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WQ0009477_Residual Annual Report 2020_20210212
Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* Annual Report Year* Permit Number (IR)* Applicant/Permittee Email Notifications ........................................................................................................................................................................ Does this need review by the hydrogeologist?* Regional Office CO Reviewer Admin Reviewer * Annual Report * Residual Annual Report r Additional Information r Other 2020 WQ0009477 Cascades Tissue Group - North Carolina, A Division of Cascades Holding US, Inc. r Yes c No Fayetteville Submittal Form Project Contact Information Rease provide information on the person to be contacted by NM Staff Name * Karen Bellamy Email Address* Karen_Bellamy@cascades.com electronic subnittal, confirmation of receipt, and other correspondence. Phone Number* 19109958292 Project Information ........ ......... ................................................................................................................................ ......... ............ .... .... ........ ... ... .... .... .... ... ... ... .... .... .... ... .... .... ......... ...... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00009477 FPas Current Existing permit number Applicant/Permittee Address* 805 Midway Rd Rockingham, NC 28379 Facility Name * Cascades Tissue Group DCAR Please provide comments/notes on your current submittal below. Cascades is submitting our Land Application Annual Report as requested . If you have any questions please call me at 910-995-8292. Karen At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Rc.) Cascades Land Application Annual Report 2020 12.88MB signed.pdf Upload only 1 FLFdocurrent (less than 250 W). Witiple docurrents mist be combined into one RDFfile unless file is larger than upload linit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/12/2021 Cascades Tissue Group — North Carolina A division of Cascades Holding US Inc. 805 Midway Road, P.p, Box 578, Rockingham, NC 28380 USA Cascade Phone: (910) 895-4033 Fax: (910) 895-9887 www,cascades. com * Into@Cascades.com Date: Feb 1 ,2021 To: State of North Carolina Department of Environment and Natural Resources Division of Water Quality Aquifer Protection Section Land Application Unit 512 N Salisbury St. Raleigh, North Carolina 27604 1-919-807-6300 From: Karen Bellamy-ORC and Preparer of 2020 Annual Deport Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. 805 Midway Road Rockingham, NC 28379 1-910-895-4033 EXT 74280 1-910-895-1877 Fax Karen B211amyOD Permit # WQ0009477 Subject: Land Application Annual Report Cover Letter Forms Included: Cover Letter and Compliance inspection Letter from DEQ Annual Land Application Certification Form DENR Form ACF Elwood Black PH D Letter on Field Application Elwood Black PH D Pan Calculation for Cascades Biosolids Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, Dry Tons, Dry tons per Acre, Long and Latitudes DENR Form DMSDF and Additional Supplemental DENR Form RSSF DENR Form RSSF-B Lab Results TCLP, Ignitability, Reactivity, & Corrosivity DENR Form PVRF 2T Letter on Vector Reduction Page 1 of 2 If K Soil, % Solids, Acres, Wet Tons, Subject; Land Application Annual Report Cover Letter. Cascades has 1 ORC and 2 Backup ORC. Karen Bellamy ORC and ( Corey Wyand as Backup).We have more employees signed up for Backup Training at NC State for 2021. Field Inspections where conducted, equipment calibration, PM work on equipment and ORC and backup ORC performed required inspections for the year_ Corey Wyand, David Sheppard and Karen Bellamy attended Rural Water Association Training in 2020 for our Continuing Education Contact Hours. Dr. Elwood Black continues to work closely with our land application Program. Advanced Residuals had No incidents in 2020. 2020- Challenging year with rain levels being high again this year. Cascades has received the New Permit for 2021. Cascades and Advanced Residuals has worked hard to make sure we have a good program that is Environmentally Friendly and also benefits the farmers. We have gotten a lot of positive feedback from farmers. Duke Goodwin is the Project Manager for Advanced Residuals project at Cascades. Mr. Goodwin has been a farmer for several years and also has worked at the City of Rockingham WWTP, so he is very familiar with regulations. Duke Goodwin also received his certification for Land Application in 2016 . Mr_ Goodwin also received his continuing Ed hours for 2020. Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also been removed from our permit, since levels have been extremely low for over 10 years. We also have testing performed by Department of Agronomics. so the farmers can have access to information. ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0009477 County: Facility Name (as shown on permit): Richmond Year: 2020 Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Land Application Operator: Karen V. Bellamy Phone. 910-895-4033 Fxt 74280 LuLs�n application of residuals its Allowed by the permit occurred during the past calendar year? 'es ❑ No - If No, skip Part A, and Part 8 and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Re±a duab; Annlientinn %immnrv- Total number ofapplication fields in the permitj Total number of fields utilized for land application during (lie year: Total amount of dry tons applied during the year for all application sites: 1 22623,12767 Total number of acres utilizes for land application during the year: Part B - Annual Compiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land applic tl�on permit (including but not limited to items 1-13 below) issued by the Division of Water Quality, U� Yes ❑ No If no please, provide a written description wiry ti►e facility was not compliant, the [fates, and explain corrective :action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in I5A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .11 1 1 were complied with (applicable to 40 CFR fart 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Karen V. Bellamy Environmental Manager Perini#tee 334ame and Title (typeAor print) Signature of Perm Duke Gain Date ofPreparcr* Date SignatureLand Ap (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR fart 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) February 1, 2021 Cascades Tissue Group P0I3 S 78 Rockingham, NC 28380 Attention: Karen Bellamy Dear Ms Bellamy; From January 1, 2020 thru December 31, 2020, FiberClay was distributed only to agricultural land. No farm field received FiberClay in a continuous year-to-year application as defined by the North Carolina Department of Environmental Quality respective to permit WQ0009477. These statements are based on information reported by Advanced Residuals Management. Sincerely: Elwood Black, Ph.D. - Soils Karen Bellamy From: Eblack d)nc rr.eorn Sent Wednesday, February 19, 20201:47 PM TO., Karen Bellamy Subject PAN calculation The Plant Available Nitrogen (PAN) calculation is widely used to estimate the N that will be available to a crop from the biasolids. The carbon to nitrogen ratio in biosolids is commonly less than 20:1 and net mineralization of N frflm the biosolids occurs. For materials with a C:N of less than 20:1 the PAN provides a good estimate of the N that may be available to the plant. However foe materials like the Cascades sail additive r which have a C:N greater than 30:1, the PAN calculation is nit appropriate. Instead of mineralization, N immobilization occurs. As a result farmers need to apply additional N to off set the N that will be immobilized as the soi[ rn icroorga nis rns assirnilate the fiber. The PAN should be 0. r Elwood Black, Ph.D.-Soils Sent from my iPhone Cascades -ATTENTION: Ce ccuMel provient de I'exterieur de Vorganisation. Ne pas cliquersur les liens et ne pas ouvdr les pieces jaintes sauf si vous reconnaissez l'expeciiteur et que vous etes sur q u e le contenu est [egitime. Cascades - CAUTION: This email is from outside the organization. Do not click on finks or open attachments unless you recognize the sender and you are sure the content is safe. - .1 k IIw�d 2420 I J. sell Foie tans T .a .W-U.rpgy Fdna Fall6 fv I Fmv MT r _ N Ao - PYr C I Ll- I Jan Goon I I I I I I I I .--_ i1t`N' I 8�r0T4 1.52Pi�?#F Card RQ ILCO I FCC Yx k-ra 2.r.Ys, NP.YL`-1 #?.i1176 3f? 3..Syi - -'--- TA'MN 3F -- SLJ 7Pid7G¢ I JW54.353N 8032M W I M&Goa Rd Monroe M28112 NEW 829.idS4 1.TSa77d2Sa 415+. FiC 4YF,Y€. 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Y➢ iF,=p7F 98 � s3Js�7d f.Rr d 13s u-345.ti co -..:gyro I I F 14a545.5[ 1— Ch—1 rd, rlerwaod, \C 2fi128 ;'EYJ 1dYrdfiG77 �.r5drF3� Oxrm 4'#9.� RC A YS,NP, 4'OS 4l.2094 113 2PA76 ?3237Ti7 i,1b17SB3 3[3593374791i4135\' I 192TC-,r `Rd R1 .ind, k+C HUM I N[44r 1TfJ�2P2d rLss'3`r]Fr ';.W,u[IRwvJs fiJ3L Raw12avzm 0.5' JiIC NIfrYW,N F,NS,NP, 5'D t4.2M6 105 34s Sr 7?#di6So 1 i-f6i6,7*�C13T - - 34 ii T71N 79 id_OSM 1 I '2'221 Pw—Cr- zrd Sld_ YJaerr., NC 2F:395 I I F lifdW702U 0ma5s"Jd J4WaJnWs'J6 F3 fi47 RJdn 1b AC N1[NW,N F,NS,NP 44.WU 72 4&.#F 21.91455 0Mssa5ai - I I34 io_i 1CN 79 aTO31'J _ -- M221 Peach Clmh rd Rd.W1 r4 NC 21.395 I r i}214 e1027 r.f33S6S5d3 AL-"FJw':rt RC Y!}' FPS -A. 6 is 96.291im i. r&u I 12457_R7dN 79 Z3-21p1Y 7H225 Peach Orchard Rd, Waeram, FJC ZU95 Now- 21 I I I I I �Forrtlh 4725"M A9N&BLIA'P I P,a3 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Q PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, adivision of Cascades Holding US inc. PHONE: 910-8954033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): L] Syrr#'ace Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part Cj Distribution and M -eting (complete Parts A, B. and C) Was the facility in operation during the past calendar year? Yes QV NO ❑ If No skip parts A, E, C and certify farm below Part A*- Part B*- i4farsth Sources(s) {include Nl'DES # if applicable) Volume (dry tans) Recipient Information Amendment) Bulking Agent Residual In Product Out Narne(s) Vol ume(dry tons) Intendeduse(s) January WQ0009477 2124,991 12 2124.991 I2 See Attached 2124.99112 Agricultural February WQ0009477 2227.35856 2227.3585.6 2227.35856 Agricultural March WQ0009477 2033.86990 2033.86990 2033.86990 Agricultural April WQ0009477 1753.89875 1753.89875 1753.89875 Agricultural May WQ0009477 1982.33568 1992.33568 1982.33568 Agricultural June WQ0009477 1814.16634 1814.16634 1814.16634 Agricultural Jaly WQ0009477 1941.779I0 1941.77910 1941.7791 Agricultural August WQ000477 1882.82157 1982.82157 1882.82157 Agricultural September WQ0009477 1316.40561 1316.40561 1316.40561 Agricultural October WQ0009477 1953.37324 1953.37324 1953.37324 Agricultural November WQ0009477 1503-28000 1503.28000 1503.28000 Agricultural December WQ0009477 2088.94780 2088.84790 2089.84780 Agricultural Total from FORM DMSDF (sap) 0 22623.12767 22.623.12767 22623.12767 Totals: Annual (dry tons): 0 22623.12767 22623.12767 .. :: ::. .. _ :: :: 22623.12767 Amendment(s) used: Bulking Agent(s) used: If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit Yes (including but not limited to items I-3 below) issued by the Division of Water Quality: ❑ No 10 If No, Explain in hlarritive I. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements %sere compiled with or, in the case of a deviation, prior authorization mm received frorn the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of low, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 44 Signatyt/e of Permittee Date Signature ofPreparer** Date (if different from Permittee) **Preparer is defined in 40 C1±R Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM DMSDF (1212006) CLASS A ANNUAL DISTRIBUTION AND MLA R_RFTINGI SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information Q PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina , a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY- Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): ❑ Su Ace Disposal (complete Part A - "Mantk", "Source(s)" and "Residual In" columns only) istribution and Ntarketing (complete Parts A, and B) Month n Part A*: Part B*: Sources(s) (include NPDES 9 if applicai}le) Volume (dry tons) Recipient Information Amendment/ Sulking Agent Residual In Product Out Narne(s) 'Volume (dry tons) Intended use(s) WQ0009477 139.27114 138.27114 L'vlaare Brothers I38.27114 aR WQ0009477 709.01297 708.01297 Jamie Caudle 708.01297 ag WQ0009477 222.18945 222.18945 Lacy Cummings 222.19945 aQ WQO009477 21.76419 21.76419 Bobby Davis 21.76419 ag WQ0009477 105.35371 105.35371 Mitch & Garrison Farms 10535371 ag WQ0009477 173.41751 173.41751 Lenivood McFarland 173.41751 ag WQ0009477 149.99229 149.99223 RogerOxendine 149.99229 ag WQ0009477 41.66239 41.66239 Charles Richardson 41.66239 ag WQ0009477 523.36109 523.36109 iwlark & Lynn Thomas .523.36109 ag WQ0009477 20.87176 20.87176 Jerry Thigpen 20.87176 ag WQ0009477 20.09462 20.09462 Cox & Watson 20.09462 as Feb WQ0009477 282.2.7016 WQ0009477 105.43064 WQ0009477 11.57344 WQ0009477 63 3.76384 WQ0009477 81.89672 WQ0009477 50.34824 WQ0009477 97.45856 WQ0009477 173.20512 WWO09477 11.86608 WQ0009477 157.21736 WQ0009477 305.29904 Totals: Annual (dry tans): 0 4035.34032 Amendment(s) used-1 Bulkin * If more space is required, attach additional information sheets (FORM DMSDF (supp)): 282.27016 John Bass 105.43064 Bruce Cuddy 11.57344 Alfred Davis 633.76384 Bobby Davis 81.89672. Tyler Davis 5034824 Cove Dove 97.45856 [Mitch & Garrison Farm 173.20512 Bill Hardin 11.86608 Jimmy Hunt 157.23736 Kirmet Locklear Lee GradX Locklear 305.29904 403 5.3 4032.. . 282.27016 ag 105.43064 ag 11.57344 ag 633.76384 ag 81.89672 ag 50.34824 ag 97.45856 a� 173.205I2 ag 11.86609 ag 157.23736 305.29904 a aQ 4035.34032 :. ... .. . Total Number of Farm DM SDI;` (Supp) 7 DENR FORM DMSDF (Supp) (1212D06) CL A ANNUAL DISTRIBUTION AND MARKETLNGI SURFACE MSPOSAL CERTIFICATION AND 5 UNINTARY FOR -let S¢pplemental Information WQ PERMIT N: WQ0009477 FACMITY NAME: Cascedes Fissuc Group %Orth Ca ohm . a Lbuion of Cascades Holding US line. PHONE: 910•39.54033 74280 COUNTY: Rldeaodd OPERATOR: Karen V. Bellamy FhCFLFTY T3`PE (pbmse eberk me): Surface Deposal (complete Part A - "Month", "Source(sj" and "Residual Fa" ca[umns only} X Distribution end M ateeum fmmmlcle Paris A. aad M Part Al: Part S'; Sourcesfi} {include N K)E5 N of applcabe) Valuoac (dry tam) RedplearloNrmation AmemdmeW Mdki� d Residual In Product Qtems} Vakffw {dry tons) Imended aefs) WQGW%77 8f_00464 8L00464 BRIVOtten&eJr. SI-09464 ag WQ0009477 89.42D4 89.4204 Lwyo endime 119.4204 a WQEWR477 14MS432 14633432 RagrrO=dim 146.59432 a 317.D3 afar WQ0009477 135.2221 135-Mi Ro rOxcadinc 1_ 135.232[ a WQDD09477 W-1333 10.8933 €hHs Rid;rdsom 10-M33 ac WQ0009477 30.0835 10.0835 Hark & Lvttn Thomas 1D.DS35 ac WQCHM477 2I IA74DD 211.47490 Glee BuHwd 211.47406 BA WQDOM77 41.03630 44.03630 Lrtrie Candle 41.03630 WQDOD9477 42.94950 42.84950 Cox&SYadson 42.849M WQDOW477 3-n.67670 329.67670 MCC caddy 3'_�9.67678 as W00009477 77.72600 77.72680 AMA Davis 77.7mw Mr- WQ0009477 109.23290 109 2329D Bob4, Davis 109-23290 as WQ00119477 05.19310 S5.39370 LvleFlovd 65.39370 ap 14Q0009477 65.9663 65.9663 wcnMI]ecobs 65.9%3 ar WQ0009477 293.1132 293.1 L39 Jennie Ko nig 293_ 1118 %`Q000,A77 76.6919 76.68I9 HMMY Lacldear IT. 76.6914 as WQ0004177 2f.457U0 2IA57N KinnclLoeklear 21.45700 9PQ00f14377 105-5703 105.3M3 LXt G 11"%;ry L05.8743 a WQ0069477 114.9218 114.92IS Eddie Marcss 114.4218 n WQK09477 191.8101 191.8101 Mikt McCormick I91.9101 e V19Q0D09477 31.261 31. h61 ❑srisitt M4itehel 31.261 ar V1`Q0009d77 76.2989 762U9 L}nnLoclfear 76.24M ;ig 3;E Tota[sc Artnnal(dry low). 