NCG030499_DMR_20210201

Anchor QEA of North Carolina, PLLC ANCHOR
231 Haywood Streetkz Asheville, North Carolina 28801 QEAi
828.281.3350
January 21, 2021
Attn: DEMLR Stormwater
Asheville Regional Office
Division of Energy, Mineral, and Land Resources
North Carolina Department of Environmental Quality
2090 U.S. 70 Highway Swannanoa, North Carolina 28778-8211
Re: Stormwater Sample Analytical Results, Period 2 2020
Crane Resistoflex
Marion, North Carolina
General Permit No. NCG030499
To Whom It May Concern,
Anchor QEA of North Carolina, PLLC (Anchor QEA), is pleased to present the following stormwater
sample analytical results. On behalf of Crane Resistoflex, Anchor QEA collected two stormwater
samples on December 14, 2020, for the referenced facility covered by National Pollutant Discharge
Elimination System Stormwater General Permit No. NCG030000 (Stormwater General Permit). This
sampling event fulfills the compliance sampling requirement for Period 2 of 2020.
In the samples collected from sampling locations OF-001 and OF-002, all constituent concentrations
detected were below or within the acceptable ranges of the benchmark values specified in the
general permit. This letter provides background information and describes the methods, findings,
and conclusions regarding the stormwater sample collection and analysis.
Background
The most recent Stormwater General Permit for metal fabrication activities was issued by the North
Carolina Department of Environmental Quality with an effective date of November 1, 2018, and it will
expire at midnight on May 31, 2021. Sample collection and reporting protocol for this event followed
the current permit requirements.
The Stormwater General Permit indicates that the permittee shall complete analytical sampling on
a semiannual schedule, once during the first half of the year (January 1 to June 30; Period 1) and
once during the second half of the year (July 1 to December 31; Period 2), at a minimum, allowing
at least 60 days between sample collection dates.
The general location of the facility is indicated in Figure 1. The facility's two permitted outfalls and
sample locations are labeled OF-001 and OF-002, as identified in Figure 2.
Stormwater Sample Analytical Results, Period 2 2020.doa
Received AL
u
FEB -1 2 2f
L a
�11d Quality 5ecgaliIII �;
Alsh®vme ^ `,

January 21, 2021
Page 3
If you would like additional information, please contact me at [phone], or contact Victoria
Boyer at [phone].
Sincerely,
Robert Cork PE, MEng
Managing Engineer
cc: Victoria Boyer, Crane Resistoflex
Duplicate, Central Files
Attachments
Figure 1 Site Location Map
Figure 2 Stormwater Discharge Outfall Locations
Attachment 1 Surface Water Sampling Logs
Attachment 2 Equipment Documentation and Instrument Calibration Data Sheet
Attachment 3 Stormwater Discharge Outfall Qualitative Monitoring Reports
Attachment 4 Semiannual Stormwater Discharge Monitoring Report
Attachment 5 Laboratory Analytical Report and Chain -of -Custody Form

Site Parcel ?
Boundary
eM
S
t
t 4l f1�(it1 r.' t s 0 10
LEGEND: NOTES:
1. Basemap from Esri Online Services
Q Site Parcel Boundary 2. Site parcel boundary from
McDowell County GIS
0 Z000
Feet
Publish Date 2021/01/12, 9:01 PM I User. cpatterseii
Filepath:QVobz\cane Reziztoflex_20G].\Maps\AQ_Fig01_SileLocalionMap.m xd
k zj� ANCHOR Figure 1
QEA Site Location Map
Stormwater Sample Analytical Results
Crane Resistoflex, Marion, North Carolina

Attachment 1
Surface Water Sampling Logs

ANCHOR
QEAu
Surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 1-loywood Street
Asheville, North Carolina 28001
Puler Name
crone �l es/r.!'9UPP. �'
Date /2/ /4/20-.0
Project Number
G9-2o6)—QI-OI
weather S `Fy Rahalr
Sam -jig Personnel
C.. PL f-kri-on
Facility Permit fl, NGGlo.3U/%7"'!
Sample Name
OF- 002
Comments
Ath !i'}.ailn)1xmleJ.
Sample Method: raU Syringe
Pump
Bailer-Disp. Other.
i Oxidation j
Dissolved Specific Cond.
I!.. pH (S.U.)
ReductionI Turbidity
Time Temp ('C)
Oxygen (mg/L) , (PS/cm)
report to 0.1 S.U.
1 Potential (mV) (NTIJ) Comments
0725
GRP
Qp
GAP
i
Sampling Container
Number of Containers
Requested Analysis
I00 n Rnler /-L Aviv
/
T7V - SVOG.r f TTU - Feri%c.'de-
2>0 mL Plastic
J
MG fA-/S (C'wr Ps, Za) 1D;j:m/r,d %le)Vr1 %T0 - Mo A/J
125 mL Plastic
!TTU-(f yanlse
-
aO mL Glass
3
'.. 7-10 - VOe.a'
1 LGlass w�fiCL
TPH Od f Greare.
Other.
-rss Z %%O- A )
Vegewvon_ Goo d Access: F /r; mt-t4-oce�dPe- &2 e
Sampling Personnel Signature: / - /Y Date: 1,Z/ / 4/20 20
Ames
Samplesare analyzed immediately upon collection
`G degrees Celsius
ps/cm rejcro-Sremen per cubic centimeter
my/L rnMigrams per liter
r,Y M,11,I1
r47U nephEometnc turbidity units
5 U standard units
Method Reterence.
Temperature SM 2550 B-2010
Specific conductivity EPA Method 1201. Rev 1992
DO SM 4500 0 G-2011
pH- SM 4500-H' B 2011
Page 1 of 1

