NCG030499_DMR_20210201 (2)

Anchor QEA of North Carolina, PLLC ANCHOR
231 Haywood Street
Asheville, North Carolina 28801 QEA �
828.281.3350
January 21, 2021
Attn: DEMLR Stormwater
Asheville Regional Office
Division of Energy, Mineral, and Land Resources
North Carolina Department of Environmental Quality
2090 U.S. 70 Highway Swannanoa, North Carolina 28778-8211
Re: Stormwater Sample Analytical Results, Period 2 2020
Crane Resistoflex
Marion, North Carolina
General Permit No. NCG030499
To Whom It May Concern,
Anchor QEA of North Carolina, PLLC (Anchor QEA), is pleased to present the following stormwater
sample analytical results. On behalf of Crane Resistoflex, Anchor QEA collected two stormwater
samples on December 14, 2020, for the referenced facility covered by National Pollutant Discharge
Elimination System Stormwater General Permit No. NCG030000 (Stormwater General Permit). This
sampling event fulfills the compliance sampling requirement for Period 2 of 2020.
In the samples collected from sampling locations OF-001 and OF-002, all constituent concentrations
detected were below or within the acceptable ranges of the benchmark values specified in the
general permit. This letter provides background information and describes the methods, findings,
and conclusions regarding the stormwater sample collection and analysis.
Background
The most recent Stormwater General Permit for metal fabrication activities was issued by the North
Carolina Department of Environmental Quality with an effective date of November 1, 2018, and it will
expire at midnight on May 31, 2021. Sample collection and reporting protocol for this event followed
the current permit requirements.
The Stormwater General Permit indicates that the permittee shall complete analytical sampling on
a semiannual schedule, once during the first half of the year (January 1 to June 30; Period 1) and
once during the second half of the year (July 1 to December 31; Period 2), at a minimum, allowing
at least 60 days between sample collection dates.
The general location of the facility is indicated in Figure 1. The facility's two permitted outfalls and
sample locations are labeled OF-001 and OF-002, as identified in Figure 2.
Stormwater Sample Analytical Results, Period 2 2020.docx
Received
FEB-1l202-1
IRV
IevNN �lShAvk

January 21, 2021
Page 2
Methods
On December 14, 2020, Anchor QEA mobilized to the Crane Resistoflex facility to collect stormwater
samples during a measurable storm event of approximately 1.35 inches of rainfall'. There had not
been a measurable storm event in the 72 hours preceding this sampling event.
The stormwater samples were collected from two outfalls labeled OF-001 and OF-002 (Figure 2).
Samples were collected as indicated in the surface water sampling logs (Attachment 1) from the
approximate center of the discharge streams and were transferred to laboratory -supplied containers.
The containers were placed in a cooler on ice and delivered to Pace Analytical Services, Inc. (Pace), in
Asheville, North Carolina, for laboratory analyses. The pH measurement was obtained in the field by
placing a probe within the flow of the respective outfall. The pH measurement was recorded once
stabilization occurred. Anchor QEA's equipment documentation and instrument calibration data
sheet is included as Attachment 2.
Anchor QEA also performed a stormwater discharge outfall (SDO) qualitative monitoring event
during the stormwater analytical sampling event. The associated SDO qualitative monitoring reports
are included as Attachment 3.
Findings
The laboratory analytical results are summarized in the Semiannual Stormwater Discharge Monitoring
Report (Attachment 4). The samples contained concentrations lower than or within the range of the
specified benchmark values for all constituents analyzed by Pace.
The field measurements of pH for both OF-001 and OF-002 were within the acceptable benchmark
value range. The field measurement results are listed in the surface water sampling logs
(Attachment 1), and pH results are shown in Attachment 4. The Pace analytical report and chain -of -
custody form are included in Attachment 5.
Conclusions
The stormwater sample results for outfalls OF-001 and OF-002 showed concentrations below or
within the range of the benchmark values specified in the general permit for all constituents.
The next analytical monitoring of stormwater discharges will be performed during another
measurable storm event between January 1 and June 30, 2021, to satisfy the Period 1 of 2021
compliance period.
����IIee h was obtained from the Weather For You online database records for the MID_F4683 gauge station in Marion, North
_`"Car'T�`a"sAvailable at:https://www.weatherforyou.com/

January 21, 2021
Page 3
If you would like additional information, please contact me at [phone], or contact Victoria
Boyer at [phone].
Sincerely,
Robert Cork PE, MEng
Managing Engineer
cc: Victoria Boyer, Crane Resistoflex
Duplicate, Central Files
Attachments
Figure 1 Site Location Map
Figure 2 Stormwater Discharge Outfall Locations
Attachment 1 Surface Water Sampling Logs
Attachment 2 Equipment Documentation and Instrument Calibration Data Sheet
Attachment 3 Stormwater Discharge Outfall Qualitative Monitoring Reports
Attachment 4 Semiannual Stormwater Discharge Monitoring Report
Attachment 5 Laboratory Analytical Report and Chain -of -Custody Form

Figures

Publish Date: 2021101112, 901 PIN I User. cpattersoii
Filepalh: pVobs\cane Resistoflea 2062\Maps\Aq_Fig01 SiteLocationMap.mxd
z�2 ANCHOR Figure 1
QEA Site Location Map
Stormwater Sample Analytical Results
Crane Resistoflex, Marion, North Carolina

Attachment 1
Surface Water Sampling Logs

ANCHOR
kz QEA —
Surface Water Samplinq Loq
Anchor QCA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carohna 28801
Fre;ect Name
L(Ane Resix 10)Cle
Date. 121 /Lf /202U
or N.,..Lei
G� -17.20�2— 0/. 01
Weather 50°fJ/Ra/nm SPr%1
m c .a; P .ormel
C Pn tfCnUn
Facility Permit s: /l/coom 19
Sample Name
OF- 00 I
Cmn-rents
Sample Method:
G b Syringe
Pump
Bader-Disp. Other.
'. Oxidation
Dissolved ' Specific Cond.
PH(S.U.)
Reduction Turbidity .
Time Temp (°Q
Oxygen (mg/L) (PS/cm)
', report to 0.1 S.U. j Potential (mV) (NTU) Comments
X55
!',AP
q 3
GAP
Sampling Container
Number of Containers
Requested Analysis
I(l0 nL A�Ler /-[ M�k 2
I
TT0-SV0rj TTO - Pert%v'd-r
250rLP'asvc
3
little Cyr P11 IDisrokeJ AeAlr/TTO AehJ
125 mL P,as6c
I
�f1215 /Z,%
Gya n.de
40 mL Glass
3
.
TTO
''. / r O — VaCI
LG'.ase ..JI HcL
2
TPH Uhl l 6re4-rc.
Otr'�r : I- L Plan/[ 250ml I
1
T TTO- ,PAe 701
vege:acon. 7cod Access. Fail-i ..5
Sampling Personnel Signature: Date: l"-/J .G 01 V
N>te:
Samp'e; are analyzed immedlat ely upon collection
`C dcw"5 Celsius
y5trr7l micrs 3lemen per cubic cenurnetel
+all md4nrem5 Per!Oer
Ci i. IT ""II
iJYJ •-epr-.elcmei n: W�b�dcy unnt
IJ .--'-ard ur:its
Method Reference'
Temperature SM 25508-2010
Specific conductivity EPA Method 120 I, Rev. 1982
DO SM 4500 O G2011
PIt Sld 4500-H' 8-2011
Page 1 of 1

tZANCHOR
QEA u
Surface Water Sampling Lag
Anchor QUA of North Carolina, PLLC
23'I 1laywood Silent
Asheville, North Carolina 28801
Project Name
Crane Rex-jt9t/Tr P..:
Date
Pro-lect Number
G9-206)—a1.01
Weather SU'F, RaIArn1f1'//
Samp"ng Persennet
G. Pa- Herran
F itci1ity Permit 111 /VGG o it T'7
Sample Name
OF.— 002
Comments
Path rota'%lxmej:
Sample Method: rab Synnge
Pump
Bailer-Disp. Other.
Oxidation
Dissolved Specific Cord.
pH (S.U.)
Reduction
Turbidity �.
Time Temp ('C)
Oxygen (mg/L) (p5/cm)
,report to 0.1 S.U. iPotential (mV)
(NTU) Comments
0725
CAP
Qp
CJO
GAP
I I
Sampling Container
Number of Containers
Requested Analysis
n`� `t IOD �tAnler
/-C��lv
M-SVOGs , 770- Pert/c.Jer
250 mL Plavoc
3
MISIa-1r (C., /n." Zn) /.JDi"r1.ej tteA&1- no /110 A/r
125 mL Flask
TTO -.CYa fide
40 mL Glass
3
T%(J - VOC.r
t LGlass,/ HCL
`�
7—PH 0"I f Grc4re
Other: I-L l'larhi
250-^t A+Ie,r Z
770- A,.)
vegetation. Goo d Access: F l/- -; m"jily y S¢tpp SI[J�CiU /Ji%J.e
Sampling Personnel Signature: / _ q � Date: /,2/ / 4/20 20
Notes
Samples are analyzed immediately upon collection
`C degrees Celsius
{.Srcm m:u0-51emen Per cubic centimeter
rng/L m:rigrem<- Per liter
m.J mub:Oh
NTU nephelometuc turbidity units
SU standard units
Method Reference.
Temperature. SM 2550 8-2010
Specific conductivity EPA Method 1201. Rev. 1982
DO SM 4500 O G-2011
pliSM 4500-H' 8 2011
Page 1 of 1

Attachment 2
Equipment Documentation and
Instrument Calibration Data Sheet

ANCHOR
0 EA ....�..:�..
bgulpment uocumentanon anci instrument Lalluratton data sneet
Aildwi QEA of North Carobna, PLLC
231 Hoyv oo(I Street
A;hevllle. North Carolina 28801
' CALIBRATION DOCUMENTATION
r L 1,� 4L.�-t'S15hr�lt X. Pclson Conducting CBhblelmn G. GA."C/ron
L,���1p2
r '( ,/1',I{tri M, Nc Dato pl field Measurements �,2/�If/Z(f Z(�
i /VCG0304q`1
,..:,m! 1 t -e11 el Inete.> 0>a'¢I to Wle
Hai h 2 i O00l& n 1510(16045207)
HF S:aentiG( MlcroT PV.' iJn 2C1'1b010.i5)
Instrument Reading
(Hach 21000)
- Instrument Reading'
(HF Scientific MicroTPW)
10 NTU
20 NTU -
100 NTU
Boo NTU
1,000 NTU
10.0 NTU
0.02 NTU
Calibration Lot No. &
Expiration Date:
Cal
Car
Cal
Car
Cal:
Cal-
.
Time
Time
Time
Ti
Time
Time
Calibration
Verification,Check
'Pre -Analysis
(10 NTU):
Meas
Time
`Pre -Analysis
Check (10 NTU):
Was
Time
`Post -Analysis
Check (10 U):
to
Time
-
t-AnaI sis.
Check (10 NTU):
Was
Time. G¢0
ySl Professional Plus Multiparameter Meter s/n *13"}B02) / % 1?115
Instrument Readings
Calibration Lot No.
& Expiration Date
Dissolved CwQen (%
saturation)
Ir t al I`:`
Cal I`
mmHg
Temperature ('C)
Tlme Gqp
DO (Site 92,
In ba11`.=
Cali >I
mmHgLure
('C'.
Time i/fP
if ao licable)`
PH 7s.u.
,ap:i�4toC,IS.
In4'a
.J9, qs
PHmV
- i6.3
Cal
7.v1
PI{mV
Tlme-
05IfE
PH 4 su.
1,075,
1,1,al-
J. 16
PH V
747•q
Cal'
4.00
pHmV.
TIm r
(�5y7
O2 22
pH105.V.
r.pH10 i5u
'^•c1y10 01
/
pNmVQo.7
W
Cal/V-O/
pHmV
Time��f,
lrVv11 l0
07�21
QC' pH 7 S.U.
rain ea b.T so
A1/l Time 055Z
tsea-7• 0 �
Mid0 -740
V
Chec" G I
PM Time
Check
Uj 1
Spec. Cond.
Imbal
Cal
Time
P
PS/cm
CA
QC^:
AM Time
Meas
Mid Day Time
Check
PM Time
Chec4:.
PS/cm`
%Recovery=
in t,al
Cal
Cl
ITime-
_._.
l/!�
Signature Date:
¢ is a• o z : •�0=•;e, e. V p n:ar.dttturcr s OparaUmi n'enwl
- 'I u rated aco-6 n9 levaloea repr esen In live of III on,., range
az P. mac=Fc Ccrlup..n; pit 7 p114 pH 1000 OPP Q[ dell
/ pgd IDS ee,,j _ pr ?pr„i8(VIdi.J'I, locanonsi[I,, UU probe must be cahbracd at VoCh sample Ste pnorto anpl,s
! p
J I ❑ a III) [ ,.duol: ay lD:. of the uu=value if QC,eaa nys are Out of laago the mlromenl needs to be recal.bmled
c Q' der c i,e"_.cs 1 :'I:'Vo t ,tit; 11 '„ sn.q to 1plchun nl sa nIpk, at a inn. mural
a J. _spl h', T,116 ,1'/, i. 1i0
1 Pcy e-c Te^ 2L082110ICc-,I-`+1,FPAMer.J1/011 GO Sr 145000 G 20111 pit SM dSnD H, a 20111 Turb.d:tq 5b1213082017
Page 1 of 1

