NC0000272_Analytical Fecal Coliform Date per Request_20180101 (7)

WWTP Laboratory Worksheet
Date:
MAR
'
Sludge
Volume Index
Composites 1st - 8 hr. Comp.
P
2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites)
1st -3Hr
2nd - 8Hr 3rd - 8Hr Average
Low Lift
Prim Effl Sec Effl
Low Lift
Prim Effl
Sec Eff! Low Lift: Prim Effl
Sec Effl Prim Infl
AS / PE. Sec Effl
5 Miniute gso
30 Minute
Zo _
3a '
Time Collected 6 ys
6 ysff 6%Ji
-
1=i°
x ld ss/,l°
1 °a i0 ��° f
,%/%%�
�'`
yso
SVI 30
Collected By: ���
ov s
�c
���
(24 Hour Composites)
Total Suspended SoFfds
-�
std Methods 2
Eta3 ,,
LL VSS
359
Low Lift
361 12 76
Acd Swer Pr Effluent Sec Eff
77 13
3e�=:Eff D�p� Dup.Diff<5.1J
78 79
1000Stnd Blank J
80
Spike smp vo1=25
Recyc:le Sludge Solids
1st - 8Hr 2nd - 8Hr 3rd - 8Hr
Time Analyzed:
Y
Time Out:
Sample Size - ml
---
it
;, 50 50
100 100 500
#3
_
_ 500 _ Blnk<.00041 50 0 500 Sample ID
std.9o0tol100 STD BLK, SPK Ft Slds gms
#3D �
/ —
Put Up By:
Filter ID
A. 01,
#1
AS #2
_
•
-
.
Weighed Bye
�_�
Filter +solids-gms�3381
i f, :
/ to /.
, :. -� �� J
. 11l:r�� Sec Eff
f. . 04- Ft Tare gms
Calculated By:
Filter - gms
g
,3�L
D/ 4
�. 02 O-'
�. /�C Avg. ppm
c �. /�S�y /'. /04�� TSS
TSS (�;4)
� �12a0
Checked By: QC
TSS ppm
�;2 ,S,$�
d'x2 O$c�
„S� s3 /5
/5 D �' /®
ace) �%y�z cs�ol
vs�
y�oA� y1za
Total Suspended Solids
1st - 8 hr. Comp.
2nd - 8 hr. Comp. 3rd - 8 hr. Comp.
Suspended Solids
Waste :iolids
Susp, Soilds Avg. ® V52
Prim Effl
Sec Effl
Prim Infl
Prim Effl-,' Sec Effl ! Prim Infl Ef l Sec Effl
�— �Prim fl
Sample Volume = 25m1
AOX Wkl Comp. Sec Eff
y p•
---
_
100
_�
200
00
S0
100 200 50
0 _ �
�� 100 200
�
Sample ID -
�_ -
Colle��ted B y�
Sample Size - ml
ID
_
PE
1A
PI
PE J 2A PI
�
PE 3A
IFilter + Solids - gms
�®; ; n;-
Time Collected:
Filter
Filter +solids -gms
g
gj��
/, F
'
/ $ / /jg _ '�
/zs•� �< ®�0 8 � 06
�
Filter Tare gms _
' - I;
I �"��1
Sample pH (Adjusted)
pH I;Adj)
Filter Tare- gms
1 /o67
iozz
_ t
LoLe-
�03 /l�1:3�
Total Sus�p. SolidsBkupSample
�; v50
Nitric Acid to obtain ph<2
Total Suspnd. Solids
i+ff
/2 /y
x2
/2 ;,c2
�� /y3$
a tip /2 //
Total Sus,p.Solids x4 i
h
736
Conductivitiy
Test Method: Std Methods 2510-B
� Cell Constants � .���
Analyzed By: 6ev
Mixed Liquor Solids
Sample Volume = 25ml
1st - 8Hr 2nd - 8Hr
3rd - 8Hr
Average
Sample Source (All Units umhos/cm)
-�
Time Sampled
Sample Temp °C
Sample umho/cm
/
Var.# cal umho/cm Conductivity
122 �c'Ju
Crucible ID
1 2
3
Calibration 5000 umho std��
'Verification
a 'fit: I� ':
ZZ�
, 7 ��-123 1000,2000,5000 +/A0%
Crucible + Solids
! p / o -
$, `10 ro
1000 umho std
5100_ �,/}�'�
���
�— 749, �I
'I24 114.9 std. (5.1 to 40.i')
Crucible Tare
! 4. G72 f , 8y3'7
/ wio
Verification 14.9 umho std
��
,�
,�
G�
284 S.E. Du Diff. <8.4 umho
6 P
Solids
3
zy�z
of y(o
v47
a �%3 %
Canton _-� - - -
Fiberville
sv
��
A
�;
-
°2�.�
-285 - Cell Constant 4.75 be 5.25
- -� -
(x4) = MLSS
.?3�,?
-
Sec. Effluent
_
�•�i� �
_
.c
a
1��___� '125 �,000, ;z,000, & s,000 stds
Crucible + Ash
/g. � z �q.8s32
8 �
yv'Z
_ _
-
Sec Eff Du',p
J�
�•`�j
'�
>
'126 are purchased.