ANCHOR
tiquipment uOCUnlentation ana Instrument Caiinration UOta ]neat
Andhol QEA of Noah Carel:na. PLLC
231Haywood Street
Asheville North Carolina 28801
CALIBRATION DOCUMENTATION uu
r lr_ , Lii (IL.Q 4�-tsi5hz(lt. X,. PelsOn(mldutluig Calibration C. P0.4/C/YO/!
l.qq-2©62 -01- 0/ 1d Pate of Cirb ahnn fit}/ y020
t T Agirtr, bli)r /VC DMOM flNtf 21 0
( r rvC0o3��99 I
- saT, u,s ego- enl <, mctei i>Hf to take me"u"I"emts
L. Equipment Type I Brand Serial Number I Date of Use. Rental Campan
Select Turbidimtten.. I43iII0DQl1 1) 1510D6045207) '
Hf S:Icnhll, Mlrl0111W (sh12006010-15)
Instrument Reading
(Hach 210DCB
Instrument Reading
(HP Scientific MicmTPW)
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Calibration Lai No. 81
Expiration Date:
Ca!
Cal
Cal
Cal
Cal:
Cal
Tate
Time
Time.
Ti
Time
Time
Calibration
Verification,
' Pre -Analysis
Check (10 NTU):
Mein
Time
-Pre-Analysis
Check (10 NTU):
Meas
Time
'Post -Analysis
Check (10 U):
M
Time
t-Anal sis
Check (10 NTU):
Meas
Time. G.tp
YSI Prafessional Plus Multipammeter Meter (s/n 181tiVIHM)
Instrument Readings
Calibration Lot No.
& Expiration Date
Diu lved Oxygen L%
saturation)
:r t al f
Cal I .
mmHg
Temperature ('C)
Time CAP
DO (Site u2,
In Ilal 1°1)
Cal (5b).
mmHo
1,awuatu, ra
rme'. CA
if ao fitable)•
pH 7 s.u.
¢pettrsCls.0
6,as
pHmV
—16'3
Cal -clpiimV
Time -
0— --
CJ5/22
pte;, l s.u.
In-!ia5. -l.0
pHmV / q-7' 1
Cal'. U, 0
PHmV:
Tim0-� 7
0�/��
PH To S.U.
rapc:n tov liu
'n¢/ Q 0 9
/
pH-V�
Cal/ o- 0 /
pHmV
Time 5"
rV17 V
0 -7/-2'
QC— pH 7 S.U.
pciI)C150
AM Time
0552
Meas-
7,02
Mid Day Time
0-740
Check
6 99
PM Time.
Check
d5/22
Spec Conti
Initial
Cal
Time
P
ps/cm
CA
QC--:
AM Time
Meas
Mid Day Time
Check
PM Time
Check.
pS/cm
`
% Recovery=
im!ial
Cal.
yule `C
Time
___
Signature: Date:
= - ,�rUan�e 116C n'am�hr.lure:SOpera4Jn nianu3l
ld t �. 'aced zrmAmp tJ value'_ rcG�ezenlatve o(hrsmnc range
e'-la aas IY -yea r1a0. ),,,r.,mr pl17 p114 pH 10 DO OPP OCehe; is
E '1. i DS e -oVa ' �h P,..Ipa 1,(. rryer,l/IpplL l 16:LOnS) I Ile DO tile muSl lie Cafliraleh al PMp 5tn111C5tC
f '' Y Pirtle 1 p`wr tO anaV9S
a-9 SP r...dvorony 10. L 01 the true value if QC 1"3d IT's -IC wil of mnne the nsin menl needs In be mcahbrated
0! Cc plrl> c l a l0 S=m;, 1 1 t f '..e"uf c iplelurn of wrnpl in at a n, rrni m
I I ..C.- T'ee l /cr'i r lbG
425'OaF91U1(c,dr•-nt,FPAMah,J)(0)IDOSIT 4.OD 06201 f I PH SM 4SOO H, a 201111 rb.dity 5112130 82017
Page 1 of 1

NCO
Environm
ental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out thisform, please visit httl)s://deq.ne.gov/about/divisions/enerev-mineral-land-
resources/energv-mineral-I and-permits/stormwater-perm its/nodes-industrial-sw#tab-4
PermitNo.: N/C/0/3/0/0/0/0/0/ or Certificate of Coverage No.: N/C/G/0/3/0/4/9/9/
Facility Name: Crane Resistoflex
County: McDowell
No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection:
06:50
Total Event Precipitation (inches): 135
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event' is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. OF-001
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 07/28/2017

7
Gnvironmentul
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfrlling out thisform, please visit htti)s:Hdeci.nc.eov/about/divisions/enerev-mineral-land-
resources/enerev-m i neral-land-permits/stormwater-roerinits/nodes-industrial-sw#tab-4
Permit No.: N/C/ 0 / 3 / 0 / 0 /0 / 0 /0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 /0 / 4 / 9 / 9 /
Facility Name: Crane Resistoflex
County: McDowell
Phone No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection: 07:25
Total Event Precipitation (inches): 1.35
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. OF-002
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.): Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
swill-242, Last modified 07/28/2017

Attachment4
Semiannual Stormwater Discharge
Monitoring Report

Attachment 5
Laboratory Analytical Report and
Chain -of -Custody Form

aceAnalgical e
wwe.pacehhs.com
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #:40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 41

aceAnalj6cal
w .Pscelabsxom
SAMPLE ANALYTE COUNT
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92511537001
OF-001
EPA1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
4.
PASI-A
EPA 200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
92511537002
OF-002
EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
4
PASI-A
EPA 200.7 Rev 4.41994
SH1
1
PASI-A
SM 2540D-2011
RED
1
PASI-A
92511537003
OF-001 TTO
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.41994
DS
12
PASI-A
EPA 245.1 Rev 3.0. 1994
S00
1
PASI-A
EPA 625.1.
PKS
58
PASI-C
EPA 624.1
SAS
35
PASI-C
EPA 420.4 Rev 1.0 1993
JKG
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92511537004
OF-002 TTO
EPA608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.41994
DS
12
PASI-A
EPA 245.1 Rev 3.01994
SOO
1
PASI-A
EPA 625.1
PKS
58
.PASI-C
EPA 624.1
SAS
35
PASI-C
EPA 420.4 Rev 1.0 1993
JKG
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 41

ac"Analytical
www.pacelebs.caa
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 Lab ID: 92511537001 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons ND mg/L 5.0 5.0 1 12/18/20 11:08
200.7 MET ICP
Copper
Lead
Hardness, Total(SM 2340B)
Zinc
200.7 MET ICP, Dissolved
Zinc, Dissolved
2540D Total Suspended Solids
Total Suspended Solids
Date: 01/11/2021 12:50 PM
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
ND ug/L
5.0
4.3
1
12/17/20 02:09
12/19/20 00:20 7440-50-8
ND ug/L
5.0
4.5
1
12/17/20 02:09
12/19/20 00:20 7439-92-1
1700 ug/L
662
131
1
12/17/20 02:09
12/19/20 00:20
35.5 ug/L
10.0
9.5
1
12/17/20 02:09
12/19/20 00:20 7440-66-6
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services
-Asheville
32.5 ug/L
10.0
2.5
1
12/15/2009:43
12/1612021:47 7440-66-6
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
7.6. mg/L 2.5 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
12/16/20 22:42
M1,R1
Page 6 of 41

