WQ0032723_Residual Annual Report 2020_20210210

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0032723
Applicant/Permittee City of Reidsville
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363993646
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00032723
Fbs Current Existing permt number
Applicant/Permittee Address* 1100 Vance Street, Reidsville, NC 27320
Facility Name * City of Reidsville DCAR
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Reidsville WTP Annual Report - WQ0032723.pdf 3.18MB
Upload only 1 FLFdocurrent (less than 250 M8). Multiple documents mist be contained into one FDFfile unless file is larger than
upload linit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/10/2021

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0032723 FACILITY NAME: Reidsville WTP
PHONE: COUNTY: Rockingham OPERATOR: City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
R3 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes No ❑ -- ► If No skip parts A, B, C and certify form below
Part A*: Part B*:
Volume (dry tons) Recipient Information
MonthSources(s) (include NPDES # if Amendment/ p
applicable) Residual In Product Out Name(s) Volume (dry tons) Intended use(s)
_ Bulking Agent
ne
December
Total from FORM DMSDF (sup)l 0 208.72 208,72 208.72
Totals: I Annual (dry tons):tons):1 0 208.72 208.72 208.72
Amendment(s) used: Bulkino Aent(s) used:
* if more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Sapp) 0
Part C.
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2_ All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0032723 FACILITY NAME: City of Reidsville WTP
PHONE: COUNTY: Rockingham OPERATOR: City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
❑ Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES 1i if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
August
City of Reidsville WTP
115.71
115.71
Ronnie Marshall
115.71
Soil Amendment
September
City of Reidsville WTP
93.01
93.01
Lofton Lovelace
93.01
Soil Amendment
Totals:
Annual (dry tons):
0
208.72
208.72 208.72
Amendment(s) used: I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - 8
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WQ0032723
Reidsville WTP
NCO046345
WWTP Name: Reidsville WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
Residual Analysis Data
Conc.
Sam le or Composite Date
Parameter Limit
(mg/kg) m /k
a 8/24/20
Percent Solids (%) NA
4.4
Arsenic 75
10.6
Cadmium 85
0.455
Copper 4,300
186
Chromium NA
47.5
Lead 840
20.6
Mercury 57
0.108
Molybdenum 75
3.07
Nickel 420
20.9
Selenium 100
7.27
Zinc 7,500
52
Total Phosphorus NA
1480
TKN NA
6070
Ammonia -Nitrogen NA
3410
Nitrate and Nitrite NA
975
e For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law,
that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalt'es for submitting Pals information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0032723 Laboratory:
Facility Name: Reidsville WTP
Residual Source
NPDES # or WQ#:
NCO046345
WWTP Name: Reidsville WTP
1) Waypoint Analytical
2)
3)
4)
5)
4 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and l5A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
404.00
Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: CgB2
Acres Used: 69 Acres Permitted: 69 Site #: RC001 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
3.03
2.83
Arsenic
0.064
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.126
Cadmium
0.003
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
1.125
0.991
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.116
Chromiuni
0.287
0.310
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.597
Lead
0.125
0.366
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.491
Mercury
0.001
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.019
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
denum
Nickel
0.126
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.218
Selenium
0.044
0.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Zinc
0.315
4.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.367
Total
Phos-
8.954
24.451
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
33.405
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/28/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
Ronnie Marshall
Operator: Ronnie Marshall
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 404.00 Site #:
Predominant Soil Series: C:;B2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 69
RC001 Acres Permitted: 69
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
8/24
78000
4.4
0.207
Reidsville WTP
Dry
<.5"
S
0.5
1 0.1
6070
3410
975
1.222
NA
Fescue
8/25
117000
4.4
0.311
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
1.833
NA
Fescue
8/26
156000
4.4
0.415
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
2.444
NA
Fescue
8/27
136500
4.4
0.363
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
2.139
NA
Fescue
8/28
1
130000
1 4.4
0.346
Reidsville WTP
Dry
<.5"
S
0.5
0.1
1 6070
3410
1 975
2.037
NA
Fescue
8/31
13000
4.4
0.035
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
0.204
NA
Fescue
9/8
117000
4.4
0.311
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
1.833
NA
Fescue
9/9
84500
4.4
0.225
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
1.324
NA
Fescue
9/10
156000
4.4
0.415
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
2.444
NA
Fescue
9/11
1
149500
4.4
0.398
Reidsville WTP
Dry
<.5"
S
0.5
0.1
6070
3410
975
2.342
NA
Fescue
0.000
0.000
0.000
7/6
58500
3.84
0.136
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
1 8470
132
2.019
NA
Fescue
0
1161000
2.694
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
40.070
0.000
TOTALS:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
59.911
0.000
Lime Applied
Annuallbs/acre
0.126 0.010 2.116 0.597 0.491 0.005 0.038 0.218 0.117 4.367 33.405
0 0 0 0 0 0 0 0 0 0
0.126 0.010 2.116 0.597 0.491 0.005 0.038 0.218 0.117 4.367
36 34 1 1338 1 267 1 15 374 1 89 1 2498
209
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 5 Acres Utilized: 69
Land Owner: Ronnie Marshall Annual Dry Tons Applied: 404.00 Site #: RC001 Acres Permitted: 69
Operator: Ronnie Marshall Predominant Soil Series: CgB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max PAN:
Q o
Q
Volume applied (enter
one)
Cu. Yds Gallons
240500
o
/o
Solids
3.84
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
(Dry,
e '
Moist)
preci p.
Past 24
Hrs.
inches
�
w
*
C
o
7 w
*
?j
;
t,
TKN
mg/kg
Z
o 5
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of CropType
yp
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/7
0.558
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
8.300
NA
Fescue
7/8
253500
3.84
0.588
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
8.749
NA
Fescue
7/9
143000
3.84
0.332
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
4.935
NA
Fescue
9/16
130000
3.84
0.302
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
4.487
NA
Fescue
9/21
39000
3.84
0.091
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
1.346
NA
Fescue
9/22
84500
3.84
0.196
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
2.916
NA
Fescue
9/23
147000
3.84
0.341
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
5.073
NA
Fescue
10/5
123500
3.84
0.287
Unifi Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
4.262
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
1161000
2.694
40.070
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
zyle 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