Ash
ppm Non -Volatile
90 qs
�o d�8
v48
_ _ -
Sec Eff Ayi; ---- -_- --
�—
�- 5 ��'�
�5 ����?
286 14.9 std. Made from
000
MLVSS
zo�z ,to92
O 1�
C)
AAid Range 2nd. Source FOR 2G!00 umho std
It�� �t:%� %1�i-
fit, 7
lei �S
-
132 Ithe std.
% Volatile
8 F.Y. 4
1st 8Hr
1 8
2nd - 8Hr
3rd - 8Hr
Target Avg = 80 to 120
Hood Face Velocities
Blankets
Time 700 A
-
1100 A
300 P
700 P
1100 P
300 A
Time A
B C D
#4 Clarifier 7kz
7`%
7
/
Feet/Minute 1
#5 Clarifier 7
7
7
2
3
#6 Clarifier -
—
i
I —
�"
`�

WWTP Laboratory Worksheet Date: MAR 13 2018
BOD (24 Hour Composites)
Time Put Up:
Put Up By:
Initial D.O. By: a
Standard Method 5210 B
Sample SourceNar. No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56
ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5
Bottle IntD.Oppm a b ,QR j 9 /�b v b 8 a 6
I/•
w acm ~, j 7. U T . /� v J�
No. 5Da o.
Sample SourceNar. No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57
ml Sample 0 30 Seed 6 Std 30 Seed/3Smpl 5 5
p /
Bottle InLD.Oppm t/ Q.ab • 4 s �•o� g a3_
NO. 5DayD.O.ppm ;0�S S,9 s, 3 /
Low Lift 158 LL Filtrate Sec (Effluent Sec Effluent ',Sec Effluent /60 I -el: Effluent `
3 5 50 ,. 150 ��2100 250 /pillow
_ _ f
/�� T' `�� - - /a i) 8�. - to $ '� �'� ['[_ 8• SS /':51` 8 ` '7
--I >_~_c6�! 5 _�_ __ ..57 �d - _ '�
LL Dup_ /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
3 4 30 100 200 1� 300
- -
s/xx;- JC�c�a
7.
5 Dav D.O. B v
Time Analyzed: 4s p
Date Analyzed: g � y
Calculated By: T�
Checked By: QC.43
Ammonia
Standard /48
T5
T6
L T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: /�aal°
Preserved By: p 1-
40 Seed/6 Std
�� 8 ,
Time
7 AM
11 AM
3 PM
NH3
DO
NH3
s� . `.
' v'
DO
, 7'~-
'.O.
V73
DO
L �
Time
9 AM
1 PM��
E5PM-
NH3
Time
SFT
10 sE�ed/o.3 smpu
SFT
10 seed/o.5 smplPreserved
-
200 Seed/6mL Spk
pH: 1.6
Checked'By:
7 PM
�
9 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3 AM A5 AM
Chk Std �- !�� Pri Influent True Color
1.0 1st 8hr 2nd h 3rcl 8hr
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time: S wA4
(24 Hour Composites)
Time Analyzed: 3� P
Checked By: FT
pH (24 Hour Composites)
Sample Source
Sample pH
Adjusted Color pH
2nd Source
100ppm 300ppm
900ppm
Verification std
500ppm Low Lift Acid Swr
/0. / Z, Z
4-- /v 3- to
Time: �" �
SE 5AM 5AM Dup
,-1
-N.
5AM Avg
Time:
SE 11AM 11AM Dup
True
IIAMAvs
Filtered
PE Turb Pr Eff PriCIEff Aerinf
T ( S' � �3
SE Avg - (o -7. (o -7. 0
Apparent(Unfiltered)
LL Acid Swr Sec. Eff.
/0. / Z. 2- ,-7
-4. �: (o I. 4o
Sid FOR
500
—
OR
Blank
Analyzed By: pL.
Calculated By: nL—
Analyzed By: 3pt_
Checked By:
Analysis ppm
X Factor
Sample ppm
Variable No.
62
Zg
63
S8V
67
�9/v
64
Ile f
/t«/
324
/q /
Iµ/
329
//
/o
22/65
/
01
23/66
11
171
172
173
174
/I
37
3 E3
103
/ 5/ i-
4'�
108
/I3
//3
141
37
g�
144
35b0
351,0
- 355
�3
�3
357
164.
_
87
175
Nitrate
Color
Color Calibration
Curve Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
SE Color Spike
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
0.2t
, R
: XL
The Analyst's Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/- 10%
P-std mg/I
1 03
/o
/.
Sample pH
#9017 Hi -color July2017
S.E. Dup Diff<2.6mg/L
New Pump setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
-)Di-
'SCq,
X Factor
1505038
PI New True: NCASI 71.01
Time Collected:
/VFfo
/�,?°r
0?
ISM
Sample ppm
#9017 Hi_color JuWO17
Time Analyzed:
Sulfide
1st
2nd
Eff Avg
Variable No.
