift Prim EffI Sec Effl Low Lift Prim EffI Sec EffI Prim Infl AS/ PEfSecffl 5 Minutesd 8SdTime Collected ,(W' G 6=1I Z� . ?- 7 Z;'P —PAY t /05YAA /vs� /�i`�l . Gl' lL P p 30 Minute 4t70Collected By: zx, Tie�o�o .ua 7E4 TRP c� .raa t,,,_ �_ ►�� 7r�1 SVI 30
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: //#'p LL°VSS, Low Lift Acd Swer Pr Effluent SeC Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: ss,4 Sample Size - ml 50 50 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: Tom' Filter ID 3 3��5 #1 AS #2 #3 #3D Std.900t01100 STD BLK SPK Ft+Slds gms I ZY/F 1,2 IS a /�
Weighed By: 7 Filter + solids - gms 4•' ' 13�� , 15 3 �. $ 5 1. I�G�4 Sec Eff j, /�l� 1060 Ft Tare gms /oi 4 ii78 y
s4�.3555 N5 ,
Calculated By: tj Filter Tare - gms 01 G,2- 1, �Q753' 6161 Avg. ppm m5q TSS 1299 s 7-7
Checked By: QC TSS ppm x2: x2 ''�(a 0� S /5 D /5 � ,0 (.2) ,0c,81 us) TSS (x4) 57,74 y9yo Slag
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. V52
Prim Infl Prim EffI Sec Effl Prim Infl Prim Eff I Sec Eff I Prim Infl Prim Effl Sec Effl Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms gs Time Collected:
Filter + solids - gms I, yy i o. os4 s 28 I �zb ( , /a0� Filter Tare - gms o 1/7 Sample pH (Adjusted)
Filter Tare - gms izo7 1, loqj lo►o / ioyz I,ii 7 /.. ?H 06,3 30 i!7;� ITotal Susp. Solids 687 Bkup Sample pH (Adj)
Total Suspnd. Solids jx2 yyo 93, /2 Z3 jx2 /094 6y /2 Zy x2 0 /2 / 7 ITotal Susp.Solids(x4) Z7y8 V50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant Ll , 93 Analyzed By:
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 0 © fii+'Yt 2to 122 5000 JQ.C.
Crucible + Solids gytg Zips- 7 D Le Verification 1000 umho std S 30 � , p a 123 1000,2000,5000+/-10%
Crucible Tare J�. �91 , gy /$ ` / Verification 14.9 umho std (7 �3b A M -7 , 124 14.9 std. (5.1 to 40.7)
Solids 7-? 75 v47 Canton Cl O M 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS opy 7-2 05 Fiberville ® ►'Y► , t 3 0 285 Cell Constant 4.75 to 5.25
Crucible +Ash fps/ 9 86z2 5 Ff2 Sec. Effluent Q o[0p G . oa 3 1 125 1,000,2,000,&5,000 stds
/ Sec Eff Dup 00 � (c. 3 J 126 are purchased.
Ash a
ppm Non-Volatile 1/0q� v48 Sec Eff Avg "a 1 286 14.9 std. Made from
M LVSS 1308 33ZZW Z S Mid Range 2nd Source FOR 2000 umho std la 10M 1 a Ole 132 the 1,000 std.