Waypointo
ANALYTICAL
9/8/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-238-0033
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/25/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
05/10/2020
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
LA037
12/31/2020
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2020
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2020
Page 1 of 1 00001/20-238-0033
Page 2 of 8

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 20-238-0033
Client Project Description: Reidsville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
87283 Reidsville WTP Solids 08/24/2020 08:45 08/25/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 20-238-0033
Date: 9/8/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 87283 (Reidsville WTP)
Analyte: Zinc
QC Batch No: 1-509850/1-509329
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. The result for the method blank and sample are flagged with the data qualifier J, Estimated Concentration.
Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected in the
method blank.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 88595
Analyte: Mercury
QC Batch No: L509028
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Project Reidsville, NC
Mr. Brent Collins
755 Yadkinville Road
Information
Mocksville , NC 27028
Report Number : 20-238-0033
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 09/08/2020
Received : 08/25/2020
Danyale Love
Project Manager
Lab No : 87283
Matrix: Solids
Sample ID : Reidsville WTP
Sampled:
8/24/2020
8:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
95.6
%
0.010
1
08/31/20 17:08
FMM
SW-DRYWT
Ammonia Nitrogen
3410
mg/Kg -
dry
568
568
1
09/02/20 15:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
975
mg/Kg -
dry
112
112
1
08/26/20 14:45
ZBD
4500NO3F-2011
Organic N
<2818
mg/Kg -
dry
2818
5682
1
08/31/20 17:10
CALCULATION
pH
6.8
S.U.
1
08/26/2013:05
ADM
9045D
Total Solids
4.40
%
0.010
0.010
1
08/31/20 17:08
FMM
2540G-2011
Total Volatile Solids
34.4
%
0.010
0.010
1
08/31/20 17:08
FMM
2540G-2011
Total Kjeldahl Nitrogen
6070
mg/Kg -
dry
5680
5
08/31/20 17:10
CLP 4500NORGD-2011
Phosphorus
1480
mg/Kg -
dry
62.7
114
1
09/03/20 05:41
DADS
6010D
Aluminum
132000
mg/Kg -
dry
105
114
1
09/03/20 05:41
DADS
6010D
Arsenic
10.63
mg/Kg -
dry
5.45
11.4
1
09/03/20 05:41
DADS
6010D
Cadmium
<0.455
mg/Kg -
dry
0.455
2.27
1
09/03/20 05:41
DADS
6010D
Calcium
9553
mg/Kg -
dry
880
1140
1
09/03/20 05:41
DADS
6010D
Chromium
47.5
mg/Kg -
dry
5.36
5.68
1
09/03/20 05:41
DADS
6010D
Copper
186
mg/Kg -
dry
7.05
11.4
1
09/03/20 05:41
DADS
6010D
Iron
42700
mg/Kg -
dry
194
227
1
09/03/20 05:41
DADS
6010D
Lead
20.6
mg/Kg -
dry
4.09
6.82
1
09/03/20 05:41
DADS
6010D
Magnesium
1390
mg/Kg -
dry
58.6
114
1
09/03/20 05:41
DADS
6010D
Manganese
5980
mg/Kg -
dry
7.39
11.4
1
09/03/20 05:41
DADS
6010D
Mercury
0.1083
mg/Kg -
dry
0.0755
0.341
1
08/31/20 11:57
DDB
7471A
Molybdenum
<3.07
mg/Kg -
dry
3.07
5.68
1
09/03/20 05:41
DADS
6010D
Nickel
20.9
mg/Kg -
dry
2.73
5.68
1
09/03/20 05:41