180
LoColor Hach #125
Analyzed By:
�;C_
S
j,(�
Time
700 A
300 P
T5 Avg
Master QC Signature:
By signing this I verity that all aC parameters have been checked COD pH initial final
Checked By:
�-'
Pri. Effl
0
0
T6 Avg

WWTP Laboratory Worksheet Date: MICR 14 2018
Sludge Volume index
Composites 1st - 8 hr. Comp. 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites) 1st - 8Hr 2nd - 8Hr 3rd - 8Hr Average
Low LiftLm $ec Effl Low Lift Prim Effl Sec EffI Low Lift Prim Effl Sec Effl Prim Infl AS / PE Sec Effl 5 Minute g6'o fro 870 8& 3
Time Collected `�� `':'" sw �sr , SS/p A) Ss�ao / �°. %<°lp I� %�°� 30 Minute o go 'rich y$
Collected By: Kit ,;,;� ��.: �Jb ��� �`D1.. -- SV130 ----
(24 Hour Composites)
Std Method's 2540 D
Sample Size - ml
Filter ID
503,
LL VSS
50
3y, VO,3a
µ ` 359 361 12
Low Lift Acd Swer Pr EffluentSec
50 100 100
#1 AS #2
3 3 A 43 67 % .f 1
/, 1601 . / a5q 499
x2 t/$ S3 s'�
2nd - 8 hr. Comp.
Prim Infl Prim Eff I Sec Effl
76 77 13
Eff Sec Eff Dp Dup.Diff<5.1
500 500 Blnk<.0004
#3 #31D Std.900to1100
, d 56/1 / /5' Sec Eff
.0ri7$ oZ //O( Avg. ppm
/5 /d /5 1 �b
3rd - 8 hr. Comp.
Prim Infl Prim Effl Sec Effl
78
1000Stnd
50
STD
, / loo�q
79
Blank
0
BLK
/ • /D�i
80
Spike
500
SPK
smp vol=25m
Sample ID
Ft+Slds gms
Ft Tare gms
Recycle Sludge Solids
1st - 8Hr 2nd - 8Hr 3rd - 8Hr
/. al68
1. o,q / /. sz 13
Total Suspended Solids
Time Analyzed: % /°
Time Out: o°
Put Up By:
Weighed By:
Calculated By:
Checked By: QC j-
Filter + solids - gms gyo
Filter Tare - gms / 98
TSS ppm x2 39b
1st - 8 hr. Comp.
Prim Infl Prim EffI Sec Effl
50 100 200
PI PE 1A
A %t/ /
/• OSS
_
TSS
/oso
033
(Y2) �I7G C)
Suspended Solids
Sample Volume = 25ml
(/s) TSS (x4)
Waste Solids
yo ro V079 -1113a
Susp. Soilds Avg. elo g6 V52
AOX Wkly Comp. Sec Eff
Total Suspended Solids
50
100
200
50
100
200
Sample ID
Collected By:
Sample Size - ml
PI
PE
2A
PI
PE
3A
Filter + Solids - gms
�, `��
Time Collected:
Filter ID
x2 7-TTS/
/, i
blvs, 1, is
/2 /7
/ �?S`3 • 1,?/0
%D'/G 1, // 3 / 17f
x2 ,3eN /2 .8
Filter Tare - gms
Total Susp. Solids
Total Susp.Solids(x4)
Conductivity
!os
zz,�y v50
Sample pH (Adjusted)
Bkup Sample pH (Adj)
Nitric Acid to obtain ph<2
Filter + solids - gms
Filter Tare - gms
1,r3o1v
!. 6 197
/./o
J. !orq
Ii s
USS
Total Suspnd. Solids
x2 z(.sy s'� /2 /�
Test Method: Std Methods 2510-B
Cell Constant
3
Analyzed By:
1.g1c2j1
Mixed Liquor Solids
Average
v47
Sample Source (All Units umhos/cm)
Calibration 5000 umho std
Verification 1000 umho std
Verification 14.9 umho std
Canton
Time Sampled
✓, oO
!�U
/(�,' Q
Sample Temp °C
�./.(�
Z/Z
Sample umho/cm
.Z$
j
�-,x�t✓
Var.#
122
123
124
284
Cal umho/cm Conductivity
J� Q•C•
1000,2000,5000 +/-10%
14.9 std. (5.1 to 40.7)
S.E. Dup Diff. <8.4 umho
Sample Volume = 25ml
1st - 8Hr
2nd = 8Hr
3rd - 8Hr
Crucible ID
1
i7 pG
/ ii
2
z
z/, yzs
G
3
• Qp
t8:6NoG
�' �
Crucible + Solids
Crucible Tare
Solids
S8s
/
v48
Fiberville
Sec. Effluent
Sec Eff Dup
Sec Eff Avg
D : �b
/D: `%U �
/0, 0
10% 0 Ad t
6, 6
Z� �
u,Q
Z5;D
� S%,�
/ �
I -egg
fg,
285
125
126
286
Cell Constant 4.75 to 5.25
1,000, 2,000, & 5,000 stds
are purchased.