0 23%.87926 2350.S79F6- :lrtrcndmrngs) used: 8o1kin8 .NSrtti(s} used: 1! mom space is ttquired, aita.cb ad[ dmal infamffLm sheets (FORM Dhi5F}F (supp)): Toia[ umber aCFarm DhdSDF (Sapp) CLASS A ANNUAL DISTRIBUTIOlti AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplementa I Information 1VQ PERMIT ft: WQW49477 FACILITY DAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc_ PEIONE: 910-8954,1333 74280 COC:N'CY: Richmond OPERATOR- Karen V. Bellamy FACILITY'n-TE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual 10" eolum os an [g) Distribution and Ma rketing (tomplete Paris A, and R) Part At: Part 13*: Month S-ources(s) (include NPDES f if applicable) Volume (dry tons) Reeipient In€ormat9on Amendment! Bulking Agent Residua[ In Product Out Narrre(s) Volume (dry tons) Intended use(s) a ril WQ0009477 125-69295 125.69295 Keith Chriscoe 125-69295 ag WQO-009477 176-40700 176.40700 Eric Clapp 176.40700 ag WQH09477 130.04595 130.04585 Adam Cooke 130-04585 a, WQM09477 IN-66055 108.66055 IiarleyDavis 109-66055 ag QDM)477 2(1-3741D 20.37410 KirmetLocklear 24-37410 ag WQ0009477 125-4322.5 125.43225 Eddie Manes t25.43225 ag AIQ0009477 139.32835 139-32935 lames Manes 139.32835 ag WQDfl09477 31I-09805 31[.09805 Jeff Manes 31I-09805 ag WQD009477 147.6747 t47.6747 Jahn Maynard 147.6747 ag WQ0009477 30.50.585 30.50585 Lee McFarland 30.50585 ag WQ0009477 40-6376,0 40.63760 [ envwnod McFarland 40-63760 as WQM09477 19-67495 1:9.67495 lawOxendine 19-67495 ag )AIQ0009477 398.06890 199.06880 Duarte Strider 198.066880 ag WQX09477 180.29775 180.29775 Steve Williamson 180-29775 ae 17 8:89875 M2V WQ0U09477 451.78048 451-78048 Joe(Bobby)Allen 451.78048 ag WQ0009477 60.49205 1 60.49208 Ruben Byrd 60.49208 ag WWO9477 85.74552 85.74552 lames Cagle 85.74552 ag WQM09477 92-16912 9116912 Dylon Chriscoe 92-16912 ae WQM09477 63-37528 63.37528 Keith Cbriscoe 6337528 ad WQM09477 291.74168 291.74168 1, Eric Clapp 291.741-68 -a ! WQX04473 30.03616 30.03616 1 Harley En -is 30.03616 ag Totals: Annual (dry tons): 0 2829.23907 2829-23907 2M.23907 - Amendmeni(s) used:[ Sulking Agent(s) used: *If more space is required, attach additional in formation sheets (FORT+! DMSDF (supp)): ToW Number of Form DMSDF (Supp) 7 CLASS A ANNUAL DISTRIBUTION AND MARKEnNG! SURFACE DISPOSAL CERTIFICATION AND S3.174'l743ARV FORM SnpplemCM21 lnfarlatiGM 1VQ PERAM N: W-00 09477 FACILITY NAME: Cascades Tissue Gromp-Pforth C=Wim . a dkisian ofCwzads Ho[dmg US Inc. PHONE: 914-895.4033 74290 COUNTY. Richri nd OPERATOR; Karen V. Bellamy FACILITY TYPE (please check one): Surtarc Disposal gcompkTc Pnrt A - ^ifonth". "Snurce(sp' and "Reskud in" enlumns Gulp} L7imributiao and 11nrl:eiine fcGMTtlete Part! A. and RI Part A•; Part R*: hlGnrh Soarces(s)(iaclmdeMMES4if nppliramej Volume filry tom) Reciydmt leformatitm m Au dmem' BLUng Agwi ResWuA lm Pmdud Cim Name(s) Valume(dry om is) lm[emled mse(s } %lav Cum onued L09.54040 3D9.54040 RagcT "rik 109.54040 WQCW9477 1 6231952 62.31952 Seth Lmcas 61.3195.2 ac SYQ0009473 64-47768 64.47763 EMdcMancss 64-47769 eL WQW09477 41.2N56 JeFfManess 4120956 ag WQM9477 53.65296 Johtm • Ma%mard 53.63M�WQN09477 57.6&5?0 Dmny0.Qmimn 57ASSA ag WQN09477 k41.20856 257.8428S DuawSaidts 257.84288 ag WQDOD9477 239.76352 Slew Wil)®asuo 239-76352 ag Wr,*QD 477 20.50464 liamhew•lAidca 1050464 ag June WQ(IOM77 47.29156 47-N156 Moth ew'Wickm 47.20L56 ag WQMD9477 w 50.5.1* fae{SGbby] Aflcu 50.54700 ag WQU "477 3344 403.53344 ScolEy Men 4M-M44 ag 0760 119.60760 Ruhat Byrif I k4,OM ag WQ-3009477 819 57.708[8 F'raC&icCagle 87.7m18 a& WLpDD9477 9964 170.69864 Dykm Chriscoe 170.69M4 aC WQODD9477 739 98.3738 Eric Clapp 99.3738 as WQOD09477 1%2?3.69271 5596 379.05598 &mce Cuddy 279.0559S ac WQ0D119477 272 273-692T2 KyleGilli 'e 273.69272 ae WQOD09477 j 1141 SL4943 Seh Lucas 55.4843WQON9477 92 9.57392 LemmmdhlcFar[std 3.87392R'Q0009477 342 59.91342 Errs hldmtis 59-91342WQo004477 578 350.47578 leslySmrmd11 15GL47576Towts: Am Wi (dly laud: 16L7 2723.1617 2321_I617 -L g .4genl(s) itse& I I MOM space 35 regmtrea. ffi7nch a(Edtirooal wtorroatrao sheets CFUR'47[]SiSI?F lstspp)J. TGeal ltiumb= ofFarm 1714SDF(Smpp} 7 CLASS A AI�'i UAL DISTRIBUTION AND MARKETING1 SURFACE DISPOSAL CERTIFICATION AND SLYINMIARY FORM Supplemental Inform fi❑ n RWQPER-,SITH: WCNW9477 FACI]1TYNARM CW48desTtmtCiroup-brardiCArolina_odivWmofCascadesHalffyUSTno_ PRONE 9 10.M4433 7428C COUN- Y. Richmond OPF,30.7 }R: Kam V. Bellamy FACI):= TYPE (pleuue chtclk uric): Su rFnre dirMul (cornplefe Para A - " MontWl, "Souroe(a}" and "Residual In" calutons only) Y D'a[63mriern amd Mzrlcc6nz (cnmoktt Prins A. And 31 --Pm,i A•: Part B•: 41oulb 5aurcc(:,)(indodeeNPUESNif Ppika ) Volume ldrvtons) Recip6ekt Information AmeadntrnU]iulkim g AN Residual In Produce Out Nis) Vol1woc(dry ]aLeaideduse(s) July XVQ0009477 10.99245 10.99245 JegMeb •).•l3[em 10.99245 ac WQ0009477 702.7251 703.725[ Scony Alkn 7027251 29 WQND9477 93.5"50 93,56854 RegoeBar5eld 43.5450 ag WQO009477 107.3319 307.3319 Gatm3mi.-nan ]R73319 n WQM04477 137.199 137.199 EricBwmk 157.194 ag WQOOD9477 42.35595 42.35595 FrmfacCack 4235595 ag WQOOM77 72.4L445 72.4144S O®nnyGriggs 71.41445 ag WQOOM77 161.45M L61.45895 Brim F[nadlad €61•45$95 ag W{4COu9477 189.37715 L89.17715 FrankluE Lee L89.17715 89 WQM09477 390.85405 290.8505 Bobby RkMudsori 290.85405 rib WQCDD94-n 102.82530 L02.82534 Duane Strider LO?8253if ag WQOO"477 11000.59162 30.6763p 30.97630 Awao WwW 34.87630 a Au" WQ00H4-n L54.42074 154.42070 3ordao Carroll 15442070 aG WQODL19477 14.52324 L0.52324 EirMetkinis LOS2324 ag WQOD 94 7 911.67W 98.67809 ltrry Snead 98.67809 as WQON9477 103.67952 ]p3.67952 Uy Wluttkn 193dr7952 ag WQOW9477 514.9090 51492840 TornmyWlOramgae 514.9294 at 9vQ00O4477 IN03916 8abbyRichardsm J00fiS91G7 ag f a[ais Asmaal (dry low): 0 M24.W67 3824.60067 382i.60067 ': }Lalel]dlritdltl5} n9td: Balking, Agent(;) aged- • 1Fmpre space is eequuetl, aAaeb addin=al iofamoatim slimu4FORNT DMSDF(sapF)} Tuial Number ofFaem DMSDF(Supp)� CLASS A ANNUAL DISTRIBUTION AND MARKE:TINCI SURFACE DISPOSAL CERTIFICATION! AND SUN ARY FORM Supplemental Information WQ PERMIT It- WQ00D9477 FAC€LrTY NA,%[E: Cascades Tissue Gmup-.'tiath Carolina, adi%isioe ofCasrades HoWingUS Inc. PFICN 910-895a4033 74290 COUNTY; Riclu[tpnd OPERATOR: Maren V. Bellamy FACWT1(TYPE (pleeoe check one]: Surface Disprmul (mmp[ele FartA - "i4fuotV, "S*Lmn(s)" sad "Rasidua3 In" caEumns only] k 1..,.....j. n--.. % ....a " Pall S•: 3fonlh Swaces[s} (iodsde rVP➢ESSif atr}dics6[ej 1'dome{d tamsl Reci ieetlu6oamafioa Ameodm W Hadlivg Agent BesidoW hi do Cw 1Varns s} Vol (dry tons] Intended use(s) 5e t WQM9477 293.58738 293.59M Adam Causcv 2DJ39738 ac NQ0009477 116-71939 [16.7[839 JamicCawgc 116-71839 at,, WQM9477 52.33356 52.33356 Adam Cooke 52.33356 ac WQM9477 517.13DT9 1 517.130E9 Frank3Aowey SE7.13419 a F 1YQDW9477 336-63W9 336.636D9 T=my William-soa 336.63mg ag Oct WQD009477 t L0.76455 110-76455 Kevin 13n=ca 110.76455 ag WQNM77 9-78484 9.3a484 JordanCatsoil 9-79484 ag WQM9477 256.34427 256-3442.7 Jamie Caudle 256.34427 BE WQMD9477 137.19732 137-1.9732 AdmmCausaw €37.19M I ag WQNDA77 105.84795 105-84795 Charles Helens L05.84795 ag WQMD4A77 96-21222 96.21223 FmftkHowey 96-21M ag WQDOM77 461.f7305 4-61-17345 6n4e.Ktmh 461.173D5 ag WQDOD9477 274.40673 274.40673 Franklin Lem 274.40673 ag WQMD9477 9.22970 9- 2870 Eric }.telmUS 9.221170 ag WQOOD9477 161.61912 161.61912 EriamPucknt 16t-619€2 ag WQ119D9477 4D.9951 40.9951 CecilRatsiosna 4,11985L kv WQ*0M77 137.2T389 137.27339 Jar= Smith 137-MlW as WQGDD9472 97-38249 87.38M49 Jerry Snead H[ MM749 ag WQM9477 65.15301 65-15301 Tommy Wi3linmspn 65.15301 ae Tatalse Atmual (dry tons)t D 3269.77985 i?G9.37885 ?? : ' ' `'-':-:-.. - .-.•.-.:-: -.. 3364-773a5 .. . . aanendmenl(s) Used: ]3uLimg A mqs) used= ' [furore spates i5 required anach additiaaat information shuns; FORM Dh4SDF (sum)): Total Number of Futm DMSDF (Sapp) CLASS A ANNUAL DISTRIBUTION AND NU RI{ET[1 Gf SURFACE DTSPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ 7LAMIT 11: WQ00D9477 FACILITY NAME: Caecadei7iiuuc Group-LNwh Carolina, a di%isem ofCascadu Holdingll3 Ear - PHONE: 9ID40.54(F3.3 742M COUNTY: Richmond OPERATOR: Karen V_ 80emy FACIIS1V TYPE (pRasc eltcckone): Surface Dispnaal (rompFetePart A- "Maoth", "Suurce(s)" and "ResidnsE fa" oalemns only) Disirihndon and Marketine (comolete Parts A. a" BI Part A`: Part B": monthSoorery(s) (�elode NYD3 5 # if ¢pplira6k) VakFme (dry tow) Rea 'ear Information Amendrnend Bulking Agem Residnal to Pmdue] Oot .4amc(s} VaEorne (dry tans) ]nteoded cse(s) typV_2D WQOOD9477 10_k91 10.193 AdamCsusey 10_E91 ng WQOOD9477 52.7433 52-7438 Adam Cooke 52.7438 ag WQGOD9477 1".47280 INAMO Kevia Bascom 104.47280 ag WQWD9477 737.08H 1 737.W88 Franklin tree 737.0E398 ag WQ3DD9477 20S.84670 1 206.84G70 Bobby Me Cullum ZM.8-0 ?O ag WQGDD9477 0.3734 633734 Michad Ross 6'a.3734 ag WQOOD9477 326.5635 321S.5635 Tommy Williamson 3265635 ag WQ009477 193.14074 193.14074 Kc%in D. Battsam 193.14074 ag WQ00VA77 79.71o2$ 79.7r0?B Ed Blalock 79.71028 ag WQQDG9477 110.31919E I14.849]a 3urnicCaufle 130.84918 ag WQO6094T7 1 L07-32 1 11.03232 Charles Frerm3a 11-03232 ag WQOW9477 L88AW% 188.4MO frank Howey 138.49090 R'QQDU9477 430.93232 430.93232 Frauldin Lee 4"a0.93232 alc WQODG9477 10.78922 30.70922 Bobby MaCollmm t6_'793422 ag WQ0009473 206.96650 206.96650 MikeMcMde 2Dfi-966150 ae WQGM477 132.31712 132.31712 Rogeroxendme 132.317E2 28 WQDN94771 217.47284 317.47294 Adrian Plums 217.47284 89 WQQD'n 94.74M 94.749M Chris Thomas 94.74909 ag H'Q00444T7 42239730 422.3973D 7artnoyVhiUL3msan 432.39730 a TOWN.. Anooal(drs lens). 0 3592.12790 3592.12780-:_: :-: - :'i:::: .:. ..:.. . .. 3592.t2790' Amcndmcm(s)used: 13vl1 iae Agci[{5] nspd • tl mare space LS ragetred. attach addtemnat rnlmynaetou sheds (rtat wt UNISOF (supple): Total Number of Fntm DMSDF (Sapp)l J ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your pennit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - D Q Permit Nuinber: WQ0009477 Laboratory: Cascades Tissue Group -North Carolina, a Faeifity Name: Cascades of Cascades Holdings US Inc. Residual Source WQ 9 or Q0009477 NPDES 0: WWTP Flame: Residua[ Annlvcic T]a#n 1) Pace AnaIytical Services LLC. 2) Waypoint Analytical 3) Summit 4) 5) Parameter (mg/kg) Ceiling Conc. Limit (m o Sample or Composite Date 01109 &14,20 02l13I20 03/03/20 04102/20 05/07/20 0618120 07109120 08/06120 09/15/20 & 09/28/20 10113/20 11/10120 12117/20 Percent Solids (%) IAA 42.70 1 47.2 43.00 39.5 42.4 40.6 435 41.3 4 2. 31 40.3 1 43 44.2 Arsenic 75 1.3 0.95 0.6 0.76 1.3 7.5 1 0.93 1.2 0.99 0.88 0.83 Cadmium 85 Not Permit Required Copper 4,300 16.6 16.2 18.1 13.9 36.8 14.7 16.3 27.5 11.8 0.49 17.3 13.8 Chromium NA Not Pen -nit Required Lead 940 NoE Permit Required Mercury 57 Ni of Permit RegtEired Molybdenum 75 Not I Permit Required Nickel 420 1.3 1.1 1.4 1.20 1.6 1.4 1.9 1.3 1.7 0.49 I.4 1 Selenium 100 N.,0t Permit Required Zinc 7.500 199 75 132 110 180 89.5 157 90.8 82 17.4 155 5 L l Total Phosphorus NA Not Permit Required TKN NA 1630 1200 1560 1580 1650 1860 t500 1730 1090 1580 1 4F07 1560 Ammonia -Nitrogen NA 2.3 19.6 22.8 24.8 19.7 20.2 18.5 22 20.4 24.4 18.7 2I.4 Nitrate and Nitrite NA 4.5 4.1 4.6 4.9 4.6 1 4.8 1 4.5 4 4.8 4.7 4.8 4.3 4.3 " For surface disposal Facilities the ceiling concentration limits [fisted in this form are nit applicable. Reference the individual permit for metals limits. " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for ' mitting false inforAwtion, including the possibility of fines and imprisonment for knowing violations." S Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (1212006) ANNtLAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling andysis results for parameters rml listed in FOR.nI RSSF that are part of die %VQ permit or were aoalyxed for aver the pnst calendar year. 113e additional forms as needed, WQPermitlamber: WQ0009477 Facility Name: Cascades Tissue Group -North Carolina, a division of Cascades Holding U5 Inc. Residual Source NPDPS N WQO(109477 ar,kYQN: WMeTP Names Residual AnalvAs Data L�Etoraton: f)Pace Anatytica3 SmiDM L1.0 2) WavpointAraalytica] 3) Summit 4] 5) Sam 1e or Composite Date OlM9 ] i,24 0?113P�U 43 63r20 {�1,q?r?0 Oii43r 06+1}& 0 p7+p9i20 0&�06+70 04115 20 & 18i1- ] 1;14,20 12f17f20 Parameter (mF,+Ts&1 0912&'20 Pan Cal 499 360 469 474 495 558 450 519 327 474 432 468 AJummum Not Permit Required CarlwnNiLm nRaliD 50 49 84A 39.9 40.53 53 68 72 70.02 57 72 55 CzbciamCarl wze Egnivalencv blot Puna[ Required PH 7 7.3 7.5 8.1 7.40 7.4 7.5 7.3 8.3 7.2 7 2 7.2 Nhgumurn 1560 1650 1570 INO 13343 1380 1480 934 1490 493 141i0 1610 Sodium tint Permit Required Potassium Nni Pertntl 3Requin d Calcium 179000 152000 172000 HMOO 199000 129M 172000 2770D 120004 1560 15_C�JO 10JOW Igpitahtipy-Suttfloit Non- 02N$r2020 Plarrtmable YD-0.446 mgft Cyanide ND-25.0 t ctivrtvSummit mgJKG t}2r0&2024 Sulfide Cmrosivily Smntna 0IUar20m 7.3 Totai -Naragm 1630 1200 1560 1580 1 1650 18b0 1500 1730 1090 I580 1440 1560 TOC 2450W 291(YJ0 297000 391DOD 308000 344U00 30MOO 3130W 32WO13 313000 3250M 290000 Volatile Solids 508000 1 501000 310000 656400 530%0 601000 530000 538000 55D40D 539000 559000 49900Q "1 certify, under penalty of law, that this document was prepared under my direction or supers'ision in accordance with a system designed to rise re that qualified personnet properly gathered and evaluated the information submiticc€. I Lim aware thal there Lire significant penalties for submitting false information, including the possibilitUl-Phes and iuepriso Fn 93ror ' ingviDlaliuns." S Date '1Teparcr is defined in 40 CFR Part 503.9(r) 4 i 5A NCAC 2T .I 102 (26) DENR FORM RSSF- 6 (aD2006) o Pace Analytical Services, t i C aceAnalXical 6701 Conference Drive maw.pacalaLa,cpm Raleigh, NC 27607 (919)934-4964 January 23, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92460661 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on January 14, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise (footnoted. Some analyses have been subcontracted outside of the pace Network, The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks pacolabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC ORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLG. Page 1 of 23 ace� Analytical www.P000labs.com ANALYTICAL RESULTS Project: Sludge Pace Project No,: 92460661 Pace Analytical Services, LLC 6701 Conference Drlve Raleigh, NC 27607 (919)834.4M sample: Sludge Samples Lab 1131 924506610D1 Collected: 01/09/20 06:10 Received: 01/14/2010:03 Matrix: Solid Results reported on a "dry weight" basis and a i adjusted for percent moisture, sample size and any efllutlans. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. 6010 MLT ICP Analytical Method: EPA 601OD Preparation Method: EPA 3050D Arsenic 1.3.1 mg/kg 1.9 0.93 1 0111512011:21 01/16/20 21:58 7440-38-2 Calcium 179000 mg/kg 372 186 20 01/1512011:21 01117/20 21:55 7440-70-2 Copper 16.6 mglkg 0-93 0.46 1 01/15/2011,21 01116/2021:58 7440-50.8 Magnesium 1660 mg/k9 18,s 0.46 1 01/16/20 11:21 01/16120 21:58 7439-96-4 Nickel 1.6 mg/kg 0.93 0.46 1 0111512011:21 01/16/20 21:58 7440-02-0 Zinc 199 mg/kg 1,9 0.93 1 01115/2011:21 01/1612021:58 7440-66-6 254OG Total Percent Solids Analytical Method: SM 2540G-2011 Total solids 42.7 % 0.10 0/000010 1 01/14/20 16:24 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 57,3 % 0.10 0.10 1 01/14/20 1614 9045 pH Sail Analytical Method: EPA 9045D pH at 25 Degrees C 7.0 Std. Units 0.10 0.10 1 01120/20 14:38 Plant Avaliable Nitrogen Analytical Method: SM 271OB-2011 Plant Available Nitrogen 489 mg/kg 0,12 0.12 1 0112312012:56 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1630 mglkg 40.0 20.0 1 01120/2013:30 7727-37-9 360.1 Ammonia Analytical Method: EPA 350.1 Rev 2.01993 Mod, Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia ND mglkg 2.3 2.3 1 01/21/20 10:38 01/21/2014:19 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1093 Nitrogen, Kjeldahl, Total 1030 mg/kg 97.6 48.8 1 01/17/20 07:38 01/18/20 03:33 7727-37-9 Date, 01/23/2020 04:29 PM REPORT OF LABORATORY ANALYSIS TWO report shall not be reproduced. except in foil, without the written consent of Pace Analytical Services, LLC. dual H3 Page 5 of 23 ac'Analyfical" www.pacaieh5,eom ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92460661 Sample: Sludge Samples Lap ID; ''92460661002 Collected: 01/14/20 08:05 Received: 01/14/20 10:08 Results reported on a dry weight" basis and are adjusted for percent moisture, sample size and any dilutions, Report Parameters Results units Limit MDL DF Prepared Analyzed Percent Moisture Percent Moisture 363.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date, 01123/2020 04:29 PM Pace Analytical Services, LLC e701 Conference Drive Ralelgh, NC 27607 (919)834.4984 Matrix: Salld CAS No. Qual Analytical Method: ASTM D2974-87 57.6 % 0.1D 0,10 1 01114/2016:39 Analytical Mad: EPA 353.2 Rev 2.01993 Preparation Method, EPA 353.2 Rev 2.0 1993 ND mgikg 9.1 4.5 1 01/14/20 22:46 01/15/20 00:17 ND mg/kg 9.1 4.5 1 01/14/20 22:46 01/15/20 00:17 14797-55-8 ND mg/kg 9.1 2.3 1 01/1412022,46 0111512000,17 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written Consent of Pace Analytical Services, U0, Page 0 of 23 Waypoint' ANALYTICAL 11769 Pace Analytical Labs Charlotte Tyri& Hooks 9800 Kindey Ave Huntersville , NC 28078 Report Number :20-015-0002 7621 Whitepine Road, Richmond, VA 23297 Main 804-743-94010Fax 804-271-6446 www.waypointanalytical.com Project 92460661 Information : RFIaoRr 0FAJ AL r5X5 Report Date : 01/22/2020 Received : 01/15/2020 d to 6 P Pauric McGroary Agronomist Lab No : 70166 Matrix: Solids Sample ID ; 92460661 Sampled: 1/9/2020 B.xO Test Results IAnalyzed Units MQL DF Date / Time By Analytical Method Moisture 56.5 0/0 0.010 1 01/16/2016,20 ADM SM-2540G Calcium Carbonate Equivalent 45.7 9'0 - dry 0J. 1 01/22/20 08:57 Drr AQAG 955.01 C/N RAnO 50 Ratio 0 1 01/16/20 16:20 CALCULATION Test Results Units MQL nr Date I Time By Analytlnal Analyzed Method Total Solids Total Volatile Solids Total Kjeldahl Nitrogen Carbon (TOC) 3.5 50.8 5910 29.5 % 0.010 1 01/16/2016:20 ADM SM-2,540G % 0.010 1 01/1612016:20 ADM SM-254OG mg/Kg - dry 575 1 01/21/20 12:00 ]P3 ;M-4500-NH3C-TKP % 0.010 1 01/16/20 16:20 CALCULATION Qualifiers/ Dp Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 21 of 23 Pace Analytical Services, LLC 6701 Conference Drive CeAnalytrcal" www.pacolabs.cam February 25, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: project: SLUDGE Dace Project No.: 92465144 Dear Ms. Bellamy: Raleigh, NC 27607 (919)t334.4994 Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hookspacelabs.com (704)875-9092 Project Manager Enclosures cc, Accounts Payable, Cascades Tissue ORT OF LABORATORY ANALYSIS This report shall not he reproduced, except In full, wlthout the written consent of Pace Analytical Services, t.1.0. Page I of 21 acmnalj6cal� www.poCalahs.eom ANALYTICAL. RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project, SLUDGE Pace Project No.: 92466144 Sample; SLUDGE Lab ID: 02465144001 Collected: 02/13/20 09:20 Received: 0211312011:13 Matrix: Solid Results reporled on a "dry weight" basis and are adjusted for percent molsture, sample sire and any dilutions. Report Parameters Results Units Limit MDL OF Prepared Analyzed CAS No, Qual 6010 MET ICP Analytical Method; EPA 6010D Preparation Method: EPA 3050B Arsenic NO i mg/kg 1.9 0.95 1 0211612010:35 02117/2012-17 7440-38-2 Calcium 152000 mg/kg 378 189 20 02/18/20 10:35 02/17/20 23:35 7440-70-2 Copper 16.2 mglkg 0.95 0,47 1 02/16/2010,35 02117120 12:1 7 7440-50-8 Magnesium 1660 mpg 18.9 0.47 1 02116/2010:35 0211712012:17 7439-95-4 Nickel 1.1 mg/4 0.95 0.47 1 02/16/201025 0211712012:17 7440.02-0 Zinc 75.0 mglkg 1.9 0.95 1 0211612010:35 0211712012:17 7440-66-6 2540G Total Percent Salida Analytical Method: SM 2540G-2011 Total Solids 47.2 % 0,10 0.000010 1 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 52.8 i % 0.10 0,10 1 9045 pH Soll Analytical Method: EPA 9046D PH at 25 Degrees