aceAnalj6cal
www.paeelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected: 12/14/20 06:55 Received: 12114/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services - Charlotte
Aldrin
ND
ug/L
0.050
0.022
1
12/15/20 14:51
12/17/20 19:39
309-00-2
alpha-BHC
ND
ug/L
0.050
0.019
1
12115/2014:51
12117/2019:39
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
12/15/20 14:51
12/17/20 19:39
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12/15/20 14:51
12/1712019:39
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
12/15/20 14:51
12/1712019:39
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.14
1
12/15/20 14:51
12/1712019:39
57-74-9
alpha -Chlordane
ND
ug/L
0.050
0.0090
1
12/15/20 14:51
121171201939
5103-71-9
gamma -Chlordane
ND.
ug/L
0.050
0.017
1
12115/2014:51
1211712019:39
5103-74-2
4,4'-DDD
ND
ug/L
0.050
0.0069
1
12/15/20 14:51
12/17/20 19:39
72-54-8
4,4'-DDE
ND
ug/L
0.050
0.0064
1
12/15/20 14:51
12/17/20 19:39
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
12/1512014:51
12/1712019:39
50-29-3
Dieldrin
ND
ug/L
0.050
0.0073
1
12/1512014:51
12/1712019:39
60-57-1
Endosulfan I
ND
ug/L
0.050
0.0094
1
12/15/20. 14:51
12/17/20 19:39
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
12/15/20 14:51
12/17/20 19:39
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/15/20 14:51
12/17/20 19:39
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12/15/20 14:51
12/17/20 19:39
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/15/20 14:51
12/17/20 19:39
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/15/20 14:51
12/17/20 19:39
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
12115/2014:51
12/17/20 19:39
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.22
1
12/15/20 14:51
12/17/20 19:39
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.32
1
12/15/20 14:51
12/17/20 19:39
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.21
1
12/15/20 14:51
12/17/20 19:39
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
0.44
1
12/15/20 14:51
12/17/20 19:39
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/15/20 14:51
12/17/20 19:39
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
12/15/20 14:51
12/17/20 19:39
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
0.30
1
12/15/20 14:51
12/17/20 19:39
11096-82-5
PCB, Total
ND
ug/L
0.50
0.50
1
12/15/20 14:51
12/17/20 19:39.
1336-36-3
Toxaphene
ND
ug/L
0.50
0.19
1
12/1512014:51
12/17/20 19:39
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
139
%
10-154
1
12/15/20 14:51
12/17/20 19:39
877-09-8
Decachlorobiphenyl (S)
172
%
10-184
1
12/15/20 14:51
12/17/20 19:39
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Antimony
3.2.1
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:27
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:27
7440-38-2
Beryllium
ND
ug/L
1.0
0.70
1
12117/2002:09
12/20/2015:27
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
12/17/20 02:09
12/20/2015:27
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12117/2002:09
12/20/2015:27
7440-47-3
Copper
ND
ug/L
5.0
4.3
1
12/17/20 02:09
12/20/2015:27
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12117/2002:09
12120/2015:27
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/17/20 02:09
12/20/20 15:27
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
1211712002:09
12120/2015:27
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:27
7440-22-4
Thallium
ND
ug/L
10.0
8.1
1
1211712002:09
12120/2015:27
7440-28-0
[74Zm]A11[el2U\-Ie]:LNl[SI Z1I/_1W&I[_?
M1
M1
M1
M1
M1
M1
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 41

aceAnaiXical
www.beaelabs.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resisto0ex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected:. 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical
Method: EPA625.1 Preparation
Method: EPA625.1
Pace Analytical Services - Charlotte
Isophorone
NO
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:16
78-59-1
Naphthalene
NO
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:16
91-20-3
Nitrobenzene
NO
ug/L
5.0
1.9
1
12/15/20. 17:36
12/17/20 04:16
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1.4
1.
12/15/20 17:36
12/17/20 04:16
88-75-5
4-Nitrophenol
NO
ug/L
10.0
6.6
1
12/15/20 17:36
12117/2004:16
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1.9
1
12115/2017:36
12/17/20 04:16
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1.3
1
12/15/20 17:36
12/17/20 04:16
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
3.0
1
12/15/20 17:36
1211712004:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1.2
1
1211512017:36
12/17/20 04:16
108-60-1
Pentachlorophenol
NO
ug/L
10.0
3.8
1
12/15/20 17:36
12/17/20 04:16
87-86-5
Phenanthrene
NO
ug/L
5.0
2.0
1
12/15/20 17:36
1211712004:16
85-01-8
Phenol
NO
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
108-95-2
Pyrene
NO
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
129-00-0
1,2,4-Trichoorobenzene
NO
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:16
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1.6
1
12115/2017:36
12/17/20 04:16
88-06-2
Surrogates
Nitrobenzene-d5.(S)
76
%
10-120
1
12115/2017:36
12117/2004:16
4165-60-0
2-Fluorobiphenyl(S)
47
%
95-120
1
12/15/20 17:36
12/17/20 04:16
321-60-8
Terphenyl-d14(S)
105
%
11-131
1
12115/2017:36
12/17/20 04:16
1718-51-0
Phenol-d6 (S)
40
%
10-120
1
12/15/20 17:36
12/17/20 04:16
13127-88-3.
2-Fluorophenol (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:16
367-12-4
2,4,6-Tribromophenol (S)
97
%
10-137
1
12/15/20 17:36
12/17/20 04:16
118-79-6
624 Volatile Organics Acrolein
Analytical Method: EPA
624.1
Pace Analytical Services - Charlotte
Acrolein
NO
ug/L
5.0
3.8
1
12/1512019:01
107-02-8
Benzene
NO
ug/L
1.0
0.38
1
12/15/20 19:01
71-43-2
Bromodichloromethane
NO
ug/L
2.0
0.24
1
12/15/20 19:01
75-27-4
Bromoform
NO
ug/L
2.0
0.40
1
12115/2019:01
75-25-2
Bromomethane
ND
ug/L
2.0
1.2
1
12/15/20 19:01
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
0.29
1
12/15/20 19:01
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12/15/20 19:01
108-90-7
Chloroethane
ND
ug/L
2.0
1.4
1
12115/2019:01
75-00-3
Chloroform
NO
ug/L
2.0
0.58
1
12/15/20 19:01
67-66-3
Chloromethane
NO
ug/L
2.0
0.73
1
12/15/20 19:01
74-87-3
Dibromochloromethane
NO
ug/L
2.0
0.32
1
12/15/20 19:01
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
0.24
1
12/15/20 19:01
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
0.31
1
12/15/20 19:01
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
0.41
1
12/15/20 19:01
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
0.51
1
12/15/20 19:01
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
0.34
1
12/15/20 19:01
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
0.41
1
12/15/20 19:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12115/2019:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12115/2019:01
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
0.27
1
12/15/20 19:01
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, U.C. Page 10 of 41