14.9 std. Made from
-
Soli - MLSS
z yo
zsoy
88.
Crucible +Ash
Ash
/ 4o
9
3GS
��, y3
`o0
o
/8• G
9'
36�/
ppm Non -Volatile
0 3 3 Mid Range 2nd Source FOR 2000 umho std //, /0 A/4 Zl/ • 3 �rj i! 3 132 the 1,000 std.
2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
300 P 700 P 1100 P 300 A Time A B C D
M LVSS / q 7,2 1 ceq0,R !
Volatile 8-f• 9)
Blankets 1st - 8Hr
Time 700 A 1100 A
%
%
�O
Feet/Minute 1
2
#4 Clarifier
#5 Clarifier
i
7
G
-"
"—`
—^
—
3
#6 Clarifier
"""

VWNTP Laboratory Worksheet Date: MAR 14 1018
BOD (24 Hour Composites)
Time Put Up:/y�l/°
Put Up By: YeA
Initial D.O. By:
Standard Method 5210 B
Sample SourceNar. No. Blank /52 Standard /54 Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate Sec Effluent Sec Effluent Sec Effluent /60 Sec Effluent
ml Sample 0 50 Seed/6 Std 30 Seed/3Smpl 30 Seed/5Smpl 5 3 5 50 150 200 250 /pillow
Bottle InitD.0ppm ��� 905 a8 G •oa 1 Ia, c r 1 S� ` o �v9 8 . cal �S �� `Oq. .06 •�a �. � .�
u �; s. s 7� 3 - 1. z SSA q /5 J
NO. eDew.o.p� Q ! � - ---
Sample SourceNar. No. Blank /53 Standard /55 Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup /57 LL Dup /59 Low Lift Sec Effluent Sec Effluent SecEff Dup /61 SecEff Filtrate
ml Sample 0 30 Seed/6 Std 30 Seed/3Smpl 5 5 3 4 30 100 200 300
9 8-/0 ` o� G•OS 10 8 0$ g •0 S 8 • g 8Checked
No. 5NyD:.pPm °-r ►� ! .7l 7 ' p3. 3 l ' �} t� e /
Bottle InitD.O ppm g.o / ELIE;E: S'
5 Day D.0_ By % 6J
Time Analyzed: q s_D p
Date Analyzed: 3 /1/5
Calculated By: G11
1°(
By: QC: '^'
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: /
Preserved By: SDl-
1
40 Seed/6 Std
• 9 8
1 1311 'q. S
Time
7 AM
NH3
DO
3
NH3
DO
NH3
DO
Time
9 AM
NH3
Time
SFT
10 Seed/0.3 Smpl
SFT
. 10 Seed/0.5 Smpl
200 Seed/6ml- Spk
7. z
Preserved pH: 1.-5
11 AM
1 PM
Checked By:
3 PM
15 PM
7 PM
19 PM
SFT
SFT
11 PM
11 AM
10 Seed/0A Smpl
10 Seed/0.6 Smpl
3 AM
15 AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
-5'0
ZL;v
.Z /b
COIOf 1
00m1 prepared sample
Laboratory Control Std
Mid Range
Sectro Photometric
p
Time:
(24 Hour Composites)
Time Analyzed: Ii Pwl
Checked By:
pH (24 Hour Composites)
Analyzed By: ,) L
Calculated By:
Analyzed By: J pt_
Checked By:
Sample Source
Sample pH
Adjusted Color pH
Analysis ppm
X Factor
Sample ppm
Variable No.
2nd Source
100ppm 300ppm
5" 21?!a
62 63F
900ppm
S/2-
67
Verification std
500ppm Low Lift Acid Swr
!O•!v Z•3
7• '4•(i
/11ir W
/ I
�9� / 9Jf ZZ,?r
1 64 1 324 1 329
Time:
SE 5AM
-T (a
-T &
1142
%
/40
22/65
5'
5AM Dup
7•h
T (.-
/
/
23/66
5AM Avg
1
/qf
171
Time:
SE 11AM 11AM Dup
172 173
True
11AMAvg
174
Filtered
PE Turb Pr Eff PriCIEff Aerinf
-4.Z `I.1 -4 •1r
SE Avg -4(o I ?-& 7 (v
225 /7-!
/ I f, /
/4}0 6-� 2 / 3
37 103 108 1 141 144
Apparent (Unfiltered)
LL Acid Swr Sec. Eff.
/v. (V Z• 3 7.
:?. ce%•(y
35S2 /o/ 1/
!
35�2 lofS"
355 357 164
Std FOR
500
�9S
87
FOR
Blank
175
Nitrate
Color
Color
Calibration
Curve
Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
0.?9
y1
3
, 3
The Analyst's Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
SE Color Spike
Sample Source
Spike
S/N 1455 880
All Stds +/- 10%
P-std mg/I
0.9 8
�.
Sample pH
#9017 HLColor JuN2017
S.E. Dup Diff<2.6mg/L
New Pump Setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
'3
S
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
Ifjp, p
/Ovi
f00?
