NC0000272_Analytical Fecal Coliform Date per Request_20180101 (8)

WWTP Laboratory Worksheet Date: 1,, ; C 1 2 " '
Sludge
Volume Index
Composites
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd - 8 hr. Comp.
(24 hour Composites)
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Low Lift
Prim Effl
Sec Effl
Low Lift
Prim Effl
Sec Effl
Low Lift
Prim Eff)
Sec Effl
Prim Infl
AS / PE
Sec Effl
5 Minute
Ssn
Sso
5AD
5-440
Time Collected
9A
_
2"'i
.2%°P
Z"—r
/6" P _
0 t' P
/J 11'
/'� P
%�� �'
I '� p
30 Minute
zso
30o
Flo
$7
Collected By:
TDt
1XP
_
• %)f
TDA.
AJ..d
I J
7-irk
ITu%
✓
V t
SVI 30
(24 Hour
Composites)
Total Suspended Solids Std Methods 2540 D
503
359
361
12
76
77
13
78
79
80
Recycle Sludge Solids
Time Analyzed: 1 ''`
LL VSS
Low Lift
Acd Swer
Pr Effluent
Sec Eff
Sec Eff DID
Dup.Diff<5.1
1000Stnd
Blank
Spike
Smp Vol=25m
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Time Out: I'+`-4
Sample Size - ml
50
50
100
100
500
500
Blnk<.0004
50
0
500
Sample ID
Put Up By:
Filter ID
1
#1
AS
#2
#3
#313
std.90otolloo
STD
BLK
SPK
Ft+Slds gms
1 y
Z ZZ7
Weighed By: ,,
Filter +solids -gms
3 .3�}0
`/
%, I I
DSS.
I/ <j
Sec Eff
Avg. ppm
�,
s'
?;�
Ft Tare gms
Calculated By: -r
Filter Tare - gms
: '
/, 037
/, 0�q3
/, Ic�G.7
/. C/�J
077
TSS
//S'r
i071/
DO
Checked By: QC
TSS ppm
x2
x2
/5
/5
(x2) (
, �00
us)
TSS (x4)
t 9G
y00 1-
Total Suspended Solids
1st - 8 hr. Comp.
2nd
- 8 hr. Comp.
3rd
- 8 hr. Comp.
Suspended Solids
Waste Solids
Susp. Soilds Avg. p V52
Prim Infl
Prim Eff I
Sec Effl
Prim Infl
Prim Effl
Sec Effl
Prim Infl
Prim Effl
Sec Effl
Sample Volume = 25ml
AOX Wkly Comp. Sec Eff
Sample Size - ml
50
100
200
50
100
200
50
100
200
Sample ID
Collected By:
Filter ID
PI
PE
1A
PI
PE
2A
PI
PE
3A
Filter + Solids - gms
/
Time Collected:
Filter + solids - gms
47
t
/6571
Filter Tare - gms
1 /
Sample pH (Adjusted)
Filter Tare - gms
U79
107F
/f 39
/. 116g
Total Susp. Solids
4p2
Bkup Sample pH (Adj)
Total Suspnd. Solids
x2 G 9y
37
/2 /2
x2 S/S
So
=/2]/
x2
(
/2
Total Susp ISolids(x4)
,Zyog V501
Nitric Acid to obtain ph<2
Conductivity
Mixed Liquor Solids
Test Method: Std Methods 2510-B
_ Cell Constant
R'3
Analyzed By:
Sample Volume = 25ml
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Sample Source (All Units umhos/cm)
Time Sampled
'Sample Temp °C
Sample _
Var.#
cal umho/cm
Conductivity
Crucible ID
1
2
3
Calibration 5000 umho std
s� 34
ZZ• 6;1
Gumho/cm
41 I► 0
1:22
C10
Q.C.
Crucible + Solids
i V. Its q
19,1016
Verification 1000 umho std
S : 30
10
,7
1;�3
1000;2000,5000 +/-10%
Crucible Tare
q ge. G7
M, F!VZF
iff,dyfl
Verification 14.9 umho std
2-7-1
124
14.9 std. (5.1 to 40.7)
Solids
5'7z
S
57
V47
Canton
�% 1 30
10. 3j
�. P1
284
S.E. Dup Diff. <8.4 umho
Fiberville
Sec. Effluent
R R y r
ll✓�17.9
/910
285
125
Cell Constant 4.75 to 5.25
1,000, 2,000, & 5,000 S,tds
(x4) = MLSS
Crucible + Ash
I1"
q S75'a
13S2
9. 86'2Y
2304A31-5
�51 0
Ash
Sec Eff Dup
q ; )S'w'�)
? �:
Say
126
are purchased.
ppm Non -Volatile
ggy
3
v48
M
Sec Eff Avg
3 0 l
IS3 7
286
14.9 std. Made from
M LVSS
/111Z
/ 96 8
Mid Range 2nd Source EDR 2000 umho std
/Q '. 3 /�✓�
Z 2 .