Attachment 3
Stormwater Discharge Outfall Qualitative
Monitoring Reports

Ki
Ire
ttnvlronmen[at
Qualify
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deg.nc.izov/about/divisions/energy-mineral-land-
resources/energy-mi neral-land-permits/stormwater-perm its/nodes-industrial-sw#tab-4
Permit No.: N/C/0/ 3 / 0 / 0 /0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 4 / 9 / 9 /
Facility Name:
County: McDowell
Crane Resistoflex
No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection:
06:50
Total Event Precipitation (inches): 1_35
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. of-001
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 07/282017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? 0 Yes 0 No.
8. Is there an oil sheen in the stormwater discharge? DYes (E)No.
9. Is there evidence of erosion or deposition at the outfall? O Yes o No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No indications of stormwater pollution were observed.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, last modified 07/28/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit httus://deg.nc.2ov/about/divisions/enerLzv-mineral-land-
resomces/energy-mineral-land-oermi is/stormwater-permits/nodes-industrial-sw#tab-4
Permit No.: N/C/D 3 / 0 / 0 / 0 / 0 /0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 4 / 9 / 9 /
Facility Name:
County: McDowell
Crane Resistoflex
No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection: 07:25
Total Event Precipitation (inches): 1.35
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. OF-002
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Q Yes Q No.
8. Is there an oil sheen in the stormwater discharge? OYes G No. _
9. Is there evidence of erosion or deposition at the outfall? O Yes o No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No indications of stormwater pollution were observed.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

Attachment 4
Semiannual Stormwater Discharge
Monitoring Report

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring. Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG03 0 4 9 8 Person Collecting Samples: Christian Patterson
Facility Name: Crane Resistoeax Laboratory Name: Pace Analytical
Facility County: McDowell Laboratory Cart. No.: 4o
Discharge during this period: Q Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes (§ No
If so, which Tier (I, 11, or III)?
Analytical Monitoring Requirements for Clutfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall1
outfall2
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Gass
C
C
N/A
Date Sample Collected MM/DD/YYYY
12/14/2020
12/14/2020
46529
24-Hour Rainfall In Inches
1.35
1.35
00552
Non -Polar Oil & Grease in mg/L (15)
<5.0
<5.0
C0530
TSS in mg/L (100 or 50*)
7.6
2.5
004DD
pH in standard units (6.0 — 9.0)
6.93
6.88
NCOIL
New Motor/Hydraulic oil Usage in
O
0
gal/month
01119
Copper, total recoverable in mg/L
<0.005
<0.005(0.010
FW, 0.005 SW)
01051
Lead, total recoverable In mg/ L
<0.005
<0.005
(0.075 FW, 0.220 SW)
01094
Zinc, total recoverable In mg/ L (0.126
0
0.0681
FW, 0.095 SW)
.0355
78141
Total Toxic Organics (TTO) In mg/L(1)
ND
NO
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HOW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L All other water classifications have a benchmark of 100 mg/L.
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, Including the possibility of fines and Imprisonment for
Authorized Individual
1-2 ( - Z021
Date

Attachment 5
Laboratory Analytical Report and
Chain -of -Custody Form

aceAnalytical
www.pecelehuom
January 11, 2021
Mr. Christian Patterson
Anchor QEA
231 Haywood Street
Asheville, NC 28801
RE: Project: Crane Resistoflex
Pace Project No.: 92511537
Dear Mr. Patterson:
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
64�
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, I.L.C.
Page 1 of 41

aceAnaljftal
wwa.pecsls6s.coa
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, -I-C.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 41

(�IaceAnalyfical'
www.pacelabs.com
SAMPLE SUMMARY
Project: Crane Resisto6ex
Pace Project No.: 92511537
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92511537001
OF-001
Water
12/14/20 06:55
12/14/20 13:15
92511537002
OF-002
Water
12/14/20 07:25
12/14/20 13:15
92511537003
OF-001 TTO
Water
12/14/20 06:55
12/14/20 13:15
92511537004
OF-002 TTO
Water
12/14/20 07:25
12/14/20 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 41

aceAnalytical
wwa.pacelabs.com
SAMPLE ANALYTE COUNT
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92511537001
OF-001
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
4
PASI-A
EPA 200.7 Rev 4.41994
SH1
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
92511537002
OF-002
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
4
PASI-A
EPA 200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
92511537003
OF-001 TTO
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12
PASI-A
EPA 245.1 Rev 3.01994
SOO
1
PASI-A
EPA625.1
PKS
58
PASI-C
EPA 624.1
SAS
35
PASI-C
EPA 420.4 Rev 1.01993
.JKG
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92511537004
OF-002 TTO
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12.
PASI-A
EPA 245.1 Rev 3.01994
SOO
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA624.1
SAS
35
PASI-C
EPA 420.4 Rev 1.01993
JKG
1
PASI-A
SM 4500-CN-E-2011
CA
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace. Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC. Page 4 of 41

aceAnalydcal
www.pacalabs.com
SUMMARY OF DETECTION
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)
1700
ug/L
662
12/19/20 00:20
EPA 200.7 Rev 4.4 1994
Zinc
35.5
ug/L
10.0
12/19/20 00:20
EPA 200.7 Rev 4.41994
Zinc, Dissolved
32.5
ug/L
10.0
12/16/2021:47 M1,R1
SM 25400-2011
Total Suspended Solids
7.6
mg/L
2.5
12/16/20 22:42
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)
2030
ug/L
662
12/19/20 00:24
EPA 200.7 Rev 4.4 1994
Zinc
68.1
ug/L
10.0
01/05/21 18:19
EPA 200.7 Rev 4.4 1994
Zinc, Dissolved
68.0
ug/L
10.0
01/05/21 17:31
SM 254OD-2011
Total Suspended Solids
2.5
mg/L
2.5
12/16/20 22:42
92511537003
OF-001 TTO
EPA 200.7 Rev 4.4 1994
Antimony
3.2J
ug/L
5.0
12/20/20 15:27
EPA 200.7 Rev 4.4 1994
Zinc
34.6
ug/L
10.0
12/20/20 15:27
92511537004
OF-002 TTO
EPA 200.7 Rev 4.4 1994
Zinc
59.7
ug/L
10.0
12/20/20 15:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, U.C.
Page 5 of 41

Pace Analytical Services, LLC
al"Analj6dal a 2225 Riverside Dr.
Asneville, NC 2880404
uww.Paaelabs.sen [phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 Lab ID: 92511537001 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters
Results Units POL
MDL
DF
Prepared
Analyzed CAS No. Oual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 5.0.
5.0
1
12/18/20 11:08
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
ND ug/L 5.0
4.3
1
12/17/20 02:09
12/19/20 00:20 7440-50-8
Lead
ND ug/L 5.0
4.5
1
12/17/20 02:09
12/19/20 00:20 7439-92-1
Hardness, Total(SM 2340B)
1700 ug/L 662
131
1
12/17/20 02:09
12/19/20 00:20
Zinc
35.5 ug/L 10.0
9.5
1
12/17/20 02:09
12/19/20 00:20 7440-66-6
200.7 MET ICP, Dissolved
Analytical Method: EPA 200.7 Rev 4.41994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pam Analytical Services -Asheville
Zinc, Dissolved
32.5 ug/L 10.0
2.5
1
12/1512009:43
12/1612021:47 7440-66-6 M1,R1
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
7.6 mg/L 2.5
2.5
1
12/16/20 22:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 41

Pace Analytical services, LLC
2225 (�
Rivers
de
IaceAnalj6cal' Asheville, NC 128804
wuu.Pscelsln.cem [phone]
ANALYTICAL RESULTS
Project: Crane Resistoflez
Pace Project No.: 92511537
Sample: OF-002 Lab ID: 92511537002 Collected: 12/14/20 07:25 Received: 12114/20 13:15 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared
Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 5.0
5.0
1
12/1812011:08
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND ug/L 5.0
4.3
1
12/17/20 02:09
12/19/20 00:24 7440-50-8
Lead
ND ug/L 5.0
4.5
1
12/17/20 02:09
12/19/20 00:24 7439-92-1
Hardness, Total(SM 2340B)
2030 ug/L 662
131
1
12/17/20 02:09
12/19/20 00:24
Zinc
68.1 ug/L 10.0
9.5
1
01/05/2113:03
01/0512118:19 7440-66-6
200.7 MET ICP, Dissolved
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Zinc, Dissolved
68.0 ug/L 10.0
2.5
1
01/05/21 15:20
01/05/21 17:31 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
2.5 mg/L 2.5
2.5
1
12/16/20 22:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 41