Sample ppm
#9017 Hi_Color_JuW017
Time Analyzed:
°.°p
// -'e
/ S19
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
El
I
Analyzed By:
"I'• (.n.
:y,G,
'�;�., ,
Time
700 A
300 P
T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial. final
Checked By:
Pri. Effl
,I
T6 Avg

WWTP Laboratory Worksheet
Date:
MAR 15 21
Sludge Volume Index
Composites 1st - 8 hr. Comp.
Low Lift Prim EffI Sec Effl
2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites)
Low Lift Prim Eff I Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS / PE Sec Effl
5 Minute
1st - 8Hr 2nd-8Hr 3rd-.8Hr Average
1?216 900 840 8TO
Time Collected 40.4
Collected By: KC�
6ffvA g ='
a.�v .i,)6�_s'��
?141rP
?'!sJ°
XV? Dw
Jule
o
140XV 1 z4f/
// //°
30 Minute
SVI 30
qso S-oo 4136 we,o
Total Suspended Solids
Time Analyzed: //i°
Time Out: I
Put Up By:
Weighed By:
Calculated By:
Checked By: QC
Total Suspended Solids
Sample Size - ml
Filter ID
Filter + solids - gms
Filter Tare - gms
Total Suspnd. Solids
Std Methods 2540 D 503
LL VSS
Sample Size - ml 50
Filter ID f6 Y 1
Filter + solids - gms 3Y4 9
Filter Tare - gms o
TSS ppm x2 3'Go
1st - 8 hr. Comp.
Prim Infl Prim Effl Sec Eff I
50 100 200
PI PE 1A
1, is 4 0 4 10G3
J./z/5 4/071 i o8
x2 482 yq /2
(24 Hour Composites)
359 361 . 12
Low Lift Acd Swer Pr Effluent
50 100 100
#1 AS #2
e o s
i, /ot/ /1 /ZS2 f, /07
x2 yoy wry 7s
2nd - 8 hr. Comp.
Prim Infl Prim Effl Sec Effl
50 100 200
PI PE 2A
1? 4.rre S
1,1046 f. // 71 1. 3r
jx2 /6y Qs /2 /y
76 77 13
Sec Eff Sec Eff Dp Dup.Diff<5.1
500 500 Blnk<.0004
#3 #3D std.9ootolloo
3 Sec Eff
r. 0 /. 1OGs Avg. ppm
/5 /3 /5 /y p
3rd - 8 hr. Comp.
Prim Infl Prim Eff I Sec Effl
50 100 200
PI PE 3A
i. hl 71V i, Izz?9
1. /os ! JIS3 /, lid I
jx2 yyG 96 /2 /G
78 79
1000Stnd Blank
50 0
STD BLK
o
/. fis i. io�8
cx2� q/8
Suspended Solids
Sample Volume = 25ml
Sample ID
Filter + Solids - gms
Filter Tare - gms
otal Susp. Solids
Total Susp.Solids(x4)
Conductivity
80 Recycle Sludge Solids
Spike Smp Vol=25m 1st - 8Hr 2nd - 8Hr 3rd - 8Hr
500 Sample ID
SPK Ft+Slds gms ozG zts1 Z74/2
,
Ft Tare gms �03/ /, �� 4 / y
TSS 94s !o 0
vs) TSS (x4) 3ggo yt8y y3gz
Waste Solids Susp. Soilds Avg. y,�/q V52
AOX Wkly Comp. Sec Eff
Collected By:
, o Time Collected:
/ ilyl Sample pH (Adjusted)
571 Bkup Sample pH (Adj)
?316 V50 Nitric Acid to obtain ph<2
Mixed Liquor Solids
Test Method: Std Methods 2510-B
Cell Constant
L`
Analyzed By:
64911
2nd - 8Hr
3rd - 8Hr
Average
V47
Sample Source (All Units umhos/cm)
Calibration 5000 umho std
Verification 1000 umho std
Verification 14.9 umho std
Canton
Time Sampled
%UQ
�j; 0,0 ,.(
5.00 �j
lo, 5Q
Sample Temp °C
Z./, 1
Z-�• 7
z
�
Sample umho/cm
5
rj 7
� /, �
Z� �
Var.#
122
123
124
284
Cal umho/cm Conductivity
>ru., Q.C.
1000,2000,5000 +/-10%
14.9 std. (5.1 to 40.7)
S.E. Dup Diff. <8.4 umho
Sample Volume = 25ml
1st - 8Hr
Crucible ID
Crucible + Solids
1
9T53
2
4 9osr
3
7 z
i 8 yo
634
Crucible Tare
/9. LG
/9. 8y13
Gt
Solids
.iy7G
08
Fiberville
Sec. Effluent
Sec Eff Dup
Sec Eff Avg
D- ` o
/O'�o
to:
10: Zo AA,
, 2.
L. S.
Z � 3
10
U
285
125
126
286
Cell Constant 4.75 to 5.25
1,000, 2,000, & 5,000 Stds
are purchased.