J �7d
132
the 1,0— std.
Volatile
8Y 1/
13.7
�.
Blankets
1st - 8Hr
2nd - 8Hr
3rd
- 8Hr
Target Avg = 80 to 120 Hood
Face Velocities
ime
700 A
1100 A
300 P
700 P
1100 P
300 A
Time
A
B
C
D
#4 Clarifier
9
9
17
q
Feet/Minute 1
#5 Clarifier 1
q
178
�i
`�
2
#6 Clarifier
—
•—
—
3
,

WWTP Laboratory Worksheet . Date: MAR 0 1 2018
BOD (24 Hour Composites)
Standard Method 5210 B
Time Put Up: 2'-F
Sample sourceNar. No.
Blank /52
Standard /54
Acid Sewer /168
Acid Sewer
Pri Effluent /56
Low Lift /58
LL Filtrate
Sec Effluent
Sec Effluent
Sec Effluent /60
Sec Effluent
Put Up By: TW
ml Sample
0
50 Seed/6 Std
30 Seed/3Smpl
30 Seed/5Smpl
5
3
5
50
150
200
250 /pillow
Initial D.O. By:
Bottle
No.
��
g,Qaf
j
G
1.;
5 Day D.O. By
LINLD.0ppm
YD.o.ppm
1 �/
.�r5
L
��.
7b
, 80
Time Analyzed` 1?30/�
SampleSource/var. No.
Blank /53
Standard /55
Acid Swr Dup A69
Pri Eff Filtrate
Pri Eff Dup /57
LL Dup /59
Low Lift
Sec Effluent
Sec Effluent
SecEff Dup /61
SecEff Filtrate
Date Analyzed: -L /
ml Sample
0
30 Seed/6 Std
30 Seed/3Smpl
5
5
3
4
30
100
200
300
Calculated By: f'
Bottle
NO.
WLD.Opprn
`-
; <
�3
/jam p
�: S
�"ILI
^�
,
Checked By: QC
5DayD.O.ppm
7�
7
�°`
'%
t
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: 01
40 Seed/6 Std
Time
NH3
DO
NH3
DO
NH3
DO
Time
NH3
Time
SFT
SFT
200 Seed/6mL Spk
Preserved By: ��.
7,
r.
i
7 AM
Z
2 Q
,3.
9 AM
10 Seed/0.3 Smpl
10 Seed/0.5 Smpl
SSo
Preserved pH: /.
3,
11 AM
1 PM
Checked By:
3 PM
5 PM
7 PM
9 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3 AM
5 AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
/ 7Z
7-05-
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time:
=A M
(24 Hour Composites,
2nd Source
verification std.
Time: ..
Time:
True
Filtered
Apparent (Unfiltered)
Std FOR
FOR
Time Analyzed: %f
Sample Source
100ppm
300ppm
900ppm
1500ppm
Low Lill.
Acid swr
SE 5AM
5AM Dup
5AM Avg
SE 11AM
11AM Dup
11AMMg
PE Turb
Pr Eff
PriC{Eff
Aerinf
LL
Acid Swr
Sec. Eff,
500
Blank
Checked By: FT
Sample pH
),0.41
q. 3
:-
'7,
0
6,7
©.
.2. 3
;
pH (24 Hour Composites)
Adjusted Color pH
7,
`7,
SE Avg
s%,
%
7(,�
(e
Analyzed By: : C'
Analysis ppm
303
997
15W
y67
7
4
/ _3J6
p
/ ?.Z
Q /
S l Z
211 I
Te
Calculated By: ..T 1 :.
X Factor
i
i
Analyzed By: : C .
Sample ppm
q 6
0�
Soo
C?
/
/` 3
/
1 3
. a
Q
/Z/
0
> `' t
Checked By:
'
Variable No.
62
63
67
64
324
329
22/65
23/66
171
172
173
174
37
103
108
141
144
355
357
164
87
175
Nitrate
Color
Color Calibration
Curve Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
SE Color Spike
11-lach
v
✓
DR 3900
Color Q.C.
Sec Eff P mg/I
0.4 7
p. &Z
417-
(a
The Analysts Initial. on This worksheet certify That
Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/- 10%
P-std mg/I
0,177
0,17
0,16The
Sample pH
#9017 Hi color July2017
S.E. Dup Diff<2.6mg/L
New Pump Setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
j�
D
r
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
V j;en
0y'
Jli► ?
Sample ppm
#9017 Hi_color_JuW017
Time Analyzed:
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
Analyzed By:
y'
`,3
Time
700 A
3°° P
T5 Avg
I.vaaster QC Signature: Or By signing this I verify that all QC parameters have been checked COD pH initial final
Checked By:
Pri. Effl
T6 Avg

WWTP Laboratory Worksheet Date: MAR 0 2 2018
Sludge
Volume Index
Composites
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd - 8 hr. Comp.