aceAnalj6d
a%ra.pacelabe.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected:.12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MOIL OF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE
Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Pace Analytical Services - Charlotte
Aldrin
NO
ug/L
0.050
0.022
1
12/15/20 14:51
12/17/20 20:37
309-00-2
alpha-BHC
NO
ug/L
0.050
0.019
1
12115/2014:51
12/17/20 20:37
319-84-6
beta-BHC
NO
ug/L
0.050
0.014
1
12/15/2014:61
12117/2020:37
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
12115/2014:51
12/17/20 20:37
319-86-8
gamma-BHC(Lindane)
ND
ug/L
0.050
0.012
1
12115/2014:51
12/1712020:37
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.14
1
1211512014:51
12/17/20 20:37
57-74-9
alpha -Chlordane
ND
ug/L
0.050
0.0090
1
1211512014:51
12/17/20 20:37
5103-71-9
gamma -Chlordane
NO
ug/L
0.050
0.017
1
12/15/20 14:51
12/17/20 20:37
5103-74-2
4,4'-DDD
NO
ug/L
0.050
0.0069
1
12/15/20 14:51
12117/2020:37
72-54-8
4,4'-DDE
NO
ug/L
0.050
0.0064
1
12/1512014:51
12/17/20 20:37
72-55-9
4,4'-DDT
NO
ug/L
0.050
0.018
1
12/1512014:51
12117/2020:37
50-29-3
Dieldrin
NO
ug/L
0.050
0.0073
1
12115/2014:51
1211712020:37
60-57-1
Endosulfan I
NO
ug/L
0.050
0.0094
1
12115/2014:51
12117/20.20:37
959-98-8
Endosulfan 11
ND
ug/L
0.050
0.0065
1
12115/2014:61
12/1712020:37
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
12/15/20 14:51
12/17/20 20:37
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
12115/2014:51
1211712020:37
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
12/1512014:51
12/17/20 20:37
7421-93-4
Heptachlor
ND
ug/L
0.050
0.016
1
12/15/20 14:51
12/17/20 20:37
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
0.0097
1
12/15/20 14:51
12/17/20 20:37
1024-57-3
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
0.22
1
12/15/20 14:51
12/17/20 20:37
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.32
1
12/15/20 14:51
12/17/20 20:37
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
0.21
1
12/15/20 14:51
12/17/20 20:37
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
0.44
1
12/15/20 14:51
12/17/20 20:37
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.34
1
12/15/20 14:51.
12/17/20 20:37
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
0.24
1
12/15/20 14:51
12/17/20 20:37
11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug/L
0.50
0.30
1
12/15/20 14:51
12/17/20 20:37
11096-82-5
PCB, Total
ND
ug/L
0.50
0.50
1
12/15/20 14:51
12/17/20 20:37
1336-36-3
Toxaphene
NO
ug/L
0.50
0.19
1
1211512014:51
12/17/20 20:37
8001-35-2
Surrogates
Tetrachloro-m-xylene(S)
209
%
10-154
1
12/1512014:51
12/1712020:37
877-09-8 S3
Decachlorobiphenyl(S)
263
%
10-184
1
12/1512014:51
12/17/20 20:37
2051-24-3 S3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Antimony
NO
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:30
7440-36-0
Arsenic
NO
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:30
7440-38-2
Beryllium
ND
ug/L
1.0
0.70
1
12117/2002:09
12/20/20 15:30
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
1211712002:09
12120/2015:30
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
12117/2002:09
1212012015:30
7440-47-3
Copper
ND
ug/L
5.0
4.3
1
12/17/20 02:09
12/20/20 15:30
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
12/17/20 02:09
12/20/20 15:30
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
12/17/20 02:09
12/20/20 15:30
7440-02-0
Selenium
NO
ug/L
10.0
4.7
1
12/17/20 02:09
12/2012015:30
7782-49-2
Silver
NO
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:30
7440-22-4
Thallium
NO
ug/L
10.0
8.1
1
12/17/20 02:09
12/20/20 15:30
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 41

Pace Analytical Services, LLC
2225 Dr.
aceAnalytical o Asheville, NC Rivers1de 28804
mra.paeelaba.eale
[phone]
ANALYTICAL RESULTS
Project: Crane Resisto0ex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical
Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services- Charlotte
Isophorone
NO
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:45
78-59-1
Naphthalene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1.4
1
12115/2017:36
12117/2004:45
88-75-5
4-Nitrophenol
ND
ug/L
10.0
6.6
1
1211512017:36
12/17/20 04:45
100-02-7
N-Nitrosodimethylamine.
ND
ug/L
5.0
1.9
1
1211512017:36
12/1712004:45
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1.3
1
12/15/20 17:36
12/17/20 04:45
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
3.0
1
12/15/20 17:36
12/17/20 04:45
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1.2
1
12/1512017:36
12/17/20 04:45
108-60-1
Pentachlorophenol
NO
ug/L
10.0
3.8
1
12/15/20 17:36
12/17/20 04:45
87-86-5
Phenanthrene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
85-01-8
Phenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
108-95-2
Pyrene
ND
ug/L
5.0
2.2
1
12/1512017:36
12117/2004:45
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:45
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:45
88-06-2
Surrogates
Nitrobenzene-d5 (S)
86
%
10-120
1
12/15/20 17:36
12/17/20 04:45
4165-60-0
2-Fluorobiphenyl (S)
52
%
15-120
1
12/15/20 17:36
12/17/20 04:45
321-60-8
Terphenyl-d14(S)
121
%
11-131
1
12/15/20 17:36
12/17/20 04:45
1718-51-0
Phenol-d6 (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:45
13127-88-3
2-Fluorophenol(S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:45
367-12-4
2,4,6-Tribromophenol (S)
90
%
10-137
1
12/15/20 17:36
12/17/20 04:45
118-79-6
624 Volatile Organics Acrolein
Analytical
Method: EPA
624.1
Pace Analytical Services - Charlotte
Acrolein
NO
ug/L
5.0
3.8
1
12/15/20 19:19
107-02-8
Benzene -
ND
ug/L
1.0
0.38
1
12/15/20 19:19
71-43-2
Bromodichloromethane
NO
ug/L
2.0
0.24
1
12115/2019:19
75-27-4
Bromoform
ND
ug/L
2.0
0.40
1
12/15/20 19:19
75-25-2
Bromomethane
ND
ug/L
2.0
1.2
1
12115/2019:19
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
0.29
1
12/15/20 19:19
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12/15/20 19:19
108-90-7
Chloroethane
NO
ug/L
2.0
1.4
1
12/15/20 19:19
75-00-3
Chloroform
NO
ug/L
2.0
0.58
1
12/15/20 19:19
67-66-3
Chloromethane
ND
ug/L
2.0
0.73
1
12/15/20 19:19
74-87-3
Dibromochloromethane
ND
ug/L
2.0
0.32
1
12115/2019:19
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
0.24
1
12/15/20 19:19
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
0.31
1
12/15/20 19:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
0.41
1
12/15/20 19:19
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
0.51
1
12/15/20 19:19
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
0.34
1
12/15/20 19:19
107-06-2 M1
1,1-Dichloroethene
ND
ug/L
2.0
0.41
1
12/15/20 19:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/15/20 19:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/1512019:19
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
0.27
1
12/1512019:19
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, -LC. Page 14 of 41