DADS
6010D
Potassium
1350
mg/Kg -
dry
140
227
1
09/03/20 05:41
DADS
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Mr. Brent Collins
Report Date : 09/08/2020
755 Yadkinville Road
Information :
Received : 08/25/2020
Mocksville , NC 27028
Danyale Love
Report Number : 20-238-0033
REPORT OFANALYSIS
Project Manager
Lab No : 87283
Matrix: Solids
Sample ID : Reidsville WTP
Sampled: 8/24/2020 8:45
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<7.27
mg/Kg - dry
7.27
11.4 1 09/03/20 05:41 3ADS 6010D
Sodium
4073
mg/Kg - dry
295
568 1 09/03/20 05:41 3ADS 6010D
Zinc
52.0 B
mg/Kg - dry
18.4
28.4 1 09/03/20 17:08 3TR 6010D
Sulfur
3230
mg/Kg - dry
118
227 1 09/03/20 05:41 3ADS 6010D
Sodium Absorption Ratio
0.413
Ratio
0.01
0.01 1 09/03/20 05:41 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-238-0033
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#100
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ory Phillips Date & Time: 08/25/2020 09:41:08
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinvilie Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSE! - Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limit(sl
Z Fed Ex ❑Lips [3uSPs
WW -Wastewater GW - Groundwater
Date Results Needed
Courier ❑Client Drop Off
DW -Drinking Water S -Soil /Solid ❑ - Dil
4. 4$10-y{ C U-Tp
{f q L
1tieaUi•f A I � Cr �
Other
P - Product M - Misc
Project Number
Project Manager Phone 4
Project Manager Email
Purchase order Number
Site/Facility 10 4
336-399-3646
brent. collins@emaresources-cam
J2e;dsv;11c WTP
Gv
-❑
A Cool t 10C Na25203 (Micro only)
B Cool c= 6C
Waypoln}
c
C HZS0None
#r/iI ■ ■ r
ANALYTICAL
m
c
Y
M
E
p
0
E
❑
W
, I'
eq it
❑ None Required
a NaOH pH�10
2790 Whitten Road
Unless noted, all containers
V
°
w
m
(SS
Q
1
C J
W
U
F HNC13 pHf2
G HCLpH�2
Memphis, 1lY 38333
o�
o
Z
[phone]
per Table II of 40 CFR Part
a
E
x
a
T
Y
H
2
❑
rr ,,
H HVC14 pH<2
Cool <= GC NA25203
136.
3
�
Date
-rime
sample Identification
Required
Analysis / Preservative
Comments/Notes
WTP
C
v-
Meta Is:X,As, Ca, Cd,Cr,Cu,Fe, Pb
M n , Mg, Mo, H g . N i, 5e, N a, R 5, K, Zn
0
IN 1Bi111111II111111111111111111111111111I11NYI111111168� 3
EMA Re-.rrurces Inc 09 40:50
Reidsv+iie NC
For Laboratory Use Only
Sampled by (Name - Print)
rat �s
Client Remarks/Comments
Sludge Samples - Report Dry Weight
1Ce
Custody
Lab Comments
6/ N
'shed
ff 11 ,,
Relinq
by; (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Elan CoolerTeemyp
Relinquished by: (SIGNATURE)
Date Time
Receiv by: IGNATURE)
Date Time
Relinquished hy: (SIGNATURE)
Date Time
Rec ved y: MATURE)
Da a Ti' e0S
1 ,
25 ze C)

aceAnalytical
National Center for Testing & Innovation
AW
ANALYTICAL REPORT
September 03, 2020
EMA Resources
Sample Delivery Group: L1254291
Samples Received: 08/25/2020
Project Number:
Description: Sludge
Site: REIDSVILLE WTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
JJwkC4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
REIDSVILLE WTP L1254291-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1254291
09/03/2015:49 2 of 21