(24 hour Composite2Eff
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Low Lift Prim Effl Sec Effl
Low Lift Prim Effl Sec Effl
Low Lift Prim Effl Sec Effl
Prim Infl AS / PE
5 Minute
Sro
660
Time Collected
°�
r,�J
eV
zs-
.rs9°
t�
0 Minute
Zoo
god��,or81
Collected By:
XEt
Gov
JJB
���
avv
JJ
L=
�"
-�
,� �"�
VI 30
(24 Hour
Composites)
Total Suspended Solids Std Methods 2540 D
503
359
361
12
76
77
13
78
79
80
Recycle Sludge Solids
Time Analyzed: /S r-�
LL VSS
Low Lift
Acd Swer
Pr Effluent
Sec Eff
Sec Eff Dp
Dup.Diff<5.1
1000Stnd
Blank
Spike
Smp Vol=25
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Time Out:
Sample Size - ml
50
50
100
100
500
500
Blnk<.0004
50
0
500
Sample ID
Put Up By: j�
Filter ID
3 , 3yCo1
#1
AS
#2
#3
#3D
Std.900to1100
STD
BLK
SPK
Ft+skis gms
Weighed By: to
Filter + solids - gms
�(
v G
/s
f 3L
�� �/ r%
Sec Eff
/�_
r l � 7
Ft Tare gms
/ O7
/, /oGG
/ �
(�
TSS
pots
/os9
10117
Calculated By: L' '~
Filter Tare - gms
,3
/', �` '
f %
/. /l�
/. C� 7
. v 6
Avg. ppm
c �
u5)
TSS (x4)
y/o
VIM
�o'%�
Checked By: r- C ""
TSS ppm
x2
x2 %�
if
l5 f
�5 f''J
,�
Total Suspended Solids
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd
- 8 hr. Comp.
Suspended Solids
Waste Solids
Susp. Soilds Avg. 7 V52
Prim Infl
Prim Effl
Sec Effl
Prim Infl
Prim Effl
Sec Effl
Prim Infl
Prim EffI
Sec Effl
Sample Volume = 25ml
AOX Wkly Comp. Sec Eff
Sample Size - ml
50
100
200
50
100
200
50
100
200
Sample ID
Collected By:
Filter ID
PI 11PE
1A
PI
PE
2A
PI
PE
3A
Filter + Solids - gms
41667
Time Collected:
Filter + solids - gms
G
i /�
It If
/,7�
�. /
d0�
Filter Tare - gms
4 ,o x
Sample pH (Adjusted)
Filter Tare - gms
/ o99
/, /os
/, //VS
/, Nof
/ //7
yy
%47
/o
/, 9
Total Susp. Solids
SZG
Bkup Sample pH (Adj)
Total Suspnd. Solids
x2 qsa
35
/2 / F
x2 V?4
yz
/2
jx2 5
,5!;"
/2 a
Total Susp.Solids(x4)
I z/oy V50
Nitric Acid to obtain ph<2
y Conductivity
(Nixed Liquor Solids
Test Method: Std Methods 2510-B
Cell Constant
� , �f 3
Analyzed By:
Sample Volume = 25ml
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Sample Source (All Units umhos/cm) Time Sampled
Sample Temp °C
Sample umho/cm
Var.#
Cal umho/cm Conductivity
Crucible ID
1
2
3
Calibration 5000 umho std lr,71
2-Z..3
122
cjl��C, Q.C.
Crucible +Solids
Verification 1000 umho std
tl :csl"�
��.�'
r1�o
123
1000,2000,5000 +/-10%
Crucible Tare
/7. S//
' �1. 5IZ 8
/ Gyo7
Verification 14.9 umho std
r ' c�:� ��
/, /
124
14.9 std. (5.1 to 40.7)
Solids
91
S
v47
Canton
j[Z;
�', r
284
S.E. Dup Diff. <8.4 umho
Fiberville
/�'C; /f
1, l�
d+�?;,
285
Cell Constant 4.75 to 5.25
(x4) = MLSS
288
1352
Crucible +Ash
i7 g2o
t yss
13�
Sec. Effluent
:) �r
36,1
/
125
�,000, 2,000, & s,000 stds
Ash
93
0
Sec Eff Dup
�; yij4,1
C), %
/J j�
126
are purchased.
ppm Non -Volatile
37z
-360
v48
Sec Eff Avg
50, /
�''
286
14.9 std. Made from
M LVSS
0
l �f0 Mid Range 2nd Source FOR 2000 umho std � � ! r � 1 7—�, r C3 132 the 1,000 std.
Volatile
83, 0
8y 2
a
Blankets
1st - 8Hr
2nd - 8Hr
3rd
- 8Hr
Target Avg = 80 to 120 Hood
Face Velocities
700 A
1100 A
300 P
700 P
1100 P
300 A
Time
A
B
C
D
ime
#4 Clarifier
9
17
9
C%
Feet/Minute 1
#5 Clarifier
9
8At
C/ I
2
i
#6 Clarifier
--
--
_
—'—
—
31
1
1
1 -

VWWTP Laboratory VWorksheet Date: MAR 0 2 1018
BOD (24 Hour Composites)
Standard Method 5210 B
Time Put Up: yU
Sample SoumeNar. No.