aceAnalj6cal
urm.pacelabe.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO
Lab ID:
92511537003
Collected:
12/14/20 06:55
Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
POL
MOIL
OF
Prepared
Analyzed
CAS No.
Qual
608 PCB Pest RVE
Analytical
Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services -
Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/15/20 14:51
12117/2019:39
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12/15/20 14:51
12/17/20 19:39
319-84-6
beta-BHC
NO
ug/L
0.050
0.014
1
12/15/20 14:51
12117/2019:39
319-85-7
M1
delta-BHC
NO
ug/L
0.050
0.020
1
12115/2014:51
12/17/20 19:39
319-86-8
M1
gamma-BHC (Lindane)
NO
ug/L
0.050
0.012
1
12/15/20 14:51
12/17/20 19:39
58-89-9
Chlordane (Technical)
NO
ug/L
0.50
0.14
1
12/1512014:51
12/17/20 19:39
57-74-9
alpha -Chlordane
NO
ug/L
0.050
0.0090
1
12/15/20 14:51
12/17/20 19:39
5103-71-9
gamma -Chlordane
ND
ug/L
0.050
0.017
1
12/15/20 14:51
12/17/20 19:39
5103-74-2
Mt
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/1512014:51
12/17/20 19:39
72-54-8
M1
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12115/2014:51
12/17/20 19:39
72-55-9
M1
4,4'-DDT
ND
u9/L
0.050
0.018
1
12115/2014:51
12/17/20 19:39
50-29-3
Dieldrin
NO
ug/L
0.050
0.0073
1
12115/2014:51
12/17/20 19:39
60-57-1
Endosulfan I
NO
ug/L
0.050
0.0094
1
12/15/20 14:51
12/17/20 19:39
959-98-8
Endosulfan 11
NO
ug/L
0.050
0,0065
1
12/15/20 14:51
12/17/20 19:39
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
0.0091
1
12/1512014:51
12/17/20 19:39
1031-07-8
M1
Endrin
NO
ug/L
0.050
0.0089
1
12/15/20 14:51
12/1712019:39
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/15/20 14:51
12/17/20 19:39
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/15/20 14:51
12/17/20 19:39
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
0.0097
1
12/15/20 14:51
12/17/20 19:39
1024-57-3
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
0.22
1
12/15/20 14:51
12/17/20 19:39
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.32
1
12/15/20 14:51
12/1712019:39
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
0.21
1
12/15/20 14:51
12/17/20 19:39
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
0.44
1
12/15120. 14:51
12/17/20 19:39
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/15/20 14:51
12/17/20 19:39
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/15/20 14:51
12/17/20 19:39
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/15/20 14:51
12/17/20 19:39
11096-82-5
PCB, Total
ND
ug/L
0.50
0.50
1
12/15/20 14:51
12/17/20 19:39.
1336-36-3
Toxaphene
ND
ug/L
0.50
0.19
1
12115/2014:51
12117/20.19:39
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
139
%
10-154
1
12/15/20 14:51
12/17/20 19:39
877-09-8
Decachlorobiphenyl (S)
172
%
10-184
1
12/15/20 14:51
12/17/20 19:39
2051-24-3
200.7 MET ICP
Analytical
Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA200.7 Rev 4.4 1994
Pace Analytical
Services -Asheville
Antimony
3.2J
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:27
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:27
7440-38-2
Beryllium
NO
ug/L
1.0
0.70
1
12/17/20 02:09
12/20/20 15:27
7440-41-7
Cadmium
NO
ug/L
1.0
0.40
1
12117/2002:09
12/20/20 15:27
7440-43-9
Chromium
NO
ug/L
5.0
3.7
1
12/17/20 02:09
12120/2015:27
7440-47-3
Copper
NO
ug/L
5.0
4.3
1
12/1712002:09
12120/2015:27
7440-50-8
Lead
NO
ug/L
5.0
4.5
1
12/1712002:09
12120/2015:27
7439-92-1
Nickel
NO
ug/L
5.0
3.5
1
12/17/20 02:09
1212012015:27
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:27
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:27
7440-22-4
Thallium
ND
ug/L
10.0
8.1
1
12/17/20 02:09
12/20/20 15:27
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, U.C. Page 8 of 41

aceAnalytical e
www.pacelabs.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc
34.6
ug/L
10.0
9.5
1
12/17/20 02:09
12/20/20 15:27
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND
ug/L
0.20
0.12
1
12/16/2012:20
12117/2012:05
7439-97-6
625 RVE
Analytical Method: EPA625.1
Preparation
Method: EPA625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
2.0
1
12115/2017:36
12/17/20 04:16
83-32-9
Acenaphthylene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/1712004:16
208-96-8
Anthracene
ND
ug/L
5.0
2.3
1
12/15/20 17:36
12/17/20 04:16
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
2.7
1
12/15/20 17:36
12/17/20 04:16
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:16
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
2.6
1
12/15/20 17:36
12/17/20 04:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
2.8
1
12/1512017:36
12/17/20 04:16
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
2.7
1
1211512017:36
12117/2004:16
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12117/2004:16
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
3.1
1
12115/2017:36
12/17/20 04:16
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
3.3
1
12115/2017:36
12/17/20 04:16
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
12/15/20 17:36
12/1712004:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:16
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.7
1
12/16/2017:36
12/17/20 04:16
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/1712004:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
7005-72-3
Chrysene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
3.0
1
12/15/20 17:36
12/17/20 04:16
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
8.1
1
12/15/20 17:36
12/17/20 04:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
120-83-2
Diethylphthalate
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:16
105-67-9
Dimelhylphthalate
ND
ug/L
5.0
2.1
1
12/1512017:36
12/17/20 04:16
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
3.4
1
12/15/20 17:36
12/17/20 04:16
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/15/20 17:36
12117/2004:16
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1.6
1
12/1512017:36
12117/2004:16
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
1211712004:16
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
3.9
1
12/15/20 17:36
12/17/20 04:16
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
3.7
1
12/15/20 17:36
12117/2004:16
117-81-7
Fluoranthene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
206-44-0
Fluorene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12/17/20 04:16
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/1712004:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12115/2017:36
1211712004:16
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.4
1
12115/2017:36
12/1712004:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
2.9
1
12/15/20 17:36
12/17/20 04:16
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 41

Pace Analytical Services, LLC
aceAnalytical a 2225 Riverside Asheville, NC 2880404
www.0aeelahs.cam
[phone]
ANALYTICAL RESULTS
Project: Crane Resistollex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected:. 12/14/2006:55 Received: 12/14/2013:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical
Method: EPA625.1 Preparation
Method: EPA625.1
Pace Analytical Services - Charlotte
Isophorone
NO
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:16
78-59-1
Naphthalene
NO
ug/L
5.0
2.1
1
12115/2017:36
12/1712004:16
91-20-3
Nitrobenzene
NO
ug/L
5.0
1.9
1
12/15/20 17:36
12117/2004:16
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
88-75-5
4-Nitrophenol
NO
ug/L
10.0
6.6
1
12115/2017:36
12117/2004:16
100-02-7
N-Nilrosodimethylamine
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/1712004:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1.3
1
12/1512017:36
12/17/20 04:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
3.0
1
12/15/20 17:36
12/1712004:16
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:16
108-60-1
Pentachlorophenol
NO
ug/L
10.0
3.8
1
12/15/20 17:36
12/17/20 04:16
87-86-5
Phenanthrene
ND
ug/L
5.0
2.0
1
12115/2017:36
12/17/20 04:16
85-01-8
Phenol
NO
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
108-95-2
Pyrene
NO
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
129-00-0
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:16
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
76
%
10-120
1
12/15/20 17:36
12/17/20 04:16
4165-60-0
2-Fluorobiphenyl (S)
47
%
15-120
1
12/15/20 17:36
12/17/20 04:16
321-60-8
Terphenyl-d14(S)
105
%
11-131
1
12/15/20 17:36
12/17/20 04:16
1718-51-0
Phenol-d6 (S)
40
%
10-120
1
12/15/20 17:36
12/17/20 04:16
13127-88-3
2-Fluorophenol (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:16
367-12-4
2,4,6-Tribromophenol(3)
97
%
10-137
1
12/1512017:36
12/17/20 04:16
118-79-6
624 Volatile Organics Acrolein
Analytical Method: EPA
624.1
Pace Analytical Services - Charlotte
Acrolein
NO
ug/L
5.0
3.8
1
12/1512019:01
107-02-8
Benzene
NO
ug/L
1.0
0.38
1
12/15/20 19:01
71-43-2
Bromodichloromelhane
ND
ug/L
2.0
0.24
1
12/15/2019;01
75-27-4
Bromoform
NO
ug/L
2.0
0.40
1
12115/2019:01
75-25-2
Bromomethane
NO
ug/L
2.0
1.2
1
12115/2019:01
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
0.29
1
12/15/20 19:01
56-23-5
Chlorobenzene
NO
ug/L
2.0
0.37
1
12/1512019:01
108-90-7
Chloroethane
NO
ug/L
2.0
1.4
1
12/15/20 19:01
75-00-3
Chloroform
NO
ug/L
2.0
0.58
1
1211512019:01
67-66-3
Chloromethane
NO
ug/L
2.0
0.73
1
12/1512019:01
74-87-3
Dibromochloromelhane
ND
ug/L
2.0
0.32
1
12/15/20 19:01
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
0.24
1
12/15/20 19:01
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
0.31
1
12115/2019:01
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
0.41
1
12/15/20 19:01
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
0.51
1
12/15/20 19:01
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
0.34
1
12/1512019:01
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
0.41
1
12/1512019:01
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
0.42
1
12/15/20 19:01
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
0.42
1
12/15/20 19:01
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
0.27
1
12/15/20 19:01
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 41

ZeAnalyficalo
www.pacelebs.cem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters
624 Volatile Organics Acrolein
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,22-Tetmchloroethane
Tetrachloroethene
Toluene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroelhene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
420.4 Phenolics, Total
Phenol
450OCNE Cyanide, Total
Cyanide
Date: 01/11/2021 12:50 PM
Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND
ug/L
2.0
0.33
1
12/1512019:01
10061-01-5
ND
ug/L
2.0
0.41
1
12/15/20 19:01
10061-02-6
ND
ug/L
1.0
0.28
1
12/15/2019:01
100-41-4
ND
ug/L
2.0
0.24
1
12/15/2019:01
75-09-2
ND
ug/L
2.0
0.34
1
12/15/2019:01
79-34-5
ND
ug/L
2.0
0.28
1
12/15/20 19:01
127-18-4
NO
ug/L
1.0
0.44
1
12/15/2019:01
108-88-3
NO
ug/L
2.0
0.35
1
12/1512019:01
71-55-6
ND
ug/L
2.0
0.31
1
1211512019:01
79-00-5
ND
ug/L
2.0
0.36
1
12/1512019:01
79-01-6
ND
ug/L,
2.0
0.28
1
12/15/2019:01
75-69-4
ND
ug/L
2.0
0.72
1
12/15/2019:01
75-01-4
94
%
70-130
1
12/15/20 19:01
460-00-4
97
%
70-130
1
12115/2019:01
2037-26-5
90
%
70-130
1
12/15/2019:01
17060-07-0
Analytical
Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
NO
mg/L
0.020
0.0076
1
12/17/20 09:35 12/17/20 15:15
108-95-2
Analytical
Method: SM
4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND
mg/L
0.0080
0.0060
1
1211512001:23 12/15/2023:37
57-12-5 M1,R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 41