% Volatile 79.3 7?/ 7
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 11°° A 3°° P 7°° P 11°° P 3°°A Time A B C D
#4 Clarifier $ 8 7 51 3' Feet/Minute 1
#5 Clarifier 7 1 1 7 7 7 ' 2
#6 Clarifier -- I I — — IF I 13

WWTP Laboratory Worksheet ®ate: MIAR 2 7
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: L0 p Sample SourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: i-i ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smp1 5 3 5 50 150 200 250 /pillow
Initial D.O. By: TW Bottle IniLD.Oppm (?ls� �� �. � , 15Li
1171
5 Day D.O. By No. 5DayD.O.pM S L? 9 3.1-5 3.o�(o ®.. .3 J. 71 � 33 �; �117 14) 2 � S"• O'C? � 3. 3S
Time Analyze 0 Sample SourceNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: f—— Q ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
Calculated By: Bottle Init.D.Oppm Q '' I �'. �r'� ' ` 1- 1 1
Checked By: QC. No. 5DayD.O.ppm 7.q • aZG .o� S� 3. G S a -3 ?• / G��� . 3 •0'�3
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: r rvL 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: J P i• 53 3 7 AM 3 - 5 y , 6 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl
Preserved pH: .�� / .� 3,�j 11 AM 1 PM >� . 76
Checked By: "j' 3 PM 15 PM
7 PM 9 PM =SFT , SFT
11 PM 1 AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 5AM
Chk Stcl Pri Influent True Color
1.0 1st 8hr 2nd 8hr 3rd 8hr
Hi Jr? 2
Color 100ml prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: A *
(24 Hour Composites) end source Verification std Time: %="�A-rti Time: True Filtered Apparent(Unfiltered) Std FOR FOR
Time Analyzed: Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PriCIEff Aerinf LL Acid Swr Sec.Eff. 500 Blank
Checked By: rr Sample pH /l•J7 1.9 :?.q I-& 1./ , IT ,
7.41
pH(24 Hour Composites) Adjusted Color pH SE Avg ,/ .fe 7.40 74
Analyzed By: L Analysis ppm ZZ- ?- � l 2 ! 2 Z� /5"70 14o e®7 3e/7
Calculated By: � L.- X Factor /
Analyzed By: Sample ppm �Z ,` 2.� /57� /!o I Via' 3`l� 4c97 '2
Checked By: Variable No. 62 1 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I d,10 O./(l 0,24 The Analyst's Initials On This Worksheet Certify That
Sample Source Spike S!N 1455680 All Stds +/- 10% P-std mg/I `,0/ 0,-v �,99 The Analyst Has Done The Test To His/Her Ability
Sample pH #9017 Hi_Color_Juty2017 S.E. Dup Diff<2.6mg/L New Pump Setting Q.C. Database
Adjusted Color pH IlLo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: .lpli_ T TZ and use
X Factor SIN 1505038 PI New True: NCASI 71.01 Time Collected: C'%�?/",I
Sample ppm #9017 Hi_Color_Jut2017 Time Analyzed: Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: p I Time 700 A 300 P T5 Avg
Master QC Signature: By signing this I verify that all OC parameters have been checked COD pH initial final Checked By: Pri. Effl I Al- IT6 Avg

VWIITP Laboratory Worksheet Date: MAR 2 8 201
Sludge Volume Index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd -8Hr 3rd - 8Hr Average
Low Lift Prim EffI Sec EffI Low Lift Prim Effl Sec EffI Low Lift Prim EffI Sec EffI Prim Infl AS/ PE Sec Effl 5 Minute gso *80 2,50 96
Time Collected G %0 4 e=v Zt9le . tee ?� s° P 0", P Z� SS P I' P �f�D � % p 30 Minute y o ,sroo 50D 9 3
Collected By: TDB T.tP ej� JJB ?o� ?.eP e� JJf `j c, bv�^` �,l %w SVI 30
,.