aceAnalj6cal
www.pacelehs.coln
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistoflex
Pace Project No.:
92511637
QC Batch:
588138
Analysis Method: EPA 1664B
QC Batch Method:
EPA 1664E
Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537001, 92511537002
METHOD BLANK: 3107878 Matrix: Water
Associated Lab Samples: 92511537001, 92511537002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L NO 5.0 5.0 12/18/20 11:08
LABORATORY CONTROL SAMPLE: 3107879
Spike LCS LCS %Rec
Parameter Units Cone. Result % Rae Limits Qualifiers
Total Petroleum Hydrocarbons mg/L - 20 15.6 78 64-132
MATRIX SPIKE SAMPLE: 3107880
35598602001 Spike MS MS % Rae
Parameter Units. Result Cone. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 5.01-1 20 11.7 54 64-132 M1
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C.
Page 16 of 41

aceAnalXical
www.patelehs.ca n
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
.
QC Batch: 587665
Analysis Method:
EPA
200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4
1994
Analysis Description:
200.7 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92511537001, 92511537002, 92511537003, 92511537004
METHOD BLANK: 3105714
Matrix:
Water
Associated Lab Samples: 92511537001, 92511537002, 92511537003, 92511537004
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Antimony
ug/L
NO
5.0
3.0
12/2012015:11
Arsenic
ug/L
NO
10.0
4.7
12120/2015:11
Beryllium
ug/L
NO
1.0
0.70
12/20/20 15:11
Cadmium
ug/L
NO
1.0
0.40
12120/2015:11
Chromium
ug/L
NO
5.0
3.7
12/20/20 15:11
Copper
ug/L
ND
5.0
4.3
12/20/20 15:11
Hardness, Total(SM 2340B)
ug/L
ND
662
131
12/20/20 15:11
Lead
ug/L
ND
5.0
4.5
12120/2015:11
Nickel
ug/L
ND
5.0
3.5
12/20/20 15:11
Selenium
ug/L
ND
10.0
4.7
12120/2015:11
Silver
ug/L
ND
5.0
2.5
12120/2015:11
Thallium
ug/L
ND
10.0
8.1.
12/2012015:11
Zinc
ug/L
NO
10.0
9.5
12/20/20 15:11
LABORATORY CONTROL SAMPLE:
3105715
Spike
LIDS
LCS
%
Rae
Parameter
Units
Cone.
Result
%Rec
Limits Qualifiers
Antimony
ug/L
500
483
97
85-115
Arsenic
ug/L
500
482
96
85-115
Beryllium
ug/L
500
489
98
85-115
Cadmium
ug/L
500
498
100
85-115
Chromium
ug/L
500
499
100.
85-115
Copper
ug/L
500
496
99
85-115
Hardness, Total(SM 2340B)
ug/L
33100
32500
98
85-115
Lead
ug/L
500
490
98
85-115
Nickel
ug/L
500
497
99
85-115
Selenium
ug/L
500
484
97
85-115
Silver
ug/L
250
246
98
85-115
Thallium
ug/L
500
497
99
85-115
Zinc
ug/L
500
498
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105716
3105717
MS
MSD
92511027001 - Spike
Spike
MS
MSD
MS MSD %Rec
Max
Parameter Units Result Cone.
Cone.
Result
Result
%Rec %Rec Limits RPD
RPD Qual
Antimony ug/L 15.6 500
500
511
507
99 98 70-130 1
20
Arsenic ug/L ND 500
500
489
484
98 97 70-130 1
20
Results presented an this page are In the units Indicated by the "Units" column except More an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 41

aceAnalXical o
www.pazelabstors
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistoflex
Pace Project No.:
92511537
QC Batch:
590708
Analysis Method: EPA 200.7 Rev 4.41994
QC Batch Method:
EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118555
Associated Lab Samples: 92511537002.
Parameter Units
Zinc ug/L
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed Qualifiers
NO 10.0. 9.5 01105/21 18:12
LABORATORY CONTROL SAMPLE: 3118556
Spike LIDS LCS % Rae
Parameter Units Cone. Result % Rae Limits Qualifiers
Zinc ug/L 500 476 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118557 3118558
MS MSD
92511537002 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD RPD Qual
Zinc ug/L 68.1 500 500. 567 580 100 102 70-130 2 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 20 of 41

(aceAnail
ts'tew.pacelebsxcn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistofiex
Pace Project No.: 92511537
QC Batch: 590706 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118545 Matrix: Water
Associated Lab Samples: 92511537002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Zinc, Dissolved ug/L NO 10.0 2.5 01/05/21 17:11
LABORATORY CONTROL SAMPLE: 3118546
Spike
LCS
LCS
%Rec
Parameter
Units
Conic.
Result
% Rec
Limits Qualifiers
Zinc, Dissolved
ug/L
500
472
94
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118547
3118548
MS
MSD
92511537002
Spike
Spike MS
MSD
MS MSD %Rec Max
Parameter
Units Result
Conic.
Conic. Result
Result
% Rec % Rec Limits RPD RPD Qua[
Zinc, Dissolved
ug/L 68.0
500
500 543
535
95 93 70-130 1 20
Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 22 of 41