aceftfj4ical e
www.patelahs.cam
ANALYTICAL RESULTS
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace. Analytical Services.-
Charlotte
Aldrin
NO
ug/L
0.050
0.022
1
12115/2014:51
12/17/20 20:37
309-00-2
alpha-BHC
NO
ug/L
0.050
0.019
1
12/15/20 14:51
12/17/20 20:37
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12115/2014:61
12/1712020:37
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/15/20 14:51
12117/2020:37
319-86-8
gamma-BHC(Lindane)
NO
ug/L
0.050
0.012
1
12115/2014:51
12/1712020:37
58-89-9
Chlordane(Technicel)
NO
ug/L
0.50
0.14
1
12115/2014:51
12/1712020:37
57-74-9
alpha -Chlordane
NO
ug/L
0.050
0.0090
1
12/1512014:51
12/17/20 20:37
5103-71-9
gamma -Chlordane
NO
ug/L
0.050
0.017
1
12/1512014:51
12/17/20 20:37
5103-74-2
4,4'-DDD
NO
ug/L
0.050
0.0069
1
12/15/20 14:51
12/17/20 20:37
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/1512014:51
12/17/20 20:37
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
1211512014:51
12/17/20 20:37
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/15/20 14:51
12117/2020:37
60-57-1
Endosulfan I
NO
ug/L
0.050
0.0094
1
12/15/20 14:51
12/17/20 20:37
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/15/20 14:51
12/17/20 20:37
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12115/2014:51
1211712020:37
1031-07-8
Endrin
NO
ug/L
0.050
0.0089
1
12/15/20 14:51
12/17/20 20:37
72-20-8
Endrin aldehyde
NO
ug/L
0.050
0.013
1
12/15/20 14:51
12/17/20 20:37
7421-93-4
Heptachlor
NO
ug/L
0.050
0.016
1
12/1512014:51
12/1712020:37
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
0.0097
1
12/15/20 14:51
12/1712020:37
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/15/20 14:51
12/17/20 20:37
12674-11-2
PCB-1221(Aroclor 1221)
ND
ug/L
0.50
0.32
1
12115/2014:51
12/17/20 20:37
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/15/20 14:51
12/17/20 20:37
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
0.44
1
12/15/20. 14:51
12/17/20 20:37
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/15/20 14:51
12/17/20 20:37
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/15/20 14:51
12/17/20 20:37
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/15/20 14:51
12/17/20 20:37
11096-82-5
PCB, Total
NO
ug/L
0.50
0.50
1
12115/2014:51
12117/2020:37
1336-36-3
Toxaphene
NO
ug/L
0.50
0.19
1
12/1512014:51
12/17/20 20:37
8001-35-2
Surrogates
Tetrachloro-m-xylene(S)
209
%
10-154
1
12/1512014:51
12/1712020:37
877-09-8 S3
Decachlorobiphenyl (S)
263
%
10-184
1
12/15/20 14:51
12/17/20 20:37
2051-24-3 S3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services
- Asheville
Antimony
NO
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:30
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:30
7440-38-2
Beryllium
ND
ug/L
1.0
0.70
1
12117/2002:09
12/20/20 15:30
7440-41-7
Cadmium
NO
ug/L
1.0
0.40
1
12/17/20 02:09
12/20/20 15:30
7440-43-9
Chromium
NO
ug/L
5.0
3.7
1
12/17/20 02:09
12120/2015:30
7440-47-3
Copper
NO
ug/L
5.0
4.3
1
12/17/20 02:09
12/20/2015:30
7440-50-8
Lead
NO
ug/L
5.0
4.5
1
12/17/20 02:09
12/20/20 15:30
7439-92-1
Nickel
NO
ug/L
5.0
3.5
1
12/17/20 02:09
12/2012015:30
7440-02-0
Selenium
NO
ug/L
10.0
4.7
1
12117/2002:09
12/2012015:30
7782-49-2
Silver
NO
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:30
7440-22-4
Thallium
ND
ug/L
10.0
8.1
1
12/17/20 02:09
12/20/20 15:30
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except In full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 41

al"Analytical
www.pacelain.co n
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc
59.7
ug/L
10.0
9.5
1
12/17/20 02:09
12/20/20 15:30
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Rev 3.0
1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND
ug/L
0.20
0.12
1
1211612012:20
12117/2012:07
7439-97-6
625 RVE
Analytical Method: EPA 625.1
Preparation
Method: EPA 625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
83-32-9
Acenaphthylene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
208-96-5
Anthracene
ND
ug/L
5.0
2.3
1
1211512017:36
12/17/20 04:45
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
2.7
1
12115/2017:36
1211712004:45
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:45
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
2.6
1
12/15/20 17:36
12/17/20 04:45
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
2.8
1
12/1512017:36
12/1712004:45
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
2.7
1
12115/2017:36
12/1712004:45
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1.8
1
12/1512017:36
12/1712004:45
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
3.1
1
12/15/20 17:36
12/17/20 04:45
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
3.3
1
12115/2017:36
12117/2004:45
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
12/15/20 17:36
12117/2004:45
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.7
1
1211512017:36
12/1712004:45
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:45
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
7005-72-3
Chrysene
ND
ug/L
5.0
2.8
1
1211512017:36
12/1712004:45
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
3.0
1
12/15/20 17:36
12/17/20 04:45
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
8.1
1
12/15/20 17:36
12/17/20 04:45
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
120-83-2
Diethylphthalate
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:45
105-67-9
Dimethylphthalate
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
10.0
3.4
1
12/15/20 17:36
12/17/20 04:45
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
26.0
1
12/15/20 17:36
12/17/20 04:45
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1.6
1
12/15/20 17:36
12/17/20 04:45
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1.7
1
12115/2017:36
12/17/20 04:45
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
3.9
1
12/15/20 17:36
12/17/20 04:45
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
3.7
1
1211512017:36
12/17/20 04:45
117-81-7
Fluoranthene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
206-44-0
Fluorene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1.8
1
12/1512017:36
12/1712004:45
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/1512017:36
12/17/20 04:45
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
2.9
1
12115/2017:36
12/1712004:45
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 41

Pace Analytical Services, LLC
(�15'ceAnalj4ical' 2225 Riverside Asheville, NC 2880404
www.pecelabs.cem [phone]
ANALYTICAL RESULTS
Project: Crane Resisto0ex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical Services- Charlotte
Isophorone
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:45
78-59-1
Naphthalene
ND
ug/L
5.0
2.1
1
12/1512017:36
12117/2004:45
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.9
1
12/1512017:36
1211712004:45
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1.4
1
12115/2017:36
1211712004:45
88-75-5
4-Nitrophenol
ND
ug/L
10.0
6.6
1
12/15/20 17:36
12/17/20 04:45
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1.3
1
1211512017:36
12/17/20 04:45
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
3.0
1
12/15/20 17:36
12/17/20 04:45
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1.2
1
12115/2017:36
12/17/20 04:45
108-60-1
Pentachlorophenol
ND
ug/L
10.0
3.8
1
12115/2017:36
12/17/20 04:45
87-86-5
Phenanthrene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
85-01-8
Phenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
108-95-2
Pyrene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:45
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.6
1
12/1512017:36
12/17/20 04:45
88-06-2
Surrogates
Nitrobenzene-d5 (S)
86
%
10-120
1
12/15/20 17:36
12/17/20 04:45
4165-60-0
2-Fluombiphenyl (S)
52
%
15-120
1
12/15/20 17:36
12/17/20 04:45
321-60-8
Terphenyl-d14 (S)
121
%
11-131
1
12/15/20 17:36
12/17/20 04:45
1718-51-0
Phenol-d6 (S)
49
%
10-120
1.
12/15120 17:36
12/17/20 04:45
13127-88-3
2-Fluorophenol (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:45
367-12-4
2,4,6-Tribromophenol(S)
90
%
10-137
1
12/15/20 17:36
12/17/20 04:45
118-79-6
624 Volatile Organics Acrolein
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
Acrolein
ND
ug/L
5.0
3.8
1
12/15/20 19:19
107-02-8
Benzene
ND
ug/L
1.0
0.38
1
12/15/20 19:19
71-43-2
Bromodichloromethane
ND
ug/L
2.0
0.24
1
12/1512019:19
75-27-4
Bromoform
ND
ug/L
2.0'
0.40
1
12/1512019:19
75-25-2
Bromomethane
ND
ug/L
2.0
1.2
1
12/15/20 19:19
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
0.29
1
12/15/20 19:19
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12115/2019:19
108-90-7
Chloroethane
ND
ug/L
2.0
1.4
1
12115/2019:19
75-00-3
Chloroform
ND
ug/L
2.0
0.58
1
12/15/20 19:19
67-66-3
Chloromethane
ND
ug/L
2.0
0.73
1
12/15/20 19:19
74-87-3
Dibromochloromethane
ND
ug/L
2.0
0.32
1
12/15/20 19:19
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
0.24
1
12/15/20 19:19
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
0,31
1
12/15/20 19:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
0A1
1
12/15/20 19:19
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
0.51
1
12115/2019:19
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
0.34
1
1211512019:19
107-06-2 M1
1,1-Dichloroethene
ND
ug/L
2.0
0.41
1
1211512019:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
1211512019:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12115/2019:19
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
0.27
1
12/15/20 19:19
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/202112:50 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 41

aceAnalj6cal
urawpecslabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters
624 Volatile Organics Acrolein
cis-1,3-Dich loropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
TeVachloroethene
Toluene
1.1,1-Trich loroethane
1,1,2-Trich loroethane
Trichloroethene
Trich lorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8(S)
1,2-Dichloroethane-d4 (S)
420.4 Phenolics, Total
Phenol
450OCNE Cyanide, Total
Cyanide
Date: 01/11/2021 12:50 PM
Results Units POL
MDL DF Prepared Analyzed CAS No. Oual
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
ND ug/L 2.0
0.33
1
12/1512019:19
10061-01-5
ND ug/L 2.0
0.41
1
12/15/2019:19
10061-02-6
ND ug/L 1.0
0.28
1
12/15/2019:19
100-41-4
ND ug/L 2.0
0.24
1
12/15/2019:19
75-09-2
ND ug/L 2.0
0.34
1
12/15/2019:19
79-34-5
ND ug/L 2.0
0.28
1
12/15/2019:19
127-18-4
ND ug/L 1.0
0.44
1
12115/2019:19
108-88-3
ND ug/L 2.0
0.35
1
12/15/2019:19
71-55-6
ND ug/L 2.0
0.31
1
12115/2019:19
79-00-5
ND ug/L 2.0
0.36
1
1211512019:19
79-01-6
ND ug/L 2.0
0.28
1
12/1512019:19
75-69-4
ND ug/L 2.0
0.72
1
1211512019:19
75-01-4
93 % 70-130
1
12115/2019:19
460-00-4
98 % 70-130
1
12115/2019:19
2037-26-5
90 % 70-130
1
12/15/2019:19
17060-07-0
Analytical Method: EPA 420.4 Rev 1.01993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.020
0.0076
1
12/17/2009:35 12/1712015:16
108-95-2
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND mg/L 0.0080
0.0060
1
12/15/20 01:23 12/15/20 23:39
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 41

aceAnalytical
vrww.pecelehe.eore
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 588138 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537001 92511537002
METHOD BLANK: 3107878 Matrix: Water
Associated Lab Samples: 92511537001, 92511537002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L NO 5.0 5.0 12/18/20 11:08
LABORATORY CONTROL SAMPLE: 3107879
Spike LCS LCS %Rec
Parameter .Units Conic. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L - 20 15.6 78 64-132
MATRIX SPIKE SAMPLE: 3107880
35598602001 Spike MS MS e/ Rec
Parameter Units. Result Conic. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 5.01.1 20 11.7 54 64-132 M7
Results presentee on this page are In the units Indicated by the "units" column except where an alternate unit Is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, -LC.
Page 16 of 41

aceAnalytical e
www.pacelablixem
QUALITY CONTROL DATA
Project: Crane Resistofiex
Pace Project No.: 92511537
QC Batch: 587409 Analysis Method: EPA 245.1 Rev 3.01994
QC Balch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3104355 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit
Mercury ug/L NO 0.20
LABORATORY CONTROL SAMPLE: 3104356
Spike LCS
Parameter Units Conc. Result
Mercury ug/L 2.5 2.2
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MDL Analyzed Qualifiers
0.12 12/17/20 11:53
LCS % Rec
%Rec Limits Qualifiers
87 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104357 3104358
MS MSD
92509470001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.3 2.4 91 95 70-130 4 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104359 3104360
MS MSD
92511537003 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result e/ Rao %Rec Limits RPD RPD Oust
Mercury ug/L ND 2.5 2.5 2.3 2.6 91 101 70-130 10 20
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 17 of 41

aceAnalXical e
wwe.pacelabs.c pt
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, INC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
-
QC Batch: 587665
Analysis Method: EPA 200.7 Rev 4.41994
QC Batch Method: EPA 200.7 Rev 4.4
1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537001, 92511537002, 92511537003, 92511537004
METHOD BLANK: 3105714
Matrix: Water
Associated Lab Samples: 92511537001, 92511537002, 92511537003, 92511537004
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Antimony
ug/L
NO 5.0
3.0
12/20/2015:11
Arsenic
ug/L
ND 10.0
4.7
12/2012015:11
Beryllium
ug/L
ND 1.0
0.70
12/2012015:11
Cadmium
ug/L
NO 1.0
0.40
12/20/2015:11
Chromium
ug/L
ND 5.0
3.7
12/20/2015:11
Copper
ug/L
NO 5.0
4.3
12/2012015:11
Hardness, Total(SM 2340B)
ug/L
NO 662
131
12/20/20 15:11
Lead
ug/L
NO 5.0
4.5
12/20/2015:11
Nickel
ug/L
NO 5.0
3.5
12/20/2015:11
Selenium
ug/L
NO 10.0
4.7
12120/2015:11
Silver
ug/L
NO 5.0
2.5
12120/2015:11
Thallium
ug/L
NO 10.0
8.1
12120/2015:11
Zinc
ug/L
NO 10.0
9.5
12120/2015:11
LABORATORY CONTROL SAMPLE:
3105715
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
%Rec
Limits Qualifiers
Antimony
ug/L
500 483
97
85-115
Arsenic
ug/L
500 482
96
85-115
Beryllium
ug/L
500 489
98
85-115
Cadmium
ug/L
500. 498
100
85-115
Chromium
ug/L
500 499
100
85-115
Copper
ug/L
500 496
99
85-115
Hardness, Total(SM 2340B)
ug/L
33100 32500
98
85-115
Lead
ug/L
500 490
98
85-115
Nickel
ug/L
500 497
99
85-115
Selenium
ug/L
500 484
97
85-115
Silver
ug/L
250 246
98
85-115
Thallium
ug/L
500 497
99
85-115
Zinc
ug/L
500 498
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105716 3105717
MS MSD
92511027001 -
Spike Spike MS
MSD
MS
MSD % Rec
Max
Parameter Units
Result
Conc. Conc. Result
Result
% Rec % Rec Limits RPD
RPD Qual
Antimony ug/L
15.6
500 500 511
507
99 98 70-130 1
20
Arsenic ug/L
NO
500 500 489
484
98 97 70-130 1
20
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 41