14.9 std. Made from
(x4) = MLSS
13sG
/ 9 g
1 s!6
q p401
5'sG
Gsi
Crucible +Ash
Ash
ppm Non -Volatile
y1?
/p
714
0
yyo
/ 4S3
Mid Range 2nd Source FOR 2000 umho std
! £j ICA.
Z
132 the 1,000 std.
M LVSS .`//G
Volatile
Blankets
81, s' 74 S
1st - 8Hr
VIZ.8
2nd - 8Hr
3rd - 8Hr
Target Avg = 80 to 120 Hood Face Velocities
300 P
700 P
1100 P
300 A
Time
A
B
C
D
Time
700 A
1100 A
7
i
7�
7
Feet/Minute 1
#4 Clarifier
6 t
7
#5 Clarifier
G
G
G
6
G
lv
2
#6 Clarifier
—
—"
'—
3

WWTP Laboratory Worksheet Date: MAR 1 5 2018
BOD (24 Hour Composites)
Standard Method 5210 B
Time Put Up: /-°i
Sample SourceNar. No.
Blank /52
Standard /54
Acid Sewer /168
Acid Sewer
Pri Effluent /56
Low Lift /58
LL Filtrate
Sec Effluent
Sec Effluent
Sec Effluent /60
Sec Effluent
Put Up By:
ml Sample
0
50 Seed/6 Std
30 Seed/3Smpl
30 Seed/5Smpl
5
3
5
50
150
200
250 /pillow
Initial D.O. By: �
Bottle InkD.OPPm
No. SDayD.O.ppm
SampleSoureeNar. No.
8 0!
3X
�. �E
Blank /53
to
/y
3.3
Standard /55
8.10
Z8�
I. ��,
Acid Swr Dup /169
�®
��
Pri Eff Filtrate
8.oZ
�q 3. b
Pri Eff Dup /57
S/ 8.oy
3 �l
LL Dup /59
5,7 $ °
31
Low Lift
4TL /o
' .55
Sec Efn"uent
? r/
Sec E-muent
!2S 8.3o
4. xq
SecE 1 Dup /61
Z4Z ' 3t�
I 1,60
SecEff Filtrate
yL--
5 Da D.O. B y
Time Analyzed: ,�? p
Date Analyzed: 3 ;a'
ml Sample
0
30 Seed/6 Std
30 Seed/3Smpl
5
5
3
4
30
100
200
300
Calculated By:
Bottle
No.
IntD.OPPm
SA
.00
Z?
X.04?
3y
80�
4�/
�.os
So
8°
SZ
S,os'
6/
.oa
72
°�
#/ '
1�
ZL/
8.3/
Z78
S.7
Checked By: C:
WayD.o.ppm
�Q
i/. SEA
3,
ql z
s =3
,i
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: j/:
40 Seed/6 Std
Time
NH3
DO
NH3
DO
NH3
DO
Time
NH3
Time
SFT
SFT
200 Seed/6ml- Spk
Preserved By: -XDi-
? $
g i0
7 AM
9 AM
10 Seed/0.3 Smpl
10 Seed/0.5 Smpl
Z 79
35
Preserved pH: Ir
3.30
11 AM
11 PM
a.aG>
Checked By:
3 PM
15 PM
7 PM
19 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3AM
5AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
A P1
till
14I Z
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time: 5
(24 Hour Composites)
Time Analyzed: p
Sample Source
2nd Source
100ppm 300ppm
900ppm
verification std
500ppm Low Lift Acid Swr
Time:
SE 5AM 5AM Dup
5AM Avg
Time:
SE 11AM 11AM Dup
True
11AMAv
Filtered Apparent(Unfiftered)
PE Turb Pr Eff PriCIEff Aerinf
LL Acid Swr Sec. Eff.
Std FOR
500
FOR
Blank
Checked By:
Sample pH
Z
Zo
� (0
:;�(o
7.s'
rE-
T, ipl
//.Z
Z0
pH (24 Hour Composites)
Adjusted Color pH
Z. G
?. G
:7-
:7 (p
SE Avg
74
X6
ZG
7G
7.G
Analyzed By: 701.
Analysis ppm
G
R87
0-
/72
1 78
4&2-
90
0
"sG
/,c
G.ra
Z3#
Calculated By: TOO
Analyzed By: �4
X Factor
Sample ppm
6
x97
Sid
/
�Y9S
IT2
17J,
/
/G2
t
I/o2
/lit
/(OZ
.5lZ
/
/90
/
gc
/
it6
G�'G
/
23
�9G
/
Checked By:
Variable No.
62
63
67
64
324
329
22165
23/661
171
172
173 1
174
37
103
108
141
144
355
357
164
87
175
Nitrate
Color
Color Calibration
Curve Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
SE Color Spike
i/
✓
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
o, o
o,v1
0 tly
v, yZ
The Analyst's Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/- 10%
P-std mg/I
o�
�� p�
Sample pH
#9017 Hi_cobr July2017
S.E. Dup Diff<2.6mg/L
New Pump Setting I
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrurr ent Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
TOG
740
X Factor
SIN 1505038
PI New True: NCASI 71.01
Time Collected:
Sample ppm
#9017 Hi_Color_July2017
Time Analyzed:
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
Analyzed By:
tC3
-5;e q,
Time
700 A
300 P
T5 Avg
Master QC Signature: By signing this I verify that all OC parameters have been checked COD pH initial final
Checked By:
3�j
Pri. Effl
1 10
�
T6 Avg

WWTP Laboratory Worksheet
Date:
MAR 16 2018
Sludge
Volume Index
2nd - 8 hr. Comp.3rd
- 8 hr. Comp.