(24 Hour Composites)
Total Suspended Solids Std Methods 2540 D 503 359 361 12 76 77 13 78 79 80 Recycle Sludge Solids
Time Analyzed: ji lts P LL VSS Low Lift Acd Swer Pr Effluent Sec Eff Sec Eff Dp Dup.Diff<5.1 1000Stnd Blank Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Out: sa Sample Size - ml 50 50 °" 100 100 500 500 Blnk<.0004 50 0 500 Sample ID
Put Up By: 'rtd Filter ID V2- #1 AS #2 #3 #3D std.9ootolloo STD BLK SPK Ft+Sldsgms f?o97
g y Filter + solids - gms 3�. N/�3 Z rl y �, i 330 �. j S gj / F? Sec Eff r T3T q Ft Tare gms o79G 1, lots /�3
Weighed B �--
Calculated By: TLC Filter Tare - gms /, 0`�J3 X3 L /. o5q 1 677� /, (� Avg. ppm 3 1017 TSS i�4i io /Z�1�
Checked By: fi"QC TSS ppm x2 9 x2 s�2. L) /5 /5 y "j (x2� � pbby vs) TSS (x4) siy y
Total Suspended Solids 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. Suspended Solids Waste Solids Susp. Soilds Avg. 51g7 V52
Prim Infl Prim Effl Sec Eff I Prim Infl Prim Eff I Sec Eff I Prim Infl Prim Effl Sec Eff I Sample Volume=25ml AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50 100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI PE 2A PI PE 3A Filter + Solids - gms 4 % Time Collected:
Filter + solids - gms f Pat. >. 1�93 � / ass, 1 �i8a yS S 2 Filter Tare - gms �, �o Sample pH (Adjusted)
Filter Tare - gms A o979 4 io 2 /. /lay A iioj /1s 1. i oLx2'
/t� / 2-0 /; Total Susp. Solids 715 Bkup Sample pH (Adj)
Total Suspnd. Solids x2 38ig Sq /2 ?o x2 X/7y 78 /2 zy S -7 r7,5 /2 Total Susp.Solids(x4) ?8�o v50 Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids Test Method: Std Methods 2510-B Cell Constant 93 Analyzed By: CRA
Sample Volume=25ml 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average Sample Source (All Units umhos/cm) Time Sampled Sample Temp °C Sample umho/cm Var.# Cal umho/cm Conductivity
Crucible ID 1 2 3 Calibration 5000 umho std 0 5-3D D 44 1 5 Y 122 g anp6 It-)-C.
Crucible + Solids y5 zl, oat 71 4,3 Verification 1000 umho std Q 5 3 0 10 m a 9 S-� 123 1000,2000,5000+/-10%
17,Crucible Tare /17, 7113, xl, ysds f8.G IKU Verification 14.9 umho std © S 30 M z . so a7 , s 124 14.9 std. (5.1 to 40.7)
Solids 7.3Z 7.r(j 7,7, v47 Canton C7"7 40 q ry) ,Q 5,9 284 S.E. Dup Diff. <8.4 umho
(x4) = MLSS 219,19 Zgs-G "�/2 vZg32 Fiberviile goo j7Py1 285 Cell Constant 4.75 to 5.25
Crucible +Ash 2g 11 VVI 7g . 6, 5 Sec. Effluent p '1/,5 Am a q 0({ 125 1,000,2,000,&5,000 Stds
Ash I.T Sec Eff Dup 0 715 �M -7 „3 a 010 La 126 are purchased.
ppm Non-Volatile G g 614 5-0 08 Sec Eff Avg a-? .3 a 0 9" 286 14.9 std. Made from
MLVSS 2I32 ?390 0 Z3 2 j Mid Range 2nd Source FOR 2000 umho std 10 S-D A M I -� -� ,q 1 90 9- 132 the 1,000 std.