C 7.3 -Std. Units 0.10 0.10 1 Plant Available Nitrogen PlantAvallable Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total KJeldahl Nitrogen Nitrogen, Neldahl, Total 363.2 Nitrogen, M021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 02125/2020 10:29 AM Analytical Method: SM 2710B-2011 02/13120 17:34 02113120 17:29 0212412016:23 H3 360 mg/kg 0.12 0.12 1 02/2412010,48 N2 Analytical Method: TKN+NO3+NQ2 Calculation 1200 mglkg 40.0 20.0 1 02/2412010:49 7727-37-9 Analytical Method; EPA 350.1 Rev 2.01993 Mod, Preparation Method: EPA 350.1 Rev 2.0 1993 Mad. ND mg/kg 19.6 19.6 1 0212012012:03 0712112012,12 7664.41-7 Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 1200 mglkg 75.6 37.8 1 02/22/20 07:21 02/23/20 17:35 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.01993 ND mg/kg 8.3 4.1 1 02/13120 22:24 02114/20 00:11 ND mg/kg 8.3 4.1 1 02/13/20 22,24 02/14/20 00:11 14797-55-8 No mg/kg 8.3 2.1 1 02113/20 22:24 02114120 00:11 14797-65.0 REPORT OF LABORATORY ANALYSIS This rapon shall not he reproduced, except In futl, without the written consent of Pace Analytical Services. LLC. Page 5 of 21 I • Wnt ANALYTICAL 11769 Pace Analyticai Labs Charlotte Tyriek Hooks 9800 Klndey Ave Hunteisville , NC 28078 Report Number : 20-049-0009 7621 White pine Road, Ric hroorld, VA 23237 Main $04-743-9401 ° Fax 004-271-6446 www.waypointanalytical.com Project 92465144 Informatlon : REPORT' OFANAL YSI,S Report bate : 02/25/2020 Received; 02/18/2020 o Paurlc McGroary Agronomist Lab No : 70522 Matrix: Solids Sample IR : 9 246.9 144 Sampled: 2/13/2020 9:20 Test Results Units MQL dF Date 1 Time By Analytical Analyzed Method Moisture $5,1 % 0.010 1 02/20/2016:22 GR SM-254OG Calcium Carbonate Equivalent 55.0 % -dry 0.1 1 02/21/20 14:00 DXT AOAC 955.01 C/N RATIO 49 Ratio 0 1 02/20M 16:22 CALCULATION Test Results Units MQl_ GF Gate 1 Time By Analytical Analyzed Method Total Solids �.o % 0.014 Total VolatJle Solids 50.1 % 0.010 Total Kjeldahl Nitrogen 595o mg/Kg - dry 557 Carbon (TOC) 29.1 % 0.010 1 02120/201622 CJR SM-2540C 1 02/20/2016:22 OR 5M-254OG 1 02/24/20 09:30 JP] iM-4500-NH3C-TK1` 1 02/20/20 16:22 CALCULATION Qualifiers/ DF dilution Factor L Limit Exceeded Definitions MQL Method Quantltation Limit Page 19 of 21 a�eAnaljftal � www.pacalehmm March 23, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 806 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Monthly- March Pace Project No.: 92467625 pace Analytical Sorvicas, LLC 6701 Conference Drive Raleigh, NC 27647 IV (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on March 03, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise 'footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com pacelabs,com (704)875-9092 Project Manager Enclosures co: Accounts payable, Cascades Tissue REPORT OF LABORATORY ANALYSIS This report shall not be roprotluced, except in full, without the written consent of Pace Analytical Servlces, LLC. Page 1 of 21 acieAnalyticalw www.pacellbs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 8701 Conference drive Raleigh, NC 27607 (919)8$4.4084 Project: Monthly- March Pace Project No.: 92467625 Sample: Regular Monthly Testing Lab ID: 92467G26001 Collected: 03/03/20 07:35 Received: 03/03/20 07:45 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample sire and any dilutions. Report Parameters Results Units Limit MDL OF ' Prepared Analyzed CAS No. Qual 6010 MET ICP I Analytical Method: EPA 6010D Preparation Method: EPA 30508 Arsenic N❑ mglkg 1.2 0.60 1 03/09/20 09:25 03/12/20 21:22 7440-38-2 Calcium 172000 mglkg 242 121 20 03/09/20 09:25 0311412014:47 7440-70-2 Copper 18.1 mglkg 0.60 0.30 1 03109120 09:25 03/1=0 21:22 7440-50-8 Magnesium 1670 mglkg 12.1 0.30 1 03109/20 09:25 03/12/20 21:22 7439-95.4 Mickel 1.4 mglkg 0.60 0,30 1 03/09/20 09:25 03/12/20 21:22 7440-02-0 Zinc 132 mglkg 1.2 0.60 1 03/09120 09:25 03112/20 21:22 7440-66-6 264OG Total Percent Solids Analytical Method: SM 2540G-2011 Total Solids 43,0 % 0.10 0.000010 1 03/03/20 17,38 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 57.0 % 0.10 0.10 1 03/03/20 17:37 9046 pH Soil Analytical Method: EPA 9045D i pH at 25 Degrees C 7,5 5td, Units 0,10 0.10 1 03116/2018:13 H1 ?lantAvailable Nitrogen Analytical Method: 5M 271OB-2011 Plant Available Nitrogen 468 mglkg 0.12 0.12 1 0311212012:11 rat Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1660 mglkg 40.0 20,0 1 0311012015:58 7727-37-9 350,1 Ammonia Analytical Method: EPA 360.1 Pev 2.0 1993 Mod. preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia ND I mglkg 22.8 22.8 1 03/09/20 09:36 03/11/20 13:30 706"1-7 361.2 Total Kieidahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993 Nitrogen, Kjeldahl, Total 1560 mglkg 96.8 48A 1 03109/20 09:15 03/10120 04:13 7727-37-9 353,2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.01993 preparation Method: EPA 353.2 Rev 2.01993 Nitrogen, NO2 plus NO3 ND mglkg 9.1 4.6 1 03103120 22:47 03/04120 00:38 Nitrogen, Nitrate ND mglkg 9.1 4.6 1 031D3/20 22:47 03/04/20 00:38 14797-55-8 Nitrogen, Nitrite ND I mglkg 9.1 2.3 1 03/03120 22:47 03/04/20 00:38 14797-65-0 Date: 03/23/2020 04:60 PM REPORT OF LABORATORY ANALYSIS I Thig report shall not be reproduoed, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 5 of 21 Waypoint.1 ANALYTICAL 11769 Pace Analyticat Labs Charlotte Tyriek kooks 9800 Kindey Ave Muntersville , NC 28079 PF 7621 Whitepine Road, Richmond, VA 23237 {plain 804-743-9401 ° Fax 904-271-6446 www.waypointanalytical.com Original Report hate : 03/11/2020 Project 92467625 ReAsed Report pate: 03/23/2020 Information : Received : 03/04/2020 Report Number: 20-064-9003 REPI]'17rOPANALV51S Lab No ; 70644 Matrlx: Solids Sample iD : 92467625 Sampled: 3/3/2020 7:35 Test Results Units MQL DF Date I Time By Analytical Analyzed Method Moisture I i 5t3,p °10 0.010 1 03/05/20 16:37 OR SM-254OG Calcium Carbonate Equivalent 40.8 % - dry 011 1 03/10/20 15:00 DXT AOAC 955.01 GIN RATIO 84.4 Ratio 0 1 03/05/20 16:37 CALCULATION Test Results Units MQI_ DF Date ! Time By Analytical Analysed Method Total Solids 42.D % 0.010 1 03/05/20 16:37 OR SM-254OG Total Volatile Solids 51.0 cy° 0.010 1 03/05/20 16:37 OR SM-2540G Total Kleldahl Nitrogen 8380 mg/Kg - dry 595 1 03/10/20 10:00 ]P) iM-450U-NH3C-7KP Carbon (TOC) 29.7 % 0.010 1 03/05/2016:37 JM CALCULATION qualifiers/ DF Dilution Factor I Definitions MQL Method Quandtatlon Limit L Limit Exceeded Page 19 of 21 122ca Analytical Services, LLC aceAnalytical" a701 conference prlue J Raleigh, NC 27607 www.paeelehg,com V (B19)834-4984 April 16, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road FAO Box 578 Rockingham, NC 28380 RE: Project: Monthly -April Pace Project No.: 92472155 Dear Ms. Bellamy: Enclosed are the analytical results for sample($) received by the laboratory an April 02, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report in Its entirety. The test results provided In this final reportwere generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@paGOlabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC DEPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except In full, wilhout the written consent of Pace Analytical Services, LLC_ Page 1 of 21 IaCEAI1c�IlCc71* w4rw,pecale6�.com ANALYTICAL. RESULTS Pace Analytical Services, LLC 6701 Conference drive Raleigh, NC 27847 (919)834.4894 Project, Monthly -April Pace Project No.: 92472155 Sample: Sludge I-ab ID: 92472155001 Collected: 04/02/20 08:06 Deceived: 04/02/20 11:06 Matrix: Solid Results reported on a "dry welght" bask and are adjusted for percent moisture, sample size and any dilutions. Deport Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. 6010 MET ICP Analytical Method: EPA 6010❑ Preparation Method: EPA 3050B Pace Analytical Services -Asheville Arsenic NO mglkg 1.5 0,76 1 04/06/20 09:15 04107/20 11:00 7440-38-2 Calcium 115000 mpg 153 76.3 10 04/06/20 09:15 04/08/20 16:34 7440-70-2 Capper 13.9 mglkg 0.76 0.38 1 04/06/20 09:15 04/07/20 11:00 7440-50-8 Magnesium 1060 mg/kg 15.3 0.38 1 0410W20 09:15 04/07/20 11:00 7439-954 Nickel 1.2 m9/k9 0.76 0.38 1 04/06/20 09:15 04/07/20 11,00 7440-02-0 Zinc Il a mg/kg 1.5 0,76 1 04/06M 09:15 04/07/20 11:00 7440-86.6 2540G Total percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 39,5 % 0,10 0,000010 1 04/03/20 17:41 Percent Moisture Analytical Method: ASTM ❑2974-87 Pace Analytical Services - Charlotte Percent Moisture 60,5 % 0.10 0.10 1 04/03120 17:31 9045 pH Soil Analytical Method: EPA 9046D Pace Analytical services -Asheville pH at 25 Degrees C 8,1 Std. Units 0.10 0,10 1 04/10120 15:57 H3 Plant Available Nitrogan Analytical Method: SM 2710B-2011 Pace Analytical services -Ashevlile Plant Available Nitrogen 474 mglkg 0.12 0.12 1 04113/2014:32 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Nitrogen 1680 mglkg 40.0 20.0 1 04/1312014,30 7727-37-9 350.1 Ammonia Analytical Method: EPA 360.1 Rev 2.01093 Mod. Preparation Method: EPA 350,1 Rev 2.01993 Mod. Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/kg 24,8 24,8 1 04/07/20 15:03 04/0812011:28 7664-41-7 351.2 Total Kjeldehl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Neldahl, Total 1580 mglkg 101 50.6 1 04/09/20 22:28 04110/20 05:51 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 NO mglkg 9.9 4.9 1 04/02/20 22:67 04/03/20 11:29 Nitrogen, Nitrate ND mglkg 9.9 4.9 1 04/02/20 22:57 04/03/20 11:29 14797-55-8 Nitrogen, Nitrite NO mglkg 9.9 2.6 1 04/02/20 22:67 04/03/20 11,29 14797-66.0 Date; 04/16/2020 04:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qual Page 5 of 21 0 Waypoit ANALYTICAL 11769 Pace Analytical Labs Charlotte 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypoiritanalytical.com Original Report Date ; 04/10/2020 Tyriek Hooks Project 92472155 Revised Report Date; 04/16/2020 9800 Klndey Ave Information : Received : 04/06/2020 Huntersvllle , NC 28078 Report Number; 20-097-90JLI REPORr0FANALYS'1'8 Lab No : 70962 Sample ID : 92472155001-sludge Matrix: Solids Sampled: 4/2/2020 8:05 Test Results Units MOL DF Date 1 Time By Analytical Analyzed Method Moisture 61.4 °/a 0.010 1 04/08/20 16:46 ADM SM-254OG Calcium Carbonate Equivalent 33.0 °/b -dry 0.1 1 04/09/20 15:00 DXT AOAC 955.01 C/N RATIO 39.9 Ratio a 1 04/98/20 16:46 CALCULATION Test Results Units MQL DF pate / Time By Analytical Analyzed Method Total Solids 38.6 °/a 0.010 1 04/0S/2016:46 ADM 5M-2540G Total Volatile Solids 65.6 % 0.010 1. 04/08/20 16:46 ADM SM-254OG Total Kjeldahl Nitrogen 4560 mg/Kg - dry 648 1 04/09/20 10:00 JPJ iM-4500-NH3C-TKP Carbon (TOC) 38.1 % 0.010 1 04/08/20 16:46 JM CALCULATION Quallfiers/ DP Dilution Factor L Limit Exceeded Definitions MQL Method Quentitation Limit Page 19 of 21 aceAnalj&al WWW,pecelabs.eom June 02, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92476770 Dear Ms, Bellamy: Pace Analytical Services, LLC 6701 Conference drive Raleigh, NC 27607 (91$)e344904 OV Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2020. The results relate only to the samples Included In this report. Analyses were performed at the Pace Analytical Services location indicated on the sarnple analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report in its entirety. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek, hooks@ pacelabs,com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group=NC REPORT OF LABORATORY ANALYSIS This report shall not be repraduced, except In full, wlthcut the written e065ent of Race Analytical Services, I.E.C. Page t of 21 Paco Analytical SarvIOM, LLC ace l naly cal" 6701 Conference drive WWW,PaCelabs.Gom Raleigh, NC 27607 (919)034-4984 ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92476770 Sample: samples Lab ID: 92476770001 Collected: 05/07/20 05:05 Received: 05/07120 09.08 Matrix: Solid Results reported on a "dry weight" basis and are adjusted far percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA So10D preparation Method: EPA 3050B Pace Analytical Services - Asheville Arsenic 1.3J , mglkg 2,1 1,1 1 05/18/20 07:39 05/21/20 11:68 7440-38-2 M6 Calcium 180000 mglkg 215 107 10 0511W20 07:39 05/20/20 17:38 7440-70-2 M6 Copper 36.8 mglkg 1.1 0,54 1 05/18/20 07:39 05/19/20 2104 1440-50-8 Magnesium 1330 mglkg 21,5 0.54 1 06/18/20 07:39 05/19/20 23:04 7439-95-4 Nickel 1.6 mglkg 1.1 0.54 1 05/18/20 07:39 05/19/20 23:04 7440-02-0 Zinc 180 mg/kg 2,1 1.1 1 06/1812007:39 05110/2023:04 7440-66-6 M1 2540G Total percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 42.4 ' % 0.10 0.000010 1 05/11/20 13:46 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture $7.6 % 0.10 0.10 1 05111/2013:36 1045 pH Soil Analytical Method: EPA 9045D Pace Analytical Services - Asheville pH at 25 Degrees C 7.4 Std. Units 0.10 0.10 1 05/1112013,21 H3 PlantAvallable Nitrogen Analytical Method: SM 2710B-2011 Pace Analytical Services -Asheville Plant Available Nitrogen 495 mglkg 0,12 0,12 1 05/14/20 16:01 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Nitrogen 1650 mglkg 40.0 20.0 1 05/1412015:27 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod, Preparation Method: EPA 350,1 Rev 2.01993 Mod. Pace Analytical Services -Asheville Nitrogen, Ammonia ND mglkg 19.7 19.7 1 05/1212017:34 06/13/20 13:47 7664-41-7 361.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351,2 Rev 2.01993 Pace Ana lytical Services -Asheville Nitrogen, Igeldahl, Total 1650 mglkg 69.4 34.7 1 05113/2013:40 05/14/20 06:02 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 3512 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mglkg 9.3 4.6 1 05/07/20 22:19 05/07/20 23:58 Nitrogen, Nitrate ND mglkg 9.3 4.6 1 05/07/20 22:19 05/07/20 23.58 14797-55-8 Nitrogen, Nitrite ND mglkg 9.3 2.3 1 05/07/20 22:19 06/07/20 23:58 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 061021202010:27 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Waypoeinto ANALYTICAL 11769 Pace Analytical Labs charlotte 7621 Whitepinie Road, Richmond, VA 23237 Main 804-743-9401 ° r=ax 804-271-6446 www.waypointanalocal.com Original Report Rate : 05/19/2020 Tyriek Hooks Project 92476770001 Revised Report pate: 06/02/2020 9800 10ndey Ave Information : Received : 05/12/2020 Huntersville , NC 28078 Report Number : 20-133-9003 REPORT QFANAL Y"S Lab No : 71342 Matrix: Solids Sample ID: 92476770001 Sampled: 5/7/2020 8:25 Test Results Emits MQL OF Date I Time By Analytical Analyzed Method Moisture 56.9 % 0.010 1 05114/2016:50 FMM 5M-2wo Calcium Carbonate Equivalent 43.1 % - dry 0.1 1 05/14/2015:00 DXT AOAC 955.01 C/N RATIO 40.51 Ratio 0 1 05/14/2(116;50 CALCULA710N Test Results Units MQL DF Date ITime By Analytical Analyzed Method Total Solids 43.1 % 0.010 1 05/14/20 16;50 FMM SM-254OG Total Volatile Solids 5310 °/a 0.010 1 05/1412016:50 FMM SM-2540G Total Ijetdahl Nitrogen 7750 mgft - dry 580 1 05118/2010:00 ]P) N-4500-NH3C-Ti(t Carbon (FOC) 30.8 % 0.010 1 05/14/20 16:50 ]M CALCULATION Quallffem/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitatlan Limit Page 19 of 21 c cic;A IalXicalo www,paealahs,com Pace Analytical Services, LLC 9701 Conference Drive Raleigh, NC 27807 (919)834.4984 lu June 23, 2020 Ms. Karen Bellamy Cascades Tissue Croup -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Monthly- June Pace Project No.. 92481106 Deer Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on June 09, 2020_ The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report In its entirety. The test results provided in this final report,were generated by each of the following laboratories within the Pace Network: * Pace Analytical Services -Asheville Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LA130RATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 1 of 22 aceAnalytical www.picollbs.com ANALYTICAL RESULTS Project: Monthly- June Pace Project No,: 92481106 Pace Analytical Services, LLC 0701 Conference Drive Raleigh, NC 27607 (e1e)634-4ee4 Sample: Monthly Sludge Lab ID: 92481106001 Collected: 06/08/20 16:00 Received: 0610912013:16 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL bP Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010D Preparation Method: EPA 3050E Pace Analytical Services -Asheville Arsenic ND mg/kg 15,0 7.5 10 06/16/20 09,33 06119/20 17:19 7440-38-2 U3 Calcium 129000 mglkg 150 75,0 10 06/10/20 09:33 06/19/20 17,19 7440-70-2 Copper 14.7 mglkg 0,75 0,37 1 06/16/20 09:33 06/17/20 00:01 7440.50-8 Magnesium 1380 mglkg 15,0 0,37 1 06/10/20 09,33 06/17/20 00:01 7439-95-4 0C Nickel 1.4 mg/kg 0.75 0.37 1 00/16120 09,33 06/17/20 00:01 7440-02-0 Zinc 89,6 mglkg 1.5 0.75 1 06/16120 09,33 06/17/20 00:01 7440-66.6 8C 254OG Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 40.6 % 0.10 0.000010 1 06/00120 17,38 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 59.3 % 0,10 0.10 1 06/09/20 17:35 045 pH Soil Analytical Method: EPA 9045D Pace Analytical Services -As hevilla pH at 25 Degrees C 1.4 Std. Units 0.10 0.10 1 06/15/20 13:45 H3 Plant Available Nitrogen Analytical Method: SM 27108-2011 Paca Analytical Services - Asheville Plant Available Nitrogen 668 ; mg/kg 0.12 0.12 1 06/22/20 17-31 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Nitrogen 1860 mg/kg 40,0 20,0 1 06117/2011:17 7727-37-9 360.1 Ammonia Analytical Method: EPA 350.1 Rev 2.01993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod, Pace Analytical Services - Asheville Nitrogen, Ammonia IUD mglkg 20.2 20.2 1 06/15/20 10,07 06115/2013:16 7664-41-7 351.2 Total K joldaht Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 1860 mglkg 94.6 47.3 1 06/16/20 02,19 06/17/20 04:06 7727-37-9 Date: 06/23/2020 04:23 PM DEPORT OF LABORATORY ANALYSIS This report shall not be fepfodurad, except In full, without the written consent of Pace Analytcal services, LLC, Page 5 of 22 JaceAnalXicalRo www.pecele6a.cam ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)8$4.4984 Project, Monthly- June Pace Project No,: 92481106 Sample: Monthly Sludge 6/9 Lab W. 92481106002 Collected: 06109/20 08:05 Received: 06/09/20 13:10 Matrix: Solid Results reported an a "dry weight" basis and are adjusted for percent molstur'e, sample size and any dilutions. Report Parameters Results Units Limit MDL ❑F Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 69.3 % 0.10 0.10 1 06/09/20 17:35 353.2 Nitrogen, NO2IN03 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2,0 1993 Pace Analytical Services -Asheville Nitrogen, NQ2 plus NO3 NO mglkg 9.7 4.8 1 06109/20 23:05 06/10/20 00:57 Nitrogen, Nitrate ND mglkg 9.7 4.8 1 06/09/20 23,05 06/10/20 00:67 14797-55-6 Nitrogen, Nitrite NO mg/kg 9.7 2A 1 06109/20 23:05 06110/20 00:57 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, axcapt in full, Date; 05/2312020 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 22 a 'ITV nt - ANALYTICAL 11769 Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 7621 Whitepine Road, Richmond, VA 237-37 Ma In 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project 92481106001 Report bate : 06/19/2020 Information : Izeceived 06/12/2020 CMG it 6AW Pauric McGmary Report Number: 20-164.0001 REPORT OFANAL YSrS Agronomist Lab No: 72621 MaMx: Solids Sample ID : 92481106001 Sampled. 