REIDSVILLE WTP L1254291-01 Waste
SAMPLE
SUMMARY
Collected by
Brent Collins
Collected date/time
08/24/2008:45
ONE LAB. NATIONWIDE.
Received date/time
08/25/2009:30
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1533291
1 08/27/20 09:26
08/27/20 09:26
JGB
Mt. Juliet, TN
Preparation by Method 1311
WG1534773
1 08/29/2018:10
08/29/2018:10
JGB
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1533669
1 08/27/20 20:19
08/28/201105
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1533680
1 08/28/20 00:00
08/28/20 00:00
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1535662
1 09/01/2014:00
09/01/2017:15
DRD
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1532512
1 08/27/20 03:00
08/27/20 03:00
CAT
Mt. Juliet, TN
Mercury by Method 7470A
WG1535259
1 08/31/20 06:55
08/31/2012:37
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1535340
1 08/31/20 08:48
08/31/2010:46
CCE
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1534071
1 08/28/2013:46
08/28/2013:46
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1535717
1 09/02/20 07:05
09/02/2014:25
MT-1
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1535604
1 09/01/201156
09/01/2019:50
MT-1
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1535602
1 09/01/20 06:59
09/01/2017:37
AO
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1254291
09/03/20 15:49
3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 4 of 21

REIDSVILLE WTP
Collected date/time: 08/24/20 08:45
Preparation by Method 1311
SAMPLE RESULTS - 01
L1254291
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
8/29/2020 6:10:10 PM
WG1534773
TCLP ZHE Extraction -
8/27/2020 9:26:19 AM
WG1533291
Fluid 1
8/29/2020 6:10:10 PM
WG1534773
Initial pH 6.58
8/29/2020 6:10:10 PM
WG1534773
Final pH 5.00
8/29/2020 6:10:10 PM
WG1534773
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
08/28/20201105 WG1533669
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/28/2020 00:00 WG1533680
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.74 T8 1 09/01/202017:15 WG1535662
Sample Narrative:
L1254291-01 WG1535662: 6.74 at 23.4C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 08/27/2020 03:00 WG1532512
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.174
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 08/31/202012:37 WG1535259
Dilution Analysis
Batch
date / time
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
1 08/31/202010:46
WG1535340
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
1 08/28/202013:46
WG1534071
SDG:
DATE/TIME: PAGE:
L1254291
09/03/20 15:49 5 of 21

REIDSVILLE WTP SAMPLE RESULTS
Collected date/time: 08/24/20 08:45 L1254291
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
08/28/202013:46
WG1534071
1,1-Dichloroethene
ND
0.0500 0.70 1
08/28/202013:46
WG1534071
2-Butanone (MEK)
ND
J0 0.500 200 1
08/28/202013:46
WG1534071
Tetrachloroethene
ND
0.0500 0.70 1
08/28/202013:46
WG1534071
Trichloroethene
ND
0.0500 0.50 1
08/28/202013:46
WG1534071
Vinyl chloride
ND
0.0500 0.20 1
08/28/202013:46
WG1534071
(S) Toluene-dH
112
80.0-120
0812812020 13.46
WG1534071
(S) 4-Bromofluorobenzene
103
77.0-126
0812812020 13.46
WG1534071
(S) 1,2-Dichloroethane-d4
91.4
70.0-130
081281202013.46
WG1534071
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 64.8
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
87.0
(S) Tetrochloro-m-xylene
72.9
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 09/02/202014:25
WG1535717
0.00200
10
1 09/02/202014:25
WG1535717
14.0-158
091021202014.25
WG1535717
Qualifier RDL Limit Dilution Analysis Batch
mg/I mg/I date / time
0.00500
0.03 1
09/01/202019:50
WG1535604
0.00500
0.02 1
09/01/202019:50
WG1535604
0.00500
0.0080 1
09/01/202019:50
WG1535604
0.00500
0.40 1
09/01/202019:50
WG1535604
0.00500
10 1
09/01/202019:50
WG1535604
0.0100
0.50 1
09/01/202019:50
WG1535604
10.0-128
091011202019.50
WG1535604
10.0-127
091011202019.50
WG1535604
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
ONE LAB. NATIONWIDE. *
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 09/01/202017:37
WG1535602
ND
0.100
0.13
1 09/01/202017:37
WG1535602
ND
0.100
0.13
1 09/01/202017:37
WG1535602
ND
0.100
0.50
1 09/01/202017:37
WG1535602
ND
0.100
3
1 09/01/202017:37
WG1535602
ND
0.100
2
1 09/01/202017:37
WG1535602
ND
0.100
5
1 09/01/202017:37
WG1535602
ND
0.100
400
1 09/01/202017:37
WG1535602
ND
0.100
200
1 09/01/202017:37
WG1535602
ND
0.100
100
1 09/01/202017:37
WG1535602
ND
0.100
400
1 09/01/202017:37
WG1535602
ND
0.100
2
1 09/01/202017:37
WG1535602
32.2
10.0-120
091011202017.37
WG1535602
19.1
10.0-120
091011202017.37
WG1535602
52.5
10.0-127
091011202017.37
WG1535602
67.9
10.0-130
091011202017.37
WG1535602
67.0
10.0-155
091011202017.37
WG1535602
77.1
10.0-128
091011202017.37
WG1535602
PROJECT:
SDG:
DATE/TIME: PAGE:
L1254291
09/03/20 15:49 6 of 21
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc

WG1533669 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1254291-01
Method Blank (MB)
(MB) R3564830-1 03/23/201101
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1254422-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1254422-01 03/23/2011:03 • (DUP) R3564330-3 03/23/201109
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND ND 1 0.000 20
L1254422-09 Original Sample (OS) • Duplicate (DUP)
(OS) L1254422-09 03/23/2011:26 • (DUP) R3564330-8 03/23/201127
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3564830-2 08/28/201102
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.38 95.1
Rec. Limits LCS Qualifier
85.0-115
L1254422-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254422-03 03/23/20 11:13 • (MS) R3564330-4 03/23/20 11:14 • (MSD) R3564330-5 03/23/20 1115
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.36 1.14 81.5 68.7 1 75.0-125 J6 17.1 20
L1254422-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254422-07 03/23/20 11:19 • (MS) R3564330-6 03/23/20 11:20 • (MSD) R3564330-7 03/23/20 1122
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.28 1.20 77.0 72.2 1 75.0-125 J6 6.42 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 7 of 21

WG1533680
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3564662-1 03/23/20 0000
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 7.63 25.0
L1254266-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1254291-01
(OS) L1254266-02 03/23/20 00:00 • (DUP) R3564662-3 03/23/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide ND ND 1 0.000 20
L1254936-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1254936-02 03/23/20 00:00 • (DUP) R3564662-6 03/23/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3564662-2 08/28/20 00:00
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 84.1 84.1
Rec. Limits LCS Qualifier
70.0-130
L1254934-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254934-01 03/23/20 00:00 • (MS) R3564662-4 03/23/20 00:00 • (MSD) R3564662-5 03/23/20 00:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND 86.9 88.0 86.9 88.0 1 70.0-130 1.33 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 3 of 21

WG1535662 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1254291-01
Laboratory Control Sample (LCS)
(LCS) R3566233-1 09/01/201715
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS:10.04 at 22.8C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 9 of 21

WG1532512 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1254291-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE. *
(LCS) R3564212-1 08/27/20 03:00 • (LCSD) R3564212-2 08/27/20 03:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 126 131 125 104 98.9 95.6-104 4.70 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 10 of 21

WG1535259
Mercury by Method 7470A
Method Blank (MB)
(MB) R3565661-1 03/31/201233
MB Result MB Qualifier MB MDL
Analyte mg/I mg/I
Mercury U 0.00330
Laboratory Control Sample (LCS)
(LCS) R3565661-2 08/31/20 12:35
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.0300 0.0314 105
QUALITY CONTROL SUMMARY
L1254291-01
MB RDL
mg/I
0.0100
Rec. Limits LCS Qualifier
80.0-120
L1254291-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1254291-01 03/31/20 12:37 • (MS) R3565661-3 03/31/20 12:39 • (MSD) R3565661-4 03/31/20 12:41
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0293
0.0311 97.5 104 1 75.0-125 6.01 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 11 of 21