Blank /52
Standard /54
Acid Sewer /168
Acid Sewer
Pri Effluent /56
Low Lift /58
LL Filtrate
Sec Effluent
Sec Effluent
Sec Effluent /60
Sec Effluent
Put Up By:
ml Sample
0
50 Seed/6 Std
30 Seed/3Smpl
30 Seed/5Smpi
5
3
5
50
150
200
250 /pillow
Initial D.O. By:
Bottle
No.
InILD.Oppm
�, l
r(J
, ON
1 I
l(
E
5 Day D.O. By 7':�
SDeyD.O.ppm
•'
!. �9
7
✓ : Z
-4
Time Analyzed: L
mple SourceNar. No.
Blank /53
Standard /55
Acid Swr Dup /169
Pri Eff Filtrate
Pri Eff Dup /57
LL Dup /59
Low Lift
Sec Effluent
Sec Effluent
SecEff Dup /61
SecEff Mitrate
Date Analyzed:
ml Sample
0
30 Seed/6 Std
30 Seed/3Smpl
5
1 5
3
4
30
100
200
300
Calculated By:_ --�,
Bottle
No.
InILD.Oppm
7
,.C'�
LL));7
d l
r
3, t%�
l
r /
y r•y
�r
V
Checked By: QC: r
SDayD.O.ppm
1 �/
!.
7/Ti
?J:
�W �i�
C'
J .
jI </
✓\ (V'
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved:
40 Seed/6 Std
Time
NI-13
DO
NH3
DO
NH3
DO
Time
NH3
Time
SFT
SFT
200 Seed/6ml- Spk
Preserved By: TL
1!
&,-
7 AM
Z ,
Z, l
9 AM
10 Seed/0.3 Smp3
10 Seed/0.5 Smpl
/
Preserved pH: /.
5
11 AM
1 PM
t�
Checked By: f #"
3 PM
15 PM
7 PM
19 PM
SFT
SFT
11 PM
11 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3AM
15AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time:
(24 Hour Composites)
2nd Source
Verification std
Time: ;j ',..
Time:
True
Filtered Apparent
(unfiltered)
Std FOR
FOR
Time Analyzed: / j
Sample Source
100ppm
300ppm
900ppm
500ppm
Low Lift
Acid Swr
SE 5AM
I 5AM Dup
5AM Avg
SE 11AM
11AM Dup
iiAmmg
PE Turb
Pr Eff
PriCIEff
Aerinf
LL
Acid Swr
Sec. Eff.
500
Blank
Checked By: .,-
Sample pH
0. r
71
72
2.0
7.3
7Z
o. /
�- �
"1
pH (24 Hour Composites)
Adjusted Color pH
%
7, ,
16
SE Avg
7,
76
2,
% (*
%' 4
7: (-
Analyzed By: ''t-
Analysis ppm
p/
/
1/9G
y�
/�(i
�0
/ '
7'I
//i
13/
3 GZ
57
b
Calculated By: •j�
X Factor
Analyzed By: _J&
Sample ppm
�D/
%
�%q
I %C.-
/�%� °
1`f�
NO
3
7
/1f3
31 1
33t L
2517.
U 1A67
Checked By:
Variable No.
62
63
67
64
324
329
22/65
23/66
171
172
173
174
37
103
108
141
144
355
357
164
87
175
Nitrate
Color
Color Calibration
Curve Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
SE Color Spike
Le -Adjusted
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
/ y/
3o
!OG
�..2G
The Analyst's Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/-10%
P-std mg/I
o
o
D. -0,
Sample pH
#9017 Hi_Colo� JuW017
S.E. Dup Diff<2.6mg/L
New Pump Setting
Q.C. Database
Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
e_
w
t-6
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
jj, 4�:f'
141)"1
1.1
Sample ppm
#9017 HLColor JuW017
Time Analyzed:
p.54�P
0.*,'
11AY
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
Analyzed By:
i
Time
700 A
3°° P
T5 Avg
(Master QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final
Checked By:
Pri. Effl
01
T6 Avg

WWTP Laboratory Worksheet Date: MAR 0 3 2018
Sludge Volume index
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd - 8 hr. Comp.
(24 hour Composites)
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Composites
Low Lift Prim Effl Sec Effl
Low Lift Prim Effl Sec Effl
Low Lift Prim Effl Sec Effl
Prim Infl AS / PE Sec Eff
5 Minute
4i0
6.sd
t6 30
63
Time Collected so 6�d 6VA ZAPt'��
ts�!' 0sf? /�; t;y ,� ow, P iOle/10 j 30 Minute
3�0 asd O gs-5
Collected By: Ec 8ov .1�6 �t6� aov
v,,� T =� zf7>°- SVI 30
w (24 Hour
Composites)
Total Suspended Solids Std Methods 2540 D
503
359
361
12
76
77
13
78
79
80
Recycle Sludge Solids
Sec Eff Sec Eff Dp Dup.Diff<5.1
1000Stnd
Blank
Spike
Smp Vol=25m
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Time Analyzed: 2 fle
LL VSS
Lodi Lift_
Acd Swer
Pr Effluent
Time Out:
Sample Size - ml
50
50
100
100
500 500 Blnk< 0004
50
0
500
Sample ID
Put Up By:
Filter ID
y16ou
_
#1
AS
#2
#3 #3D Std.900to1100
STD
BLK
SPK
Ft+Slds gms
/ toto
3
Weighed By:
Filter + solids - gms
,30
, /,
/. /.