6/8/202015:15 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 58.6 % 0.010 1 06115/2016:53 FMM SM-254OG Calcium Carbonate Equivalent 35.1 % - dry 0.1 1 06/18/20 07:53 DXT AOAC 955.01 C/N RATIO 53 Ratio 0 1 06/15/20 16,53 CALCULATION Test Results units MOL ❑F Date / Tlme By Analytical Analyzed Method Total Solids 41.4 % 0.010 1 06/15/20 16:53 FMM SM-2540G Total Volatile Solids 60.1 % 0.1110 1 06/15/20 16:53 FMM SM-254OG Total Kjeldahl Nitrogen 6590 mg/Kg - dry 604 1 06/1812010:00 ]P] iM-4500-NH3C-TKP Carbon "C) 34.9 % 0.010 1 06/15/20 16.53 CALCULATION Qualltiers/ DIN Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 20 of 22 aceAnalytical www.paealaGstam August 05, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Monthly- July Pace Project No.: 92485434 Dear Ms. Bellamy: Paco Analytical Servicas, LLC 6701 Conference Drlve Raleigh, NC 27607 (919)854.4994 Enclosed are the analytical results for sample(s) received by the laboratory on July 09, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample anelyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network, The test report from the external subcontractor is attached to this report in its entirety. The test results provided in this final report were generated by each of the following laboratories within the Pace Network, Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Cascades Tissue Group- Rockingham, Divsion of Cascades Bolding US Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written Consent of Pace Analytical Sarvlces, LLC. Page 1 of 20 1aueAna1j4ica1'5 www.Ppcelabs.com ANALYTICAL. RESULTS Project: Monthly- July Pace Project No.: 92485434 Paco Analytical Services, LLC 8701 Conference Drive Raleigh, NC 27607 (919jB3�1a19B4 Sample: Sludge Monthly Testing Lab ID: 92486434001 Collected: 07/09/20 07:41 Received: 07/09120 10:40 Matrix: Solid Results reported on a "dry weight" basis and are acrjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DI" prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA3050B Pace Analytical Services -Asheville Arsenic ND mglkg 2,1 1.0 1 07/16/20 09:54 07/20/20 10:21 7440-38-2 Calcium 172000 mglkg 205 103 10 07/16/20 09,54 07/21/2011:19 7440-70-2 MS Copper 16.3 mglkg 1,0 0,61 1 07116120 09,54 07120/2010:21 7440-50-8 Magnesium 1480 mglkg 20.5 0,51 1 07/16120 09:64 0712012010:21 7439-95-4 Nickel 1.9 mglkg 1.0 0.51 1 07/16/20 09:54 07120/20 10:21 7440-02-0 Zinc 157 mglkg 2A 1.0 1 07/16120 09:54 07/20/20 10:21 7440-66-6 MI 26400 Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 43.5 % 0.10 0.000010 1 07/10/20 00:56 Percent Moisture Percent Moisture 9045 pH Sail pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 360.1 Ammonia Nitrogen, Ammonia 351,2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 363.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 0810512020 11 :51 AM Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte 56.5 % 0.10 0.10 1 07/10/20 00:39 Analytical Method: EPA 90451) Pace Analytical Services - Asheville 7.5 Std. Units 0.10 0,10 1 07/13120 15:25 Analytical Method: SM 2714B-2011 Pace Analytical Services - Asheville 450 mglkg 0.12 0.12 1 08/0412017:13 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Ashevl lie 1500 mg/kg 40.0 20.0 1 08/0412017:05 7727-37-9 Analytical Method: EPA 350.1 Rev 2.01993 Mod, Preparation Method: EPA 380.1 Rev 2.01993 Mod. Pace Analytical Services -Asheville ND mglkg 18.5 18,5 1 07/17120 07:41 07/17120 11.23 7664-41-7 Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 1500 mglkg 88.4 44.2 1 08/03/20 23:47 08/04/20 06,28 7727-37-9 Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA363.2 Rev 2.0 1993 Pace Analytical Services -Asheville ND mglkg 8.9 4.5 1 07/09/20 22:16 07/09120 2249 ND mglkg 8.9 4.5 1 07/09120 22,16 07109120 22.49 14797-SS-8 ND mglkg 8.9 2.2 1 07109M 22,16 07109120 22.49 14797-SS-0 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced. except In furl, wilhout the written Consent of Pace Analytical sarvloea, LI,C. H3 N2 M1 M1 Page 5 of 20 Waypoit ANALYTICAL 11769 Pace Analytical Labs Charlotte Project 92485434 Tyriek Hooks 9800 Klndey Ave Information Huntersville , NC 28078 7621 Whitepine Road, Richmond, VA 23237 Main 804-749-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Pate ; 07/21/2020 Received : 07/14/2020 Pauric McGroary Report Number : 20-196-0005 REPO&rDXANALYSIS Agronomist Lab No : 73037 Matrix: Solids Sample ID : 92485434 Sampled: 7/9/2420 0:00 Test Results Unite MQL DF Date I Time By Analytical Analyzed Method Moisture Calcium Carbonate Equivalent C/N RATIO Test Total Solids Total Volatile Solids Total Ijeldahl Nitrogen Carbon CrOC) 57.0 % 0.010 6.4 % - dry 0.1 68 Ravo 0 Results Units MQL 43.0 11/0 0.010 53.0 % 0.010 4510 mg/Kg - dry 581 30.9 % 0.010 Qufallflers/ DF Dilution Factor Definitions MQL Method Quantitation Limit 1 07/16/2016,53 FMM SM-254OG 1 07/20/2012.51 DXT AOAC 955,01 1 07/16/20 16:53 CALCULATION DF Date / Time By Analytical Analyzed Method 1 07/16/2016:53 FMM SM-254OG 1 07/16/2016:53 FMM SM-254OG 1 07/19/20 14:39 ]P] iM-4500-NH3G--W 1 07/16/20 16:53 CALCULATION L Limit Exceeded Page 10 of 20 Pace Analytical Services, LLC 6701 Confarance Ddve aceAnalyticai" www.pisculabs.com August 24, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Monthly -August Pace Project No.: 92489568 Dear Ms. Bellamy: Raleigh, NC 27607 (919)834.48$4 Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location Indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report in Its entirety. The test results provided In this final report were generated by each of the following laboratories within the Pace Network: Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek. hooks@ pacelabs,com (704)875-9092 Project Manager Enclosures cc: Cascades Tissue Group- Rockingham, Divsion of Cascades Holding US Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC_ Page 1 of 21 aceAnalyrFical" wwW.paceli5�.com ANALYTICAL RESULTS Pace Analytical Services, LLC B'101 Conference Drive Raleigh, NC 27607 ($19)6344964 Project: Monthly -August Pace Project No.: 92489568 Sample: Cascades Sludge Lab ID: 92489566001 Collected: 08/06/20 07:35 Received: 08/06/20 08:56 Matrix: Solid Results reported on a "dry weigh!" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Ctual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Pace Analytical Services -Asheville Arsenic ND mglkg 1.9 0.93 1 08/10120 20:13 08/11/20 1&23 7440-38-2 Calcium 27700 mglkg 93.2 46.6 5 08/10/20 20:13 08/11/20 18:30 7440-70-2 Copper 27.5 mglkg 0.93 0.47 1 08/10/20 20:13 08/11/20 16:23 7440-50-8 Magnesium 934 mg/kg 18.6 0.47 1 08/10/20 20:13 08/11/20 16:23 7439-95-4 Nickel 1.3 mg/kg 0.93 0.47 1 08/10/20 20:13 08111/20 16:23 7440-02-0 Zino s0,8 mglkg 1.9 0.93 1 08/10/20 20:13 Q6111120 16:23 7440-66-6 2540G Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 41.3 % 0.10 0/000010 1 08/06120 17:25 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 58.7 % 0.10 0.10 1 08106/20 17:18 9045 pH Salt Analytical Method: EPA 9045D PaceAnalytleal Services -Asheville pH at 25 Degrees C 7.3 Std. Units 0.10 0.10 1 08/1012016:22 H3 Plant Available Nitrogen Analytical Method: SM 2710B-2011 Pace Analytical Services - Asheville Plant Available Nitrogen 519 mglkg 0.12 0.12 1 08/19/20 10:51 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Nitrogen 1730 mglkg 40.0 20.0 1 08/19/2010:40 7727-37-9 360.1 Ammonia Analytical Method: EPA 35M1 Rev 2.01993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Pace Analytical Services -Asheville Nitrogen, Ammonia N❑ mglkg 22.0 22.0 1 08/11120 07:33 08/11120 11:13 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 1730 mg/kg 115 57.7 1 08/18/20 13:50 08119/20 04;36 7727-37-9 363.2 Nitrogen, N021NO3 Analytical Method: EPA 363.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2,01993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg/kg 9.7 4.8 1 08/07/2010:05 08107/20 11.57 Nitrogen, Nitrate ND mg/kg 9.7 4.8 1 08/07/20 %G5 08107/20 11,57 14797-56-8 Nitrogen, Nitrite ND mg/kg 9.7 2.4 1 08/07/2010:05 08/07/20 11,57 14797-65-0 Date: 08/2412020 02:36 PM REPORT OF LABORATORY ANALYSIS This report shwa not be reproduced, except in full, without the written consent of Pece Analytical Services, LLC. Page 5 of 21 0 Waypoi 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 11769 Pace Analytical Labs Charlotte Project Cascades sludge Tyriek Hooks Report Date: 08/14/2020 9800 Klndey Ave InfbrrnaVan ; 92489568 Received : 08/07/2020 Huntersville , NC 28078 Pauric Mc Groary Ph.D., CPA Report Number: 20-220-0008 REPORT OFAIVACVW Agronomist Lab No, 73314 Matrix; Solids Sample ID : Cascades Sludge - 92489568 Sampled: 8/6/2020 7:35 Test Results Units MQL DF Data 171me By Analytical Analyzed Method Moisture 58.6 0/0 0.010 1 08112/2016:51 FMM SM-2540G Calcium Carbonate Fqulvalent 54.1 % - dry 0.1 1 08/12/20 12:15 DXT AQAC 955.01 C/N RATIO 72 Ratio 0 1 08/12/20 16.51 CALCULATION Test Results Units MOL DF Date / Time By Analytical Analyzed Method Total Solids 41,4 % 0.010 1 08/12/20 16:51 FMM SM-2540G Total Volatile Solids 53.6 % 0.010 1 08/12/20 16:51 FMM SM-254OG Total Kjeldahl Nitrogen 4350 mg/Kg - dry 604 1 08/13/20 09.00 3P] ;M-4500-NH3C 7Kt Carbon (fOC) 31.3 % 0.010 1 08/12/20 16:51 CALCULATION Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Pago 19 of 21 Paco Analytical Services, LLC 6701 Conference Drive acleAnalyticale WWW,pacelehaxom October 15, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: SLUDGE Pace Project No.: 9249588E Dear Ms. Bellamy: ,V Raleigh, 14C 276a7 (� (919)934 1984 Enclosed are the analytical results for sample(s) received by the laboratory between September 15, 2020 and September 29. 2020, The results relate only to the samples included in this report_ Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontraCtor is attached to this report in its entirety. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte Revision 1- This report replaces the October 12, 2020 report. This report was reissued on October 15, 2020 to include C/N ratio per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@paeelabs.com (704)875-9092 Project Manager Enclosures cc: Cascades Tissue Group- Rockingham, Divslon of REPORT OF LABORATORY ANALYSIS This report shall not be reprotluced, except In Full, without the written consent of Pace Analytical Services, I.I.C. Page 1 of 21 (17a4 eA Ialyfi a " www pacurabs.com ANALYTICAL RESULTS Project: SLUDGE Pace Project No.: 92495886 Pace Analytical Services, LLC 6701 Conferaric D&e Ralelgh, NC 27607 (919)834.4884 Sample: CASCADES SLUDGE Lab ID: 82495886001 Collected: 09/15/20 08:05 Received: 09115/2010:23 Matrix: Salld Results reported on a "dry weight" basis and are adjusted for percent raoistare, sample size and any dilutions. Report Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 60100 Preparation Method: EPA 3050E Pace Analytical Services - Asheville Arsenic 1.2J mglkg 2.0 0.99 1 09/17/20 14:23 09/18/20 23.53 7440-38-2 Calclurn 120000 mglkg 197 98.6 10 09/17/20 14:23 09/19/20 20:57 7440-70-2 Copper 11.8 mglkg 0.99 0A9 1 09/17120 14:23 09/18120 23:63 7440-50-8 Magnesium 1490 mglkg 19.7 0.49 1 09/17/20 14:23 09/18/20 23:63 7439-95-4 Nickel 1.7 mglkg 0.09 0.49 1 09117/20 14:23 09118)20 23:53 7440-02-0 Zinc 82.0 mglkg 2.0 0.99 1 09/17120 14:23 09/18/20 23:53 7440.66.6 2640G Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total SCIId6 42.3 % 0.10 0,000010 1 09/16/20 18:08 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 57.7 % 0.10 0.10 1 09/16/20 17:52 )45 pH Soil Analytical Method: EPA 9045D Pace Analytical Services - Asheville pH at 25 Degrees C B.3 Std, Units 0.10 0.10 1 09128120 15:08 H3 Plant Available Nitrogen Analytical Method: SPA 2710D-2011 Pace Analytical Services -Asheville PlantAvallable Nitrogen 327 mglkg 0.12 0.12 1 0912912011,26 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3tNO2 Calculation Pace Analytical Services -Asheville Nitrogen 1090 mglkg 40.0 20.0 1 0912412013:51 7727-37-9 350.1 Ammonia Analytical Method: EPA 360.1 Rev 2.0 1903 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Pace Analytical Services -Asheville Nitrogen, Ammonia ND mglkg 20.4 20.4 1 09123120 13:00 09/24/20 11:00 7664-41-7 361.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl. Total 1090 mg/kg 84.5 42.3 1 09/23/20 12:55 09/24/20 06:55 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mglkg 9.3 4.7 1 09/16/20 22:28 09/17/20 00:14 Nitrogen, Nitrate ND mg/kg 9.3 4.7 1 09116/20 22:28 09/17120 00:14 14797-55-8 Nitrogen. Nitrite NO mglkg 9.3 2.3 1 09116/20 22:28 09M7120 00:14 14797-65.0 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, exmpt In full, Date: 10/1512020 11:56 AM without the wdtlen Consent of Pace Analyteal Services, LLC. Page 5 of 21 Waypoint, 762i SNhltepine Rand, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 11759 ANALYTICAL www.waypointanaiytical,com Pace Analytical Labs Charlotte Project Cascades Tissue NC Original Report bate , 10/15/2020 Tynek Hooks Revised Report Date: 10/15/2020 9800 Kindey Ave Information : Received ; 10/01/2020 Huntersville , NC 28078 Report Number: 20-275.0011 REPORrOFAIVALYSIS Lab No : 73855 Sample ID : Cascades Tissue NC 92495886 Matrix: Solids Sampled: 9/28/2020 12,00 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 54.7 `ya 01010 1 10/05/20 17:18 FMM SM-2540C Calcium Carbonate Equivalent 41.5 % - dry 0.1 1 10/08/20 14:20 DXP AOAC 955.01 C/N RATIO 70.02 RaiJo i CALCULATION Test Results Units MQL DF Date / Tlme By Analytical Analyzed Method Total Solids 45,3 % 0.010 1 10/05/20 17.18 FMM SM-2540G Total Volatile Solids 55.0 % 0.010 1 10/05/20 17:18 FMM SM 2544G Total Kjeldahl Nitrogen 2090 mg/Kg 250 1 10/07/20 10:00 JPJ iM-4500-NH3C-TKP Carbon CTOC) 32.0 % 0.010 1 10/05/20 17:18 ]M CALCULATION qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Urnit Page 19 of 21 IAnalj4ical" www.pacelehs.cem October 26, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: 10-995-8292/ Monthly- Oct. Pace Project No.: 92500173 Dear Ms. Bellamy: Pace Analytical Sarvlcas, LLC $701 Conference Drive Raleigh, NC 27607 (91 S)8344984 Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyle page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report In Its entirety, The test results provided In this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Cascades Tissue Group- Rockingham, Divsion of Cascades Holding US Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Sarvlcas, LLC, Page 1 of 19 acleAnalXica( www,pacolabs.com ANALYTICAL RESULTS Project: 10-995-82921 Monthly- Oct Pace Project No.: 92500173 Pace Analytical 5erviceo, LLC 67M Conference Drive Raleigh, NC 2761)7 (919)834-4994 Sample: CASCADES SLUDGE Lab ID; 92500173001 Collected: 10/13120 07,55 Received: 10/13/2010:04 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET iCP Analytical Method: EPA 601 DID Preparation Method: EPA 3050B Pace Analytical Services -Asheville Arsenic ND mg/kg 2.0 0.99 1 10/14/20 12:50 10/17/20 02:37 7440-38-2 Calcium 1560 mglkg 19.7 919 1 10/14120 12:50 10/17/20 0237 7440-70-2 Capper NO mglkg 0.99 0.49 1 10/14/20 12:50 10/17/20 02:37 7440-50-8 Magnesium 483 mglkg 19.7 0.49 1 10/14/2012:50 10/17/20 02:37 7439-95-4 Nickel ND mglkg 0.99 0.49 1 10/14/2012,50 10117/20 02:37 7440-02-0 Zinc 17.4 mglkg 2.0 0.99 1 10/14/20 12:50 10/17/20 02:37 7440.66-6 25400 Total Percent Solids Analytical Method: SM 2540G-2011 Pace Analytical Services - Charlotte Total Solids 40.3 % 0.10 0,000010 1 10/13/20 17:44 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 69.7 % 0A0 0.10 1 10/13120 17:37 )45 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date,10/2612020 03:28 PM Analytical Method: EPA 90450 Pace Analytical Services -Asheville 7.2 SW_ Units 0.10 0.10 1 10/26/2013:43 Analytical Method: SM 27103-2011 Pace Analytical Services - Asheville 474 mg/kg 0.12 0.12 1 10/26/2016,14 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville 1580 mglkg 40.0 20.0 1 1012612015:12 7727-37-9 Analytical Method: EPA 350.1 Rev 2.01993 Mod. Preparation Method: EPA 350,1 Rev 2.0 1993 Mad. Pace Analytical Services - Asheville N❑ mglkg 24A 24.4 1 10114/2015:12 10/1512010,26 7664-41-7 Analytical Method- EPA 351.2 Rev 2,01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 1580 mglkg 92.0 46,0 1 10/24/20 01:39 10124/20 06:39 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.01903 Pace Analytical Services - Asheville NO mg/kg 9.6 4.8 1 10/14/20 08:39 10/14/2010:37 ND mglkg 9.6 4.8 1 10/14/20 08:39 10114/2010:37 14797-55-8 ND mglkg 9.6 2.4 1 10/14/20 08:39 10114/2010:37 14797-65-C REPORT Or LABORATORY ANALYSIS This report shall not be reproduced, except in full, wlthoul the written consent of Pace Analytical Services, LLC. H3 N2 M1 Page 5 of 19 