WG1535340
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1254291-01
(MB) R3565632-1 03/31/201030
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic 0.0581
J
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3565632-2 03/31/201033
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
Arsenic 10.0
9.72
97.2
80.0-120
Barium 10.0
9.91
99.1
80.0-120
Cadmium 10.0
9.71
97.1
80.0-120
Chromium 10.0
9.50
95.0
80.0-120
Lead 10.0
9.77
97.7
80.0-120
Selenium 10.0
10.1
101
80.0-120
Silver 2.00
1.88
93.9
80.0-120
LCS Qualifier
L1254947-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254947-01 03/31/20 10:36 • (MS) R3565632-4 03/31/20 10:41 • (MSD) R3565632-5 03/31/20 10:43
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.89
9.91
98.9
99.1
1 75.0-125
Barium
10.0
ND
9.89
9.92
98.1
98.4
1 75.0-125
Cadmium
10.0
ND
9.72
9.77
97.2
97.7
1 75.0-125
Chromium
10.0
ND
9.49
9.62
94.2
95.5
1 75.0-125
Lead
10.0
0.325
10.1
10.1
97.9
97.9
1 75.0-125
Selenium
10.0
ND
10.2
10.2
102
101
1 75.0-125
Silver
2.00
ND
1.88
1.90
94.1
94.9
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.159
0.308
0.541
1.33
0.0514
0.266
0.819
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 12 of 21

WG1534071 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1254291-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3564853-3 03/23/201043
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
110
80.0-120
(S) 4-Bromofluorobenzene
102
77.0-126
(S) 1,2-Dichloroethane-d4
91.4
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3564853-1 08/28/20 08:05 • (LCSD) R3564853-2 08/28/20 09:38
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.219
0.230
87.6
92.0
70.0-123
Carbon tetrachloride
0.250
0.243
0.214
97.2
85.6
68.0-126
Chlorobenzene
0.250
0.248
0.255
99.2
102
80.0-121
Chloroform
0.250
0.217
0.227
86.8
90.8
73.0-120
1,2-Dichloroethane
0.250
0.220
0.222
88.0
88.8
70.0-128
1,1-Dichloroethene
0.250
0.237
0.222
94.8
88.8
71.0-124
2-Butanone (MEK)
1.25
1.02
0.999
81.6
79.9
44.0-160
Tetrachloroethene
0.250
0.250
0.240
100
96.0
72.0-132
Trichloroethene
0.250
0.237
0.247
94.8
98.8
78.0-124
Vinyl chloride
0.250
0.215
0.213
86.0
85.2
67.0-131
(S) Toluene-dH
108
109
80.0-120
(S) 4-Bromofluorobenzene
101
101
77.0-126
(S) 1,2-Dichloroethane-d4
96.9
95.6
70.0-130
LCS Qualifier
LCSD Qualifier RPD
4.90
12.7
2.78
4.50
0.905
6.54
2.08
4.08
4.13
0.935
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 13 of 21

WG1534071 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1254291-01
L1254673-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1254673-01 08/28/20 14:06 • (MS) R3564853-4 03/23/20 1427
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.186
74.4
1 17.0-158
Carbon tetrachloride
0.250
ND
0.185
74.0
1 23.0-159
Chlorobenzene
0.250
ND
0.217
86.8
1 33.0-152
Chloroform
0.250
ND
ND
77.2
1 29.0-154
1,2-Dichloroethane
0.250
ND
0.205
82.0
1 29.0-151
1,1-Dichloroethene
0.250
ND
0.173
69.2
1 11.0-160
2-Butanone (MEK)
1.25
ND
0.961
76.9
1 10.0-160
Tetrachloroethene
0.250
ND
0.197
78.8
1 10.0-160
Trichloroethene
0.250
ND
0.194
77.6
1 10.0-160
Vinyl chloride
0.250
ND
0.171
68.4
1 10.0-160
(S) Toluene-dH
106
80.0-120
(S) 4-Bromofluorobenzene
98.4
77.0-126
(S) 1,2-Dichloroethane-d4
92.2
70.0-130
L1254266-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1254266-04 03/23/20 13:05 • (MS) R3564353-6 03/23/20 14:43 • (MSD) R3564353-7 03/23/2015:07
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.187
0.194
74.8
77.6 1
Carbon tetrachloride
0.250
ND
0.180
0.194
72.0
77.6 1
Chlorobenzene
0.250
ND
0.229
0.238
91.6
95.2 1
Chloroform
0.250
ND
ND
ND
79.2
83.2 1
1,2-Dichloroethane
0.250
ND
0.218
0.221
87.2
88.4 1
1,1-Dichloroethene
0.250
ND
0.168
0.186
67.2
74.4 1
2-Butanone (MEK)
1.25
ND
1.15
1.11
92.0
88.8 1
Tetrachloroethene
0.250
ND
0.193
0.207
77.2
82.8 1
Trichloroethene
0.250
ND
0.189
0.203
75.6
81.2 1
Vinyl chloride
0.250
ND
0.155
0.182
62.0
72.8 1
(S) Toluene-dH
107
109
(S) 4-Bromofluorobenzene
97.6
101
(S) 1,2-Dichloroethane-d4
93.5
95.5
Rec. Limits
17.0-158
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80.0-120
77.0-126
70.0-130
MS Qualifier MSD Qualifier RPD RPD Limits
3.67
27
7.49
28
3.85
27
4.93
28
1.37
27
10.2
29
3.54
32
7.00
27
7.14
25
16.0
27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 14 of 21