Pace Analytical Services, LLC
ZeAnalj4icalo
2225 RiversideC28 04
Asheville, NC 288g4
www.paeelabs.con
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3105716
3105717
MS
MSD
92511027001
Spike
Spike
MS
MSD
Ms
MSD
% Rae
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Beryllium
ug/L
ND
500
500
498
492
100
98
70-130
1
20
Cadmium
ug/L
ND
500
500
492
485
98
97
70-130
1
20
Chromium
ug/L
ND
500
500
489
481
97
96
70-130
1
20
Copper
ug/L
7.6
500
500
518
514
102
101
70-130
1
20
Hardness, Total(SM 2340B)
ug/L
9800
33100
33100
43300
42700
101
100
70-130
1
20
Lead
ug/L
ND
500
500
481
473
96
95
70-130
2
20
Nickel
ug/L
ND
500
500
496
490
99
98
70-130
1
20
Selenium
ug/L
ND
500
500
504
507
101
101
70-130
1
20
Silver
ug/L
ND
250
250
253
253
101
101
70-130
0
20
Thallium
ug/L
ND
500
500
476
466
95
93
70-130
2
20
Zinc
ug/L
106
500
500
602
591
99
97
70-130
2
20
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3105718
3105719
MS
MSD
92511033003
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rae
% Rae
Limits
RPD
RPD Qual
Antimony
ug/L
23.8
500
500
511
518
97
99
70-130
1
20
Arsenic
ug/L
ND
500
500
502
508
100
101
70-130
1
20
Beryllium
ug/L
ND
500
500
503
508
101
102
70-130
1
20
Cadmium
ug/L
3.3
500
500
494
500
98
99
70-130
1
20
Chromium
ug/L
235
500
500
721
725
97
98
70-130
1
20
Copper
ug/L
327
500
500
866
871
108
109
70-130
1
20
Hardness, Total(SM 2340B)
ug/L
108000
33100
33100
140000
141000
97
100
70-130
1
20
Lead
ug/L
114
500
500
611
619
99
101
70-130
1
20
Nickel
ug/L
103
500
500
597
595
99
98
70-130
0
20
Selenium
ug/L
ND
500
500
495
499
99
100
70-130
1
20
Silver
ug/L
ND
250
250
255
257
102
103
70-130
1
20
Thallium
ug/L
ND
500
500
441
450
88
90
70-130
2
20
Zinc
ug/L
6290
500
500
6540
6640
50
70
70-130
2
20 Mt
Results presented on this page are In Me units Indicated by Me "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/111202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 19 of 41

aceAnaljftal
www.lracelabs.com
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 590708
QC Batch Method: EPA 200.7 Rev 4.4 1994
QUALITY CONTROL DATA
Analysis Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118555 Matrix: Water
Associated Lab Samples: 92611537002
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Blank
Reporting
Parameter Units
Result
Limit MDL
Analyzed Qualifiers
Zinc ug/L
ND 10.0.
9.5 01/05/21 18:12
LABORATORY CONTROL SAMPLE: 3118556
Spike
LCS LCS
% Rae
Parameter Units
Conc.
Result %Rec
Limits Qualifiers
Zinc ug/L
500
476 95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118557 3118558
MS MSD
92511537002 Spike Spike MS MSD MS MSD % Rae Max
Parameter Units Result Conc. Cones Result Result % Rae % Rae Limits RPD RPD Qual
Zinc ug/L 68.1 500 500 567 580 100 102 70-130 2 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, U.C. Page 20 of 41

aceAnalydcal
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 586977
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537001
METHOD BLANK: 3102330
Matrix: Water
Associated Lab Samples: 92511537001
Blank Reporting
Parameter Units
Result Limit MOIL Analyzed Qualifiers
Zinc, Dissolved ug/L
ND 10.0 2.5 12/16/2021:40
LABORATORY CONTROL SAMPLE: 3102331
Spike LCS LCS %Rec
Parameter Units
Conc. Result %RecLimits Qualifiers
Zinc, Dissolved ug/L
500 449 90 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102332 3102333
MS MSD
92511537001
Spike Spike MS MSD MS MSD %Rec
Max
-, Parameter Units Result
Conc. Conc. Result Result %Rec %Rec Limits RPD
RPD Qual
Zinc, Dissolved ug/L 32.5
500 500 62.3 470 6 88 70-130 153
20 M1,R1
Results presented on this page are In the units Indicated by the "units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C.
Page 21 of 41

aceAnalytical
www.pacelabs.caR
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistofiex
Pace Project No.:
92511537
QC Batch:
590706
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method:
EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118545 Matrix: Water
Associated Lab Samples: 92511537002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Zinc, Dissolved ug/L NO 10.0 2.5 01/05/21 17:11
LABORATORY CONTROL SAMPLE: 3118546
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
%Rec
Limits Qualifiers
Zinc, Dissolved
ug/L
Soo
472
94
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118547
3118548
MS
MSD
92511537002
Spike
Spike MS
.MSD
MS MSD %Rec Max
Parameter
Units Result
Cone.
Cone. Result
Result.
%Rec %Rec Limits RPD RPD Qual
Zinc, Dissolved
ug/L 68.0
500
500 543
535
95 93 70-130 1 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01111/202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 22 of 41

aceAnalytical
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QUALITY CONTROL DATA
Project: Crane Resistofiex
Pace Project No.: - 92511537
QC Batch: 587031
Analysis Method:
EPA 624.1
QC Batch Method: EPA 624.1
Analysis Description:
624 MSV with
Acrolein
Laboratory:
Pace Analytical Services
- Charlotte
Associated Lab Samples: 92511537003,
92511537004
METHOD BLANK: 3102522
Matrix: Water
Associated Lab Samples: 92511537003,
92511537004
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
1. 1, 1 -Trichloroethane
ug/L
ND
2.0
0.35
12/15/20 11:41
1, 1,2,2-Tetrachloroethane
ug/L
ND
2.0
0.34
12/1512011:41
1,1,2-Trichloroethane
ug/L
ND
2.0
0.31
12/1512011:41
1,1-Dichloroethane
ug/L
ND
2.0
0.51
12/15/20 11:41
1,1-Dichloroethene
ug/L
ND
2.0
0.41
12/15/20 11:41
1,2-Dichlorobenzene
ug/L
ND
2.0
0.24
12/15/20 11:41
1,2-Dichloroethane
ug/L
ND
2.0
0.34
12/15/20 11:41
1,2-Dichloropropane
ug/L
ND
2.0
0.27
12/15/20 11:41
1,3-Dichlorobenzene
ug/L
ND
2.0
0.31
12/15/20 11:41
1,4-Dichlorobenzene
ug/L
ND
2.0
0.41
12/15/20 11:41
Acrolein
ug/L
ND
5.0
3.8
12115/2011:41
Benzene
ug/L
ND
1.0
0.38
12/15/20 11:41
Bromodichloromethane
ug/L
ND
2.0
0.24
12115/2011:41
Bromoform
ug/L
ND
2.0
0.40
12/15/20 11:41
Bromomethane
ug/L
ND
2.0
1.2
12115/2011:41
Carbon tetrachloride
ug/L
ND
2.0
0.29
12/15/20 11:41
Chlorobenzene
ug/L
ND
2.0
0.37
12/1512011:41
Chloroethane
ug/L
ND
2.0
1.4
12/15/20 11:41
Chloroform
ug/L
ND
2.0
0.58
12/15/2011:41
Chloromethane
ug/L
ND
2.0
0.73
12/1512011:41
cis-1,2-Dichloroethene
ug/L
ND
2.0
0.42
12/1512011:41
cis-1,3-Dichloropropene
ug/L
ND
2.0
0.33
12/1512011:41
Dibromochloromethane
ug/L
ND
2.0
0.32
12/15/20 11:41
Ethylbenzene
ug/L
ND
1.0
0.28
12/15/20 11:41
Methylene Chloride
ug/L
ND
2.0
0.24
12/15/20 11:41
Tetrachloroelhene
ug/L
ND
2.0
0.28
12/15/20 11:41
Toluene
ug/L
ND
1.0
0.44
12/15/2011 :41
trans-1,2-Dichloroethene
ug/L
ND
2.0
0.42
12/15/20 11:41
trans-1,3-Dichloropropene
ug/L
ND
2.0
0.41
12/1512011:41
Trichloroethene
ug/L
ND
2.0
0.36
12/1512011:41
Trichlorofluoromethane
ug/L
ND
2.0
0.28
12/1512011:41
Vinyl chloride
ug/L
ND
2.0
0.72
12/15/20 11:41
1,2-Dichloroethane-d4 (S)
%
91
70-130
12/15/20 11:41
4-Bromofluorobenzene (S)
%
95
70-130
12/15/20 11:41
Toluene-d8 (S)
%
97
70-130
12/15/20 11:41
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C. Page 23 of 41