(24 hour Composites)
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Composites
1st
Low Lift
- 8 hr. Comp.
Prim Effl Sec Effl
Low Lift
Prim Effl
Sec Effl
Low Lift
Prim Effl
Sec Effl
Prim Infl
AS / PE
Sec Effl
5 Minute
8 7v
aZo�
1b5; f
ran P
CVp
os P
�� I>
i °� p
30 Minute
$CD
.30
Sra�
Time Collected
Collected By:
j r 1.
..�.-�
-3K
r�
v Yr/-
c' D
D�
?J!^n
T
`r'i
I�
TlL
SVI 30
(24 Hour
Composites)
78 79
80
Recycle Sludge Solids
Suspended Solids
Totalp
Std Methods 2540 D
503
359
Low Lift
361
Acd Swer
12
Pr Effluen
76
77
13
Sec Eff
Sec Eff Dp
Dup.Diff<5.1
1000Stnd
Blank
Spike
Smp Vol=25
1st - 8Hr
2nd - 8Hr
3r - r
Time Analyzed: �'j-
Sample Size - ml
LL VSS
50
50
100
100
500
500
Blnk<.0004
50
0
500
Sample ID
Time Out: sC 4
SPK
Ft+Slds
�, 18�,3
Filter ID
3 3��
#1
1
AS
#2
#3
#3D
Std.900to1100
STD
BLK
gms
Put U B
p y
Tare
12
��
Filter + solids - gms
3 �'
, 3
15 `�
1 7
�,
7 1
3
Sec Eff
1(�
�'�
Ft gms
D o
06
Weighed By:
/J
TSS
/°0?3
/� 3�
/ S 7
B ��
Calculated y
Filter Tare -gms
/.53
i �E
��
Avg. ppm
`�
TSS (x4)
y
�0?8
Checked By: ri QC
TSS ppm I—x2,3x2
�,
1
;
/5
3rd
/5y
- 8 hr. Comp.
c�IN �
Suspended Solids
Waste Solids
o2
Susp. Soilds Avg. 4//y V52
Total Suspended Solids
1st - 8 hr. Comp.
p
EffI
2nd
Prim Infl
- 8 hr. Comp.
Prim Effl Sec Effl
Prim Infl
Prim EffI
Sec Effl
Sample Volume = 25m1
AOX Wkl y Comp. Sec Eff
Prim Infl
Prim Effl
Sec
200
Sample ID
Collected By:
200
50
100
200
50
100
Sample Size - ml
50
100
Pl
PE
2A
PI
PE
3A
Filter + Solids - gms
/. / S
Time Collected:
Filter ID
PI
PE
1A
g®1
Filter Tare - gms
io
Sample pH (Adjusted)
3
v
Filter + solids - gms
/$y8
o
// $
0�
1l q3
!I 3
Total Susp. Solids
ADZ/
Bkup Sample pH (Adj)
Filter Tare - gms
40,119
icz
f, �/�
< <
4
/, /,to
/2
a
x2 �z
.
"75
/2
Total Susp.Solids(x4)
f(o v50
Nitric Acid to obtain ph<2
Total Suspnd. Solids
x2 g
s 7
/2
x2 868
5
p
,
Conductivity
Cell Constant
.z13
Analyzed By:
Test Method: Std Methods 2510-B
Mixed Liquor Solids
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Sample Source (All Units umhos/cm)
Time Sampled
Sample Temp °C
Sam umh /cm
Var.#
Cal umho/cm
Conductivity
Q.C.
= 25ml
Sample Volume
1
2
3
Calibration 5000 umho std
5--- �Q
Z1.
122
Crucible ID
� 3 0
123
1000,2000,5000 +/-10%
Crucible + Solids
�. 13
I �9�f
Verification 1000 umho std
C!
124
14.9 std. (5.1 to 40.7)
Crucible Tare
17
2l, �/268
it 6yoo
Verification 14.9 umho std
S.. !
9 � Q
�Q•.
284
S.E. Dup Diff. <8.4 umho
Solids
8�
�
j
v47
Canton
79'
285
Cell Constant 4.75 to 5.25
,
(x4) = MLSS
3502
o
W
a l
FiberviUe
! { j-'
. %
p
MOO
125
�,000, 2,000, & s,000 star
Crucible +Ash
q8
91,36S
1 Y. (,5b �
Sec. Effluent
�' ��
7irQ. %
MIS
126
are purchased.
Ash
7
Sec Eff Dup
jqs
286
14.9 std. Made from
ppm Non -Volatile
3�-
v48
D
Sec Eff Avg
2�•O
90
132
the 1,000 std.