WG1535717
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3566697-1 09/02/201311
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 61.4
Acid
QUALITY CONTROL SUMMARY
L1254291-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3566697-3 09/02/20 13:40
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
2,4-D 0.0500
2,4,5-TP (Silvex) 0.0500
(S) Z4-Dichlorophenyl Acetic
Acid
0.0309 61.8 50.0-120
0.0334 66.8 50.0-125
672 14.0-158
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 15 of 21

WG1535604
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1254291-01
(MB) R3566335-1 09/01/201746
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
89.7
10.0-128
(S) Tetrochloro-m-xylene
77.6
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3566335-2 09/01/20 1758
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00908
90.8
55.0-129
Endrin
0.0100
0.00913
91.3
57.0-134
Heptachlor
0.0100
0.00840
84.0
27.0-132
Methoxychlor
0.0100
0.00923
92.3
54.0-155
(S) Decachlorobiphenyl
91.1
10.0-128
(S) Tetrochloro-m-xylene
70.5
10.0-127
L1252949-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1252949-01 09/01/20 13:11 • (MS) R3566335-3 09/01/20 13:23 • (MSD) R3566335-4 09/01/20 13 35
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00899
0.00885
89.9
88.5
1 14.0-141
Endrin
0.0100
ND
0.00915
0.00925
91.5
92.5
1 10.0-160
Heptachlor
0.0100
ND
0.00874
0.00875
87.4
87.5
1 16.0-136
Methoxychlor
0.0100
ND
0.00938
0.00970
93.8
97.0
1 10.0-160
(S) Decachlorobiphenyl
79.3
80.4
10.0-128
(S) Tetrochloro-m-xylene
76.3
74.2
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
1.57 40
1.09 39
0.114 40
3.35 34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 16 of 21

WG1535602 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1254291-01
Method Blank (MB)
(MB) R3566149-2 09/01/201156
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
65.3
10.0-127
(S) 2-Fluorobiphenyl
84.4
10.0-130
(S) p-Terphenyl-d14
84.7
10.0-128
(S) Phenol-d5
22.9
10.0-120
(S) 2-Fluorophenol
39.7
10.0-120
(S) 2,4, 6-Tribromophenol
78.5
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3566149-1 09/01/20 1135
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.413
82.6
18.0-120
2,4-Dinitrotoluene 0.500
0.489
97.8
49.0-124
Hexachlorobenzene 0.500
0.435
87.0
44.0-120
Hexachloro-1,3-butadiene 0.500
0.353
70.6
19.0-120
Hexachloroethane 0.500
0.394
78.8
15.0-120
Nitrobenzene 0.500
0.366
73.2
27.0-120
Pyridine 0.500
0.0587
11.7
10.0-120
2-Methylphenol 0.500
0.334
66.8
28.0-120
3&4-Methyl Phenol 0.500
0.327
65.4
31.0-120
Pentachlorophenol 0.500
0.488
97.6
23.0-120
2,4,5-Trichlorophenol 0.500
0.486
97.2
44.0-120
2,4,6-Trichlorophenol 0.500
0.472
94.4
42.0-120
(S) Nitrobenzene-d5
60.4
10.0-127
(S) 2-Fluorobiphenyl
84.8
10.0-130
(S) p-Terphenyl-d14
86.2
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1254291 09/03/20 15:49 17 of 21