0 Waypos��ti 7621 Wliitepine Road, Richmond, VA 23297 Main 804-743.9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 11769 Pace Analytical Labs Charlotte Project Cascades Sludge 92500173 Tyriek Hooks Report Date! 10/23/2020 9800 Kindey Ave Information : Received; 10/15/2020 Huntersville , NC 28078 Report Number: 20-289-0005 I±rEPORTOFANALYSIS Paurlc Mc Groary Ph.D., CPA Agronomist Lab No: 73961 Matrix: Solids sample ID : Cascades Sludge 92500173 Sampled: 10/13/2020 7:55 Test Results Units MQL DF Date / Time gy Analytical Analyzed Method Moisture 59.3 % 0.010 1 10119/2017:07 FMM SM-2540G Calcium Carbonate Equivalent 46.4 °k - dry 0.1 1 10/21/20 13:00 DkT AOAC 955.01 C/N RATIO 57 Ratlo 0 1 10/19/20 11:30 CALCULATION Test Results Units MQL DF date / Time By Analytical Analyzed Method Total Solids 40.7 % 0.010 1 10/19/20 17:07 FMM SM-2540C Total Volatile Solids 53.9 % 0.010 1 10/19/20 17:07 FMM sM-2540G Total Kjeldahl Nitrogen 5500 mg/Kg - dry 614 1 10/19/20 11:30 ]P] ,M-4500-NH3C-TK1` Carbon (TOC) 31.3 °/a 0.010 1 10/19/20 17:07 CALCULATION Qualifiets/ ❑F Dilution Factor L Limit Exceeded Definitions MQL Method Quantitatlon Limit Page 17 of 19 Pace Analytical Services, LLC $701 Conference Drive aceAnalyfical " aww,paselab.com December 29, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PG Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92505092 Dear Ms. Bellamy: Raleigh, NC 27807 (919)834-4984 Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2020, The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network, The test report from the external subcontractor Is attached to this report In its entirety. The test results provided In this final report were generated by each of the following laboratories within the Pace Network: Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek,hooks@pacelabs,com (704)875-9092 Project Manager Enclosures cc; Cascades Tissue Group- Rockingham, ❑ivsion of Cascades Voiding US Inc. REPORT OF LABORATORY ANALYSIS Thls report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 1 of 22 (,7a1c,eAna1jdica1" www.picalibs.com ANALYTICAL RESULTS Project: SludUo Pace Project No.: 92505092 Pace Analytical Services, LLC 6701 Conference Drive Ralelgh, NC 27607 (919)834.4984 Sample: Sludge Lab ID: 92505092001 Collected: 11/10/20 07:40 Received; 11/10/20 10:13 Matrix: Solid Results reported on a "dry weight" basis andare adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E Pace Analytical Services - Asheville Arsenic NO mglkg 4.4 0.88 1 12/13/2013:58 12/24/2017:05 7440-38-2 Calcium 163000 mg/kg 660 330 50 11111/2011:54 11/1412017:23 7440-70-2 Copper 17.3 mglkg 0.66 0.33 1 11/11120 11:54 11/13/20 23,56 7440-50.8 Magnesium 1480 mg/kg 13.2 0.33 1 11/11/20 11:54 11/13/20 23,56 7439-95-4 Nickel 1.4 mg/kg 0,66 0.33 1 11/11/20 11:54 11/13/20 23,56 7440-02-0 Zinc 155 mg/kg 1.3 0.66 1 1111112011:54 11/13/20 23,56 7440.66-6 254OG Total Percent Solids Analytical Method: 5M 25400-2011 Pace Analytical Services - Charlotte Total Solids 43.0 % 0.10 0.000010 1 1111012017:27 Percent Moisture Analytical Method: ASTM Q2974-87 Pace Analytical Services - Charlotte Percent Moisture 57.0 % 0,10 0.10 1 11/1012017:19 146 pH Soil Analytical Method: EPA 9045D Pace Analytical Services -Asheville pH at 25 Degrees C 7.2 Std. Units 0.10 0,10 1 1112312013:10 H3 Plant Available Nitrogen Analytical Method: SM 271OB-2011 Pace Analytical Services -Asheville Plant Available Nitrogen 432 mg/kg 0,12 0.12 1 11123/2013:33 N2 Total Nitrogen Calculation Ana lytica 1. Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Nitrogen 1440 mglkg 40.0 20.0 1 11/2312013:30 7727-37-9 350.1 Ammonia Analytical Method: EPA 350,1 Rev 2.0 1993 Mad. Preparation Method: EPA 350.1 Rev 2.0 1993 Mad, Pace Analytical Services - Asheville Nitrogen, Ammonia ND mg/kg 18.7 18.7 1 11/1112013:32 11/12/20 08:26 7664-41-7 361.2 Total KJeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 1440 mg/kg 83.0 41.5 1 11120/20 22:56 11/21120 05:35 7727-37-9 M1, R1 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 3512 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 N❑ mglkg 8.6 4.3 1 11110120 22:05 11111/20 01:01 Nitrogen, Nitrate N❑ mg/kg 8.6 4.3 1 11/10120 22,05 11/11/20 01:01 14797-55-8 Nitrogen, Nitrite ND mg/kg 8.6 2.2 1 11/10/20 22:05 11/11/20 01:01 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproducad, except In full, Data: 12/2912020 03:58 PM without the written consent of Pace Analytical Setices, LLC. Page 5 of 22 WavI3061 to ANALYTICAL 11769 Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Report Number: 20-318-t}a15 Lab No., 74207 Sample ID : Sludge 92505092 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com project Sludge 92505092 Information : REPORT OFANAL YSIS Report Date : 11/20/2020 Received : 11/13/2020 41� - M' ko W Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 11/10/2020 7:40 Test Results Units MOL DF Date / Time By Analytical Analyzed Method Moisture 57.0 °/a 0.010 1 11117/2016:40 FMM SM-254OG Calcium Carbonate Equivalent 99.7 % - dry 0.1 1 11/18/2011:25 DXT AOAC 955.01 C/N RATIO 72 Ratio 0 1 11/17/20 16A0 CALCULATION Test Results Units MQL DF Date I Time By Analytical Analyzed Method Total Solids 43,0 % 0.010 1 11/17/20 16:40 FMM SM-254OG Total Volatile Solids S5.9 % 0.010 1 11/17/2016:40 FMM SM-254OG Total K)eldahl Nitrogen 45JLO mg/Kg - dry 581 1 11/1912010:00 ]P] ;M-4500-NH3C-TKP Carbon (TOC) 32.5 °/a 0.010 1 11/17/2016:40 CALCULATION qualiflers/ or Dilution Factor L Limit Exceeded nei:tnitions MQL Method Quantitation Limit Page 20 of 22 Pace Anelytical Services, LLC 6701 Conrerence 17rlve aceAnalyfical WWW.pae6103.00m January 05, 2021 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: SLUDGE Pace Project No.: 92512633 Dear Ms. Bellamy: Ralelgh, NC 27607 (919)8344984 Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2020. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is attached to this report in its entirety. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville F Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacetabs.com (704)875-9092 Project Manager Enclosures cc: Cascades Tlsstie Group- Rockingham, Divsion of Cascades Holding US Inc. REPORT OF LABORATORY ANALYSIS This report $hall not ba reproduced, except In full, without the written consent of Pace Analytical 5ervioe$, LLC. Page 1 of 20 aCeAnalytical® WWWO15b3.com ANALYTICAL_ RESULTS Project: SLUDGE Pace Project No.: 92512633 Pace Analytical Services, LLC 6701 Conference Drive Raleigh. NC 27807 (919)B34-4984 Sample. SLUDGE CASCADES Lab ID: 92512633001 Collected: 12/17/20 07:07 Received: 1211712012:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MOL OF Prepared Analyzed CAS No. Qual 6010 MET IGP Analytical Method: EPA 6010❑ Preparation Method: EPA 3050E Pace Analytical Services - Asheville Arsenic ND mglkg 4.2 0.83 1 12/20/20 12:07 12/30/20 22:03 7440-38-2 Calcium 107000 mglkg 416 83.3 10 12120/2012:07 1213112010:36 7440-70-2 Copper 13.8 mglkg 8.3 0.42 1 12/20120 12:07 12/30/20 22:03 7440-60-8 Magnesium 1610 mglkg 16.7 0.42 1 12/20/20 12:07 12/30/20 22:03 7430-95-4 Nickel 1.0 mglkg 0.83 0.42 1 12/20120 12:07 12130/20 22:03 7440-02-0 Zinc 51.1 mglkg 1.7 M83 1 12120/20 12:07 12/30/20 22:03 7440.66.6 2540G Total Percent Solids Analytical Method: SM 2640G-2011 Pace Analytical Services - Charlotte Total Solids 44.2 % 0,10 0.000010 1 12/17/20 17:44 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 65.8 % 0.10 0.10 1 12/17120 17:19 '045 pH Soil Analytical Method: EPA 9045D PaceAnalytical Services -Asheville pH at 25 Degrees C 7.2 Std. Units 0.10 0.10 1 12129/2015:38 H3 Plant Available Nitrogen Analytical Method: SM 27103-2011 Pace Analytical Services -Asheville Plant Available Nitrogen 408 mglkg 0.12 0.12 1 12/3012017:38 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Servlces -Asheville Nitrogen 1560 mglkg 40.0 20.0 1 12124/2017:05 7727-37-9 350.1 Ammonia Analytical Metfiod: EPA 350.1 Rev 2.01993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Pace Analytical Services -Asheville Nitrogen, Ammonia ND mglkg 21.4 21.4 1 12/30/20 09:37 12/30/20 14:02 7654-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kf eldahl, Total 1560 mglkg 103 51.5 1 12/22/20 18:38 12/23/20 06:37 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, 1402 plus NO3 ND mglkg 8.6 4-3 1 12/17/20 22:23 12/18120 01:03 Nitrogen, Nitrate ND mglkg 8.6 4.3 1 12/17/20 22:23 12/18/20 01:03 14797-55-8 Nitrogen, Nitrite ND mglkg 8.6 2.2 1 12/17/20 22:23 12118120 01:03 14797-65-0 Date: 01/05/2021 02:08 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wri0an consent of Pace Analytical Servlcas, LLC. Page 5 of 20 Waypolta ANALYTICAL 11769 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271.6445 www.waypointenaiytical.com Pace Analytical Labs Charlotte Project Sludge 92512633 Tyrlek Hooks Report Date: 12/31/2020 9800 Kindey Ave Information ; Received ; 12/22/2020 Huntersville , NC 28078 � 6 � ko IV Report Number! 20-357.0004 REPosrO 'ANALWS Pauric Mc Groary Ph.D., CPA Agronomist Lab No ; 74487 Matrix: solids Sample ID : Sludge Cascades 92512633001 Sampled: 12/17/2020 7:07 Test Results Units MOO DF Rate / Time By Analytical Analyzed Method Moisture 58.3 °/a 0.010 1 12/23/20 16:31 FMM SM-254OG Calcium Carbonate Equivalent 64.9 °/a - dry 0.1 1 12/30/20 13:00 DXT AOAC 955.01 C/N RATIO 55 Ratio 0 1 12/23/20 16:31 CALCULATION Test Results Units MOL DF Date / Time By Analytical Anaiyaed Method Total Solids 41.7 % 0.010 1 12/23/20 16:31 FMM SM-2540C Total volatile Solids 49.9 % 0.010 1 12/23/20 16.31 FMM SM-254OG Total Kjeldahl Nitrogen 5300 mg/Kg - dry 600 1 12/29/20 12:00 JPJ iM-4500-NN3C-TKP Carbon (TOC) 29.0 % 0.010 1 12/23/20 16:31 CALCULATION Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantltation Limit Page 18 of 20 IT EN VIIZONtdENTALP1 SLIW!M INC AntilyUCa1 Laboratorlee February 21, 2020 Summit Envlromnenlal r'echnologles, 111g, 3310 Win St. Cuyahoga rolls Ohio 44223 TEL, (330) 253-8211 FAX: (330) 253-4489 Wehslte; 1 /�Iavr, a .cor Karen Bellamy Cascades Tissue Group - North Carolina Inc 805 Midway Road Rockingham, NC 28379 TEL: 910-895-4033 FAX: 910-895-9887 RE: Waste Characterization Dear Karen Bellamy: Order No.: 20020508 Summit Environmental Technologies, Inc. received 1 sample($) on 2/8/2020 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted, If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Holly Florea Project Manager 3310 Win 3t. Cuyahoga Falls, Ohio 44223 Arkansas U-0735, California 07256CA, Colorado, C011MCCHcul PH-0108, Qalnware, Clarida NEIAC E87688, Georgia E87688, Idaho OH00923, Illinois 20006 i, Indiana C-OH-13, Kansas E-10347, Kcnlucky (Underground Slbragc Tank) 3, Kenlueky 90146, Lonisiana 04061, Maryland 339, Mirmcrbla 409711, New Elampshire2996, New Jersey ol-1006, New York 11777, Notth Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Aklaiioma 9940, Oregon OH2O4041, Pennsylvania 010, Rhoda Fslnnd LA000317, 5oull, CAMliha 92016001, Texas T104704466-11-5, IA111 01-1009232011-1, Virginia VELAP 9456, Wnsl,inglon C891 Page I of 36 ' 5uhr1lrrrf L•nvironhseniol Technologies. 1,rc, SUMMIT 3310 Win 3i, Case Narrative Et4Vii40NMCNTAL Yi:CIINOLOGIES, INC_ Crryalroga Fulls, Ohio 44223 rtWOE: 20020508 ,raly0cal Ln1lara10r10s TEL: (330) 2534211 FAX: (330) 233-4489 Websife; AYM& ,Lill .selhe 02 Data: 212Xl2020 CLIENT: Cascades Tissue Group -North Carolina Inc Protect: Waste Characterization WorkOrder Narrative: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary ,Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program A.nalytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc, or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the „-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 20020508-001 A TCLP-SVOC-8270E: Possible low bias for Hexachloroethane due to low recovery in LCS-42030. Original Page 2 of 36 SUMMIeff- SuruMit Environmental Technoiogles, Inc. Workordear 3310 WirtSt. ENVI)IONWNTAL TccaNbl;,(►131% INC Cuyahoga Falls, Oluo 44223 Sample Summary Analytical TEL: (330) 253-821I FU,' (330) 253-4489 W04: 200205Q$ t'Yubsrle; 1 ://� iu� r r ffak. ,2l-Feb-20 CLIENT; Cascades Tissue Group - North Carolina Inc Project: 'Waste Characterization Lab 5amplaID Client Sample jo 'Fag No Date Collected Rate Received Matrix 20020508-001 Sludge 2/7/2020 8:00:00 AM 2/8/2020 8:21'00 AM Sludge Page 3 of 36 msummsu mril Envlronmeniv/ Technologies, Inc. ur 3310 if in S1. 0i1VInaNMLiJ1gL7EcrINo C,C�ips.INC Cuyahoga Falls. Ohio44223 Analylfcal Laborarorlas 2"EL: (330) 253-8211 FAX.- (330) 253-4489 We6s11e: 1 :/A,rtin v corn WO#: 20020508 Date Reported: 2/21/2020 Company: Cascades Tissue Group - North Carolina I Address: 805 Midway Road Rockingham NC 28379 Received: 2/8/2020 Project#; Waste Characteri TCLP Metals Analysis (SW1311/6010) Client ID# Lab ID# Collected Analyse Rep Lmt Result Units Matrix Method Dl; RegLvl Run Analyst Sludge 001 2£7/2020 TCLP Arsenic(As) 0.500 ND mg/L Sludge EPA 6010 1 5,00 2/13/2Q2o EAM D Sludge 001 217/2020 TCLP Barium(Ba) 5.00 ND mg/L Sludge EPA 6010 1 100 2/13/2020 EAM D Sludge 001 2/7/2020 TCLP Cadmium(U) 0.100 ND mg/L sludge EPA 6010 1 1.00 2/13/2020 EAM D Sludge 001 2/7/2020 TCLP Chromium(Cr) 0.200 NO mg/L Sludge EPA 6010 1 5-00 2113/2020 EAM D Sludge 001 2/7/2020 TCLP Lead(Pb) 0.500 ND mg1L Sludge EPA 6010 1 5.00 2/1312020 EAM D Sludge 001 2/7/2020 TCLP Sefenium(Se) 0,0500 ND mg/L Sludge EPA 6010 1 1.00 2/13/2020 EAM D Sludge 001 2/7/2020 TCLP 5liver(Ag) 0,500 ND mg/L Sludge EPA 6010 1 5,00 2113/2020 EAM D TCLP Mercury Analysis (SW1311/7470) Client ill# Lab ID# Collected Analyse Rep Lmt Result Units Matrix Method DP RegLvl Run Analyst Sludge 001 2/7/2020 TCLP Mercury 0,00200 NI) mg/L Sludge EPA 7470 A 1 0.200 2/17/2020 MJM TCLP Pesticides Analysis (SW1311/8081) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DIF RegLvl Run Analyst Sludge 001 217/2020 Chlordane, total 0.125 N❑ mg/L Sludge EPA 80816 5 0.0300 2/1512020 SEK Sludge 001 2/7/2020 Toxaphene 0.250 ND mg& Sludge EPA 8081E 5 0.500 2/15/2020 SEK Sludge 001 2r7/2020 Enddn 0,0125 ND mg/L Sludge EPA 8081E 5 0,0200 2/15/2020 SEK Sludge 001 2/7/2020 gamma-BHC 0.0125 ND mg1L Sludge EPA 808113 5 0.400 2/1512020 SEK Sludge 001 2f7/202O Heptachlor 0,0125 ND mg1L Sludge EPA 8081E 5 0.00800 2/1512020 SEK Sludge 001 217/2020 Heptachlor epoxide 0.0125 ND mg1L Sludge EPA 8081E 5 0,00800 2/15/2020 SP-K Sludge 001 217/2020 Melhoxyahlor 0.0125 ND mg/L Sludge EPA 80816 5 10.0 2/15/2020 SEK Sludge 001 2/7/2020 Surr, TCMX 10-110 55.1 %Rec Sludge EPA 00818 5 2115/2020 SEK Sludge 001 217/2020 Sum OCI3 10-119 84.8 %Rec Sludge EPA 8081E 5 2115/2020 SEK Page 4 of 36 SUMM-9S I 3310 Win S!. WON: 20020508 LT FNVlnQN4l1 NTAL TLC14NOLp{31ES, Inc Cuyahoga FoOhio 44223 Date tiells, P orted: Z121120 0 ntilyrlcal Laborarorles 79L: (330) 253-8211 FAX.• (330) 253-4489 Company: Cascades Tissue Group - North Carolina I Webslre: tt :/An ttjtk.eon, Address: 805 Midway Road Rockingham NC 28379 Received: 2/8/2020 Project#: Waste Characteri TCLP'Volatiles Analysis Client ID# Lab ID# Collected Analyte Rep Lrnt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 2FI2020 1,1-Dichloroethsne 0,100 ND mg/L Sludge EPA 8260D 100 0,700 2/13/2020 MES Sludge 001 2/7/2020 1,2-Dichloroethane 0.100 ND mg/L Sludge EPA 8260D 100 0,600 2/13/2020 MES Sludge 001 2/7/2020 MEK 2.00 ND mg/L Sludge EPA 8260D 100 200 2/13/2020 MES Sludge 001 2/7/2020 Benzene 0.100 NO mg/L Sludge EPA 8260D 100 0.500 2113/2020 MES Sludge 001 2/7/2020 Carbon tetrachlorlde 0,100 ND mg/L Sludge EPA 8260D 100 0,500 2/13/2020 MES Sludge 001 2/7/2020 Chlorobenzene 1.00 ND mg/L Sludge EPA 8260D 100 100 2113/2020 MES Sludge 001 2/7/2020 Chloroform 0.100 N❑ mg/L Sludge EPA 8260D 100 6.00 2/13/2020 MES Sludge 001 2/712020 Tetrachloroelhene 0,100 ND mglL Sludge EPA 8260D 100 0.700 2/1312020 MES Sludge 001 2/7/2020 Trichlaroethene 0.100 ND mg/L Sludge EPA 8260D 100 0.500 2/13/2020 MES Sludge 001 2/712020 Vinyl chloride 0.0500 ND mg/L Sludge EPA 8260D 100 0.200 2/13/2020 MES Sludge 001 2/7/2020 Surr; 4- 70-130 93.7 %Roe Sludge EPA 8260D 100 2/13/2020 MES 8romofluorobenzene Sludge 001 2/7/2020 Surr: 70-130 98.8 %Rec Sludge EPA 8260D 100 2/1312020 MES Dlbromofluaromethane Sludge 001 2/7/2020 Surr: Toiuene-d8 70-130 98.8 %Rec Sludge EPA 8260❑ 100 2/13/2020 MES TCLP Semi-Volatiles Analysis (S'WI 311/8270) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 2/7/2020 IIA-Dichlorobenzene 0.200 ND mg/L Sludge EPA 8270E 2 7.50 2/14/2020 SFG Sludge 001 2/7/2020 2,4,5 Triehlorophenol 0.500 N❑ mgll, Sludge EPA 8270E 2 400 2114/2020 SFG Sludge 001 2f7/202O 2AA-Trlchloraphenal 0,500 ND mg1L Sludge EPA 8270E 2 2.00 2/14/2020 SFG Sludge 001 2/7/2020 2,4-Dinitrotoluene 0.100 ND mg1L Sludge EPA 8270E 2 0.130 2/14/2020 SFG Sludge 001 2/7/2020 Cresols, Total 10.0 NO mg/L Sludge EPA 8270E 2 200 2/1412020 SFG Sludge 001 2/7/2020 Hexechloro-1,3- 0.0400 NO mgll� Sludge EPA 8270E 2 0.500 2/14/2020 SFG buladlene Sludge 001 2/7/2020 Hexachlorobenxene 0.100 ND mg/L Sludge EPA 8270E 2 0.130 2/14/2020 SFG Sludge 001 2/7/2020 Hexachloroalhane 0.200 ND mg/L Sludge EPA 8270E 2 3.00 2/14/2020 SFG Sludge 001 2/7/2020 Nitrobenzene 0.200 N❑ mg/L Sludge EPA 8270E 2 2.00 2/14/2020 SFG Sludge 001 2/7/2020 Pentachlorophenol 0.500 ND mglL Sludge EPA 8270E 2 100 2114/2020 SFG Sludge 001 217/2020 Pyridine 0.500 ND mglL Sludge EPA 8270E 2 5.00 2/14/2020 SFG Sludge 001 2/7/2020 Surr: 2-Fluorophenol 10-109 70.6 %Rao Sludge EPA 8270E 2 2/14/2020 SFG Sludge 001 217/2020 Surr: Phenol-d6 10-109 75.6 %Rec Sludge EPA 8270E 2 2/1412020 SFG Sludge 001 2/7/2020 Surr: Nitrobenzene- 19-120 72.2 %Rec Sludge EPA 8270E 2 2/14/2020 SFG d5 Sludge 001 217/2020 Surr: 2,4,6- 10-120 93.5 %aRoe Sludge EPA 8270E 2 2/14/2020 SFG Trlbromaphenol Sludge 001 2/7/2020 Surr: 2- 22-117 67.2 %Rec Sludge EPA 8270E 2 2/1412020 SFG FluorobEphenyl Sludge 001 2/712020 Surr: p-Terphenyl- 34-116 91.1 9/.Rec Sludge EPA 8270E 2 2/14/2020 SFG d14 Page 5 of 36 Summil Environmental Technologies, lac. �TSUMEAIEI- 3310 Win&. rHC Cuyahoga Falls, Ohio 44223 An,.7ty(joal Laboraiorlog TEL: (330) 253-8211 FAX (330) 253-4489 Websile: htt altek.c n WO#: 20020508 Date Reported; 2/21/2020 Company: Cascades Tissue Group -North Carolina I Address: 805 Midway Road Rockingham NC 28379 Received: 2/8/2020 ProjectO: Waste Characters TCLP Herbicides by EPA 83215 Client ID# Lab IN Collected Analyse Rep Lmt Result Units Matrix Method DIF RegiLvl Run Analyst Sludge 001 2/712020 2,4-d 0,500 0.600 mg/L Sludge EPA8321D 50 10.0 2/1312020 BJH Sludge 001 217/2020 2,4,5-TP 0.500 NIA mg& Sludge EPA 8329E 50 1.00 2113/2020 BJH Sludge 001 2/712020 Surr: DC,AA 70-130 98.7 %Re4 Sludge EPA 8321B 50 2/13/2020 BJH Page 6 of 36 �tUl111t1f GrtyN•onNtanid! 