�. / /
, (o . / D Sec Eff
1.16
/, /080
Ft Tare gms
i, /ayy
4 /103
�/Sf
Calculated By:
Filter Tare - gms
/?a
, IDLY-
D I a3. / /0617 Avg. ppm
/5 /5 8
A/ G GAMA
TSS
1094
11,0
!O / a
c) �0 2 —, vz�a
vs) TSS (x4)
yIyy �gGa t/vr/g
Checked By:prQC
TSS ppm x2 8y
2 & ..
x�f
Total Suspended Solids
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd - 8 hr. Comp.
Suspended Solids
Waste Solids
Susp. Soilds Avg. f6o$/ V52
Prim Infl Prim Effl Sec Effl
Prim Infl Prim Effl Sec Effl
Prim Infl Prim Effl Sec Effl
Sample Volume = 25ml
AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50
100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI
PE 2A PI PE 3A Filter + Solids - gms �,,� o Time Collected:
lter +solids -gms y //3A a8 i o
/z�r/ /. ,33 /. // B /o?•� Filter Tare - gms j, y Sample pH (Adjusted)
[FilterTare -gms !, iz32 i v �, ors 1, io
illro i, 38 • % y O oy Total Susp. Solids s Bkup Sample pH (Adj)
otal Suspnd. Solids x2 S y y /2 `08
3/ /2 G , I 58 /2 /0 Total Susp.Solids(x4) ��y v50 Nitric Acid to obtain ph<2
y Conductivity
Mixed Liquor Solids
Test Method: Std Methods 2510-B
Cell Constant
> 9�
Analyzed By:
fA
Sample Volume = 25ml
1st - 8Hr
2nd - 8Hr.
3rd -:SHr
Average
Sample Source (All Units umhos/cm) Time Sampled
Sample Temp °C
Sample umho/cm
Var.#
Cal umho/cm Conductivity
Crucible ID
1
2
3
Calibration 5000 umho std '. ,'l_': °
-17-1
7 ��C
122
d�c� Q.C.
Crucible +Solids
9zSx
-
q �o
8. rlv
Verification 1000 umho std /_,'� _,: , ,� `
C ' o'
C
123
1000,2000,5000 +/-10%
Crucible Tare
i9 8GG5
�4. I,/Z7
19,Gyos
Verification 14.9 umho std
' _
_
[
124
14.9 std. (5.1 to 40.7)
Solids
S87
4z
G
v47
Canton
2$4
S.E. Dup Diff. <8.4 umho
,./
i� l S•,
Fibervilie
1/`°;; �'• ` ; `
pr'
285
Cell Constant 4.75 to 5.25
(x4) = MLSS
ZS Y8
oZ 01a
Crucible + Ash
/9, F777
Z
8S'Y1
iis`
8 . GS/6
/06
Sec. Effluent
Sec Eff Dup
; 0 ! f
�c__; =`
,
, %
Zo17
125
126
1,000, 2,000, & 5,000 stds
are purchased.
Ash
ppm Non -Volatile
y
416o
4/3a
08
Sec Eff Avg
fit: ,!�
j),
;fir{6>
286
14.9 std. Made from
Mid Range 2nd Source FOR 2000 urn ho std r /� Z , (� 132 the 1,000 std.
M LVSS
Volatile
90,17
717
g • 8
Blankets
1st - 8Hr
2nd - 8Hr
3rd
- 8Hr
Target Avg = 80 to 120 Hood
Face Velocities
70o A
i100 A
3°° "
7°° P
11°p° P
3°° A
Time
A
B
C
D
i ime
#4 Clarifier
919
9
9
-/
Feet/Minute 1
9
is
8 %2
2
#5 Clarifier
#6 Clarifier
--
'i
"�
-
-------
3

WWTP Laboratory Worksheet Date: MAR 0 3 2018
BOD (24 Hour Composites)
Standard Method 5210 B
Time Put Up:
Sample SourceNar. No.