(�ImAna(Xicalo
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
3102523
Spike LCS
LCS
% Rae
Parameter
Units
Cone. Result
%Rec
Limits
Qualifiers
1,1,1-Trichloroethane
ug/L
20
16.2
81
70-130
1, 1,2,2-Tetrachloroethane
ug/L
20
21.9
110
70-130
1,1,2-Trichloroethane
ug/L
20
17.8
89
70-130
1,1-Dichloroethane
ug/L
20
16.3
81
70-130
1,1-Dichloroethene
ug/L
20
16.0
80
70-132
1,2-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,2-Dichloroethane
ug/L
20
15.1
76
70-130
1,2-Dichloropropane
ug/L
20
18.4
92
70-130
1,3-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,4-Dichlorobenzene.
ug/L
20
23.7
118
70-130
Acrolein
ug/L
100
106
106
60-140
Benzene
ug/L
20
18.1
91
70-130.
Bromodichloromethane
ug/L
20
16.9
85
70-130
Bromoform
ug/L
20
18.7
94
70-130
Bromomethane
ug/L
20
18.1
91
30-177
Carbon tetrachloride
ug/L
20
17.9
89
70-130
Chlorobenzene
ug/L
20
21.8
109
70-130
Chloroethane
ug/L
20
15.8.
79
46-131
Chloroform
ug/L
20
15.5
78
70-130
Chloromethane
ug/L
20
14.8
74
49-130
cis-1,2-Dichloroethene
ug/L
20
15.3
77
70-130
cis-1,3-Dichloropropene
ug/L
20
18.6
93
70-130
Dibromochloromethane
ug/L
20
21.7
109
70-130
Ethylbenzene
ug/L
20
21.5
108
70-130
Methylene Chloride
ug/L
20
14.1
71
68-130
Tetrachloroethene
ug/L
20
22.1
110
70-130
Toluene
ug/L
20
18.1
90
70-130
trans-1,2-Dichloroethene
ug/L
20
16.3
82
70-130
trans-1,3-Dichloropropene
ug/L
20
18.0
90
70-130
Trichloroethene
ug/L
20
18.8
94
70-130
Trichlorofluoromethane
ug/L
20
16.7
84
61-130
Vinyl chloride
ug/L
20
15.4
77
59-142
1,2-Dichloroethane-d4(S)
%
87
70-130
4-Bromofluorobenzene (S)
e/
97
70-130
Toluene-d8(S)
%
94
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102524
3102525
MS MSD
92511537004
Spike Spike
MS
MSD
MS MSD
%Rec Max
Parameter
Units
Result
Cone. Cone.
Result
Result
% Rae % Rae
Limits RPD RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20 20
15.9
18.1
80 90
70-148 13 21
1,1,2,2-Tetrachloroethane
ug/L
ND
20 20
20.1
21.4
100 107
70-131 7 30
1,1,2-Trichloroethane
ug/L
NO
20 20
16.9
18.2
85 91
70-136 7 27
1,1-Dichloroethane
ug/L
NO
20 20
15.5
17.8
77 89
71-143 14 30
1,1-Dichloroethene
ug/L
NO
20 20
14.8
17.6
74 88
70-158 17 30
Results presented on this page are In site units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 41

(�Ia'ceAnalj4icale
wa i.pacelabs.con
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistofiex
Pace Project No.:
92511537
QC Batch:
587108
Analysis Method: EPA608.3
QC Batch Method:
EPA608.3
Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3103046
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
4,4'-DDD
ug/L
NO
0.050
0.0069
12/17/20 22:19
4,4'-DDE
ug/L
NO
0.050
0.0064
12/17/20 22:19
4,4'-DDT
ug/L
ND.
0.050
0.018
12117/2022:19
Aldrin
ug/L
NO
0.050
0.022
12/17/20 22:19
alpha-BHC
ug/L
NO
0.050
0.019
12/17/20 22:19
alpha -Chlordane
ug/L
NO
0.050
0.0090
12117/2022:19
beta-BHC
ug/L
NO
0.050
0.014
12/17/20 22:19
Chlordane (Technical)
ug/L
NO
0.50
0.14
12117/2022:19
delta-BHC
ug/L
NO
0.050
0.020
1211712022:19
Dieldrin
ug/L
NO
0.050
0.0073
12/1712022:19
Endosulfanl
ug/L
NO
0.050
0.0094
12/17/20 22:19
Endosulfan II
ug/L
NO
0.050
0.0065
12/17/20 22:19
Endosulfan sulfate
ug/L
ND
0.050
0.0091
12/1712022:19
Endrin
ug/L
ND
0.050
0.0089
12/17/20 22:19
Endrin aldehyde
ug/L
ND
0.050
0.013
12117/2022:19
gamma-BHC(Lindane)
ug/L
NO
0.050
0.012
12117/2022:19
gamma -Chlordane
ug/L
ND
0.050
0.017
12/17/20 22:19
Heptachlor
ug/L
NO
0.050
0.016
12/17/20 22:19
Heptachlor epoxide
ug/L
NO
0.050
0.0097
12/17/20 22:19
PCB-1016 (Aroclor 1016)
ug/L
NO
0.50
0.22
12/17/20 22:19
PCB-1221(Aroclor 1221)
ug/L
NO
0.50
0.32
12117/2022:19
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
0.21
12/17/20 22:19
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
0.44
12/17/20 22:19
PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
0.34
12/1712022:19
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
0.24
12/17/20 22:19
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
0.30
12/17/20 22:19
Toxaphene
ug/L
ND
0.50
0.19
12/1712022:19
Decachlorobiphenyl(S)
%
231
10-184
12/17/2022:19 S3
Tetrachloro-m-xylene(S)
%
133
10-154
12117/2022:19
LABORATORY CONTROL SAMPLE:
3103047
Spike LCS LCS
% Rec
Parameter
.Units
Conc. Result %Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 4.4 89
50-137
PCB-1260 (Aroclor 1260)
ug/L
5 4.5 89
42-140
Decachlorobiphenyl (S)
%
209
10-184 SO
Tetrachloro-m-xylene(S)
%
117
10-154
Results presented on this page are In Me units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 41

aceAnalj&cal e
t .pecelblxrzom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103080
3103081
MS
MSD
92511537003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qua]
Endosulfan II
ug/L
ND
0.25
0.25
0.39
0.38
155
151
27-176
3
53
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.39
0.38
157
154
31-144
2
38 M1
Endrin
ug/L
ND
0.25
0.25
0.37
0.36
147
143
30-147
3
48
Endrin aldehyde
ug/L
ND
0.25
0.25
0.32
0.33
127
130
16-177
3
30
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.33
0.34
130
137
32-140
5
39
gamma -Chlordane
ug/L
ND
0.25
0.25
0.40
0.39
161
155
45-140
4
35 M1
Heptachlor
ug/L
ND
0.25
0.25
0.26
0.31
102
122
34-140
17
43
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.32
0.30
130
121
37-142
7
26
Decachlorobiphenyl(S)
%
232
289
10-184
SO
Tetrachloro-m-xylene (S)
%
127
222
10-154
SO
Results presentee on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, L-C. Page 28 of 41