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QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE: 3102523
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conic.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
20
16.2
81
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
21.9
110
70-130
1,1,2-Trichloroethane
ug/L
20
17.8
89
70-130
1,1-Dichloroethane
ug/L
20
16.3
81
70-130
1,1-Dichloroethene
ug/L
20
16.0
80
70-132
1,2-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,2-Dichloroethane
ug/L
20
15.1
76
70-130
1,2-Dichloropropane
ug/L
20
18.4
92
70-130
1,3-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,4-Dichlorobenzene
ug/L
20
23.7
118
70-130
Acrolein
ug/L
100
106
106
60-140
Benzene
ug/L
20
18.1
91
70-130
Bromodichloromethane
ug/L
20
16.9
85
70-130
Bromoform
ug/L
20
18.7
94
70-130
Bromomethene
ug/L
20
18.1
91
30-177
Carbon tetrachloride
ug/L
20
17.9
89
70-130
Chlorobenzene
ug/L
20
21.8
109
70-130
Chloroethane
ug/L
20
15.8
79
46-131
Chloroform
ug/L
20
15.5
78
70-130
Chloromethane
ug/L
20
14.8
74
49-130
cis-1,2-Dichloroethene
ug/L
20
15.3
77
70-130
cis-1,3-Dichloropropene
ug/L
20
18.6
93
70-130
Dibromochloromethane
ug/L
20
21.7
109
70-130
Ethylbenzene
ug/L
20
21.5
108
70-130
Methylene Chloride
ug/L
20
14.1
71
68-130
Tetrachloroethene
ug/L
20
22.1
110
70-130
Toluene
ug/L
20
18.1
90
70-130
trans-1,2-Dichloroethene
ug/L
20
16.3
82
70-130
trans-1,3-Dichloropropene
ug/L
20
18.0
90
70-130
Trichloroethene
ug/L
20
18.8
94
70-130
Trichlorofluoromethane
ug/L
20
16.7
84
61-130
Vinyl chloride
ug/L
20
15.4
77
59-142
1,2-Dichloroethane-d4(S)
%
87
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-dB(S)
%
94
70-130
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 3102524
3102525
MS
MSD
92511537004
Spike
Spike
MS
MSD
MS
MSD
e/ Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qua]
1,1,1-Trichloroethane
ug/L
NO
20
20
15.9
18.1
80
90
70-148
13
21
1,1,2,2-Tetachloroethane
ug/L
NO
20
20
20.1
21.4
100
107
70-131
7
30
1,1,2-Trichloroethane
ug/L
ND
20
20
16.9
18.2
85
91
70-136
7
27
1,1-Dichloroethane
ug/L
ND
20
20
15.5
17.8
77
89
71-143
14
30
1,1-Dichloroethene
ug/L
ND
20
20
14.8
17.6
74
88
70-158
17
30
Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 41

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102524 3102525
MS MSD
92511537004 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result e/ Rae % Rae Limits RPD RPD Dual
1,2-Dichlorobenzene
ug/L
NO
20
20
21.5
24.1
107
121
70-133
12
30
1,2-Dichloroethane
ug/L
NO
20
20
13.9
16.3
70
81
72-137
15
29 M1
1,2-Dichloropropane
ug/L
NO
20
20
17.3
19.5
87
98
70-138
12
30
1,3-Dichlorobenzene
ug/L
NO
20
20
22.0
24.6
110
123
75-133
11
24
1,4-Dichlorobenzene
ug/L
NO
20
20
21.8
24.2
109
121
70-133
11
30
Acrolein
ug/L
ND
100
100
91.6
101
92
101
50-150
9
30
Benzene
ug/L
ND
20
20
17.5
19.5
88
97
75-125
11
30
Bromodichloromethane
ug/L
ND
20
20
15.3
17.4
77
87
70-138
13
30
Bromoform
ug/L
ND
20
20
15.8
18.8
79
94
57-138
17
25
Bromomethane
ug/L
ND
20
20
16.0
17.8
80
89
10-200
10
35
Carbon tetrachloride
ug/L
ND
20
20
17.0
18.9
85
94
70-125
10
26
Chlorobenzene
ug/L
ND
20
20
21.0
23.3
105
117
82-137
10
29
Chloroethane
ug/L
ND
20
20
14.7
17.9
74
90
51-166
20
30
Chloroform
ug/L
ND
20
20
15.3
17.6
77
88
70-121
14
30
Chloromethane
ug/L
ND
20
20
13.6
16.0
68
80
24-161
16
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
14.6
17.1
73
85
67-148
16
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
17.4
19.5
87
98
70-142
11
30
Dibromochloromethane
ug/L
ND
20
20
19.4
22.4
97
112
69-133
14
30
Ethylbenzene
ug/L
ND
20
20
20.5
22.7
102
113
75-134
10
30
Methylene Chloride
ug/L
ND
20
20
13.0
14.9
65
75
64-148
14
30
Tetrachloroethene
ug/L
ND
20
20
21.2
23.7
106
119
70-133
11
23
Toluene
ug/L
ND
20
20
17.2
18.8
86
94
75-134
9
22
trans-1,2-Dichloroethene
ug/L
ND
20
20
14.8
17.7
74
89
70-143
18
27
trans-1,3-Dichloropropene
ug/L
ND
20
20
16.4
18.2
82
91
70-138
10
30
Trichloroethene
ug/L
ND
20
20
18.2
20.4
91
102
75-138
11
29
Trichlorofluoromethane
ug/L
NO
20
20
14.7
18.4
74
92
61-154
22
30
Vinyl chloride
ug/L
NO
20
20
14.5
17.1
73
85
55-172
16
30
1,2-Dichloroethane-d4 (S)
%
85
93
70-130
4-Bromofluorobenzene (S)
%
93
98
70-130
Toluene-d8(S)
%
93
94
70-130
Results presented on this page are in the units Indicated by the "unite' column except where an alternate unit Is prosentod to the right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 41

aceAnalytical
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Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587108
QC Batch Method: EPA 608.3
QUALITY CONTROL DATA
Analysis Method: EPA608.3
Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3103046 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Parameter
Units
Blank
Result
Reporting
Limit
MDL
Analyzed Qualifiers
4,4'-DDD
ug/L
NO
0,050
0.0069
12/17/20 22:19
4,4'-DDE
ug/L
NO
0.050
0.0064
12/17/20 22:19
4,4'-DDT
ug/L
NO
0.050
0.018
12/17/20 22:19
Aldrin
ug/L
NO
0.050
0.022
12/17/20 22:19
alpha-BHC
ug/L
ND
0.050
0.019
1211712022:19
alpha -Chlordane
ug/L
NO
0.050
0.0090
12/17/20 22:19
beta-BHC -
ug/L
NO
0.050
0.014
12/17/20 22:19
Chlordane (Technical)
ug/L
NO
0.50
0.14
12/1712022:19
delta-BHC
ug/L
NO
0.050
0.020
12/17/20 22:19
Dielddn
ug/L
ND
0.050
0.0073
12/17/20 22:19
Endosulfan I
ug/L
ND
0.050
0.0094
12/1712022:19
Endosulfan 11
ug/L
NO
0.050
0,0065
12/1712022:19
Endosulfan sulfate
ug/L
ND
0.050
0.0091
12/17/20 22:19
Endrin
ug/L
ND
0.050
0.0089
12/17/20 22:19
Endrm aldehyde
ug/L
NO
0.050
0.013
12/1712022:19
gamma-BHC(Lindane)
ug/L
NO
0.050
0.012
12/1712022:19
gamma -Chlordane
ug/L
NO
0.050
0.017
12117/2022:19
Heptachlor
ug/L
ND
0.050
0.016
12/17/20 22:19
Heptachlor epoxide
ug/L
ND
0.050
0.0097
12117/2022:19
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
0.22
12/17/20 22:19
PCB-1 221 (Aroclor 1221)
ug/L
ND
0.50
0.32
12/17/20 22:19
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
0.21
12/17/20 22:19
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
0.44
12/17/20 22:19
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
0.34
12/17/20 22:19
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
0.24
12/17/20 22:19
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
0.30
12/17/20 22:19
Toxaphene
ug/L
ND
0.50
0.19
12117/2022:19
Decachlorobiphenyl (S)
%
231
10-184
12/17/20 22:19 S3
Tetrachloro-m-xylene (S)
%
133
10-154
12/17/20 22:19
LABORATORY CONTROL SAMPLE:
3103047
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result %Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 4.4 89
50-137
PCB-1260 (Aroclor 1260)
ug/L
5 4.5 89
42-140
Decachlorobiphenyl (S)
%
209
10-184 SO
Tetrachloro-m-xylene (S)
%
117
10-154
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C. Page 26 of 41

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
3103079
Spike
LCS
LCS
% Rae
Parameter
Units
Cone. Result
%Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.28
114
45-141
4,4'-DDE
ug/L
0.25
0.26
104
37-141
4,4'-DDT
ug/L
0.25
0.33
133
52-160
Aldrin
ug/L
0.25
0.14
55
42-130
alpha-BHC
ug/L
0.25
0.30
121
37-139
alpha -Chlordane
ug/L
0.25
0.25
100
45-139
beta-BHC
ug/L
0.25
0.34
134
39-147
delta-BHC
ug/L
0.25
0.28
113
39-140
Dieldrin
ug/L
0.25
0.28
112
40-146
Endosulfan I
ug/L
0.25
0.27
107
45-145
Endosulfan II
ug/L
0.25
0.30
119
47-153
Endosulfan sulfate
ug/L
0.25
0.34
136
48-144
Endrin
ug/L
0.25
0.27
109
41-147
Endrin aldehyde
ug/L
0.25
0.30
119
45-146
gamma-BHC (Lindane)
ug/L
0.25
0.31
125
42-140
gamma -Chlordane
ug/L
0.25
0.29
117
45-140
Heptachlor
ug/L
0.25
0.19
77
34-135
Heptachlor epoxide
ug/L
0.25
0.24
97
39-142
Decachlorobiphenyl (S)
%
245
10-184 SO
Tetrachloro-m-xylene (S)
%
154
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103048
3103049
MS MSD
92511537003
Spike Spike
MS
MSD
MS MSD
% Rec
Max
Parameter Units
Result
Cone. Cone.
Result
Result
%Rec %Rec
Limits
RPD RPD Qual
PCB-1016 (Aroclor 1016) ug/L
NO
5
5 4.7
5.0
93 100
50-140
7 36
PCB-1260 (Aroclor 1260) ug/L
NO
5
5 5.2
5.6
104 112
42-140
7 38
Decachlorobiphenyl (S) %
184 179
10-184
Tetrachloro-m-xylene (S) %
129 125
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103080
3103081
MS
MSD
92511537003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rae
% Rae
Limits RPD
RPD Qual
4,4'-DDD
ug/L
NO
0.25
0.25
0.40
0.37
159
146
36-141
9
39 M1
4,4'-DDE
ug/L
ND
0.25
0.25
0.37
0.37
146
147
31-145
1
35 M1
4,4'-DDT
ug/L
ND
0.25
0.25
0.36
0.36
145
143
25-160
1
42
Aldrin
ug/L
ND
0.25
0.25
0.21
0.26
86
105
42-140
21
35
alpha-BHC
ug/L
NO
0.25
0.25
0.29
0.30
117
120
37-140
3
36
alpha -Chlordane
ug/L
NO
0.25
0.25
0.34
0.34
136
135
45-140
1
35
beta-BHC
ug/L
NO
0.25
0.25
0.42
0.43
167
172
30-147
3
44 M1
delta-BHC
ug/L
NO
0.25
0.25
0.37
0.38
147
153
32-140
4
52 M1
Dieldrin
ug/L
NO
0.25
0.25
0.35
0.31
138
123
36-146
11
49
Endosulfan I
ug/L
NO
0.25
0.25
0.33
0.35
133
138
45-153
3
28
Results presented on this page are In the units Indicated
by the
"Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, -LC. Page 27 of 41

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103080
3103081
MS
MSD
92511537003
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rao
Limits
RPD
RPD Qual
Endosulfan II
ug/L
ND
0.25
0.25
0.39
0.38
155
151
27-176
3
53
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.39
0.38
157
154
31-144
2
38 M1
Enddn
ug/L
ND
0.25
0.25
0.37
0.36
147
143
30-147
3
48
Endrin aldehyde
ug/L
ND
0.25
0.25
0.32
0.33
127
130
16-177
3
30
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.33
0.34
130
137
32-140
5
39
gamma -Chlordane
ug/L
ND
0.25
0.25
0.40
0.39.
161
155
45-140
4
35 M1
Heptachlor
ug/L
ND
0.25
0.25
0.26
0.31
102
122
34-140
17
43
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.32
0.30
130
121
37-142
7
26
Dfumchlorobiphenyl (S)
%
232
289
10-184
SO
Tetrachloro-m-xylene (S)
%
127
222
10-154
SO
Results presented on this page are In the units Indicated by the 'V nits" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 41