2nd Source FOR 2000 umho std
/Q Q
MLVSS
9v
a',39-
Z
v�
Mid Range
% Volatile
2nd - 8Hr
3rd - 8Hr
Target Avg = 80 to 120
Hood Face Velocities
Blankets
1st - 8Hr
300 A
Time
A
B
C
D
300 P
700 P
1100 P
Time
700 A
1100 A
(,�/ 2
7Feet/Minute
1
#4 Clarifier
02
2
47
#5 Clarifier
_
t
L
3
#6 Clarifier
-�
I -

VWUTP Laboratory Worksheet Date: MAR 16 2018 ,
BOD (24 Hour Composites)
Time Put Up: zL r sample sourceNar. No. .
Put Up By: i ml Sample
Initial D.O. By: 'r W Bottle IniLD.Oppm
5 Day D.O. By �'��' NO. MayD.o.ppm
Time Analyzed: io h Sample SourceNar, No.
Date Analyzed: A,Iis' ml Sample
Calculated B Bottle IniLD.O ppm
B QC. No. 5DayD.O.ppm
Y
Ammonia
Time Preserved: /1Z0'rP
Preserved By: :u`c_
Blank /52
0
jV7 r p�
✓11 j ,t��
Blank /53
0
3Checked
Standard /54
50 Seed/6 Std
C
J 0
Standard /55
30 Seed/6 Std
q Ll 3, y
Standard /48
40 Seed/6 Std
$,, 2, 6
3, 3U
Standard Method 5210 B
Acid Sewer /168 Acid Sewer Pri Effluent /56 Low Lift /58 LL Filtrate
30 Seed/3Sm.Gpl 30 Seed/5SmpI 5 3 5/
ri //n 4 J I. (a �1� 1 �11 / O 2-3-
1 /' �.'� W l 3� r Z�� 9
Acid Swr Dup /169 Pri Eff Filtrate Pri Eff Dup 157 LL Dup /59 Low Lift ':
30 Seed/3Smpl 5 5 3 4 - ..
2, 5 LELA3'
3
"'. - �' 3, 3 3
T5 T6 T7 T7 T2
Time NH3 DO NH3 DO NH3 DO Time NH3 Time
7 AM , () �aQ �j . 9 AM
Sec Effluent Sec Effluent
50c 2 150
F "
2%
Sec Effluent ISec Effluent
30 100
-h5 ; / - _3
ZZ
Stripper Feed Tank
SFT SFT
10 Seed/0.3 Smpl 10 Seed/0.5 Smpl
Sec Effluent /60
200
/ 7,
SecEff Dup /6 i
200
3z
Sec Effluent
250 /pillow
SecEff Filtrate
300
3 5 1"
Sec Eff Spike /177
200 Seed/6mL Spk
Z3 -
Preserved pH: 5
11 AM
11 PM
Checked By: Pr
3 PM
5 PM
7 PM
9 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3AM
15AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time: 5%✓'
(24 Hour Composites)
2nd Source
100ppm 300ppm
q
62 63
Color Calibration
Verification std Time: Time:
900ppm 500ppm Low Lift Acid Swr SE 5AM 5AM Dup 5AM Avg SE 11AM
%'P• �( R, 5 $, 3 8,3
7. . G ?v&
) 5 jg41 7/31
gve 505 19:!� rq1 / 3 6 73 73
67 64 324 329 22/65 23/66 171 172
Curve Dates
True
11AM Dup 11AMAvg
1
173 1 174
Phosphate
Fihaied
SE Avg
/?3
37
1st
PE Turb
1
I 7
103
2nd
Pr Eff
711
7, �e
3o?-
302-
108
3rd
PrICIEff
7, 4
7, V
3SY
354
141
Avg
Apparent (Unfiltered) Std FOR FOR
Aerinf LL Acid Swr Sec. Eff. 500 Blank
`I. I )VI ff A - 5 9.3
71 , i 7.4- , (o
�i44( (a-9l 33Z O
p ;2ON 33Z 23c) 467$ a
144 1 355 357 164 87 175
NPDES Reported
Time Analyzed: / j@-�Sample Source
Checked By: p Sample pH
pH (24 Hour composites) Adjusted Color pH
Analyzed By: ', C' Analysis ppm
Calculated By: C X Factor
Analyzed By: Sample ppm
Checked By: Variable No.
Nitrate Color
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
G
,S7
S
,
The Analyst's Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
SE Color Spike
Sample Source
Spike
ISM 1455680
All Stds +/- 10%
P-std mg/I
/, d0
Sample pH
✓
#9017 Hi_Cobr JuW017
S.E. Dup Diff<2.6mg/L
New Pump setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
TC
TWrd1
TO
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
b'�—P
Ip¢P
' (o?P
Sample ppm
#9017 Hi_Color July2017
Time Analyzed:
I t°-'P
1 I0P
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
Analyzed By:
brA
D►N)
Time
700 A
300 P
T5 Avg
Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final
Checked B
yOr
r _y -r
JPri.
Effl Q T6 Avg ,