Blank /52
Standard /54
Acid Sewer /168
Acid Sewer
Pri Effluent /56
Low Lift /58
LL Filtrate
Sec Effluent
Sec Effluent
Sec Effluent /60
Sec Effluent
Put Up By:
ml Sample
0
50 Seed/6 Std
30 Seed/3Smpl
30 Seed/5Smpf
5
3
5
50
150
200
250 /pillow
Initial D.O. By:
Bottle
No.
mn.D.o m
c
02.
g,0q
1
/�
Q 1
/
`
•Q.3
19mt3
73
l
.07
�p
/ '
0. as
• �
� .oq
_ 7, y3 =
.�
CK0 -7
`
�
`'�
y3
6
71
5 Day D.O. By
eDeyn:
? 88
3:
3 /o
Y 7$
S, 5
S, oo
, c:3
Time Analyzed:
sample SourceNar. No.
Blank /53
Standard /55
Acid Swr Dup /169
Pri Eff Filtrate
Pri Eff Dup /57
LL Dup /59
Love Lift
Sec Effluent
Sec Effluent
SecEff Dup /61
SecEff` Filtrate
Date Analyzed: d1zly
ml Sample
10
30 Seed/6 Std
30 Seed/3Smpl
5
5
3
4
30
100
200
300
Calculated By: W f
Bottle
No.
INLD.Oppm
,Q5
631
�. O
�f
`
.0
.0�
8.-O'7
/ /
�
�y
l G.3�
,/
�Z
Checked By:
QC:
MayD.O.ppm
7. q/
3. 70
3.21
�,00
y 80
S. 39
7 69
S ov
7 o �
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: / la
40 Seed/6 Std
Time
NH3
DO
NH3
DO
NH3
DO
Time
NH3
Time
SFT
SFT
200 Seed/6mL Spk
Preserved By: '��,
�'ap
BOO
g - C30
7 AM
�,
, "
,
9 AM
10 seed/a.3 smpl:
10 seed/o.5 smpl
,
Preserved pH: 1,
3.51
11 AM
1 PM
Checked By:
3 PM
5 PM
7 PM
19 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpi
3AM
5AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
338
/(e
A9I
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time:
(24 Hour Composites)
2nd Source
Verification std
Time:
Time:
True
Filtered
Apparent (UnfiOtered)
Std FOR
EOP
Time Analyzed: /
Sample Source
100ppm
300ppm
900ppm
500ppm
Low Lift
Acid Swr
SE 5AM
5AM Dup
5AM Avg
SE 11AM
11AM Dup
11AMAvg
PE Turb
Pr Eff
PriClEff
Aerinf
LL
Acid Swr
Sec. Eff.
500
Blank
Checked By:
Sample pH
s:3
711
7.3
4r.4
!D•'f
.. If
19.3
pH (24 Hour Composites)
Adjusted Color pH
7.
,12
-7,&
%Lo
Sir Avg
17
7.4
Analyzed By: =rC.
Analysis ppm
is
q
p
qC
130
141
1 A"F
1
1 SZ
135
12g1
.231
q/
Calculated By: SL
X Factor
I
I
I
►
1
I
%
I
►
i
/
I
►
/
Analyzed By:
Sample ppm
S
Q
$'5(,
50q
1 qC2
3o
141
f��
/ -
i
15Z -
135
1.14
2 7i4
931
'i`
-7
Checked By:
Variable No.
62
63
67
64
324
329
22/65
23/66
171
172
173
174
37
103
108
141
144
355
357
164
87
175
Nitrate
Color
Color Calibration
Curve Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Deported
SE Color Spike
�
a.
V
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
o 1
.8.3
0
U
The Analyst's initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/- 10%
P-std mg/I
/ o 7
- y8
.1717
Sample pH
#9017 HL Color JuW017
S.E. Dup Diff<2.6mg/L
New Pump setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
Tc-
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
usQP
Sample ppm
#9017 HLCo1oL JuW017
Time Analyzed:
wo—pSulfide
UAddSwrSEProcess
1st
2nd
Eff Avg
Variable No.
180
Lo ColorHach #125
Analyzed By:
5Time
700A
300P
T5 Avg
.✓Iaster QC Signature: By signing this I verify that all QC parameters have been checked COD pH initial final
Checked By:
~"Pri.
Effl
0
0
T6 Avg

VWNTP Laboratory Worksheet Date: MAR 0 4 2018
Sludge Volume Index
' 2nd - 8 hr. Comp. 3rd - 8 hr. Comp. (24 hour Composites)
Composites 1st - 8 hr. Comp. p•
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Low Lift Prim Effl Sec Effl Prim Infl AS / PE Sec Effl 5 Minute
6!ro
70a
®
(9-S
Time Collected xtae 1 fq/ Z"io 16 nlp 10,'s f (�o �v� 30 Minute
170
Yao
1'/
Collected By: 101 T< 600, eEeF Gov ✓�6 �, cSVi 30
(24 Hour Composites)
Total Suspended Solids Std Methods.2540 D
503
359 361 12
76 77 13
78
79
80
Recycle Sludge Solids
Time Analyzed:
LL VSS
Low Lift Acd Swer Pr Effluent
Sec Eff Sec Eff Dp Dup.Diff<5.1
1000Stnd
Blank
Spike
Smp Vol=25m 1st - 8Hr 2nd-8Hr 3rd-8Hr
Time Out: Sample Size - ml
50
50 100 100
500 500 Blnk<.0004
50
0
500
Sample ID
Put Up By: isd Filter ID
f tj3a
#1 AS #2
#3 #3D std.900tol100
STD
BLK
SPK
Ft+Sldsgms j y
Weighed By: S {;5 Filter +solids -gms
/3�
, : �[� . / %
/%'� Sec Eff
, /a;
/ ©
Ft Tare gms o o i iosG �, l
� `1
= i0��
TSS
oy
>03
/d��
Calculated By: C !:' Filter Tare - gms
J%�
IX9
% �"E.%�� �?C! • lv �`�
x2
%: c?7?C� , 106� Avg• ppm
/5 /5 /0 `
(x2) D $ 1 — rc17-14
us) TSS (x4)
r7G ylf4 tir1�
Checked By: f C P-7-
TSS ppm
Total Suspended Solids
1st - 8 hr. Comp.