aceAnalj6cal
www.peceiabs.com
QUALITY CONTROL DATA
Project: Crane Resistoflez
Pace Project No.: 92511537
METHOD BLANK: 3103116
Matrix:
Water
Associated Lab Samples: 92511537003, 92511537004
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Hexachloroethane
ug/L
ND
5.0
1.4
12/16/2010:45
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
2.9
12/16/20 10:45
Isophorone
ug/L
ND
10.0
1.7
12/16/2010:45
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
1.3
12/16/2010:45
N-Nitrosodimethylamine
ug/L
NO
5.0
1.9
12/16/2010:45
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
1211612010:45
Naphthalene
ug/L
NO
5.0
2.1
12116/2010:45
Nitrobenzene
ug/L
ND
5.0
1.9
12116/2010:45
Pentachlorophenol
ug/L
NO
10.0
3.8
12116/2010:45
Phenanthrene
ug/L
NO
5.0
2.0
12/16/2010:45
Phenol
ug/L
NO
5.0
1.4
12/16/2010:45
Pyrene
ug/L
NO
5.0
2.2
1211612010:45
2,4,6-Tribromophenol (S)
%
107
10-137
12/16/20 10:45
2-Fluorobiphenyl (S)
%
74.
15-120
12/16/20 10:45
2-Fluorophenol(S)
%
63
10-120
12/16/2010:45
Nitrobenzene-d5 (S)
%
109
10-120
12/16/2010:45
Phenol-d6 (S)
%
56
10-120
12/16/20 10:45
Terphenyl-d14 (S)
%
125
11-131
12/16/20 10:45
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3103117
Units
Spike
Conc.
LCS
Result
LCS
% Rao
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
24.9
50
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
35.9
72
36-166
2,4,6-Trichlorophenol
ug/L
50
44.6
89
37-144
2,4-Dichlorophenol
ug/L
50
41.0
82
1-191
2,4-Dimethylphenol
ug/L
50
41.3
83
32-119
2,4-Dinitrophenol
ug/L
250
282
113
1-181
2,4-Dinitrotoluene
ug/L
50
38.3
77
39-139
2,6-Dinitrotoluene
ug/L
50
46.5
93
50-158
2-Chloronaphthalene
ug/L
50
34.4
69
60-118
2-Chlorophenol
ug/L
50
38.8
78
23-134
2-Nitrophenol
ug/L
50
45.0
90
29-182
3,3'-Dichlorobenzidine
ug/L
100
88.5
89
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
143
143
1-181
4-Bromophenylphenyl ether
ug/L
50
42.5
85
53-127
4-Chloro-3-methylphenol
ug/L
100
94.3
94
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.2
76
25-158
4-Nitrophenol
ug/L
250
202
81
1-132
Acenaphthene
ug/L
50
36.6
73
47-145
Acenaphthylene
ug/L
50
36.8
74
33-145
Anthracene
ug/L
50
36.5
73
1-166
Benzo(a)anthraoene
ug/L
50
41.2
82
33-143
Benzo(a)pyrene
ug/L
50
41.4
83
17-163
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 41

aceAnalj6cal e
www.pacelaba.cam
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118
3103119
MS
MSD
92511577001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rao
Limits
RPD
RPD Qual
2,4-Dichlorophenol
ug/L
NO
50
50
48.7
42.5
97
85
1-191
14
30
2,4-Dimethylphenol
ug/L
NO
50
50
47.7
38.2
95
76
32-119
22
30
2,4-Dinitrophenol
ug/L
NO
250
250
77.6
NO
31
7
1-181
30
2,4-Dinitrotoluene
ug/L
NO
50
50
44.1
39.1
88
78
39-139
12
30
2,6-Dinitrotoluene
ug/L
NO
50
50
59.9
56.1
120
112
50-158
7
30
2-Chloronaphthalene
ug/L
NO
50
50
33.3
30.2
67
60
60-118
10
30.
2-Chlorophenol
ug/L
NO
50
50
46.0
40.7
92
81
23-134
12
30
2-Nitrophenol
ug/L
NO
50
50
54.1
48.5
108
97
29-182
11
30.
3,3'-Dichlorobenzidine
ug/L
NO
100
100
108.
108
108
108
1-262
0
30
4,6-Dinitro-2-methylphenol
ug/L
NO
100
100
141
38.3
141
38
1-181
115
30 R1
4-Bromophenylphenyl ether
ug/L
NO
50
50
47.0
43.9
94
88
53-127
7
30
4-Chloro-3-methylphenol
ug/L
NO
100
100
113
105
113
105
22-147
7
30
4-Chlorophenylphenyl ether
ug/L
NO
50
50
40.2
36.5
80
73
25-158
10
30
4-Nitrophenol
ug/L
NO
250
250
146
35.8
58
14
1-132
121
30 R1
Acenaphthene
ug/L
NO
50
50
39.5
34.7
79
69
47-145
13
30.
Acenaphthylene
ug/L
NO
50
5o
41.0
- 36.7
82
73
33-145.
11
30
Anthracene
ug/L
NO
50
50
44.0
41.5
88
83
1-166
6
30
Benzo(a)anthracene
ug/L
NO
50
50
52.0
51.3
104
103
33-143
2
30
Benzo(a)pyrene
ug/L
NO
50
50
53.5
52.2
107
104
17-163
3
30
Benzo(b)fluoranthene
ug/L
NO
50
50
52.2
51.7
104
103
24-159
1
30
Benzo(g,hJ)perylene
ug/L
NO
50
50
55.2
55.3
110
Ill
1-219
0
30
Benzo(k)fluoranthene
ug/L
NO
50
50
53.1
52.5
106
105
11-162
1
30
bis(2-
ug/L
NO
50
50
48.5
46.6
97
93
33-184
4
30
Ch loroethoxy)methane
bis(2-Chlorcethyl) ether
ug/L
NO
50
50
48.3
44.8
97
90.
12-158
8
30
bis(2-Ethylhexyl)phthalate
ug/L
NO
50
50
59.6
59.6
119
119
8-158
0
30
Butylbenzylphthalate
ug/L
NO
50
50
62.0
60.8
124
122
1-152
2
30
Chrysene
ug/L
NO
50
50
51.2
50.3
102
101
17-168
2
30
Di-n-butylphthalale
ug/L
NO
50
50
56.3
54.8
113
110
1-118
3
30
Di-n-oclylphthalate
ug/L
NO
50
50
65.4
64.9
131
130
4-146
1
30
Dibenz(a,h)anthracene
ug/L
NO
50
50
56.9
57.1
114
114
1-227
0
30
Diethylphthalate
ug/L
NO
50
50
52.5
50.1
105
100
1-114
5
30
Dimethylphthalate
ug/L
NO
50
50
50.0
46.5
100
93
1-112
7
30
Fluoranthene
ug/L
NO
50
50
53.3
51.2
107
102
26-137
4
30
Fluorene
ug/L
NO
50
50
44.1
39.6
88
79
59-121
11
30
Hexachloro-1,3-butadiene
ug/L
NO
50
50
4.9J
4.OJ
10
8
24-116
30 Mt
Hexachlorobenzene
ug/L
NO
50
50
43.8
41.1
88
82
1-152
6
30
Hezachlorocyclopentadiene
ug/L
NO
50
50
8.61
7.1J
17
14
25-150
30 M1
Hexachloroethane
ug/L
ND
50
50
6.9
5.4
14
11
40-113
24
30 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
57.4
56.9
115
114
1-171
1
30
Isophorone
ug/L
ND
50
50
43.2
40.9
86
82
21-196
5
30
N-Nitroso-di-n-propylamIna
ug/L
ND
50
50
44.4
42.6
89
85
1-230
4
30
N-Nitrosodimethylamine
ug/L
NO
50
50
48.1
46.1
96
92
25-150
4
30
N-Nitrosodiphenylamine
ug/L
NO
50
50
50.5
46.9
101
94
25-150
7
30
Naphthalene
ug/L
NO
50
50
31.3
28.4
63
57
21-133
10
30
Nitrobenzene
ug/L
NO
50
50
46.3
43.8
93
88
35-180
6
30
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to Me right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, U.C. Page 32 of 41