(�IaceAnalyfical'
www.pacelabsxea
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587125
QC Batch Method: EPA 625.1
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3103116
Associated Lab Samples: 92511537003, 92511537004
QUALITY CONTROL DATA
Analysis Method: EPA 625.1
Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Matrix: Water
Parameter
Units
Blank
Result
1,2,4-Trichlorobenzene
ug/L
NO
2,2'-Oxybis(1-chloropropane)
ug/L
NO
2,4,6-Trichlorophenol
ug/L
ND
2,4-Dichlorophenol
ug/L
ND
2,4-Dimethylphenol
ug/L
ND
2,4-Dinitrophenol
ug/L
ND
2,4-Dinitrotoluene
ug/L
ND
2,6-Dinitrotoluene
ug/L
NO
2-Chloronaphthalene
ug/L
NO
2-Chlorophenol
ug/L
NO
2-Nitrophenol
ug/L
NO
3,3'-Dichlorobenzidine
ug/L
ND
4,6-Dinitro-2-methylphenol
ug/L
ND
4-Bromophenylphenyl ether
ug/L
ND
4-Chloro-3-methylphenol
ug/L
ND
4-Chlorophenylphenyl ether
ug/L
ND
4-Nitrophenol
ug/L
ND
Acenaphthene
ug/L
ND
Acenaphthylene
ug/L
NO
Anthracene
ug/L
NO
Benzo(a)anthracene
ug/L
NO
Benzo(a)pyrene
ug/L
NO
Benzo(b)fluoranthene
ug/L
NO
Benzo(g,h,i)perylene
ug/L
NO
Benzo(k)fluoranthene
ug/L
NO
bis(2-Chloroethoxy)methane
ug/L
NO
bis(2-Chloroethyl) ether
ug/L
NO
bis(2-Ethylhexyl)phthalate
ug/L
NO
Butylbenzylphthalate
ug/L
ND
Chrysene
ug/L
ND
Di-n-butylphthalate
ug/L
ND
Di-n-octylphthalate
ug/L
ND
Dibenz(a,h)anthracene
ug/L
ND
Diethylphthalate
ug/L
ND
Dimethylphthalate
ug/L
ND
Fluoranthene
ug/L
ND
Fluorene
ug/L
ND
Hexachloro-1,3-butadiene
ug/L
ND
Hexachlorobenzene
ug/L
ND
Hexachlorocyclopentadiene
ug/L
ND
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Reporting
Limit
MDL
Analyzed Qualifiers
5.0
1.7
12116/2010:45
5.0
1.2
12/1612010:45
10.0
1.6
12116/2010:45
5.0
1.4
12116/2010:45
10.0
1.7
12/1612010:45
50.0
26.0
12/1612010:45
5.0
1.6
12/16/20 10:45
5.0
1.7
12/16/20 10:45
5.0
1.7
12116/2010:45
5.0
1.2
12116/2010:45
5.0
1.4
12/16/20 10:45
10.0
8.1
12116/2010:45
10.0
3.4
12/16/20 10:45
5.0
1.8
12/16/20 10:45
5.0
3.3
12/16/20 10:45
5.0
2.0
12116/2010:45
10.0
6.6
12/1612010:45
5.0
2.0
12116/2010:45
5.0
2.0
12116/2010:45
5.0
2.3
12116/2010:45
5.0
2.7
12116/2010:45
5.0
2.8
12/16/20 10:45
5.0
2.6
12116/2010:45
5.0
2.8
12/16/20 10:45
5.0
2.7
12/16/20 10:45
10.0
1.8
12/16/20 10:45
5.0
1.9
12/1612010:45
5.0
3.7
12/16/20 10:45
5.0
3.1
12/16/20 10:45
5.0
2.8
12/1612010:45
5.0
2.2
12/1612010:45
5.0
3.9
12/1612010:45
5.0
3.0
12/1612010:45
5.0
2.0
12/16/20 10:45
5.0
2.1
12/16/20 10:45
5.0
2.2
12/16/20 10:45
5.0
2.1
12/16/20 10:45
5.0
1.8
12/16/20 10:45
5.0
2.2
12116/2010:45
10.0
1.6
12116/2010:45
Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 41

aceAnalytical
trww.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resisto8ex
Pace Project No.: 92511537
METHOD BLANK: 3103116
Matrix:
Water
Associated Lab Samples: 92511537003, 92511537004
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Hexachloroethane
ug/L
ND
5.0
1.4
12/16/20 10:45
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
2.9
12/16/20 10:45
Isophorone
ug/L
ND
10.0
1.7
12/16/20 10:45
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
1.3
12/16/20 10:45
N-Nitrosodimethylamine
ug/L
NO
5.0
1.9
12/16/20 10:45
N-Nilrosodiphenylamine
ug/L
NO
10.0
3.0
1211612010:45
Naphthalene
ug/L
NO
5.0
2.1
12116/2010:45
Nitrobenzene
ug/L
ND
5.0
1.9
12116/2010:45
Pentachlorophenol
ug/L.
ND
10.0
3.8
12/16/20 10:45
Phenanthrene
ug/L .
ND
5.0
2.0
12/1612010:45
Phenol
ug/L
NO
5.0
1.4
12/16/20 10:45
Pyrene
ug/L
NO
5.0
2.2
12/16/20 10:45
2,4,6-Tribromophenol (S)
%
107
10-137
12/16/20 10:45
2-Fluorobiphenyl (S)
e/
74
15-120
12/16/20 10:45
2-Fluorophenol (S)
%
63
10-120
12/16/20 10:45
Nitrobenzene-d5 (S)
%
109
10-120
12/16/20 10:45
Phenol-d6 (S)
%
56
10-120
12/16/20 10:45
Terphenyl-d14 (S)
%
125
11-131
12/16/20 10:45
LABORATORY CONTROL SAMPLE:
3103117
Spike
1-CS LCS
%Rec
Parameter
Units
Conc.
Result %Rec
Limits Qualifiers
1,2,4-Trichlorobenzene -
ug/L
50
24.9
50
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
35.9
72
36-166
2,4,6-Trichlorophenol
ug/L
50
44.6
89
37-144
2,4-Dichlorophenol
ug/L
50
41.0
82
1-191
2,4-Dimethylphenol
ug/L
50
41.3
83
32-119
2,4-Dinitrophenol
ug/L
250
282
113
1-181
2,4-Dinitrotoluene
ug/L
50
38.3
77
39-139
2,6-Dinitrotoluene
ug/L
50
46.5
93
50-158
2-Chloronaphthalene
ug/L
50
34.4
69
60-118
2-Chlorophenol
ug/L
50
38.8
78
23-134
2-Nitrophenol
ug/L
50
45.0
90
29-182
3,3'-Dichlorobenzidine
ug/L
100
88.5
89
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
143
143
1-181
4-Bromophenylphenyl ether
ug/L
50
42.5
85
53-127
4-Chloro-3-methylphenol
ug/L
100
94.3
94
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.2
76
25-158
4-Nitrophenol
ug/L
250
202
81
1-132
Acenaphthene
ug/L
50
36.6
73
47-145
Acenaphthylene
ug/L
50
36.8
74
33-145
Anthracene
ug/L
50
36.5
73
1-166
Benzo(a)anthracene
ug/L
50
41.2
82
33-143
Benzo(a)pyrene
ug/L
50
41.4
83
17-163
Results presented on this page are in the units Indicated by the "Units"
column except where an alternate
unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C. Page 30 of 41

aceAnalytical
tytem.pecelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
3103117
Spike LIDS
LCS
% Rec
Parameter
Units
Conic. Result
% Rec
Limits Qualifiers
Benzo(b)fluoranthene
ug/L
50
40.9
82
24-159
Benzo(g,h,i)perylene
ug/L
50
44.2
88
1-219
Benzo(k)fluoranthene
ug/L
50
40.8
82
11-162
bis(2-Chloroethoxy)methane
ug/L
50
39.8
80
33-184
bis(2-Chlorcethyl) ether
ug/L
50
36.4
73
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
49.3
99
8-158
Butylbenzylphthalate
ug/L
50
50.3
101
1-152
Chrysene
ug/L
50
40.6
81
17-168
Di-n-butylphthalate
ug/L
50
44.4
89
1-118
Di-n-octylphthalate
ug/L
50
54.5
109
4-146
Dibenz(a,h)anthracene
ug/L
50
45.4
91
1-227
Diethylphthalate
ug/L
50
41.1
82
1-114
Dimethylphthalate
ug/L
50
39.4
79
1-112
Fluoranthene
ug/L
50
42.1
84
26-137
Fluorene
ug/L
50
38.6
77
59-121
Hexachloro-1,3-butadiene
ug/L
50
20.9
42
24-116
Hexachlorobenzene
ug/L
50
38.2
76
1-152
Hexachlorocyclopentadiene
ug/L
50
25.5
51
25-150
Hexachloroethane
ug/L
50
21.4
43
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
45.6
91
1-171
Isophorone
ug/L
50
34.8
70
21-196
N-Nitroso-di-n-propylamine
ug/L
50
35.9
72
1-230
N-Nitrosodimethylamine
ug/L
50
45.8
92
25-150
N-Nitrosodiphenylamine
ug/L
50
40.6
81
25-150
Naphthalene
ug/L
50
28.9
58
21-133
Nitrobenzene
ug/L
50
36.8
74
35-180
Pentachlorophenol
ug/L
100
95.4
95
14-176
Phenanthrene
ug/L
50
40.7
81
54-120
Phenol
ug/L
50
32.5
65
5-112
Pyrene
ug/L
50
40.4
81
52-115
2,4,6-Tribromophenol(S)
%
110
10-137
2-Fluorobiphenyl (S)
%
67
15-120
2-Fluorophenol (S)
%
67
10-120
Nitrobenzene-d5(S)
%
79
10-120
Phenol-d6 (S)
%
58
10-120
Terphenyl-d14 (S)
%
93
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118
3103119
MS MSD
92511577001
Spike Spike
MS
MSD
MS MSD
% Rec Max
Parameter Units
Result
Conc. Conc.
Result
Result
%Rec %Rec
Limits RPD RPD Qual
1,2,4-Trichlorobenzene ug/L
NO
50 50
18.7
16.5
37 33
44-142 12 30 Mt
2,2'-Oxybis(1- ug/L
NO
50 50
46.8
42.8
94 86
36-166 9 30
chloropropane)
2,4,6-Trichlorophenol ug/L
NO
50 50
54.2
33.7
108 67
37-144 47 30 R1
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 41