Volatile 7G.2 79,2 ZZ,
Blankets 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time 700 A 1100 A 300 P 700 P 1100 P 300 A Time A B C D
#4 Clarifier 7 r2 r ?r 7 Feet/Minute 1
#5 Clarifier 7 7 7 - 7 2
#6 Clarifier — -- 3

WWTP Laboratory Worksheet Date: MAR 2 8
BOD (24 Hour Composites) Standard Method 5210 B
Time Put Up: j" � SampleSourceNar.No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
Put Up By: (. Q ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 50 150 200 250 /)pillow
Initial D.O. By: t- Bottle [11nit.D.0ppm ,2 �S $. 2 z `/ 3 12
Z3 ell
�. 2�3 �Z �!�y 9 /. a�5 Day D.O. By No. DayD.O.ppm .dL . 8 3. 3 S !. . G S. 7� 3 3 '
Time Analyzed: S�/p SampleSouroeNar.No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
Date Analyzed: 1{-",t49 ml Sample I 0 30 Seed/6 Std 30 Seed/3Smpl 5 5J 7 3 4 30 100 <f� 200 300
Calculated By: Bottle IniLD.O ppm S� 0.�3 /� J• 7 T / , Z.' �. �� �' ry.�~ ��4 )4� JI c/ �Jv / �Checked By: QC: No. 5DayD.O.ppm g.Vs v( 3. / 7 � 3.36 5' 03 ('' .6x J 5. 7A �{ f 7 L'7'
5 0
Ammonia Standard /48 T5 T6 T7 T7 T2 Stripper Feed Tank Sec Eff Spike /177
Time Preserved: , 40 Seed/6 Std Time NH3 DO NH3 DO NH3 DO Time NH3 Time SFT SFT 200 Seed/6mL Spk
Preserved By: C g 2l 7 AM . Q .-1 9 AM 10 Seed/0.3 Smpl 10 Seed/0.5 Smpl
Preserved pH: / 2-' 3. (nZ/ 11 AM
1 PM d` S
Checked By:
3 PM 5 PM
7 PM 9 PM SFT SFT
11 PM II AM 10 Seed/0.4 Smpl 10 Seed/0.6 Smpl
3AM 15AM
Chk Stcl Pri Influent True Color
1 st 8hr 2nd 8hr 3rd 8hr
1.0
,�o t Z 7o 19
COIOr 100m1 prepared sample Laboratory Control Std Mid Range Spectro Photometric Time: $
(24 Hour Composites) 2nd Source Verification std Time: -Q Time: True Filtered Apparent(Unfiltered) Std FOR FOR
-0
Time Analyzed: Sample Source 100ppm 300ppm 900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM 11AM Dup 11AMAvg PE Turb Pr Eff PrICIEff Aerinf LL Acid Swr Sec.Eff. 5OO Blank
Checked By: Sample pH /� � q
C 8, S 7.1
pH(24 Hour Composites) Adjusted Color pH 7,(� l&I �(o SE Avg 7, 7►� �3.C
Analyzed By: J-6- Analysis ppm .�(� g � Z a
Calculated By: X Factor
8' � `� 4c4,
Analyzed By: Sample ppm 9 ,2�D C,o 3 3 Z"3� 5 140 �tSGe / `f ��
Checked By: Variable No. 62 63 67 64 324 329 22/65 23/66 171 172 173 174 37 103 108 141 144 355 357 164 87 175
Nitrate Color Color Calibration Curve Dates Phosphate 1st 2nd 3rd Avg NPDES Reported
SE Color Spike Hach DR 3900 Color Q.C. Sec Eff P mg/I O.tv 0.3 - The Analyst's Initials On This Worksheet Certify That
Sample Source Spike ,� siN 1455sao All Stds +/- 10% P-std mg/I v 4 02 ;9a! The Analyst Has Done The Test To His/Her Ability
Sample pH ✓ #9017 Hi_color Ju1y2017 S.E. Dup Diff<2.6mg/L New Pump setting Q.C. Database
Adjusted Color pH I Lo Color Hach#125 Test Method: NCASI 253 pH Grab Samples LL Acid Swr SE Process Control, Instrument Calibration
Analysis ppm Hach DR 3900 All Except PI New True Collected By: 3- bM 'T"hJ and use
X Factor S/N 1505038 PI New True: NCASI 71.01 Time Collected: 10AP log? b EJ �
Sample ppm #9017 Hi_Cobr Juty2017El I Time Analyzed: P op t0P Sulfide 1st 2nd Eff Avg
Variable No. 180 Lo Color Hach#125 Analyzed By: � ` Time 700 A 300 P T5 Avg
Master QC Signature: p By signing this I verify that all QC parameters have been checked COD pH rj,q initial 5 final Checked By:
g° Pri. Effl ,rr IT6 Avg