7`echnoJdgies, Inc. �T�'Summllr IlltllC�.I OP> 3310 FYin SL � P ENVIEIQNh1814TALTMINDLOGiFS, INN. Clryah09dFalls. Ohio 44223 (consolidated) A,7alyttea! Letts raiarl s TEL: (330) 233-8211 F.4d': (330) 253,4489 WO#: 20070508 Websile: hffp://lpn+li,seliek-rnrrr Date Deported: 2/21/2020 CLIENT: Cascades Tissue Group - North Carolina Inc Collection Date; 2/7/2020 8:00:00 AM Project; Waste Characterization Lab ID: 20020508-001 Matrix: SLUDGE Client Sample ID: Sludge Analyses Result PQL Qual Units DF Date Analyzed RCI-SOLID-Wl IGNITABILITY1030 REACTIVE CYANIDE (901417.3.3.2)-SOLID Cyanide, Reactive NIA 0.446 mg1Kq RCI-SOLID-WI IGNITABILITY1030 ICNITABILITY OF SOLIDS (SW�846: 1030) Ignitability non-flammable RCI-SOLID WI IGNITABILITY1030 PH (5W9045D) pH T3 RCI-SOLID-WI IGNITABILITY1030 REACTIVE SULFIDE (9034)/7.n.4.2 Sti lde, Reactive ND SW9014 SW1030 mmisec SW9045D s.u.@z0-oC SW9034 25.0 mg/Kg Analyst: MS 1 2119/2020 10:33:00 AM Analyst: AJT 1 2/10/2020 1:00:00 PM Analyst: VVK 1 211012020 4:22:07 PM Analyst: MS 1 2/19/2020 10:33:00 AM Qualifiers: H Holding tlmaemrPreparalionoronolplsaxaeaded M Menusllmogrntineused 1pdetorminenraereapamo ND Mot Dateded ESL Permit Limit ES RFD outsida accgplcd reeovary limits RL Raparting DeterAgn Limit W Sample Wnlpiner tOMPOMUra id wl offirrdt N apeelfrad of tartcodq Original Page 7 of 36 Summit Environmenraf Technoio tes, Ina R~' 14 3310lYhTSF. QC SUMMARY REPORT ENVIRONPAKNTALT CH=L0019S,:hc Cuyahoga Fails Ohio44223 A,r 0yrical LAl rlrator'l�e TEL: (330) 253-8211 F.4X- (330) 253-4489 WON: 20020508 Websrre: coal 2I-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Projeet; Waste Characterization BatchlD• 41983 Sample I❑: 1013-41983 SampType: MBLK TeslCode: TCLP VOC-M Units: mg1L Prep Date: 2H112020 Client ID., Pes Batch I❑: 41983 TesM: SW8260 SW1311M Analysis ❑ale: 21'1212o2o Analyte, Result PQL SPK value SPK Ref Val %REC Lowl-imil HeghUmit RPD Ref Val 1,1-Dic4lamethene ND 0,0500 1,2-❑ialoroethane ND 0.0500 MEK ND 1.00 Benzene NO 0.05DQ Carbon letrachlodde No 0.0500 Chlembenzene ND 0.500 Chlorofarrn ND 0.0500 Tetrachloroethene ND 0.0500 TOchloraethene ND DA500 Vinyl chloride ND 0.0200 Surr.4-Btnmolluorobenzene 459 504.0 91.8 70 130 Surr. ❑ibromo0ucromethane 500 500.0 100 70 130 Sun' Tolvene48 497 500.0 99.3 70 130 Qualifiers: B Anaiyte detected in the associated Method Blank d Analyte detected below quantitstion l imi is NO Not ❑elected R RPD outside, accepted recovery limits RunNo: 1 U9311 SegNo: 2626133 %RPO RP❑Urnil Qual E Matue above gt=11tation range H Holding limes for preparation or anal% M Manual Integration used to determine area response MC valtte isbelow M inimum Compound P Second column confirmation exceCds. PL Permit Limit lL Reporting Detection Limit S Spike Recovery outside accepted reap Original Page 8 of 36 r �w.3 g EJ- 33117WInA QC SUMMARY 5�w1m�t£rav�o�enlerr�a� Technologies, for. REPORT EKIVInONNI�WnLYCHNOt,0ei_=S, 1KC Cuyahoga Falls, Ohio 44223 rlrr�rlgticalLabafalorf_s TESL:(330)253-8211FAX--030j253-4499 O#: 20020508 IFrebsile_ hay.lA inr.sellekcoon 2I-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchID: 42013 3ample10: ME3.42013 SampType: M3LK TestCode: MU-TCLP-7(5 Units: mg1L Prep Date: 211312020 RunNo- 109289 :Genf ID: PBS Batch ID: 42013 Testhla: SW6014d SW3010A Analysis Rate: 211312020 SegNo- 2626427 4nalyte Result PCL SPK value SPK Ref Val %REC Lowt<irnit Hghl-hlt RPD Ref Val %RPD RPDLitnh Qual TCLP ArsenMAs) ND 0.500 TCLP Barium(Sa) ND 5.00 TCLP Cadmium(Cd) N€] 0.100 TCLP Chromium(Cr) ND 0200 TCLP Lead{Pb) ND 0.500 TCLP Selenium(Se) ND 0.0500 TCLP Si[ver(Ag) ND 0.500 iample 10, LCS-42013 SampType: LCS TestCode: Mil TCLP-7(6 Units: mg1L Prep Date: 7f1312020 RunNo: 109289 :fient ID: LOSS Balch lD: 4ZO13 TestNo: SW60100 SW3010A Analysis Date: 2f1312020 SegNo: 2626428 4na[yle Result PQL SPK value SPK Ref Val %REC Lowl-irnit H[ghLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.11 0.500 2Ad0 0 105 80 120 TCLP Barium(Ba) HD 5.00 2.000 0 111 80 120 TCLP Cadmium(Cd) 9.96 0.100 2.000 0 9B.2 80 120 TCLP Chromiutn(Cr) 2.06 0.200 2.000 0 103 80 120 TCLP Lead(Pb) 2.14 0500 2.000 0 147 80 120 TCLP Selenlum(Se) 2.05 0.0500 2.000 0 103 80 120 TCLP Silver(Ag) 2.25 0.500 2.000 0 113 80 120 QuAlleerst B Analyte detected in the associated Method Blank E Value above quantiiation range H Holding times for preparation or analt J Analym detected below quentitation limits M Manual imtegratian used to determine area response MC Value is belmv Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside aomepted recovery limits Rt. Reporting Detection limit S S pike Recovery outside accepted reap Page 9 of 36 �"' F��"} f'?suik�-U SruRmil Enuironrirer�lQ1 Teehnologfes, One,(�C SU Ml.C� i �j Lll�TM9 Y; �;� 4�i 331 p Whi 8L ENVIROMME -qTAL TECH NOL(76]$S;, MrC Cuyahoga Falls, Ohio 44223 Am-FtytlC3l Labar--torf s TEL: (330) 253-8211 FAX' (330) 253-4489 O#: 20020508 Websile' hfrP.-1An t.Selfek.caa! 2I-Fa20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchlD- 42013 Sample ID: TCLP BLANK 211212 SampType: MBLK TestCode: MtC TCLP-7(5 Unift mgiL Prep Date: 21131202E RunNo: 109289 Client 10: PBS Batch ID: 42013 TestNo, SW601CID SW3010A Analysis Date. 211312020 SegNb: 262B42S Analyle, Result PQL SPK value SPK Ref Val %IEC LowLirnA Night-imit RPD Ref Val %RPD RPE)Limit Qual TCLP Arsenic(As) ND 0.500 TCLP Barium(Sa) ND 5.00 TCLP Cadmium(Cd) ND 0.100 TCLP Chromium(Cr) ND 0.200 TCLP Lead(Pb) ND 0.500 TCLP Selenium(Se) ND 0.0500 TCLP Silver(Ag) ND 0.500 Sample ID. 2002050MOIAMS SampType: ENS TeslCode. Mtl-TCLP-7(6 Units: mgiL Prep Date: 211312020 RunNa: 1092a9 Client ID: BatchQC Batch ID: 42013 TeslNo: SW6010D SW3010A Analysis Date: ?113f2020 SegNo: 2626438 +byte Resu t PQL SPK value SPK Ref Val "%REC LowL'onit Hight-imit RPD Ref Val %RPD RPDUrnit Qua? TCLP Arsenic(As) 2.16 0.500 2.000 0 108 70 130 TCLP Badum(Sa) ND 5.00 2.00D 0.2736 81.2 70 130 TCLP Cadmium(Cd) 1.75 0.100 2.OW 0.4D2100 87.5 70 130 TCLP Chromium(Cry 1.84 0200 2.000 0.008900 91.8 70 13D TCLP Lead(Pb) 1.80 0.500 2.000 0.009000 89.8 70 130 TCLP Setenbrn(Se) 2.11 0.0500 2.000 0 105 70 130 TCLP Silver(Ag) 1.98 0.600 2.001) 0.007300 98.7 70 130 Qualifiers: B Analyte detected in the associated Method Blank E Value abavc quantitation range H Hold ing times for preparation ar anal% 3 Ar►alyte detected below quantitalion limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds FL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Lim it S Spike Recovery Outside accepted recO Page 10 of 36 5'emorr�ii ErrvirawrrAertfaf Tetfinologres, fne. (TSUMMOT 3310 Win Sf. C SUMMARY REPORT eMWIGMAEwALTEr—HnC)LC) Gi�S.lr,C Cuyahoga Falls. Ohio 44223 Analy lical LaLamor!_s TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 20020508 IYebsiie: hfl :IhrtviN.seffek.Com 21-Fe i-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchII}- 42013 Sample 10: 20020BOMO1AMSO SarnpType: MSD TestCade: Mll-TCLP-7(6 Units: mgrL Client ID: BatchQC Balch 10: 42013 Testhlo: SW5010D SW3010A Analyle TCLP Arsenko As) TCLP Barium(Ba) TCLP Cadrniurn(Cd) TCLP Chroml n(Cr} TCLP Lead(Pb) TCLP Selenfum(Se) TCLP Silver(Ag) Result PQL SPK value SPK Ref Val Prep Date: XIN2020 RunNo: 109289 Analysis Date: 2 IN2020 SegNo. 2626439 %REC LowLlmil Highl-iniit RPD Ref Val %RPD RPDI-imit {dual 2,14 0.500 2.000 0 107 70 130 2.156 0.698 20 ND 5.00 2.000 0.2736 80.5 70 130 0 0 20 1.76 0.100 2-000 0.002100 87.6 70 130 1.753 0.114 20 1.84 0200 2.000 0.008900 91.4 70 130 1.844 0.435 20 1.80 0.500 2.000 0.009000 89.6 70 130 1.805 0.166 20 2.09 0.0500 2.000 0 106 70 130 2.108 0.762 20 1.96 0.500 2.000 0.007300 97.7 70 130 1.982 1.07 20 Qualifiers: B Analyie detected in the associated Method Blank J Analyte detected Wow quantitatian limits ND brat Detected R RPD outside aeeepted recovery limits E Value above quantitatian range H Holding times fflr preparation or anal} M Manuat lntegiation used to aeiermine area response MC Value is WOW Min imam Compaurnd P Second column confirmation exceeds PL Permit Limit RL Reponiag Detection Limit S SPike Recovery outside aoeepled reco Original Page 11 of 36 smEWSPlifumEnmental Tehnofg, I.�=�,{ �_;�,.CUMMARY S�r����� � 3310 i3'rrrSt. REPORT�' QL. k7 V ENVINONPal EMTRLTEE CHNOLOrIES, p.0 CtWkogaOhro44223 AJ?,rrtytlJa� ! abcraromc TEL: (330) 253-8211 FAX:030) 253-4489 O#: 20020508 Ilebsire:hrr :Ihrahi_serrekeorn 21-Feb-29 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchrD- 42030 Sample ID: MB-42030 SampType: MBLK TestCode,. SVOC-BNA T Units: mgJL Prep Date: V131202D RunNo: Client 1D: PBS Batch iD: 42030 TesINo: SW8270 SW351dC Analysis Date: 1o94o7 2MV2020 Seghla: 2629241 Analyte Result PQL SPK value SPK Ref Val °%REC Low l-im it N9hUmit RPD Ref Val %RPD RPDLim ft Qual 1.4-Dichlora6enzene ND 0.100 2,4.5-Triehlomphenol ND 0260 2,4.6-Trichlorophenol HD 0.250 2.4-Dinitroteluene ND 0.0600 o-Cresol ND 0.250 Cresols, Total ND 5.00 Hexachlom-1,3-butadiene ND 0.0200 Hexachiorobenzene HD 0.0500 Hexachloraethane ND 0.100 Ni-Irobenxene NO 0.100 Penlachlorophenal ND 0.250 Pyridine HD 025D Surf 2-Fluorap4enol 0.630 i.000 63.0 10 109 Surr Phenol-d6 0.674 i.000 67,4 10 109 Surr. Nitmtenzene-d5 0.696 1.000 69.6 19 120 Surr. 2,4.6-Tribromophenal 0.863 1.000 N.3 10 120 Surr. 2-Fluorobiphenyl 0.683 1.000 68.3 22 117 Surr; p-Terphenyl-d14 0.992 1.000 99.2 34 116 ¢uzlifers: S Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analt J Anslyte detected below quantitateon limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Seoond column confimmtion exceeds PL Permit Limit QriginaI R RFD outside accepted recavery limits RL Reporting Detection Um it S Spike Recovery outside accepted reco Page 12 of 36 SUPR�Rm 5�rr+lAril L�rtuFronmer�iQi Techrrofogies. fire.L. '�li 1i.Crr V� 3310 Win Si- E2VJR0tJL]=wrrAL 7�c raAliS tpS. I:JC Cuyahoga Falls, Ohio 44223 Armlydcal LiEnraios�t� TEL. (330) 253-8211 FAX-- (330) 253448.9 WO#: 20M508 13'sbsfre: f ii :!l�i�mt ,seiiekcoon 21-Fe&20 Client: Cascades Tissue Group - North Carolina Inc Frojecf: Waste Characterization SatchID: 42030 Sample ID: LCS-42030 SampType: LCS TesWode: SVOC-BRA T LlMs: mglL Prep Date: 2f73f2ff20 Client ID: LCS5 Batch ID; 42030 TeatNo: SVV8270 SW3510C Analysis Date: 211412020 Ana[yle Result PQL SPK vatue SPK Ref Val %REC LowL[mit HighLim[k RPD Ret Val 1-Dichlorobenzene 0.345 0.100 0,8000 4 43.1 36A 130 2,4,5-Trichlorophenal 0.819 0.250 0-8000 0 102 31.7 132 2,4,6-Trichloroirheno[ 0.811 0.250 0.800o 0 101 31-1 133 2,4-DINrotoluene 0.843 0.0500 0-8000 0 105 43.3 130 o-Cresol 0.579 0.250 0.8000 0 72A 32.9 130 Cresols, Total ND 5.00 1.600 0 76.1 31.7 130 Hexachloro-1,3-buladiene Q.374 0.0200 0.8000 0 46.8 31.4 130 Hexachlorobenzene 0.644 0.0500 0.8000 0 80.6 43.1 130 Hexachloroethane 0.279 4.100 0.8000 0 34.9 36.5 130 Nftbenzene 0.528 0.100 0.8000 0 66.0 39.5 130 Penta&loropheno[ 0.675 0.254 0-8000 0 84.4 34 130 Pyridine 0.503 0.250 0.B000 4 62.8 10 130 Surr. 2-FluorophenaJ 0.659 1.000 65.9 17.1 130 Surr: Phenol-d6 0-709 1.000 70.9 10 130 Surr. Nitrobenzene-d5 0.698 1.000 89-8 32.6 130 Sun: 2,4, 6-TNbromophanol 0.981 1.000 96.1 4.43 130 Surr, 2-F[uorob[pheny[ 0.731 1.000 73.1 41.8 130 Surr. p-Terphenyl-c!14 0.950 1.000 95.0 36.4 130 Qua€ifier& B Analyze detected in the assoeiared Melhod D tank J Analyze detected h orw quantita#ion limits ND Not Detected R RPD outside accepted recovery limils RunNo: 10940T SegNo. 2629242 %RPD RPDUrnil Qual E Value above quaotitation range H Ho[ding limes forprepamtion or anal% M Manual lnlegra#inn used to determine area response MC VaItte is below Min[mum Compound P 3=0nd column cumfumation exceeds PL Perm it limit RL Reporting Detection Limit S Spike Recovery outside accepted repo Original Page 13 of 36 s SifmlAll EAVlTOJ7AY217tQl TeCfPllwOg!@Sr Inc. tI C SU �1TIr1 REPORT 33f0VIinst. Y ,l. ENVVIONP11EWAt -uCwjmn4�i=s,pic CrryahogaFalls, Ohio 4223 - Anariy6cal Labor-21orks TEL. (330) 253-8211 FAX: (330) 253-4489 WO#: 20020508 Welsife: �il�Aroirmicserrekeam 21_Feb-26 Client: Cascades Tissue Group -North Carolina Inc Project: Waste Characterization HatchlD: 42030 Sample ID. 20020506-OOIAMS SampType: MS TestCode: SVOC-BNA T Units: mglL Prep Date: 2M31202a RunKo; 10407 Ciienl ID: BatchQC Batch rD: 42030 TestNG, SW8270 SW3510C Analysis Date: 2114J2020 SegNcx 2629245 AaWe ResuEt PQL SPK value SPK Ref Val %REC LowLirnil Highl_itnit RP[) Ref Val %PPD RPDUrnil Qual 1,4-01chlorobenzete 0.536 0.200 0.8000 0 67.0 33.8 126 2,45-Trichlorophenol 1.03 0.500 0.8000 0 129 28.7 144 2.4,6-Triehlomphenol 0.988 0.500 0.80U0 0 124 12.8 153 2,4-olnitrotoluene 1.04 0.100 0.8000 0 129 20.4 155 0-Cres01 0.825 0.500 0.8000 0 103 10 148 Cresols, Total ND 10.0 1.600 0 106 10 148 Hexachloro-1,3-butadiene 0.472 0.0400 0.8000 0 59.0 29 126 Hexachlorobenzene 0.774 0.100 a.a000 0 96.8 33.7 134 Hexachloroethane 0.418 0.200 0.8000 0 52-3 32.8 132 Nitrobenzene 0.740 0.200 0.8000 0 92.5 20 158 Per0chlorophenol 0.705 0.500 0.8000 0 88.1 10 176 Pyri&ne 0.672 0.500 0.8000 0 84.0 10 130 Surr. 2-Fluaropheaol 0.968 1.000 95.8 3.39 130 Surr, Phenokc!6 0.991 1.000 99.1 5 130 Surr Hlimberawe-d5 0.972 1.000 97.2 14.5 154 Surr 2,4,6-Tribrnmaphenol 1.16 1.000 116 19.5 130 Surr 2-Fiuombiphenyl 0.894 1.000 89.4 34.4 130 Surr: p-Terpheny€-d 14 1.11 1.000 ill 8.86 156 Qualifiers: 3 Analyte detected in the associated Method Blank J Analyte detected belawquan6tatioo limits ND Not Delected R RP€1 outside accepted reeovery limits E Value abovequantitation range H Holding times for preparation aranaE; M Manual integration used to determine area response MC Value is belrnv Minimum Compound P Second culumn confirmation exceeds PL Permit Limit RL Reporting Detection limit S Spi}:e, Remvery outside accepted MC0 Original Page 14 of 36 Smrmil EnvirnnmLnw1 Technologies, Inc. m9summn 33101fffn sr_ QC SUMMARY REPORT E %11r(OAiMENTAL i-ciinoLar3;s. rp,c C*WhvgaFafls. Ohio 44223 Anar ylfa4l L-aboraforlee TEL: (330) 253-8211 FAX.- 030) 253-4489 WON: 2002MB Websire: hrr ll inu.sertekevnr 2I-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchlD: 42030 Sample JD. 2002050MOIAMSO SampType: MS Tes[Ude: SVQC-SNA T Units: mgFL Client ID: BatehQC Batch ID: 42030 TesINo. SW8270 SW3510C AnWyte 1,4-D'ochlorobenzene 2,4,fi-Trichfaropbenof 2,4,6Tdchlorophenvl 2,4-Dinr#rotoluene o-Cresol Cresols, Total Hmuchloro-1,3-butadiene Hexachlorobenaene Hexachraroethane, Nitrobenzene Penlachlorophenol PyFkflne Burr. 2-Fluormphenol Surr. Phenol-& Surr. N-drobenzeneAS Surr: 2,4,6-Tribromophenol Surr: 2-Fruorobiphenyl Surr. p-Terphenyl-d14 Result POL SPK value SPK Ref Val Prep Date: 211312020 Analysis Dale: 21u=o %REC LowLrmil HighUMit RPb Ref Val RunNo: 1094g7 SegNva 2629246 °%RPD RPDLirnt Qual 0.322 0.200 0.8000 0 40.3 33.8 126 0.5360 49.8 30 0.8% 0.5m 0.8000 0 107 28.7 144 1.030 18.0 30 0.859 0_500 0.8000 0 107 128 153 0.9884 14.0 30 0.852 0.100 0.8000 0 106 20.4 155 1.036 %5 30 0.5% 0.500 0.8000 0 74.6 10 148 6.8252 32.2 30 ND 10.0 1.600 0 79.4 10 148 0 0 3G 0.336 O.&WO 0.8000 0 42.1 29 126 0.4716 33.5 30 0.652 0.100 0.81)00 O 81.6 33.7 134 0.7744 17.1 30 0.280 0.200 0.8000 0 35.0 32.8 132 OA184 39.5 30 0.563 0.200 0.8UOO 0 70.4 20 158 0.7396 27.1 30 0.616 0.500 0.8000 0 77.0 10 176 0.7048 13.5 30 ND 0.500 0.8000 0 51.3 10 130 0.6720 200 3fl 0•6m 1•00D 63.0 3.39 130 0 0.73D 1.000 73.0 10 130 0 0.754 1.000 75.4 14.5 154 0 4.975 1.000 97.5 19.5 130 0 0.751 1.000 75.1 34.4 130 0 O.909 1.000 90.9 8.86 156 0 Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected belottt quantitat ion I Emits ND Not Detected R RPD outside accepted recovery limits E Value ahave quanlitation range H Holding times for preparatitm oranal+ M Manual Integration used to deterni[ne area response MC Valeta Is below Minimum Compound P Second column confirmation exceeds PL Perm rt Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco R R R R R Ori&a.] Page 15 of 36 SummirE" ronmenlal Technafngles, h7c. 3310 Win Si. YC U JL.lJti EsNVII?Ol�lFIENTALTC3�t�,OLOGIC-S,itxC CxgahggffFaRs Ohio44223 SUMMARY REPT Anaiyilcaf Laboralorl" TEI • (330) 253-8211 FAX.• (330) 253-� 0p O#: 20020508 WeiWee. hgv.-/Ainwvserrekcom 2I-Feb20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchID: 42055 Sample ID: MB.42055 Client ID, PBS Analyte TCLP Mercury Sample ID: LCS42055 Client ID: LCSS Analyle TCLP Mercury SampType: PdBLK Batch 1D: 42055 Result ND SampType: LCS Balch 111: 42055 Result 0.00390 Sample ID: TCLP BLANK 2-13-2 SampType: MBLK Cltertt ID: PBS Balch 1D: 42055 Analyle Result TCLP Mercury ND Sample ID: 20020549-001AMS SampType: MS Client ID: BatehOC Balch ID. 42055 Anatyte Resutl TCLP Mercury 0.00450 TestCode: HG TCLP�74 Urflts- PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 TestCode: HG_TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.0020Q 0.00400 0 TestCode: HG_TCLP{74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 TestCode: HG_TrLP{74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 0.00400 0 Prep Date- 2l1712020 Analysis Date: 2f17f2020 °Io-REC LowL!mft Hight-imit RPD Ref Val Prep Date: 211712020 Analysis Dale: 211712020 %REC LowLlmil Highl-hit RPD Ref Val 97.5 80 120 Prep Date: 2 I712020 Analysis Date- 211772D20 %REC Lowt-imit HighUrnit RPD Re4 Val Prep Date: 2117/2020 Analysis Date: 2f1712420 %REC Lowl-knit HighLumi# RPD Ref Val 112 75 125 RunNo: Z09429 SegNo: 263♦)9413 %RPD RPDLimit Qual RunNo: 189429 SegNo: 2630911 %RPO RPDLirn t Qua1 RunNo.