ZeAnalytical'
www.pscelahs.cra
Project: Crane Resistofiex
Pace Project No.: 92511537
QC Batch: 587549
QC Batch Method: SM 254OD-2011
Associated Lab Samples: 92511537001. 92511537002
QUALITY CONTROL DATA
Analysis Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3105210 Matrix: Water
Associated Lab Samples: 92511537001, 92511537002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 2.5 12/16/20 22:28
LABORATORY CONTROL SAMPLE: 3105211
Parameter. Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 3105691
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 3105692
Parameter
Units
Total Suspended Solids
mg/L
Spike LCS LCS %Rec
Conic. Result % Rec Limits Qualifiers
250 254 102 90-110
92511268001 Cup Max
Result Result RPD RPD Qualifiers
348 388 11 25
92511502001 Dup Max
Result Result RPD RPD Qualifiers
659 595 10 25
Results presented on this page are In the units Indicated by Me "linlb" column except where an alternate unit Is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/111202112:50 PM without the written consent of Pace Analytical Services,LLC.
Page 34 of 41

ZeAnalj6calo
www.paceleblixom
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Crane Resistoflex
Pace Project No.:
92511537
QC Batch:
586885
Analysis Method:
SM 4500-CN-E-2011
QC Batch Method:
SM 4500-CN-E-2011
Analysis Description:
450OCNE Cyanide, Total
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3102109 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit MOIL Analyzed Qualifiers
Cyanide mg/L NO 0.0080 0.0060 12/15/20 23:30
LABORATORY CONTROL SAMPLE: 3102110
Spike LCS LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide mg/L 0.1 0.10 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102144
3102145
MS
MSD
92511537003 Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter Units Result Conic.
Conic.
Result
Result
%Rec
%Rec
Limits
RPD RPD Qual
Cyanide mg/L ND 0.1
0.1
0.020
0.064
19
64
80-120
105 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102146
3102147
MS
MSD
92511537004 Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter Units Result Conc.
Conc.
Result
.Result
%Rec
%Rec
Limits
RPD RPD Qual
Cyanide mg/L NO 0.1
0.1
0.091
0.084
91
84
80-120
7 10
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 41

aceAnaiXical e
w .paceiabs.cora
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Crane Resistoflex
92511537
Analytical
Lab ID
Sample
ID
QC Batch Method
QC Batch
Analytical Method
Batch
92511537001
OF-001
EPA 1664B
588138
92511537002
OF-002
EPA 1664B
588138
92511537003
OF-001
TTO
EPA 608.3
587108
EPA 608.3
587726
92511537004
OF-002
TTO
EPA 608.3
587108
EPA 608.3
587726
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537002
OF•002
EPA 200.7 Rev 4.4 1994
590708
EPA 200.7 Rev 4.4 1994
590740
92511537003
OF-001
TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537004
OF-002
TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7 Rev 4.4 1994
587689
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
586977
EPA 200.7 Rev 4.4 1994
587006
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
590706
EPA 200.7 Rev 4.4 1994
590776
92511537003
OF-001
TTO
EPA 245.1 Rev 3.0 1994
587409
EPA 245.1 Rev 3.0 1994
587457
92511537004
OF-002
TTO
EPA 245.1 Rev 3.0 1994
587409
EPA 245.1 Rev 3.0 1994
587457
92511537003
OF-001
TTO
EPA625.1
587125
EPA 625.1
587394
92511537004
OF-002
TTO
EPA625.1
587125
EPA 625.1
587394
92511537003
OF-001
TTO
EPA 624.1
587031
92511537004
OF-002
TTO
EPA 624.1
587031
92511537001
OF-001
SM 254OD-2011
587549
92511537002
OF-002
SM 254OD-2011
587549
92511537003
OF-001
TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4 Rev 1.0 1993
587822
92511537004
OF-002
TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4 Rev 1.0 1993
587822
92511537003
OF-001
TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
92511537004
OF-002
TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 41

Document Name:
Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
.. r7CBAA8jyilCBj-
I
F•CAR-05,033-Rev.07
Pace Carolinas Quality Off ice
*Check mark top half of box if pH and/or dechlorlmotion is Project N W1 I®# ; 92511537 _
verified and within the acceptance range for preservation Due Date: 12/21/20
samples. pm: UP
Exceptions: VOA, California, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 83—ALTAMONT
**Bottom half of box is to list number of bottles
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pH Adjustment Log for Preserved Samples
Sample to
Type of Preservative
PH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Loth
adjusted
added
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 40 of 41