2nd - 8 hr. Comp.
3rd - 8 hr. Comp.
Suspended Solids
Waste Solids
Susp. Soilds Avg. yrJ V52
Prim Infl Prim EffI Sec EffI
Prim Infl Prim Effl Sec Eff I
Prim Infl Prim Effl Sec Effl
Sample Volume = 25ml
AOX Wkly Comp. Sec Eff
Sample Size - ml 50 100 200 50
100 200 50 100 200 Sample ID Collected By:
Filter ID PI PE 1A PI
PE 2A PI PE 3A Filter + Solids - gms 14 Xq Time Collected:
Filter + solids - gms , [ low 77 f.I fIr
1. /ii i/ a �� /0?047 %+ / / 9) Filter Tare - gms / o Sample pH (Adjusted)
Filter Tare - gms 1041 9t /, /0v7 / ss /10
d
/. //77 / / I 106 I l f '7 Total Susp. Solids 5 s- Bkup Sample pH (Adj)
Total Suspnd. Solids x2 /ry 3z /2 io x2 ltllz
y,f /2 7 jx2 ul- 8 /2 Total Susp.Solids(x4) V50 Nitric Acid to obtain ph<2
r Conductivity
Mixed Liquor Solids
Test Method: Std Methods 2510-B
Cell Constants
3
Analyzed By:
Sample Volume = 25ml
1st - 8Hr
2nd - 8Hr
3rd - 8Hr
Average
Sample Source (All Units umhos/cm) Time Sampled
Sample Temp °C
Sample umho/cm
Var.#
Cal umho/cm Conductivity
Crucible ID
1
2
3
Calibration 5000 umho std , ,! ti!`
7-2
122
jCA-0 0 Q.C.
Crucible + Solids
xt y q
81 0�
Verification 1000 umho std
�! J ,�%"+
�' . �,
r `
123
1000,2000,5000 +/-10%
Crucible Tare
S/oz
3J. yx,,g
Verification 14.9 umho std
%ram f ^
z.. Z
/- , Z
124
14.9 std. (5.1 to 40.7)
Solids
5-qg
G33
(0-3v47
$erve
Canton
' " ,
L
L
284
S.E. Dup Diff. <8.4 umho
Fibill
'i :: `%�
, "
285
Cell Constant 4.75 to 5.25
(x4) = MLSS
370
' 2S3Z
02 j �6
Crucible +Ash
� ^z p2is-
,.
< l • y s'
�
Sec. Effluent
' �t'y�
2.�.
125
�,000, 2,000, & 5,000 stds
Ash
���
/a
O
Sec Eff Dup
'+'•C'�2 /,yf";
z "g
% " �y
126
are purchased.
ppm Non -Volatile
y�z
yoy
8D
v4 8
Q-�
Sec Eff Avg
c , �'
Z' g'
1 '? C
286
14.9 std. Made from
MBd Range 2nd Source FOR 2000 umho std
��. { �/'�,
�,
,7�
t�132
the 1,000 std.
MLVSS
/9
zit?
O ��
Volatile 0 8Y o - ' /`
Blankets 1st - 8Hr
2nd - 8Hr 3rd - 8Hr Target Avg = 80 to 120 Hood Face Velocities
Time
700 A
1100 A
300 P
700 P
1100 P
300 A
Time
A
B
C
D
#4 Clarifier
9
1
Feet/Minute 1
#5 Clarifier
q
2
#6 Clarifier
--
—
3

VW11TP Laboratory Worksheet Date: LIAR 0 4 2018
BOD (24 Hour Composites)
Standard Method 5210 B
Time Put Up:
Sample SourceNar. No.
Blank /52
Standard /54
Acid Sewer /168
Acid Sewer
Pri Effluent /56
Low Lift /58
LL Filtrate
Sec Effluent
Sec Effluent
Sec Effluent /60
Sec Effluent
Put Up By:
Initial D.O. B y�
ml Sample
Bottle InILD.OPPm
No. 5DayD.O.ppm
Sample SourceNar. No.