aceAnalytical
lassiPetelabs.aara
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118 3103119
Parameter
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,3'-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-
Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethyl hexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentad iene
Hexachloroethene
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosod im ethylamine
N-Nitrosod iphenylamine
Naphthalene
Nitrobenzene
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MS
MSD
92511577001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Units
Result
Cono.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Dual
ug/L
NO
50
50
48.7
42.5
97
85
1.-191
14
30
ug/L
ND
50
50
47.7
38.2
95
76
32-119
22
30
ug/L
ND
250
250
77.6
NO
31
7
1-181
30
ug/L
NO
50
50
44.1
39.1
88
78
39-139
12
30
ug/L
NO
50
50
59.9
56.1
120
112
50-158
7
30
ug/L
ND
50
50
33.3
30.2
67
60
60-118
10
30
ug/L
ND
50
50
46.0
40.7
92
81
23-134
12
30
ug/L
ND
50
50
54.1
48.5
108
97
29-182
11
30.
ug/L
NO
100
100
108.
108
108
108
1-262
0
30
ug/L
NO
100
100
141
38.3
141
38
1-181
115
30 Rl
ug/L
NO
50
50
47.0
43.9
94
88
53-127
7
30
ug/L
NO
100
100
113
105
113
105
22-147
7
30
ug/L
NO
50
50
40.2
36.5
80
73
25-158
10
30
ug/L
NO
250
250
146
35.8
58
14
1-132
121
30 R1
ug/L
NO
50
50
39.5
34.7
79
69
47-145
13
30
ug/L
ND
50
50
41.0
36.7
82
73
33-145
11
30
ug/L
NO
50
50
44.0
41.5
88
83
1-166
6
30
ug/L
ND
50
50
52.0
51.3
104
103
33-143
2
30
ug/L
ND
50
50
53.5
52.2
107
104
17-163
3
30
ug/L
ND
50
50
52.2
51.7
104
103
24-159
1
30
ug/L
ND
50
50
55.2
55.3
110
111
1-219
0
30
ug/L
NO
50
50
53.1
52.5
106
105
11-162
1
30
ug/L
NO
50
50
48.5
46.6
97
93
33-184
4
30
ug/L
NO
50
50
48.3
44.8
97
90
12-158
8
30
ug/L
NO
50
50
59.6
59.6
119
119
8-158
0
30
ug/L
NO
50
50
62.0
60.8
124
122
1-152
2
30
ug/L
ND
50
50
51.2
50.3
102
101
17-168
2
30
ug/L
NO
50
50
56.3
54.8
113
110
1-118
3
30
ug/L
NO
50
50
65.4
64.9
131
130
4-146
1
30
ug/L
NO
50
50
56.9
57.1
114
114
1-227
0
30
ug/L
NO
50
50
52.5
50.1
105
100
1-114
5
30
ug/L
ND
50
50
50.0
46.5
100
93
1-112
7
30
ug/L
ND
50
50
53.3
51.2
107
102
26-137
4
30
ug/L
ND
50
50
44.1
39.6
88
79
59-121
11
30
ug/L
ND
50
50
4.9.1
4.0.1
10
8
24-116
30 M1
ug/L
NO
50
50
43.8
41.1
88
82
1-152
6
30
ug/L
NO
50
50
8.6.1
7.1J
17
14
25-150
30 Ml
ug/L
NO
50
50
6.9
5.4
14
11
40-113
24
30 Ml
ug/L
NO
50
50
57.4
56.9
115
114
1-171
1
30
ug/L
ND
50
50
43.2
40.9
86
82
21-196
5
30
ug/L
ND
50
50
44.4
42.6
89
85
1-230
4
30
ug/L
ND
50
50
48.1
46.1
96
92
25-150
4
30
ug/L
ND
50
50
50.5
46.9
101
94
25-150
7
30
ug/L
ND
50
50
31.3
28.4
63
57
21-133
10
30
ug/L
ND
50
50
46.3
43.8
93
88
35-180
6
30
Results presented on this page are In the units Indicated by Me'Vnits" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C. Page 32 of 41

aceAnalytical
tyww.pacelabs.com
QUALITY CONTROL DATA
Project: Crane Resisto6ex
Pace Project No.: 92511537
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 3103118
3103119
MS
MSD
92511577001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rao
Limits
RPD
RPD Qual
Pentachlorophenol
ug/L
ND
100
100
122
49.3
122
49
14-176
85
30 R1
Phenanthrene
ug/L
ND
50
50
48.7
45.7
97
91
54-120
7
30
Phenol
ug/L
ND
50
50
33.8
31.0
68
62
5-112
9
30
Pyrene
ug/L
ND
50
50
49.3
48.7
99
97
52-115
1
30
2,4,6-Tribromophenol (S)
%
136
109
10-137
2-Fluorobiphenyl(S)
%
53
50
15-120
2-Fluorophenol (S)
%
65
53
10-120
Nitrobenzene-d5(S)
%
90
89
10-120
Phenol-d6 (S)
%
55
55
10-120
Terphenyl-d14 (S)
%
115
115
11-131
Results presentee on this page are In the units Indicated by the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/202112:50 PM without the written consent of Pace Analytical Services, I.I.C.
Page 33 of 41

aceAnalj6cal
wancilacslabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistofiex
Pace Project No.:
92511537
QC Batch:
587549
Analysis Method: SM 254OD-2011
QC Batch Method:
SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537001, 92511537002
METHOD BLANK: 3105210 Matrix: Water
Associated Lab Samples: 92511537001, 92511537002
Parameter
Total Suspended Solids
Blank Reporting
Units Result Limit MDL Analyzed Qualifiers
mg/L NO 2.5 2.5 12/16/2022:28
LABORATORY CONTROL SAMPLE: 3105211
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 254 102 90-110
SAMPLE DUPLICATE: 3105691
92511268001 Dup. Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 348 388 11 25
SAMPLE DUPLICATE: 3105692
92511502001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 659 595 10 25
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 41

aceAnalytical e
W .hacllabs.COR
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistoflex
Pace Project No.:
92511537
OC Batch:
587535
Analysis Method: EPA 420.4 Rev 1.0 1993
OC Batch Method:
EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3105108
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Phenol mg/L
LABORATORY CONTROL SAMPLE: 3105109
Parameter Units
Phenol mg/L
Matrix: Water
Blank
Result
ND
Spike
Conic.
0.05
Reporting
Limit MDL Analyzed Qualifiers
0.020 0.0076 12/17/2014:45
LCS LCS % Rec
Result e/ Rec Limits Qualifiers
0.047 93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105110
3105111
MS
MSD
35596343001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result Conc.
Conic.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Phenol mg/L 0.0076U 0.05
0.05
0.055
0.040
97
67
90-110
32
10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105125
3105126
MS
MSD
92511148001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Phenol mg/L ND 0.05
0.05
0.050
0.044
96
85
90-110
12
10 M1,R1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C.
Page 35 of 41

aceAnalytical®
www.pecelabs.com
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistofiex
Pace Project No.: 92511537
QC Batch: 586885 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3102109 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L NO 0.0080 0.0060 12115/2023:30
LABORATORY CONTROL SAMPLE:
3102110
Spike
LCS
LCS
%Rec
Parameter
Units
Cone.
Result
%Red
Limits Qualifiers
Cyanide
mg/L
0.1
0.10
100
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102144
3102145
MS
MSD
92511537003
Spike
Spike MS
MSD
MS MSD % Rec
Max
Parameter Units
Result
Cone.
Cone. Result
Result..
%Rec %Rec Limits
RPD RPD Qual
Cyanide mg/L
NO
0.1
0.1 0.020
0.064
19 64 80-120
105 10. M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102146 3102147
MS MSD
92511537004 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual
Cyanide mg/L NO 0.1 0.1 0.091 0.084 91 84 80-120 7 10
Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, I.I.C.
Page 36 of 41

IMAnalyfical'
www.paeelahs.cam
QUALIFIERS
Project: Crane Resistoflex
Pace Project No.: 92511537
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL -Adjusted Method Detection Limit.
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
POL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
so Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 41

ac"Analytical
tvww.pacelibe.con
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resisto0ex
Pace Project No.:
92511537
Analytical
Lab ID
Sample ID
OC Batch Method
OC Batch
Analytical Method
Batch
92511537001
OF-001
EPA 1664B
588138
92511537002
OF-002
EPA 1664B
588138
92511537003
OF-001 TTO
EPA 608.3
587108
EPA 608.3
587726
92511537004
OF-002 TTO
EPA 608.3
587108
EPA608.3
587726
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
590708
EPA 200.7 Rev 4.4 1994
590740
92511537003
OF-001 TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537004
OF-002 TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537001
OF-001.
EPA 200.7 Rev 4.41994
586977
EPA 200.7 Rev 4.41994
587006
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
590706
EPA 200.7 Rev 4.4 1994
590776
92511537003
OF-001. TTO
EPA 245.1 Rev 3.0 1994
587409
EPA 245.1 Rev 3.0 1994
587457
92511537004
OF-002 TTO
EPA245.1 Rev 3.01994
587409
EPA 245.1 Rev 3.01994
587457
92511537003
OF-001 TTO
EPA 625.1
587125
EPA 625.1
587394
92511537004
OF-002 TTO
EPA 625.1
587125
EPA 625.1
587394
92511537003
OF-001 TTO
EPA624.1
587031
92511537004
OF-002 TTO
EPA624.1
587031
92511537001
OF-001
SM 254OD-2011
587549
92511537002
OF-002
SM 254OD-2011
587549
92511537003
OF-001 TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4 Rev 1.0 1993
587822
92511537004
OF-002 TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4 Rev 1.0 1993
587822
92511537003
OF-001 TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
92511537004
OF-002 TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, -LC. Page 38 of 41

Laboratory receiving samples:
Asheville, Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Client Name:
Project #:
Courier; ❑Fed Ex Ljups I❑USPS .Client
❑ Commercial ❑Pace ❑Other:_
Custody Seal Present? Dyes )ZNo
Packing Material: ❑Bubble Wrap
Seals Intact? []Yes ❑No
0ubble Bags ❑None ❑ Other
Thermomet r: � ,./
IRGun ID: C' r Type of ice: / �Iwet ❑Blue
jj Correction Factor:
Cooler Temp: �' rl' Add/Subtract (°C�),tn
Cooler Temp Corrected (`C): 5 , a 1
USDA Regulated Sail (Q N/A, water sample
les Did samporiginate ilia quarantine zone within the United States: CA, NY, or SC (check maps)?
WO#:92511537
92511537
Date/Initials Person Examining Contents: r Z "la lif C)
Biological Tissue frozen?
[-]Yes❑No ON/A
❑None
Temp should be above freezing to6°C
❑samples out of Temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
....n.a,..,u�.u,n end m,nnn Rirnl] my. V IlNo
Comments/Discrepant
Chain of Custody Present?
liyas
No
❑N/A
1.
Samples Arrived within Hold Time?
0Yes
❑No
❑N/A
2.
Short Hold Time Analysis(<72 hr.)?
Dyes
No
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
No
❑N/A
4.
.Sufficient Volume?
i Yes
❑No
❑N/A
5.
Correct Containers Used?
Pace Containers Used?
(res
es
❑No
ONO
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No.
N/A
7.
Dissolved analysis: Samples Field Flltered?
yes
EIN.
❑N/A
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
,]yes
L(-
❑No
❑N/A
9.
Headspace in VDA Vials (>5-6mm)?
❑Yes
No
❑NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Dyes
Dyes
No
❑No
❑N/A
N/A
11.
►I
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spilt containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Field Data Required? [-]Yes ONO
Protect Manager SCURF Review: ;r�— Date;
Project Manager SRF Review; Date: / I -
Page 39 of 41

Document Name:
Document No.:
*Check mark top half of box if pH and/or dechlorination is Project N
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, D8O/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
2 of
PM: UP Due Date: 12/21/20
CLIENT: 93-ALTAMONT
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PH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
PH upon receipt
Date preservation adjusted
Timepreservatfon
Amount of Preservative
Lot B
adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this torm will us sent to the Nonn Laraine uehivc t,emocaumi �111Lv ..v.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 40 of 41

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MATRI%CODE Ilea valid wd., to leh)
ID
SAMPLE TYPE (G=GRAB CaGONIP)
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Pr
SAMPLE TEMP AT COUECTIDN
p
AZ
N OF CONTAINERS
Unpreservetl
02
K
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H2SO4
m r'y
n
0
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HNO3
-D
#
3
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pfle5'
}
u
HCIAC
m
7m7
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a
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9
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m
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Malhsn"
i
m
Other
Analyses Test
YIN
a
f
y
Tell
3
x
Metals ICU, Pb, Zn)
inz°
m
Dissolved Melels - Geld filler
N
TPH Oiland Grease
en
NX
TTO Molals
x
TTO-Cyanide
r
g
TTO- Phenol
TTO-VOCs
0
TTO-SVOCs
Q
if
m
x
TTO.Peslicides
i
N
TEMP in C
a
p
m
Residual Chlorine (YIN)
S
c
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y
(YIN)
a
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Page 41 of 41