- TO$429 SegNo: 2531230 °%RPD RPDLimh Quat RM N4: 109429 SegNo: 263124-F °%RPD RRDLimit Qual Qualifiers: B Analyte detected in the asucialed Method Blank E Value above quantitation range H Holding times for preparation or anat3 7 Analyte detected below quantitation I units M Manual Integration used to determine area response MC Value is below Min imum Compound ND Not Detected P Second column confermatinn exceeds PL Permit Lim[[ Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside ailed reca Page 16 of 36 sumn-arv SrernrnirEnvirnnrnenrafTerhnofagies,Inc, 3310 Ilan Sr. QC SUMMARY PORT Eli VIRONIAEhJTAL rcHNoLOG!cS. IF2C Cvymkoga Falls, Ohio 44223 Analyi1 a1 Labarmarles TEL. (330) 253-821 f FAX- (339) 253-4484 WO#: 20020508 'ebsile: hrr Ihino�v.serrekrom 2I-Fe&20 Client: Cascades Tissue Group - North Carolina Inc Project Waste Characterization BatchlD: 42055 Sample lD: 20020549-0OIAIIIIS SampType: MS Tes#Cade: HG_TCLP174 Units: ppM Prep Date: 211712620 RunNo: 109429 Client 10., BatchQC Balch ID: 42055 TestNo: SW7470A SW7470A Analysis Date: 211712020 SegNa: 2631241 Analyle Result PQL SPK value SPK Ref Val %REC LowLtmll Hlgh m it RPD Ref Var %RPD RPDUrnR Qual SamPle ID: 2002iM49-041AMSD Catent ID: BatchQG SampType: i ISD Batch ID: 42055 TestCode: HG_TCLP(74 TestNa: SW7470A R3niis: PPM SW7470A Prep Date: V1712020 Analysis Date: 2 I712020 RunNo: '109429 SecINO: 2631242 Analyte TCLP Mercury Result 0.00421 PQL SPK value SPK Ref Val 0.0024D 0.00400 0 %REC Lowl-irrt it HighUmit RPD Rel Val 105 75 125 0-00450 %RPD RPDUmit Qual 6-66 20 Sample ID: M132-42055 Client ID: PBS SampType: MBLK Batch ID: 42055 TestCode: HG_TCLP(74 TestNo: SW7470A Uit]ts: PPM SW7470A Prep Dale: 21171ZD20 Analysis Date: 211712020 RunNo: 109429 Segft 2631244 Analyte Result PQL SPK value SPK Fief Val %REG LowLimit Htghl imil RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND O.Oo20O Sample tD: TCLP BLANK 2-14-2 SampType: MaLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 2d1712020 RunNo: 109429 Client ID: PBS Batch ID: 42055 TestNO: SVV7470A SW7470A Analysis Date: 2117f2420 SegNo: 2631260 Analyte Result PQL SPK Value SPK Ref Val %REC LowlUfmft Highl-imi# RPD Ref Val %RPD RPDLirnit Qua] TCLP Mercury ND 0.0=0 Qualifiers: B Analyte detected in the associated Method i3tank E Value above quantitation range I•f Hording times rorprepamtinn oranai% J Analyte detected below quantitation limits M Manual Inlegoiion used to determine area response MC Valae is betawM1111imum Compound ND Not Detected P Smund Column confirmation weeds PL Perm it Limit Original P, RFD outside accepted recovery limits RL Reporting Detection Lim it 5 Spike Reoouery outside accepted taco Page 17 of 36 A SummrrErrvirnfrnr¢Mral Teehnniogres, frre. QCSUMMARY r �ll� t "w , IT 33f0WnSf, � ENVrP0?JPd1n%1TJkL,;trC Cxyaah09aFldls.Ohro44223 A;?7—FtYGCCI LaboFarorf_ c TEL (330) 253-8211 FAX.- (330) 253-4489 WO#: 20020308 IiKebsrre: hCrn_lhYu�s_se[ret�earat 21-Feh-20 Client: Cascades Tissue Group - Forth Carolina Inc Project: Waste Characterization Batchl]D: 42055 Sample tlx: M83-42055 SampType: MBLK TeatCode: HG 7CLP(74 Units: PPM Prep Date: 211712020 RunNo- 109429 Clent ID: PBS Batch ID: 42055 TestNo: SW7470A SW7470A Analysis fate: 211712p20 SegNo: 2531265 Anaty to Result PQL S PK value SPK Ref Val %REC LawLi n ft HighLimit RPD Ref Val %RPD RPDLimil Quaff TCLP Mercury NO 0.00200 Quolifters: B Anslyte detected in the associated Method Blank .r Anaiyte detected below quantization limits ND Not Detecied R RPD oazside accepted recovery limits E Value above quantitation range H Molding times for preparation or anal; M Manual Integration used to determine area response MC Value is below Minimums Compound P Seoond column confirmation exceeds PL Perm it Limit RL Reporting Detectian Lim it S Spike Recovery outside accepted reco Original Page 18 of 36 � ��; 3314WnT SurMmit Eravirnrrmentaf Tecfi�vfagies, foe_ QC SUMMARY REPORT 3wi M T 5t_ ENVIftOA MENTAL TECliNOLOG9�S, MC Cuyahoga Faifs, Ohio 44223 ARaIJg[Cai L2b0rnrcrfes TEL: (330) 253-8211 FAX-- (330) 2S3-4489 Wile,: 20020508 Febrile: 21-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization Batchl:D: R109137 Sample ID: CHECK 7 Ckent ID: LOSS Analyte PH SampType: LCS Balch ID: R109137 Result 7.0 TestCode: pl- S(9045D) Unils: s.u.@20.4C Prep Date: TestNo: SW90450 Analysis Date: X1012020 PQL SPK value SPK Ref Val °%REC LawLirnit HlghLimil RPD Ref Val 7.0 0 100 90 110 RunNo: 109137 SegNv: 2518522 %RPD RPDLitnit Qual Qualifiers: 3 Arra€yre detected in the associated Method Stank E Valve above quantitation range H Holding times for preparation nr anal, J Artalyte detected below quanli Cation 1 Emits M Manual Integration used to determine area response Me Value is below Minimum Compound ND lot Detected P Second column canfirmaticm exceeds PL Permit Limit Original R RFD outside accepted recovery limits RL Reponing Deaection Limit S Spike Recovery outside accepted reco Page 19 of 36 ffJ ZU5RM2EW- .SummitF-rrvFr'oMmeMralTeehtafngfes,fnr. 3310Win & QC SUMMARY REPORT ENVIPONfat_nTALTr- cHnoLCGIES, ]gC CuyahogarFalls, Ohio 44223 Arraiy€:cal Laboraloaio s TEL (330) 253-8211 F,iX.- (330) 253-4489 WON: 20020508 il{efuife: hrin_lhr�vti_seiledcco 21-Feb-20 CI ent: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchID• R109137 Sample Id: LCS-RJ09137 Cllent ID: LCSW Analyte PH SarnpType: LCS Batch 10: R109137 Result 7.0 TestCade: p>i_oil(9045 Units: &u.@i20.3C Prep Cate: TeStNo: MUM Analysis Cale, 2MD1202U PQL SPK value SPK Ref Val %REC LowUrnit HEghUmit RP0 Fief Va[ 7.0 0 100 90 110 Sample10. 2D020536-001ADUP SampType: DUP TestCode: pH_O[I(9045 Units: s.u.@20.5i; Prep Date: Crrenl 10. Batrhoc Batch Id: R109137 TestNa: SW9045D Analysis Cate: 211012020 Analyle pH Rcsull POL SPK value SPK Ref Val 6.8 0 Qna lifters: 13 Analyte de€ecled in the associated Mclhod 8 [aok J Analyte detected below quantitation limits NI) Not Detected R RPD outside accepted recovery limits %REC Lowl-imit H-39hLimit RPD Ref Val 0 67 RunNo. 109137 SegNa: 2616611 %RP0 RPCLimil Qual RunNo: 109137 SegNa: 2616SJ 8 %RPC RPDLirnit Qual 0.4 10 E Value abovequantiiation range H Holding times for preparation or anal, M Manual Integration used to determine area response MC Value is beloly Minimum Compound P Second column confirmaliarL exceeds PL Permit i. mEt RL RePm ng Delectloo Limit 5 Spike Recowery antside accepted Teco original Page 20 4f 36 ! Summfl Envfreamenrof Technologies, Inc. Ewa 33lD�rr sr. REPORT UjS Ui4wEPIVOIONMENTALT-.r;HKOtAGIES, JF.0 Cuyahoga FaRs.Okra 44223 447aPyrIcal Lvbo€8l0rdcs TEL: (330) M-82f1 FAX. 030) 253-4489 O#: 20020508 €vebsile: 2I-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Project. Waste Characterizattton BatchID• R109137 Sample ID: CHECK 7 Gent ID: LCSW Anaiyte pH SampType. LCS Batch ID: R109137 Result 7.0 TestCode: pH_MPW(450 UniIS: s.u.@22.4C Prep Date: Test€do: SW9045D Analysis Date: 211012(]20 PQL S PK value SPK Ref Val "%REC LcwE. m t HighUrnil RPD Ref Val 7.0 0 99.9 98.6 101.4 RtmhlO: 109137 5eghfa: 2616783 %RPD RPDLimit QuaJ Qualifiers: 9 Analyte detected in the associated Method Blank E Value above quanti[ation range H Holding limes for preparation or anal, I Analytedetected below gaantiEation Timis M Manual Integration used to deterntine area response MC Value is 6elaw Minimum Compound ND Not Detected P Second column conlirnudoo exceeds PL Perme[ Limit Orj&8l R RPD outside accepted FarovPry limits RL Reporting Detection Limit S Spike Recovery outside accepted recn Page 21 of 36 Summit ErrvTroFuieenlaf Terhrrafogies, IncRI S �Y` 7 Et-d ors{ Tj— 3310 fYrn 57_ LJ � �' SUMMARY REPORT dA+litON l lf:.NTAL S`C: MZLOGMS, INT Cuyahoga Falls; 0/no 44223 rrsh; fr i Libormlorles TEL.• (330) 2i3-82J1 FAX- (330) 1S3-4489 WQ#: 20020508 Websire: ht .1Armv.mmzk.com 21-Feb-20 Client: Cascades Tissue Croup - Noah Carolina hic Project: Waste Characterization BatchII1: R109180 Sample ID: LCS-R109180 SampType: LCS TestCade. Ignitabiifty_S Unb: Irttrysec Prep Dale: RunNa: 14918U Client ID: LCSS Batch ID: R109180 TesWa: SW103D Analysis Date: 2f1U12020 SegNo: 2619308 Analyte Result PQL SPK value SPK fief Va[ %REC Lo►IrLimit HfghLimit RPD Ref Vat %RPD RPDLi nit Qua] Ignitability 8.02 7.240 0 111 70 130 Sample 1D: 20020386-002ADUP SampType: DUP TestCode: Ignitabiifty_S Unils: mmisec Prep Date: RuriNo: 149180 Client [D: 9atehQC Batch ID: R109180 Tes€No: SW1031) Analysis Date: 2j1012020 SegNo: 2619310 Analyte Result PQL SPK value SPK Ref Val %REC LavuLimiit I fight-imit RPD Ref Val %RPD RPDLimit Qua[ Ignitabilily nan-flammable 0 a 20 Sample ID: 20020010"OIADUP 5ampTypa: DUP Client [D: BatchQC Batch rD: RIM80 Analyte Result Ignitabil4 non-flammable Sample ID: 200200OM02ADUP SampType: DUP Client ID: EatchQC Batch ID: R109180 Analyte Ignitability Result 0.380 TestCode: Ignitabillty_S Units: mmisec TestNa. SW103D PQL SPK value SPK Ref Val TestCode: l9nitability_S Units: mmisec TeslNo: SW1031) PQL SPK value SPK Ref Val Qualiriers: B Analyte deteeted in the associated Method Blank 3 Analyte detected belowquentitatian limits ND -Out Detected R RPD outside accepted recovery limits Prep Date: Analysis date. 7J1012D20 %REC LowL[mit HighlJmit RPl7 Ref Val 4 Prep Date: Analysis Dale: 21101202D %REC LowLimit HighLfmit RPD Ref Vat 0.4000 RunNa: 'fu9?80 SegNa: 2619312 %RPD RPMrnit Qual 0 20 RunNo: 109180 SegNa: 2619314 %RPD RPDLi nf# Qual 5.13 2.0 E Value above gaantite6on range H Holding times for preparation or anal+ M Manual Integration used to determine area response MC Valve is below Minimum Compound P Second milumn confrnnat[an exceeds PL Permit Limit Original RL Reporting Detcct[on Limit S S pike Recovery outside accepted reca Page 22 of 36 Swnmif Environme"tal Techrinftrgws, fnc. t MOT 3310JFin& QC SUMAURY REPORT FNVIPONMENTAL—= €H0LOG1r-S, [KC CLTaM90 Falk Ohio 44223 Anafy(I'vaf Labaralanee TEL, (330) 253-8211 FAX. (330) 253-4489 WO#: 20020508 webslfe_ hiia:!ltt�vri ,selrekCOM 2I-Feb-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Cltaracbuization BatchlD: R109180 Sample ID: 20020008-OO SUP SampType: DUP Client ID. BatchQC Balch JD. R109180 Anatyle Result Sample ID: 20020005-042ATRIP Samp7ype: DUP Client ID. BatchQC Batch ID; R109180 Ana[yte Result IgnitabiGty 0.430 Sample ID: 2002NO6403ADUP SampType: DUP Client 0: Bauch= Batch ID: R109180 Arralyte Result Ignitabil[ty not propagate Sample 1D: 20020006-003ATRIP Samp7ype: DUP Cfienl ID: BatchQC Batch ID: R109iso Analyte Result Ignitabdity not propagate TestCode: IgnitabilHy_S Unlfs: rnmisec TestNo: SWt030 PQL SPK value SPK Ref Val TeslCade: lgnitabi[ity_9 Units: mmisec TestNo: SWI030 PQL SPK value SPK Ref Va[ TestCode: Ignitabiiity_S Unb: mmisec TeslNo: SW1030 PQL SPK value SPK Ref Val TestCode: I9ttltability_5 Units: mmisec Tesftr SW1030 PQL SPK value SPK Ref Val Qualifiers, 13 Analyte detected in the associated Method Blank J Anaiyte detected below quantita[ion I Emits ND Not Detected R RPD outside accepted recovery limits Prep Date: Analysis Date: Pf1012U20 %REC LowLirnii HighLimil RPD Ref Val Prep Dale: Analysis Date: 211of202o %REC LnwLImit Hight-imit RPD Ref Val 0A000 Prep Date: Analysis Date: 211012020 %REC LowUrnit HighLimit RPD Ref Val 4 Prep Date: Analysis Date: 2110120211 %REC LowLimit Hfghl-irnit RPD Ref Val 0 RunNo: 109180 SegNo: 2619314 %RPD RPDUmd Dual RunNo: 109180 SegN0: 2619315 %RPD RPDLimit Qual 7.23 20 RunNo: 1091si3 SegNa: 2619317 %RPD RPDUmit Dual 0 20 RunNo: 109180 SegNw. 2619313 %RPD RPDLimit Dual 0 20 E Value above gwwitation range H Holding times for preparation or anal+ M Manual Intepra[ion used to dManirte area response MC Value is Mow Minimum Compound P Second column confirmation exceeds PL Permit Limit Origuial RL Reporting Detection Limit S Spike Recovery outside accepted reca Page 23 of 36 r_. Sumntlf EnvironmentalTechaofogies, inc. S� F -1 T 3310WinSh QC SUMMARY REPORT E NVlitOIJEn_NTAL r-CHI'MLOr i!�S. INC Cwfalmga Falls; Ohio 44223 WON: 2 l}Z0508 AnaJ�xJ rfcal iaborato_ s TEL: (330) 2534211 FAX. • (330) 253 -448 9 Websife_ hifp 2I-Fah-20 Client: Cascades Tissue Group - North Carotins Inc Project: Waste Characf n ation BatchM RI09I80 Sample rD: 2002000"04ADUP SampType: DUP Client 111. SatchQC Batch la: R109180 Analyte Result €gnitabiity 3.23 Sample ID: 20020006r004ATR€P SampType: DUP Client ID: SatchQC Batch €D: R109180 Analyte Result Igrtilability 3.09 TestCade: lgllltability_5 Unils: mmisec TestNo: SWI030 PQL SPK value SPK Ref Val TestCode: Ignitabil4_S Units: mrnlsec TestNo-. 5 W i G30 PQL SPK value SPK Ref Val Prep Date: Analysis Date. 2f101zD20 %REC Lowl-knit Highlimi€ RPD Ref Val 2.830 Prep Date: Analysis Date: 2110i2020 %REC Lawl imit HighLSmit RPD Ref Val 2.830 RunNo: 1051II4 SegN0. 2619320 %RPD RPDL'onK Qual 13.2 20 RunNo,. 14918o Segl~la: 2619321 %RPD RPDlrimit Qual 8.78 20 Sample ID: 20020006.005ADUP SampType: DUP TestCade. Ignitabirity_S Units: mmfsec Prep Date: RunNo: logl80 Client ID: BatchQC Batch ID: R109180 TestNo. SW1030 Analysis Date: 211W2020 SegNo: 2619323 Analyle Result PQL SPK value SPK Ref Val %REC LOWUrnit H€ghl-imY RPD Ref Val %RPD RPDL€mit Qual tgnitability non-flammable 0 0 20 Sample 10: 20420293-O02ADUP SampType: DUP TestCDde: Ignidability_S Units: mrnJsec Prep Date: RunNio: 109180 Client ID: Batch= Batch ID: R109180 TestNa. SW1030 Analysis Date: 2J1012020 SegNo: 2619325 Analyte Result PQL SPK value SPK Ref Val %REC LcwL€mit HighL€mit RPD Ref Val %RPD RPDLimit Qual Ignitabiity 4.46 5.190 15.1 20 QnaliRers: 3 Analyte defected in the associated Method Blank E Value above quantitation range H Holding times for preparation oranat; d Analyte detected below quantization t imits M Manual Integmlion used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column con fiirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit 3 Spike Recovery outside accepted recD Page 24 of 36 �7 � r�; �, F.'� �-� Srrmmii ErrviJror?Jrtenlgf TeehJaologies, Irzc. F • Fr..r J �._ �: �� 0 �L, SUMMARY REPORT �'� r �F�� 3+ � 3310 win si. EN%gPON rd'cNTJ LL TV r- NOLOG I ES, p C Cu)lahnga Falls, Ohio 44223 AnMyricni Labofofar of TEL: (330) 253-8211 FffX.• (330) 253-4489 wO#- 20020508 Websfie: hQ./Anrwseuekcom 23-Fei-20 Client: Cascades '!; issue Group - NOrth Carolina Inc Project: Waste Characterization BatcBID: R109180 Sample €D: 2002M3-OU2ADUP SampType: DUP TeskCoda: Ignitability S Ur its: mm1sec Prep Date: Run€do: 10918a Client ID: BatchQC Balch ID: R109180 Testhfo: SW1030 Analysis date: 2f1012020 S o: 2619325 Anatyte Result PQL SPK value SPK Ref Val %REC LowLimil HighLimit RPD Ref Val %RPD RPDLirr[k Qual Sample fD: 20020293-002A7RiP SampType: DUP TestCode: Ignitability 3 Units: mmisec Prep fate: RunNo. CNet ID: EwchQC Batch 1D: R109180 TestNo: SWIC30 Analysis Dale: 2l1df2020 109180 SegNo: 2619326 Anatyte Result PQL SPK value SPK Ref Val %REC Lowl-imil HighLimit RPO Ref Val %RPD RPDLimh Qual lgnilabifity q•q.g 5.190 14.7 20 Sample ID: 20020507-001ADUP SampType: DUP Client IV: Batchw Batch ID: R109180 Anatyte Result lgnilautity not propagale. Sample ID: 20020507-001ATRIP SampType: DUP Client ID: BatchQC Batch ID: R109180 Anatyte Result fgnilability not propagale Tes[Code: ignitallarn S Units: rnmfsec TestNo: SWI030 PQL SPK value SPK Ref Val TeslCode: ignitabil€ty_S Units: mnVsec TestNo: SW1030 PQL SPK value SPK Ref Val Prep Date: Analysis Date. 211012020 %REC La iimit 1-1 ghtimil RPD Ref Val 0 Prep date: Analysis Date: 2110f2Q20 %REC Lowl-imh 1-righLimit RPD Ref Val 0 Ruallo: 109180 SegNo: 2619328 %RPQ RPDLimit Qua] 0 20 RunNa: 109180 SegNo: 2619329 %RPD RPDLimit Qual 0 20 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H holding tirnw for preparation or anal+ J Analyte detected below guanti tation limits M Manual Integration used to detemtine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit O ienaI R RPD outside accepted rcoovery limits RL Reporting Detection Limit S Spike RecuveJy outside accepted Fern Page 25 of 36 daRg r-� fz SrmrmitEr+viranrnerrfaf Technologies, Inc. (��" SUMMARYi3�j� l � �� � 7 Y rev! �.•�Y��F"_� � 33i4�ifirrrSi. ENVI1 OM1,1FNTAL TFECIINCLO Or S, MC Cuyahoga Fails, Ohio 44223 Anjtytfcigi L 2i3arsrorlis TEL: (330) 253-8211 FAX.- (330) 253-4489 WOO: 20020508 Ff'ebsiie: hrr�_linriv_selfe#.eaar 21-F'eh-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatchID: R109130 Sample ID: 2002t}So8-001ADUP SampType: ❑UP Client ID: Sludge Batch ID, R109180 Analyte Result IgnRabiliq non-flammable Qualifiers: 8 Analyze detected in the associated Method Blank J Aoalytedeteeted belowquawitation limits MJ Not Detected R KPD outside accepted recovery limits TeSICade: Ignitability_S Units: mirNsec Tests: SWID30 PQL SPK vaWe 5PK Ref Val Prep Date: Analysis Dale: 7JI012020 %REC Lowl-imil HighLhnit RPD Ref Val 0 RunNo: ilasi8o SegNa: 2519331 %RPD RPDLimit Qual 0 20 E Value aboveyuentitation range H Holding times fbr preparation oranal3 M Manual Integration used to determine area response MC Value is below Minimum Campourtd P SECOnd column conftt 363Ft exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery autside uceepted reao Original Page 26 of 36 Sumr�rFlF.rr�ironmearafTeci+Mofogies.