0
r�
? 0#
Blank /53
50 Seed/6 Std
�4
Standard /55
30 Seed/3Smpl
frIt
V
! 5
3 y
Acid Swr Dup /169
30 ,,,Seed/5Smpl
,
Pri Eff Filtrate
5
Pri Eff Dup /57
3
LL Dup /59
5
LOW Lift
50
-71
Sec Effluent
150
Sec Effluent
200
!L
SecEff Dup i61
250 /pillow
I-�'7
f
SecEff Filtrate
5 Day D.O. By
Time Analyzed: ksp
Date Analyzed:
Calculated By: �}
ml Sample
Bottle IniLD.Oppm
No. MayD.O.ppm
0
�� �TJ r
Q
S, 3
30 Seed/6 Std
r /
3,?S'
30 Seed/3Smpl
r) e
3./l
5
�' i
`j y
`) �', �
5 /
��� t `�
� ' 5.03
3 r
/' % i. 1
(L (
S"Yv
4
-, -
��'`
30
w' 6
7 �
100
�." 1 l �1
k' �
200
/ 1
C�
~' Y. ?o
30�0''
7` ""
,�;95"
Checked By: r QC.
Ammonia
Standard /48
T5
T6
T7
T7
T2
Stripper Feed Tank
Sec Eff Spike /177
Time Preserved: 1? f'
40 Seed/6 Std
Time
NH3
DO
NH3
DO
NH3
DO
Time
NH3
Time
SFT
SFT
200 Seed/6mL Spk
Preserved By: �'C'
//
7 AM
9 AM
10 Seed/0.3 Smpl
10 Seed/0.5 Smpl
r
C�
Preserved pH: ��5
3. sl
11 AM
1 PM
Checked By:
7 PM
9 PM
SFT
SFT
11 PM
1 AM
10 Seed/0.4 Smpl
10 Seed/0.6 Smpl
3 AM
5AM
Chk Std
Pri Influent True Color
1.0
1 st 8hr
2nd 8hr
3rd 8hr
/9q
/22^
v7
Color
100ml prepared sample
Laboratory Control Std
Mid Range
Spectro Photometric
Time:: S -' 4
(24 Hour Composites)
Time Analyzed:
Sample Source
2nd Source
100ppm 300ppm
900ppm
verification std
500ppm Low Lift Add Swr
Time: 5 �%R�.
SE: 5AM 5AM Dup
5AM Avg
Time:
SE 11AM 11AM Dup
True
11AMAv9
Filtered
PE Turb Pr Eff PriC1Eff Aerinf
Apparent (Unfiltered)
I l_ Acid Swr Sec. Eff.
Std FOR
500
FOR
Blank
Checked By: .,.-
Sample pH
�1
,S
7i
Z
7
7-2-
10 r
a.
pH (24 Hour Composites)
Adjusted Color pH
} . 4
%.
SE Avg
(�
(�
, 6
7. 4,
7' t,'
.
Analyzed By: ,j '
Calculated By: 'C
Analyzed By: I C
Analysis ppm
X Factor
Sample ppm
q,7
;�9
.2 1Y
$g
6,og-
OL,
I
K.
$
r
12q
JAI
I Aq
1 RIqq
I
G
t 31
133
3 3
31 I `-i`
IY
5
Q35
ff 3
/ `�
r'
Checked By:
Variable No.
62
63
67
64
324
329
22/65
23/66
171
172
173
174
37
103
108
141
144
355
357
1 44
87
175
Nitrate
Color
Color
,s
✓
Calibration
Curve
Dates
Phosphate
1st
2nd
3rd
Avg
NPDES Reported
SE Color Spike
Hach DR 3900
Color Q.C.
Sec Eff P mg/I
0.4v
a 6/
r 6
1 6-
The Analysts Initials On This Worksheet Certify That
The Analyst Has Done The Test To His/Her Ability
Sample Source
Spike
S/N 1455680
All Stds +/- 10%
P-std mg/I
lot
/,00
A 'aJ?
Sample pH
#9017 HLColor July2017
S.E. Dup Diff<2.6mg/L
New Pump Setting
Q.C. Database
Adjusted Color pH
Lo Color Hach #125
Test Method: NCASI 253
pH Grab Samples
LL
Acid Swr
SE
Process Control, Instrument Calibration
and use
Analysis ppm
Hach DR 3900
All Except PI New True
Collected By:
7C 1
: T(,
Cr g
X Factor
S/N 1505038
PI New True: NCASI 71.01
Time Collected:
/
100/1
J1�
Sample ppm
#9017 Hi_Color_July2017
Time Analyzed:
Cti'1
JAY
OS?
Sulfide
1st
2nd
Eff Avg
Variable No.
180
Lo Color Hach #125
Analyzed By:
�'G.
3G
Time
700 A
300 P
T5 Avg
Master QC Signature: P r-By signing this I verify that all OC parameters have been checked COD pH initial final
Checked By:
f
Pri. Effl
10 `
T6 Avg