WG1535602 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1254291-01
Laboratory Control Sample (LCS)
(LCS) R3566149-1 09/01/20 1135
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 23.4 10.0-120
(S) 2-Fluorophenol 39.8 10.0-120
(S) 2,4, 6-Tribromophenol 83.5 10. 0-155
L1253440-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1253440-01 09/01/2013:42 • (MS) R3566149-3 09/01/2014:03 • (MSD) R3566149-4 09/01/2014:25
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.268
0.282
53.6
56.4
1 17.0-120
5.09
2,4-Dinitrotoluene
0.500
ND
0.382
0.386
76.4
77.2
1 39.0-125
1.04
Hexachlorobenzene
0.500
ND
0.342
0.346
68.4
69.2
1 35.0-122
1.16
Hexachloro-1,3-butadiene
0.500
ND
0.253
0.254
50.6
50.8
1 12.0-120
0.394
Hexachloroethane
0.500
ND
0.253
0.272
50.6
54.4
1 10.0-120
7.24
Nitrobenzene
0.500
ND
0.255
0.271
51.0
54.2
1 12.0-120
6.08
Pyridine
0.500
ND
ND
0.113
18.5
22.6
1 10.0-120
20.1
2-Methylphenol
0.500
ND
0.247
0.257
49.4
51.4
1 10.0-120
3.97
3&4-Methyl Phenol
0.500
ND
0.244
0.264
48.8
52.8
1 10.0-120
7.87
Pentachlorophenol
0.500
ND
0.442
0.427
88.4
85.4
1 10.0-128
3.45
2,4,5-Trichlorophenol
0.500
ND
0.414
0.414
82.8
82.8
1 33.0-120
0.000
2,4,6-Trichlorophenol
0.500
ND
0.394
0.391
78.8
78.2
1 26.0-120
0.764
(S) Nitrobenzene-d5
46.0
49.6
10.0-127
(S) 2-Fluorobiphenyl
66.5
66.1
10.0-130
(S) p-Terphenyl-d14
76.3
74.3
10.0-128
(S) Phenol-d5
18.2
19.0
10.0-120
(S) 2-Fluorophenol
27.8
28.4
10.0-120
(S)2,4,6-Tribromophenol
80.5
77.0
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1254291 09/03/20 15:49 13 of 21

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J0
J0: The identification ofthe analyte is acceptable, but the reported concentration is an estimate. The calibration met
method criteria.
J6
The sample matrix interfered with the abilityto make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1254291 09/03/20 15:49 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
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VWY
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CA co
KS
W o �AZ NM O�
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ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L12 542 91 09/03/2 0 15:49 20 of 21

EMA Resources
i755 Yadkinville Road
Mocksville, NC 27028
Billing Information: l
Mr. Brent Collins Pres
755 Yadkinville Road Chk
Mocksville, NC 27028
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Container
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12065 Lebanon Rd 0!v
Mount Juliet, TN 37122 `
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Email To: [e-mail]
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Please Circle:
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Phone [phone]
Fax: [phone]
Client Project a
Lab Project #
Collected by (print):
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Site/Facility ID a
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Packed on Ice IN Y
Rush? (Lab MUST Be Notified) Quote a
—Same Day Five Day
_ Next Day _ 5 Day (Rod Only) Date Results Needed
_ Two Day —10 Day (Rad Only) No.
—Three Day of
Sample ID
Comp/Grab
Matrix •
Depth
Date
Time
ntr5
Remarks Sample p[[ab onlYl
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55 Soil AIR - Air F- Filter
SS - -Groundwater B - FilterBioassayCOC
WW - Wastewater
OW - DrinkinQVaer
OT Other C
pH Temp
Flow Other
Sample t' i
CCC Seal Present/Intact: _NP r N
signed/Accuratm : � _N
Bottles arrive intact: _A _N
Correct bottles used: y,A _N
Sufficient volume sent: �l mmN
If Aanlicadle
von zero Headspace: y N
Preservation Correct/Checked: �Y N
RAD Screen <0.5 1nR/hr: XHCL�*
Samples returned via:
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Relinquished by: (Signature)
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Trip Blank Received: Yes /
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Relinquished by : (Signature)
Date:
Time
Received by: (Signature)]
c Bottles Received:
If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date:
Time:
Re cei d for lab by, nature)
Time
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