}rre. supi�nmm 03310 Win Si. L. SUMMARY PORT E[VVJitOl�dcnlTa��Lceteo�c� f=S.l;2C CzTa&ngaFalls, Ohio44223 Am-34'r3ca1 LBLunr3larlr-� TEL. (330� 253-8211 FAX. (330) 253-4499 O#: 20020508 WeBsite. huP.11§nrw.seuekeam 21-Feb-20 Client. Cascades Tissue Group - North Carolina Inc Project: Waste Characterization Batch1l): R109573 Sample ID. 20421049-007AMS SampType: MS TestCode: Cyanide,Rea Units: mglKg Client ID: Batch= Batch ID: RI D9673 TestNo: SW9014 Analyle Cyanide, Reactive Result PQL SPK value SPK Ref Val ND 0.500 10.00 0 Sample ID: 20021049-MAMSO SampType: NISD Tes1Cade: Cyanide,Rea Units: mgfKg Client ID: BafchQC Batch ID. R109573 TeslNo: SW9014 Analyte Cyanide, Reactive Result PQL SPK value SPK Ref Val ND 0.495 10.00 0 Prep Date: Analysis Date: 211912420 %REC LowL[mil Highl-imit RPD Ref Val 0 81.6 122 Prep Date: Analysis Date: 2l1912020 %REC LawLinit H[ghUrnil RPDRefVal 0 81.6 122 0 Run No: '109573 SegNo: 2637160 %RPD RPDLimit €dual 5 RunNo: 109573 SegNo: 26371fi1 %RPD RPDL[mrt Qual 0 5 S Qualifiers: 13 Aea[yte detected in the assoc[ated. Methad Blank F Value above quttntitation range H 14o[d'tng times for preparation ar anal! J Analyre detected Wow quantitation Timits M Manual Integration used tndetermine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery liatim RL ffeporting Detection Limit S Spike Recovery outside accepted reco Page 27 of 36 Smwmd Environmenfuf Technologies, msummov 331*lifir7Sl_ QC SUMMARY REPORT RAVl110t+JMENTAL T-cCPUOLd rtLS, tF;C CtryahagaFaffs, Ohio 49223 A Rai} i1ta1 L abora[orrt t TE£ (330) 253-821 f FAX., (330) 253-4489 AV0: 20020508 Websile. hlfn.11iv�re�.sellek,com 2I-F6-20 Client: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization BatrhID: R109573 Sample ID: Blank SampType: MBLK TestCode: Cyan[de,Rea Units: mg1L Prep date: RunNo: 109573 Client ID: PBW Balch ID: R109573 TestNo, 5W94'4 Analysis Date: 211912o20 SegNo: 2837134 Analyte Result PQL SPK value SPK Ref Val %REC LowLimil HighUrnit RPD Ref Val %RPD RPOI-imit Qua[ Cyanide, Reactive ND 0.485 Sample ID. LfiS Client [D: LCSW SampType: LCS Batch ID: RIOW3 TeslCode: Gyanide,Rea Units: mgfL TeslNa: SW9014 Prep Date: Analysis Date: 2f1912020 RunNo: '109873 SegNo: 263713S Analyte Result PQL SPK value SPK Ref Val %REC LawLimit Highl imit RPD Ref Val %RPL) RPDLimi[ Qual Cyanide, Reactive 9.52 0.490 10.00 0 95.2 85 115 Sample 10. RLCheck Menl ID. BatchQG SampType: RLC Batch ID. R709S73 TestCode. Cyanfde,Rea Unils: rng1L TestNts: SW90-14 Prep Date. Analysis Date- 211T2020 RunNo: 109573 SegNo: 2637137 AnWe Result PQL SPK value SICK Ref Val %REC LowLimit HighL[mit RPD Ref Val %RPt3 RPDLimit Quad Cyanide. Reactive Na 0.485 0.5000 0 74.8 50 150 Qualifiers: 13 Analyte detected in the associated Method Blanc d Analyte detected below quandtation limits ND Mot Detected R RPD outside accepted recovery limits E Value above quaatitationrange M Manua[ Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit H Holding times for Preparation or anal] MC Value is below Minimum Compound PL Permit Limit S Spike Recovery outside accepted recc Original Page 28 of 36 sup,.-..m Summit ErruironmeMrQl TeeFrnologres, frte.�L �.7 V MAR� n.POli 1� 33f0 :n Sr. ECtWPONMENTA CE4N4� �=5, 's2�w Crryathoga Falls, Ohfo 44223 A,?AV(dcaf Laborolar}es TEL- (330) 253-8211 F.Y.- {330) 253-4499 WO#: 20020508 websire. r',rru=lhr mcseuek com 21-Feb-20 Client: Cascades Tissue Group - Forth Carolina Inc Project: Waste Characterization BatehID: R109591 Sample ID: 20029049-007AMS SampType: MS TestCcde: Sulfide,React Units: rngfKg Client ID: BatrhQC Batch ID: 1111109591 TestNo: SWS034 Analyte Sulfide, Reactive Result PQL SPK value SPK Ref Val 4530 25.0 4800 0 Sample ID. 20021049,DO7AMSD SampType: MSD TestCode: Sulfide,Reaat Units: mglKg Client ID: BatchQC Batch ID. R1095si TestNo: SW9034 Analyte Sulfide. Reactive Result PQL SPK value SPK Ref Val 450 25.0 4800 0 Qualifiers: B Analyte detecled in the$ssoriated Method Blank 1 Analyte detected belmv quantimlion l units ND Not Detected R RPD outside accepted reoouery limits Prep Date: Analysis Date- 211912020 %REC Lawt-unit Hight -unit RPD Ref Val 94-4 so 120 Prep Date: Analysis Date: 2l9 912a20 %REC LOWUMit HighLEmit RPD Ref Val 95.0 80 120 4530 SegNa. 2638334 %RPD RPDLimit Qual RunNo: 10959'1 SegNo: 2SM35 %RPD RPOLirnit Qual 0.560 30 E< Value above quantitadon range H Holding times for preparation or anal+ M Manual Integration used to determine area response MC Value is ielawMinimum Compound P Second column confirmation exceeds FL Permit Limit RL Reporting Detea# on Limit S Spike Recovery outside accepted reco Original Page 29 of 36 _ Sawniff Enpfronmentai Technologies. frrc_ QC SUMMARY REPORT EKVltk[3tlidEWAL �mc:M0Lnw;� s, rNC Cuyahoga FaUA Ohio 44223 ARMyr[cv-1 i.aborat: rfes TEL: {33it 233 811! FAX.• (330) 253-4489 WOW. 20020509 Websife: hffo:1Avunr.seffek.com 21-FL-b-20 Client: Cascades Tissue Group -North Carolina Inc Project: Waste Characterization BatchlD: R109591 iample ID: MB-RIO9591 SampType: MBLK TesiCade: SuFffde,React Units: rnglL Prep Dale: RunNo. 10MI iloerrt ID: PBW Balch la: R109591 TestNo: SW9034 Analysis Date: 211912020 SegNo: 2638284 Inalyte Result PQL SPK value SPK Ref Val %REC !_ wLirnl HighLimit RPD Ref Val %RPtO RPOLiml Qual 'aulftde, Reactive ND 25.0 iample ID: LCS-RIO9591 SampType: LCS TestCade: Sulfide,React Units: mgiL Prep Date: RunNo: 1095131 silent ID: LCSW Batch ID: R109591 Tes[No: SWS034 Analysis Date: 211912020 SegNo: 2638286 knalyte Result PQL SPK value SPK Ref Val %REC LowLimil Hight- m it RPD Ref Val %RPD RPDLim it Qua] 3ultide, Reactive 4660 25.0 4800 0 97.1 85 115 Qualifitrs: B Analyte detected in the associated Method Blank E Value above quantitation rangy H Hn3ding times For preparation or anal+ I Analyte detected below quanti[ation 1hits M Manual Integration used to determine area response MC Value is 17ei6w Minimum Compound ND Not Detected P Seiand aoturnn canfirmatian exceeds ?L Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit 3 Spike Peouvery outside accepted reco Original Page 30 4f 36 Suet!ttlt Environmental Technologies, In Qualifiers and Acronyms CTSUMM111L 9310 WIII 5 ENVInONP45NTAL TECHNOL001$8, INC Clryahoga Falls, Ohio 442e Wok: 2oD20;Os t}ltalyrlc:tl Labor4toxles TEL: (330) 253-8211 rr1X: (330) 253-446 ifebslte: t / �y,settekwro Date: 2121/2020 These commonly used Qualifiers and Acronyms May or may not be present in this report, Qualifiers U The compound was analyzed for but was not delected, 3 The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit, The result exceeds the Regulatory Limit or Maximum Contamination Limit. m Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response, P The sceond column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GC1MS Analysis was performed. B/MB+ The analyte was detected in the associated blank, G The ICB or CCI3 contained reportable amounts of analyte, QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or WSD recovery failed low (-) or high (+), QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+)• QMR The MS/MSD RPD was outside of accepted recovery limits, QV-/+ The ICV recovcry failed low (-) or high (+), S The spike result was outside of accepted recovery limits, Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected lit. Reporting Urnit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level ofDctection LCS Laboratory Control Sample LOQ Level a f Quantitation LCSD Laboratory Control Samplc Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required QUantilation Limit DUP Duplicate PL Permit Limit NIS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicatc MCL Maximum Contamination Limit RPD Relative Pcreont Different MInCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Rccxtraction CCV Continuing Calibration VcHriication TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Clieck Cl+ Calibration Factor Di+ Dilution Factor RT Response rector This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 31 of 36 S�rmmii E�viranmenral Technologies, }rre, 3310 Win Sr. EHVJ110A].v JTALTECHVOLor�i=S.I+:C. CvyuhogaFalls .Ohio 44223 Ar+�i f+c�1 La o�aforlet TEL: (3301) 253-9211 FAX. (330) 253-4499 Wehsiie: hrf :1AP1viv.sefrek.com Client: Cascades Tissue Group -North Carolfna Inc Project: Waste Characterization DATES REPORT woof 20020509 2 Sample M Client Sample lD Collection Date Matrix Test Name L.earhate Date Pre Date P Analysis Date 20U20508-0UTA Sludge 17110208:00:00AM Sludge ignitabilityofSolids (3W-846:I030) 211012020 1:UU:00 PM pH (S W 9045D) 21I012020 4:22:07 PM Resclive Cyanide RU1417.33.2}Sotid 211912020 10:33:DU AM Reactive Sulfide (9034)f7-3.4.2 TCLP HefblCides by EPA832113 2J €112020 5:00:00 Pius 2119121320 1033:00 AM 211312020 5:36 00 AM TCLP McNMFYAnalysis (SWI31 i174nii w2020 5:00:DU Plvi 211712Q2O 9:00.00 AM 2/1712420 2:08:00 PM TCLP Metals Analysis (SW131116D10'213 1120ZD 3:00:00 PM 211312020 8:50:00 AM 211312020 2:43:06 PM TCLP Peslicides Analysis (SWI31 €/K211 I12026 5:00:00 PM 2J1212020 9:45:00 AM 2115/2020 3:12:00 AM TCLP Semi-Valati€es Analysis 21I 112020 5.00:00 PM 211312020 10:30:00 Am 211412020 W:19:00 PM (SW 131119270) TCLP Volatiles Analysis 211112020 3:00:00 PM 2n 3M20 123 &00 AM Original Page 32 of 36 fflsummm Stmu,rit Envlronineirtal Technologies. hnc. Accreditation Program 331OWinSt. t=NYlltaNidL:tJTAL 7�otstwot,nc,r;r, t(ac Cuyalro a Fulls, Ohio hla 44��3 Anal tes Report ilrralytlt dl Lalioralorlos TC'L: (330) 253-8,211 FAX (130) 253-4489 WON, 20020508 Websi[e: 21-Feb-30 Client; Cascades Tissue Group - North Carolina Inc State: NW Project: Waste Characterization Program Name: NC W W SCM Sample ID Matrix Test Name Ana[yle Status 20020508-OOIA Sludge lgnilnbilityofSolids (SW-846:1030) Ignitability A Sludgy pH (SW9045D) Hydrogen Ion (prl) A Sludgy Reactive Cyanide (9014)7.3.3,2)-Solid Cyanide, Reactive U Sludge Reactive Sulfide (9034)17.3A.2 Sulfide, Reactive U Sludge TCLP Herbicides by EPA 8321 B 2,4,5-TP A Sludgc TCLP Herbicides by EPA 8321 B 2,4-D A Sludge TCLP Mercury Analysis (S W I311/7470) Mercury A Sludge TCLP Metals Analysis (SW 131 116010) Arsenic A Sludgc TCLP Metals Analysis (SWI31116010) Barium A Sludge TCLP Metals Analysis (S W 131116010) Cadmium A Sludge TCLP Metals Analysis (SW [31 1/6010) Chromium A Sludge TCLP Metals Analysis (SW13I V6010) Lead A Sludge TCLP Motels Analysis (SW1311160 10) Selenium A Sludge TCLP Metals Analysis (SW 131 l/6010) Silver A Sludge TCLP Pesticides Analysis (SW 1311/8081) Chlordane, total A Sludge TCLP Pesticides Analy5i5(SW1311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW131 1/8081) gamma-BVIC A Sludge TCLP Pesticides Analysis (S W 1311/808 [) f [eptachlor A Sludge TCLP Pesticidcs Analysis (SW 131 1/8081) [-Icptachlor epoxide A Sludge TCLP Pesticidcs Analysis (SW131118081) Mcthoxychlor A Sludge TCLP Pesticidcs Analysis (S W 13 l 118081) Toxophene A Sludgc TCLP Semi-Volatiles Analysis (SW 131118270) 1,4-Dichlorobenxene A Sludge TCLP Semi-Volatilcs Analysis (SW 131118270) 2,4,5-Ti-Milorophenol A Sludgc TCLP Semi-VoIndIcs Analysis (SW 131 l/8270) 2,4,6-Trichlorophenol A Sludge TCLP Semi-Volatilcs Analysis (SW I311/8270) 2,4-Dinintoluene A Sludge TCLP Semi-Volatilcs Analysis (SW 1311/8270) cmwls, Total A Sludge TCLP Semi-Volatilcs Anniysis (SW1311/8270) 1-[exachloroben7.cnc A Sludge rcu3 Semi-Volatiles Analysis (SW 131118270) Hexachiorobutadiene A Sludge TCLP Somi-Volatilcs Analysis (SW 131 [/8270) I- lcxachloroathane A Sludge TCLP Semi-Volatilcs Analysis (SW 131 IM270) . Nitrobcnxane A Sludge TCLP Semi-Volatiles Analysis (SW 1311/8270) Pealnchlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW 1311/8270) Pyridina A Original #I Page 33 of 36 Supi ink Environmental Technologies, Inc. Accreditation Program MSUMMMIr Analytes Report 5NV1110NrA NTALTEfHNQL0GJ1 , I C'�ryalwa Falls,3Ohio 44223 rlrlalyft,gi La&aiatarles TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 20020508 Wei7slte; ltliti;//tirivir..sellek�rnnr Client; Cascades Tissue Group - North Carolina Inc State: NW Project: Waste Characterization program Name: NC`WW_SCM Sample ID Matrix 'rest Name Anatyte Stnllrs 20020508-OOIA Sludgc TCLP Volatiles Analysis I,I-Dichhlorocthcne A Sludgc TCLP Volatiles Analysis 1,2-Dirlllurociliano A Sludgc TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis PenzenC A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Cl,ivrobevene A Sludge TCLP Volatiles Analysis Chlorafnrm A Sludge TCLP Volatiles Analysis Tetrachlarnethene A Sludgc TCLP Volatiles Analysis Trichloroothene A ShtdJ e TCLP Volatiles Analysis Vinyl chloride A Original # 1 Page 34 of 36 111 CM rD LU Ln 0 LU 41 lip -lots 1 13C+Q4COC338 Pirr 4.3 Analysis Request I Chain of Custody 1 �� EflVEBOFE4 NTILtTECHNd19G1ES,INC. 5£T FarSwomlt_ renmenaylTxfi�1 n 331019 &151rxxt G�� S1q Ohio �d2 Rt4er to Terms "d Co,wlic[wm at mr+ Amck t-m %VO M2MTN K4- Cllml l as Analytical Parameters and Methods Requested sue}s� rl Q Pnlra Steast l,aarr8 �+ c i6 Shoe L Dl r Atr+ FJp M ' GcCS. 3 C _ o n U v22 v me �j 1err Calyt rums 'Qtvbr m r _y £ [ilrnlEoaR rus PR510 , — o 9 myp+rbv*w +kesrsdldWa Regnlremeyee OdloVld' 00bIoEVA3,b.Cu PeM: F�j1pqdy) �[UI'tolll llhtrr tsrnpQm[! H'DthorOrmpEaea�t5istaFrozram1- a y to d �n e =� R E For6 ugr,endn he d tetghb!1f5W b Tee mrjY° �r H a 13 '� $emptePde[16 soda ldeail!'actlku 6m Celkrted Tme Cellttro! cL G t7 C1 z` m a: ]-� 1 IDO J�`L Rdw d by. hate Mme Rtcdvrd by. Date Timm Yotq; Camene111sr ; p 1 yv+ Sow kwvolnaarpmlded toru4QC'_' ONIU• YES []NO R st 5ornmEr Ih;ts Tima Carrier R=b Requetcd: nwAg) hltm bwnipprorrtlbyUbliooygcrPrexat' Rsarlred ri.YFSr7KRE1dHF1.TED �A-L K wwwauffowaLg6rh 5frmmif Environme tal Technologies, Inc. MgSUMMIT3310 Win St. ENVIFION14ENTAL TiCI�tJQt p(;I! $, INC. Cuyahoga Falls, Ohio 44223 Sample Log -in Check List Analyfical Laboratcrloe TEL: (330) 253-8211 FAX: (330) 253-4489 websile; haDWsvIt ll, sefrek.enm Client Name: CAS.NC-28379 Work Order Number: 20020508 FxcptNo: 1 Logged 4y: Jacqueline Raslle 21812020 8:21;00 AM Completed By: Jacqueline Raslte 219/2020 12:4$:40 PM � Reviewed By: holly Florea 211112020 11:40:21 AIVI Chain of Custr gfy 1, Is Chain of Custody complete? yes ❑ No ❑ Not Present [� 2, Now was the sample delivered? sSummlk Loci In 3. Coolers are present? Yes Q No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes ❑v No ❑ Custody seals Intact an shipping container/cooler? Yes ❑ No ❑ Not Present SO No. Seal Date: Signed By: g, Was an attempt made to cool the samples? Yes J❑ No ❑ NA ❑ g, Were all samples received at a temperature of �O° C to e,OoC Yes No ❑ NA ❑ 7, Sample(s) In proper container(s)? Yes © No ❑ 8, Sufficient sample volume for Indicated test(s)? Yes d No ❑ g, Are samples (except VOA and ONG) properly preserved? Yes ® No d 10. Was preservative added to bottles? Yes ❑ No 0 NA 11, Is the headspace In the VOA vials less than 1/4 Inch or 6 mm? Yes ❑ No ❑ No VOA Vials (,/ 12, Were any sample containers received broken? Yes © No d +13- Does paperwork match bottle labels? Yes © No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes No 0 15. Is it clear what analyses ware requested? Yes ❑v No ❑ 10, Were all holding times able to be met? Yes No ❑ (If n❑, notl(y customer for authorization.) ,pecial Handling (if ataplicah►e 17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ./❑ Person Notified: Date: 11 By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 18, Additional remarks., Cooler Information Cooler No Tem °C Condition Seal Intact Seal No Seal Date Signed B 1 1.4 Good Not Present 2 1.5 Good Not Present Page 36 of 36 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Cascades Tissue Group -North Carolina,a division of Facility Name: Cascades Holding US Inc, , WQ Permit Number WWTP Name: NPDES Number: WQ0009477 Monitoring Period: From 1/l/2020 To 12/20/2020 Pathogen Reduction (I5A NCAC 02T .)1i106) - Please indicate level achieved and alternative performed: Glass A: Alt. A (tune/tcin) ❑ 1 Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑ AIt.D (No Prior Too ❑ Process to FUrdit�r Reduce Patbogengs ❑ If applicable to Alternative performed (Clans A only-) indicate "Process to Further Reduce Pathogens": Compost 131 Heat Drying ❑ Heat Treatment ❑ Thennol}hilic ❑ Beta Ray ❑ Gamma Ray ❑ PElsteurization ❑ Glass B: 1AIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce 1}tttho eljs ❑ If applicable to alternative performed (Class B attly) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Il Air Drying ❑ Com ostir1A ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ ::... . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level in Sludge Pathogen Density Number of Excee- deuces Frequency of Analysis SampleParameter 'I' a yp Analytical 'I'ech- nique Minimu Geo. Mean Maximun Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN NA NA CFU NA NA 1000 nips per gram of total solid (dry Weight) NA NA Salmonella bacteria (in lieuu of fecal coliform) 3 MPN per 4 grams total solid (dry Weight) NA ee NA Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed. Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. S (Drying - Unstable) ❑ Alt_ 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ GERRTT ICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T. 1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." i��❑ 41 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Karen V. Bellamy Environmental Manager Duke Goodwin project Manager Ireparel Name and Title (type or print) Land Appl' an nd Title (if applicable)(type ;�D pYte wl Si na re o P eparer* Date Sigltiature of sand Applier (if applicable) *Preparer is defined in 40 CF'R Part 503.9(r) and 15A NCAC 2T ,1 102 (26) DENR FORM PVRF 02T (12/2006) "k A-2 Cascades Date, Feb 1, 2021 Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc. 805 Midway Road, Post Office Box 578 Rockingham, NC 28380 USA Phone, (910) 895-4033 Fax: (910) 895-9987 From: Karen Bellamy Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Po Box 578 805 Midway Rd. Rockingham, NC 28380 Phone 1-910-895-4033-Ext 74280 Fax 1-910-895-9887 Email; Karen Bellarny(Wascades.com Permit: WQ0009477 Subject: Fecal Testing Cascades Material is a lime material, so we don't perform vector reduction. Should your office have any question please contact me at the above numbers or email. wren V. Bellamy Environmental Manager Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.